. ,. ROJAC 

AIR TESTING 

I SERVICES, 

INC. 

120 Mountain Avenue Bloomfield, CT 06002 

Compliance Test Report 

Redland Brick, Inc. - KF Plant 

Tunnel Kiln 

South Windsor, Connecticut 

Prepared For: 

Mr. Brian Hastings 

Plant Manager 

Prepared By: 

Mr. Leigh A. Garnrnie 

August 1999 

ROJAC Project No. RBKF9903 

860-243-9800 

I 
REPORT CERTIFICATION 

I have personally examined and am familiar with the information submitted in this bound 

document and certify that based on reasonable investigation, including my inquiry of those 

individuals responsible for obtaining the information, the submitted information is true, accurate 

and complete to the best of my knowledge and belief. 

Leigh A. Gamrnie 

President 

RBKF9903 

KF Tunnel Kiln Final Report 

<J /kc9 q{ 

Date 

ROJAC 

AIR TESTING 

SERVICES, 

INC. 
Table of Contents 

Section Page 

1.0 INTRODUCTION ......................................................................................................................................... I 

1.1 Summary of Test Program ....................................................................................................................... I 

1.2 Test Program Organization ...................................................................................................................... I 

2.0 SOURCE DESCRIPTION ............................................................................................................................ 2 

2.1 Process Description ................................................................................................................................... 2 

2.2 Control Equipment. ................................................................................................................................... 2 

2.3 Flue Gas Sampling Locations ................................................................................................................... 2 

3.0 SUMMARY AND DISCUSSION OF RESULTS ........................................................................................ 4 

3.1 Objectives and Test Matrix ...................................................................................................................... 4 

3.2 Field Test Changes .................................................................................................................................... 4 

3.3 Summary of Results .................................................................................................................................. 4 

4.0 SAMPLING AND ANALYTICAL PROCEDURES ..............•................................................................... 6 

4.1 Continuous Emission Monitoring·············································································'······························ 6 4.1.1 Instrumentation ..................................................................................................................................... 6 

4.1.2 Analyzer Calibrations ........................................................................................................................... 6 

4.1.3 Data Reduction ...................................................................................................................................... 7 

4.2 Exhaust Gas Velocity Measurements··································'··································································· 7 4.3 Hydrogen Chloride and Hydrogen Fluoride ........................................................................................... 7 

5.0 QA/QC ACTIVITIES .................................................................................................................................... 9 

5.1 QC Procedures ...................................................................................... -..................................................... 9 

5.2 Sampling QA/QC ....................................................................................................................................... 9 

5.3 Laboratory Analytical QA/QC ................................................................................................ ~ ................ 9 

APPENDICES 

RBKF9903 

KF Tunnel Kiln Final Report 

ROJAC 

AIR TESTING 

SERVICES, 

INC. '1.3 
1.0 INTRODUCTION 

1.1 Summary of Test Program 

ROJAC Air Testing Services, Inc. (ROJAC) was retained by Redland Brick to conduct an 

emission measurement test program on their tunnel brick kiln located at the KF Plant in South 

Windsor, CT. The compliance test program was conducted to satisfy the State of Connecticut, 

Department of Environmental Protection (CTDEP) permitting requirements. 

Emissions measured in determining compliance included sulfur dioxides (S02), hydrogen 

chloride (HCl), and hydrogen fluoride (HF). The tests were carried out in conformance with 

Title 40, Code of Federal Regulations, Part 60 (40CFR60), Appendix A, using EPA Methods 1-

4, 6C, and 26A for determining volumetric flowrates, moisture content, S02 and HCl!HF 

emissions, respectively. 

1.2 Test Program Organization 

The following is a listing of the test program organization with names and phone numbers of 

responsible individuals: 

Mr. Brian Hastings 

Mr. Leigh A. Gammie 

Mr. Carl Ekroth 

Mr. Ron McLeod 

RBKF9903 

KF Tunnel Kiln Report 

Redland Brick 

ROJAC 

CTDEP 

Philip Analytical Services 

- I -

800-366-2742 

860-243-9800 

860-724-4082 

905-332-8788 

ROJAC 

AIR TESTING 

SERVICES, g cj. 

INC. lJ 
2.0 SOURCE DESCRIPTION 

2.1 Process Description 

The KF Plant is a brick manufacturing facility that is permitted to process 21.6 tons per hour of 

unfired bricks which is equivalent to a maximum daily push rate of 15 cars. As part of the 

manufacturing process, Redland employs a natural gas fired tunnel kiln to dry and fire the bricks 

with a maximum kiln temperature of2100°F. The tunnel kiln has a maximum fuel-firing rate of 

25 MMBTu per hour or 25,000 cubic feet of natural gas per hour. For the June 10, 1999 test 

program the push rate averaged 13 cars per hour. A graph depicting process conditions is shown 

in Appendix D. "t -\-o'v- ·\\.,_r I~ :1 '2. ,. f'A' ~ ~s-1'""\ 

2.2 Control Equipment 

Emissions from the tunnel kiln were ducted to a dry cascade absorber supplied by BACT 

Engineering, Inc./Hellmich GmbH & Co. The absorber controls S02, HCl, And HF emissions, 

which are released from the brick material when dried. The absorbent media consisted of 

Canadian limestone pellets smaller than 3/8" in size. The pressure drop across the absorber 

averaged 1 inch of water column (W.C.) The peeling drum timer was set at 60 seconds on and 

13 minutes off. Based on the CTDEP Operating Permit (Town No. 169, Premise No. 005, 

Permit No. 0032, Stack No. 20) dated June 16, 1998, the brick plant has the following emission 

limits. 

Absorber 

Exhaust 

13.2 

Table 2-1 

Redland Brick, Inc. 

KF Plant Tunnel Kiln 

Emission Limitations 

2.85_. 2.35 

Results from this test program are based on the average of three test runs and reported on a 

pounds per hour basis taking into account the actual and dry standard t1owrate measurements 

recorded during the tests. 

2.3 Flue Gas Sampling Locations 

The absorber outlet sampling location was located in a 47" circular section of steel stack. Two 

sampling ports in a horizontal plane gave access to the gas stream. The ports were 352 inches 

RBKF9903 

KF Tunnel Kiln Report 

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ROJAC ,t. AIR TESTING _s 

I SERVICES, a 

INC. ~., 
(7.5 duct diameters) downstream ofthe induced draft fan and 470 inches (10 duct diameter) 

upstream to the top of the stack. Based upon the above parameters, EPA Method 1 required the 

use of twelve sampling points (six points on a traverse). A schematic diagram of the outlet test 

location, along with the individual traverse point locations, is shown in Appendix A. 

RBKF9903 

KF Tunnel Kiln Report 

.., -.) -

ROJAC 

AIR TESTING ~ 

SERVICES, L 

INC. ~ 
3.0 SUMMARY AND DISCUSSION OF RESULTS 

3.1 Objectives and Test Matrix 

The purpose of this test program was to determine the sulfur dioxide (S02), hydrogen chloride 

(HCI), and hydrogen fluoride (HF) emissions from the tunnel brick kiln during production that 

was greater than 90% of maximum capacity rating (MCR). Table 3-1 presents the sampling and 

analytical matrix. 

Absorber soz 

Exhaust 

Absorber HCI 

Exhaust 

Absorber HF 

Exhaust 

3.2 Field Test Changes 

Table 3-1 

Redland Brick, Inc. 

KF Plant Tunnel Kiln 

Sampling and Analytical Matrix 

3 M6C ROJAC 

3 M26A ROJAC 

3 Ml-4 ROJAC 

84 CEMIUV 

84 IC 

84 I C. 

All field sampling occurred without any deviations from the test protocol. Analyses of the hydrogen 

fluoride samples encountered a matrix interference via ion chromatography (I C). These samples were 

reanalyzed by ion specific electrode and are reported on the laboratory certificate of analysis. For 

reporting purposes the ion chromatography results were reported as less than 1000 micrograms (<1000 

ug) for all three runs, these results are shown in Table 3-2. The ion specific electrode results were not 

effected by the interference; these results were reported lower than the IC results. 

3.3 Summary of Results 

Results from the emissions tests performed on June 10, 1999 are presented on Table 3-2. The average 

hydrogen fluoride emissions were less than 0.05 pounds per hour, which are below the emission limit of 

2.35 pounds per hour. Hydrogen chloride emissions averaged 1.14 pounds per hour, these emissions are 

below the limit of2.85 pounds per hour. The average sulfur dioxide emissions were 6.14 pounds per 

hour, which is also below the 13. 2 pound per hour limit. 

RBKF9903 

KF Tunnel Kiln Report 

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ROJAC 

AIR TESTING 

SERVICES, 

INC. 
Table 3-2 

Summary of Emissions Data 

Absorber Outlet Stack 

Redland Brick!KF Plant 

South Windsor, Connecticut 

June 10, 1999 

Outlet Run 1 Run 2 

Method/Component Units/Time 1003 -1132 1239- 1409 

Method 2 Flowrate dscfm 21623 21462 

Method 3-02 % 17.6 17.8 

Method 3 - C02 % 2.0 2.0 

Method 4 - Moisture % 5.72 5.23 

Method 26A - HF lb/hr <0.05 <0.05 

Method 26A - HC1 lb/hr 1.27 1.06 

Method 6C - S02 lb/hr 6.84 5.67 

dscfm - dry standard cubtc feet per mmute 

% -percent, dry basis 

lb/hr- pounds per hour 

RBKF9903 

KF Tunnel Kiln Report 

- 5 -

Run3 

1444- 1612 

20951 

17.8 

2.0 

5.34 

<0.05 

1.09 

5.92 

Avg. 

21346 

17.7 

2.0 

5.43 

<0.05 

1.14 

6.14 

ROJAC 

AIR TESTING 9 

SERVICES, ~ 

INC. 
4.0 SAMPLING AND ANALYTICAL PROCEDURES 

4.1 Continuous Emission Monitoring 

ROJAC conducted the outlet gas measurements for S02 and 0 2 using EPA Reference Methods 

6C and 3A, respectively. A schematic diagram of the sampling system is shown in Appendix A. 

The continuous emission monitoring system (CEMS) draws flue gas in through a stainless steel 

heated probe with a heated out-of-stack filtration system. The gas sample is drawn through the 

probe and filter(s) by a heated Teflon lined diaphragm vacuum pump. From the pump, the 

sample is sent through a heated Teflon sample line, through an electronic condenser, into a 

manifold, and finally to the S02 and 0 2 analyzers. Analyzer outputs will be recorded by a data 

acquisition system (DAS) at ten ( 1 0) second intervals. 

A total of three 60-minute CEM test runs were performed with a zero and mid-range calibration 

check between each test run. In addition, a full range calibration and linearity check was 

performed on each reference method analyzer at the beginning of the test day. Emissions were 

reported in parts per million (ppm) and pounds per hour (lblhr). All field data reporting and 

calculations were conducted in accordance with the guidelines presented in EPA Reference 

Method 6C. Copies of the field data sheets are included in Appendix C. . 

4.1.1 Instrumentation 

The S02 instrument was a Western Research/Bovar Model 721AT2 analyzer. This instrument 

measures the S02 concentration by means of ultraviolet (UV) radiation. The UV radiation is 

selectively absorbed by so2 molecules in the gas stream thus allowing for their quantitative 

measurement. 

The 0 2 instrument was a Servomex Model 1400 analyzer, which measures 0 2 concentration by 

means of the paramagnetic susceptibility of the sample gas using a proven magneto-typemeasuring cell. Oxygen molecules are attracted more strongly by the magnetic field than are 

molecules of other gases, and their concentrations can thereby be measured. 

4.1.2 Analyzer Calibrations 

Certified EPA Protocol 1 compressed span gases of S02, and 0 2 were used as the calibration 

standards. High purity nitrogen (N2) was used as the zero gas. For the field tests, the analyzers 

were calibrated and linearized at three points along their measurement ranges at the beginning of 

the test day. The 0 2 analyzer operated on the 0-25% range and the S02 analyzer operated on the 

0-100 ppm range. Copies of the calibration gases certificate of analysis are contained in 

Appendix E. The system bias and drift tests were conducted with appropriate mid-level dilution 

gases based on the source emissions. These system calibrations were repeated after each 60-

minute test run. The gases passed through all components of the sampling system except the 

sampling probe. 

RBKF9903 

KF Tunnel Kiln Report 

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ROJAC 

,. 

AIR TESTING Cf 

I SERVICES, /o 

INC. 4 
4.1.3 Data Reduction 

The system calibrations were performed to document any instrument drift. Using Equation 6C-l 

( 40CFR60, Appendix A), the ppm and percent values were corrected to account for the zero and 

span values plus any instrument drift as follows where: 

cgas emissions concentration (ppm or %) 

-

c = average emissions reading (ppm or%) 

co average zero reading (ppm or %) 

em average span reading (ppm or %) 

em a span gas concentration (ppm or %) 

The corrected ppm and percent averages were then be used to calculate emission rates in the 

appropriate standard units. 

4.2 Exhaust Gas Velocity Measurements 

Exhaust gas velocities were measured at points chosen in accordance with EPA Method 1, taking 

into account duct size, shape, and local flow disturbances. An S-type pitot tube and inclined 

manometer were used to measure velocity pressure in accordance with EPA Method 2. ·A 

thermocouple and thermocouple thermometer were used to measure stack gas temperatures. The 

thermocouple was attached to the pitot tube assembly. Pitot tubes and thermocouples were 

calibrated in the ROJAC laboratory prior to the sampling program in accordance with EPA 

Method 2. The pitot tube and thermocouple are shown in Appendix A. 

4.3 Hydrogen Chloride and Hydrogen Fluoride 

Triplicate isokinetic hydrogen chloride and hydrogen fluoride (HCl/HF) tests were performed 

concurrently with the CEM tests. Each HCIIHF test was 84 minutes in duration and was 

conducted in accordance with EPA Method 26A. The EPA Method 26A sampling train is 

depicted in Appendix A. The HCl/HF sampling train will consisted of a quartz glass button hook~ 

nozzle, a heated glass lined sample probe, a Teflon filter and frit housed in a heated box, flexible 

Teflon transfer line, a set of 5 glass impingers connected in series contained in an ice bath, a 

leakless vacuum pump, a calibrated orifice, an inclined manometer, and a calibrated dry gas 

meter. 

The sample probe and oven box were maintained at a temperature between 248°F and 275°F to 

prevent moisture condensation. A cyclone was not be used with the ROJAC sampling train. The 

ROJAC 

,. 

AIR TESTING/0 I SERVICES, 

INC. q 

RBKF9903 

KF Tunnel Kiln Report 

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5.0 QA/QC ACTIVITIES 

5.1 QC Procedures 

Specific quality control (QC) procedures were followed to ensure the continuous production of 

useful and valid data throughout the course of this test program. The QC checks and procedures 

described in this section represent an integral part ofthe overall sampling and analytical scheme. 

Strict adherence to prescribed procedures is quite often the most applicable QC check. A 

discussion of both the sampling and analytical QC checks that were utilized during this program 

is presented below. 

5.2 Sampling QA/QC 

All measurement devices including sample nozzles, probes, and dry gas meters were uniquely identified 

and calibrated prior to and at the completion of this test program. All post test calibrations met their 

acceptable ranges. Sampling isokinetics were within their acceptable range for all extractive tests. CEM 

analyzers met their daily calibration and drift requirements. Copies of all equipment calibrations are 

contained in Appendix E. 

5.3 Laboratory Analytical QAJQC 

Field blanks of all applicable sampling reagents were taken in accordance with their respective sampling 

methods. Due to the negligible contaminants found in the reagent blanks, blank corrections were not 

calculated for the final results. Compressed gases used as CEM calibration standards were NIST 

traceable. Laboratory method blanks, spike recovery and duplicate analyses were performed where 

applicable and met their targeted ranges. · 

RBKF9903 

KF Tunnel Kiln Report 

- 9-

ROJAC 

AIR TESTING 

SERVICES, II 

INC. ~~ 
:> 

:> 

) 

) 

) 

' .. 

--

) ~~ 

Stack 

Will 

• ~ ~ ~ I ~ t~ ~~ Calibration Valve I Teflon Sample. Pump THC ;=== Analyzer 

co 

Analyze

NO/NOX 

Analyze

~ Heated ss Probe ~~~ I Condenser 1 ~ I J Heated Teflon Sample 

- Teflon Sample Line I Line 

I 

I 

--------

PermaPure Dryer 

·r 

so2 

Analyzer 

Oxygen 

Analyzer 

co 

Analyze

't •• 

EPA Reference Methods JA, 6C, 7E, 10, and 25A 

Continuous Emissions Monitoring Sampling System 
Appendix B 

Summary of Test Results 

RBKF9903 

KF Tunnel Kiln Final Report 

ROJAC 

;3 

f?~ 

AIR TESTING 

SERVICES, 

INC. 
RUN NO.: 

DATE: 

TIME: 

PBAR, (in. Hg) 

STACK AREA, (Sq. Ft.) 

NOZZLE DIA., (in.) 

TOTAL TIME, (minutes) 

CALIBRATION FACTOR 

PITOT COEFFICIENT 

SQ.RT.DELTA P, (in. H20) 

DELTA H, (in. H20) 

METER TEMP., (Degree F) 

STATIC PRESS., (in. H20) 

STACK TEMP., (Degree F) 

METER VOLUME, (cu.ft.) 

TOTAL H20 VAPOR, (ml) 

C02 IN STACK GAS,(%) 

02 IN STACK GAS,(%) 

CO IN STACK GAS, (%) 

N2 IN STACK GAS,(%) 

TOTAL HCI CATCH, (mg) 

HYDROGEN IN FUEL, (%) 

CARBON IN FUEL, (%) 

SULFUR IN FUEL,(%) 

NITROGEN IN FUEL, (%) 

OXYGEN IN FUEL, (%) 

GCV, (BTU/Ib) 

F-FACTOR, (DSCF/MMBTU) 

METER VOL. STD, (cu.ft.) 

H20 IN STACK GAS,(%) 

STACK GAS MOLECULAR WT 

EXCESS AIR, (%) 

STACK GAS VEL., (FPM) 

GAS FLOWRA TE, (ACFM) 

STP FLOWRATE, (DSCFM) 

ISOKINETIC, (%) 

HCI CONC., (GR/ACF) 

HCI CONC., (GR/DSCF) 

HCI CONC., (GR/DSCF@7%02) 

CONC., (GR/DSCF@12%C02) 

CONC, (GR/DSCF@50%EA) 

EMISSION RATE, (lb/hr) 

F-FACTOR, (DSCF/MMBTU) 

EMISSIONS, (lb/MMBTU) 

Acid Gas Summary 

RBKF9903 

Summary of Hydrochloric Acid Emissions 

Absorber Outlet Stack 

Redland Brick/KF Plant 

South Windsor, Connecticut 

M26A-1 M26A-2 M26A-3 

6/10/99 6/10/99 6/10/99 

1003- 1132 1239 -1409 1444- 1612 

30.05 30.05 30.05 

12.05 12.05 12.05 

0.283 0.283 0.283 

84 84 84 

1.0091 1.0091 1.0091 

0.84 0.84 0.84 

0.6760 0.6680 0.6520 

2.016 2.0175 1.9333 

96 111 110 

0.5 0.5 0.5 

313 312 311 

65.027 65.586 64.445 

81.1 72.4 72.8 

2.0 2.0 2.0 

17.6 17.8 17.8 

0.0 0.0 0.0 

80.4 80.2 80.2 

28.00 23.00 24.00 

9570 9570 9570 

62.93 61.78 60.76 

5.72 5.23 5.34 

28.39 28.46 28.44 

485.4 527.8 527.8 

2770 2733.67 2665.83 

33382 32941 32123 

21623 21462 20951 

95.6 94.6 95.3 

4.45E-03 3.74E-03 3.98E-03 

6.87E-03 5.74E-03 6.09E-03 

2.89E-02 2.58E-02 2.73E-02 

4.12E-02 3.45E-02 3.66E-02 

2.68E-02 2.40E-02 2.55E-02 

1.27 1.06 1.09 

9570 9570 9570 

5.95E-02 5.30E-02 5.62E-02 

AVERAGE 

30.05 

12.05 

0.283 

84 

1.0091 

0.84 

0.6653 

1.99 

106 

0.50 

312 

65.019 

75.43 

2.0 

17.7 

0.0 

80.3 

25.00 

0.00 

0.00 

0.00 

0.00 

0.00 

0 

9570 / 

61.82 

5.4 

28.43 

513.6 

2723.27 

32815 

21346 -~ 

95.2 

4.06E-03 

6.23E-03 

2.73E-02 

3.74E-02 

2.54E-02 

1.14 

9570 

5.62E-02 14 

¢ 

ROJAC Air Testing 
RUN NO.: 

D.~TE: 

TIME: 

PBAR, (in. Hg) 

STACK AREA, (Sq. Ft.) 

NOZZLE DIA., (in.) 

TOTAL TIME, (minutes) 

CALIBRATION FACTOR 

PITOT COEFFICIENT 

SQ.RT.DELTA P, (in. H20) 

DELTA H, (in. H20) 

METER TEMP., (Degree F) 

STATIC PRESS., (in. H20) 

STACK TEMP., (Degree F) 

METER VOLUME, (cu.ft.) 

TOTAL H20 VAPOR, (ml) 

C02 IN STACK GAS, (%) 

02 IN STACK GAS,(%) 

CO IN STACK GAS,(%) 

N21N STACK GAS,(%) 

TOTAL HF CATCH, (mg) < 

HYDROGEN IN FUEL, (%) 

CARBON IN FUEL, (%) 

SULFUR IN FUEL, (%) 

NITROGEN IN FUEL, (%) 

OXYGEN IN FUEL, (%) 

GCV, (BTU/Ib) 

F-FACTOR, (DSCF/MMBTU) 

METER VOL. STD. (cu.ft.) 

H20 IN STACK GAS,(%) 

STACK GAS MOLECULAR WT 

EXCESS AIR, (%) 

STACK GAS VEL., (FPM) 

GAS FLOWRATE, (ACFM) 

STP FLOWRA TE, (DSCFM) 

ISOKINETIC, (%) 

HF CONC., (GR/ACF) < 

HF CONC., (GRIDSCF) < 

HF CONC., (GR/DSCF@7%02) < 

CONC., (GR/DSCF@12%C02) < 

CONC, (GR/DSCF@50%EA) < 

EMISSION RATE, (lb/hr) 

F-FACTOR," (DSCF/MMBTU) 

EMISSIONS, (lb/MMBTU) 

Acid Gas Summary 

RBKF9903 

Summary of Hydrogen Fluoride Acid Emissions 

Absorber Outlet Stack 

Redland Brick/KF Plant 

South Windsor, Connecticut 

M26A-1 M26A-2 M26A-3 

6/10/99 6/10/99 6/10/99 

1003-1132 1239-1409 1444-1612 

30.05 30.05 30.05 

12.05 12.05 12.05 

0.283 0.283 0.283 

84 84 84 

1.0091 1.0091 1.0091 

0.84 0.84 0.84 

0.6760 0.6680 0.6520 

2.016 2.0175 1.9333 

96 111 110 

0.5 0.5 0.5 

313 312 311 

65.027 65.586 64.445 

81.1 72.4 72.8 

2.0 2.0 2.0 

17.6 17.8 17.8 

0.0 0.0 0.0 

80.4 80.2 80.2 

1.00 < 1.00 < 1.00 < 

62.93 61.78 60.76 

5.72 5.23 5.34 

28.39 28.46 "28.44 

485.4 527.8 527.8 

2770 2733.67 2665.83 

33382 32941 32123 

21623 21462 20951 

95.6 94.6 95.3 

1.59E-04 < 1.63E-04 < 1.66E-04 < 

2.45E-04 < 2.50E-04 < 2.54E-04 < 

1.03E-03 < 1.12E-03 < 1.14E-03 < 

1.47E-03 < 1.50E-03 < 1.52E-03 < 

9.57E-04 < 1.05E-03 < 1.06E-03 < 

0.05 0.05 0.05 

O.OOE+OO O.OOE+OO O.OOE+OO 

AVERAGE 

30.05 

12.05 

0.283 

84 

1.0091 

0.84 

0.6653 

1.99 

106 

0.50 

312 

65.019 

75.43 

2.0 

17.7 

0.0 

80.3 

1.00 

61.82 

5.4 

28.43 

513.6 

2723.27 

32815 

21346 

95.2 

1.62E-04 

2.50E-04 

1.10E-03 

1.50E-03 

1.02E-03 

0.05 

0 

O.OOE+OO r)" 

r?t 

ROJAC Air Testing 

- - - - -
EPA Method 1 Sample and Velocity Traverse· 

for Stationary Sources 

Firm Redland Brick, Inc. Total Traverse Points Required __ --~12

Location South Windsor, CT Number ~~-------- of Ports Diameters Upstream 10 Points Per Port-----------------z:----------

Diameters Downstream_7.~...:·~5 ___ Traverse (Horizontal or Vertical)_H _____ _ 

·MINIMUM NUMBER OF TRAVERSE POINTS FOR PARTICULATE AND NONPARTICULATE TRAVERSES 

Duct Diameters Upstream from Flow Disturbance 

(Distance A) 

50~....-~....-~~--~--~--~T----r---.---, 

0.5 1.5 2.0 

HIGHEit NUUIIUI &S POit 

ltiC'TAHGULAA rTACJtS OA Duc:TI 

PARTICULATE 

1 8 18 rTACit Dw.IETE" > G.lla 12& kJ 

-------------------~--~ \__NONPARTICULATE •--- _.___....,..;.;,

2

;o.a_o_r_8_--1 

r~ .. I 

1 

l 

Deq • 2LW = L+W · -v---

Sample 

Port 

r 

352" 

02~....-~----~-~----~--~--~~-~-~10 r---------------------~ 

Duct Diameters Downstream CROSS-SECTIONAL LAYOUT from Flow Disturbance FOR RECTANGULAR STACKS · {Distance B) Total 

LOCATION OF TRAVERSE POINTS IN CIRCULAR STACKS 

Point (Percent of stack diameter from 

Number inside wall to traverse point) 

On A Number Of Traverse Points On A Di_ameter 

Diameter 4 6 8 10 12 

1 6.7 4.4 3.2 2.6 2.1 

2 25.0 14.6 10.5 8.2 6.7 

3 75.0 29.6 19 .4· 14.6 11.8 

4 93.3 70.4 32.3 22.6 17.7 

5 85.4 67.7 34.2 25.0 

6 95.6 80.6 65.8 35.6 

7 89.5 77.4 64~4 

a 96.8 85.4 75.0 

9 91.8 82.3 

10 97.4 88.2 

Traverse Points Matrix 

3x3 · 4x3 

4x4 

5x4 

5x5 

No. 

1 

2 

3 

4 

5 

6 

7 

8 

9 

10 

11 

9 

12 

16 

20 

25 

.TRAVERSE POINT LOCATIONS 

Distance Nipple ·Total 

From Wall Size Distance 

2.0 3.5 5-5 6.9 3.5 10.4 

13-9 3.5 17.4 

33.1 3-5 36.6 

40.1 3-5 43.6 

44-9 3-5 48.4 

. 

-

0 

t 

~ 

0 

-J 

~ 

11 93.3 12 

1? 

000 ~ 
EPA METHOD2 

VELOCilY TRAVERSE AND FLOWRATE DETERMINATION 

Date 

Plant 

Location 

Stack Dimensions 

Barometric Pressure, (Pb) 

Static Pressure, (Ps) 

Stack Molecular Wt., (Ms) 

Moisture Content 

Point 

A--I 

d-.. 

3 

1-

~c;-

C:, 

13- I 

.:::2 

..) 

1-

s0 

Average 

-11--L-r_'_' __ Area /.;7 ~o 5 rt'2 

.....,1~.....::..<1....:..'...:..\:... __ , __ ln. Hg. 

_____ ln. H20 

-----" 

DeltaP Ts Cyclonic 

inch H20 {'F) Flow Angle 

:5/C:C /C 

_7. II /0 

3'/?- /0 

c? I 'f c;;: 

.sis ~~ 

Jtl /C 

3/.9. /s 

J/..:3 ~I") 

Jls- 1<:::::: 

21+ ~ 

..313 /0 

JIJ ~ 

Abaolute Gaa Temperature • Ta + 480"R 

Abaolute Gu Preuure. Pg • Pb + Pa/13.1 

Ta + 400 

Gaa Velocity. Va • (IS.4D) ll (Cp) ll (Delta P"1/2)avg x SORT ( ---1 

Pg X lob 

~ual Gaa Flowrate, Qa • (Va) x 10 x Ina 

· Page or -----

Pitot No. '

1 

6 ( 

Leak Check ../ ln. H20 

Pitot Coefficient 0 t 84 

Tester 

0 9a:J 

Other Other 

_____ tlaec 

____ .....;ACFM 

Standard Gaa Flowrate. Qatd • (Qa) x ~ X fJl X 100 - 'I(.H20 _____ DSCFM 

Ta 100 /l(\111110 
/008 ~0 CEMSSYSTEMCALffiRATIONAND.DRIFTDATA f 1'3'-- Jl68 

Project No.; R (J iC rcr era 3 Date; G ,,1) ''i1 Run No.:_l_ 

Test Location: ,4--b 50 r 6 e.r 0'-'1. 1--'1 e. f Start Time: g 11- End Time: I I 2 0 

'? 1'!2..-7 .,, ;') 1 Sowce Equipment: 70 ...., A-(: ( K, 7 f') Start Scan#: .) v '- End Scan#: _ n ........... ~--

Comments: 

I~ 

~ 

00 015 
CEMS SYSTEM CALIBRATION ANI} DRIFT DATA 

Project No.: 

Test Location: r ----~----------------

Date: b /10 /1) Run No.:~ 

Start Time: 1/L/fi End Time: __../ ..... lf....;;o~F/~-

Source Equipment:------------------ Start Scan#: /l_${) End Scan#: ZCO,'( 

Comments: 
CEMS SYSTEM CALIBRATION AND DRIFT DATA 

Project No.: _______ _ 

Test Location: -------------- Source Equipment: ___________ __ 

Comments: 

Date: -------- Run No.:$ 

End Time:~ 

End Scan#:~ 

Start Time: ~L{ "Z.:f 

Start Scan#: 1,114 
CEMS ANALYZER CALIBRATION DATA 

Date: June I 0, 1999 Source Equipment/Mode: Kiln Tunnel 

Project No.: RBKF9903 

---------------------------

Test Location: Absorber Outlet Stack 

0 2 Analyzer ID: 1400 

---------------~ 

0 2 Span Value: 25.0 

0 2 zero: 

0 2 mid: 10 to 15 % 

0 2 high: 20 to 25 % 

C02 Analyzer ID: 1400 

---------------~ C02 Span Value: 20.0 

C02 zero: N2 or 

C02 mid: 8 

C02 high: 16 to 20 % 

S02 Analyzer ID: 741 

---------------~ S02 Span Value: 100.0 

S02 zero: or air( <0.25% of span) 

so2 mid: 40 to 60 ppm 

S02 high: 80 to 100 ppm 

NO. Analyzer ID: 

----------------~····························· NO. Span Value: 100.0 

NO. zero: N2 or air(<0.25% of span) 

NO. mid: 40 to 60 ppm 

NO. high: 80 to 100 ppm 

0.0 

12.0 

StartCal: 814 -------- Start Scan#: _______ ....:........ 69 

Analyzer 

Response: 

0.0 

12.0 

CO Analyzer ID: ------------~ > >>< >•···•·:c·:·····•·•·•·······•·•••.:.:cc.:·••••••• 

CO Value: 100.0 

CO zero: pure N2 

CO low: approx. 30 

CO mid: approx. 60 

co high: approx. I 00 ppm 

Analyzer ID: ---------------~ 

THC Span Value: 100.0 

Cal Gas: 

THC zero: 

THC low: 25 to 35 ppm 0.0 0.0 #DlV/0! 

THC mid: 45 to 55 ppm 0.0 0.0 #DIV/0! 

THC high: 80 to 90 ppm 0.0 0.0 #DIV/0! 

CEM Data Results RBKF9903 Analyzer Cals 

End Cal: 855 

End Scan#: 285 

#DIV/0! #DIV/0! 

#DIV/0! #DIV/0! 

#DIV/0! #DIV/0! 

ROJAC Air Testing 
CEMS SYSTEM CALIBRATION AND DRIFT DATA 

Date: June I 0. 1999 Project No.: RBKF9903 RunNo.:_2_ 

Test Location: Absorber Outlet Stack Start Time: 1239 End Time: 1409 --------- --------- Source Equipment: Kiln Tunnel Start Scan#: 1575 End Scan#: 2095 

----------------------------

11.9 

17.6 

12.0 

17.8 

0.0 

10.1 

2.0 

10.1 

2.0 

0.8 

49.3 

26.1 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

Comments: 

CEM Data Results RBKF9903 R2 ROJAC Air Testing 

"""'"'"""-.4 
CEMS SYSTEM CALIBRATION AND DRIFT DATA 

Date: June I 0 1999 Project No.: RBKF9903 Run No.:_3._ 

Test Location: Absorber Outlet Stack Start Time: 1444 End Time: 1612 --------- ---------- Source Equipment: Kiln Tunnel Start Scan#: 2297 End Scan#: 2802 

----------------------------- ---------

Pre~Cal·· Syste..r~ · .· Post~Cal . >····.·.··· .. · .. 

$ystem Bias .System 

-0. I 

CEM Data Results RBKF9903 R3 

Bias < • ····•·• ])rift : . ·:·.·._:. :··.-.. :: .. ·. 

(<5% spa~} (<J )~§pan) 

0.4% -0.1 

Il.8 

17.5 

12.0 

17.8 

0.0 

10.1 

2.0 

10.1 

2.0 

0.6 

49.3 

27.7 

50.6 

28.2 

0.0 

0.0 

0.0 

0.0 

ROJAC Air Testing 

{\(\(\('\r}f') 
EPA METHODS FIELD DATA 

RUN NO. .}l.. 

PROJ. NO. &3 99d J 

MODULE NO. ;J...f r 7 PITOT LEAK CHECK 

DGM, Y 1. dtJ 9, 

DATE_$L.uJ/97 

FIRM NAME;hlj.,.,..J' 

MOD.&-!@ ' (/ 7 7 

1.0. G 4 r 

PLANT Loc.J:. M-ves-,..1, cr PITOT (Cp) 0. r¥ 

NOZ. DIA. c) •. .;l-J' 3 

f'/CS FILTER 1.0. /I/ /.ITRAV. 

PT 

I 

;>-. 

.] 

'T 

r 

c; 

a 1 

31.. 

.J 

.,., 

1-

t:. 

TARE WT. AI ,4-' 

SAMPLE 

TIME 

(min) 

_'2_ 

/.J:l7 

CLOCK VEL. ORIFICE 

TIME I llP I llH 

(hours) 

r. t:!r 1' ,. 111.-=f'" I _d._ c,- ? 

l.1+f 3 lo._r.rl iJ tr-0 lo ( .% r ..a.ft'f . /3 tJ7 IO· ILrY 

/.11 Ykf,.y.r l.hti 

I 3 J-l __ / 111. s= 21 !7-· o-

/.3 0.'.:r·5" Yf 

/ .//C/3' if:'.:-..('.:1__l_a_dG: 

t . .:r-s-1 o.3 1 /, 3 

la.3G" 1 ;"r f4.3 

v ¥ iJ·CK. ro. J ,;1_ 1 /, ¢1 

,;>__4.z..J. 

AVERAGE I llP I 

SORT (llP) ,. H 9 .i' {7 ') 

DGM 

Tmln 

"F 

P9 

//Y" 

/d-r.J 

/Oi,;L. 

./,,1 . .2-

/II 

/...:1.3' 

'.Ldl-.3 

$3' 

/:2./ 

DGM 

Tmout 

"F 

£L. 

/{)I 

/t:rL 

L.Clc:J-. 

/cJ...3 

/0..:3 

/d-..3 

/cJ..:J 

/e!JS" 

,rc..J 

/oCJ 

/6<fl 

II 0.1.::; 

INITIAL ./ 

FINAL 

TRAIN LEAK CHECK 

INITIAL.:::l, d /0 ft @ /6 in. Hg. 

FINAl(H41C' ft @ 11 ln. Hg. 

SAMPLING TIME J?'Y min. 

INITIAL 9 

FINAL / ro--9 

STACK I GAS SAMPLE 

TEMP. VOLUME Vm 

T• • F ft 

.3_;)-{j 

'!J,;o 

...JarJ 

.ALf 

.;Lff; 

j.-:J.-1 

3d-/ 

1.2/& 

3/0 

\ 

j_ 

TOTAL 

31t,'} ' lb.5' A 'S8'b 

COND. 

OUTLET 

"F 

S7" 

..r.z... £8 

..::J::.1L 

..51' 

s:9' 

rY 

_s--y 

".y.. s'¥' 

HEATER 

BOX 

"F 

cJ. yJ 

L-:iz._-!'r IO' y OJ. 

VC 

d "?' 7 

AS9 

ol(]-/ 

.;tVd 

cJ-rY 

c? crJ 

cJ..W 

PROBE 

TEMP. 

"F 

ass 

cJZ..JP 

.-ils-7 

::,.ts-G 

61-J-y 

STACKCO

STATIC 

DUC

DUC

AMBIENT 

AMB

....• BAR

FILTE

OUTL

•f 

ORSAT BAG ANALYSIS 

REMARKS 

lmpingers H20 Gain b } 

Sili:a Gel H20 Gain l J · '-'1 

Total Moiatwe Gain /Z.'f 

1 2 3 AVERAGE 

l ;· I I I I 

IS'J 

/0? 

100 
RUN NO. '3 

PROJ. NO. 

DATE. 

FIRM NAME 

PLANT LOC. 

TRAV. SAMPLE CLOCK 

PT TIME TIME 

(min) (hours) 

7 /7"'1</ 

,d._, I /"/,'J~/ .:1 I /Y"."'I"i?' 

J I /ftl.<" 

t' ~"" /,-101-

·_,- 1-t" /'I 

(, /."r ..:;...' lir 1 .J ·3a /r~7 J- 7 11-·/y ~7 I / .. J..J/ 

<i -, l!r-.J? ~ \ 1/..:; /.1 .r 

c; v 1/l' / ;JAVERAGE AP 

SORT (AP) 

:> 

:> lmpingers H20 Gain 5" 6 

::> 

::> Sili::a Gel H20 Gain /b. g 

J 

n Tot.! MoiaiiA'e Gain "7 Z.t ~~ ~ EPA METHODS FIELD DATA SHEET. MODULE NO. .-J.tf-~7 PITOT LEAK CHECK STACKC

DGM,Y t,c::rV~ INITIAL y" STAl

MOD.AH@ t..,7.Z FINAL- v D

PROBE I.D. ·cot. TRAIN LEAK CHECK DU

PITOT (Cp) CZ.·L.'L INITIAL.d. OdJ=' ft • @ / Z,. in. Hg. 

NOZ.DIA. f2., rl.l:..3 FINAL(}, cloy ft • @ /q2- ln. Hg. AMBIENT 

FILTER I.D. ..u~ SAMPLING TIME B:t min. AM

TAREWT. /VA INITIAL /cr4;'if BA

FINAL /G'/ VEL. ORIFICE DGM DGM STACK GAS SAMPLE COND. HEATER PROBE FILT

AP AH Tmln Tmout TEMP. VOLUMEVm OUTLET BOX TEMP. OUT

"F •f Ta •f tt• I ~v a .. 4 .52::l •f •f ·F "F 

(),S.] ..:?, 3 :;z. /Qr:J /.n) '?I 7 -rfi'" ~ ~(/~ 

t1,.1"".-J .;.. 1/J- //~ /cJ :?- -~~~ s-O ~v·s- .:2. .,.-:2.. 

Ill ~rr., ~ .. <19 ~~I /LJ ") ~.;2( ..s',....:l- ~ .,.,;, .J_ '7"7' 

1'1-~ ;.~ ·.::J.d.. / £) ·<I -~/=? -~ ;J_ .:J_'y .,;LS-:L 

() '.J !" /,.Jt) ;;JJ /C) ~q ~ol £"/ "3.2 J- .)..)! 

d, 3t" / r7 ~~ 10# :::tCJ:J 1""/ ~ :J I 1.::?-~~ 

(),?Y ~4 (;if"' /// iJi-1.£.. :J / Ji :-r--:1 .:J .r·-,... l.;t S"" .J 

Vi.rY :;:;,ySf' /.:1-0 /tJ y' ':l . .:J../ ..:j-.3 ~""]/" --:J. c l, 

'o. TI I 77"7 /Jn /rJ ¥ """"'1/J- 5'7 ~ (, (J ....:2.:rr- 

la • .11 ':;). ::1"7 j~ //) y -:1/P f7 _). .f?' .;l. .,-,.)... 

It?, J' .:1.. /.¥7" :/;:) :.z /(')(/ .:fi?Y' .r7 .:> "/ .-r- .;2~-~- 

a -:1 .1.. /,J'O !.;;;b . '/af? ~;.<J J7 .:5)..3 ~ .J.s-.3 

2. ~.20 lOa Sf". !l'l.J J. 933~ I/ rJ :Sib.!.:. TOTAL ro.~ 7,5 ''"" .'1'"'15 REMARKS ORSAT BAG ANALYSIS JTPflow«M( 

1 2 3 AVERAGE J ; I I I I fi% I 1'-1! 7t.; Iff 
... _, = 18.8 -, f:" 

.::.. .... .J 18. ·:;. 

4. '3 18. 1 

:4.8 18.2 

4. '3 18.:2 

5.5 18.3 

5.7 18.3 

5.4 18.3 

5.4 18.3 

5. 4 18.3 

5. '3 18.2 

5.7 18.2 

3.8 18.2 

3. '3 :1.8. 2 

5.8 18.3 

s.o 18.3 

5. '3 18.4 

3. ~3 8. 1 

3.:2 1. 4 

. 4 o . 1. 

.0 --0.0 •:'.I • -1 ·-0. 0 

.5 0.0 

. 4· -0.0 

/6 

I I!(/ 

~eel/a/lei !J1,-lc-k 

;c r tJI C{ /1. t0.0 1. 70 6':3 172502 

0.0 1. 60 70 172512 

0.0 2. 10 y--:• ..:.. 81448 

0.0 .-. 

..::... 10 73 81458 

0.0 2.10 74 81508 

0.0 ~. .. ::. . 10 75 81518 

0.0 2. 10 76 81528 

0.0 ..::.. -. 10 77 81538 

0.0 2.10 78 81548 

0.0 2.10 79 81558 

o.o 2.10 80 81608 

0.0 2.10 81 81618 

o.o 2. 1<) 8·-=· ..:.. 81627 

0.0 2.10 83 81638 

0.0 2 .. 10 84 81648 

0.0 2.10 85 81658 

0.0 2.00 86 81708 

0.0 0. ':30 87 8171':3 

0.0 0.10 88 817:2'3 

0.0 -0.00 89 817·::f·O 

0.0 -0.10 '30 81751 

0.0 --0. 10 '31 81801 

0.0 -0.10 '32 8:1. 81:!. 

0.0 -0. 1.0 •::J~3 81821 

....... - -·------~ _, 

~ - - -- ~ ·~ 
me 

. 2 

.0 

. 8 

• 7 

• 7 

. 7 

. 7 

0. 1 

0.6 

0.5 

(> .. 5 

.2 

0.3 

C) • :.~ 

c). 3 

0.5 

0.3 

0.5 

0.3 

0.8 

0.3 

(l. 2 

0.5 

0.5 

~). 3 

:).3 

:). 5 

:).7 

:). 2 

:) • 5 

:) .. 3 

). 6 

). 7 

). 3 

). 2 

). 3 

). 6 

). 6 

). 7 

). 5 

). 5 

). 6 

). 8 

). 5 

)~ 3 

). 5 

). 7 

). 7 

). 5 

). 7 

). 8 

). 7 

). 8 

). 7 

). 7 

). 8 

) . 5 

). 8 

) . 8 

) n 5 

) . 8 

0.0 

-0.0 

0.0 

0.0 

-0.1 

-0.0 

-0.0 

-0.0 

-0.0 

-0.0 

-0.1 

0.0 

--0. 1 . 

-0.1 

--0.0 

0.0 

0.1 

.::J .• 9 

11.3 

1:2 .. 3 1 .-. r:::- ..::. • ...J 

12.5 

12.5 

12.5 

12.5 

12.5 

12.5 

12.5 1 .-. C' 

..::..~ 

12.5 

12.6 

12.5 

12.5 

12.5 

12.5 

12.5 

12.5 

12.5 

12.5 

12.5 

12. E. 

12.5 

12.5 

12.6 

12.5 

12.5 

12.5 

12. E. 

15. E. 

21.1 

21.7 

22.0 

21.9 

21.9 

22. (> 

21. •3 

2:2. (l 

21.'3 

21. '3 

0.0 

0 .. 0 

0.0 

0.0 

·o.o 

o.o 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

.0. 0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

-0. 10 

-0. 10 

-0.10 

-0. 10 

-0.10 

-0.10 

-0. 10 

-0.10 

-0.10 

--0. 10 

-0. 10 

-0.10 

-0.10 

0.00 

0.00 

0.00 

0 .. 00 

1. 00 

9.30 

10.70 

10. '30 

10. '30 

10. '30 

10. '30 

11.00 

10.90 

11.00 

11.00 

11.00 

11.00 

11.00 

11.00 

11.00 

11.00 

11.00 

11.00 

11.00 

11. 00 

11.00 

11.00 

11..00 

11.00 

1 ., {')(~ 

.i, ... "" ... · •• 

1.1.00 

11~00 

11. 00 

11.00 

11.00 

12.70 

18.80 

1'3. 20 

19.50 

1'3. 50 

1'3. 50 

1'3. 50 

19.50 

1'3. 50 

1'3. 50 

1'3. 50 

1'3. 50 

1'3. 50 

96 

'37 

'38 

'3'3 

100 

101 

102 

103 

104 

105 

106 

107 

108 

109 

11 i) 

111 

112 

113 

114 

1.15 

116 

117 

118 

11'3 

120 

1:21 

122 

123 

124 

125 

126 

127 

128 

12'3 

130 

131 

132 

133 

134 

135 

136 

137 

,! .-.--. ! . . ::.;·:_ .. _; 

13'3 

140 

141 

142 

143 

144 

145 

146 

147 

148 

149 

150 

151 

152 

153 

154 

155 

156 

81851 

81901 

81910-

81'321 

81'330 

81941 

81951 

82001 

82012 

82(>22 

82032 

82042 

82052 

82102 

82111 

82122 

82133 

82143 

82153 

82:203 

82213 8 .-.. -. .-.,..... ..::...::....::.w 

82243 

82253 

823t)3 

8:2314 

8232·4 

82335 

82346 

82357 

82407 

82417 

82426 

82437 

82447 

82457 

82507 

82516 

82527 

82537 

82547 

8:2557 

82608 

82619 

82630 

82640 

82650 

8265'3 

82710 

82722 

82732 

82742 

82752 

82802 

8281:2 

82822 

82833 

82843 

82853 
y ..::: ~ • l_l '.). \.) l 0 • l.JV • .:::...::-=+ ~"tJ,.::H:l 

' ·21. 0 0.0 18.00 225 8454'3 

\Jl o\ ( I . 5 21.0 0.0 18. 10 :"226 84600 \ I . 

/L .· ;\ D,o7 . 6 21.0 0.0 18. 10 22iT 84610 ' ./ .1 

.6 :21.0 0.0 18.00 ~"228 84621 

6 21.0 0.0 18.00 22'3 84631 . ' 

.6 20. '3 0.0 18. 10 230 84641 

.6 20.6 0.0 17. '30 231 84651 

' '3 17.3 0.0 15 .. 60 23:2 84701 

. 1 1...., .-. ,:, • L 0.0 1.1. 60 .-,,.....1""'\ 

L...::J..:J 847Ll _ .. -

.. '3 1"? . ., ~· ~ 0.0 10.40 ~:34 84721 

. 4 12.0 0.0 10.30 235 84731 

. 8 11.'3 0.0 236 /s4741 

·- g;j -···. . (~! 237 ./84752 •.. ,. -~- . 

.6 - 0.0 238 84803 

.4 

.6 

12.0 

12.0 0.0 

0.0 

10.20 

1(i. 2(1 

:23'3 

:;~.:.~() 

84813 C\h\ I~")/ 84823 

.6 12.0 0.0 10.20 241 84833 

:.6 11. '3 0.0 10.20 242 84843 / .6 12.0 0.0 10.20 243 

.6 12.0 0.0 10.20 244 

.6 11.8 0.0 10.20 245 

.4 4.5 0.0 4. 10 .-.4y/ ..::. ' 84'325 

;. 7 0.6 0.0 o. 60 _......./2~7 84'336 

L.7 C) • 1 0.0 0. 21)/.- 248 84'346 

)4,. 2 -0.0 0.0 _ .......... o·:·f() 24'3 84'357 

)2. 9 0.0 0.0 / .• - o. 10 250 85007 

:... 8 0.0 0 lY.- o. 10 251 85018 

5. 5 -0. 1 ~~~) 0.10 :25:;~ 85029 

L5 -0. 1 · o.o o. 10 ~"253 8504<) 

5. 4 o.o 0.0 0. 10 254 85051 

~ -0.0 0.0 0. 10 255 85101 

). o. 0.0 0.0 0. 10 256 85111 

3. 2 -0.0 0.0 0. 10 257 85121 

:;. 4 -0.0 0.0 0. 10 258 85131 

).. •::J· (),. 2 0.0 0.20 25'3 85141 

5.0 4 .. '3 0.0 2.60 260 "85150 

~. B 1.0. 5 0.0 8.60 261 85201 

.. 4 1 1.7 o.o 9. '30 ~"252 85212 

.• 4 1 1. '3 0.0 10.20 263 8522:'2 

6 1 1. '3 o.o 10.20 264 85233 )'I ) .. 3 1 1.'3 0.0 10.20 265 852~43 
.0 

. 2 

o. 1 

~): 1 

':> •'-' 

·3. 6 

3. '3 

3. 3 

3. 4 

' 

). 2 

C•2 

ne 

,) • '3 

). 4 

0.2 

). 4 

:). 6 

3.4 

7. 7 

). 5 

2.5 

7. '3 

:).7 

2. 0 

2. 6 

.3. 0 

?:. 6 

3. 6 

:+.4 

~- 6 

4.6 

3 . ~ ...., 

1. 1 

.7 

.6 

.6 

. o 

.6 

' 1 

,._, 1:" 

11. '3 

12.0 

11. '3 

'3 .. 9 .-. .... ..::..u 

(l ':> ..... ,_] 

0.0 

-0.0 

0.0 

-0.0 

0.0 

0.0 

-0.0 

(>2 

-0.0 

-0. 1 

-0.0 

0.0 

0.0 

11.:2 

16.8 

17.8 

17.8 

17.'3 

17.'3 

17. '3 

17.7 

17.7 

17.6 

17.6 

17.5 

17.5 

12.3 

12.0 

11. '3 

12.0 

12.0 

11. '3 

11.'3 

0.0 

0.0 

o.o 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0.0 

0~0 

0.0 

o.o 

0.0 

0.0 

0.0 

0.0 

0.0 

o.o 

0.0 

0.0 

o.o 

- - - -·- 10.20 

10.20 

10.20 

'3.30 

2. 2() 

0.40 

0. 10 

0.00 

o. 10 

0.10 

0. 10 

0.00 

1. 20 

1. '30 

1. 80 

1. '30 

1. '30 

1. '30 

1. '30 

2.00 

2~00 

2.00 

.-. 

..::.. 10 

2.10 

2. 10 

5.00 

'3. 30 

10.00 

10. 10 

10. 10 

10. 10 

10 • 10 

26'3 

270 

271 

272 

273 

274 

275 

276 

277 

278 

27'3 

280 

281 

282 

283 

28··1-

285 

286 

287 

288 

28'3 

2'30 

2'31 

2'32 

2•33 

2'34 

2'95 

2'3E, 

2'37 

2'38 

2'3'3 

300 

301 

302 

303 

304 

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3. 1 16.6 0.0 2. 2() 132'3 115636 

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3. 5 18.8 0.0 0.80 1335 11573'3 

7. 5 1'3. 0 0.0 0.70 1336 115750 

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7. 5 18.9 0.0 0.80 1338 115812 

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7. 5 17.5 0.0 1.90 134'3 120007 

7. '3 17.5 0.0 2.00 1350 120017 

7. 9 17.5 0.0 1. '30 1351 120027 

3. 0 17.5 0.0 2.00 1352 120037 

3. 1 17.5 0.0 2.00 1353 120047 

3. 6 17.5 0.0 1. '30 1354 120056 

3. 6 17.5 0.0 2.00 1355 120107 

3. 7 17.5 0.0 1. '30 1356 120117 

3. 8 17.5 0.0 2.00 1357 120127 

3. 5 17.6 0.0 1. '30 1358 120138 

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3. 5 17.6 0.0 1. '30 1364 120240 

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3. 2 17.5 0.0 2.00 1368 120323 

3. 6 17.6 0.0 2.00 136'3 120334 

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3. 0 17.7 0.0 1. '30 1385 120624 

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3. 5 17.5 0.0 2.00 1387 120646 

3.4 17.6 0.0 2.00 1388 120657 

3.5 17.6 0.0 2.00 138'3 120707 

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3. 4 17.6 0.0 2.00 13'35 120810 

3. 0 17.6 0.0 2.00 13'36 120821 

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3. 5 17.5 0.0 :2.10 1405 "120'352 

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3. 6 17.6 0.0 2.00 1407 121013 

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3. 7 17.7 0.0 2.00 140'3 121033 

3. 5 17.6 0.0 2.00 1410 121044 

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3. 6 17.5 0.0 2.10 1414 121124 

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3. 8 17.5 0.0 :2. 10 1470 122114 

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l. 8 16.4 o.o 2. 2<) 1553 123531 

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.L... ·-:· 10 2834 161737 ·-:· ..:.... 10 :2835 161747 

2. 10 2836 161758 

2" 10 2837 16180'3 .-, 

..::.. 10 :2838 16181'3 

2. 10 283'3 161830 

2. 10 2840 161840 .-. 

...::.. 10 2841 161850 

:211 10 2842 161'300 

2 .. 10 :2:843 161'310 

~~~ .. 10 2844 161'320 

2a 10 2845 161'32'3 

:"2 • 10 2846 161'33'3 

cc,:2: scan t 

.-. 

..::..u 10 :2847 161'350 

2. 10 2848 162001 

;~A 10 284'3 162010 

.-, 

..::. .. 10 2850 16:2021 

2. 10 2851 16203:2 

:2. 10 28~32 16204:2 r 

2. 10 2853 162053 ~--'""' . :2. 10 :2854 162103 ,.-....._ _,., .....: 

2.00 :2:855 162113 t' .... / 

,· \......· . 

-

-··---····-·····-···· 

·~rctj 

\ .-. 

.. ::.. 00 2!3!56 16:2123 

2 .. 00 2857 162133 

1 . '30 2858 162143 

:~~II 00 :285'3 152152 

~A .r)/( 1 . '30 2860 16220:3 c t'-- - - - -
-----

5Di h ,ty:r-u 

i 

7 . '3 17.6 0.0 2.00 2864 16:2243 

J 7. '3 17.5 0.0 2 .. 10 2865 162254 

3. 0 15.0 o. 0 2.00 :7~866 16:2305 

7. 1 r-, 

..:J. 1 0.0 0.60 2867 162316 

1 . J o. 4 0. 0 0. 10 2868 16:2326 .r 

). 8 0. 1 0.0 0. 10 :286'3 162336 

j • 

,..., 

..;:, -0.0 0.0 0.00 2870 1.62346 

7. 0 -0.0 0.0 0.00 2871 162356 

7. 5 -0.0 0.0 0.00 287:::-~ l. f::,2 ::i. <) :.s 

( 3. 1 0.0 0.0 0.00 2873 162415 

:3. ·~1- ·-0. l. 0.0 0.00 2874 162426 

3. 6 o. 0 0.0 0.00 2875 162436 

3. = -0.0 0.0 0.00 2876 16:2446 

X ...J 

3. 0 -0. 1 0. 0 0.00 2877 162456 

3. 1 --0. l. 0. 0 0.00 2878 16:2505 

~- 0 -0. 1 0.0 0.00 287'3 162515 

3. 5 --0.0 0.0 0.00 2880 16:2525 

I 

- l --0. 1 0.0 0.00 2881 162536 :J • 

L 0 -0. 1 0.0 0.00 :2882 162547 

3. 2 -0.0 0.0 0.00 2883 152558 

--0. 1 0.0 0.00 :2884 16:260'3 

0.0 2885 162620 

0.0 2886 162632 

0.0 2B87 162641 .,.·:~G .... -:::t·~· ! f:Jy" 

1. L':." ·") ·..J 11 .8 o.o z911-· 

10. 10 

'· 5 -0. 1 0.0 0.00 :2888 162652 

J. 7 -0. 1 0.0 0.00 288'3 162702 

' .. 5 -0. 1 0.0 0.00 28'30 162712 

.i. 5 -0.0 o.o 0.00 28'31 162722 

,= • ,_J o . '3 0.0 0.20 :7:8'32 16273:2 

.• G 8q6 0.0 6.70 28'33 162742 

\~\0 :. 4 1 1 .3 0.0 '3. 50 28'3•::J. 162751 

'· 1 1 1.7 0.0 10.00 28'35 162802 

.4 11.8 0.0 10.00 .28'36 162811 

.-

.. 

'3 

::. 

. 11 

11 .8 

.8 

0.0 

0.0 

10.00 

10.00 

28'38 

28'37 

162832 

162822 ~/ '3 11.8 0.0 10. 10 28'3'3 162843 

0 1 1 .8 0.0 10.00 2'300 162853 

2 11 .8 0.0 10. 10 2'301 162'303 

·:; 1:2. 0 0 .. 0 8. '30 2'3(>2 162'313 

6 1 1 .9 0.0 10.00 2'303 162923 

G 11 .8 0.0 10. 10 2'304 1{:. .-.. ]'""'"' .... , .• ::. . \.71·.:J 

6 1 1 .8 o.o 10. 10 2'305 1E2942 

~ lt .~ CJ,o ith 1..0 2'el09 1630~1$ 

l· 11 • '3 o.o 10. 10 2'311 :t63c)4 7 
6 

1 

6 

_____ / 

ll.t:l 

11.8 

.)

. 1 :1.. 8 

11.8 

11.8 

o.o 

0.0 

0.0 

0.0 

0.0 

10.10 

10.10 

10.10 

10.10 

10.10 

2'313 

2'314 

2'320 

2":j21 

163108 

163118 

Cy;N 

v 

1. 63:~~08 

163218 

15322'3 

0 

rtffr 
Appendix D 

Tunnel Kiln Process Data 

RBKF9903 

KF Tunnel Kiln Final Report 

ROJAC 

AIR TESTING 

SERVICES, 

INC. 

{) {) n n •~· ·-· 
Pounds per Brick 

13 

tl0l)'07G 
RBKF9903 

KF Tunnel Kiln Final Report 

Appendix E 

Equipment Calibrations 

ROJAC 

AIR TESTING 

SERVICES, 

INC. 
:=:> 

:=:> 

=:> 

=:> 

......] 

:0 

Method 5 tJ 

Date: June 11,1999 Module #: 2827 

Bar. Ps., (Pb}: 30.44 in. Hg Std. Meter: 570415 

Standard Meter 

Module Volume 

Orifice Vs 

Setting (ft3) 

(in. H20) 

2.0 11.425 

2.0 11.555 

2.0 11.546 

Correlation Line Equation 

Q = m (OF) + b 

Vs (Pb + 

Y= 

Vm (Pb + 

dHa = (Q QJH) 

Factor 

Ys 

0.999 

0.999 

0.999 

~ 

13.6 

dl:L.....l 

13.6 

dH 

Temp. Pressure Volume 

ts Ps Vm tmi 

(oF) (in. H20) (ftl) (oF) 

72 -0.3 11.693 100 

72 -0.3 11.857 100 

72 -0.3 11.857 103 

' 

Y = Ratio of roading of wettest meter to dry test meter; 

tolerance for individual values +/- 0.02 from avg. 

dH@ = Orifice pressure differential that equates to 0. 75 

cfm of air @65degF and 29.92" Hg, in. H20; tolerance 

for individual values +/- 0.20 from avg. 

(Tm + 460) Ys 

( Ts + 460) 

[(lli + ~§Q) @ l' 

Reference 

thermo 

OF 

70 

Actual 

tmi 

OF 

70 

Post-test 

Module Meter 

Time Delta 

tmo @ Ha 

("F) (min) y (in. H20) 

82 15.00 1.0054 1.85 

85 15.00 1.0055 1.80 

86 15.00 1.0083 1.80 

Averages 1.0064 1.82 

Acceptance Criteria: 

Error 

0.00% 

Perform 3 calibration runs at a single, intermediate 

maximum vacuum reached during test series. If Y 

than 5%, recalibrate meter over all five orifice settin

Thermocouple Calibration 

Actual 

tmo I Error 

"F 

70 I 0.00% 

Calibrated 

By: R

Date 

Calibrated: 

Pb (tm + 460) [ Vs Ys l' 

~i~IImiHtifi~J~I~[!l

Module Quality Control Checks 

(Pb + __QJJ_} Module Cleaned: ..~..Y.;;.es~---

a = Y {17.64) Vm 13.6 Pitot Manometer Leak Check: yes @ 6

(tm + 460) @ Module Leak Check: yes @ 0

Orifice factor = [(Ts + 460) dH ].5 Calibrated by: ..;.P_.R..;.._S~t.!..yl..;.e_r ------- Date: J

[ Pb .I ].5 

~ 

~ 

c:lmy documentslmodule calibrationsl[three point calibration.xls]a 6/11/99 11:15 ~(Q){P)V 

Reviewed by: L.A. Gammie Date: J
) 

Method 5 Module Calibration 

Date: 11 FEB 99 Module #: 2827 

Bar. Ps., (Pb): 30.38 in. Hg Std. Meter: 570415 Pre-test 

Standard Meter Module Meter 

Module Volume 

Orifice Vs 

Setting (ft') 

(in. H20) 

0.5 5.787 

1.0 8.299 

1.5 9.972 

2.0 11.344 

3.0 13.208 

Correlation Line EQilation 

Q = m (OF) + b 

Vs (Pb + 

y = 

Vm IPb + 

dHa 

Temp. Pressure Volume Temperatures 

Factor 

Ys 

1.0069 

1.0069 

1.0068 

1.0065 

1.0063 

ts Ps Vm tmi 

(Of) (in. H20l (ft') (Of) 

71 -0.2 5.900 90 

71 -0.2 8.495 95 

71 -0.3 10.557 100 

71 -0.3 11.729 105 

71 -0.3 13.831 107 

Acceptance Criteria (5 point cal.): 

Y = Ratio of reading of wet test meter to dry test meter; 

tolerance for individual values +/- 0.02 from avg. 

dH@ = Orifice pressure differential (in. W .C.) that equates to 0. 75 

elm of air @65degF and 29.92" Hg. Tolerance 

for individual values +/- 0.20 from avg. 

EL__J (Tm + 460) Ys 

13.6 

.d.J:L_J I Ts + 460 I 

13.6 

Refenmce 

thermo 

Of 

70 

Actual 

tmi 

OF 

70 

tmo 

(Of) 

79 

87 

91 

93 

95 

Error 

0.00% 

Time Delta 

@ Ha 

(min) y (in. H20l 

15.00 1 .011 0 1.79 

15.00 1.0178 1.72 

15.00 0.9906 1.77 

15.00 1.0191 1.82 

14.00 1.0072 1.75 

Averages 1.0091 1.77 

Acceptance Criteria (post test cal.): 

Perform 3 calibration runs at a single, intermediate o

maximum vacuum reached during test series. If Y h

than 5o/o, recalibrate meter over all live orifice settin

Thermocouple Calibration 

Actual 

tmo I Error Calibrated 

OF By: R

70 0.00% Date 

Calibrated: 

(0 03!71 dH 

Pb (tm + 460) 

!Us + 4601 @ 1' 

I Vs Ys I' 

~~t/)))f~t~l~~?Ili~tit~~

( Pb + ___dl:j_J 

Q Y(17.64)Vm 13.6 

(tm + 460) @ 

Orifice factor = fiTs+ 460) dH ].5 

I Pb ].5 

~~ 

i 

c:\my documents\deta sheets and lists\lmodcal.xls)a 2/9/99 16:12 

Module Quality Control Checks 

Module Cleaned: ....~Y~e:..:s ___ _ 

Pitot Manometer Leak Check: --'yc..:e'-s ___ _ 

Module Leak Check: --'y~e:..:s ___ _ 

Calibrated by: ....:..;R::.:M.:....::Z;.:;a;.;n;.;ni:.._ _______ _ 

Reviewed by: LA Gammie 

@ 

@ 

3

2

Date: 1

Date: 1
Method 5 Module Calibration 

Date: May 10,1999 Module#: 1399 

Bar. Ps .. (Pb): 30.07 in. Hg Std. Meter: 570415 Pre-test .. · f : . ...

\,:~::::::;/ 1 :., 

-....:..~

Standard Meter Module Meter 

Module Volume . Temp. Pressure Volume Temperatures Time Delta 

Orifice . Vs 

Setting (ttl) 

(in. H20) 

0.5 6.177 

1.0 8.308 

1.5 10.273 

2.0 11.722 

3.0 14.280 

Correlation Line Equation 

Q = m (OF) + b 

Y= 

dHa = 

Vs (Pb + 

Vm (Pb + 

(0 0317) dH 

Pb (tm + 460) 

(Pb 

Factor 

Ys 

1.0001 

1.0016 

1 

0.999 

1.0002 

ts Ps Vm tmi 

(oF) (in. H20) (ft3) (oF) 

70 -0.1 6.238 86 

70 -0.15 8.543 98 

70 -0.2 10.574 100 

70 -0.25 12.046 100 

70 -0.3 14.640 104 

Y = Ratio of reading of wettest meter to dry test meter; 

tolerance for individual values +/- 0.02 from avg. 

dH@ = Orifice pressure differential that equates to o. 75 

cfm of air @65degf and 29.92" Hg, in. H20; tolerance 

for individual values +/- 0.20 from avg. 

EL-l (Tm + 460) Ys 

13.6 

dl:L__.J ( Ts + 460 ) 

13.6 

({Is + 460) @ ]2 

[ Vs Ys )2 

+ .....dl::L....l 

tmo @ Ha 

(oF) (min) y (in. H20) 

84 15.00 1.0169 1.60 

88 15.00 1.0135 1.74 

84 15.00 1.0077 1.72 

90 15.00 1.0124 1.75 

92 15.00 1.0189 1.76 

Averages 1.0139 1.71 

Acceptance Criteria: 

Perform 3 calibration runs at a single, intermediate o

maximum vacuum reached during test series. If Y h

than 5%, recalibrate meter over all five orifice setting

Module Quality Control Checks 

Module Cleaned: ..t..y..:..es=-----

Q Y (17.64) Vm 13.6 Pitot Manometer Leak Check: yes @ 

(tm + 460) @ Module Leak Check: yes @ 

Orifice factor = [(Ts + 460) dH ).5 Calibrated by PHILLIP STYLER Date: Ma

[ Pb .).5 

j. 

~~ 

Reviewed by: LEIGH GAMMIE ~/19 Date: Ma

c:\my documentslmodule calibrationsl(five point calibration.xlsja 5/10/99 14:36 
SPEI:TRH IJHSES INI:. 

3434 Route 22 West • Branchburg, NJ 08876 USA Tel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 

Shipped From: 80 Industrial Drive • Alpha, NJ 08865 

~ ~ ~============================================~~ ~, 

CERTIFICATE OF ANALYSIS 

CUSTOMER: 

SGI ORDER#: 

ITEM#: 

P.O.#: 

ROJAC 

138485 

3 

VERBAL-ESTER 

CERTIFICATION DATE: 12/28/98 

EXPIRATION DATE: 12/28/2000 

CERTIFICATION HISTORY 

COMPONENT 

Sulfur Dioxide 

BALANCE 

DATE OF 

ASSAY 

12/18/98 

12/28/98 

Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# 

Sulfur Dioxide NTRM-R81694 

INSTRUMENTATION 

COMPONENT MAKE/MODEL 

Sulfur Dioxide Horiba VIA-51 0 

EPA PROTOCOL MIXTURE 

PROCEDURE # : G1 

CYLINDER# : CC94697 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

MEAN CERTIFIED ANALYTICAL 

CONCENTRATION CONCENTRATION ACCURACY 

49.36 ppm 

49.31 ppm 

CYLINDER# 

CC53339 

SERIAL# 

851221093 

49.3 ppm 

CONCENTRATION 

96.0 ppm 

DETECTOR 

NDIR 

+/-1% 

CALl BRA TION 

DATE(S) 

12/18/98 

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

/)~_ ANALYST: __ -:/'::.........;~:__-=------ DATE: 12/28/98 

FRED PIKULA -------

0 0 0 0 :~ 1 
SPECTRA GASES 

277 Coit St. •Irvington, NJ 07111 USA Tel.: (973) 372-2060 • {BOO) 932-0624 • Fax: {973) 372-8551 

Shipped From: 80 Industrial Drive • Alpha, N.J. 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: 

SGI ORDER#: 

ITEM#: 

P.O.#: 

ROJAC 

132923 

1 

R981015 

CERTIFICATION DATE: 5111/98 

EXPIRATION DATE: 5/11/2000 

CERTIFICATION HISTORY 

DATE OF 

COMPONENT ASSAY 

Sulfur Dioxide 5/4/98 

5/11/98 

BALANCE N1trogen 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# 

Sulfur Dioxide NTRM-R81694 

INSTRUMENTATION 

COMPONENT MAKE/MODEL 

Sulfur Dioxide Horiba VIA-510 

MEAN 

CONCENTRATION 

95.18 ppm 

94.98 ppm 

CYLINDER# 

CC53339 

SERIAL# 

851221093 

EPA PROTOCOL MIXTURE 

PROCEDURE # : G1 

CYLINDER#: CC90959 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

CERTIFIED ANALYTICAL 

CONCENTRATION ACCURACY 

95.1 ppm +/-1% 

CONCENTRATION 

96.0 ppm 

DETECTOR CALl BRA TION 

DATE(S) 

NDIR 4/29/98 

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANALYST: __ '·-~....;;.::..-.-'--~...;../2-=~:;;...~' """"""''-- DATE: 5/11/98 

FRED PIKULA -------

000082 --------------------------·-·- j 
SPEl:TRH liHSES INI:. ~ .. 3434 Route 22 West • Branchburg, NJ 08876 USA Tel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 l.il Shipped From: 80 Industrial Drive • Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: 

SGI ORDER#: 

ITEM#: 

P.O.#: 

Rojac 

137740 

6 

R98104 

CERTIFICATION DATE: 11/11/98 

EXPIRATION DATE: 11/11/2000 

CERTIFICATION HISTORY 

· DATE OF 

COMPONENT ASSAY 

Sulfur Dioxide 2/23/98 

11/11/98 

BALANCE Nitrogen 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# 

Sulfur Dioxide GMIS-1 

INSTRUMENTATION 

COMPONENT MAKE/MODEL 

Sulfur Dioxide Horiba VIA-510 

MEAN 

CONCENTRATION 

250.7 ppm 

249.9 ppm 

CYLINDER# 

CC85046 

SERIAL# 

851221093 

EPA PROTOCOL MIXTURE 

PROCEDURE # : G2 

CYLINDER # : CC85016 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 660 

CERTIFIED ANALYTICAL 

CONCENTRATION ACCURACY 

250 ppm +/-1% 

CONCENTRATION 

192.9 ppm 

DETECTOR CALIBRATION 

DATE(S) 

NDIR 10/20/98 

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

c:'l /1. ANALYST:_~.C~..,.~~:.-.-,,"'-4...,h:;..'../1.-=:::..==--- DATE: ------- 11/11/98 

FRED PIKULA !of) 

~ 

000083 
SPEI:TRH GHSES INI:. 

3434 Route 22 West • Branchburg, NJ 08876 USA Tel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 

Shipped From: 80 Industrial Drive • Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: 

SGI ORDER#: 

ITEM#: 

P.O.#: 

ROJAC 

141252 

1 

981054 

CERTIFICATION DATE: 3/26/99 

EXPIRATION DATE: 3/25/2001 

CERTIFICATION HISTORY 

DATE OF 

COMPONENT ASSAY 

Sulfur Dioxide 12/7/98 . 

3/25/99 

Nitric Oxide 12/7/98 

3/25/99 

NOx 

Carbon Monoxide 12/7/98 

3/26/99 

Propane 12/8/98 

BALANCE Nitrogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# 

Sulfur Dioxide NTRM-R81694 

Nitric Oxide NTRM81684 

Carbon Monoxide NTRM-81679 

Propane SRM-2643a 

INSTRUMENTATION 

COMPONENT MAKE/MODEL 

Sulfur Dioxide Horiba VIA-510 

Nitric Oxide Teco 10 

Carbon Monoxide Horiba VIA-510 

Propane H. Packard 6890 

EPA PROTOCOL MIXTURE 

PROCEDURE# : G1 

CYLINDER # : CC94644 

CYLINDER PRES: 1200 PSIG 

CGA OUTLET: 660 

MEAN CERTIFIED ANALYTICAL 

CONCENTRATION CONCENTRATION ACCURACY 

50.78 ppm 50.6 ppm +/-1% 

50.37 ppm 

50.13 ppm· 50.1 ppm +/-1% 

50.12 ppm 

50.2 ppm Reference Value Only 

50.08 ppm 50.2 ppm +/- 1% 

50.35 ppm 

50.34 ppm 50.3 ppm +/- 1% 

CYLINDER# CONCENTRATION 

CC53353 96.0 ppm 

CC79984 98.6 ppm 

CC88660 97.4 ppm 

SX20148 99.1 ppm 

SERIAL# DETECTOR CALIBRATION 

DATE(S) 

851221093 NDIR 3/25/99 

1 OAR-34979-249 Cheml 3/9/99 

570423011 NDIR 3/12/99 

US00001434 GC- FlO 11/2/98 

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANAL YST:. ___ ~---=...P__;;_. ---- DATE: 3/26/99 

FRED PIKULA -------
SPEI:TRH GHSES INI:. 

3434 Route 22 West • Branchburg, NJ 08876 USA Tel.: (908) 252-9300 • (800) 932-0624 • Fax: (908) 252-0811 

Shipped From: 80 Industrial Drive • Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: 

SGI ORDER#: 

ITEM#: 

P.O.#: 

ROJAC 

141369 

2 

R991073 

CERTIFICATION DATE: 4/2/99 

EXPIRATION DATE: 4/2/2002 

CERTIFICATION HISTORY 

DATE OF 

COMPONENT ASSAY 

Oxygen 4/2/99 

Carbon Dioxide 4/2/99 

BALANCE N1trogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# 

Oxygen NTRM-82659X 

Carbon Dioxide NTRM-827 45x 

INSTRUMENTATION 

COMPONENT MAKE/MODEL 

Oxygen Horiba MPA-510 

Carbon Dioxide Horiba VIA-51 0 

MEAN 

CONCENTRATION 

12.01% 

10.05% 

CYLINDER# 

CC83900 

CC79944 

SERIAL# 

570694081 

571417045 

EPA PROTOCOL MIXTURE 

PROCEDURE # : G1 

CYLINDER#: CC106789 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 590 

CERTIFIED ANALYTICAL 

CONCENTRATION ACCURACY 

12.01 % +/-1% 

10.05% +/-1% 

CONCENTRATION 

22.80% 

20.00% 

DETECTOR CALIBRATION 

DATE(S) 

PM 4/2/99 

NDIR 3/29/99 

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

ANAL YST: __ __....;;_ao. __ ·_. ___ _ DATE: ___ 4/2/99 ;..;;;;...:~--

FRED PIKULA 

·----~--------

~'), 

<V? 

00008S 
.. - ~3~~~~~~rnn~~.~~~76 ~~T~;908) 252-~00 • (800) 9320624 • f~ (908) 2520811 1..1 Shipped From: 80 Industrial Drive • Alpha, NJ 08865 

CERTIFICATE OF ANALYSIS 

CUSTOMER: 

SGI ORDER#: 

ITEM#: 

P.O.#: 

ROJAC 

141369 

1 

R991073 

CERTIFICATION DATE: 4/2/99 

EXPIRATION DATE: 4/2/2002 

CERTIFICATION HISTORY 

DATE OF 

COMPONENT ASSAY 

Oxygen 4/2/99 

Carbon Dioxide 4/2/99 

BALANCE N1trogen 

PREVIOUS CERTIFICATION DATES: None 

REFERENCE STANDARDS 

COMPONENT SRM/NTRM# 

Oxygen NTRM-82659X 

Carbon Dioxide NTRM-82745x 

INSTRUMENTATION 

COMPONENT MAKE/MODEL 

Oxygen Horiba MPA-51 0 

Carbon Dioxide Horiba VIA-510 

MEAN 

CONCENTRATION 

20.9% 

18.01% 

CYLINDER# 

CC83900 

CC79944 

SERIAL# 

570694081 

571417045 

EPA PROTOCOL MIXTURE 

PROCEDURE # : G1 

CYLINDER#: CC106813 

CYLINDER PRES: 2000 PSIG 

CGA OUTLET: 590 

CERTIFIED ANALYTICAL 

CONCENTRATION ACCURACY 

20.9% +/-1% 

18.01% +/- 1% 

CONCENTRATION 

22.80% 

20.00% 

DETECTOR CALIBRATION 

DATE(S) 

PM 4/2/99 

NDIR 3/29/99 

THIS STANDARD WAS CERTIFIED ACCORDING TO THE EPA PROTOCOL PROCEDURES. 

DO NOT USE THIS STANDARD IF THE CYLINDER PRESSURE IS LESS THAN 150 PSIG. 

DATE: 4/2/99 ------- ANALYST: ___ ~_-p? __-___ _ FRED PIKULA 

oooosr:; -----------------------------···----··· 
Appendix F 

Laboratory Analytical Data 

RBKF9903 

KF Tunnel Kiln Final Report ,. 

ROJAC 

AIR TESTING 

I SERVICES, 

INC. 
f5§111ij 

PHILIP SERVICES 

INORGANIC DATA PACKAGE 

FOR 

ROJAC AIR TESTING SERVICES INC. 

Project #RBKF9903 

Philip Analytical Services Corporation 

5555 N ortb Service Road 

Burlington, ON L 7L 5H7 

Submission#: 9F0571 

Prepared by: Janice Joseph- CSR 

Approved by : Dr. Ron McLeod - Principal Scientist 

P!tlt.IP A~,-.J_, ;J~ ... \I. St-:K\ If :r:. ... c( ),~, .• _.,l·\Tioi': 

000088 
00001 

1. CASE NARRATIVE 

f\ 1"\ 1"1 f'\ "r. 
PROJECT NARRATIVE 

PHILIP Analytical Services (Burlington ON) 

Philip Project: AN990616. 

Philip Submission #:9F0571 

Client: Rojac Air Testing Services 

Client Project: RBKF9903 

I. SAMPLE RECEIPT/ANALYSIS 

a) Sample Listing 

Philip 

ID 

Client 

SampleiD 

Date Date 

Sampled Received 

Fluoride via Probe 

031859 99 Method Blank 99/06/11 99/06/15 

03186099 M26-1 99/06111 99/06115 

03186199 M26-2 99/06111 99/06/15 

031862 99 M26-3 99/06/11 99/06115 

031863 99 M26-4 99/06/11 99/06115 

Hydrogen Fluoride via EPA Method 26A 

031859 99 Method Blank 99/06/11 99/06/15 

031860 99 M26-1 99/06111 99/06115 

031861 99 M26-2 99/06/11 99/06/15 

031862 99 M26-3 99/06111 99/06/15 

031863 99 M26-4 99/06/11 99/06/15 

Hydrogen Chloride via EPA Method 26A 

031859 99 Method Blank 99/06111 99/06/15 

031860 99 M26-1 99/06111 99/06/15 

031861 99 M26-2 99/06/11 99/06/15 

031862 99 M26-3 99/06/11 99106115 

031863 99 M26-4 99/06/11 99/06/15 

Date 

Prepped 

99/07/13 

99/07/13 

99/07/13 

99/07/13 

99/07/13 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

Run 

Date 

99/07/13 

99/07/13 

99/07/13 

99/07/13 

99/07/13 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

99/06/21 

00002 

Run Date is defmed as the date of injection of the last calibration standard (12 hour or less) prior to the 

samples analyzed within that run sequence. Therefore the time of calibration injection that defines the 

run date is always within 12 hours of the time of sample injection. 

b) Shipping Problems: none encountered 

c) Documentation Problems: none encountered 

II. SAMPLE PREP: 

No problems encountered 
III. SAMPLE ANALYSIS: 

Fluroide analysis via ion chromatography (IC - M26A) on these samples showed the presence of 

significant interference. Therefore the samples were also analyzed for fluroide via selected ion 

electrode. We believe that these data provide interference free fluoride levels in the samples. 

See also comments within the appropriate Certificate of Analysis. 

a) Hold Times: all within recommended hold times 

b) Instrument Calibration: all within control limits 

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, for other than the conditions detailed above. 

00003 

In addition, I certify, that to the best of my knowledge and belief, the data as reported are true and accurate. 

Release of the data contained in this data package has been authorized by the cognizant laboratory 

official or his/her designee, as verified by this signature. 

Date 
00004 

2. CERTIFICATE OF ANALYSIS 

flOOOQ? 
OUDOS 

Certificate of Analysis 

CLIENT INFORMATION LABORATORY INFORMATION 

Attention: 

Client Name: 

Project: 

Project Desc: 

Address: 

Fax Number: 

Leigh Gammie 

Rojac Air Testing Services 

RBKF9903 

Stack Emissions 

120 Mountain Avenue 

Bloomfield, CT 

6002 

860-243-9801 

Contact: Ron McLeod 

Project: AN990616 

Date Received: 99/06/15 

Date Reported: 99/07/21 

Submission No.: 9F0571 

Sample No.: 031859-031863 

Phone Number: 860-243-9800 

NOTES: "-'=not analysed '<'=less than Method Detection Limit (l.tDL) 'NA' =no data available 

LOQ can by determined for all analytes by multiplying the appropriate MDL X 3.33 

Solids data is based on dry weight except for biota analyses. 

Organic analyses are not corrected for extraction recovery standards except for isotope 

dilution methods, (i.e. CARB 429 PAH, all PCDDIF and DBDIDBF analyses) 

Methods used by PASC are based upon those found in 'Standard Methods for the Examination ofWa~er and 

Wastewater', Nineteenth Edition. Other methods are based on the principles of MISA or EPA methodologies. 

New York State: ELAP Identification Number 10756. 

All work recorded herein has been done in accordance with normal professional standards using accepted testing 

methodologies, quality assurance and quality control procedures except where otherwise agreed to by the client 

and testing company in writing. Any and all use of these test results shall be limited to the actual cost of the 

pertinent analysis done. There is no other warranty expressed or implied. Your samples will be retained at 

P ASC for a period of three weeks from receipt of data or as per contract. 

COMMENTS: 

*Matrix interference 

Certified by: ki1 _{Y\J~ Page 1 

000093 
0 

0 

0 

0 

w 

~ 

7/20/99 

Clie11tiD: 

Lab No.: 

Date Sampled: 

Component MDL 

Impinger volume measured 

Fluoride via Probe 5.0 

Hydrogen Fluoride- method 26 50.0 

Hydrogen Chloride- method 26A 100 

~__£) 

-

Method 

Blank 

031859 99 

-

Units 

ml -

ug < 

ug < 

II < 

PASC- Certificate of Analysis 

Blank Blank Blank Blank 

Spike #I Spike #I Spike #2 Spike #2 

031859 99 031859 99 031859 99 031859 99 

- - - -

% Recoveries % Recoveries 

- - - -

- - - -

200 96 200 96 

330 110 330 110 

M26-l M26-l 

031860 99 031860 99 

9910611 I 99/06/11 

Duplicate 

200 

730 740 

<1000* <1000* 

28000 28000 

Client:Rojac Air Testin
0 

0 

0 

0 

:..0 

:'Ji 

7120199 

Cliellt ID: 

Lab No.: 

Date Sampled: 

Component MDL 

lmpinger volume measured 

Fluoride via Probe 5.0 

Hydrogen Fluoride • method 26 50.0 

Hydrogen Chloride- method 26A 100 

~~ 

M26-l 

031860 99 

99/06111 

Units M. Spike 

ml -

ug 840 

ug 13000 

" 42000 

PASC- Certificate of Analysis 

M26-l M26-l M26-l M26-2 

031860 99 031860 99 031860 99 031861 99 

99/06/11 99/06111 99/06111 99/06/11 

MS %Rec. MS Dup MSD%Rec. 

- - - 180 

110 - - 470 

96 13000 95 <1000* 

96 42000 92 23000 

M26-3 M26-4 

031862 99 031863 99 

99/06111 99106111 

150 130 

360 < 

<1000* <250* 

24000 < 

Client:Rojac Air Testin
00008 7120199 PASC- Summary of Analysis Pre. Dates Page MS-4 of 4 

Batch Code: 

Fluoride via Probe 

Run Date: 

Date of Sample Prep: 

Batch Code: 

Hydrogen Fluoride - method 26 

Run Date: 

Date of Sample Prep: 

Batch Code: 

Hydrogen Chloride - method 26A 

Run Date: 

Date of Sample Prep: 

0713IGA2 

031859 99 

031860 99 

031861 99 

031862 99 

031863 99 

99/07/13 

99/07/13 

062IASAI 

031859 99 

031860 99 

03186199 

031862 99 

031863 99 

99/06/21 

99/06/21 

062IASAI 

031859 99 

031860 99 

031861 99 

031862 99 

031863 99 

99/06/21 

99/06/21 

Client:Rojac Air Testing Services Project:RBKF9903 

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