ft 6^1/2. 77-I32S

CONTAINER

BOARD

report no. 96

September 1977

NBS Collaborative Reference Fourdrinier Kraft Board Group

Program for Containerboard American Paper Institute, Inc. and U.S. Department of

Commerce, National Bureau

of Standards
NBS COLLABORATIVE REFERENCE PROGRAMS

i 'APPI Paper and Board (6 times per year)

Bursting strength

Tearing strength

Tensile breaking strength

Elongation to break

Tensile energy absorption

Folding endurance

Stiffness

Air resistance

Grammage

Smoothness

Surface pick strength

K & N ink absorption

PH

Opacity

Blue reflectance (brightness)

Specular gloss, 75°

Thickness

Concora (flat crush)

Ring crush

FKBG-API Containerboard (48 times per year)

Mullen burst of linerboard

Concora test of medium

MCCA Color and Appearance (4 times per year)

Gloss at 60°

Color and color difference

Retroref lect ivity

Rubber (4 times per year)

Tensile strength, ultimate elongation and tensile stress

Hardness

Mooney viscosity

Vulcanization properties

ASTM Textiles (3 times per year)

Flammability (FF3-71 and FF5-74)

ASTM Cement (2 times per year)

Chemical (11 chemical components)

Physical (8 characteristics)

AASHTO Bituminous

Asphalt cement (2 times per year)

Cutbacks (once a year)

let

saafl

Collaborative Reference Programs

B360 Polymer Building

National Bureau of Standards

Washington, D.C. 20234

Rev. 4/77
CONTAINER

BOARD

Collaborative Reference

Program for

Containerboard

report no. 96

September 1977

E.B. Randall, Jr., J. Horlick

Laboratory Evaluation Technology

Section, Standards Application

and Analysis Division, Institute for

Applied Technology

R.G. Powell

NBS Research Associate

Collaborative Testing

Services, Inc.

U.S. Department of Commerce, Fourdrinier Kraft Board Group

National Bureau of Standards American Paper Institute, Inc.

Introduction

The Collaborative Reference Program for Containerboard is sponsored

by the Fourdrinier Kraft Board Group (FKBG) of the American Insititute

of Paper, Inc., with the cooperation of the Techrical Association of

the Pulp and Paper Industry (TAPPIj and the Collaborative Testing

Services, Inc. In this program, samples of three weights of linerboard, nominally 26 lb, 42 lb, and 69 lb and of corrugating medium

(26 It) are randomized separately from uniform narrow rolls and

packaged for distribution to the participants. Each month, sufficient

test material for four weekly tests, the material for each consisting

of 20 test pieces of 42 lb board and 20 test pieces of 26 or 69 lb

board, the latter in alternate months, is mailed to participants for

Mullen bursting strength, or for each week five sheets of corrugating

medium, each sheet for four tests of Concora flat crush strength.

The participants return their test results to NBS for analysis and

receive two monthly reports from NBS: a "preliminary" (individualized

report) comparing a laboratory's results with the industrial mean,

and a longer report (as illustrated by this report) showing the data

from all participants.

Comments Regarding Report No. 96

Beginning with Report No. 88 (January 1977), Concora medium data and

Mullen linerboard data appear in the same combined report.

Edwin B. Randall, Jr., Administrator

Collaborative Reference Programs

Laboratory Evaluation Technology Section

(301) 921-2946

November 4, 1977
'

hf . 4

'

.

•
TABLE OF CONTENTS

Page

1

4

5

6

8

10

12

Explanation of Tables

Instrument Codes

Use of Average Mean as a Reference Standard

Bursting Strength, Linerboard 42H4, weeks 1-4

Bursting Strength, Linerboard 6913, week 1

Bursting Strength, Linerboard 6914, weeks 2-4

Concora Flat Crush, Corrugating Medium 26C2

EXPLANATION OF TABLES

Each table shows laboratory test results for Mullen bursting strength

of linerboard or Concora flat crush strength of corrugating medium.

The data are divided into three time spans. On the left of each table

is an analysis for each week of the month. In t Tie center is cumulative

data for the month and on the right is cumulative data for up to 16

weeks.

Conservative statistical tests have been used in excluding extreme

data from the analyses. Thus, where the mean (average) for one laboratory is compared with the average for many laboratories, limits have

been used that would exclude only one laboratory in a hundred if all

laboratories followed exactly the same testing procedure. Consequently,

laboratories receiving "X" flags should review their testing procedures,

instrument calibration, and control processes. Similar conservative

criteria were used in flagging within- laboratory standard deviations

and other statistics.

lab means this month

WEEKLY VALUES : CODE V WK-1 WK-2 WK-3 WK-4

LAB CODE - Confidential laboratory identification number known only to the

participant and the Collaborative Reference Program staff.

V - Code for indicating instrument type, units used, and any other

variation in test procedure or conditions. A '+' in this column

means a non-standard variation. Data marked '+' are not included

in the combined averages for all laboratories, (see page 4).

MEANS THIS MONTH - For each laboratory each weekly mean is the average of

individual test determinations, usually an average of 20

determinations

FLAGS (following means and standard deviations) -

X - Data excluded from an AV MEAN or average standard deviation

because value deviated from the AV MEAN or average standard

deviation by more than 2.576 times the appropriate standard

deviation. A laboratory following the prescribed test method

could obtain such an extreme value by chance only one time in

a hundred. Corrective action is almost certainly required .

* _ Data included in the CUMULATIVE AV MEAN but the value deviated

from this mean by more than 1.960 and less that 2.576 times the

SD CUM MEAN. A laboratory following the prescribed test method

could obtain such an extreme value by chance only one time in

twenty. Corrective action may be desired.

1
AV MEAN -

SDR -

AV SDR -

SD LABS -

NO. INCL

NO. OMIT

NOT RCD -

SD SHTS -

This is a warning to the laboratory but does not affect inclusion

or exclusion of the laboratory's results from the corresponding

AV MEAN. This flag indicates an extremely high or low within-laboratory standard deviation (SDR, not shown) that could occur by

chance only one time in a hundred if the laboratory is following

the prescribed test method.

(at bottom of table) - The average for the indicated week of the means for all laboratories, except those laboratories marked '+' in column V and those means marked with an 'X'.

(not shown) - The standard deviation of within-laboratory measurements; i.e., the Standard Deviation of the Replicate measurements

made at one time in one laboratory on one package of test pieces.

The average for the indicated week of the SDR's of all the laboratories, except those omitted from the AV MEAN. Also an extremely

high or low SDR as compared with the AV SDR based on the remaining

laboratories is omitted from the AV SDR and the letter 'S' is

placed after the laboratory mean for that week. The AV SDR is an index of the within-laboratory precision for repeated measurements;

i.e., a measure of the ability of an average laboratory to repeat

its results over a short period of time. It includes measurement

error and sample variation.

For each week the standard deviation of the means about the AV MEAN

for that week after omitting those means marked with an 'X' or noted '+' in column V. The SD LABS is an index of the among- labora

tory precision of the test method as applied by the participating

laboratories; i.e., a measure of the ability of laboratories to get

comparable results.

The number of laboratory means included in the AV MEAN for that

week

.

The number of laboratory means reported but omitted from AV MEAN

because of non-standard equipment, environment or procedure ('+' in

column V) or because of extreme results (X following mean).

The number of laboratories failing to report data on time or in

usable form for this week (but who reported data for at least one of the other weeks of this month) , or who received test pieces

from a different sample of material and whose data therefore are shown in another table of this report.

(Concora only) The average for the indicated week of the amongsheet within-laboratory standard deviations. The SD SHTS is an index primarily of the variability among sheets.

2
THIS MONTH

VALUES THIS MONTH: MEAN SDR SDWKS

MEAN - The average for the indicated laboratory of the reported weekly

MEANS THIS MONTH.

SDR - The average for the indicated laboratory of the weekly SDRs for

the current month.

SDWKS - For the indicated laboratory, the standard deviation among the

laboratory's weekly MEANS THIS MONTH (including those means marked with an 'X' )

CUMULATIVE

CUMULATIVE VALUES : MEAN SDR SDWKS WKS

MEAN - The average for the indicated laboratory of all its weekly means

for the number of weeks indicated, including those for the current

month. An or 'X' following this CUMULATIVE MEAN indicates the

laboratory is running consistently low or high. (See above for

explanation of these flags)

SDR - The average for the indicated laboratory of the weekly SDRs for

the indicated number of weeks.

SDWKS - For the indicated laboratory, the standard deviation among the

laboratory's weekly means (including those means marked with an

'X'). SDWKS is an index of the week to week precision; i.e., a measure of the ability of a laboratory to repeat its results from

week to week.

WKS - Number of weeks for which usable results have been reported by

that laboratory. At most, 16 weeks of data are included.

GRAND AVERAGES

GRAND AVERAGES : THIS MONTH CUMULATIVE 12 WEEKS

THIS MONTH - Averages for the four weeks of the quantities shown to the left.

CUMULATIVE - Averages for the indicated number of weeks, including the four

weeks of the current month.

3
AV SDWKS - The average of the SDWKS for all laboratories excluding those

marked ' + ' in column V or with an 'X' following the corre- sponding THIS MONTH or CUMULATIVE MEAN or SDWKS.

SD CUM MEAN - The larger of either (1) the standard deviation of the

CUMULATIVE MEANS about the average CUMULATIVE MEAN after

omitting those CUMULATIVE MEANS marked with an 'X' or with

a '+' in column V, or (2) the CUMULATIVE SD LABS divided by

the square root of the number of weeks cumulated. The

former will be appreciably larger than the latter only when

there are persistent systematic differences among the

laboratories

.

INSTRUMENT CODES

FOR

MULLEN BURST TESTERS

(Column V)

CODE DESCRIPTION

A Unknown Model, assumed to be Model AH,

Hydraulic Clamp

B Model A, Air Operated Clamp

C Model A, Hand Operated Clamp

D Model AH, with Pressure Transducer

E Model A, Converted to AH

F Model AH, Hydraulic Clamp

G Model A, Hydraulic Clamp

Z Unknown Model, Please Describe Instrument

Make and Model

If an incorrect instrument code has been assigned to your laboratory,

please inform us.

4
Use of Average Mean as a Reference Standard

A la:'ge supply of ] inerboard in three weights was randomized and placed

in sealed packages ready for shipment. The supply for each weight of

board was divided into several narrow "rolls" or cross-machine "positions"

of a larger roll, and each position was separately randomized. Each

package contains test pieces from one position only. The position is

designated by the number following the letter in the code marked on the

package. Thu:- 42H J_ indicates that this package contains 42 lb board

from position 1 of lot H. Samples from the first position are distributed

until exhausted, then from the second position, and so forth for each

weight of board. Thus for short periods of time (several weeks to months)

,

the samples that the participants test are from the same position of a lot,

and for a longer period from the same lot.

The three weights of linerboard distributed in this program may be used as reference standards. The best reference values are the cumulative grand

AV MEANs in the latest reports. These values are given at the bottom right

of each table. For each weight of board, comparisons should be made first

for measurements made on the same position, i.e., for checking your current

measurement, use grand AV MEANs that have the same position code as on the

packages being tested. The position is shown in the upper left corner of

the table. If no report is yet available on the current position, grand

AV MEANs from previously tested positions of the same lot may be used as approximate reference values.

Similarly a large supply of a 26 lb corrugating medium was randomized,

after dividing into several narrow rolls or positions. The above

discussion for linerboard also applies to the corrugating medium.

We are currently using the third lot of linerboard and the second

lot of corrugating medium:

Lot Material Codes Used

1 linerboard A, B,C October 1969 - April 1973

2 linerboard D,E,F September 1972 - September 1976

3 linerboard G,H, I October 1976 -

1 corrugating medium (A) May 1973 - March 1976

2 corrugating medium B April 1976 - February 1977

3 corrugating medium C March 1977 -

5
LINFRR8ARD 42 H 4 CoLLABeKAT

VE kEFFRENCE PROGRAM SLPTFMRFk 1977 REPORT NS. 96 BURSTING STRENGTH (MULLEN), PSt

LAB MEANS TBIS MONTH THIS MONTH CUMULATIVE

CODE V WK-1 WK-2 WK-3 WK-4 MEAN SDR SDWKS MEAN SLH snwxs WKS

too A 126.0 125. 1 124.7 126.7 125.7 7. 3 .9 124.5 7.3 1 .

3

1 1 101 F 124.8 124.1 124.1 125.5 124.6 6.6 .7 125.7 7.0 1.4 1 1 103 A 125.0 121.6 122.2 123.2 123. 0 9.9 1 .5 124.0 8. 5 2.6 1 1 105 A 124.5 126.3 125.3 122.2 1 24. 6 8.3 1 .7 124.6 9.1 2.0 8 106 A 122.3 127.2 122.9 124. 3 124. 2 8.9 2.2 123.8 9.3 2. 3 1 1

107 C 126.5 126.5 126.6 131.0 1 27. 7 9.4 2.2 129.5 9.7 5.4X 1 1 108 D 129.7 133.8 128.3 130. 6 9.1 2.9 129.4 9.6 2.6 8 109 F 116.0 118.6 120.4 1 18. 3 1 1 .2 2.2 119.2* 8.9 3, 1 1 0 110 D 132.4 132.8 125.6 131 .6S 130. 6 7.5 3.4 131.2 8.5 2.4 1 1 111 D 130.4 128.2 133.8 131.2 130. 9 9.0 2.3 130.8 10.0 2.9 1 1

112 A 127.7 128.6 127.0 133.2 129.2 11.0 2.8 126.6 9.1 2.9 1 0 113 B 121.8 126.9 123.4 125.3 124. 4 7.5 2.2 123.8 7.4 1.5 1 1 114 C 124.8 127.5 125.5 124.8 125.7 9.1 1 .3 126.5 9.9 2.7 1 1 115 B 122.8S 119.2 118.2 120.4 120. 2 9.7 2.0 119.9 9.6 2.2 1 1 116 B 124.5 122.9 130.1 127.8 126. 3 9.6 3.2 126.4 9.7 2.4 1 1

117 A 128.4 129.7 121.4 119.2 124. 7 7.9 5.1 121.7 8.0 4. ex 1 1 119 A 120.0 130.1 129.7 126. 6 9.6 5.7 125.7 9.1 4.1 9

120 B 129.9 127.5 121.5 127.2 126. 5 1 0.7 3.6 125.9 10.2 3. 1 1 1 121 D 126.3 123.7 123.8 125.2 124. 8 9.8 1 .2 128.7 9.0 3.6 1 1 123 A 120.3 119.9 122.8 130.3 123. 4 8.8 4.8 123.5 6.6 3.3 8

125 F 129.2 128.1 124.6 125.4 126. 8 8.2 2.2 128.0 8.7 2.8 11 127 A 122.6 123.7 124.3 120.4 122.8 8. 8 1.7 122.2 7.8 1.7 1 1 128 F 126.0 124.4 128.0 120. IS 124. 6 11.7 3.4 125.2 10.4 3.3 1 1 129 A 120.8 129.4 121 .3S 123. 8 6.3 4.9 123. 1 4.6X 2.8 10 130 A 132.6 132. 2 129.2 127.4 130. 4 9.8 2.5 130.6 9.1 1.6 1 1

131 B 105. 2X 108. 7X 127.3 120.5 115. 4X 1 0.8 10.2 111 .3X 9.7 6.8X 11 133 B 120.8 120.2 120.1 123.2 121.1 8.9 1.5 120.3 8. 0 1.6 1 1 134 F 122.8 123.0 123.1 122.1 122. 8 8.8 .4 121.4 8.3 2.8 1 1 135 A 122.0 127.2 123.3 125.3 124. 5 1 0. 1 2.3 122. 3 8. 8 4.2 1 1 136 A 118.3 127.0 122.7 6.9 6.2 119.4 6.2X 3.4 8

137 F 124.7 117.6 119.8 122.3 121.2 8.7 3.0 122.4 9.0 2. 5 1 1 138 A 129.6 126.3 131 .

129.8 129. 2 10.7 2.0 129.5 10.8 2.5 1 1 139 B 121.3 126.6 131.1 123.1 125.5 1 0.5 4.3 125. 8 9.5 3.2 1 1 140 F 129. 4S 124.3 124.3 125. 1 125. 8 5.1 2.4 125.9 7.7 2.6 1 1 141 F 1 19. OS 121.3 123.1 123.7 121.8 5.1 2.1 122.8 5.2X 3.0 9

142 C 129.4 127.6 127.8 130.7 128.9 9.3 1 .5 1 27 • 9 8.7 2.6 1 1 143 B 125.7 124.9 125.2 125.3 8.6 .4 124.1 9.7 1.0 10 145 F 118. 4S 112. 9X 132.4 120.4 121.0 5.0 8.2 121.9 4.7X 8. 2X 6 147 A 132.7 130.3 128.7 124.2 129. 0 e.3 3.6 128.7 9.2 2. 6 1 1 149 F 123.1 128.4 129.9 126.5 127. 0 9.7 2.9 129.0 9.7 3.3 1 1

151 F 122.2 123.9 124.2 122.9 123. 3 8. 0 .9 123.7 7.7 2.0 1 0 153 E 1 30.8 132.3 129.3 132.8 131.3 8.6 1 .6 131.6* 7.8 1 .

8

1 1 157 A 121.4 123.4 118.4 122.6 121.

5

9.4 2.2 123.0 10.0 3.5 1 1 159 A 126.9 127.2 124.6 123.8 125.7 9.6 1 .7 126.0 9.4 1.5 1 1 161 A 126.7 126.7 9.7 126.5 9.8 2.5 8 163 A 122.7 127.7 126.6 125. 7 9.7 2.6 125. 1 9.8 2.9 10 165 B 128.9 122.5 123.1 124. 8 9.9 3.5 126.2 9.3 2.6 10 166 F 117.6 122.5 118.9 122.8 120. 5 6.5 2.6 120.8 6.9 1.7 1 1 167 F 125.9 125.7 125.9 122.7 125. 0 6. 1 1 .6 122.6 S.6X 2.8 1 1 168 A 133. 2S 142. ex 137. 3X 139. 8X 138. 3X 12.1 4.1 136. OX 11.2 3.4 1 1 169 A 125. 8 126.4 126.4 125.3 126. 0 9.4 .5 126.2 9.3 1.1 8 170 A 135.7 130.7 126.5 128.5 130. 4 10.0 4.0 128.7 9.9 3.0 1 1 171 A 126.2 123.9 122.2 125.5 124. 5 8.6 1.8 124.5 8.5 4.0 10

172 A 126.4 127.0 125.5 126.7 126. 4 7.8 .6 124.8 7.7 1.8 1

173 A 122.8 122.5 122.0 122.4 122. 4 6. 1 .3 123. 1 6. 6 .9 1

6
L I NE BBOARD 42B4 COLLABORATIVE REFERENCE PROGRAM SF PI fckl BEK 1977 REPORT NO. 96 BUMSTING STKENOTH ( MULLEN )

,

P9I LAB MEANS IBIS MONTE THIS MONTH CUMULATIVE

CADE V UK-1 WK-2 WK-3 WK-4 MEAN SOB SDWKS MEAN SDR SDWKS WKS

174 A 130.5 126.7 125.1 126.3 127. 2 9.3 2.3 128.2 9.5 2.0 11 175 A 124.4 126.0 122.9 120.8 123. 5 8.3 2.2 123.9 8.6 2.8 1 1 176 A 128.3 128.0 128.7 125.3 127.6 11.5 1.5 127.

10.5 2.6 1 1 177 A 123.5 126.5 121 .

120.6 1 23. 0 7.3 2.7 122.4 8.2 1.8 1 1 178 A 134.6 130.9 132.0 140. 9X 134. 6X 11.0 4.5 133.1* 9.9 3. 1 1 1

182 A 127.4 128.8 129.1 129.9 128. 8 8.8 1.0 127.3 9.4 1.9 1 1 184 F 127.6 125.5 122.7 129.2 126. 3 8.3 2.8 126. 1 8.7 2.5 1 1 186 E 124.7 125.3 129.0 130.2 127. 3 7.9 2.7 123.6 8.4 3.4 11 188 E 124.1 124.1 122.1 126.8 124.3 8.2 1 .9 124.0 7.7 1.2 11 198 B 119.7 119.9 118.8 124.0 120. 6 6.9 2.3 120.1 7.5 2.8 1 1

274 A 123.3 123.7 123.2 124.5 1 23. 7 6.2 .6 123.2 6.6 .8 11 283 A 120.9 120.8 120.1 121.1 120.7 5.7 .4 120.4 5.7X .6 1 1 287 C 131.5 127.1 125.2 127.2 127. 8 8.5 2.7 126.0 8.8 3.3 1 1 327 F 128.6 123.9 130.2 126.1 127. 2 9.9 2.8 125. 5 9.0 3.2 8 350 F 133.4 133.3 126.6 127.1 130. 1 9.1 3.8 127. 7 9.7 4.0 1 1

375 G 130.5 130.9 131 .9 127.2 130. 1 9.9 2.0 129.3 9.4 1 1 568 A 132.9 129.4 128.2 129.1 129. 9 9.0 2.0 1.3.9 9.4 2.5 1 1 569 A 127.8 125.0 124.3 126.6 125.9 8.2 1.6 125.3 7.7 2.6 9 590 A 133.3 133.3 128.9 124.9 130. 1 8.4 4.0 129.0 9.6 3. 1 1 1

GRAND AVERAGES

WK-1 WK-2 WK-3 WK-4 THIS MONTH CUMULATIVE 11 WEEKS

AV MEAN 126. 1 1 25.8 125.6 125.4 AV MEAN 125.7 125.4

AV SDR 8.8 8.7 8.6 8.7 AV SDR 8.7 8.6

SD LABS 4.5 3.7 3.8 3.4 SD LABS 3.9 4.0

NO. INCL 70 67 70 70 NO. INCL 69. 2 70.1

NO. OMIT 1 3 1 2 AV SDWKS 2.6 2.5 NOT BCD 3 4 3 2 SD CUM MEAN 3.0

7
LINERBOARD 69i: { COLLAE flR AT I VE REFERENCE PROGRAM SEPTEMBER 197^ REPORT NO. 96 BURSTING STRENGTH (MULLEN). PSI

LAB CODE V WK-l MEANS THIS MONTH

WK-2 WK-3 WK-4 THIS MONTH

MEAN SDR SDWKS MEAN CUMULATIVE

SDk SD*KS WKS

100 A 151.1 151.1 14.2 154.3 12.4 2.6 7 101 F 155.1 1 55. 1 10.2 151.9 9.6 1.5 7 103 A 150.7 150. 7 12.8 148.8 13.9 2.3 7 106 A 151.2 151.2 18.4 150.7 16.3 5. 1 7 107 C 156.5 156. 5 9.6 152.8 12.0 2.5 7

109 F 156.1 156. 1 14.2 156.3 13.0 .7 7 110 D 156.4 156.4 12.3 158.5 14.0 4.8 7 111 D 151.7 151.7 1 5.3 159.0* 15.1 4. 4 7 112 A 159.4 159. 4 17.8 155.6 17.7 8. IX 7 113 B 154.5 154. 5 12.8 151 .

11.5 2.0 7

114 C 153.8 1 53. 8 15.4 156. 1 14.3 5. 4 7 HE B 153.8 153. 8 15.6 154.0 16.3 4. 4 7

1 1 6 B 148.3 148. 3 13.1 150.7 13.9 3. 4 7 117 A 163.0 163.0 10.3 157.2 10.1 4.7 7 120 B 157.2 157. 2 14.5 155.5 15.2 4.9 7

12 1 D 155.6 155. 6 16.9 154.4 13.4 3.6 - 122 A 137. 7X 1 37. 7X 15.1 147. 5 14.0 CD CD X 3 125 F 154.0 1 54. 0 14.6 152.2 12.7 3. 1 7 127 A 155.8 155. 8 6.0 155.5 e.7 . 4 7 128 c 148.9 148. 9 17.2 146.2* 14.5 4.4 7

130 A 152.7 152.7 18.4 152.4 15.9 4.

131 B 113. IX 1 13. IX 1 0.6 146.0* 14.1 2 2. IX 4 133 B 141 .9X 141. 9X 14.2 144.7* 12.3 3.8 7 134 F 144.6 144. 6 11.5 149.6 9.8 3.4 ~7 135 A 144.6 144. 8 16.5 141 . 3X 12.0 2. 9 7

136 A 156.7 156.7 12.7 149 .4 10.5 5.0 6 137 F 150.5 1 50. 5 1 1 .9 152.7 15.1 2. 3 6 136 A 156.6 156.6 14.0 154.8 15.4 5. 1 7 139 B 153.2 153. 2 15.1 152.0 14.0 4.6 7 140 F 158.3 158. 3 11.9 154.1 13.8 2.8 7

141 F 145.3 145. 3 9.5 151.9 7.2X 5. 7 7 142 C 150.5 150.5 12.3 154. 1 12.1 4.2 7 143 B 149.4 149.4 10.7 147.2 12.2 7.0 7 145 F 154.7 1 54. 7 6.2 156.7 9.1 4.7 6 147 A 157.5 157. 5 18.3 153. 8 1 3.1 3. 7 7

149 F 156.2 156.2 11.7 153.8 12.9 3. 5 7

151 F 151 .9 151.9 8.8 154.6 11.2 1 .

6 153 E 163.6 1 63. 6 16.7 156.0 11.1 4.3 7 157 A 1 3e.'7X 1 38. 7X 15.2 148.2 15.8 8. 9X 7 159 A 154.2 1 54. 2 15.3 151.1 14.5 5.1 7

161 A 155.1 155. 1 15.3 151.5 l 3.9 3.9 7 163 A 153.1 1 53. 1 13.3 149.6 15.1 3.9 6 165 B 159.3 159. 3 9.0 151.1 12.2 6.3 6 166 F 152.0 152. 0 9.7 157.1 10.7 3.4 5 167 F 154.3 154.3 5.9 151.3 9. 0 2.6 7

166 A 154.9 154.9 13.5 158. 6 15.8 7.6 7 169 A 157.3 157. 3 10.4 154.2 12.4 2.8 3 170 A 155.6 155. 6 12.3 153.7 14.6 1.7 7

171 A 152.0 1 52.0 13.7 152. 3 1 4. 0 5.6 7 172 A 155.1 155. 1 8.4 154.5 1 0.9 1. 1 7

173 A 153.4 153. 4 8.2 155. 1 10.8 3.0 7 174 A 169. 4X 169. 4X 1 5.4 156.4 14.9 9. OX 7 175 A 154.7 154.7 16.5 151.9 14.4 4.4 7 176 A 146.2 146. 2 1 5.9 1 55 • 0 15.9 6.4 t 177 A 147.3 1 47. 3 11.4 147.2 12.4 2. 8 6

8
LINEKBOARD 6913 COLLADO RAT I VE REFERENCE PROGRAM REPORT NO. 96 BURSTING STRENGTH (MULLEN), PSI

SEPTEMBER 1977

LAB CODE V WK-1 MEANS THIS MONTH

WK-2 WK-3 WK-4 THIS MONTH

MEAN SDR SDWKS MEAN CUMULATIVE

SDR SDWKS WKS

176 A 160.2 160. 2 20.3 158.5 16.0 5. 1 7

18 2 A 152.5 152.5 14.0 150.6 15.3 4.8 7 184 F 159.9 1 59.9 17.1 149.9 13.8 6.4 7 186 E 155.6 15 5. 6 10.8 156.0 11.1 1.0 7 168 E 151.0 151.0 9.9 152.3 10.2 2.4 7

198 B 154.3 154.3 13.7 149.9 12.9 2.6 7 274 A 153.4 153. 4 7.1 153.9 8.2 . 8 7 283 A 153.5 153.5 6.7 155. 8 9.9 1.7 7 287 C 151.2 151.2 18.1 149.6 15.3 3. 1 7 327 F 154.0 154. 0 15.6 153.7 14.0 2.5 3

350 F 153.3 153. 3 i e.s 151.9 13.9 4. 1 7 375 G 159.5 1 59. 5 6.7 155.0 12.3 3.8 7

56 8 A 161.4 161.4 1 1 .3 154.1 12.9 4.7 7 569 A 151.1 151.

1

1 1 .7 146.9 13.0 3. 1 5 590 A 154.5 154.5 13.7 151.7 14.3 5.4 7

GRAND AVERAGES

Wk-1 WK-2 WK-3 WK-4 THIS MONTH CUMULATIVE 7 WEEKS

AV MEAN 154.0 AV MEAN 154.0 152.8

AV SDR 13.0 AV SDR 13.0 12.9

SD LABS 4 .

0

SD LABS 4.0 4.7

N0. INCL 65 NO. INCL 65. 0 68. 1 NS. OMIT c AV SDWKS .0 3.7

SD CUM MEAN 3.1

9
LINEBB6ARD 6514 COLLABORATIVE REPERENCE PROGRAM

REPORT NO. 96 BURSTING STRENGTH (MULLEN), PSI

SEPTEMBER 1977

LAB MEANS THIS MONTH

CODE V WK-l WK-2 WK-3 WK-4

ICO A 1 60.0 164.1 156.2

101 F 151.2 151 1 51 .2 103 A 154.9 149.8 152.3

106 A 166.0 160.3 146.6

1 07 C 152.3 148.8 158.6

108 D 156.2 153.4 154. 5 109 F 156.5 156.3

110 D 164.7 158.6 163.6

11 D 164.0 163.5 161.1

112 A 157.4 156.8 155.1

113 B 154.0 155.1 154.3

114 C 152.2 153.1 160. 3 115 B 150.0 142. IX 150.6

116 B 148.7 157.2 155.8

ll^ A 161.2 155.2 155.0

119 A 162.2 158.9 162.3

120 B 158.1 155.1 154.2

12 1 D 150.8 1 51 • 153.7

123 A 146.5 151 .0 1 58.7

125 F 153.7 152.3 153.4

127 A 155.6 156.0 154.6

128 F 149.2 145.7 151.5

129 A 159.9 152.1 151.6S

130 A 155.4 158.7 152.0

131 B 1 1 4. nc 146.5 152.6

133 B 150.8 147.5 145.8

134 F 145.7 149.6 150.5

135 146.4 152.3 159.8

136 A 1 59.3

137 F 149.6 148.5 150.6

138 A 151.9 167. 5X 149.0

139 B 156.2 155.6 149.7

140 F 168. 4 155.6 158.3

14 1 F 145.1 144. 9S 149.7

142 C 154.6 160.3 159.8

143 B 152.0 151.3

145 F 147.4 156.1 154.3

147 A 151.1 162.1 154.8

149 F 158.6 160.8 154.5

151 F 153.1 1 5 4 .

1 50.9

153 E 165. 0 158.1 157. 1 157 A 141.8 148.6 151.7

159 A 150.0 157.5 143. OX

163 A 149.9 148.3

165 B 155.8 149.6

166 F 160.3 153.7 156.1

167 F 155. 0 149.0 1 S 1 .0 168 A 168.2 160.4 175. 9X

169 A 155.6 153.7 157. 8 170 A 164.5 159.9 160.0

171 A 157.7 157.3 159.7

172 A 156.5 154.8 159.3

173 A 150.5 148.7 152.5

174 A 168.9 167. 3X 167. 9X

175 A 147.0 152.9 146.0

THIS MONTH CUMULATIVE

MEAN SDR SDWFS MEAN SDR SDWKS WKS

160. 1 11.6 3.9 160.1 11.6 3.9 3 151 .

9.5 .3 151.4 9.5 . 3 3 152. 3 14.5 2.6 152. 3 14.5 2.6 "3 157. 7 14.4 10.0 157.7 14.4 1 O.OX 3 153. 2 16.4 5.0 153.2 16.4 5.

3

1 54. 7 15.4 1 .4 154.7 15.4 1 .

3 156. 4 16.8 . 1 156.4 16.8 . 1 2 162.3 12.1 3.2 162.3 12.1 3. 2 3 162.9 16.1 1.5 162.9* 16.1 1.5 3 156. 4 15.7 1 .2 156.4 15.7 1.2 3 154.5 11.1 .6 154. 5 11.1 .6 3

1 55. 2 13.6 4.4 155. 2 13.6 4.4 3 147. 6 17.4 4.7 147.6 17.4 4.7 3 153.9 12.9 4.5 153.9 12.9 4.5 3 158. 5 9.8 3.1 158.5 9.8 3. 1 3

161.2 16.2 1 .9 161.2 16.2 1.9 3

1 57. 1 1 8.9 2.6 1 57. 1 18.9 2.6 3 152. 1 5.6 1.5 152.1 9.8 1.5 3 152.2 14.3 6.0 152.2 14.3 6.0 3 153. 1 11.6 .7 153.1 11.6 .7 3

1 55. 4 12.2 .7 155. 4 12.2 .7 3 148. 8 15.1 2.9 148.8 15.1 2.9 7 154. 5 10.1 4.6 154.5 10.1 4.6 3 155. 4 13.0 3.4 155.4 13.0 3.4 3 138. 4X 13.0 21.2 138. 4X 13.0 21. 2X 3

149. 4 13.8 1.7 149.4 13.8 1.7 3 150. 1 8.7 .7 150.1 8 . 7 . 7 3

1 52. 9 13.5 6.7 152.9 13.5 6.7 3 159. 3 1 5.8 159.3 1 5. 8 1 149. 6 12.0 1 .1 149.6 12.0 1.1 3

156. 2 12.5 10.0 156. 2 12.9 1 0. OX 3 153. 9 14.8 3.6 153.9 14.8 3.6 3 160. 8 10.2 6.7 160.8 10.2 6.7 3 146. 6 7.6 2.7 146.6* 7.6 2.7 3 158. 2 15.0 3.2 158.2 15.0 3.2 3 151.6 12.5 .5 151 .

12.5 .5 2 152. 6 5.2 4.6 152.6 9.2 4.6 3 156. 0 15.1 5.6 156.0 15.1 5.6 3 158. 0 1 5.0 3.2 158.0 15.0 3.2 3

1 52. 7 9.5 1.6 152. 9.9 1 .6 3

160. 1 12.8 4.3 160.1 12.8 4.3 3 147. 4 13.6 5.0 147.4* 13.6 5.0 3

1 50. 2 1 5.6 7.3 150.2 15.6 7.3 3 149. 1 1 3.8 1 .2 149.1 13.8 1.2 2 152.7 16.6 4 .4 152.7 16.6 4.4 2 156.7 9.4 3.3 156.7 9.4 3.3 3 151.7 8.4 3.1 151.7 8.4 3. 1 3 168. 2X 14.0 7.8 168. 2X 14.0 7. 0X 3

1 55. 7 1 0.9 2 . 1 155.7 1 0.9 2 . 1 3 161.5 14.4 2.6 161.5 14.4 2.6 3 158.2 16.3 1 .3 158. 2 16.3 1.3 3

1 57. 0 12.8 2.2 157.0 12.8 2.2 3 150. 6 9.3 1 .5 150.6 9.3 1 .9 3

1 68. OX 15.4 .8 1 68. OX 15.4 .8 3 148. 6 12.9 3.7 148.6 1 2 .9 3.7 3

10
LINFRBOARD 69 14 COLLABORATIVE REFERENCE PROGRAM

REPORT NO. 96

BURSTING STRENGTH (MULLEN), PSI

SEPTEMBFR 197-*

LAB MEANS THIS MONTH THIS MONTH CUMULATIVE

CODE V WI -1 WK-2 WK-3 WK-4 MEAN SDR SDWKS MEAN SDR SDWKS WKS

176 A 151 .9S 156.3 162.3 156.9 1 8.7 5.2 156.9 1 8.7 5.2 3 177 A 160.2 148.2 148.9 152.5 10.0 6.7 152.5 10.0 6.7 3 176 A 151.4 152.8 168.6X 157. 6 14.6 9.6 157.6 14.6 9.6X

162 A 150.5 159.6 158.2 156. 1 13.0 4.9 156.1 1 3.0 4.9 3 184 F 154.2 158.3 149.9 154. 1 14.5 4.2 154.1 14.5 4.2 3

1 86 E 155.8 156.5 165. OX 1 59. 6 11.5 4.7 159.8 11.5 4.7 3 186 E 154.8 152.0 151.9 152.9 6.8 1.6 152.9 8.8 1.6 3 198 R 155.3 156.0 157.7 1 57. 0 14.3 1 .5 157.0 14.3 1.5 3

2 T 4 A 154.1 153.1 153.3 153. 5 8.4 .5 153.5 8.4 .5 3 283 A 156.4 155.3 156.3 1 56. 0 8.6 .6 156.0 8.6 .6 3

28"’ C 156.2 155.0 151.7 154. 3 13.8 2.4 154. 7 13.8 2.4 3 327 F 159.5 154.9 156.6 157.0 12.4 2. 3 157.0 12.4 2.3 3 350 F 155.4 147.4 155.8 152.9 16.1 4.7 152.9 16.1 4.7 3 375 0 157.9 160.6 153.8 157. 4 13.5 3.4 157.4 13.5 3.4 3 568 A 161.5 156.3 157.9 158.6 13.6 2.7 158.6 13.6 2.7 3

569 A 153.0 151.2 153.2 1 52. 5 13.8 1 .1 152.5 1 3.8 1 . 1 3 59 0 A 163.5 '58.3 155.2 159. 0 17.1 4.2 159.0 17.1 4.2 3

GRAND AVERAGES

WK-1 WK-2 WK-3 WK-4 THI S MONTH CUMULATIVE 3 WEEKS

AV MEAN 155.6 154.7 154.4 AV MEAN 154.9 154.9

AV SDR 13.4 13.3 12.6 AV SDR 13. 1 13.1

SD LABS 5.9 4.5 4.0 SD LABS 4.8 4.8

NO. INCL 68 67 66 NO. INCL 67. 0 67.0

NO. OMIT 1 3 5 AV SDWKS 3.6 3.0 NOT RCD 3 2 1 SD CUM MEAN 3.8

11
CORRUG. MEDIUM 2oC2 COLLA BO RAT I VH REFERENCE PROGRAM SEPTEMBER 1 577

REPORT NO. 96 FLAT CRUSH STRENGTH (CONCORA). LB

LAB MEANS THIS MONTH THIS MONTH CUMULATIVE

CODE V WK-1 WK-2 WK-3 WK-4 MEAN SDR SDWKS MEAN SDR SDWKS WKS

IOO 64.7 62.2 61 .4 62.2.7 1 .7 62.5 2.8 .8 15 105 65. 1 66.4 68. OX 69. OX 67. 2X 3.1 1.7 66. 6X 3.2 2.4 H

1 06 64 .4 66.0 65. 7S 67.8 66. 0 4.3 1 .4 65.2 3.7 1.5 16 110 66.5 62 .

63.7 65. 0 64.5 2.3 1.6 6 3.9 1 .8 1.4 16 113 64.2 64.4 63.5 62.4 63. 6 2.9 .9 63. 0 2.8 1.0 1 6

114 61 .2 62.3 63.2 63.0 62. 4 2.5 .9 61.2 2.8 1.6 1 4 115 57. 4X 62.9 62.2 62.1 61.2 3.3 2.5 60.5* 3.3 2.3 15 116 58. 5X 61 .

60.5 61.6 60.5 2.0 1.4 61.3 2.3 1.5 16 119 63.0 63. 8 61.7 62.8 2.9 1.1 63.0 3.2 .9 1 3 120 62.6 64.3 66.2 ;>e.7 63. 0 3.2 3.2 63.6 3.2 2.5 16

125 68. 3X 67.2 66.3 <>6.7 67. IX 2.7 .9 67. 9X 3.1 1.5 16 128 62.4 62.5 62.1 63. 1 62.5 2.6 . 4 62 .

2.8 .9 16 136 62.3 61.9 63.3 64.1 62.9 3.5 1.0 63.7 3.3 1.4 16 140 64.3 62.6 62.7 64.3 63. 5 3.1 1.0 62.8 3.0 1.1 16

143 61.0 60.9 62. 1 61.4 2.5 .6 62.1 2.6 .7 15

164 63.0 62.9 62.4 62.9 62. 8 2.5 . 3 63 .

2.5 .6 1 5

16’’ 66.1 67.4 64.2 6 J.3 65. 3 2.9 1 .8 64.5 3.0 1.4 1 6 177 63.3 62.0 62.5 62.5 62.

2.6 .6 63.

2.5 1 .16 182 64.2 67.3 65.

64.6 65. 4 3.1 1 .4 65.0 3.3 .9 1 1 186 62.0 63.8 61 .0 60.7 61.9 2.1 1.4 62.6 2.1 1.2 16

198 61.8 61.6 62.0 60.7 61.3.4 .6 62.9 3*. 5 1.6 14 237 63.0 62. 1 62.8 62.3 62. 6 2.8 .4 62.4 2.9 1.0 16 250 64.8 61.1 63.4 61.5 62.7 2.3 1 .7 62.

2.0 1.6 1 1 269 61.5 61 .

61 .7 61.3 61.4 2.2 .3 61.1 2.2 .8 16 274 63.3 63.2 63.2 63.6 63.3 2.2 .2 63.2 2.3 .4 16

283 63.9 63.5 63.0 63.7 63.5 2.3 . 4 63.6 2.

. 5 16 284 65.4 65.8 65.8 66.7 65. 9 3.4 .5 66.0* 3.6 1.2 16 287 62.6 63.6 65.4 66.1 64.4 3.1 1.6 64.8 3.3 1.4 16 292 60.3 61.9 61 .3 65.2 62. 2 3.1 2.1 62.0 2.7 1.7 16 327 60.7 63.4 62.0 62.4 62. 1 3.1 1 . 1 61.7 2.9 1.2 12

350 67. 8X 68. 0 67. 9X 2.7 .1 67. ’I 2.7 1.9 14 351 60.2 62.2 60.7 60.8 61 .

1.9 .8 61 .2 1 .8 1.3 16

35 3 61.2 64.2 64.9 66. 1 64. 1 3.0 2.1 62.9 3.0 1.6 16 355 64.2 61.3 61 .6 61.2 62. 1 2.3 1.4 61.0 2.4 1.1 16 357 63.3 63.9 63.6 63.0 63.5 1 .9 .4 62.8 2.2 1 .

12

361 65. 1 64.8 65.3 63.9 64. 8 2.8 .6 63.9 2.5 .9 15 363 61.9 62.2 64.6 59.5 62. 1 3.1 2.1 62.5 3.0 2.0 16 365 61.3 60.3 59.8 60.2 60.4 2.3 .7 60.9 2.6 .9 16 367 64.8 65.0 65.0 64.8 64. 9 3.5 . 1 65.4 3.3 1 .

15 369 62.4 61.9 61.8 62.9 62.2 2.6 .5 62.9 2.8 .7 1 6

377 64.3 63. 8 65.2 64. 5 3.8 .7 63.6 3.1 .9 1 4 379 62.6 63.3 62.9 63.8 63.2 2.5 .5 63.2 2.9 1.0 IS 381 57. 41 62.3 62.4 59.8 60. 5 2.5 2.4 62.8 2.7 2.4 16 383 64.3 63.9 63.0 64.0 63. 8 3.1 .5 63.3 3.2 1 .

16 385 59.8 58. OX 65.7 60.9 61.1 3.1 3.3 61.4 3.1 2 . ex 1 6 387 62.4 64.5 61 .

63.2 62. 9 3.1 1.3 63.4 3.1 1.3 16

391 64.6 63.6 64.4 63.8 64. 1 2.4 .5 64.2 2.4 .7 13 393 62.6 63.7 63.7 63.2 63.3 1.9 .5 64.0 2.5 .9 16 395 65.1 63.8 64.4 67.0 65. 1 3.0 1 .4 64.6 3.1 .9 16 397 61.9 61 .

60.0 63.2 61.7 2.8 1.3 62.5 2.7 2.0 15

399 63.4 59.3 60.8 62.0 61.4 2.6 1 .7 61.3 2.5 2.0 16

56 8 62.7 62.0 63.2 62.5 62. 6 3.8 .5 61 .

3.2 2.0 16 572 63.9 63.3 67.7 65.0 3.4 2.4 65.4 3.5 2. 1 15

57 8 62.0 64.5 64.0 64.0 63. 6 2.6 1.1 62.4 2.7 4. OX 16 579 64.3 64.0 64.2 1.6 .2 64.0 2.2 .7 1 4

GRAND AVERAGES

WK-1 WK-2 IS" 3 WK-4 THIS MONTH CUMULATIVE 16 WEEKS

AV MEAN 63. 1 63.3 63.2 63.3 AV MEAN 63.2 63.2

AV SDR 2 . 8 2.7 2.9 2.8 AV SDR 2.8 2.8

SD LABS 1.6 1 .7 1.6 2.2 SD LABS 1.8 1.8

NO. INCL 47 52 51 53 N0. INCL 50.7 51.2

NO. OMIT 5 1 1 1 AV SDWKS 1. 1 1 .

NOT RCD 3 2 3 1 SD CUM MEAN 1 .

SD SHTS 1 .7 1 .8 1.9 1.9

12
NBS-1 14A (REV. 7 7.1)

U .S. DEPT. OF COMM. BIBLIOGRAPHIC DATA

SHEET

1. PUBLICATION OR REPORT NO. FKBG CRP 96

2. Gov't Accession

No.

3. Recipient's Ai cession No.

4. TITLE AND SUBTITLE

CONTAINERBOARD

Collaborative Reference Program for Containerboard

5. Puhl icat ion Date November 4, 1977

6. Performing Organization Code

7. AUTHOR(S) 8. Performing Organ. Report No. NBSIR 77-1320

9. PERFORMING ORGANIZATION NAME AND ADDRESS

NATIONAL BUREAU OF STANDARDS

DEPARTMENT OF COMMERCE

WASHINGTON, D.C. 20234

10. Project/Task/Work Unit No. 4015578

11. Contract/Grant No.

12. Sponsoring Organization Name and Complete Address (Street, City, State, ZIP)

Collaborative Testing Services, Inc., 9241 Wood Glade Drive

Great Falls, Virginia 22066, and American Paper Institute/

Fourdrinier Kraft Board Group

13. Type of Report & Period Covered

Final

14. Sponsoring Agency Code

15. SUPPLEMENTARY NOTES

16. ABSTRACT (A 200-word or less factual summary of most significant information. If document includes a significant

bibliography or literature survey, mention it here.)

Collaborative Reference Programs provide participating laboratories with the means

for checking periodically the level and uniformity of their testing in comparison

with that of other participating laboratories. An important by-product of the

progrmas is the provision of realistic pictures of the state of the testing art.

This is one of the periodic reports showing averages for each participant,

within and between laboratory variability, and other information for participants

and standards committees.

17. KEY WORDS (six to twelve entries; alphabetical order; capitalize only the first letter of the first key word unless a proper name; separated by semicolons)

Collaborative reference program; Containerboard ; Laboratory evaluation; Precision;

Reference samples; Testing calibration.

18. AVAILABILITY | Uni imited

lv For Official Distribution. Do Not Release to NTIS

2 Order From Sup. of Doc., U.S. Government Printing Office Washington, D.C. 20402, SD Cat. No, Cll

Order From National Technical Information Service (NTIS)

Springfield, Virginia 22151

19. SECURITY CLASS 21. NO. OF PAGES

(THIS REPORT)

UNCL ASSIFIED

19

20. SECURITY CLASS 22. Price (THIS PAGE)

UNCLASSIFIED

USCOMM-DC 29042-P74
.

'

'