Instructionsfor completing the Fuel Material AnalysisInformation

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony,beryllium, cadmium, chromium,cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facilitybut is designed to allow multiple (up to 4) fuel analyses at that specificboiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets.Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Pleasename each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).

Pleaserefer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet. 2. Please enter the test date on the Boiler Informationworksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet.For example:"ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet(orange tab). If the units

measurethat you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choosethe units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 compositesamples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony,beryllium, cadmium, chromium,cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facilitybut is designed to allow multiple (up to 4) fuel analyses at that specificboiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet.

down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet.For example:"ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet(orange tab). If the unitsof

measurethat you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choosethe units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 compositesamples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

715 McManus Unit 1 No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description No.6 Fuel Oil (residual or bunker C)EIA

Facility CodeFacility Name Boiler IDBasis Analyte

715McManus Unit 1 As Received Higher Heating Value 715McManus Unit 1 As Received % Moisture 715McManus Unit 1 As Received % Ash 715McManus Unit 1 As Received % Sulfur 715McManus Unit 1 Dry basis Higher Heating Value 715McManus Unit 1 Dry basis % Ash 715McManus Unit 1 Dry basis % Sulfur 715McManus Unit 1 Dry basis Antimony 715McManus Unit 1 Dry basis Arsenic 715McManus Unit 1 Dry basis Beryllium 715McManus Unit 1 Dry basis Cadmium 715McManus Unit 1 Dry basis Chlorine 715McManus Unit 1 Dry basis Chromium 715McManus Unit 1 Dry basis Cobalt 715McManus Unit 1 Dry basis Fluorine 715McManus Unit 1 Dry basis Lead 715McManus Unit 1 Dry basis Manganese 715McManus Unit 1 Dry basis Mercury 715McManus Unit 1 Dry basis Nickel 715McManus Unit 1 Dry basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D95 ASTM D482 ASTM D4294 ASTM D5865 corrected for moisture ASTM D482 corrected for moisture ASTM D4294 corrected for moisture EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010B EPA SW-846-6010BEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 715McManus Unit 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY)Higher Heating Value (HHV) (as received) HHV Units 1 4/7/2010 4/7/2010 18280 Btu/lb 2 4/7/2010 4/7/2010 18205 Btu/lb 3 4/7/2010 4/7/2010 18293 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.3 0.074 1.90 18335 Btu/lb 0.074 1.90 0.3 0.028 1.89 18260 Btu/lb 0.028 1.89 0.3 0.049 1.9 18348 Btu/lb 0.049 1.90Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 15.346 mg/L 116.349 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.651 16.048 mg/L 105.316 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.465 14.845 mg/L 100.301 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.599Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead UnitsManganese (Dry Basis)Manganese

Units mg/Kg <0.07 mg/Kg <0.07 mg/Kg <0.17 mg/Kg 0.273 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.268 mg/Kg 0.312 mg/Kg mg/Kg <0.07 mg/Kg 0.169 mg/Kg <0.17 mg/Kg 0.272 mg/KgNickel (Dry

Basis) Nickel UnitsSelenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 27.081 mg/Kg <0.7 mg/Kg 4.112mg/L 0.478 mg/Kg 0.3 19.358 mg/Kg <0.7 mg/Kg 3.611mg/L 0.346 mg/Kg 0.3 26.379 mg/Kg <0.7 mg/Kg 3.009mg/L 0.451 mg/Kg 0.3 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

0.074 88.48 10.291 <0.75 1.906 0.028 84.68 10.411 <0.75 1.896 0.049 86.38 10.451 <0.75 1.906 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

<0.75 2.231 <0.75EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 715McManus Unit 1 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 1 4/8/2010 4/8/2010 18276 Btu/lb 2 4/8/2010 4/8/2010 18254 Btu/lb 1 4/11/2010 4/11/2010 18199 Btu/lb 2 4/11/2010 4/11/2010 18271 Btu/lb 3 4/11/2010 4/11/2010 18278 Btu/lb 1 4/12/2010 4/12/2010 18214 Btu/lb 2 4/12/2010 4/12/2010 18290 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.4 0.049 1.9 18349 Btu/lb 0.049 1.90 0.3 0.043 1.9 18309 Btu/lb 0.043 1.90 0.5 0.042 1.89 18290 Btu/lb 0.042 1.89 0.4 0.051 1.9 18344 Btu/lb 0.051 1.90 0.5 0.05 1.9 18370 Btu/lb 0.050 1.90 0.4 0.056 1.9 18287 Btu/lb 0.056 1.90 0.5 0.053 1.9 18382 Btu/lb 0.053 1.90Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 17.6 mg/L 96.4 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.5 12.7 mg/L 103.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 17.6 mg/L 74.4 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 16.0 mg/L 38.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.5 11.8 mg/L 123.6 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 12.2 mg/L 86.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 12.2 mg/L 62.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.8Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead UnitsManganese (Dry Basis)Manganese

Units mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg 1.6 mg/Kg <0.17 mg/Kg 0.6 mg/Kg mg/Kg <0.07 mg/Kg 0.2 mg/Kg 1.4 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 1.0 mg/Kg 0.4 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.2 mg/KgNickel (Dry

Basis) Nickel UnitsSelenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 19.8 mg/Kg <0.7 mg/Kg 3.8 mg/L 0.3 mg/Kg 29.7 mg/Kg <0.7 mg/Kg 3.5 mg/L 0.5 mg/Kg 28.6 mg/Kg <0.7 mg/Kg 3.9 mg/L 0.5 mg/Kg 18.2 mg/Kg <0.7 mg/Kg 3.7 mg/L 0.3 mg/Kg 23.6 mg/Kg <0.7 mg/Kg 3.2 mg/L 0.4 mg/Kg 28.5 mg/Kg <0.7 mg/Kg 3.5 mg/L 0.8 mg/Kg 34.5 mg/Kg <0.7 mg/Kg 3.4 mg/L 0.6 mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 0.4 0.049 87.25 10.422 <0.75 1.92 0.3 0.043 86.06 10.401 <0.75 1.92 0.5 0.042 86.08 10.503 <0.75 1.90 0.4 0.051 86.44 10.432 <0.75 1.91 0.5 0.050 86.70 10.603 <0.75 1.91 0.4 0.056 86.79 10.643 <0.75 1.91 0.5 0.053 86.55 10.553 <0.75 1.91 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75EIA

Facility Code Facility

Name Boiler IDHAPs Test Group 715McManus Unit 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/6/2010 4/6/2010 18276 Btu/lb 2 4/6/2010 4/6/2010 18232 Btu/lb 3 4/6/2010 4/6/2010 18333 Btu/lb 1 4/8/2010 4/8/2010 18276 Btu/lb 2 4/8/2010 4/8/2010 18254 Btu/lb 1 4/11/2010 4/11/2010 18199 Btu/lb 2 4/11/2010 4/11/2010 18271 Btu/lb 3 4/11/2010 4/11/2010 18278 Btu/lb 1 4/13/2010 4/13/2010 18239 Btu/lb 2 4/13/2010 4/13/2010 18249 Btu/lb 3 4/13/2010 4/13/2010 18229 Btu/lb 1 4/14/2010 4/14/2010 18260 Btu/lb 2 4/14/2010 4/14/2010 18288 Btu/lb 3 4/14/2010 4/14/2010 18229 Btu/lb 4 4/14/2010 4/14/2010 18223 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.4 0.05 1.88 18349 Btu/lb 0.050 1.88 0.3 0.047 1.89 18287 Btu/lb 0.047 1.89 0.2 0.041 1.91 18370 Btu/lb 0.041 1.91 0.4 0.049 1.9 18349 Btu/lb 0.049 1.90 0.3 0.043 1.9 18309 Btu/lb 0.043 1.90 0.5 0.042 1.89 18290 Btu/lb 0.042 1.89 0.4 0.051 1.9 18344 Btu/lb 0.051 1.90 0.5 0.05 1.9 18370 Btu/lb 0.050 1.90 0.4 0.049 1.9 18312 Btu/lb 0.049 1.90 0.4 0.05 1.9 18322 Btu/lb 0.050 1.90 0.2 0.051 1.9 18266 Btu/lb 0.051 1.90 0.5 0.048 1.86 18352 Btu/lb 0.048 1.86 0.5 0.038 1.89 18380 Btu/lb 0.038 1.89 0.3 0.066 1.88 18284 Btu/lb 0.066 1.88 0.4 0.059 1.9 18296 Btu/lb 0.059 1.90Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 15.3 mg/L 62.2 mg/Kg 1.0 mg/Kg <0.7 mg/Kg <0.07 14.9 mg/L 76.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.4 15.5 mg/L 88.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.4 17.6 mg/L 96.4 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.5 12.7 mg/L 103.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 17.6 mg/L 74.4 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 16.0 mg/L 38.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.5 11.8 mg/L 123.6 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 15.9 mg/L 64.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.8 13.0 mg/L 65.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 31.5 mg/L 42.1 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 18.6 mg/L 91.5 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 15.9 mg/L 80.4 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.8 16.0 mg/L 61.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 19.2 mg/L 47.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.8Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead UnitsManganese (Dry Basis)Manganese

Units mg/Kg <0.07 mg/Kg 2.7 mg/Kg <0.17 mg/Kg 0.3 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg 1.6 mg/Kg <0.17 mg/Kg 0.6 mg/Kg mg/Kg <0.07 mg/Kg 0.2 mg/Kg 1.4 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.4 mg/Kg 0.4 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.3 mg/Kg mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg 1.4 mg/Kg 0.5 mg/Kg 0.5 mg/Kg mg/Kg <0.07 mg/Kg 0.7 mg/Kg 0.3 mg/Kg 0.6 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.8 mg/Kg 0.3 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.4 mg/Kg 0.3 mg/KgNickel (Dry

Basis) Nickel UnitsSelenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 2.6 mg/Kg <0.7 mg/Kg 3.9 mg/L <0.07 mg/Kg 0.4 16.4 mg/Kg <0.7 mg/Kg 3.6 mg/L 0.3 mg/Kg 0.3 19.0 mg/Kg <0.7 mg/Kg 3.4 mg/L 0.7 mg/Kg 0.2 19.8 mg/Kg <0.7 mg/Kg 3.8 mg/L 0.3 mg/Kg 0.4 29.7 mg/Kg <0.7 mg/Kg 3.5 mg/L 0.5 mg/Kg 0.3 28.6 mg/Kg <0.7 mg/Kg 3.9 mg/L 0.5 mg/Kg 0.5 18.2 mg/Kg <0.7 mg/Kg 3.7 mg/L 0.3 mg/Kg 0.4 23.6 mg/Kg <0.7 mg/Kg 3.2 mg/L 0.4 mg/Kg 0.5 34.8 mg/Kg <0.7 mg/Kg 3.4 mg/L 0.6 mg/Kg 0.4 32.3 mg/Kg <0.7 mg/Kg 3.5 mg/L 0.5 mg/Kg 0.4 32.5 mg/Kg <0.7 mg/Kg 4.3 mg/L 0.7 mg/Kg 0.2 32.4 mg/Kg <0.7 mg/Kg 4.1 mg/L 0.6 mg/Kg 0.5 335.0 mg/Kg <0.7 mg/Kg 3.8 mg/L 0.6 mg/Kg 0.5 31.1 mg/Kg <0.7 mg/Kg 4.1 mg/L 0.7 mg/Kg 0.3 34.4 mg/Kg <0.7 mg/Kg 3.8 mg/L 0.7 mg/Kg 0.4 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed CarbonCarbon Hydrogen Nitrogen Total Sulfur Oxygen

0.050 85.23 10.502 <0.75 1.89 1.579 0.047 85.54 10.542 <0.75 1.90 1.229 0.041 87.42 10.411 <0.75 1.91 <0.75 0.049 87.25 10.422 <0.75 1.92 <0.75 0.043 86.06 10.401 <0.75 1.92 <0.75 0.042 86.08 10.503 <0.75 1.90 <0.75 0.051 86.44 10.432 <0.75 1.91 <0.75 0.050 86.70 10.603 <0.75 1.91 <0.75 0.049 87.11 10.482 <0.75 1.91 <0.75 0.050 86.40 10.512 <0.75 1.91 <0.75 0.051 86.07 10.431 <0.75 1.90 <0.75 0.048 86.54 10.673 <0.75 1.87 <0.75 0.038 86.04 10.643 <0.75 1.90 <0.75 0.066 87.04 10.642 <0.75 1.89 <0.75 0.059 86.53 10.542 <0.75 1.91 <0.75 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 715McManus Unit 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 4/6/2010 4/6/2010 18276 Btu/lb 2 4/6/2010 4/6/2010 18232 Btu/lb 3 4/6/2010 4/6/2010 18333 Btu/lb 1 4/7/2010 4/7/2010 18280 Btu/lb 2 4/7/2010 4/7/2010 18205 Btu/lb 3 4/7/2010 4/7/2010 18293 Btu/lb 1 4/11/2010 4/11/2010 18199 Btu/lb 2 4/11/2010 4/11/2010 18271 Btu/lb 3 4/11/2010 4/11/2010 18278 Btu/lb 1 4/12/2010 4/12/2010 18214 Btu/lb 2 4/12/2010 4/12/2010 18290 Btu/lb 1 4/13/2010 4/13/2010 18239 Btu/lb 2 4/13/2010 4/13/2010 18249 Btu/lb 3 4/13/2010 4/13/2010 18229 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.4 0.05 1.88 18349 Btu/lb 0.050 1.88 0.3 0.047 1.89 18287 Btu/lb 0.047 1.89 0.2 0.041 1.91 18370 Btu/lb 0.041 1.91 0.3 0.074 1.90 18335 Btu/lb 0.074 1.90 0.3 0.028 1.89 18260 Btu/lb 0.028 1.89 0.3 0.049 1.9 18348 Btu/lb 0.049 1.90 0.5 0.042 1.89 18290 Btu/lb 0.042 1.89 0.4 0.051 1.9 18344 Btu/lb 0.051 1.90 0.5 0.05 1.9 18370 Btu/lb 0.050 1.90 0.4 0.056 1.9 18287 Btu/lb 0.056 1.90 0.5 0.053 1.9 18382 Btu/lb 0.053 1.90 0.4 0.049 1.9 18312 Btu/lb 0.049 1.90 0.4 0.05 1.9 18322 Btu/lb 0.050 1.90 0.2 0.051 1.9 18266 Btu/lb 0.051 1.90Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 15.3 mg/L 62.2 mg/Kg 1.0 mg/Kg <0.7 mg/Kg <0.07 14.9 mg/L 76.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.4 15.5 mg/L 88.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.4 15.346 mg/L 116.349 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.651 16.048 mg/L 105.316 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.465 14.845 mg/L 100.301 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.599 17.6 mg/L 74.4 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 16.0 mg/L 38.2 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.5 11.8 mg/L 123.6 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 12.2 mg/L 86.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.6 12.2 mg/L 62.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.8 15.9 mg/L 64.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.8 13.0 mg/L 65.3 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7 31.5 mg/L 42.1 mg/Kg <0.35 mg/Kg <0.7 mg/Kg 0.7Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)Chromium

Units Lead (Dry

Basis) Lead UnitsManganese (Dry Basis)Manganese

Units mg/Kg <0.07 mg/Kg 2.7 mg/Kg <0.17 mg/Kg 0.3 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg <0.17 mg/Kg 0.273 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.268 mg/Kg 0.312 mg/Kg mg/Kg <0.07 mg/Kg 0.169 mg/Kg <0.17 mg/Kg 0.272 mg/Kg mg/Kg <0.07 mg/Kg 0.2 mg/Kg 1.4 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 1.0 mg/Kg 0.4 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.2 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.4 mg/Kg 0.4 mg/Kg mg/Kg <0.07 mg/Kg <0.07 mg/Kg 0.2 mg/Kg 0.3 mg/Kg mg/Kg <0.07 mg/Kg 0.3 mg/Kg 0.2 mg/Kg 0.2 mg/KgNickel (Dry

Basis) Nickel UnitsSelenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 2.6 mg/Kg <0.7 mg/Kg 3.9 mg/L <0.07 mg/Kg 0.4 16.4 mg/Kg <0.7 mg/Kg 3.6 mg/L 0.3 mg/Kg 0.3 19.0 mg/Kg <0.7 mg/Kg 3.4 mg/L 0.7 mg/Kg 0.2 27.081 mg/Kg <0.7 mg/Kg 4.112 mg/L 0.478 mg/Kg 0.3 19.358 mg/Kg <0.7 mg/Kg 3.611 mg/L 0.346 mg/Kg 0.3 26.379 mg/Kg <0.7 mg/Kg 3.009 mg/L 0.451 mg/Kg 0.3 28.6 mg/Kg <0.7 mg/Kg 3.9 mg/L 0.5 mg/Kg 0.5 18.2 mg/Kg <0.7 mg/Kg 3.7 mg/L 0.3 mg/Kg 0.4 23.6 mg/Kg <0.7 mg/Kg 3.2 mg/L 0.4 mg/Kg 0.5 28.5 mg/Kg <0.7 mg/Kg 3.5 mg/L 0.8 mg/Kg 0.4 34.5 mg/Kg <0.7 mg/Kg 3.4 mg/L 0.6 mg/Kg 0.5 34.8 mg/Kg <0.7 mg/Kg 3.4 mg/L 0.6 mg/Kg 0.4 32.3 mg/Kg <0.7 mg/Kg 3.5 mg/L 0.5 mg/Kg 0.4 32.5 mg/Kg <0.7 mg/Kg 4.3 mg/L 0.7 mg/Kg 0.2 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

0.050 85.23 10.502 <0.75 1.89 1.579 0.047 85.54 10.542 <0.75 1.90 1.229 0.041 87.42 10.411 <0.75 1.91 <0.75 0.074 88.48 10.291 <0.75 1.906 <0.75 0.028 84.68 10.411 <0.75 1.896 2.231 0.049 86.38 10.451 <0.75 1.906 <0.75 0.042 86.08 10.503 <0.75 1.90 <0.75 0.051 86.44 10.432 <0.75 1.91 <0.75 0.050 86.70 10.603 <0.75 1.91 <0.75 0.056 86.79 10.643 <0.75 1.91 <0.75 0.053 86.55 10.553 <0.75 1.91 <0.75 0.049 87.11 10.482 <0.75 1.91 <0.75 0.050 86.40 10.512 <0.75 1.91 <0.75 0.051 86.07 10.431 <0.75 1.90 <0.75 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bituminous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to theorangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm mg/L