InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.SelecttheHAPsTestGroup(i.e.,HAPsurrogate)forwhichthetab'sdatareflects(orangehighlightedcell).7.ProvidetheSampleNumberandSampleDateontheFuelsSampleResultsworksheet.Youmustprovideaminimumof3compositesamplesconsistingof3combinedgrabsampleseach,butyouarenotlimitedtothatnumberifyouhavecollectedmore.8.Providetheresultsoftheanalysesforeachconstituentrequested.Usethedrop‐downboxestofillintheunitsofmeasure.

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 864 Meredosia 5

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV)

(as received) HHV Units 

# Fuel Testing Results

# % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the P

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Proximate Analyses, %

# roximate/Ultimate data below should be recorded on a dry basis (including ash).

Ash Fixed Carbo n Carbon Hydrogen Nitrogen Total Sulfur Oxygen % by w t Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 864 Meredosia 5

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher

Heating

Value (HHV)

(as

received) HHV Units 

# Fuel Testing Results

# % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the Proximate/U

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Proximate Analyses, % by wt

# ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbo n Carbon Hydrogen Nitrogen Total Sulfur Oxygen Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 864 Meredosia 5

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV)

(as received) HHV Units 

# Fuel Testing Results

# % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the Proximate/U

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Proximate Analyses, % by w

# ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen wt Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID



# 864 Meredosia 5

Sample Number

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value

(HHV)

(as received)



# Run 1 

# 03/30/2010 03/30/2010 8903

Run 2 03/31/2010 03/31/2010 9222

Run 5 04/01/2010 04/01/2010 9178

Run 6 04/01/2010 04/01/2010 9231

Run 7 04/01/2010 04/01/2010 9041 Fuel Testing Results

# HAPs Test Group



# Mercury and non

‐ mercury metalic HAPs

HHV Units % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis)



# Btu/lb 29.93 4.25 0.24 12705

Btu/lb 27.82 4.18 0.22 12777

Btu/lb 27.86 4.23 0.19 12723

Btu/lb 27.97 4.62 0.25 12815

Btu/lb 28.99 4.2 0.27 12732

# HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units



# Btu/lb 6.07 0.34 0.0034 % 0.050 μ g/g

Btu/lb 5.79 0.31 0.0017 % 0.037 μ g/g

Btu/lb 5.86 0.27 0.0015 % 0.036 μ g/g

Btu/lb 6.41 0.35 0.0024 % 0.050 μ g/g

Btu/lb 5.91 0.38 0.0024 % 0.038 μ g/g

# Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)



# 0.228 μ g/g 1.15 μ g/g 0.269 μ g/g 0.0538 μ g/g 4.70

0.113 μ g/g 1.54 μ g/g 0.222 μ g/g 0.0536 μ g/g 3.75

0.120 μ g/g 1.46 μ g/g 0.235 μ g/g 0.0478 μ g/g 3.68

0.138 μ g/g 2.31 μ g/g 0.270 μ g/g 0.0873 μ g/g 4.14

0.146 μ g/g 1.21 μ g/g 0.259 μ g/g 0.0756 μ g/g 4.36

# Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium

(Dry Basis) Selenium

Units



# μ g/g 2.91 μ g/g 10.58 μ g/g 4.13 μ g/g [<1] μ g/g

μ g/g 2.22 μ g/g 7.44 μ g/g 4.02 μ g/g [<1] μ g/g

μ g/g 2.20 μ g/g 5.43 μ g/g 3.21 μ g/g [<1] μ g/g

μ g/g 2.91 μ g/g 5.85 μ g/g 3.47 μ g/g [<1] μ g/g

μ g/g 2.65 μ g/g 9.26 μ g/g 4.46 μ g/g [<1] μ g/g

# Note the Proximate/Ultimate data belo w

Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon



# 1.69 μ g/g 29.93 49.94 6.07 43.99

1.68 μ g/g 27.82 51.88 5.79 42.33

1.46 μ g/g 27.86 51.18 5.86 42.96

1.61 μ g/g 27.97 50.26 6.41 43.33

1.82 μ g/g 28.99 50.01 5.91 44.08 Proximate Analyses, % by wt

# w should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen



# 69.87 5.53 2.48 0.34 15.71

70.34 5.53 2.48 0.31 15.55

70.75 5.78 2.46 0.27 14.88

69.96 5.75 2.45 0.35 15.08

70.26 5.35 2.38 0.38 15.72 Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID Fuel Type 1

864 Meredosia 5 

# subbituminous

# Fuel Type 2 Fuel Type 3 Other Fuel Description

# EIA Facility Code Facility Name Boiler ID Basis Analyte



# 864 Meredosia 5 As Received Higher Heating Value



# 864 Meredosia 5 As Received % Moisture



# 864 Meredosia 5 As Received % Ash



# 864 Meredosia 5 As Received % Sulfur



# 864 Meredosia 5 Dry basis Higher Heating Value



# 864 Meredosia 5 Dry basis % Ash



# 864 Meredosia 5 Dry basis % Sulfur



# 864 Meredosia 5 Dry basis Antimony



# 864 Meredosia 5 Dry basis Arsenic



# 864 Meredosia 5 Dry basis Beryllium



# 864 Meredosia 5 Dry basis Cadmium



# 864 Meredosia 5 Dry basis Chlorine



# 864 Meredosia 5 Dry basis Chromium



# 864 Meredosia 5 Dry basis Cobalt



# 864 Meredosia 5 Dry basis Fluorine



# 864 Meredosia 5 Dry basis Lead



# 864 Meredosia 5 Dry basis Manganese



# 864 Meredosia 5 Dry basis Mercury



# 864 Meredosia 5 Dry basis Nickel



# 864 Meredosia 5 Dry basis Selenium

# A na l ys i s M e th o d f or eac h A na l y t e

(example: ASTM D5865-04)



# ASTM D5865

ASTM D5142

ASTM D5142

ASTM D4239

ASTM D5865

ASTM D5142

ASTM D5142

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

ASTM D6722

ASTM D5987, ASTM D6357

ASTM D5987, ASTM D6357

# Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μ g/g

othe r mg/Kg

# re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm