### . ,. ROJAC AIRTESTING 

# I SERVICES, INC. 120Mountain Avenue Bloomfield, CT 06002



### ComplianceTestReport Redland Brick, Inc.

- KFPlant TunnelKiln SouthWindsor, Connecticut

PreparedFor:



### Mr. BrianHastings Plant Manager

Prepared By:

Mr. LeighA. 

### Garnrnie

August 1999

ROJAC Project No. RBKF9903 860-243-9800



# I

### REPORT CERTIFICATION

I have personally examined and am familiar with the information submitted in this bound document and certify thatbased on reasonable investigation, including my inquiry ofthose individuals responsible for obtaining the information, the submitted information is true, accurate and complete to the best ofmy knowledge and belief.

Leigh A. 

### Gamrnie President

RBKF9903 KFTunnel Kiln Final Report 

# <J 

# /kc9 q{ Date

ROJAC AIRTESTING SERVICES, INC.

### Table ofContents

Section Page 1.0 INTRODUCTION ......................................................................................................................................... I 1.1 Summary ofTest Program ....................................................................................................................... I 1.2 Test Program Organization...................................................................................................................... I 2.0 SOURCE DESCRIPTION............................................................................................................................ 2 2.1 Process Description ................................................................................................................................... 2 2.2 Control Equipment.................................................................................................................................... 2 2.3 Flue Gas Sampling Locations................................................................................................................... 2 3.0 SUMMARY AND DISCUSSION OFRESULTS........................................................................................ 4 3.1 Objectives and Test Matrix ...................................................................................................................... 4 3.2 Field TestChanges .................................................................................................................................... 4 3.3 Summary ofResults .................................................................................................................................. 4 4.0 SAMPLING AND ANALYTICAL PROCEDURES..............•................................................................... 6 4.1 Continuous Emission Monitoring·············································································'······························ 6 4.1.1 Instrumentation..................................................................................................................................... 6 4.1.2 Analyzer Calibrations........................................................................................................................... 6 4.1.3 Data Reduction...................................................................................................................................... 7 4.2 Exhaust Gas Velocity Measurements··································'··································································· 7 4.3 Hydrogen Chloride and Hydrogen Fluoride........................................................................................... 7 5.0 QA/QC ACTIVITIES.................................................................................................................................... 9 5.1 QC Procedures......................................................................................- ..................................................... 9 5.2 Sampling QA/QC....................................................................................................................................... 9 5.3 Laboratory Analytical QA/QC................................................................................................

**~**................ 9

APPENDICES

RBKF9903 KF Tunnel Kiln Final Report 

### ROJAC AIRTESTING SERVICES, INC. 

# '1.3

## 1.0 INTRODUCTION

1.1 Summary ofTestProgram ROJAC Air Testing Services, Inc. (ROJAC) was retained by Redland Brick to conduct an emission measurementtest program on theirtunnel brick kiln located at the KF Plant in South Windsor, CT. The compliance test program was conducted to satisfy the State ofConnecticut, Department ofEnvironmental Protection (CTDEP) permitting requirements.

Emissions measured in determining compliance included sulfur dioxides (S02), 

### hydrogen chloride (HCl), and hydrogen fluoride (HF). The tests were carried out in conformance with Title 40, Code ofFederal Regulations, Part 60 (40CFR60), Appendix A, using EPA Methods 1- 4, 6C, and 26A for determining volumetric flowrates, moisture content, S02 

### and HCl!HF emissions, respectively.



### 1.2 Test Program Organization The following is a listing ofthe test program organization with names and phone numbers of responsible individuals:

Mr. 

### Brian Hastings Mr. 

### Leigh A. 

### Gammie Mr. 

### Carl Ekroth Mr. Ron McLeod

RBKF9903 KF Tunnel Kiln Report 

### Redland Brick ROJAC CTDEP Philip Analytical Services

- I - 

### 800-366-2742 860-243-9800 860-724-4082 905-332-8788

ROJAC AIRTESTING SERVICES, 

### g 

# cj. INC. 

### lJ

## 2.0 SOURCEDESCRIPTION

2.1 Process Description The KF Plant is a brick manufacturing facility thatis permitted to process 21.6 tons perhour of unfired bricks which is equivalent to a maximum daily push rate of 15 cars. As part ofthe manufacturing process, Redland employs a natural gas fired tunnel kiln to dry and fire the bricks with a maximum kiln temperature of2100°F. The tunnel kiln has a maximum fuel-firing rate of 25 MMBTuperhour or 25,000 cubic feet ofnatural gas per hour. Forthe June 10, 1999 test program the push rate averaged 13 cars perhour. A graph depicting process conditions is shown in Appendix D. 

### "t -\-o'v- 

### ·\\.,_r**I~** :1 '2.
,. f'A'**~ ~s-1'""\**  

### Control Equipment 2.2 Emissions from the tunnel kiln were ducted to a dry cascade absorber supplied by BACT Engineering, Inc./Hellmich GmbH & 

### Co. The absorber controls S02, 

### HCl, And HF emissions, which are released from the brickmaterial when dried. The absorbent media consisted of Canadian limestonepellets smaller than 3/8" in size. The pressure drop across the absorber averaged 1inch ofwater column (W.C.) The peeling drum timer was set at 60 seconds on and 13 minutes off. Based on the CTDEP Operating Permit (TownNo. 169, Premise No. 005, PermitNo. 0032, Stack No. 20) dated June 16, 1998, the brick planthas the following emission limits.

Absorber Exhaust 13.2 Table2-1

Redland Brick,Inc. KFPlantTunnel Kiln Emission Limitations

2.85_. 2.35



### Results from this test program are based on the average ofthree test runs and reported on a pounds per hour basis taking into account the actual and dry standard t1owrate measurements recorded during the tests.



### 2.3 Flue Gas Sampling Locations The absorber outlet sampling location was located in a 47" circular section ofsteel stack. Two sampling ports in a horizontal plane gave access to the gas stream. The ports were 352 inches

RBKF9903 KF Tunnel Kiln Report

- 2- 

### ROJAC 

# ,t. AIRTESTING 

## _s 

# I SERVICES, 

## a INC.**~.,**

### (7.5 duct diameters) downstream ofthe induced draft fan and 470 inches (10 duct diameter) upstream to the top ofthe stack. Based upon the above parameters, EPA Method 1required the

use oftwelve sampling points (six points on a traverse). A schematic diagram ofthe outlet test location, along with the individual traverse point locations, is shown in Appendix A.

RBKF9903 KFTunnel Kiln Report

..,



## - .) 

### - ROJAC AIRTESTING**~** 

### SERVICES, 

### L INC.**~**

## 3.0 SUMMARYAND DISCUSSION OF RESULTS

3.1 Objectives andTest Matrix The purpose ofthis test program was to determine the sulfur dioxide (S02), 

### hydrogen chloride (HCI), and hydrogen fluoride (HF) emissions from the tunnel brick kiln during production that

was greater than 90% ofmaximum capacity rating (MCR). Table 3-1 presents the sampling and analytical matrix.

Absorber 

# soz Exhaust

Absorber HCI Exhaust

Absorber HF Exhaust



### 3.2 

### FieldTest Changes Table 3-1

Redland Brick,Inc. KFPlantTunnel Kiln Sampling and Analytical Matrix

3 M6C ROJAC

3 M26A ROJAC

3 Ml-4 ROJAC 84 CEMIUV

84 IC

84 I

### C.

All field sampling occurred without any deviations from the testprotocol. Analyses ofthe hydrogen fluoride samples encountered a matrix interference via ion chromatography (IC). These samples were reanalyzed by ion specific electrode and are reported on the laboratory certificate ofanalysis. For reporting purposes the ion chromatography results were reported as less than 1000 micrograms (<1000 ug) for all three runs, these results are shown in Table 3-2. The ion specific electrode results were not effected by the interference; these results were reported lowerthan the IC results.



### 3.3 

### Summary ofResults
Results from the emissions tests performed on June 10, 1999 are presented on Table 3-2. The average hydrogen fluoride emissions were less than 0.05 pounds perhour, which are below the emission limit of 2.35 pounds per hour. Hydrogen chloride emissions averaged 1.14 pounds per hour, these emissions are below the limit of2.85 pounds per hour. The average sulfur dioxide emissions were 6.14 pounds per hour, which is also below the 13. 2 pound per hour limit.

RBKF9903 KFTunnel Kiln Report

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### ROJAC AIR TESTING 

### SERVICES, INC.

### Table 3-2 Summary ofEmissions Data Absorber Outlet Stack Redland Brick!KF Plant South Windsor, Connecticut June 10, 1999

Outlet Run 1 Run 2 Method/Component Units/Time 1003 -1132 1239- 1409 Method 2 Flowrate dscfm 21623 21462 Method 3-02 % 

### 17.6 17.8 Method 3 - C02 % 

### 2.0 2.0 Method4

- Moisture % 

### 5.72 5.23 Method 26A

- HF lb/hr <0.05 <0.05 Method26A

- HC1 lb/hr 1.27 1.06 Method 6C

- S02 

### lb/hr 6.84 5.67

dscfm

- dry standard cubtc feet per mmute % -percent, dry basis lb/hr- pounds perhour

RBKF9903 KFTunnel Kiln Report

- 5

- 

### Run3 1444- 1612 20951

17.8
2.0
5.34 <0.05

1.09 5.92 Avg. 21346

17.7
2.0
5.43 <0.05

1.14 6.14

ROJAC AIRTESTING 

## 9 SERVICES,

**~** 

### INC.

## 4.0 SAMPLING AND ANALYTICAL PROCEDURES

4.1 Continuous Emission Monitoring ROJAC conducted the outlet gas measurements for S02 

### and 0 2 

### using EPA Reference Methods 6C and 3A, respectively. A schematic diagram ofthe sampling system is shown in Appendix A. The continuous emission monitoring system (CEMS) draws flue gas inthrough a stainless steel heated probe with a heated out-of-stack filtration system. The gas sample is drawn through the probe and filter(s) by a heated Teflon lined diaphragm vacuum pump. From thepump, the sample is sent through a heated Teflon sample line, through an electronic condenser, into a manifold, and finally to the S02 

### and 0 2 

### analyzers. Analyzer outputs will be recorded by a data acquisition system (DAS) at ten ( 1 0) second intervals.

A total ofthree 60-minute CEMtest runs were performed with a zero and mid-range calibration checkbetween each testrun. In addition, a full range calibration and linearity check was performed oneach reference method analyzer at the beginning ofthe test day. Emissions were reported inparts permillion (ppm) and pounds perhour (lblhr). All field datareporting and calculations were conducted in accordance with the guidelines presented in EPAReference Method 6C. Copies ofthe field data sheets are included in Appendix C.

.



### 4.1.1 Instrumentation The S02 

### instrument was a Western Research/BovarModel 721AT2 analyzer. This instrument

measures the S02 

### concentrationby means ofultraviolet (UV) radiation. TheUV radiation is selectively absorbed by

## so2 molecules in the gas stream thus allowing for their quantitative
measurement.

The 0 2 

### instrument was a Servomex Model 1400 analyzer, which measures 0 2 

### concentrationby

means ofthe paramagnetic susceptibility ofthe sample gas using a proven magneto-typemeasuring cell. Oxygen molecules are attracted more strongly by the magnetic field than are molecules ofother gases, and their concentrations can thereby be measured.



### 4.1.2 Analyzer Calibrations Certified EPA Protocol 1 compressed span gases ofS02, 

### and 0 2 

### were used as the calibration standards. Highpurity nitrogen (N2) 

### was used as the zero gas. Forthe field tests, the analyzers

were calibrated and linearized at three points along their measurement ranges atthe beginning of thetest day. The 0 2 

### analyzeroperated on the 0-25% range and the S02 

### analyzer operated onthe 0-100 ppm range. Copies ofthe calibration gases certificate ofanalysis are contained in Appendix E. The system bias and drift tests were conducted with appropriate mid-level dilution gases based on the source emissions. These system calibrations were repeated after each 60- minute test run. The gases passed through all components ofthe sampling system exceptthe sampling probe.

RBKF9903 KF Tunnel Kiln Report

- 6- 

### ROJAC

,. AIRTESTING 

### Cf 

# I SERVICES, 

### /o INC. 

### 4

### 4.1.3 Data Reduction The system calibrations were performed to document any instrument drift. Using Equation 6C-l (40CFR60, Appendix A), the ppm and percent values were corrected to account for the zero and span values plus any instrument drift as follows where:


# cgas emissions concentration (ppm or %)

- 

# c = average emissions reading (ppm or%)



# co average zero reading (ppm or %)



## em average span reading (ppm or %)



## ema 

### span gas concentration (ppm or %)

The corrected ppm and percent averages were then be used to calculate emissionrates in the appropriate standard units.

4.2 Exhaust Gas Velocity Measurements Exhaust gas velocities were measured at points chosen in accordance with EPA Method 1, taking into account duct size, shape, and local flow disturbances. An S-type pitot tube and inclined manometerwere used to measure velocity pressure in accordance with EPAMethod 2. ·A thermocouple and thermocouple thermometer were used to measure stackgas temperatures. The thermocouple was attached to the pitot tube assembly. Pitot tubes and thermocouples were calibrated in the ROJAC laboratory priorto the samplingprogram in accordance withEPA Method 2. The pitot tube and thermocouple are shown in Appendix A.

4.3 Hydrogen Chloride and Hydrogen Fluoride Triplicate isokinetic hydrogen chloride and hydrogen fluoride (HCl/HF) tests were performed concurrently with the CEM tests. Each HCIIHF test was 84 minutes in duration and was conducted in accordance with EPAMethod 26A. The EPA Method 26A sampling train is depicted in Appendix A. 

### The HCl/HF sampling train will consisted ofa quartz glass button**hook~** 

### nozzle, aheated glass lined sample probe, a Teflon filter and frit housed in a heated box, flexible Teflontransfer line, a set of

### 5 glass impingers connected in series contained in an ice bath, a leakless vacuum pump, a calibrated orifice, an inclined manometer, and a calibrated dry gas meter.

The sample probe and oven box were maintained at atemperature between 248°F and 275°F to prevent moisture condensation. A cyclone was not be used with the ROJAC sampling train. The ROJAC

,. AIRTESTING/0 

# I SERVICES, INC. 

# q RBKF9903 KFTunnel Kiln Report

- 7-

## 5.0 QA/QC ACTIVITIES

5.1 QC Procedures Specific quality control (QC) procedures were followed to ensure the continuous production of useful and valid data throughout the course ofthis test program. The QC checks and procedures described in this section represent an integral part ofthe overall sampling and analytical scheme. Strict adherence to prescribed procedures is quite often the most applicable QC check. A discussion ofboth the sampling and analytical QC checks that were utilized during this program is presented below.

5.2 Sampling QA/QC
All measurement devices including sample nozzles, probes, and dry gas meters were uniquelyidentified and calibrated priorto and at the completion ofthis test program. All post test calibrations met their acceptable ranges. Sampling isokinetics were within their acceptable range for all extractive tests. CEM analyzers mettheir daily calibration and drift requirements. Copies ofall equipment calibrations are contained in Appendix E.



### 5.3 Laboratory Analytical QAJQC Field blanks ofall applicable sampling reagents were taken in accordance with their respective sampling methods. Due to the negligible contaminants found in the reagent blanks, blank corrections were not calculated for the final results. Compressed gases used as CEM calibration standards were

### NIST traceable. Laboratorymethod blanks, spike recovery and duplicate analyses were performed where applicable and met their targeted ranges. ·

RBKF9903 KF Tunnel Kiln Report

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### ROJAC AIRTESTING SERVICES, 

### II INC.



### ~~:> :> ) ) ) ' .. --

) **~~** Stack Will •
**~**

**~**

**~** I **~ t~** 

**~~** Calibration Valve I Teflon Sample. Pump THC ;===

Analyzer co Analyzer NO/NOX Analyzer

**~** Heated ss Probe **~~~** I Condenser 1

**~** I

J Heated Teflon Sample

- Teflon Sample Line

I Line

I I -------- PermaPure Dryer

·r

so 2 Analyzer Oxygen Analyzer co Analyzer

't •• EPA Reference Methods JA, 6C, 7E, 10, and 25A

Continuous Emissions Monitoring Sampling System

### AppendixB
Summary ofTestResults

RBKF9903 KF Tunnel Kiln Final Report 

### ROJAC 

## ;3

**f?~** 

### AIRTESTING SERVICES, INC.RUN NO.: DATE: TIME:

PBAR, (in. Hg) STACK AREA, (Sq. Ft.) NOZZLE DIA., (in.) TOTAL TIME, (minutes) CALIBRATION FACTOR PITOT COEFFICIENT SQ.RT.DELTA P, (in. H20) DELTA H, (in. H20) METER TEMP., (Degree F) STATIC PRESS., (in. H20) STACKTEMP., (Degree F) METER VOLUME, (cu.ft.) TOTAL H20 VAPOR, (ml) C02 IN STACK GAS,(%) 02 IN STACK GAS,(%) CO IN STACK GAS, (%) N2 IN STACK GAS,(%) TOTAL HCI CATCH, (mg) HYDROGEN IN FUEL, (%) CARBON IN FUEL, (%) SULFUR IN FUEL,(%) NITROGEN IN FUEL, (%) OXYGEN IN FUEL, (%) GCV, (BTU/Ib) F-FACTOR, (DSCF/MMBTU)

METER VOL. STD, (cu.ft.) H20 IN STACK GAS,(%) STACK GAS MOLECULAR 

### WT EXCESS AIR, (%) STACK GAS VEL., (FPM) GAS FLOWRA TE, (ACFM) STP FLOWRATE, (DSCFM) ISOKINETIC, (%) HCI CONC., (GR/ACF) HCI CONC., (GR/DSCF) HCI CONC., (GR/DSCF@7%02) CONC., (GR/DSCF@12%C02) CONC, (GR/DSCF@50%EA) EMISSION RATE, (lb/hr) F-FACTOR, (DSCF/MMBTU) EMISSIONS, (lb/MMBTU)

Acid Gas Summary RBKF9903 Summary of Hydrochloric Acid Emissions Absorber Outlet Stack Redland Brick/KF Plant South Windsor, Connecticut

M26A-1 M26A-2 M26A-3 6/10/99 6/10/99 6/10/99 1003- 1132 1239 -1409 1444- 1612

30.05 30.05 30.05

12.05 12.05 12.05 0.283 0.283 0.283 84 84 84 1.0091 1.0091 1.0091 0.84 0.84 0.84 0.6760 0.6680 0.6520

2.016 2.0175 1.9333 96 111 110 0.5 0.5 0.5 313 312 311 65.027 65.586 64.445 81.1 72.4 72.8

2.0 2.0 2.0 17.6 17.8 17.8

0.0 0.0 0.0 80.4 80.2 80.2 28.00 23.00 24.00

9570 9570 9570

62.93 61.78 60.76

5.72 5.23 5.34 28.39 28.46 28.44 485.4 527.8 527.8 2770 2733.67 2665.83 33382 32941 32123 21623 21462 20951

95.6 94.6 95.3 4.45E-03 3.74E-03 3.98E-03 6.87E-03 5.74E-03 6.09E-03 2.89E-02 2.58E-02 2.73E-02 4.12E-02 3.45E-02 3.66E-02 2.68E-02 2.40E-02 2.55E-02 1.27 1.06 1.09 9570 9570 9570 5.95E-02 5.30E-02 5.62E-02 AVERAGE

30.05 12.05 0.283 84 1.0091 0.84 0.6653 1.99 106 0.50 312 65.019

75.43 2.0 17.7

0.0 80.3 25.00

0.00 0.00 0.00 0.00 0.00 0 

# / 9570

61.82 5.4 28.43 513.6 2723.27

32815 21346

**-~**

95.2 4.06E-03 6.23E-03 2.73E-02 3.74E-02 2.54E-02 1.14 9570 5.62E-02 

# 14 ¢

ROJAC AirTestingRUN NO.:

**D.~TE:** TIME:

PBAR, (in. Hg) STACK AREA, (Sq. Ft.) NOZZLE DIA., (in.) TOTAL TIME, (minutes) CALIBRATION FACTOR PITOT COEFFICIENT SQ.RT.DELTA P, (in. H20) DELTA H, (in. H20) METER TEMP., (Degree F) STATIC PRESS., (in. H20) STACK TEMP., (Degree F) METER VOLUME, (cu.ft.) TOTAL H20 VAPOR, (ml) C02 IN STACK GAS, (%) 02 IN STACK GAS,(%) CO IN STACK GAS,(%) N21N STACK GAS,(%) TOTAL HF CATCH, (mg) < HYDROGEN IN FUEL, (%) CARBON IN FUEL, (%) SULFUR IN FUEL, (%) NITROGEN IN FUEL, (%) OXYGEN IN FUEL, (%) GCV, (BTU/Ib) F-FACTOR, (DSCF/MMBTU)

METER VOL. STD. (cu.ft.) H20 IN STACK GAS,(%) STACK GAS MOLECULAR 

### WT EXCESS AIR, (%) STACK GAS VEL., (FPM) GAS FLOWRATE, (ACFM) STP FLOWRA TE, (DSCFM) ISOKINETIC, (%) HF CONC., (GR/ACF) < HF CONC., (GRIDSCF) < HF CONC., (GR/DSCF@7%02) < CONC., (GR/DSCF@12%C02) < CONC, (GR/DSCF@50%EA) < EMISSION RATE, (lb/hr) F-FACTOR,"(DSCF/MMBTU) EMISSIONS, (lb/MMBTU)

Acid Gas Summary RBKF9903 Summary of Hydrogen Fluoride Acid Emissions Absorber Outlet Stack Redland Brick/KF Plant South Windsor, Connecticut

M26A-1 M26A-2 M26A-3 6/10/99 6/10/99 6/10/99 1003-1132 1239-1409 1444-1612

30.05 30.05 30.05

12.05 12.05 12.05 0.283 0.283 0.283 84 84 84 1.0091 1.0091 1.0091 0.84 0.84 0.84 0.6760 0.6680 0.6520

2.016 2.0175 1.9333 96 111 110 0.5 0.5 0.5 313 312 311 65.027 65.586 64.445 81.1 72.4 72.8

2.0 2.0 2.0 17.6 17.8 17.8

0.0 0.0 0.0 80.4 80.2 80.2 1.00 < 1.00 < 1.00 <

62.93 61.78 60.76

5.72 5.23 5.34 28.39 28.46 "28.44 485.4 527.8 527.8 2770 2733.67 2665.83 33382 32941 32123 21623 21462 20951

95.6 94.6 95.3 1.59E-04 < 1.63E-04 < 1.66E-04 < 2.45E-04 < 2.50E-04 < 2.54E-04 < 1.03E-03 < 1.12E-03 < 1.14E-03 < 1.47E-03 < 1.50E-03 < 1.52E-03 < 9.57E-04 < 1.05E-03 < 1.06E-03 < 0.05 0.05 0.05

O.OOE+OO O.OOE+OO O.OOE+OO AVERAGE

30.05 12.05 0.283 84 1.0091 0.84 0.6653 1.99 106 0.50 312 65.019

75.43 2.0 17.7

0.0 80.3 1.00

61.82 5.4 28.43 513.6 2723.27

32815 21346

95.2 1.62E-04 2.50E-04 1.10E-03 1.50E-03 1.02E-03 0.05 0 O.OOE+OO 

# r)" 

# r?t

ROJAC Air Testing

- - - - -

## EPA Method 1 Sample and Velocity Traverse· for Stationary Sources 

### Firm Redland Brick, Inc. 

### Total Traverse Points Required

__ **--~ 12** 



### ~~-------- 

### Location South Windsor, CT 

### Number of Ports Diameters Upstream 10 Points Per Port-----------------z:---------- Diameters

**Downstream_7.~...:·~5**

### ___ Traverse (Horizontal or Vertical)_H

_____ _ ·MINIMUM NUMBER OF TRAVERSE POINTS FOR PARTICULATE AND NONPARTICULATE TRAVERSES Duct Diameters Upstream from Flow Disturbance (Distance A) 

### 0.5 1.5 2.0 **50~....-~....-~~--~--~--~T----r---.---,** HIGHEit NUUIIUI &S POit ltiC'TAHGULAA rTACJtS OA Duc:TI

PARTICULATE

1 8 18 rTACit Dw.IETE"

### >G.lla 12& kJ



## -------------------~--~ \__NONPARTICULATE •--- _.___....,..;.;,2 ;o.a_o_r_8_--1 

### r~ 

# ..I

# 1 

# l

Deq • 2LW = 

### L+W · 

# -v--- Sample Port

# r

352"



## 02~....-~----~-~----~--~--~~-~-~10 **r---------------------~** CROSS-SECTIONAL LAYOUT Duct Diameters Downstream from Flow Disturbance FOR RECTANGULAR STACKS
· {Distance B) 

### Total LOCATION OF TRAVERSE POINTS IN CIRCULAR STACKS

Point (Percent of stack diameter from inside wall to traverse point) Number

On A Number Of Traverse Points On ADi_ameter Diameter 

### 4 6 8 

### 10 

## 12 1 6.7 4.4 3.2 2.6 2.1 

## 2 25.0 14.6 10.5 8.2 6.7 3 75.0 29.6 19.4· 14.6 11.8 4 93.3 70.4 32.3 22.6 

## 17.7 5 85.4 67.7 34.2 25.0 6 

### 95.6 80.6 65.8 35.6 7 89.5 77.4

**64~4** 

# a 96.8 85.4 75.0 9 91.8 82.3 

### 10 97.4 88.2 Traverse Points Matrix 

### 3x3 · 4x3 4x4 5x4 5x5

No.

1 

### 2 3 

### 4 5 6 

### 7 8 

### 9 

### 10 11 9 

### 12 16 20 25
.TRAVERSE POINT LOCATIONS Distance Nipple ·Total From Wall Size Distance 2.0 3.5 5-5 6.9 3.5 10.4 13-9 3.5 17.4 33.1 3-5 36.6 40.1 3-5 43.6 44-9 3-5 48.4

. 

# - 0 

# t

**~** 0 -J

**~**



### 11 

### 93.3 12



## 000

**~** 1?

### EPA METHOD2 VELOCilYTRAVERSE AND FLOWRATE DETERMINATION

Date Plant Location

Stack Dimensions Barometric Pressure, (Pb) Static Pressure, (Ps) Stack MolecularWt., (Ms) Moisture Content



### Point 

# A--I d-.. 

## 31-

**~c;-** C:, 

## 13- I 

### .:::2 ..) 

## 1-

## s0

Average 

## -11--L-r_'_'

__ Area 

### /.;7

**~o**

### 5 rt'2

**.....,1~.....::..<1....:..'...:..\:...** __

, __ ln. Hg.

_____ ln. H20 

# -----"

DeltaP 

### Ts Cyclonic 

### inch H20 {'F) 

### FlowAngle :5/C:C /C _7. 

### II 

### /0 3'/?- /0 c? I 

### 'f 

## c;;: 

# .sis

**~~** Jtl /C 3/.9. 

# /s
J/..:3

**~I")** Jls- 1<:::::: 

## 21+

**~** 

### ..313 /0 JIJ



### ~

Abaolute GaaTemperature • Ta + 480"R

Abaolute GuPreuure.Pg • Pb + Pa/13.1
Ta + 400 Gaa Velocity. Va • (IS.4D) ll (Cp) ll (Delta P"1/2)avg x SORT ( ---1 Pg X lob

**~ual** Gaa Flowrate, Qa • (Va) x 10 x Ina · Page 

### or



# -----

Pitot No. ' 1

### 6 ( Leak Check ../ ln. H20 Pitot Coefficient 

### 0 t 

## 84

Tester

0 

### 9a:J Other 

### Other

_____ tlaec

____ .....;ACFM

Standard GaaFlowrate. Qatd • (Qa) x

**~** X fJl X 100

- 'I(.H20
_____ DSCFM
Ta 100 /l(\111110

# /008

**~0** CEMSSYSTEMCALffiRATIONAND.DRIFTDATA 

# f

# 1'3'-- Jl68

Project No.; 

## R(J

### iC

# rcrera3 Date; 

# G 

# ,,1)

# ''i1
Run No.:_l_

Test Location: 

### ,4--b 50

### r 6 

### e.r 0'-'1.1--'1e.

## f StartTime: 

# g11- End Time: 

# II

# 20

'?1'!2..-7
.,, ;') 

### 1 Sowce Equipment: 

## 70
...., A-(: ( 

## K,

## 7 f') Start Scan#: .)

### v '- End Scan#: 

### n



# _...........

**~--**



### Comments: 

### I~



## ~ 

# 00 015CEMS SYSTEM CALIBRATION ANI}DRIFT DATA

Project No.:
Test Location: r

**----~----------------** Date: 

# b

# /10/1) Run



# No.:~ StartTime: 

# 1/L/fi EndTime:__../

.....



## lf....;;o~F/~- Source Equipment:------------------ Start Scan#: 

### /l_${) End Scan#: 

## ZCO,'(

Comments:CEMS SYSTEM CALIBRATION AND DRIFTDATA

Project No.:

_______ _ Test Location:



# -------------- SourceEquipment:

___________ __

Comments: Date:



# -------- Run No.:$
End



## Time:~ End



## Scan#:~ Start Time:



### ~L{

# "Z.:f

Start Scan#: 

# 1,114CEMS ANALYZER CALIBRATION DATA

Source Equipment/Mode: Kiln Tunnel Date: June I0, 1999 Project No.: RBKF9903 

# ---------------------------

Test Location: Absorber Outlet Stack

0 2 Analyzer ID: 1400**---------------~** 0 2 Span Value: 25.0

0 2 zero:
0 2 mid: 10 to 15 %
0 2 high: 20 to 25 %

C02 Analyzer ID: 1400**---------------~** C02 Span Value: 20.0

C02 zero: N2or
C02 mid: 8
C02 high: 16 to 20 %

S02 Analyzer ID: 741**---------------~** S02 Span Value: 100.0

S02 zero: or air(<0.25% ofspan) 

### so2 mid: 40 to 60 ppm
S02 high: 80 to 100 ppm
NO. Analyzer ID:**----------------~·····························** NO. Span Value: 100.0

NO. zero: N2orair(<0.25% ofspan)
NO. mid: 40 to 60 ppm
NO. high: 80 to 100 ppm 0.0

12.0 StartCal: 814



## -------- Start Scan#: 69 

# _______....:........

Analyzer Response:

0.0

12.0

CO Analyzer ID:

### ------------~ 

### >

### >>< >•···•·:c·:·····•·•·•·······•·•••.:.:cc.:·••••••• CO Value: 100.0
CO zero: pureN2
CO low: approx. 30

CO mid: approx. 60


### co high: approx. I00 ppm Analyzer ID:**---------------~** THC Span Value: 100.0

Cal Gas:

THC zero:
THC low: 25 to 35 ppm 0.0 0.0 #DlV/0!

THC mid: 45 to 55 ppm 0.0 0.0 #DIV/0!

THC high: 80 to 90 ppm 0.0 0.0 #DIV/0!

CEM Data Results RBKF9903 Analyzer Cals End Cal: 855

End Scan#: 285

#DIV/0! #DIV/0!

#DIV/0! #DIV/0!
#DIV/0! #DIV/0!

ROJAC AirTestingCEMS SYSTEM CALIBRATIONAND DRIFT DATA

Date: June I0. 1999 Project No.: RBKF9903 RunNo.:_2_
Test Location: Absorber Outlet Stack Start Time: 1239 End Time: 1409



### --------- 

## --------- Source Equipment: Kiln Tunnel Start Scan#: 1575 End Scan#: 2095



# ----------------------------

11.9
17.6
12.0
17.8

0.0 10.1
2.0 10.1
2.0
0.8
49.3
26.1

0.0 0.0 0.0 0.0

0.0 0.0 0.0

Comments:

CEM Data Results RBKF9903 R2 ROJAC AirTesting """'"'"""-.4CEMS SYSTEM CALIBRATION AND DRIFTDATA

Date: June I0 1999 ProjectNo.: RBKF9903 Run No.:_3._
Test Location: AbsorberOutlet Stack Start Time: 1444 End Time: 1612

--------- 

## ---------- Source Equipment: Kiln Tunnel Start Scan#: 2297 End Scan#: 2802



# ----------------------------- ---------

**Pre~Cal·· Syste..r~**  ·.·

**Post~Cal** .

>····.·.···

..· .. $ystem Bias .System

-0.I

CEM Data Results RBKF9903 R3 Bias < • ····•·• ])rift

: . ·:·.·._:. :··.-

..::

..·. (<5%

**spa~}**

**(<J )~§pan)**  0.4% -0.1
Il.8

17.5
12.0
17.8
0.0
10.1
2.0
10.1
2.0
0.6
49.3

27.7
50.6
28.2

0.0
0.0
0.0
0.0

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### 17.5 0.0 2. 10 765 101'32'3 1:.2 

### 02 

### mt 

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### 17.5 0.0 2.00 77'3 102156 

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### 17.4 

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### 17.4 

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### 10 825

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### 17.6 0.0 2.00 827 103010 3. 2 

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### 17.4 

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### '3 17.6 0.0 2. 10 841 1()3232_ l. 8 

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### 17.6 0.0 2. 10 843 103251 l.4 

### 17.5 0.0 2. l.O 844 103302 l. 3 

### 17.5 0.0 2. 10 845 103312 1.2 

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### 17.2 0.0 2.40 860 103544 

### t. 5 

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### 17.1 

## o.o 2.50 863 103614 2. 0 

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### 1'3.0 0.0 0.80 885 104001 5. 7 

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### 1 18.'3 0.0 0.80 887 104021 

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### mt CC•2 s•:an 

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## o.o 1. 80 '316 104516 L. 7 17.'3 0.0 1.80 '317 104526 L. 7 17. '3 0.0 1. 80 '318 104536 L. 4 17.'3 

## o

..o 1. 80 '319 104546 l. 3 17.'3 0.0 1. 80 '320 104557 L. 4 17.9 0.0 1.80 921 104608 L .-.



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## :z.oo '336 104840 ). 9 17.6 0.0 2.00 '337 104851 ) • '3 17.5 0.0 2.00 '338 104'301 L. 3 17.7 

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## o.o 1.'30 '343 104'353 ) • '3 1.7.7 0.0 1.90 '344 105004 ). 8 17.7 0.0 1.90 945 105014 l. 3 17.5 0.0 2.00 '345 105025 l. 2 17.5 0.0 2.00 '347 105035 l • :'2 17.6 0.0 2.00 '348 105048 l. 4 17.7 0.0 2.00 949 105057 l. 4 17.7 0.0 1.90 '350 105108 l.0 17.7 0.0 2.00 '351 105118 l. 4 17.7 0.0 2.00 '352 105129 l.3 17.5 0.0 2.00 '353 105140 l. 4 17.7 

## o.o 1.90 954 105150 l. 4 17.7 0.0 2.00 '355 105200 l. 4 17.5 0.0 2.00 '356 105211 l D 4 17.5 0.0 2.00 '357 105221 l. 4 17.6 0.0 2.00 '358 105231 l. 4 17.6 0.0 2.00 '35'3 105242 l. 4 17.7 0.0 2.00 960 105253 l. 7 17.7 0.0 1.'30 961 105303 

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### 17.7 0.0 2.00 '368 10541'3 

### 1.4 17.6 0.0 2.00 969 105429 

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### 17.5 0.0 2. 10 '370 105440 1.3 17.4 0.0 2.10 971 105452.. 1.4 

### 17.5 0.0 2. 10 '372 105501 1.3 17.5 

## o.o 2. 10 '373 105512 1.3 17.5 0.0 2. 10 '374 105521 1.3 17.5 0.0 2.00 975 105532 :.2 

### 02 

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### t me 1.3 17.6 0.0 2.00 976 105542 1.4 

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### t.O 17.5 0.0 2. 10 '380 105625 1 ":::>



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### 17.7 0.0 2.00 '383 105657 ).7 17.5 0.0 2.10 '384 105707 0.8 17.6 0.0 2.00 '385 105717 0.8 17.6 0.0 2.00 986 105727 1.0 17.7 0.0 1.'30 '387 105737 :). 8 17.7 0.0 2.00 '388 105747 1. 3 

### 17.7 0.0 2.00 98'3 105756 0. '3 

### 17.6 0.0 2.00 '3'30 105807 1.0 17.6 0.0 2.00 '391 105817 0.9 

### 17.6 0.0 2.00 9'32 105826 1.0 17.6 0.0 2.00 '3'33 :!_()5837 

### 1.4 17.6 0.0 2.00 '3'34 105847 1.4 17.5 0.0 2.00 '3'35 105858 1.3 17.5 0.0 2.00 '396 105908 1.4 17.7 0.0 2.00 '3'37 105918 1.4 17.6 

## o.o 2.00 '3'38 105928 1.4 17.5 0.0 2. 10 '3'3'3 105'338 1. 3 

### 17.5 0.0 2. 10 1000 105948 1. 2 

### 17.4 

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### 17.7 0.0 2.00 1004 110028 ). 9 

### 17.5 0.0 2. 10 1005 11003'3 1.4 17.5 0.0 2. 1(I 

### 1006 110050 1.3 17.4 0.0 2. 10 1007 11005'3 1.3 17.5 

## o.o 2. 10 1008 11010'3 1.4 17.5 0.0 2. 10 1009 110120 1.4 17.5 0.0 2. 10 1010 110131 1.7 17.5 

## o.o 2.10 1011 110141 1.4 17.6 0.0 2. 10 1012 110152 1.7 17.5 0.0 2.00 1013 110203 1.7 17.7 0.0 2.00 1014 110213 1.4 17.7 0.0 2.00 1015 110223 1.4 

### 17.7 0.0 2.00 1016 110234 1.0 17.5 0.0 2. 10 1017 110244 1.4 17.5 0.0 2. 10 1018 110254 1.0 17.5 0.0 2. 10 1019 110304 1 ":::>



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### 17.5 0.0 2.10 1023 110344 1.4 17.6 0.0 2.00 1024 110353 1. 2 

### 17.6 

## o.o 2.00 1025 110403 ) • '3 

### 17.5 

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# +o ). 9 

### 17.5 0.0 2.10 1027 11042!5 

# W1 1.0 17.4 

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## o.o 1. 90 1043 110713 j 3. ':3 17. '3 0.0 1. '30 1044 110723 I ! 0.1 17. '3 0.0 1. '30 1045 110733 I 

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# I I 3. 5 17.'3 

## o.o 1.80 1055 110915 ·3. 5 17.9 0.0 1. 80 1056 110'325

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# t '3. 5 17.6 

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### 19.0 0.0 0.80 1113 111'314 8.6 18.5 0.0 1.00 1114 111'325 8.1 18.2 0.0 1.20 1115 111'335 r:•2 

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### 17.5 0.0 1. '30 1125 112122 '3. 2 

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### 17.5 0.0 2.00 1130 112212 '3. 9 17.5 0.0 2.00 1131 112223 

### 9.8 17.6 0.0 1.90 1132 112233 

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## o.o 2.00 1140 112357 9.9 17.6 0.0 2.00 1141 112406 9.9 17.5 0.0 2.00 1142 112417 9.9 17.6 0.0 1.'30 1143 112428 9.8 17.6 0.0 2.00 1144 112438 9.8 17.7 0.0 1.90 1145 112448 9.6 17.7 

## o.o 2.00 1146 112458 '3. 6 17.7 0.0 1. "30 1147 112507 9.5 17.7 0.0 1.90 1148 112518 9. 1 17.7 

## o.o 1.'30 114'3 11252'3 '3. 5 17.6 0.0 2.00 1150 112539 9.5 17.6 

## o.o 2.00 1151 112549 9.5 17.6 0.0 2.00 1152 112600 '3. 0 17.7 0.0 1.'30 1153 112611 

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.. 3(> 2.

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### 2.00 l.. 60 2616 2617 2618 261'3 2620 2621 

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# END

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# 0 

# rtffr

### AppendixD

Tunnel Kiln Process Data

RBKF9903 KF Tunnel Kiln Final Report 

### ROJAC AIRTESTING SERVICES, INC.

{) {) n n

**•~·** ·-·

# PoundsperBrick

13 

# tl0l)'07GRBKF9903 KF Tunnel Kiln Final Report 

### Appendix E
Equipment Calibrations



### ROJAC AIRTESTING SERVICES, INC.:=:> :=:> =:> =:> ......] :0 Method 5 tJ

Date: June 11,1999 Module #: 2827

Bar.

Ps., (Pb}: 30.44 in. Hg Std. Meter: 570415

Standard Meter

Module Volume
Orifice Vs Setting (ft3)

(in. H 2 0) 2.0 11.425

2.0 11.555

2.0 11.546 Correlation Line Equation

Q = m (OF) + b Vs (Pb +

Y= Vm (Pb +

dHa = (Q QJH) Factor Ys 0.999 0.999 0.999 **~** 13.6 dl:L.....l 13.6

dH Temp. Pressure Volume

ts Ps Vm tmi

(oF) (in. H 2 0) (ftl) (oF)

72 -0.3 11.693 100

72 -0.3 11.857 100

72 -0.3 11.857 103

'

Y = Ratio of roading of wettest meter to dry test meter;

tolerance for individual values +/- 0.02 from avg.

dH@ = Orifice pressure differential that equates to 0. 75

cfm

of air @65degF and 29.92" Hg, in. H20; tolerance

for

individual values +/- 0.20 from avg.

(Tm + 460) Ys

( Ts + 460)

[(lli + **~§Q)** @ l' Reference thermo OF 70 Actual tmi OF 70 Post-test Module Meter Time Delta Module

tmo

@ Ha Flowrate

("F) (min) y (in. H 2 0) Q (SCFM)

82 15.00 1.0054 1.85 0.7674

85

15.00 1.0055 1.80 0.7762

86

15.00 1.0083 1.80 0.7756

Averages 1.0064 1.82

Acceptance Criteria:

Error 0.00% Perform 3 calibration runs at a single, intermediate orifice setting at the

maximum vacuum reached during test series. If Y has changed by more

than

5%, recalibrate meter over all five orifice settings. Thermocouple Calibration

Actual tmo I

Error

"F 70 I 0.00% Calibrated By: R.M. ZANNI

Date Calibrated: 01 March 1999 OF 6.0168 6.0250 6.0359

Pb (tm + 460) [ Vs Ys l' **~i~IImiHtifi~J~I~[!ltJ{iJJtttii~Iiftt~J@?fiimJttiWftfti!lt/Iii:**

Module Quality Control Checks

(Pb + __QJJ_} Module Cleaned:

**..~..Y.;;.es~---**

a

= Y {17.64) Vm 13.6 Pitot Manometer Leak Check: yes @ 6.0"wc

(tm + 460) @ Module Leak Check: yes @ 0.00cu.ft.@29"hg

Orifice factor = [(Ts + 460) dH ].5 Calibrated by:

**..;.P_.R..;.._S~t.!..yl..;.e_r** ------- Date: June 11

, 1999

[

Pb .I ].5

**~ ~**  c:lmy documentslmodule calibrationsl[three point calibration.xls]a 6/11/99 11:15 **~(Q){P)V** Reviewed by: L.A. Gammie Date: June 11, 1999) Method 5 Module Calibration

Date: 11 FEB 99 Module #: 2827

Bar.

Ps., (Pb): 30.38 in. Hg Std. Meter: 570415 Pre-test

Standard Meter Module Meter

Module

Volume
Orifice Vs Setting (ft')

(in. H 2 0) 0.5 5.787

1.0 8.299

1.5 9.972

2.0 11.344

3.0 13.208 Correlation Line EQilation

Q = m (OF) + b Vs (Pb +

y = Vm IPb +

dHa Temp. Pressure Volume Temperatures

Factor Ys 1.0069 1.0069 1.0068 1.0065 1.0063 ts Ps Vm tmi

(Of) (in. H20l (ft') (Of)

71 -0.2 5.900 90

71 -0.2 8.495 95

71 -0.3 10.557 100

71 -0.3 11.729 105

71 -0.3 13.831 107

Acceptance Criteria (5 point cal.):

Y = Ratio of reading of wet test meter to dry test meter;

tolerance

for individual values +/- 0.02 from avg.

dH@ = Orifice pressure differential (in. W .C.) that equates to 0. 75

elm

of air @65degF and 29.92" Hg. Tolerance

for individual values +/- 0.20 from avg.

EL__J (Tm + 460) Ys

13.6 .d.J:L_J I Ts + 460 I

13.6 Refenmce thermo Of 70 Actual tmi OF 70 tmo (Of) 79 87 91 93 95 Error 0.00% Time Delta Module

@ Ha Flow rate

(min)

y (in. H20l Q (SCFM)

15.00 1 .011 0 1.79 0.3919

15.00 1.0178 1.72 0.5620

15.00 0.9906 1.77 0.6750

15.00 1.0191 1.82 0.7677

14.00 1.0072 1.75 0.9574

Averages 1.0091 1.77
Acceptance Criteria (post test cal.):

Perform 3 calibration runs at a single, intermediate orifice setting at the

maximum vacuum reached during test series. If Y has changed by more

than

5o/o, recalibrate meter over all live orifice settings. Thermocouple Calibration
Actual tmo I

Error Calibrated

OF By: RM Zanni

70 0.00% Date Calibrated: 14 JAN 99 OF 2.9936 4.2587 5.2371 6.0663 7.4430

(0 03!71 dH

Pb (tm + 460) !Us + 4601 @ 1'

I Vs Ys I' **~~t/)))f~t~l~~?Ili~tit~~t~~~ttttitt~i~?i\t~ttit?~it~i~~\~/{ttti~ff/f)ffi~i**

( Pb + ___dl:j_J

Q Y(17.64)Vm 13.6

(tm + 460) @

Orifice factor = fiTs+ 460) dH ].5

I Pb ].5

**~~** i

c:\my documents\deta sheets and lists\lmodcal.xls)a 2/9/99 16:12 Module Quality Control Checks

Module Cleaned:

**....~Y~e:..:s** ___ _

Pitot

Manometer Leak Check: --'yc..:e'-s

___ _

Module

Leak Check:

**--'y~e:..:s** ___ _

Calibrated by: ....:..;R::.:M.:....::Z;.:;a;.;n;.;ni:.._

_______ _

Reviewed by: LA Gammie @ @ 3.6" Hg 23.0" Hg
Date: 11 FEB 99
Date: 11 FEB 99Method 5 Module Calibration

Date: May 10,1999 Module#: 1399

Bar.

Ps

.. (Pb): 30.07 in. Hg Std. Meter: 570415 Pre-test .. · f : . ..... ·-·.::·-· .... **\,:~::::::;/ 1**  :., ; : **~j'\:v7 -....:..~:::>'lJ**  lr

Standard Meter Module Meter

Module

Volume

. Temp. Pressure Volume Temperatures Time Delta Module

Orifice . Vs Setting (ttl)

(in. H 2 0) 0.5 6.177

1.0 8.308

1.5 10.273

2.0 11.722

3.0 14.280 Correlation Line Equation

Q = m (OF) + b
Y= dHa = Vs (Pb +
Vm (Pb +

(0 0317) dH

Pb (tm + 460) (Pb Factor Ys 1.0001 1.0016 1 0.999 1.0002 ts Ps Vm tmi

(oF) (in. H 2 0) (ft3) (oF)

70 -0.1 6.238 86

70 -0.15 8.543 98

70 -0.2 10.574 100

70 -0.25 12.046 100

70 -0.3 14.640 104

Y = Ratio of reading of wettest meter to dry test meter;

tolerance for individual values +/- 0.02 from avg.

dH@ = Orifice pressure differential that equates to o. 75

cfm of air @65degf and 29.92" Hg, in. H20; tolerance

for individual values +/- 0.20 from avg.

EL-l (Tm + 460) Ys

13.6 dl:L__.J ( Ts + 460 )

13.6 ({Is + 460) @ ]2

[ Vs Ys )2

+ .....dl::L....l tmo @ Ha Flowrate

(oF) (min) y (in. H 2 0) Q (SCFM)

84 15.00 1.0169 1.60 0.4121

88 15.00 1.0135 1.74 0.5550

84

15.00 1.0077 1.72 0.6851

90

15.00 1.0124 1.75 0.7808

92

15.00 1.0189 1.76 0.9523

Averages 1.0139 1.71

Acceptance Criteria: Perform 3 calibration runs at a single, intermediate orifice setting at the

maximum vacuum reached during test series. If Y has changed by more

than

5%, recalibrate meter over all five orifice settings.

Module Quality Control Checks

Module Cleaned: ..t..y..:..es=-----

Q

Y (17.64) Vm 13.6 Pitot Manometer Leak Check: yes @ 4

(tm + 460) @ Module Leak Check: yes @ 24

Orifice factor = [(Ts + 460) dH ).5 Calibrated by PHILLIP STYLER Date: May 10,1999

[

Pb .).5

j.

**~~** Reviewed by: LEIGH GAMMIE

**~/19** Date: May 10

, 1999

c:\my documentslmodule calibrationsl(five point calibration.xlsja 5/10/99 14:36 ':!"'

! I
OF I 3.0103 4.2884 5.2475 6.0757 7.4612

# SPEI:TRH IJHSES INI:.

3434 Route 22 West • Branchburg, NJ 08876 USA Tel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 Shipped From: 80 Industrial Drive •Alpha, NJ 08865



# ~ **~============================================~~**

**~**

**~,** 

### CERTIFICATE OF ANALYSIS

CUSTOMER: SGI ORDER#: ITEM#: P.O.#: ROJAC 138485 3 VERBAL-ESTER

CERTIFICATION DATE: 12/28/98 EXPIRATION DATE: 12/28/2000

CERTIFICATION HISTORY

COMPONENT Sulfur Dioxide

BALANCE DATE OF ASSAY 12/18/98 12/28/98

Nitrogen PREVIOUS CERTIFICATION DATES: None

REFERENCE STANDARDS COMPONENT SRM/NTRM# Sulfur Dioxide NTRM-R81694

INSTRUMENTATION COMPONENT MAKE/MODEL

Sulfur Dioxide Horiba VIA-510 

### EPA PROTOCOL MIXTURE PROCEDURE # : G1

CYLINDER# : CC94697 CYLINDER PRES: 2000 PSIG CGA OUTLET: 660

MEAN CERTIFIED ANALYTICAL ACCURACY CONCENTRATION CONCENTRATION 49.36 ppm 49.31 ppm

CYLINDER#

CC53339

SERIAL#

851221093 49.3 ppm

CONCENTRATION 96.0 ppm

DETECTOR

NDIR +/-1%

CALlBRATION DATE(S) 12/18/98

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG.

**/)~_** DATE: 12/28/98 ANALYST:

__ **-:/'::.........;~:__-=------** 

# ------- FRED PIKULA



# 0000

**:~** 

# 1

# SPECTRA GASES

277 Coit St. •Irvington, NJ 07111 USA Tel.: (973) 372-2060 • {BOO) 932-0624 • Fax: {973) 372-8551 Shipped From: 80 Industrial Drive • Alpha, N.J. 08865



### CERTIFICATE OFANALYSIS

CUSTOMER: SGI ORDER#: ITEM#: P.O.#: ROJAC 132923 1 R981015

CERTIFICATION DATE: 5111/98 EXPIRATION DATE: 5/11/2000

CERTIFICATION HISTORY DATE OF COMPONENT ASSAY Sulfur Dioxide 5/4/98 5/11/98

BALANCE N1trogen

REFERENCE STANDARDS COMPONENT SRM/NTRM# Sulfur Dioxide NTRM-R81694

INSTRUMENTATION COMPONENT MAKE/MODEL

Sulfur Dioxide Horiba VIA-510 MEAN CONCENTRATION 95.18 ppm 94.98 ppm

CYLINDER#

CC53339

SERIAL#

851221093 

### EPA PROTOCOL MIXTURE PROCEDURE # : G1

CYLINDER#: CC90959 CYLINDER PRES: 2000 PSIG CGA OUTLET: 660

CERTIFIED ANALYTICAL CONCENTRATION ACCURACY 95.1 ppm +/-1%

CONCENTRATION 96.0 ppm

DETECTOR CALlBRA TION DATE(S) NDIR 4/29/98

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG.

DATE: 5/11/98 ANALYST:

__ 

## '·-~....;;.::..-.-'--~...;../2-=~:;;...~' """"""''-- FRED PIKULA 

# -------

000082

--------------------------·-·- j

# SPEl:TRH liHSES INI:.



# ~ .. 3434 Route 22 West • Branchburg, NJ 08876 USA Tel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 

# l.il Shipped From: 80 Industrial Drive •Alpha, NJ 08865



### CERTIFICATE OF ANALYSIS

CUSTOMER: SGI ORDER#: ITEM#: P.O.#: Rojac 137740 6 R98104

CERTIFICATION DATE: 11/11/98 EXPIRATION DATE: 11/11/2000

CERTIFICATION HISTORY

· DATE OF COMPONENT ASSAY Sulfur Dioxide 2/23/98 11/11/98

BALANCE Nitrogen

REFERENCE STANDARDS COMPONENT SRM/NTRM# Sulfur Dioxide GMIS-1

INSTRUMENTATION COMPONENT MAKE/MODEL

Sulfur Dioxide Horiba VIA-510 MEAN CONCENTRATION 250.7 ppm 249.9 ppm

CYLINDER#

CC85046

SERIAL#

851221093 

### EPA PROTOCOL MIXTURE PROCEDURE # : G2

CYLINDER # : CC85016 CYLINDER PRES: 2000 PSIG CGA OUTLET: 660

CERTIFIED ANALYTICAL CONCENTRATION ACCURACY 250 ppm +/-1%

CONCENTRATION 192.9 ppm

DETECTOR CALIBRATION DATE(S) NDIR 10/20/98

THIS STANDARDWAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IFTHE CYLINDER PRESSURE IS LESS THAN 150 PSIG.



### c:'l /1.

**ANALYST:_~.C~..,.~~:.-.-,,"'-4...,h:;..'../1.-=:::..==---** DATE:



## ------- 11/11/98 FRED PIKULA 

# !of)



# ~ 

# 000083

# SPEI:TRH GHSES INI:.

3434 Route 22 West • Branchburg, NJ 08876 USATel.: (908) 252-9300 •(800) 932-0624 • Fax: (908) 252-0811 Shipped From: 80 Industrial Drive •Alpha, NJ 08865



### CERTIFICATE OF ANALYSIS

CUSTOMER: SGI ORDER#: ITEM#: P.O.#: ROJAC 141252 1 981054

CERTIFICATION DATE: 3/26/99 EXPIRATION DATE: 3/25/2001

CERTIFICATION HISTORY DATE OF COMPONENT ASSAY Sulfur Dioxide 12/7/98

. 3/25/99 Nitric Oxide 12/7/98 3/25/99
NOx
Carbon Monoxide 12/7/98 3/26/99 Propane 12/8/98

BALANCE Nitrogen PREVIOUS CERTIFICATION DATES: None

REFERENCE STANDARDS COMPONENT SRM/NTRM# Sulfur Dioxide NTRM-R81694

Nitric Oxide NTRM81684 Carbon Monoxide NTRM-81679 Propane SRM-2643a

INSTRUMENTATION COMPONENT MAKE/MODEL

Sulfur Dioxide Horiba VIA-510

Nitric Oxide Teco 10 Carbon Monoxide Horiba VIA-510 Propane H. Packard 6890 

### EPA PROTOCOL MIXTURE PROCEDURE# : G1

CYLINDER # : CC94644 CYLINDER PRES: 1200 PSIG CGA OUTLET: 660

MEAN CERTIFIED ANALYTICAL CONCENTRATION CONCENTRATION ACCURACY 50.78 ppm 50.6 ppm +/-1% 50.37 ppm 50.13 ppm· 50.1 ppm +/-1% 50.12 ppm
50.2 ppm Reference Value Only 50.08 ppm 50.2 ppm +/- 1% 50.35 ppm 50.34 ppm 50.3 ppm +/- 1%

CYLINDER# CONCENTRATION

CC53353 96.0 ppm CC79984 98.6 ppm CC88660 97.4 ppm SX20148 99.1 ppm

SERIAL# DETECTOR CALIBRATION DATE(S) 851221093 NDIR 3/25/99 1 OAR-34979-249 Cheml 3/9/99

570423011 NDIR 3/12/99 US00001434 GC- FlO 11/2/98

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG.

ANALYST:.

___ 

# ~---=...P__;;_. ---- DATE: 3/26/99



# ------- FRED PIKULA

# SPEI:TRH GHSES INI:.

3434 Route 22 West • Branchburg, NJ 08876 USATel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 Shipped From: 80 Industrial Drive •Alpha, NJ 08865



### CERTIFICATE OF ANALYSIS

CUSTOMER: SGI ORDER#: ITEM#: P.O.#: ROJAC 141369 2 R991073

CERTIFICATION DATE: 4/2/99 EXPIRATION DATE: 4/2/2002

CERTIFICATION HISTORY DATE OF COMPONENT ASSAY Oxygen 4/2/99

Carbon Dioxide 4/2/99

BALANCE N1trogen PREVIOUS CERTIFICATION DATES: None

REFERENCE STANDARDS COMPONENT SRM/NTRM# Oxygen NTRM-82659X Carbon Dioxide NTRM-82745x

INSTRUMENTATION COMPONENT MAKE/MODEL

Oxygen Horiba MPA-510 Carbon Dioxide Horiba VIA-51 0 MEAN CONCENTRATION 12.01%

10.05%

CYLINDER#

CC83900 CC79944

SERIAL#

570694081 571417045 

### EPA PROTOCOL MIXTURE PROCEDURE # : G1

CYLINDER#: CC106789 CYLINDER PRES: 2000 PSIG CGA OUTLET: 590

CERTIFIED ANALYTICAL CONCENTRATION ACCURACY 12.01 % +/-1%

10.05% +/-1%

CONCENTRATION 22.80% 20.00%

DETECTOR CALIBRATION DATE(S) PM 4/2/99 NDIR 3/29/99

THIS STANDARDWAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG.

ANAL YST:

__ 

# __....;;_ao.

__ ·_.

___ _ DATE: 4/2/99



# ___ **;..;;;;...:~--** FRED PIKULA

**·----~--------** 

### ~'), 

# <V? 

# 00008S.. - 

# ~3~~~~~~rnn~~.~~~76

**~~T~;908) 252-~00**  • (800) 9320624 •



# f~ (908) 2520811 

# 1..1 Shipped From: 80 Industrial Drive •Alpha, NJ 08865



### CERTIFICATE OF ANALYSIS

CUSTOMER: SGI ORDER#: ITEM#: P.O.#: ROJAC 141369 1 R991073

CERTIFICATION DATE: 4/2/99 EXPIRATION DATE: 4/2/2002

CERTIFICATION HISTORY DATE OF COMPONENT ASSAY Oxygen 4/2/99

Carbon Dioxide 4/2/99

BALANCE N1trogen PREVIOUS CERTIFICATION DATES: None

REFERENCE STANDARDS COMPONENT SRM/NTRM# Oxygen NTRM-82659X Carbon Dioxide NTRM-82745x

INSTRUMENTATION COMPONENT MAKE/MODEL
Oxygen Horiba MPA-510 Carbon Dioxide Horiba VIA-510 MEAN CONCENTRATION 20.9%

18.01%

CYLINDER#

CC83900 CC79944

SERIAL#

570694081 571417045 

### EPA PROTOCOL MIXTURE PROCEDURE # : G1

CYLINDER#: CC106813 CYLINDER PRES: 2000 PSIG CGA OUTLET: 590

CERTIFIED ANALYTICAL CONCENTRATION ACCURACY 20.9% +/-1%

18.01% +/- 1%

CONCENTRATION 22.80% 20.00%

DETECTOR CALIBRATION DATE(S) PM 4/2/99 NDIR 3/29/99

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG.

DATE: 4/2/99



# ------- ANALYST:

___



# ~_-



# p?

__ -___ _ FRED PIKULA


# oooosr:; 

# -----------------------------···----···

### AppendixF
LaboratoryAnalytical Data

RBKF9903 KF Tunnel Kiln Final Report 

### ,. ROJAC AIRTESTING 

# I SERVICES, INC.

# f5§111ij

PHILIP SERVICES



## INORGANICDATA PACKAGE FOR ROJAC AIRTESTING SERVICES INC. Project#RBKF9903



### Philip Analytical Services Corporation 5555 Nortb ServiceRoad Burlington, ON L7L 5H7

Submission#: 9F0571
Prepared by: JaniceJoseph- CSR Approvedby : Dr. RonMcLeod

- Principal Scientist

P!tlt.IP

**A~,-.J_,**
**;J~** ... \I. St-:K\ If:r:.

... c(

**),~,**.•_.,l·\Tioi': 

# 000088

# 00001

1. CASE NARRATIVE

f\ 1"\ 1"1 f'\ 

## "r.PROJECTNARRATIVE

PHILIPAnalytical Services (Burlington ON) Philip Project: AN990616. Philip Submission#:9F0571

Client: Rojac AirTesting Services ClientProject: RBKF9903

I. SAMPLERECEIPT/ANALYSIS

a) SampleListing

Philip

ID Client SampleiD Date Date Sampled Received

Fluoride via Probe

031859 99 Method Blank 99/06/11 99/06/15 03186099 M26-1 99/06111 99/06115 03186199 M26-2 99/06111 99/06/15 031862 99 M26-3 99/06/11 99/06115 031863 99 M26-4 99/06/11 99/06115 Hydrogen Fluoride via EPAMethod26A

031859 99 MethodBlank 99/06/11 99/06/15 031860 99 M26-1 99/06111 99/06115 031861 99 M26-2 99/06/11 99/06/15 031862 99 M26-3 99/06111 99/06/15 031863 99 M26-4 99/06/11 99/06/15 Hydrogen Chloride viaEPA Method26A

031859 99 Method Blank 99/06111 99/06/15 031860 99 M26-1 99/06111 99/06/15 031861 99 M26-2 99/06/11 99/06/15 031862 99 M26-3 99/06/11 99106115 031863 99 M26-4 99/06/11 99/06/15 Date Prepped

99/07/13 99/07/13 99/07/13 99/07/13 99/07/13

99/06/21 99/06/21 99/06/21 99/06/21 99/06/21

99/06/21 99/06/21 99/06/21 99/06/21 99/06/21 Run Date

99/07/13 99/07/13 99/07/13 99/07/13 99/07/13

99/06/21 99/06/21 99/06/21 99/06/21 99/06/21

99/06/21 99/06/21 99/06/21 99/06/21 99/06/21 

# 00002

Run Dateis defmed as the date ofinjection ofthe last calibration standard (12 hour orless) priorto the samplesanalyzed within that run sequence. Therefore the time ofcalibration injection that defines the
run date is always within 12 hours ofthe time ofsample injection.

b) Shipping Problems: none encountered

c) DocumentationProblems: none encountered

II. SAMPLEPREP:

Noproblems encounteredIII. SAMPLE ANALYSIS:

Fluroide analysis via ion chromatography (IC

- M26A) on these samples showed the presence of significant interference. Therefore the samples were also analyzed for fluroide via selected ion electrode. We believe that these dataprovide interference free fluoride levels in the samples.

See also comments within the appropriate Certificate ofAnalysis.

a) Hold Times: all within recommended hold times

b) Instrument Calibration: all within control limits

I certifythat this data package is in compliance with the terms and conditions ofthe contract, both technically and for completeness, for otherthan the conditions detailed above. 

# 00003

In addition, I certify, that to the best ofmy knowledge and belief, the data as reported are true and accurate. Release ofthe data contained in this data package has been authorizedby the cognizant laboratory official or his/her designee, as verifiedbythis signature.

Date

# 00004

2. CERTIFICATE OFANALYSIS



## flOOOQ?

# OUDOS

Certificate of Analysis

CLIENTINFORMATION LABORATORY INFORMATION

Attention: ClientName: Project: ProjectDesc:

Address:

Fax Number: Leigh Gammie Rojac AirTesting Services RBKF9903 Stack Emissions

120 MountainAvenue Bloomfield, CT 6002 860-243-9801 Contact: Ron McLeod Project: AN990616 Date Received: 99/06/15 DateReported: 99/07/21

Submission No.: 9F0571 SampleNo.: 031859-031863

PhoneNumber: 860-243-9800

NOTES: "-'=not analysed '<'=less thanMethodDetection Limit (l.tDL) 'NA' =nodata available LOQcan bydetermined for allanalytes bymultiplying the appropriateMDLX 3.33 Solids data is basedon dry weight except for biota analyses. Organicanalyses arenotcorrected for extraction recoverystandards except for isotope dilution methods, (i.e. CARB429PAH, allPCDDIFandDBDIDBFanalyses)

Methods used by PASC are based upon those found in 'Standard Methods for the Examination

**ofWa~er** and Wastewater', Nineteenth Edition. Other methods are based on the principles ofMISA orEPA methodologies. New York State: ELAP Identification Number 10756.

All work recorded herein has been done in accordance with normal professional standards using accepted testing methodologies, quality assurance and quality control procedures except where otherwise agreed to by the client and testing company in writing. Any and all use ofthese test results shall be limited to the actual cost ofthe pertinent analysis done. There is no otherwarranty expressed or implied. Your sampleswill be retained at PASC for aperiod ofthree weeks from receipt ofdata or as per contract.

COMMENTS:

*Matrix interference



### Certifiedby:

# ki1

**_{Y\J~** Page 1 

# 0000930 0 0 0 w **~** 7/20/99 Clie11tiD: Lab No.: Date Sampled:
Component MDL

Impinger volume measured Fluoride via Probe 5.0

Hydrogen Fluoride- method 26 50.0

Hydrogen Chloride- method 26A 100

**~__£)** - Method Blank 031859 99

- Units ml -

ug <

ug <

II < PASC- Certificate of Analysis

Blank Blank Blank Blank

Spike #I Spike #I Spike #2 Spike #2

031859 99 031859 99 031859 99 031859 99

- - - -

%

Recoveries % Recoveries

- - - -

- - - -

200 96 200 96

330 110 330 110 Page 2 of4

M26-l M26-l 031860 99 031860 99 9910611 I 99/06/11 Duplicate

200 730 740 <1000* <1000* 28000 28000 Client:Rojac Air Testing Services Project:RBKF9903 a a 0 CJ 0\0 0 0 0 :..0 :'Ji 7120199 Cliellt ID: Lab No.: Date Sampled:
Component MDL

lmpinger volume measured Fluoride via Probe 5.0

Hydrogen Fluoride • method 26 50.0

Hydrogen Chloride- method 26A 100

**~~** M26-l 031860 99 99/06111 Units M. Spike

ml -

ug 840

ug 13000

" 42000 PASC- Certificate of Analysis M26-l M26-l M26-l M26-2

031860 99 031860 99 031860 99 031861 99

99/06/11 99/06111 99/06111 99/06/11

MS %Rec. MS Dup MSD%Rec. - - - 180

110 - - 470

96 13000 95 <1000*

96 42000 92 23000 Page 3 of4

M26-3 M26-4 031862 99 031863 99 99/06111 99106111

150 130

360 < <1000* <250* 24000 < Client:Rojac Air Testing Services Project:RBKF9903 0 0 0 0 "-l

# 00008 7120199 

## PASC- Summaryof AnalysisPre. Dates PageMS-4 of4

Batch Code: Fluoridevia Probe

Run Date: Date ofSamplePrep:

Batch Code: Hydrogen Fluoride

- method 26

Run Date: Date ofSample Prep:

Batch Code: Hydrogen Chloride

- method 26A

Run Date: Date ofSample Prep: 0713IGA2 031859 99 031860 99 031861 99 031862 99 031863 99 99/07/13 99/07/13

062IASAI 031859 99 031860 99 03186199 031862 99 031863 99 99/06/21 99/06/21

062IASAI 031859 99 031860 99 031861 99 031862 99 031863 99 99/06/21 99/06/21

Client:Rojac AirTesting Services Project:RBKF9903 

# nnnn<1r: