GE Energy Bruce Randall

Project Manager

ISO 9001 Accredited

Quality System

PARTICULATE MAnER EMISSIONS COMPLIANCE STUDY

Performed At

Minnkota Power Cooperative

M.R. Young Station

Unit2

Center, North Dakota

Test Date

May 7,2008

Report No.

GE Energy Management Services, Inc. Report M22A0427B

Report Submittal Date

June 13, 2008

GE Energy Management Services, Inc

1301 Corporate Center Drive - Suite 177

Eagan, MN 55121 T 651-686-0700

USA F 651-686-4434
GE Energy

TABLE OFCONTENTS

CERTIFICATION SHEET i

1.0 INTRODUCTION 1

RV And discussion OF RESULTS : 1 . l'

1'~.'Sft3.0TEST URES 1 / .. t<,. I>:;; 3.1 Desc . n of Sampling Location :: 2

f,r,' ".,,,",,'i.? Filtera M Determination by USEPA Method 17 2

~~~;~~c1e Determination by Electrozone (Elzone) Technique 2

4.0 CR\?Atl~ ASS NCE PROCEDURES 3

. 'Yr,,';'" ,,~' .! . '&.O~@,..RESU~::,UMMARV 4 ."t..... >. if ~I'C.I'~

. :ARgE.t:H~I~,_~... . ····::ProJect Participants 6

Process Operating Data : 7

Sampling Train Diagram 13

Calculation Nomenclature and Formulas 14

Reference Method Test Data and Results 18

Laboratory Analytical Data 24

Calibration Data , 38

Field Data Sheets , , 46
GE Energy

CERTIFICATION SHEET

Having reviewed the test program described in this report, I hereby certify the data,

information and results in this report to be accurate and true according to the

methods and procedures used. .

Data collected under the supervision of others is included in this report, and is

presumed to have been gathered in accordance with recognized standards.

GE ENERGY MANAGEMENT SERVICES,INC.

Bruce Randall

Emissions Testing ServiceDirector

© 2008, General Electric Company. pJl rights reserved. The contents ofthis document are the property ofGeneral Electric

Company. No part ofthis work may be reproduced or transmitted in any form or by any means, except as permitted in written

license agreement with General Electric Company. General Electric Compony has made every reasonable attempt to ensure the

completeness and accuracy ofthis document The GE logo is a registered trademark ofGeneral Electric Company.

1
GE Energy

PARTICULATE EMISSIONS COMPLIANCE STUDY

Performed For .

Minnkota Power Cooperative

At The

M.R. Young Station

Unit2

Center, North Dakota

May 7,2008

1.0 INTRODUCTION

GE Energy Management Services, Inc., (uGE Energy"l performed a Particulate Matter

(PMl emission compliance test program on Unit 2 at the M.R. Young Station of

Minnkota Power Cooperative (Minnkotal near Center, North Dakota on May 7, 2008.

The tests were authorized by and performed for Minnkota.

The purpose of this test program was to determine emission rates of PM, and

Particulate Matter less than 10 microns in diameter (PMlOl during normal operating

conditions. These tests were performed concurrently with. a PM correlation test

program for the PM Continuous Emissions Monitoring System installed on Unit 2. The

results of the correlation test program are presented under separate cover.

2.0 SUMMARV AND DISCUSSION OF RESULTS

The results of the test program are summarized in the following table:

2 PM

. PMlO

O.009Ib/MMBtu

28.7Ib/hr

O.llb/MMBtu

315.1Ib/hr

. Complete test results summaries are presented in Section 5.0.

3.0 TEST PROCEDURES

All testing, sampling, analytical, and calibration procedures used for this test program

were performed as described in the Title 40, Code of Federal Regulations, Part 60

(40CFR60l, Appendix A, Method 17 and.the latest revisions thereof. Where applicable,

the Quality Assurance Handbook for Air Pollution Measurement Systems, Volume III,

GE Energy Project M22A04278 1
GE Energy

Stationary Source Specific Methods, United States Environmental Protection Agency

(USEPA!600/4-77-027b was used to determine the precise procedures.

3.1 Description of Sampling Location

The sample location at Unit 2 was a vertical circular stack equipped with multiple

sample ports. The ports used for this program were located 5.8 duct diameters

upstream, and 12.8 duct diameters downstream from the nearest disturbance in

flow. Sample point location was determined in accordance with USEPAMethod 1.

3.2 Filterable PM Determination by USEPA Method 17

This method is applicable for the determination of filterable (front-half or dry-catch!

PM emissions from stationary sources where PM concentrations are known to be

independent of temperature over the normal range of temperatures characteristic of

emissions from a specified source category. Sample was drawn from the source

through a buttonhook nozzle, an in-stack filter and a stainless steel-lined. The probe

was followed in series by: an impinger train immersed in an ice bath, a pump and a

dry test meter. Velocity pressures were determined during sampling with a calibrated

S-type pitot tube and inclined manometer. All temperatures were measured using Ktype thermocouples with calibrated digital temperature indicators.

The entire sample system was checked for leaks prior to sampling~ At the conclusion

of- samp1jng~thE-~tire~sampl-e:>ystem~0$--check-ed-f"Of-i~Gks-et--er-veetltlffl~~f€et"€r---~- .~_-~~~-_~

than or equal to the highest sample vacuum observed during the test run. All sample

contact surfaces of the upstream of the filter were rinsed and brushed with HPLC

reagent-grade acetone. These washes were placed in sealed and marked containers

for analysis. The filter was recovered to a Petri dish.

All sample recovery was performed at the test site. All final sample analyses were

performed by GE Energy personnel at the GE Energy laboratory in Eagan, Minnesota.

3.3 Particle Size Determination by Electrozone (Elzone) Technique

Upon completion of Method 17 analysis. samples were tested for particle size by the

Elzone technique. Particles suspended in a conductive fluid flow serially through an

.orifice under differential pressure. Electrodes are immersed on each side of the

orifice. As each particle passes through the aperture. it replaces its own volume of

electrolyte within the aperture. momentarily changing the resistance value between

the electrodes. This change produces a voltage pulse of short duration having a

magnitude proportional to particle volume. The resulting series of pulses is

electronically amplified, scaled, and counted. Raw data processing is performed by a

PDP-1103 minicomputer in such a manner that a population histogram of 128 or 256

channels of information can be acquired. Acquired data is conditioned by applying

calibration, extrapolation. volume (weight!. or area conversions. Normalization of size

and quantity axes to the types of scales required by the researcher is also possible.

GE Energy Project M22A0427B 2
GE Energy

. The conductive particle suspension medium is an important consideration in

Electrozone technology. Typically, aqueous isotonic saline (0.9% by weight) or a 4%

by weight sodium pyrophosphate is used as a dispersing and particle suspension

medium. For certain analyses that cannot be run in an· aqueous medium, 4%

weight/volume lithium chloride in isopropyl alcohol is effective.

4.0 QUALlTV ASSURANCE PROCEDURES

GE Energy recognizes the previously described test methods to be very technique

oriented and attempts to minimize all factors which can increase error by

implementing its Quality Assurance Program into every segment of its testing

activities.

GE Energy Project M22A0427B 3
GE Energy

5.0 TEST RESULTS SUMMARV

Company: Minnkota

Plant: MRYoung

Unit: Unit 2

est Run Number 1 2 3

ate . 5/07/2008 5/07/2008 5/07/2008

Start Time 08:20 09:06 10:13

End Time 09:38 10:27 11:33

otal Sample Time (Min): 60.0 60.0 60.0

verage Duct Temp (oF): 172.5 175.4 174.3

verage Duct Vel (ft/sec): 63.74 62.57 63.94

Moisture Content (Bws): 0.197/ 0.196 0.198

02 Content l%voll: 7.3 7.4 7.4

~._~.-"".,.........,..."-~.~. - ~-ontent(%vol)~..-.-.----.--.----~-------.-.---- ~-----,i:~:5·~---- ~.~.-1"3:5-~

et MW lIb/lbmole-mole): 28.00 28.02 28.00

olume Flow Rate (ACFM): 77243 1842919 1883297

olume Flow Rate (SCFM): 1449468 1416305 1450130

olume Flow Rate (DSCFM): 1163794 1139102 1162311

Sample Volume (dscfl: 32.907 33.677 33.077

PM Collected (mg):

Filterable: 8.3 9.2 9.6

Filterable PM10: 5.2 7.7 6.1

PM Concentration (gr/dscf):

Filterable: 0.0039 0.0042 0.0045

Filterable PM10: 0.0024 0.0035 0.0028

PM Emission Rate Ub/hr): ~'6.'1

Filterable: 38.94 41.05

Filterable PM10: 23.96 34.21

PM Emission Rate Ub/MMBtu):

Filterable: 0.0079 0.0085 0.0090

Filterable PM10: 0.0049 0.0071 0.0057

:i Isokinetic Variance 101.0 99.7 101.6

GE Energy Project M22A04278 4
APPENDIX

5
Project Participatants

Agency Observers

Jim Semerad, Ben Gress

GE Energy Project Manager

Bruce Randall

GE Energy Test Crew

Tim Singer, Alan Phillips, Mike Hoehn, Wayne Zoeteman

6
company: Minnkota Power Coop B2

Plant: Milton R. Young Station Hwy 25

City/St: Center, ND 58530

Source: UNIT 2

GE Energy NetDAHS©

Average Values Report

Generated: 6/9/2008 09:24

version 44.'0

Period Start: 5/7/2008 10:13

Period End: 5/7/2008 11:33

Validation Type: 1/1 min

Averaging Period: 1 min

Type: BlockAvg

Period Start:

05/07/2008 10:13

05/07/2008 10:14

05/07/2008 10:15

05/07/2008 10:16·

05/07/2008 10:17

05/07/2008 10:18

05/07/2008 10:19

05/07/2008 10:20

05/07/2008·10:21

05/07/2008 10:22

05/07/2008 10:23

05/07/2008 10:24

05/07/2008 10:25

05/07/2008 10:26

05/07/2008 10:27

05/07/2008 10:28

05/07/2008 10:29

05/07/2008 10:30

05/07/2008 10:31

05/07/2008 10:32

05/07/2008 10:33

05/07/2008 10:34

05/07/2008 10:35

05/07/2008 10:36

05/07/2008 10:37

05/07/2008 10:38

05/07/2008 10:39

05/07/2008 10:40

~S/07/2008 10:41

05/07/2008 10:42

05/07/2008 10:43

05/07/2008 10:44

OS/0~/2008 10:45

05/07/2008 10:46

05/07/2008 10:47

·05/07/2008 10:48

05/07/2008 10:49

05/07/2008 10:50

05/07/2008 10:51

05/07/2008 10:52

05/07/2008 10:53

05/07/2008 10:54

05/07/2008 10:55

05/07/2008 10:56

05/07/2008 10:57

05/07/2008 10:58

. 05/07/2008 10:59

05/07/2008 11:00

05/07/2008 11:01

05/07/2008 11:02

05/07/2008 11:03

05/07/2008 11:04

05/07/200811:05

05/07/2008 11:06

05/07/2008. 11:07

05/07/2008 11:08

05/07/2008 11:09

05/07/2008 11:10

05/0.7/2008 11:11

05/07/2008 11:12

05/07/2008 11:13

05/07/2008 11:14

Average

Unit_Load

MW

470.4

470.6

470.7

466.8

468.9

464.8

461.9

466.1

465.5

467.1

468.6

467.9

469.2

466.9

465.9

465.8

466.8

466.2

466.7

470.2

468.6

467.6

469.2

468.2

464.0

462.2

463.4

464.1

467.1

468.8

468.3

467.9

468.1

470.8

469.1

471.2

467.7

465.3

465.4

467.0

466.3

466.8

466.0

470.6

470.1

465.0

465.2

466.3

466.2

466.6

464.0

462.7

463.3

465.4

469.1

468.3

466.8

470.3

469.0

466.8

467.7

464.6

Average

Opacity

%

9.4

9.3

9.3

9.3

9.3

9.4

9.6

9.6

9.6

9.5

9.5

9.4

9.3

9.3

9.3

9.3

9.3

9.3

9.4

9.2

9.1

9.0

9.1

9.0

9.0

9.1

9.4

9.4

9.3

9.4

9.3

9.2

9.2

9.4

9.6

9.7

9.2

9.6

9.9

9.7

9.7

12.6

10.1

10.2

9.4

9.1

9.1

9.1

8.9

9.2

9.1

9.2·

9.3

9.3

9.3

9.1

9.3

9.1

9.1

8.9

8.9

8.9

Page 1 of 2

7
per:i.od start:

05/07/2008 11:15

05/07/2008 11:16

05/07/2008 11:17

05/07/2008 11:18

05/07/2008 11:19

05/07/2008 11:20

05/07/2008 11:21

05/07/2008 11:22

05/07/2008 11:23

05/07/2008 11:24

05/07/2008 11:25

05/07/2008 11:26

05/07/2008 11:27

05/07/2008 11:28

05/07/2008 11:29

05/07/2008 11:30

05/07/2008 11:31

05/07/2008 11:32

05/07/2008 11:33

Daily Average*

Maximum*

Minimum*

Average

Un:i.t _Load

MW

463.8

466.8

466.4

465.3

464.1

465.3

462.9

464.3

464.8

465.8

470.1

466.9

464.9

463.3

463.4

466.1

462.9

463.4

467.4

466.6

471.2

05/07/2008

10:48

461.9

05/07/2008

10:19

GE Energy NetDAHS©

Average

Opacity

%

9.0

9.0

9.0

9.0

9.3

9.1

9.2

9.1

9.2

9.1

9.0

8.9

8.9

8.9

8.9

8.9

9.0

9.1

9.1

9.3

12.6

05/07/2008

10:54

8.9

05/07/2008

11:30

Version 44.0

* Does not include Invalid Averaging Periods (liN/A")

8

Page 2 of 2
GE Energy NetDAHS@

Average Values Report

Generated: 6/9/2008 09:26

company: Minnkota Power Coop B2

Plant: Milton R. Young Station Hwy 25

City/St: Center, ND 58530

Source: UNIT 2

Average Average

Unit_Load Opacity

Period Start: MW %

05/07/2008 08:20 465.6 9.7

05/07/2008 08:21 466.9 9.6

05/07/2008 08:22 469.6 9.7

05/07/2008 08 :23 470.7 9.6

05/07/2008 08:24 470.4 9.6

05/07/2008 08:25 472.6 9.5

05/07/2008 08:26 472.2 9.4

05/07/2008 08:27 468.5 9.5

05/07/2008 08:28 468.0 9.6

05/07/2008 08:29 465.4 9.6

05/07/2008 08:30 467.1 9.7

05/07/2008 08:31 468.8 9.8

05/07/2008 08:32 466.6 9.7

05/07/2008 08 :33 469.1 9.7

05/07/2008 08:34 469.5 9.5

05/07/2008 08:35 470.2 9.5

05/07/2008 08:36 470.8 9.4

05/07/2008 08:37 468.1 9.5

05/07/2008 08:38 469.8 9.4

05/07/2008 08:39 468.9 9.4

05/07/2008 08:40 471.5 9.5

05/07/2008 08:41 468.0 9.5

05/07/2008 08:42 468.3 9.6

05/07/2008 08:43 465.8 9.7

05/07/2008 08:44 465.1 9.6

05/07/2008 08:45 465.9 9.8

05/07/2008 08:46 465.2 10.2

05/07/2008 08:47 469.5 10.4

05/07/2008 08:48 469.5 10.5

05/07/2008 08:49 469.0 10.2

05/07/2008 08:'50 472.5 9.5

05/07/2008 08:51 471.0 9.5

05/07/2008 08:52 472.4 9.5

05/07/2008 08:53 472.9 9.6

05/07/2008 08:54 469.4 9.8

05/07/2008 08:55 467.5 10.1

05/07/2008 08:56 466.5 10.0

05/07/2008 08:57 464.6 9.7

05/07/2008 08 :58 466.5 9,4

05/07/2008 08:59 466.4 9.5

05/07/2008 09:00 468.5 9.5

05/07/2008 09:01 466.5 9.4

05/07/2008 09:02 470.0 9.3

05/07/2008 09:03 472.0 9.3

05/07/2008 09:04 467.6 9.4

05/07/2008 09:05 464.4 9.4

05/07/2008 09:06 465.2 9.5

05/07/2008 09:07 463.4 9.7

05/07/2008 09:08 463.7 9.7

05/07/2008 09:09 466.6 9.9

05/07/2008 09:10 467.3 9.6

05/07/2008 09:11 470.0 9.7

05/07/2008 09:12 468.6 9.5

05/07/2008 09:13 471.8 9.4

05/07/2008 09:14 469.9 9.4

05/07/2008 09:15 470.0 9.4

05/07/2008 09:16 466.8 9.4

05/07/2008 09:17 468.0 9.5

05/07/2008 09:18 467.3 9.5

05/07/2008 09:19 470.6 9.6

05/07/2008 09:20 468.1 9.6

05/07/2008 09:21 471.4 9.5

9

Page 1 of 2

version 44.'0

Period Start: 5/7/2008 08:20

Period End: 5/7/2008 09:38

Validation Type: 1/1 min

Averaging Period: 1 min

Type: Block Avg
Per:i.od Start:

05/07/2008 09:22

05/07/2008 09:23

05/07/2008 09:24

05/07/2008 09:25

05/07/2008 09:26

05/07/2008 09:27

05/07/2008 09:28

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05/07/2008 0~:33

05/07/2008 09:34

05/07/2008 09:35

05/07/2008 09:36

. 05/07/2008 09:37

05/07/2008 09:38

Daily Average*

Maximum*

Minimum*

Average

Un:i.t Load

MW

470.1

471.6

470.5

470.2

467.6

466.3

467.2

466.8

466.5

471. 7

470.9

471.1

469.4

471.0

467.8

466.7

467.9

468.6

472.9

05/07/2008

8:53

463.4

05/07/2008

9:07

GE Energy NetDAHS©

Average

Opac:i.ty

%

9.4

9.4

9.4

9.4

9.5

9.5

9.7

9.7

9.7

9.6

9.5

9.5

9.4

9.3

9.3

9.4

9.4

9.6

10.5

05/07/2008

8:48

9.3

05/07/2008

9:36

version 44.0

* Does not include Invalid Averaging Periods (liN/Ali)

10

Page 2 of 2
company: Minnkota Power coop B2

Plant: Milton R. Young Station Hwy 25

City/St: Center, NO 58530

Source: UNiT 2

GE Energy NetDAHS@

Average Values Report

Generated: 6/9/2008 09:28

Version 44:0

Period Start: 5/7/2008 09:06

Period End: 5/7/2008 10:27

Validation Type: 1/1 min

Averaging Period: 1 min

Type: Biock Avg

Period start:

05/07/2008 09~06

05/07/2008 09:07

05/07/2008 09:08.

05/07/2008 09:09

05/07/2008 09:10

05/07/2008 09:11

05/07/2008 09:12

05/07/2008 09:13

05/07/2008 09:14

05/07/2008 09:15

05/07/2008 09:16

05/07/2008 09:17

05/07/2008 09:18

05/07/2008 09:19

05/07/2008 09:20

05/07/2008 09:21

05/07/2008 09:22

05/07/2008 09:23

05/07/2008 09:24

05/07/2008 09:25

05/07/2008 09:26

05/07/2008 09:27

05/07/2008 09:28

05/07/2008 09:29

05/07/2008 09:30

05/07/2008 09:31

05/07/2008 09:32

05/07/2008 09:33

05/07/2008 09:34

05/07/2008 09:35

05/07/2008 09:36

05/07/2008 09:37

05/07/2008 09:38

05/07/2008 09:39

Osi07/2008 09:40

05/07/2008 09:41

05/07/2008 09:42

05/07/2008 09:43

05/07/2008 09:44

05/07/2008 09:45

05/07/2008 09:46

'05/07/2008 09:47

05/07/2008 09:48

05/07/2008 09:49

05/07/2008 09:50

05/07/2008 09:51

05/07/2008 09:52

05/07/2008 09:53

05/07/2008 09:54

05/07/2008 09:55

05/07/2008 09:56

05/07/2008 09:57

05/07/2008 09:58

05/07/2008 09:59

05/07/2008 10:00

05/07/2008 10:01

05/07/2008 10:02

05/07/2008 10:03

05/07/2008 10:04

05/07/2008 10:05

05/07/2008 10:06

05/07/2008 10:07

Average

Unit_Load

MW

465.2

463.4

463.7

466.6

467.3

470.0

468.6

471.8

469.9

470.0

466.8

468.0

467.3

470.6

468.1

471.4

470.1

471.6

470.5

470.2

467.6

466.3

467.2

466.8

466.5

471.7

470.9

471.1

469.4

471.0

467.8

466.7

467.9

469.6

468.3

471.0

469.9

466.8

468.2

468.1

466.4

465.2

465.1

462.1

466.4

469.1

471.2

468.6

468.1

471.2

469.9

466.9

472.2

468.2

470.3

470.2

469.6

471.7

466.1

469.3

466.7

465.2

Average

Opacity

%

9.5

9.7

9.7

9.9

9.6

9.7

9.5

9.4

9.4

9.4

9.4

9.5

9.5

9.6

9.6

9.5

9.4:

9.4

9.4

9.4

9.5

9.5

9.7

9.7

9.7

9.6

9.5

9.5

9.4

9.3

9.3

9.4

9.4

9.5

9.4

9.3

9.3

9.4

9.4

9.4

9.9

10.1

10.4

10.0

9.8

9.9

9.8

9.7

9.9

10.1

10.1

9.7

. 9.5

9.5

9.5

9.5

9.5

9.4

9.5

9.3

9.4

9.4

Page 1 of 2

11
Period start:

05/07/2008 10:08

05/07/2008 10:09

05/07/2008 10:10

05/07/2008 10:11

05/07/2008 10:12

05/07/2008 10:13

05/07/2008 10:14

05/07/2008 10:15

05/07/2008 10:16

05/07/2008 10:17

05/07/2008 10:18

05/07/2008 10:19

05/07/2008 10:20

05/07/2008 10:21

05/07/2008 10:22

05/07/2008 10:23

05/07/2008 10:24

05/07/2008 10:25

05/07/2008 10:26

05/07/2008 10:27

Daily Average*

Maximum*

Minimum*

Average

Unit Load

MW

462.6

466.4

467.2

465.6

469.1

470.4

470.6

470.7

466.8

468.9

464.8

461.9

466.1

465.5

467.1

468.6

467.9

469.2

466.9

465.9

468.1

472.2

05/07/2008

9:58

461.9

05/07/2008

10:19

GE Energy NetDAHS©

Average

Opacity

%

9.4

9.5

9.6

9.5

9.5

9.4

9.3

9.3

9.3

9.3

9.4

9.6

9.6

9.6

9.5

9.5

9.4

9.3

9.3

9.3

9.5

10.4

05/07/2008

9:48

9.3

05/07/2008

10:27

Version 44.0

* Does not include Invalid Averaging Periods ("N/A")

12

Page 2 of 2
GE Energy

Particulate Sampling T.rain Equipped With In-5tack Filter

USEPA Method 17

II

II

II

II

II

"

Empty Silica Gel

Ie X :Ie X X X X X X Ie Ie X

X • X X X X Ie X

Ie X It X II II II II Ie X X Ie

Ie X X X X X X X

Ie X X X

100 ml water

1 1

[~}. i

Probe

With In-Stock Filter

Stock Wall

Orifice

1

T

Vocuum

Gouge

fOOi"OI

T

Ice 80th

Temperature

Sensor

Dwg-P

1.3
Company:

Plant:

Unit:

Run:

Minnkota

MRYoung

Unit 2

1

Example Calculations

Page 1 of4

Dry Molecular Weight

Md = 0.44 x(%C02) + 0.32 x (%02) + 0.28 x %N2

13.5 7.3

Md=

Wet Molecular Weight

%02 = -----.... %N2 = ------ 79.2

Ms;:: Md x (1-Bws) + (18.0 x Bws)

Md=

Ms=

Flue Gas Pressure

30.45 0.20

Ps = Pbar + (Pstaticl13.6)

Pbar= 27.76 Pstatic = -1.20

Ps = 27.67

Average Meter Temperature

n

Avg Tin = ~Tin 1=1

n

n

Avg Tout = 1: Tout

1=1

n

Tm = 460+ (Avg Tin + Avg Tout)/2

Avg Tin =

Tm=

74.3

532.8

Avg Tout =

1.4

71.3
Example Calculations

Page 2 of4 .

Ideallsokinetic Sampling Nozzle Inside Diameter (based on initial assumptions):

On = (0.0353 x Qm x Pm x (ls x MS)0.5 )0.5

(TmxCpx(1-Bws)x(PsXAP) )

Qm= 0.70 Pm= 27.89 Ts=

Ms= 27.93 Tm= 540.0 Cp=

Bws = 0.20 Ps= 27.6? AP=

Dn= 0.215

Actual On = 0.205

640.0

0.840

1.10

Isokinetic Sampling ..x.. Factor (based on initial assumptions):

X= 846.72 x On4 x AH@i xCp~ x (1-Bwst x (Md * Ps)

(Ms * Pm)

On=

Bws =

Ms=

_--..;;,0_.2~05~_AH@1= __1....;.7...;;;.3~4__Cp =

__0;;.;,.2;;;.;0~_Md = 30.42 Ps =

27.93 Pm = 27.89 -----

0.840

27.67

X= 1.265

Actual X= 1.Z65

AH at Sample Point - Example Point Ai

AHi= xx APi x (lini)

(Tsi)

1.10 Tsi= 635 ----- Tini= 530 ..,..--...:..;:;.=..--_- APi =

----- AHi= 1.16

Meter Volume at Standard Conditions

Vm(std) = YxVm x 528 x

29.92

(pbar +AHavg/13.6)

Tm

Y=

AHavg =

1.004

1.08

27.76

Vm(std) = ·32.907

:15
Example Calculations

Page 30f4

Volume of Water Vapor Condensed

Vwc(std) =

Vwc(std) =

Moisture Content

Bws =

Vwc(std) =

Bws =

Average Duct Velocity

0.0471 x (net H20 gain)

171.5

Vwc(std)

(Vwc(std)+Vm(std»

__8_.0_7-,-8__Vm(std) _~32:;;;';'..;;.,;90;.,;.7__

Vs = 85.49 x Cp x Sqrt AP (avg) x (Ts (avg)/ (Ps x MS»1/2

Cp=

Ps=

_---..;;o.;..;.84~O__Tsavg = _.----;6.....;,.32=...;;..5__Sqrt AP (avg):

-~~~- 27.67 Ms = 28.00

1.005

Volumetric Flow Rate (Actual Basis)

Q = Vs xAx60

Vs=

Q= 1920687

490.873

Volumetric Flow Rate (Standard Basis)

Qstd = Qx Ps

Tsavg

x 528

29.92

Q= 1920687 Ps= 27.67 632.5

Qstd= 1483007
Example Calculations

Page 4 of4

Volumetric Flow Rate (Standard Dry Basis)

Qstd(dry) = Qstd x (1-Bws)

Qstd=.

Qstd(dry) =

Isokinetic Variation:

1483007 Bws =

1190722

0.197

%150=

Ts=

An=

Bws =

%ISO=

0.0945 x Ts x Vm(std)

Vs x 0 x-An x Ps x (1-Bws)

_~6~32;;:;;.,;;;.5__Vm(std) _~32;;:;;'.;;.;90:...:.7__Vs =

_..;;.0';";'00..;.00;;.:;2;:;;:2;.;;;.9_0 = 60.0 Ps =

0.20

65.213

27.67

~M Concentration - example for filterable:

Co=

M=

Co=

M *0.0154

Vm(std}

__..;.80;.;;,3__Vm(std} _~32;;;;';".;;.;90:...:.7__

0.0039 gr/dscf

PM Emission Rate (Ib/hr) - example for filterable:

ER = Co * 0.00858 * Qstd(dry}

Co=

ER=

0.0039

39.68 Ib/hr

Qstd(dry} = 1190722

:17
LoW 1

Test Date: 5/7/2008

Orcular

25.00 Feet

490.873 Sq.Ft.

ITEST DATA

Project Number:

TEST PARAMETERS

Company:

Plant:

Test Location:

Source Condition:

Test Crew:

TempID:

MeterID:

Meter calibration Factor:

PitotID:

Pitot Tube Coefficient:

Probe Length:

-Probe Liner Material:

Nozzle Diameter:

Train Type:

STACK CONDmONS

Method 5/202

M22A0427

Minnkota

MRYoung

Unit 2

NonnalPM

T. Singer

ES6

ES6

1.004

049A

0.821

9.0 ft.

Stainless-Steel

0.205 in.

M17

Run No.:

Duct Shape:

Diameter:

Duct Area:

Sample Plane:

Port Length:

Port Size (diameter):

PortType:

Number of Ports Sampled:

Number of Points per Port:

Minutes per Point:

Total Number ofTraverse Points:

Test Length:

MOISTURE DETERMINATION

Horizontal

4.00

8.00

Range

4

3

5.0

12

60

in.

in.

min.

Barometric Pressure (Pb):

Static Pressure:

Flue Pressure (Ps):

in. Hg. Imp # Contents Initialwt. Finalwt. Net Gain

in.HzO 1 100mlH20 774.0 928.9 154.9

in. Hg. abs. 2 100 ml H20 747.0 756.0 9.0

3 Empty 630.5 631.3 0.8

Leak Check 4 Silica Gel 798.5 805.3 6.8

carbon Dioxide:

Oxygen:

Nitrogen:

27.76

-1.20

27.67

Pre: ok

Post: 0.004

@ 6.00

13.5

7.3

79.2

In. Hg.

°/0

°/0

°/0 Total Water Gain: 171.5

----~---~---------- -------------------------------- ------~------------_._---

STACK PARAMETERS

Delta If:

MeterTemperature, Tm:

SqrtAP:

Stack Temperature, Ts:

Meter Volume, Vm:

MeterVolume, Vmstd:

Meter Volume, Vwstd:

Moisture, Bws:

EMISSION DATA

1.08

72.8

1.005

172.5

35.542

32.907

8.Q78

0.197

InChes H20

OF

Inches H20

OF

Cubic Feet

dsd

wsd

-Gas Weigiti:diy,Md:

Gas Weight wet, Ms:

Excess Air:

Gas Velocity, Vs:

Volumetric: Flow, ACFM:

Volumetric Flow, DSCFM:

Volumetric Flow, SCFM:

Isokinetic Variance, %1:

30.452

27.998

53.642

63.738

1,8n,243

1,163,794

1,449,468

. 101.0

-Ib/lb mole

Ib/lb mole

0/0

Type ofFuel Firing:

Fuel Factor Fd (dsd/mmBtu):

Fuel Factor Fe (dsdlmmBtu):

Coal

1910

Process Rate: (Units)

PARTICULATE LABORATORY ANALYSIS

Filter/Beaker Weights I Sample Blank Data

I Tare(gT I Final (g) I Net (g) I .Vol (mil I _ Mass (a)

Filterable Fraction:

Filter: 0.1096 0.1159 0.0063

Glassware Rin!!e: 73.2162 73.2188 0.0026 44.00

Less Acetone Blank: -0.0006 88.00 0.0012

Filterable Fraction Total; 0.0083

GE Enerav
Company: Minnkota

Plant: MR Young

Location: Unit 2

X-Factor: 1.265

Test Run: Low 1

Start Time: 8:20

End Time: 9:38

Velocity Orifice A~al Stack MeterTemp Pump Point

Port- Clock Head.Ap Sqlt .AH MeterVol. Temp Inlet Outlet Vacuum Vel

Point tio. Time in. H2O .Ap in. H2O ft3 of of of in. Hg ft/sec

Al 8:20:00 1.10 1.049 1.16 197.031 175 70 69 3.0 66.64

A2 8:25:00 1.10 1.049 1.17 173 70 70 3.0 66.54

A3 8:30:00 0.86 0.927 0.93 160 71 70 3.0 58.22

8:35:00 205.894

B1 8:41:00 1.10 1.049 1.17 173 71 70 3.0 66.54

B2 8:46:00 1.10 1.049 1.17 174 74 70 3.0 66.59

B3 8:51:00 0.95 0.975 1.02 173 75 71 3.0 61.83

8:56:00 214.953

Cl 9:02:00 1.10 1.049 1.17 . 174 74 71 3.0 66.59

C2 9:07:00 1.00 ·1.000 .. 1.07 175 76 72 3.0 63.54

C3 9:12:00 0.89 0.943 0.96 173 77 73 3.0 59.85

9:17:00 223.851

01 9:23:00 1.10 1.049 1.18 173 76 73 3.0 66.54

02 9:28:00 0.97 0.985 1.04 174 78 73 3.0 62.53

03 9:33:00 0.88 0.938 0.95 173 79 74 3.0 59.51

9:38:00 232.573

1.005 L08 35.542 173 74 71 .,. 72.79

Field Notes/Comments:

GEEnergy

:19
ITEST DATA Method 5/202 Run No.: Low 2

Project Number: M22A0427 Test Date: 5{7/2oo8

TEST PARAMETERS

Company: Minnkota Duct Shape: Orcular

Plant: MRYoung Diameter: 25.00 Feet

Test Location: Unit 2

Source Condition: Normal PM Duct Area: 490.873 Sq.Ft.

Test Crew: A. Phillips

TempID: E48 Sample Plane: Horizontal

MeterID: E48 Port Length: 4.00 in.

Meter Calibration Factor: 1.001 Port Size (diameter): 8.00 in.

PilotID: 050A PortType: Range

PilotTube Coeffident: 0.828 Number of Ports Sampled: 4

Probe Length: 9.0 ft. Number of Points per Port: 3

Probe Uner Material: Stainless-Steel Minutes per Point: 5.0

Nozzle Diameter: 0.211 in. Total Number ofTraverse Points: 12

Train Type: M17 Test Length: 60 min.

STACK CONDmONS MOISTURE DETERMINATION

Barometric Pressure (Pb): 27.76 in. Hg. Imp # Contents Inltialwt. Final wt. Net Gain

Static Pressure: -1.20 in. H20 1 100 ml H20 754.8 908.0 153.2

Flue Pressure (Ps): 27.67 In. Hg. abs. 2 100 ml H20 796.5 809.1 12.6

3 Empty 639.3 640.3 1.0

Leak Check Pre: ok 4 Silica Gel 847.8 855.0 7.2

Post: 0.002

@ 10.00 in. Hg.

Carbon Dioxide: 13.5 0/0

Oxygen: 7.4 0/0

Nitrogen: 79.1 0/0 Total Water Gain: 174.0

STACK PARAMETERS ",-,-~-_.-.,~

."~~~~--~~----

Delta H: 1.19 Inches H2O Gas Weight dry, Md: 30.456 Ibllb mole

Meter Temperature, Tm: 71.5 OF Gas Weight wet, Ms: 28;018 Ib/lbmole

SqrtaP: 0.976 Inches H2O Excess Air: 54.886 0/0

Stack Temperature, Ts: 175.4 OF Gas Velocity, Vs: 62.573

Meter Volume, Vm: 36.384 CUbic Feet Volumetric Flow, ACFM: 1,842,919

Meter Volume, Vmstd: 33.677 dscf Volumetric Flow, DSCFM: 1,139,102

Meter Volume, Vwstd: 8.195 wscf Volumetric Flow, SCFM: 1,416,305

Moisture, Bws: 0.196 Isokinetic Variance, 0/01: 99.7

EMISSION DATA

Type .of Fuel Firing:

Fuel Factor Fd (dscf/mmBtu):

Fuel Factor Fe (dscf/mmBtu):

coal

1910

Process Rate: (Units)

PARTICULATE LABORATORY ANALYSIS

I FilterlBeakerWelahts I Sample Blank Data

I Tare (g) I Final Ca) I NetCgl I Vol Cml) I Mass Ca)

Filterable Fraction:

Filter: 0.1107 0.1176 0.0069

Glassware Rinse: 76.1321 76.1348 0.0027 32.00

Less Acetone Blank: -0.0004 88.00 0.0012

. Filterable Fraction Total: 0.0092

20

GE Enerav
ITRAVERSE DATA: Method 5/202

Test Run: Low 2

Start TIme: 9:06

End Time: 10:27

Company: Minnkota

Plant: MR Young

Location: Unit 2

X-Factor'. 1.486

Velocity Orifice Actual Stack Meter Temp Pump Point

Port- Clock HeadAp Sqrt. AH MeterVol. Temp Inlet Outlet Vacuum Vel

Point No. Time in. H20 Ap in. H20 of of of in. Hg ft/sec

A1 ·9:06:00 1.10 1.049 1.37 755.891 172 70 70 4.0 67.03

A2. 9:11:00 0.95· 0.975 1.18 173 70 70 4.0 62.34

A3 9:16:00 0.76 0.872 0.95 173 71 70 3.0 55.76

9:21:00 764.916

61 9:28:00 1.10 1.049 ·1..37 175 71 70 4.0 67.19

82 9:33:00 0.99 0.994 1.23 175 72 71 4.0 63.68

63 9:38:00 0.89 0.943 1.11 174 73 71 4.0 60.39

9:43:00 774.162

Cl 9:50:00 1.10 1.049 1.36 177 . 71 71 4.0 67.29

C2 9:55:00 0.91 0.954 1.13 177 73 71 4.0 61.21

C3 10:00:00 0.85 0.922 1.06 176 74 72 4.0 59.11

10:05:00 783.213

01 10:12:00 1.10 1.049 1.36 178 72 72 4.0 67.35

02 10:17:00 0.97 0.985 1.21 177 74 71 4.0 63.19

03 10:22:00 0.77 0.877 0.96 178 74 71 4.0 56.35

10:27:00 792.275.

0.976 1.19 36.384 175 72 71

71.46

Field NoteS/Comments:

21

GE Energy
ITEST DATA

Project Number:

TEST PARAMETERS

Method 5/202

M22A0427

Run No.: Low 3

Test Date: 5/7/2008

COmpany:

Plant:

Test Location:

Source COndition:

Test Crew:

TemplD:

MeterlD:

Meter calibration Factor:

PitotID:

PitotTube Coefficient:

Probe Length:

Probe Uner Material:

Nozzle Diameter:

Train Type: .

STACK CONDmONS

Minnkota

·MRYoung

Unit 2

NonnalPM

T. Singer

E56

E56

1.004

049A

0.821

9.0 it.

Stainless-Steel

0.205 in.

M17

Duct Shape:

Diameter:

DuctArea:

sample Plane:

Port Length:

Port Size (diameter):

PortType:

Number of Ports sampled:

Number ofPoints per Port:

Minutes per Point:

Total Number ofTraver.ie Points:

Test Length:

MOISTUREDETERMINAnON

Orcular

25.00

490.873

Holizontal

4.00

8.00

Range

4

3

5.0

12

60

Feet

Sq.Ft.

in.

in.

min.

Barometric Pressure (Pb):

Static Pressure:

Flue Pressure CPs):

in.Hg. Imp # Contents Initialwt. Finalwt. NetGain

in. H2O 1 100mlH20 749.0 904.5 155.5

in. Hg. abs. 2 100mlH20 760.6 769.4 8.8

3 Empty 621.9 623.3 1.4

Leak Check 4 Silica Gel 854.3 862.5 8.2

carbon Dioxide:

Oxygen:

Nitrogen:

STACK PARAMETERS

27.76

-1.20

27.67

Pre: 01<

Post: 0.004

@ 6.00

13.6

7.4

79.0

in. Hg.

°/0

0/0

0/0 Total Water Gain: 173.9

Delta H:

MeterTemperature, Tm:

SqrtAP:

Stack Temperature, Ts:

Meter Volume, Vm:

MeterVolume, Vmstd:

Meter Volume, Vwstd:

Moisture, Bws:

EMISSION DATA

1.09

75.9

1.007

174.3

35.934

33.077

8.191

0.198

Inches H20

OF

Inches H20

OF

Cubic Feet

dscf

wscf

GasWeightaty, Md:

GasWeightwet, Ms:

Excess Air:

Gas Velocity, Vs:

Volumetric Flow, ACFM:

Volumetric Flow, DSCFM:

Volumetric Flow, SCFM:

Isokinetic Variance, %1:

30A72

27.997

54.994

63.944

1,883,297

1,162,311

1,450,130

101.6

Ibllbmole

Ibllbmole

0/0

Type of Fuel Firing:

Fuel Factor Fd (dscflmmBtu):

Fuel Factor Fe (dscf/mmBtu):

Coal

1910

Process Rate: (Units)

PARTICULATE LABORATORYANALYSIS

I Filter/Beaker Welahts I Sample Blank Data

I Tare (a) I Final (g) I Net(g) I Vol (mil I Mass (g)

Filterable Fraction:

. Filter: 0.1175 0.1256 0.0081

Glassware Rinse: 73.3297 73.3317 0.0020 40.00

Less Acetone Blank: -0.0005 88.00 0.0012

Filterable Fraction Total: 0.0096

GE Enerav

22
ITRAVERSE DATA: Method 5/202

Test Run: Low 3

Start Time: 10:13

End Time: 11:33

Company: Minnkota

Plant: .MR Young

Location: Unit2

X-Factor'. 1.265

Velocity Orifice Actual Stack Meter Temp Pump Point

Port- Clock HeadAp Sqrt.. AH MeterVol. Temp Inlet Outlet Vacuum Vel

Point No. Time in. H2O Ap in. H2O W CIJ: OF OF in. Hg ft./se(:

A1 10:13:00 1.10 1.049 1.18 232.739 174 76 74 3.0 66.59

A2 10:18:00 1.10 1.049 1.17 175 75 74 3.0 66.64

IU 10:23:.()0 0.89 0.943 0.95 174 76 74 3.0 59.90

10:28:00 241.908

B1 10:36:00 1.10 1.049· 1.18 174 76 74 4.0 66.59

B2 10:41:00 1.10 1.049 1.18 174 77 74 3.0· 66.59

B3 10:46:00 0.88· 0.938 0.94 174 78 74 3.0 59.56

·10:51:00 250.961

C1 10:57:00 1.10 1.049 1.18 174 77 75 3.0 66.59

C2 11:02:00 1.00 1.000 1.07 174 78 75 3.0 63.49

C3 11:07:00 0.88 0.938 0.95 174 79 75 3.0 59.56

11:12:00 259.728

01 11:18:00 1.10 1.049 1.18 174 77 75 3.0 66.59

02 11:23:00 1.10 1049 1.18 175 79 75 3.0 66.64

03 11:28:00 0.85 0.922 0.91 175 80 75 3.0 58.58

11:33:00 268.673

1.007 1.09 35.934 174 77 75

75.92

Field NoteslComments:

GE Enerav

23
No. of Test Runs:

AnalysIs RequIred:

FSR#:

Project:

Method 5/201A

:r-P'--,uu; - -·",v)· _.

,tv,2,2- A0'\'2..1 - - I

f"'\\'I\.v-..k:o~ t>~ i , I

_l-L I

• , I MMhod~\l i

Cl Method 201A I

[J Method 202 I '

!

'larr- -- An--- --;15 I ----I

- -"- . Source: '-(tV,! 2- - L.c<..0 ~A,\)

Project Manager: Sr~_

Analyst: \J~A- \--- c..!;;J~.Ja..a(.'

FilterAnalvsis I

Sample Filter Tare Daterrime ~~temme DatelTlme Final Net

1.0. 1.0. Weicht WelahtlBY , elahtIBv ' -','" ,,: WeiohVBv Weloht Welaht

G.~.OJ ,I I~ ot, y .

.:;. 06, oS I '1 ;,

,'. 1 '-,

It,}w 1 c;£2.- 2c/j:l 0./0'(<0 ',-'_.:-,'

o \ .... 9) 1 U~c. 0·'\\54 1 t--J-~c.. ,,:d. " , I (), //5"'1 O. ()()(P'3 , l ':> - ., .~ .;....'.. ~.

5. o~.O'b 1 1'." b, C'~.QJ ( l~·.co .. ~;. 1

;Jt2 -''2,,07 0, (107

a,l \1'S' JI('c.. (') .\\'1!~ , N~G. 1 0, 117~ 0, ()Of;9

.;, (f&J.7S I ~1 '. z.. - J 1 CS1 1

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0_)151 1 ~ec 0, i 2..S~ , ~~~ I. tJ ,/~-S;(", O,oorI

<:5. /Yl> .ott> 1 l'. 30 ~- 1

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i:?Dg.o1' 135-=)

C ,\ '2.l.-\i I ~e.-- O.I2.4-} ,r>~ I (/./~tf3 (), 001, (J

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Method 5/201A •

7.:1: 3~/7 Ia()oz,.o

7t.'/3lfB I 0, C02?

73.?-f~g I (), fldZf;:

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p.:, ~q I ~~(...

5~D3 .e~ 1 llc. ~;o

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~-~'l~

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1~.·~L.."\1 r®

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1\.1
555 Rogers street • Downers Grove. IL 60515 • 630-969-2703 • FAX630-969-2745

INTERPRETING YOUR ELECTROZONE FINE PARTICLE ANALYSIS

INTRODUCTION

Your samples have been analyzed on an Elzone computerized particle size analyzer, with a working range of approximately

1.01!m to 3501!m diameter Electrozone analysis provides the highest resolution of any type of analyzer on the market today.

This instrument uses the same detection principle and statistical information as the Coulter Counter. . .

The electrozone technique is not sensitive to color, refractive index, density, conductivity or particle opacity; however, it IS

sensitive to the envelope VOLUME ofthe individual particles that are counted and sized. A typical Electrozone statistical report

is composed of a population base of approximately 250.000 particles over the analytical range. with the data being presented

on the basis ofthe EQUIVALENTSPHERICAL DIAMETER.

In the electrozone measurement principle, particles suspended in an electrolyte are caused to flow through a small orifICe made

of a non-conduetive material (sapphire), along with an electric current Particles traverse the orifice one at a time, causing

electrical pulses at rates from a few thousand to a few hundred per second, or lower, .depending upon the orifice size and

particle concentration The amplitude of each voltage pulse is directly proportional to the VOLUME displacement of the particle

as sensed by its "electrical envelope" within the sensing orifice. While the· system responds to particle volume, the computer

reports the DIAMETER of a sphere ofequal volume, hence, the term "EQUIVALENTSPHERICAL DIAMETER" is used.

. Since e1eetrozone analyzers are true particle COUNlCRS, data can be reported in two formats - POPULATION (count) and

VOLUME (mass). For your reference. the data has been reported using both ofthese formats.

POPULATION (COUNTor FREQUENCy) DATA .

On Page 1 is the DIFFERENTIAL FREQUENCY histogram. which plots the NUMBER of partiCles detected versus the size of

the particles detected, on a log scale. As the Elzone is a true 128-channel analyzer, ahigh-resolution graph is produced The

bottom, left-hand side of the page contains··basic statistical information.· Under the heading of PERCENTILES, data is

presented at specific equal distant points (0.77 sigma intervals) for plotting on·Iog-probability graph paper(K&E #46.8040)

On Page 2, the number following "Total Popl" indicates the numberof particles detected during the analysis. (In some cases,

this number can be very large and does not directly represent the number of particles counted due to a computer data blending

operation ·or factor normalization for some specific type of analyses). The number data is then tabulated according to EIzone·

channel number, size in microns at that channel, counts in that channel and, finally, the Cumulative Percentage of Counts

GreaterThan or Equal To the indicated micron size.

VOLUME (MASS) DATA

On Page 3 is the DIFFERENTIAL VOLUME PERCeNTAGE graph, which plots the VOLUME (mass) of particles detected

versusthe size of the particles detected. on a log scale. The statistical information following the histogram is the same asfound

on Page 1, except that the data has been converted to a VOLUME (mass) format. .

Finally. on Page 4, there will be a large numberfollowing "Total VoIm" This figure represents the total VOLUME (mass) of all

the particles, (as listed under Total PopO, determined in the analysis Again, this number may not represent the cumulative

volume ofall particles directly counted due to a computer data blending operation or factor normalization for some specific types

of analyses. This number, however, does represent both volume and mass interchangeably when a Density Of 1.0 is assumed.

Thus. whOe this value may be·thought of in terms of micrograms, grams or pounds, the percentages listed in the tabulation

information at specifIC size intervals allow one to calculate how many micrograms. grams. or pounds of material can be found at

these specific sizes. Data is tabulated according to Elzone channel number. size in microns at that channel, relative mass in

that channel and, finally, the Cumulative Percentage of Relative Mass GreaterThan or Equal To the. iridicated micron size.

Foradditional qtJ9sUons specific to your analysis results, please contact us dIrectly.

www.particletechlabs.com

DR:\Elzone-0903:728

25

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ELZONE(tm) Particle Size Analysis

For: GE ENERGY MANAGEMENT SERVICES, INC.

1301 CORPORATE CENTER DR, SUITE 111

EAGAN, MN 56121

By: PARTICLE TECHNOLOGY LABS, LTD.

665 ROGERS STREET

DOwNERS GROVE, Il 60515

Operator: OJ

COmments:

POPULATION (count) DATA

Date done: 13:36 28 May 2008

Disk File: 16391·1Z.HST

Sample #: lOW 1i CIIl1 COMBINE

lot/Job #: 16391; 64904,64901

Material: AIR EXHAUST

Source: MR. BRUCE RANDALL

5.013 6.919 9. 52 13.19

DIAM Microns

2.1 --

LOG-LINEARPLOT (RELATIVE) _ Sample: LOW 1; ClJL1 COM

1.000 1.380 1.906 2.630 3.631 5.013 6.919 9.552 13.19 18.20 25.13 34.68 47.88

~~ +---+---'~-·'-··-···Lf-~_--.:-~-: ...-Ij-..:-~~-::·-:~+I:-·=-.~;""":~-l!--·-:~-.-~·~..ft-_-._.-~-_:+-: ~---·~-~4-1t!-::-:.-·.~-~+t-~-:_-~.--t!-·_:-.:_-·:-=-+l-::-~:--.~ £ i I ! j l -; J i i ----- +_.. -- +.-- --t--- ---1---'--'1-'- +.--_..+--.--+-- --"'f'-' .._. iii j ; ; I ! ; .......+.- ...... ·li--._ ..........!.. -..:. ........~. - - - .. pf·_ .... _. -i-- .---~~-- --·+----t--···--

iii i I ! i t

- I J ' iiI ! I -t·····-··-t------ I------t---t---·i---·--t-·--t--····t-·····

I I I ' j . , , I .! !. I 1 1 •

I -:_~ =l~~-~.·:~:~~:]-~~~:.r~~~-~.L ~:~ 1.:~~:~: ::~ ~:'~:=:. I I------.-L-J----i i ! !

f ~.~=+ ·c~· --i~··=·'f ..=_.!.. -.... _-}-_.- ._..:~=-=t .._.- .. -----.-------,----- I i i j f J i

.•.-1- -- ." ··i·-_.....+..... -_. f·.. --. -. -f-. -" ---j. -_.---t··_-_·· I I ; I ! 1 1 ! f i ! I !

1.2

P

C 0_9

T

0.6-

0.3

C

o

U 1.8

N

T 1.6

S

Geometric Mean Size:

Geom. Std Deviation:

Geom. Skewness:

Georn. Coeff Variation:

Arithmetic Mean Size:

Median Size:

Mode Size:

Kurtosis:

Arith Std Deviation

2.012 um

1.661 um

0.190

11,60

2.271 um

1.818 um

1.716 um

32.413

1.606 um

- PERCENTILES :...

0.100% Counts above 19.25 urn

1 .000% COunts above 8.223 urn

6.000% Counts above 4.106 urn

22.00% COunts above 2.729 urn

60.00% Counts above 1.902 um

18.00% Counts above 1.391 urn

94.00% Counts above 1.124 um

99.00% Counts above 1.026 um

99.90% Counts above 1.011 um

t

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26
ELZONE<tDl) Particle Size Analysis Date done: 13:36 28 May 2008

For: GE ENERGY MANAGEMENT SERVICES, INC Disk File:· 16391·1Z.HST

1301 CORPORATE CENTER DR, SUITE 177

EAGAN, MN 55121 Sample #: lOW 1; CllL1 COMBINE

By: PARTiClE TECHNOLOGY LABS, l.TD. Lot/Job #: 16391;64904,64907

555 ROGERS STREET

DOWNERS GROVE, Il 60515 Material: AIR EXHAUST

Operator: OJ Source: MR. BRUCE RANDALL

Comments:

POPULATION (count) DATA

-- Frequency Distrfbution Data

Total Popl; 85989259

Chnl Size Counts CLlBl! Oml Size Counts CLllll! Chnl Size Counts Ct:llll~ Chnl Size COUnts CUDU

I 1000 0 100 0 . 33 2.806 1581970 20.4 65 7 872 -- 97 2209 7716 0.04

2 1033 1536141 991 34 2898 1480440 18.6 66 8.130 98 22 81 6041 0.03

3 1 067 1633372 97 3 35 2 993 1381721 17.0 67 8.396 99 2356 4696 o02

4 1 102 1729821 95.3 36 3091 1286916 15-4 68 8.671 100 2433 3645 o 02

5 1138 1824648 93.2 37 3192 1196111 14.0 69 8.955 101 25.13 2841 o 01

6 1.175 1917426 91.1 38 3.296 1108754 12.6 70 9 249 102 2595 2228 0.01

7 1.213 2006777 888 39 3404 1024171 114 7 552 103 26.80 1761 o01

8 1 253 2091913 864 40 3 516 941334 10.2 104 2768 1402 0.01

9 1294 2171933 83.9 41 3631 860629 919 105 2858 1121 0.01

10 1337 2245961 81.4 42 3750 782835 823 106 29 52 904 001

11 1 380 2313164 78.7 43 3.873 708543 7.37 75 10.87 27954 0.70 107 30 49 735 000

12 1.426 2372782 76 0 44 4000 638507 6.58 76 11-22 28455 o 67 108 3149 603 000

13 1.472 2424157 73.2 45 4.131 573732 5.88 77 11.59 28781 064 109 3252 498 0.00

14 1521 2466686 70 3 46 4266 513709 525 78 11 97 28973 0.60 110 33.58 413 o00

15 1.570 2499877 67 5 47 4406 458489 468 79 12.36 29185 0.57 ' 111 34.68 339 000

16 1.622 2523341 645 48 4550 407905 4.18 80 1277 29650 054 112 35~82 275 000

17 1.675 2536802 616 49 4 700 361069 3.73 81 13 19 30442 050 113 36.99 219 0,00

18 1 730 2540142 586 50 4.853 317338 3.34 82 13.62 31464- 046 114 38 21 173 000

19 1 787 2533267 557 51 5.013 276807 2.99 83 14.06 32512 043 115 3946 136 000

20 1845 2516180 52 8 52 5177 239188 2 69 84 14 52 33296 039 116 40.75 108 0.00

21 1906 .2489073 49.8 53 5346 204928 243 85 15 00 33576 o 35 117 4209 87 o 00

22 1.968 2452460 470 64 5522 174924 2.21 86 1549 33222 o 31 118 4346 71 0.00

23 2 032 2406749 441 55 5 702 149504 2.02 87 1600 32210 0.27 119 44 89 56 0.00

24 2099 2353007 414 56 5.889 l28556 1 86 88 16 52 30595 0.24 120 46 36 45 0.00

25 2.168 2291959 38.7 57 6.082· 111778 1. 72 89 17 06 28496 0.20 121 47.88 36 o00

25 2.239 2224033 361 58 6 282 98187 1 60 90 17.62 26021 0.17 122 4945. 30 a 00

27 2.312 2149263 33.5 59 6.487 86733 1.49 91 18 20 23290 . 014 123 5107 15 000

28 2388 2067962 31 1 60 6 700 73248 1.40 92 18.80 20418 o12 124 52 74 20 o00

29 2466 1979733 28 7 61 6.919 68456 1-32 93 19 41 17518 o 09 125 54 47 12 o00

30 2.547 1885510 26.5 62 7.146 57621 1.24 94 20.05 14701 0.08 126 5625 6 0.00

31 2630 1786591 243 63 7.380 54148 1 18 95 20.71 12082 o 06 127 58 10 4 0.00

32 2.717 1684770 223 64 7622 48096 1.12 96 21 39 9735 005 128 60 00 0 o00

27
azONEctm>Particle Size AnalY~is

For: GE ENERGY MANAGEMENT SERVICES, INC.

1301 CORPORATE CENTER OR, SUITE 177

EAGAN, MN 55121

BV: PARTICLE TECHNOLOGY LABS, LTD.

555 ROGERS STREET

DOWNERS GROVE, IL 60516

Operator: OJ

Comments:

VOLUME (mass) DATA

Date done: 13:36 28 MaV 2008

Disk File: 16391-1Z.HST

sample #: LOW 1; CIIL1 COMBINE

Lot/Job #: 16391; 64904, 64907

Material: AIR EXHAUST

Source: MR. BRUCE RANDALL

LOG-UNEAR PLOT (RELAnvE) t'a13Il Sample: LOW 1; CIJll COM

1.000 1..380 1.906 2.630 3.631 5.013 6.919 9.552 13.19 18.20 25.13 34.68 47.88

D 40 , : t i J 36 ( ! I ( iIi: ! t ( i !

. '--':"-'f-" _.r' ....r--'" -r····-"T '-""-r"'-'r...--'I'._.... r---T-.-. 'r-'---r--.. 3.2 .·--_··t "'-"-t- -- --. ·t--.- -'"1' <7~Yi('W\j -""'oj ••• ··t-·- -__r_ """--r .-.-. ··t-··-"-f"' '" V 2'.8 f i i ~.; i ! I ! I I o .. --..-r--····t· ..·······r-.. ···"r·.. ··--j--·· ..T· " "-j- --"'-T- ·······i-..--..r·--. r"-'

L 2.4 ···----j··..--·+---··-i--- ..-··4-···_·-· f-- ---.-~ ..-._- .~- ..-..j --~ ···--·+------l· ..··· u i 1 iii iii ! [ i

M 2.0 .. _ ...•-t -.--. t! - j .. - --J.-. --- +- -.-- .1_•..•...•L -..__ I -.i-- .1.._ '" .1..-.-. -

E i I ! iii i' ! I !

1.6 .. "-'+.......-. t· -'-'-+..._.-+_..--+...... -+ ..-----+- -.... ~-- ...... ....----f-----

p . ! I I j ! iii i !

C 1~2 •.. -- --r0..... ·t..··· ..i-·-····1·---·--t-·-··-i·-······ ---·--1-- ..··T···- --.~_...:_____.:r_~-----ll----- . =::---l I . . -+---------.--.-....--..- 0.8 ._._ ....i--.....J.....-.._1. '.. ';.":.: .>.:.......... 1..- .=o.J...-._~~ ...__. I I I I I ! i i • I I

0.4 ----4·.......·-·.. · .·-----f- ...- .. f

o -lTwlwm.¥A yP,~~

1.000

Geometric Mean Size:

Geom. Std Deviation:

Geom. Skewness:

Geom, Coeff Variation:

Arithmetic Mean Size:

Median Size;

Mode Size:

Kurtosis:

Arith Std Deviation

10.18 um

2.316 um

-3.143

22.75

13.52 um

13.89 um

17.46 um

2.046

9.405 um

-- PERCENTILES -

0.. 100% Vofume above 53.13 um

1.000% Volume above 40.14 um

6.000% Volume above 26,74 um

22.00% Volume above 19.53 um

50.00% Volume above 14.23 um

78.00% Volume above 4.349 um

94.00% Volume above 2.306 urn

99.00% Volume above 1.466 um

. 99..90% Volume above 1.097 um

28
ELZONE<tIn) Particle Size Analysis Date done: 13:36 28 May 2008

For: GE ENERGY MANAGEMENT SERVICES, INC, Disk File: 16391-1Z,HST

1301 CORPORATE CENTER DR, SUITE 177

EAGAN, MN 55121 Sample #: LOW 1; CI1l1 COMBINE

By: PARTICLE TECHNOLOGY LABS, l TO. Lot/Job #: 16391;64904,64907

555 ROGERS STREET

DOWNERS GROVE, IL 60515 Material: AIR EXHAUST

Operator: OJ Source: MR. BRUCE RANDALL

Comments:

VOLUME (mass) DATA evtV\ , -- Volume Distribution Data

Total Volm: 2373891389

Chnl Size Vollll1e ClIIlU Chnl Size Volune tuml: Chnl Size Volume CURtI: Chol Size VollJllle ClJlll%

1 1 000 - 0 100.0 33 2 806 183£7 89.8 65 1.10El- 66 5 97 22.09 4.35El 13 2

2 1033 885973 100 0 34 2.898 1 89E7 89 1 66 1IOEl 660 98 22 81 375El 115

3 1.067 1037715 999 35 2.993 194El 883 67 1.10£7 655 99 2356 3.21El 10.0

4 1102 1210592 999 36 3.091 199£1 87.4 68 IIDEl 65.1 100 24.33 276El 8.76

5 1.138 1406628 99.8 37 3192 2.04£7 86.6 69 115£7 64.6 101 25 13 236£7 7 68

6 1.175 1628255 99.8 38 3.296 208El 857 70 1.21E7 641 102 2695 204El 6 76

7 1.213 1877182 99.7 39 3404 . 2.12E7 84.8 71 6 103 26 80 1.77fJ 596

8 1253 2155532 996 40 3516 214£7 839 1.36£7 6 104 2768 156El 525

9 1294 2465250 995 41 3 631 216£7 830 3 10.19 48£7 105 28.58 1.37fJ 4.64

10 1337 2808150 994 42 3750 216£7 821 74 10 2 1 67E7 106 29 52 1.22£l 4.09

11 1380 3185857 99.3 43'3873 2.16£7 812 75 10.87 188E7 61.0 107 30 49 l.09£] 3.61

12 1 426 3599839 991 44 4000 2.14£7 80.3 76 1122 2.l1fJ 60.2 108 31 49 9850115 317

13 1.472 4051255 990 45 4131 2.12E7 79.4 77 11 59 2 35E7 592 109 3252 8973885 277

14 1 521 4540946 98 8 46 4266 209fJ 78 5 78 11.97 260fJ 582 110 33.58 8193840 2 41

15 1570 5069378 986 47 4.406 Z 05£7 777 79 12.36 289E7 57.1 III 3468 7414013 208

16 1.622 5636579 984 48 4550 2.01fJ 76.8 80 1277 3.23E7 55.8 112 35.82 6611413 1 79

17 1 675 6242088 981 49 4 700 1.96£7 76 0 81 1319 365£7 54.3 113 36.99 5814551 1.52

18 1730 6885015 978 50 4853 190£7 . 75.1 82 13 62 4:16E7 52 7 114 3821 5043249 130

19 1.787 7563651 975 51 5013 183E7 74.4 . 83 14.06 474£7 508 115 3946 4373296 1.10

20 1.845 8275528 97.2 52 5177 1.74£7 73.6 84 14.52 534El 487 116 40 75 3824762 093

21 1.906 9017690 96.8 53 5346 1.64£1 72.9 85 1500 593E7 463 117 42.09 3381069 077

22 1 968 9787307 964 54 5.522 1 54E7 72 2 86 15 49 6 47E7 43.7 118 4346 3060831 0.64

23 2.032 106E7 960 55 5.702 145fJ 71.6 87 16 00 6.91El 409 119 44 89 2670886 0.52

24 2099 114£7 956 56 5 889 137fJ 710 88 16.52 7 23E7 37.9 120 4636 2352948 o41 ,

, 25 2168 1.22fJ 951 57 6.082 1.32E7 704 89 17.06 7. 41E7 348 121 4788 2077637 0.32 t

26 2.239 131fJ 94.5 58 6.282 1.27£7 69.9 90 17 62 746fJ 31.7 122 49.45 1899084 023 I

I

27 2 312 139£7 94.0 59 6.487 1.24£7 694 91 18 20 735El 28.6 123 51.07 1048576 0.17 I

28 2388 lA7E7 93.3 60 6 700 1.15E7 689 92 18,80 7.10£7 25 5 .124 5274 1572864 o12 j.

! 29 2466 l.55fJ 92.7 61 6 919 II9£] 68.4 93 19.41 6.71El 22.6 125 54.47 1048576 006 J 30 2.547 163fJ 920 62 7.146 1.10fJ 67.9 94 20 05 620£7 199 126 56.25 524288 o03

31 2.630 1.70£7 91.3 63 7380 114£7 674 95 2071 562E7 174 127 58 10 410676 0.01

32 2717 177£7 90 6 64 7.622 1 12E7 669 96 21 39 499E7 IS 2 128 6000 0 0.00

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29
ElZONE<tm> Particle Size Analysis

For: GE ENERGY MANAGEMENT SERVICES, INC,

1301 CORPORATE CENTER DR, SUITE 177

EAGAN, MN 55121

By: PARTIClE TECHNOLOGY LABS, LTD.

555 ROGERS STREET

DOWNERS GROVE, IL 60516

Operator: OJ

Comments:

POPULATION (count) DATA

Date done: 17:51 29 May 2008

Disk File: 16391-2Z.HST

Sample #: LOW 2; CJIl2 COMBINE

LotIJob #: 16391; 64906, 64908

Material: AIR EXHAUST

Source: MR, BRUCE RANDALL

- PERCENTILES -

0.100% Counts above 26.83 um

1.000% Counts above 18.04 urn

6.000% Counts above 8.082 um

22.00% Counts above 3.621 um

50.00% Counts above 2.583 um

78.00% Counts above 1.983 um

94.00% Counts above 1.657 um

99.00% Counts above 1.533 um

99.90% Counts above 1.523 urn

2.886 um

1.670 um

0.339

57.85

3.455 um

2,568 um

2.321 um

14.616

3,117 urn

Geometric Mean Size:

Geom. Std Deviation:

Geom. Skewness:

Geom, Coeff Variation:

Arithmetic Mean Size:

Median Size:

Mode Size:

Kurtosis:

Arith Std Deviation

1.6

0.4

LOG-UNEAR PLOT (RELATIVE) IllIIl!!I Sample: LOW 2; CJU COM

1.500 2.005 2..681 3..584 4.792 6.407 8.566 11.45 15.31 20.47 27.37 36.60 48.93

D 4.0 +----1-,--ti--tj, -~i--+I----1il----ti--t-!----fi--+,--11---+j--,

I ! I 'I'!!! I I '

F 3.6 _. - .. ·r-·~- ·"1- -_ -1 ~- .. -."i-- ---- -t-- ·t- ..-i ~.-. t--_.-t----_. -t·_- -. --;- -_ .. t-... _.....

F 3.2 _. __._~-. + t· 1- ~_.--.+ -.+-_.--+---.-i-----.. f--·-·+ + t·--·- i i ! iii ; i ! I .---1'---- "r--'-1--"'-r"-·---r----·T--.... T" ....-r·........1---..-1----

! J I I i Iii i ." !- "1"-' + 'f-''''- --- 1'---..-t---_..+-"--r---'"--;- .- '.~ "T"· ._~

! r I , Ii! , I I

1 ..L--.... .l1-. __+-. -1. __ ._1.._...-_.1._ ......L..-- ...J.---_..t-...-- ! . ! ! t i

j ! i ! J 1 i i ! .- "1- .-- --f'-'-"'~"'-'-"'~--"" ."-- ._ ••t---·_··..··-- ---f..- .." .-..> .....-

r f f iii ! I

--! ~==t~=t=t:~:t::=t~:t:~t-:t::~~_·_--~· i I . I ! i i ! ~~----+-.--~ ,

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-,..... --....i· ...------4-.- - _. ~-- -----J.------1-- .... _..... l- .. .-....._~ .....-- • r i i ! i ! i i .. iii

36.60 48.93 !

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31
ElZONE<tm) Particle Size Analysis

For: GE ENERGY MANAGEMENT SERVICES, INCo

1301 CORPORATE CENTER DR, SUITE 177

EAGAN, MN 55121

BV: PARTICLE TECHNOLOGY LABS, LTO.

556 ROGERS STREET

DOWNERS GROVE, IL 60615

Operator: OJ

Comments:

VOLUME (mass) DATA

Date done: 17:51 29 May 2008

Disk Rle: 16391-2ZoHST

Sample #: LOW 2; CJJl.2 COMBINE

Lot/Job #: 16391;64905,64908

Material: AIR EXHAUST

Source: MR. BRUCE RANDALL

eCAv1 Z1.6

P

C 1 2

o:lf

04

62.8

L 2.4

U

M 200

E

LOG-UNEAR PLOT (RELATIVE) I§!§!I. Sample: LOW 2; CJIl2 COM

t.5oo 2.005 2.681 3.584 4.792 8.407 8.566 11.45 15.31 20.47 27.37 36.60 48.93

r::: +-.-....._-1.~'-.-_-.•-.+1..--.-...-...~-t'-.--.-..-.+1.-....-~.-...J---._-..-...+-t.-.+..-.~-+!.- ..-..-_-.rf-;_-..-_-.+!.-.-._-..-,.t!-.--.-. '-"i+!'--"-'.-..--f.!-_.-._--.".

. F . ! I ! i j ! ! I i ! !

3.2 ·_ ..-.·i ._.. _._~- .....-i·..· .-" 4-· --._·i··;...··.--i·· .. - .L.__._} __.._ L ... _.-l ..._ ..--i-._....... ....•

j f f f f r f r f LIt ....__ ..·.. t·-'-..·T·~·tD· -o/ttm·t..·_. :.. ---+.- ._... -t -----t....._-+-- .. --r--"

iii'iii ! '! it! - ~_.. --f.. --...-... {--- -.. - o} ...-- ... _. +--- .._..t-_· ..--..i..·.. --+ _'· __0 • _._f--. .. --- -¥....... _.... _1 ..-.. -

i ! i ! iii iii -.. ' _..L._.··t··-··.. ...I.•._.._L_..._..L .---1.-. ·i-- .-too _......i._.._--i.- "'" 1 ! i i ! !! I I I I J I ! ! I [ . i i ....... ·r·"-'· --1-- .... " ..r·....·i' ......-T-....·..-r·_· '''-r ~--_.. t"'''-··r-''''

I -! j iii i f i

.~.:~~:' 4:';~-~~~r~:~~~~IL: ·~·~l:·:~:·~r:~'~ ~~:: -:-~ - ...~.-r~:~~:1~~~ ~----_._--------_..__._. •. _.. I

.. ----~ .--._.f---. 1 - ! ......-1 ...... __ I •• ......

+r.w~~

.:~ Ii!

Geometric Mean Size:

Georn. Std Deviation:

Georn. Skewness:

Georno Coeff Variation:

Arithmetic Mean Size:

Median Size:

Mode Size:

Kurtosis:

Arith Std Deviation

15.34 um

10849 um

-1.701

12.06

17083 um

16.099 um

18.48 urn

2.766

9.021 um

32

~. PERCENTILES --

0.100% Volume above 56.23 urn

1.000% Volume above 44.62 um

6.000% Volume above 31.93 urn

22.00% Volume above 23.12 urn

50.00% Volume above 17.29 um

78.00% Volume above 11.86 um

94.00% Volume above 4.012 urn

99000% Volume above 2.264 urn

99090% Volume above 1.664 um
ElZONE(tIII) Particle Size Analysis Date done: 17:51 29 May 2008

For: GE ENERGY MANAGEMENT. SERVICES, INC, Disk Ale: 16391·2Z.HST

1301 CORPORATE CENTER DR, SUITE 177

EAGAN, MN 55121 sample #: lOW 2; CJJl.2 COMBINE

By: PARTIClE TECHNOLOGy LABS, LTO. Lot/Job #: 16391;64906.64908

555 ROGERS STREET

DOWNERS GROVE, IL 60515 Material: AIR EXHAUST

Operator: OJ Source: MR BRUCE RANDALL

Comments: ,e <A Vl VOLUME (mass) DATA '2.-

-- Volume Oistr1butiOIl Data .

Total Volm: 1108345176

Chnl Size Volume Cum); Chnl Size Volume CunlS Chnl Size Volune CtJm1% thol Size Volune CUdlf cnc= ca===----_ -- I 1.600 0 100 0 33 3 798 3661172 94.6 97 24.37 2.16E7 18.2

2 1544 301749 100.0 34 3 910 ·3547856 943 843 98 25.09 197fJ 16 4

3 1589 352866 100.0 35 4.026 3502515 940 83 99 25 83 1.80E7 14 7

4 1.636 410531 999 36 4144 3417985 93 7 7 100 26 59 1.63fJ 13 1

5 1684 475175 99.9 37 4 266 3305604 934 69 10.81 I1DEl 81 8 101 27 37 149El 117

6 1 734 547186 99.8 38 4 392 3182234 93.1 70 11.12 122E7 807 102 28 18 1.37E7 10.4

7 1785 626882 998 39 4.622 3064543 92.8 71 11.45 134El 79.6 103 29 01 126El 924

8 1.838 714511 99.7 40 4655 2964214 ·92.5 72 11 79 1.48E7 783 104 29.86 115E7 8.15

9 1.892 810223 997 41 4.792 2888435 92.2 73 12 ..14 161El 76.9 105 3074 1.04E7 7 16

10 1948 914061 996 42 4 933 2836587 920 74 12.50 175E7 754 106 31 65 9346361 6 2,7

11 2005 1025912 995 43 5.079 2802522 91 7 75 12.86 1 89E7 138 107 3258 8313555 5.48

12 2064 1145564 994 44- 5228 2782220 91 5 76 13.24 203El 120 108 33.54 7331417 4.77

13 2125 1272626 99.3 45 5.382 2771650 91 2 77 1363 215El 70 1 109 34 53 6468077 4.15

14 2188' 1406543 99.2 46 5541 2766560 91.0 78 14.03 228£7 68.1 110 3565 5716104 3.60

15 2 252 1546600 99.0 47 5.704 2764004 90.7 79 1446 241£7 66.0 III 36.60 5055918 3.11

16 2.318 1591902 989 48 5 872 2762334 90.5 80 14.87 255£7 637 112 3768 4480162 2.68

17 2.387 1841373 98.7 49 6.045 2756655 902 81 15.31 2.70E7 61.4 113 38 79 3971522 2.30

18 2467 1993802 985 50 6223 2746863 900 82 15 76 285£7 589 114 3993 3533129 1.96

19 2 529 2147801 984 51 6407 2737365 89.7 83 16.23 3 OOE7 56.2 115 41.11 3091096 1 66

20 2 604 2301851 982 52 6.596 2732068 89.5 84 1671 313E7 53.5 116 42.32 2737679 1.40

21 2 681 2454317 97 9 53 6.790 2736885 89.2 85 1720 3.23£7 50.6 117 4356 2380872 1.17

22 2760 2603494 97 7 54 6990 2758743 89 0 86 1771 3:31E7 476 118 4485 2078098 0.97

23 2 841 2747604 975 65 7.196 2795850 88 7 87 18.23 3.34E7 446 119 46 17 1803521 079

24 2925 2862303 972 56 7 408 2846651 88.5 88 18.76 334E7 416 120 4753 1574168 OM

25 3011 2953447 97 0 57 7 627 2913027 88 2 89 19 32 3.30£7 386 121 48 93 1349447 051

26 3.100 3028326 967 58 7.851 3145788· 88 0 90 19 89 324£7 35.7 122 50 37 1137686 o 40

27 3191 3099490 96.4 59 8 083 3407845 87 7 91 20.47 314E7 328 123 ·51.86 949197 0.30

28 3285 3175477 961 60 8 321 3670127 87.3 92 21.08 3.02El 300 124 5338 876285 022

29 3382 3263144 958 61 8 566 4194143 87 a . 93 21.70 287fJ 274 125 54 96 695317 o15

30 3482 3355899 95.6 62 8 818 4980640 86.6 94 22 34 2.71E7 249 126 66 58 663790 o09

31 3.684 3443754 95.2 63 9.078 55049n 861 95 22.99 2 54fJ· 225 127 58 24 413840 0.04

32 3690 3512874 949 64 9346 6291657 856 96 23.67 235£7 20.3 128 6996 225758 0.01

AA~ 16

q.c,05' £?I. :3

/0,20 63~f;?

/0·0 0~,O j

,i

,

!

t

!

i _ f ... :

33
azONECbI) Particle Size Analysis

For: GE ENERGY MANAGEMENT SERVICES, INC.

1301 CORPORATE CENTER DR, SUITE 171

EAGAN, MN 65121

By: PARTICLE TECHNOLOGY LABS, lTD

555 ROGERS STREET

DOWNERS GROVE,.Il 60516

Operator: OJ

Comments:

POPULATION (count) DATA

Date done: 10:09 31 May 2008

Disk RIe: 16391·3Z.HST

sample #: lOW 3; CKJl.3 COMBINE

lot/Job #: 16391; 64906,64909

Material: AIR EXHAUST

Source: MR. BRUCE RANDAU

47.88

LOG-UNEAR PLOT (RELATIVE) _ Sample: LOW 3; CKJ1..3 COM

1.000 1..380 1.906 2.630 3.631 5.013 6.919 9.552 13.19 18.20 25.13 34.68 47.88

F

p :~: +---+--::-t--.. -...+-1.-..-..-..-!1L..-.. _-..-+!-- ..-...-.-.+f-1_-...-..-...-t~-..-...-.-..+-!---.-.-..-11

1-..---.-...;.-+1- ..-..-..-.f-I..-..-..-..-tl

-...-..-'

! i , i ! i i ! i !

F 2.4 ! .-.. --{.....-.. f,......--f.. _..+..-···i.-.. -.-t··_·..+_... -··1·· ...... t---· ! 'i! I ! ! t' ; i 1 (1' i i I! I

"''''''''i ··..····1· ·__·-t.--_. --'---T'- .. ·t.... -. ··t·..·-'1""-'-'r'--' . i ! I I ! ! i. i l -_.....r ..... __ 4 _ ....!.. -~ .....·r... ·- ... ---j-----......... .,:..... -~--.~-.- ... L.... _. - F --_._,.;.- - -_ ..

i [ iiI i -t-.. ·-t-'--1-'---+-'···t-_.··t··..----t--.-- +-.. ,.._+ . I ._._Ii;

L.........1. ...J... O' ..1 -- .__ -1-.. -----f...--.-l.. '_"0-1 _ . ! . . j I ! ; I I I I ' I

~t~:~t~~t::t.·. ·J~1~:J·:~:l:·-.. ~+·~~ -.~-~---...--..._------:-.~~._.-- ! ! iii i !

._.- f---- -1-- ~-- -t·---~··· t- -_.~~. T~· M • ••+... ·-~·l-· f ! I. t ! l f

g2.1

U

N

T

5

p

C -------.-------------.....:=f

Geometric Mean Size:

Geom. Std Deviation:

Geom. Skewness:

Geom. Coeff Variation:

Arithmetic Mean Size:

Median Size:

Mode Size:

Kurtosis:

Arith Std Deviation

2.034 um

1.564 urn

0.177

76.89

2.298 um

1.881 um

1.768 urn

36.914

1.633 urn

- PERCENTILES -

0.100% Counts above 20.04 um

1.000% Counts above 8.412 urn

6.000% Counts above 4.161 um

22.00% Counts above 2.757 urn

50.00% Counts above 1.924 urn

78.00% Counts above 1.407 um

94.00% Counts above 1.130 urn

99.00% Counts above 1.026 um

99.90% Counts above 1 .011 urn

34
El20NE<tm) Particle Size Analysis Date done: 10:09 31 May 2008

For: GE ENERGY MANAGEMENT SERVICES, INC" Disk Fde: 16391-3Z.HST

1301 CORPOMTE CENTER DR, SUITE 177

EAGAN, MN 55121 Sample #: lOW 3; CKA.3 COMBINE

By: PARTICLE TECHNOLOGY LABS, LTD. LotIJob #: 18391; 64906,64909

565 ROGERS STREET

DOWNERS GROVE, IL 60515 Material: AIR EXHAUST

Operator: OJ Source: MR BRUCE RANDALL

Comments:

POPULATION (count) DATA

_. Frequency Distr'ibution Data

Total Popl: 88844225

Chnl Size Counts CunU Cltnl Size Counts CuliU Chnl Size ColIIts eunu- Chnl Size Counts Cumu -- .. - ...........::a&C... "-ZMPI'" --.-.... 1 1.000 0 100.0 33 2.806 1671952 21 0 65 7.872 51306 111 97 22 09 9932 0.06

2 1033 1494035 992 34 2898 156]064 19 2 66 8 130 47516 1 06 98 2281 8466 0.05

3 1067 1595724 97.4 35 2993 1465496 175 67 8396 44551 1 00 99 23.56 7107 0.04

4 1 102 1697335 956 36 3091 1366987 . 15 9 68 8671 42252 0.95 100 24.33 5874 o 03

5 1.138 1798003 93.6 37 3 192 1271360 144 69 8955 40399 o91 101 25.13 4784 003

6 1 175 1897140 91.5 38 3296 1177822 13 0 70 9.249 38813 o86 102 2595 3855 o 02

7 1 213 1993554 89 3 39 3404 1085566 118 71 9 552 37373 0.82 103 26.80 3088 0.02

8 1.253 2086284 870 40 3 516 994809 10.6 72 9.865 35979 o78 104 2768 2473 0.01

,9 1294 2174354 846 41 3631 906795 953 73 10 19 34616 074 ' 105 2858 1988 o01

10 1.337 2256797 82.1 42 3750 822678 8.56 74 1052 33323 0.70 106 29.52 1606 0.01

11 1.380 2332672 79.6 43 3 873 743590 768 75 10.87 32147 0.66 107 30 49 1306 o01

12 1 426 2401128 769 44 4000 670337 688 76 11.22 31131 063 108 3149 1068 o01

13 1 472 2461368 74 2 45 4.131 602969 6.17 77 11.59 30334 0.69 109 3252 880 . 0 01

14· 1 621 2512683 714 46 4266 540803 5.52 78 11.97 29749 056 110 3358 731 0.00

15 1.570 2554465 68.5 47 4-406 483295 4.95 79 1236 29347 0.53 111 34.68 611 0.00

16 1.622 2586215 656 48 4550 430221 443 80 12.77 29096 0.49 112 35.82 513 000 j 17 1 675 2607548 627 49 4.700 381286 3 97 81 13 19 28970 046 113 36.99 432 0.00

18 1.730 2618258 59.8 50 4853 . 336418 367 82 13.62 28918 043 114 38.21 363 o I 00

19 1.787 2618143 56.8 51 5 013 295871 3 21 83 14 06 28885 040 115 '3946 304 0.00 I

I

20 1 845 2607092 53.9 52 5.177 259478 2 90 84 14.52 28786 0.36 116 40,75, 254 0.00 ! 21 1 906 2585216 50.9 53 5346 226851 2 63 85 15.00 . 28513 0.33 117 4209 211 000

22 1 968 2552927 481 54 5.522 197768 2 39 86 15 49 27970 0.30 118 43.46 172 000

23 2.032 2510913 45.2 55 5 702 171985 2.18 87 1600 27109 027 119 44.89 141 o00 j

24 2099 2460250 424 56 5.889 . 149214 200 88 16 52 25916 024 120 46 36 115 OJJO I 25 2 168 2401759 39.7 57 6 082 129431 1.84 89 17 06 24415 0.21 121 4788 93 0.00

26 2.239 2335527 37.0 58 6282 112579 1.71 90 17 62 22675 018 122 49.45 66 0.00

27 2.312 2261285 34.4 59 6.487 98402 1.59 91 18.20 20776 016 123 51.07 66 o00 I

28 2.388 2178728 31 9 60 6.700 86589 1.48 92 18.80 18805 o 14 124 6274 43 000 !

29 2466 2087743 29 5 61 6.919 76794 1.39 93 19 41 16846 o12 125 54.47 30 0.00 !

30 2.647 1989197 27.2 62 7146 68621 1.31 94 20.05 14960 o10 126 56 25 17 o00 1

31 2.630 1885454 25 0 63 7380 61749 1.24 95 20.71 13115 0.08 127 5810 10 0.00 ! 32 2717 1778879 23 0 64 7.622 56018 1 17 96 21 39 11501 o 07 128 60.00 0 o00

,

J

i

,

1

I

35
Date done: 10:09 31 May 2008

Disk File: 16391 ~3Z.HST

Sample #: LOW 3; CKJL3 COMBINE

LotIJob #: 16391; 64906,64909

ELZONE<tm> Particle Size Analysis

For: GE ENERGY MANAGEMENT SERVICES, INC.

1301 CORPORATE CENTER DR, SUITE 177

EAGAN, MN 55121

By: PARTICLE TECHNOLOGY LABS, LTD,

555 ROGERS STREET

DOWNERS GROVE, IL 60515

Operator: OJ

-Comments:

VOLUME (mass) DATA

Material:

Source:

AIR EXHAUST

MR. BRUCE RANDALL

03

LOG-LINEAR PLOT (RELATIVE> Il'i'Si!I Sample: LOW 3; CKJ1.3 COM

1.000 1380 1.906 2.630 3.631 5.013 6.919 9.652 13.19 18.20 25.13 34.68 47.88

D 3 0 -l---+-.----f--+---!---+-.,...-J---!-I------!----Jf---4---4-----f-....,

2.7 -_······t· ··..··l········J·..·····J· ····t....··..l._..-.~ ....-1"-....... + """ r"--'l-'-r--"

F 2.4 Iii i i ! ! i ! I i ··......T-..... 't ..-.. ·,,;·......t..··..·· i ..·-t·..·_-t .. ·..'t .... -1- ·_·r..--·-T·'·

V 21 i" I I lL" l !•••••_1. __.. , o . .-- r .... 'i·.. ·..":f10.l7M fPVt.... ·f<"'r ....... 1"... i' r I

b 1.8 -t·..·_·t---·.. l ...·.-+... ·....+·..···_+- -i '--..+. . +-- ·..--i----·..J· ---.

M 1.5 ----t...... -·..t--·--·+----i···-..-i-·-··t· ·+ ._. -.-~...-...~---- E iiiIii I .. i I

P 1.2 , t-·..-- ..I +-·-·-1·~..·· ..+----.. ·1-··· ..-+· -- -_·-l-- ·-t..-·-· . I ! J ! J : ! : i

C 0.9 - ·_·-t .-...-t--.....cr-.--L-"+---'-i""'-" i" .+ _.. _. f"-.. -.----..-~-- 0".6" L .1 '_.- . •••. ..... •j-- ...... t·.... I I . I

Geometric Mean Size:

Geom. Std Deviation:

Geom, Skewness:

Geom. Coeff Variation:

Arithmetic Mean Size:

Median Size:

Mode Size:

Kurtosis:

Arith Std Deviation

10.84 urn

2.386um

-3.168

22,01

14.75 um

14.33 um

18.4Oum

2.044

10.87 urn

- PERCENTILES ••

0.100% Volume above t>5.30 um

1.000% Volume above 46.21 um

6.000% Volume above 31.43 um

22.00% Volume above 21.69 um

50.00% Volume above 14.61 um

78.00% Volume above 4.640 um

94.00% Volume above 2.359 urn

99.00% Volume above 1.494 um

99.90% Volume above 1.106 um

36
ELZONE<tm) Particle Size AnalysiS Date done: 10:09 31 May 2008

For: GE ENERGY MANAGEMENT SERVICES, INC. Disk File: 16391-3Z..HST

1301 CORPORATE CENTER DR, SUITE 177

EAGAN,MN 65121 Sample #: LOW 3; CKJL3 COMBINE

By: PARTICLE TECHNOLOGY LABS, LTD. LotIJob #: 16391; 64906,64909

555 ROGERS STREET

DOWNERS GROVE, Il 60515 Material: AIR EXHAUST

Operator: OJ Source: MR. BRUCE RANDALL

Comments:

VOLUME (mass) DATA

-- Volume Distribution Data

Total Volm: 2622111967

oml Size Voltne emU: aml Size VollJIIe CuIlIlS Chnl Size Volure Cunl: Chnl Size Volune CllmU .....- 1 1.000 0 100.0 33 2.806 1.93E7 90.4 65 67.5 97 22.09 5.60El 20.5

2 1033 861688 100 0 34 2898 200£7 89.7 66 670 98 22 81 5.26£7 18 4

3 1.067 1013796 99.9 35 2.993 206£7 889 67 66.5 99 23 56 486£7 16 5

4 1 102 1187857 999 36 3.091 2 llE7 88 1 68 65.9 100 24 33 443E7 14 7

5 1 138 1386087 99.9 37 3192· 216£1 87.3 69 65.4 . 101 25 13 3.97E7 13.1

6 1 175 1611028 99.8 38 3296 2.21E7 86 5 70 648 102 25.95 353E7 117

7 1213 l864813 99 7 39 3.404 224E7 856 71 64.1 103 2680 3.11E7 lOA

8 1.263 2149732 99.7 40 3.516 226£7 848 63. 104 27 68 2.75El 9 32

9 1.294 2467998 99 6 41 363! 221£7 83 9 .7 105 28.58 . 2.43E7 8.33

10 1337 2821698 99.5 42 3.750 227El 83.0 62.0 106 29.52 . 216£7 7.46

11 1380 3212739 994 43 3 873 226£7 82.2 75 2.16£7 612 107 30.49 194E7 6.68

12 1.426 3642844 99 2 44 4000 2.25£7 81.3 76 2.30El 603 108 3149 1.7SE7 5 97

13 1.472 4113442 99 1 45 4 131 2.23E7 80.4 77 247[7 594 109 32.52 1 S8E7 534

14 1 521 4625623 989 46 4 266 2.2G£7 79 6 78 26m 58.5 110 33.58 1.45El 4.76

15 1 570 5180076 98.7 47 4.406 216[7 78.8 79 2.90E7 574 111 34.68 1.34£7 4 23

16 1.622 5777025 98.5 48 4550 2.12E7 78.0 80 3.17El 562 112 35.82 123£7 374

17 1 675 6416165 98.3 49 4.700 2.07El n.2 81 3.4&7 55.0 113 3699 11SE7 3.28

18 1 730 7096747 98.0 50 4.853 201El 764 82 382£7 53.6 114 38.21 1.06£7 286

19 1 787 7817067 97 7 61 5 013 1.95£7 75.6 83 4.21[7 520 115 39.46 9789174 2 47

20 1845 8574531 97.4 52 6.177 1.88£7 74.9 84 4.62E7 50.4 116 40.75 8986418 2 12

21 1 906 9366009 97.1 63 5346 182£7 742 85 504£7 48.5 117 4209 8251991 1 79

22 1 968 1.02[7 967 64 5.522 1.74E7 735 86 5.44E7 465 118 43.46 7391309 1 49

23 2 032 1 10E7 963 55 5.702 167[7 72.9 87 5.81E7 444 119 44.89 6690337 1.22

24 2099 1 19£7 95.9 56 5889 1.60£7 72.2 88 6.12E1 421 120 46.36 6014438 0.98

25 2.168 1.28E7 95.4 57 6082 152E7 716 89 635[7 39 7 121 47 88 5370084 0.76

26 2 239 1.37E7 94.9 58 6.282 1.46£7 71.1 90 650£7 37 3 122 4945 4194304 058

27 2 312 146E7 943 59 6.487 1 41E7 70.5 91 6.56[7 34.8 123 51 07 4614199 o 41

28 2388 1.55£7 93.8 . 60 6.700 1.36£7 70 0 92 6.64El 323 124 52.74 3292600 0.26

29 2.466 1 64E7 93.2 61 6 919 1 33£7 69.5 93 6.45El 298 125 54.47 2572307 0.15

30 2.547 1 72E7 92.5 62 7:146 131E7 69 0 94 631El 274 126 56.25 1572864 0.07

31 2630. 180£7 91 9 63 7.380 . 1.30£7 685 95 612E7 250 127 5810 1048576 o02

32 2.717 187El 91 2 64 7.622 1.30E7 680 96 5.89£7 22.7 128 60.00 0 o00

dt- a W'\ (c7 ~UA

I·fh~ cP3)

(0, It} ro2~ 1 S:

i

G3.2- ;

{O.O J

l

F

37
UNIT:

DATE:

PITOT TUBE CALIBRATION

CALIBRATED BY:

___"<>"<,,,,,,;,;;' STANDARD PITOT:

A SIDE CALIBRATION

dPstd

RUN No. "H20

1

2

dP(s)

"H20

B SIDE CALIBRATION

RUN No.

dPstd

"H20

dP(s)

"H20

Cp(B)

CP(s)

0.837

0.828

0.828

0.831

DEVIATION

Cp(s)-Cp(B)

0.006

0.003

-0.003

--------.-.---------Avg::f)~yi~tiQftt\_must-be_lessihan-or_equaHo.-e~------·--·--------------.--------------------------­

Avg Deviation B must be less than or equal to 0.01

ICp(A)-Cp(B)1 must be less than or equal to 0.01

Avg Deviation (A):

Avg Deviation (B):

0.00

0.00

ICp(A)-Cp(B) I

Cp

38

0.01

0.826
TYPE S PITOT TUBE lNSPECTION DATA FORM

Pitot tube assembly level? yes no

Pitot tube openings damaged? yes (explain below) no

z=Asiny= 0.017 (in.); «0.125 in.)

w=AsinO= 0~099 (in.); «0.03125 in.)

(in.) PA = 0.475 (in.), PB = 0.475 (in.), Dt = -- ,

(in.)

Calibration required? --!-yes no Pitot Repair/Calibration Required

Pitot Tube No.:

_ _.- - _.

Date::::;~ ..i:ii;,~14ii.~n~:~::;:' .': . Name:

,/"

r:

1---------- 1:l!J

LI----_____=::: \j A 1fj;.'r---~-:- v..6_______ :; :' , .._ . -------_.. . , , , : '

NOTE:

C

·05 ~<Pf <1.50 0

PA = PB

0.48 CM ~Df ~0.95 CM

(3/16 IN.) (3/8 IN.)

,

,

.

,

,

TRANSVERSE. :

---V--A-6ffBE-3-------!!!!!-E--~!~~~-----Fi------

1 F"ACE : :. OPENING'~

: PLANES: , . . ,

'%WIT~~"l·A ~5f------ "\ ~_----.

--- 7---~----

(11

B F"Low1

- A . -----·---------c

-----r-~ --------- '-(11

e

----· ------.-}---.--- .____ B . ::-:}_~ __ •

A "'}Pl -.--'--' ------ ------

..·z

:f

H

-------VA--------E-3-.;----

Pitot Calibration Form

•

fi•,~.;;h, I

I' It' • I , • I I I I,

• I I I ., "

TRANSVERSE~::j ~::.i IlIeE AXIS__ ' m !l.. ' _

.,

,. I I

. .,

" , ., ,

. '. , ." ., ,.

,.

" ,,

. " . " , " . 39 GE Energy
dP(s)

"H20

2

3

RUN No.

1

PITOT TUBE CALIBRATION

UNIT: ir.Q~~,'J;~;i';!;~0i?;Ei:;:; CALIBRATED BY:

DATE: ~~~f,Q'~l.9'~;i:j"y STANDARD PITOT:

A SIDE CALIBRATION

B SIDE CALIBRATION

dPstd dP(s)

RUN No. "H20 "H20 ~;"'1::-----h==== "':'.'rl--~~j-L-""""'~~-;

2

3

-.----.---..----~vg .. DevlatK>nf\~le-ss1tran-ore__quattCT()~()1--------------.-.------~----.--.----.----.--.--­

Avg Deviation B must be less than or equal to 0.01

ICp(A)-Cp(B)1 must be less than or equal to 0.01

Avg Deviation (A):

Avg Deviation (B):

0.00

0.00

ICp(A)-Cp(B) I

Cp

0.00

0.827

40
TYPE S PITOT TUBE INSPECTION DATA FORM

Pitot tube aSsembly level? yes no

Pitot tube openings damaged? yes (explain below)

z=Asiny= 0.017 (in.); «0.125 in.)

w=Asine= 0.066 (in.); «0.03125 in.)

(in.) (in.)

Calibration required? ....!-yes no --- Pitot Repair/Calibration Required

Pitot Tube No.:

o'Yo

r-:

..

o.:_... _......-----

l'i

..:

~: A

o

Name:

Pitot Calibration Form

NOTE:

C

.05 l\<P, <1.50 0

P

A =PB

0.48 CM ~D, ~0.95 CM

(3/16 IN.) (3/8 IN.)

o

o

,

,

TRANSVERSE. :

---V--A"6ir-BE-?7-------~!lE-~~~~:-'~----F=Ef------

. ,

: FACE:

OPENING

: PLANES: . . , .

17I',. :.~./ n'I I' • t' I I

" I " II

WVm'_~-----~----~-------. I , • •

I r • I

I • I I

I , I I

I • • I

I • • I

• , I t I I • ,

I I I I

I • • • 4:1

8 ---- -----.--J-.----.- B --_ !2 ----- _._._-----------

A ___::J!~ _

('Z

rr------=-_ " -------h------ u

(-3-s----

GE Energy
Control Module No.

Standard Meter No.

Standard Meter (Yr)

E48

13124821

1.001

:

!

Pre Test DG¥ Calibration

Date:

Calibrated By:

Barometric Pressure:

3/5/08

MH

29.20

I

i

i

I

Orifice Orifice Standard Meter Control Module Standard Meter

~ct";:'~ Dry Gas Meter Dry Gas Meter

Setting in. H2O Setting in. H2O Volume DGMVolume Temp.F Outlet Temp. F Avg. Temp.F Time Time

Run Number (set value) (read value) Vr Vd tr i tdi tdo td Min. Sec. y ~H@ I

i

I

Initial 40.844 660.812 68 73 71

Final 44.685 664.669 68 I 73 71

Difference 1 I 0.81 0.80 3.841 3.857 68 I 73 71 721 71 30 I 1.001 I 1.734

Initial 35.163 655.1l1 68 I 73 71

Final 40.375 660.345 68 74 71

Difference 2 I 1.6\ 1.60 5.212 5.234 68 73.5 71 72.25\ 7\ 30 I 1.000 I 1.883

Initial 28.079 648.033 68 73 71

Final

2.41

34.559 654.519 68 74 71

Difference 3 I 2.40 6.480 6.486 68 73.5 '71 72.251 71 30 I 1.001 1 1.827

I

I

Specifications: CFR 40. Part 60, Appendix A, Method 5, section 10.3.1. Calibration Before Use. I Pre Test Calibration Factor (Y) 1.001 1.815

i

,

~.

N

QE Enorgy E4S-0305200S.xls
Run Time (min):

Vm (dcf):

TmrR):

Pbar ("Hg):

l\Havg ("H20):

Md:

Orifice AH@I:

MeterYi:

Yqa:

Calibration Status:

Method 5 Post Test Calibration

Low 2

60

36.384

531.46

27.76

1.19

30.46

1.815

1.001

1.017

Pass

51712008 Meter #:

Low 4 Low 6

60 60

36.201 37.042

532.42 532.92

27.76 27.76

1.17 1.24

30.44 30.44

1.815 1.815

1.001 1.001

1.014 1.022

E48

Low 8

60

37.531

534.54

27.76

1.26

30.43

1.815

1.001

1.017

43

Average

1.001

1.018
Date:

Calibrated By:

Barometric Pressure :

Control Module No•.

Standard Meter No.

Standard Meter (Yr)

E56

13124821

1.001

I

Pre TestDGk Calibration

!

!

I

!

03/07/2008

TS

29.75

Run Number

Orifice

Setting in. H20

(set value)

Orifice

Setting in. H20

(read value)

Standard Meter

Volume

Vr

Control Module

DGMVolume

Vd

Standard Meter

Temp.F

tr

Dry Gas Meter

Inlet Temp. F

tdi

Dry Gas Meter

Outlet Temp. F

tdo

Dry Gas Meter

Avg. Temp. F

td

Time

Min.

Time

Sec. Y AH@

I

Initial 181.392 77.676 65 1 74 70 ,

Final

1 I 0.81

185.202 81.473. 65 75 70

Difference 0.80 3.810 3.797 65 74.5 70 72.251 71 30 I 1.0151 1.709

Initial 170,447 66.715 65 73 69 I

Final

1.61

175.810 72.104 65 I 75 70

Difference 2 1 1.60 5.363 5.389 65 74 69.5 71.751 71 30 I 1.004\ 1.727

Initial 158.575 54.740 65 70 69

Final

2.41

165.078 61.319 65 74 69

Difference 3 I 2.40 6.503 6.579 65 I 72 69 70.51 71 30'1 0.9931 1.766

I

Specifications: CFR 40, Part 60, Appendix A, Method 5, section 10.3.1. Calibration Before Use.

I

Pre Test Calibration Factor (Y) 1.004 1.734

I

~.

GE Enotgy E56·03072008.xls
Run Time (min):

Vm (dcf):

.TmrR):

Pbar ("Hg):

l\.Havg ("H20):

Md:

Orifice AH@I:

MeterYi:

Yqa:

Calibration Status:

Method 5 Post Test Calibration

Low 1

60

35.542

532..79

27.76

1.08

30.45

1.734

1.004

1.016

Pass

51712008 Meter #:

·Low3 Low 5

60 60

35.934 35.594

535:92 535.50

27.76 27.76

1.09 1.09

30.47 30.45

1.734 1.734

1.004 1.004

1.012 1.023

4S

E56

Low 7

60

35.652

536.75

27;76

1.09

30.45

1.734

1.004

1.021

Average

1.004

1.018
FSR #: M22A0427 Method Used: 17 :

L..~ f

¢:S g-/7/Q-!" t;,-'7-Ce

Test Run #: .e.!1'" <::l:J .q_ Run Date: -ie=~~",,=:::::£...:::: -f O~

2S.0ft

or

Downstream ----- Vertical

or

Diameter: ------

W Check here if same test parameters are the same as recorded for prevlo~s run - make changes as necessary

Company: Minnkota Power ' DJct Shape (select): Rectangular • !

Plant: Unit2\ Length:

Test Location: Stack ± Width:

Source Condition: MID 0 ct Area (sq. feet): 490.873

Test Engineer: r: Sm ~v~ OJ urbance (In diameters): Upstream

Temp ID: $a pie Plane (select): C8o'rizonffij)

Meter 10: ,£'$(, Prt length: """,5~'_~_

Meter calibration' Factors: Y =/~uoi.llli.@l = ('; 73. 't P rt Inside Diameter: ~&l.o!'~"'--'-' _

Pitot 10: tJ~ 2 Prt Type: ...:F~la:;..:.:n:.;;z.ge=-- _

Pitot Cp: N mber of Ports Sampled: ....;F:..;:o:.;:u::..r _

Probe Length: "'9 ft N mber of Points per Port: _Th.:..:.::.;re:::.::e=-- _

Probe Liner Material SS .Mi utes per Point: ---l-S-=::.- _

Nozzle Diameter (In.): 1f9tal # of Traverse Points: Twelve

Train setup: Method 17 1T~st Length (min): -...:<'e=CJ _ I

\

'O"~Y

1;5'</

Final Wt

=rze ·4 l~'O

C021.'

006.~

1

6l.~

e:. ,8 . '.,..---- _____ /7D ,lc

Tare wt:

Tare wt:

.0 scription of imph'lger liquid:

SI ca gel spent?:

S MPLE COLL CTION

imble#:

FiI~er #: C,e?-20'C;7

MbISTURE DETERMINATION

~.pinger # Tare wt., J

.-J 1 . 11'"'(to

-1 2 1 t.-{ /,0 -<

I, 3. 30..}S

\ 4 1<ffl ,2)

,j

STACK CQNpmONS

Barometric Pressure ("Hg): -Z 7- 7 b

Static Pressure ("H20):

Flue Pressure ("Hg):

Sample Train Leak Check: Pre: !pt"Ili;-Post: 100 <t @ &. ''I-Ig

.!!.,'IIJ/ 3 r1d1z-. Pitot Leak Check: Pre: . ~'- Post

carbon Dioxide (%): /2\ c;-

Oxygen (%): .7t '3

Method 3 technique: Orsat Fryrite Analyzer

Fuel Type:

Fd Factor:

Fc Factor:

COMMENTS:

I

5 ftArt-./frd-- GE Energy- Form 1053
5MIi'~I/r , FIELD TEST DAtA SHEET - ISOKINETIC SAMPUNG )(:;-. I, 'z",c, "J"

Test Method Used: 17

~=.---::'l L_ ./ I .- ,.-1'7/CJ' Test Run No. 7i?7 MI'-tJt..,- .vP'(.A/ I....:; I

Date: ~4-e. V Traverse Sheet 1- of

FSR#: -.:...:M=22=-A=.04..:.::2:::..7 ---o._~ __

Company/Plant: Mlnnkota Power i

UnitfTest Location: _U::.;n:..::.lt.:..;2::..:.Sta==ck.:...~ ..i...___

08Z()

Oflz~

()~30 I y( . 1 w2 I -/-rr...c .'ry ; I .; i~-" I """7 .; I -.; ",.. I 7LLC- 1-

lJIr3~, I -I- I· '-0:;>' lrq ~\f+ I caZ!h" I -I 1- -.- '-

I I I: , j I I I I ,

Ztlff - - frO, 8

2'T'S"' - - ~( 3

z. t./s- .- - G?"L .3

-

=t=t=~3 -I ?2.. I (,3 ' Z-A//) 10G1/7 I - I- I ./ 7 S Xs;;tl \ I - I - I- I- 1-1·'-- 1-

",.1 I 'I :

I ()qt.3 2'-{ - - .3

z.. () :z~ 2Y¥ - - !3

3 b9'33 i "Z'fG"' - - .3

?-/VIO OC}5~ ..--- ~' ---- - '--'" -

=Data does not get entered In Excel

5:·~.2~!Pf (\2 f.2Q7S- ;., \':":,' l"Jy _. r ... :I; 'I:; GE Energy- F0ll111026
FSR #: M22A0427 Method Used: 17 .' I

\

((J'''''.2... ' ~_-,__C-~ -D'rL,

Test Run #: %A,td 6 Run Date: -b-~=4~

Round

25.0 ft

or

_____ Downstream

Vertical

490.873

Upstream

Horizontal

Check here If same test parameters are the same as recorded for previo~s run -makechanges as necessary "

Company: Mlnnkbta Power DU~ Shape (select): ,Rectangular or

Plant: Unit 2 I Length: Diameter:

Test Location: Stack I Width: I

Source Condition: . OUt Area (sq. feet):

Test Engineer: A Phrlllp::} Di turbance (in diameters):

Temp ID: Sa pie Plane (select):

Meter ID: e-q8 PO~ length:

Meter calibration Factors: Y = l~a:;/ l\H@1 = (_ref) po~ Inside Diameter:

Pitot ID: oSUllt . po~ Type: .....:F~la=n=ge=--_· _

Pitot Cp: 0. eqo Number of Ports Sampled: Four

Probe Length: "'9 ft ~uh,ber of Points per Port: ....;T:...;:h:;.::;r:.:..ee------~-

Probe Liner Material . SS MiTutes per Point:

Nozzle Diameter (In.): 6. Z/I TPfal # of Traverse Points: Twelve

Train Setup: Method 17 Te~t Length (min):

MepISTURE DETERMINATION

.scription of Impinger liquid:

~11 ca gel spent?:

S PtE COLLECTION

111imble #:

FiI~er #: .' {ac-z.. -Z£J"?

i

!

STACK CONDITIONS

Barometric Pressure ("Hg): 21.1 (p

Static Pressure ("H20): - I( Z. I:

Flue Pressure ("Hg): \

00 Sample Train Leak Check:' Pre: e'j~ Post: tOO 2. @ (0 "Hg

Pitot Leak Check: Pre: ect'5- Post _

Carbon Dioxide (%): . tl,-;?:::....'...:~:...·---

Oxygen (%): 1,t-.

Method 3 technique: Orsat Fryrlte Analyzer

Fuel Type:

Fd Factor:

Fc Factor:

COMMENTS:

5~l~ If f

_3'_ner#

,) 2, T

I 3

j 4

~1-- , I

• i I

Tare wt. 7,54.zJ

lete,.5-·

<O~'1,'

~C17·S

Tare wt:

Tare wt:

Final Wt

o/<l'B"O ISV2_

t7cJ7', I C(,~?r 12..

?<{O",:3 If 6

fiJ55""~ 0 -,. z..

o,{(o1

GE Energy - Form 1053
FIELD TEST DATA SHEET - ISOKINEnC SAMPUNG

Test Method Used: _1=7 _

Test Run ~o. . 7Si r;rl3 !=ti g low 2.

Date: . 5-~-08' • Traverse Sheet of _

FSR#: _M:..:=;:22=.A.;=.O..:,:42::.:.7 _

Company/Plant: Minnkota Power

.....:-.------------------.....---------- Unit/Test Location: _U-",-n;.;.;i",-t.;;;;.2.,;;;;.S.,;;;;ta:;.:;ck=- _

i.(

~{

$'1

,..

247

'2..i.ts

2 '17

( 7S"' I 7 I I '7() I '2. '1 7 . I I I 5"3

l '7 i.f I 7j I 71 I '2.. l.f 7 I I I 5" (

'~75' 1'72- 17/ I ?1.f7 I I 150

3

z.

f)(

~IIJljcL7 I V. II I~' '" I '7;~',i7~ I ! to. I' I I" ··1- 1'\ t=1- ~I' 11

. . = Data does not get.entered in Excel .. ". . .... .' . " .. ..,:.

( . 't' ~.;.

3~~~~IP51'·:·" ":'>.: X"< /,c:(1Je, ;. ,;:: " r'·'~1 _. F'" q; "I:" GE Energy - Form 1026
Method Used: 17 --=-----+---- FSR #: M22A0427 Test Run #: Low'3 Run Date: 5 ( 7I (J 6

_____ Downstream

or Vertical

or

_____ Diameter: _2=5:.:,.O::;...:..:ft_-_

l;l.I' Check here If same test parameters are the same as recorded for previoJ~ run - make changes as necessary

Company: Minnkota Power Ouch: Shape (select): Rectangular

Plant: Unit 2 j Length:

Test Location: Stack j . Width:

Source Condition: 1..,~ DUf Area (sq. feet):

Test Engineer: j ~:::)!~ V Di, .urbance (In diameters):

Temp ID: Sa, pie Plane (select):

Meter ID: e-s-c" POltt t

length:

Meter calibration Factors: Y =I· cot .aH@I:=' I, '7? "I Po. Inside Diameter: _(,,~,_Y _

Pitot ID: ~] C;" P~ Type: -:F:..:;la::;.;n:.;;z.ge=-- _

Pitot Cp: Nu ber of Ports Sampled: ...;F;...;o~u,,-r _

Probe Length: "'9 ft N~ ber of Points per Port: _T~h:.:.;re:;;:e:.....;,. _

Probe Liner Material SS M,I utes per Pqint: _5_" _

Nozzle Diameter (in.): Tp at # of Traverse Points: Twelve

Train Setup: Method 17 Tb~t length (min): --l:l&:;...(J~__

~(~f (cuke! l~ rf ~01 jv(tfV1' eve ;jft

5 vtA~'lA /,PrI

Analyzer

27./b

-(·2

CJ1

o

STACK CONDmONS

Barometric Pressure ("Hg):

Static Pressure ("H20):

Flue Pressure ("Hg):

Sample Train Leak Check: Pre:, c:oV 7" Post: , tJo c.f

::>I-I!J" i (I Pitot Leak Check: Pre: ~~ Post S

Carbon Dioxide (%): l2.

Oxygen (%): 1· '1-

Method 3 technique: Orsat Fryrite

Fuel Type:

Fd Factor:

Fe Factor:

COMMENTS;

.@---': ''Hg

",'ISTURE DETERMINATION

I~,,rnger # Tare wt.

, 1 749,u

: 2 . -( (PO .Go

-,-1 3 'Gz(·1

: 1 4 65G/ , ,,::>

, 1

11

q scription of impinger liquid:

$1 ca gel spent?:

S MPLE COLLE ON

Tt1imble #:

FiI~er #: G0 2 -2~

I

i

. Final Wt

crQc..{ 1 cs- I r.r:)'

023.3 8.7

7b9,i /''1

zCR2.~ 8.'-

Tare wt:

Tare wt: 0 . ( (7 ":)-

GE Energy - Fonn 1053
::J> #'IIPI / j? I-'

It::: /, '2 (,.§"

";,'

",

'''2.- of z. -'

FIELD TEST DATA SHEET - ISOKINETIC SAMPUNG

Test Method Used: ....;1=.:.7.--_=-_

Test Run No. Low'3

Date: $" (71(J e Traverse Sheet

FSR#: ....;M;..:;2=2;:;..;A;.:;:..04..:..;;;2;.;;..7 _

Company/Plant: Mlnnkota Power -----------'---------..,..-- Unit/Test Location: _U:::;.;n:.:.:l;..t=.2.=S.:;;ta:.;::ck:..:..- -:- _

&/v,

B J

Z

S

~L;:'

--

2Lf7 - - 'Yel oS

Z. LfS- - - 't'tJ .?

2.'-13 - - z;e; .3 - - -, "'''~

'7'S"" z~ .- - SI :3

7S- Z.fo/- - '- .s7J :3 , 1' __

. ' .. 7S- "2,/$ - - 5"0 .5

-

G: /

£,vtCJ

3

z.

ull\.i2

~.l . 1-: I ". I' ..... I--L-' ....... - •

= Data does not get entered In Excel

., '''9j~!tf ~../..~ .r-. L c.~ . -d' -r'/"

v

1'_- . ....".-,.(,i1.". 7 •

. J /1'

GE Energy - Form 1026