UNITED STATES AIR FORCE

AFIOH

IOH-RS-BR-SR-2005-0002

Sampling and Analysis Plan for the 

Collection of Ambient Air Samples 

at Receptor Locations from Open 

Pit Burning Operations in the Pit Burning Operations in the

Deployed Environment

Nancy L. Hanna-Beauregard

Trajen, Incorporated

3131 Briarcrest

Bryan, TX 77802

Mark D. Wade

Karta Technologies, Incorporated

5555 Northwest Parkway

San Antonio, TX 78249

Vincent D. Falls, Captain, USAF, BSC

Luis J. Medina

January 2005

Air Force Institute for Operational Health

Approved for public release;

distribution is unlimited. 

Air Force Institute for Operational Health

Risk Analysis Directorate

Environmental Analysis Division

2513 Kennedy Circle

Brooks City-Base TX 78235-5116


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iii

TABLE OF CONTENTS 

 PAGE

LIST OF TABLES iv 

1. INTRODUCTION 1 

2. OBJECTIVE 1 

3. SAMPLE TYPES 1 

4. SAMPLING FREQUENCY 2 

5. SAMPLING PROCEDURES 3 

6 SAMPLING EQUIPMENT & ANALYSES 4 

Appendix A: MiniVol Field Manual 7 

Appendix B: SUMMA Canister Sampling for Ambient VOCs – (TO-14A) 31 

Appendix C: PS1 Sampling Instructions – (TO-14A) 45 

Appendix D: Oil Well Fire Equipment List 65 
iv

LIST OF TABLES 

TABLE PAGE

1 Type of Samples 2 

2 Sample Frequency 3 
1

SAMPLING AND ANALYSIS PLAN FOR THE COLLECTION OF 

AMBIENT AIR SAMPLES AT RECEPTOR LOCATIONS FROM OPEN 

PIT BURING OPERATIONS IN THE DEPLOYED ENVIRONMENT

1. Introduction 

In response to a CENTAF (F)/SG Priority A task concerning the health effects of solid waste 

burning at OIF sites, the Air Force Institute of Operational Health, Risk Analysis Directorate, 

Environmental Analysis Division (AFIOH/RSE) developed a sampling and analysis plan for the 

collection of ambient air samples to quantify air contaminants produced by open pit burning 

operations. The plan is devised so that samples can be taken at receptor locations in the 

deployed environment. AFIOH/RSE personnel researched and identified the sampling 

technologies needed to capture the exposures, developed a list of possible contaminants, and 

assessed the costs involved with the ambient air sampling process. This sampling plan is 

intended to provide the specific ambient air sampling protocols and analysis methodologies 

required for deployed base-level personnel to initiate sample collection, shipment and analyses 

necessary to quantify the levels of contaminants generated by open pit burning. The ambient air 

sampling methodologies and analytical methods applied in this plan are based on methodologies 

developed by the U.S. Environmental Protection Agency (EPA). Specific, step-by-step 

instructions for air sample collection procedures are outlined in detail in U.S. Army Center for 

Health Promotion and Preventive Medicine (USACCHPPM) Technical Guide (TG) 251. 

The air pollutants of concern are generated during the open pit burning of solid waste. Specific 

types/amounts of each pollutant depend on the composition of the waste materials being burned. 

Heat and airflow also contribute to the amount of contaminants released in air because 

incomplete combustion that results in low heat and smoldering tends to produce more smoke. 

Generally, pollutants may include varying amounts of dioxins, furans, particulate matter, 

polycyclic aromatic hydrocarbons, volatile organic compounds, carbon monoxide, and 

hexachlorobenzene. Ambient air samples will be collected during the open pit burn operations 

at receptor sites affected. Affected sites will depend on local meteorological conditions and their 

impact on the plume direction and concentration. 

2. Objective

The objective of this sampling and analysis plan is to provide to the deployed BEE the type of 

samples to collect, the method of sampling to use, and the proper analysis to request when 

quantifying the exposure levels of deployed personnel to contaminants generated during open pit 

burning. This plan is generic in nature so that it can be applied to most receptor locations. 

3. Sample Types

To quantify the exposures of open pit burning the following samples should be collected using 

the referenced method. 
2

TABLE 1. Sampling Types 

Contaminants Number of 

Samples 

Method Media/Sampling Device 

PM10 Particulates 12 40 CFR, Parts 1-51, 

Part 50, Appendix J, 

July 1, 1993 

MiniVol Sampler HighVolume Particulate Sampling

Volatile Organic 

Compounds 

8 EPA Method TO-14 SUMMA Canisters 

Dioxins/Furans & 

PAHs 

12 EPA Method TO-9A PUF Sampler 

Semi-Volatile 

Organic 

Compounds 

8 EPA Method TO-13A PUF or XAD (fiberglass) 

high volume method. 

**Meteorological 

Conditions 

1 reading per 

hour on 

sampling days 

 Weather services or direct 

reading instruments if 

available 

**Accurately recording existing meteorological conditions is imperative to the sampling process. 

The analytical results of the air sampling are just the beginning. Adequate health risk 

evaluations for populations located down wind of the burn pit mandate the constant collection of 

wind direction, wind speed, temperature, barometric conditions, and observations of changing 

weather conditions, e.g. low-hanging overcast skies, clear skies, etc. Meteorological conditions 

have a direct impact on predicting the amount of contaminants that could reach downwind 

populations. These data must be accurately recorded on at least an hourly basis throughout the 

24-hour sampling period. If direct reading instruments are not readily available then the 

sampling team may rely upon local weather services, but personal, first hand observations of the 

plume and surrounding environmental conditions should also be noted on the sample collection 

forms. 

4. Sampling Frequency 

The amount of samples taken will depend on the sampling equipment that is available at the 

deployed location. At a minimum, one set of samples should be placed at the receptor location 

and one set should be located in an upwind position in relation to the burn pit to capture 

background concentrations. Ideally, multiple samples should be collected at all established wind 

directions to better define pollutants contributed by other sources located upwind and downwind 

under all meteorological conditions. Sampler inlets should be pointed to face into oncoming 

wind at a height of about breathing zone level (approximately 2 meters above ground). The end 

result of downwind sampling will constitute a “worst-case” picture of pollutant concentrations 

for future health risk evaluations. Upwind and crosswind sample results should establish levels 

of pollutants contributed by other sources of pollution and the background levels present in 

ambient air. With the exception of VOCs, ambient air samples will be collected at the afore 
3

mentioned locations over periods of 24 hours beginning immediately after burn initiation and 

continually throughout the 24-hour burn period or until combustion is complete, to include 

smoldering periods. To measure dioxins and furans in their expected concentration range the 

sampling period will have to be extended from the EPA Method TO-9A time of 24 hours to 72 

hours. This will allow enough volume of air to pass through the sampler so that a measurable 

amount of contaminant is collected. Sampling frequency is illustrated in chart provided below: 

Table 2. Sampling Frequency 

Wind Direction: 

Sample 

Location: 

NE 

(background) 

SE 

(background) 

SW 

(background) 

NW 

(background) 

RECEPTOR 

Location 

Dioxins/Furans 2– 72 hour 

samples

2– 72 hour 

samples

2– 72 hour 

samples

2– 72 hour 

samples

4– 72 hour 

samples

VOCs 1 - 8 hour 

samples

1- 8 hour 

samples

1- 8 hour 

samples

1- 8 hour 

samples

4- 8 hour 

samples

Particulates 

(PM10) 24 hour 

samples 

2– 24 hour 

samples

2– 24 hour 

samples

2– 24 hour 

samples

2– 24 hour 

samples

4– 24 hour 

samples

Meteorological 

Data Collection 

Hourly x 72 

hours 

Hourly x 72 

hours 

Hourly x 72 

hours 

Hourly x 72 

hours 

Hourly x 72 

hours 

5. Sampling Procedures 

Particulate Sampling - Airmetrics MiniVol Particulate Sampler Instructions

The MiniVol samples the air at 5 liters per minute for particulate matter (TSP, PM10, and 

PM2.5). The sampler is designed to be portable to sample the air at a discrete location or to be 

used in saturation sampling. Electrical power or a permanent structure is not required. While the 

MiniVol is not EPA approved as a reference method, it has been proven to equivalent to the 

standard reference methods. The sample battery pack is designed for 24-hour continuous 

sampling. For detailed sample collection procedures of PM10 samples using the MiniVol PM 

Sampler, refer to the AFIOH Field Manual (v4.2), March 2000, provided in Attachment 1. 

VOC Sampling - Ambient Air Volatile Organic Compound (VOC) Summa Canister 

Sampling (TO-14A)

VOCs are collected according to EPA Method TO-14A using SUMMA polished, evacuated 

stainless steel canisters. Sub-atmospheric, passive, sampling does not require a power source. 

This type of sampling provides a high level of portability for remote field sampling. Sampling 

periods from 8 hours, 24 hours, and up to one week may be selected for the sampling mission 

requirements. Eight-hour samples are all that is required for this particular sampling plan. Flow 

rates are determined by the capacity of the canister, the desired sampling period, and the ambient 

conditions (temperature and barometric pressure). Flow rates are controlled using a flow 
4

restrictor manufactured by Entech and canister vacuum measurements are taken with the vacuum 

gauge attached to the restrictor. The canisters and flow restrictors will be prepared in advance 

and the vacuum gauge on the flow restrictors will be calibrated according to TO-14A prior to 

field deployment. Field personnel will only need to set/calibrate the flow rate of the restrictor at 

the sampling location. For detailed sample collection and equipment operation procedures refer 

to Attachment 2, Excerpt Taken from USACHPPM DRAFT TG-251. 

Dioxins/Furans and PAH Sampling – PS1 Sampling Instructions 

The PS-1 sampler is used to conduct the following EPA reference methods: 

• TO-4A Polichlorinated/polybrominated 

• TO-9A chlorinated/brominated debenzo-p-dioxins and dibenzofurans 

• TO-13A polycyclic aromatic hydrocarbons (PAHs) 

These sampling methods are used for source specific sampling (i.e. incinerators, open burning, 

manufacturing facilities, aerial spraying of crops, etc). This method will be used during this 

sampling effort as the plan is designed for open pit burning surveillance to establish baseline 

levels. For detailed sample collection and equipment operation procedures, refer to Attachment 

3, PS1 Sampling Instructions. 

6. Sampling Equipment & Analyses 

If sampling equipment is not available it must be requested through the analytical laboratory 

along with the sampling media. The oil well sampling kits maintained by AFIOH/RSE will 

include the mini-vol and TSP, (see Attachment 4 for kit inventory) but SUMMA canisters must 

be ordered directly from the laboratory. The analytical laboratory of choice will provide special 

packaging requirements; storage conditions and shipping procedures will be provided along with 

sampling media and devices upon request. Contact one of the following laboratories to obtain 

supplies, equipment and collection devices: 

 U.S. Air Force: http://www.brooks.af.mil/afioh/Laboratories/sdc_sdce.htm

AFIOH/SDCE - Technical Analysis Branch 

2350 Gillingham Drive 

Brooks City-Base TX 78235-5103 

DSN 240-6176/6177 

COMM (210) 536-6176/6177 

FAX DSN 240-4578 
5

 U.S. Army: http://chppm-www.apgea.army.mil/dls/default.asp

For Routine Correspondence/Samples:

 Commander, USACHPPM 

 ATTN: MCHB-TS-LID (Sample Management Laboratory) 

 5158 Blackhawk Road 

 Aberdeen Proving Ground, MD 21010-5403 

FedEx® UPS®

For Sample Shipments:

 Commander, USACHPPM 

 ATTN: MCHB-TS-LID (Sample Management Laboratory) 

 Building E2100 

 Aberdeen Proving Ground, MD 21010-5403 
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Appendix A 

MiniVol Field Manual 
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9

FIELD MANUAL 

Ambient Monitoring for Particulate Matter 

using the 

MiniVolTM Portable PM Sampler (V4.2) 

Prepared By: 

Deployment Environmental Surveillance 

Air Force Institute for Environment, Safety and 

Occupational Health Risk Analysis (AFIERA) 

2513 Kennedy Circle Brooks AFB, TX 78235-5123 

DSN 240-3305; COMM 210-536-3305 

March 2000 
10

TABLE OF CONTENTS 

 PAGE

1.0 BACKGROUND........................................................................... 1 

2.0 EQUIPMENT, ACCESSORIES AND SUPPLIES................................. 2 

3.0 MINIVOLTM OVERVIEW.................................................................. 3 

3.1 FEATURES............................................................................... .......4 

4.0 PM SAMPLING PROCEDURES....................................................... 6 

4.1 PRECALIBRATION................................................................... .........6 

 4.1.1 Filter/Pre-separator Configuration.................................................6 

 4.1.2 Filter Assembly and Impactor Preparation...........................................7 

 4.1.3 Filter Handling and Processing..........................................................8 

4.2 CALIBRATION.................................................................................9 

4.3 SAMPLING ROUTINE........................................................................11 

 4.3.1 Pre-sampling............................................................................11 

 4.3.2 Field Procedures...................................................................... 11 

 4.3.3 Post Sampling.............................................................................13 

4.4 SITING...........................................................................................15 

4.5 RECORDKEEPING And REPORTING................................................ ..16 

APPENDICES 

A. Field Datasheets 

B. Meterological Data Forms 
11

1.0 BACKGROUND

This manual was developed as a practical field guide for environmental surveillance 

personnel who will perform monitoring of ambient airborne particulate matter (PM) 

with the MinivolTM portable air sampler. The manual provides a basic overview of the 

instrument and the ambient PM sampling method, along with a sampling protocol that 

guides the operator through sequential, step-by-step monitoring tasks. This manual 

consolidates relevant information from EPA sampling methods, the manufacturer’s 

technical manual, field studies, lessons learned from previous users, and guidance 

from AFIERA personnel with a background in air contaminant monitoring. The PM 

ambient monitoring process presents numerous opportunities to introduce error. This 

guide was designed to highlight those pitfalls, guide personnel around them, and to 

promote continuity from sample event to sample event. Additional technical advice 

may be needed from AFIERA on occasion; information such as schematics or part 

numbers can be obtained from the manufacturer’s technical manual provided with the 

instrument. 

 

The Airmetrics MinivolTM, as equipped, can 

be configured to sample particulate matter 

having an aerodynamic diameter less than 

or equal to a nominal 2.5 micrometers 

(PM2.5), as well as PM10 and total 

suspended particulates (TSP). Toxic 

metals can be sampled as well. 

This instrument was developed jointly by 

the US Environmental Protection Agency 

(EPA) and Lane Regional Air Pollution 

Authority. It was specifically designed for 

use in remote locations. The MinivolTM is 

compact, lightweight, weather resistant, 

and can be operated by AC or battery 

power. Although not a federal reference 

method (FRM) sampler, the instrument 

provides results that closely proximate 

reference method data, when used as 

directed. The instrument has been used 

successfully by the US EPA, Army, State 

Agencies, and private industry. 

AFIERA would like to thank Jim Howes (CH2M Hill, International) and the Deployment 

Environmental Surveillance Program, US Army Center for Health Promotion and Preventive 

Medicine (CHPPM) for their inputs in the development of this instruction manual. 

 
12

2.0 EQUIPMENT, ACCESSORIES AND SUPPLIES 

2.1 Each sampler comes equipped with the following items, as viewed left to 

 right in the photograph below: 

3⁄4 Air Sampler Module w/(2) 

Rechargeable Batteries 

3⁄4 AC Power Cable 

3⁄4 Filter Holder Assemblies (2) 

3⁄4 Preseparator Adaptors (2) 

3⁄4 Impactor Assemblies 

(2 each: PM2.5 and PM10)

3⁄4 Raincaps (2) 

3⁄4 Spare Parts Kit 

3⁄4 Manf’s Technical Manual 

 

Basic Sampler Package 

2.2 In addition, the following items were added with the shipment: 

3⁄4 Bottle, Solvent 

3⁄4 Calibrator, BIOS DC-Lite 12K 

3⁄4 Calibration Adaptor 

3⁄4 Cleaning Brush 

3⁄4 Dropper Bottle (for solvent/grease application) 

3⁄4 Filter Cassettes (2, extra) 

3⁄4 Filter Cassette Shoe (to open cassettes) 

3⁄4 Forceps, Non-Serrated 

3⁄4 Gloves, Nitrile, Non-powder 

3⁄4 Grease, Glisseal (60g) 

3⁄4 Rubber Bands (to secure petri dish covers) 

3⁄4 Telescoping Hoisting Pole Assembly 

3⁄4 Tripod Pole Support 

3⁄4 Utility Wipes, Lint-free 

3⁄4 Zip Lock Bags (filter assembly transport/shipping of filters & paperwork) 
13

2.3 The following supplies should be acquired locally: 

3⁄4 AA Alkaline Batteries (replace timer battery at 6 months or once/rotation) 

3⁄4 Hexane, Unleaded MoGas, Lighter Fluid, or Lantern Gas (grease 

solvent/cleaning agent) 

3.0 MINIVOLTM OVERVIEW 

The MinivolTM portable air sampler is designed to sample at a constant rate of 5 liters per 

minute for particulate matter (PM2.5, PM10, and TSP). The filters can subsequently be 

analyzed for toxic metals. The MinivolTM can also be used to collect ambient air samples for 

non-reactive gas (CO/NOx) analysis. However, the instrument will not be used for this 

purpose and is therefore not equipped for this procedure. Disregard those sections in the 

manufacturer’s technical manual regarding gas sampling. 

Ambient monitoring is based on EPA sampling protocol, which incorporates stringent Quality 

Control. Because the method requires precision mass measurement of PM in the micrometer 

range, there is very little margin for deviation from the detailed procedures outlined in this 

manual. Although there are similarities to industrial hygiene air monitoring, the equipment 

and overall process is significantly more involved and tedious. Personnel must take the time 

to familiarize themselves with the equipment and the proper monitoring procedures before 

initiating PM sampling. Pay special attention to the precautions that have been highlighted in 

blue. The Minivol is essentially a constant flow pump with a number of control and diagnostic 

features. The primary operational features of the instrument are described below. 

Access the control panel by pressing the two release pins on the front of the instrument 

casing simultaneously. Grasp the top cap and lift the pump/control panel assembly out of the 

PVC casing. One way to accomplish this procedure is by performing the operation while 

standing behind the instrument. The pump/panel assembly will not lift completely out! It 

is attached to the unit by the power line, which is in the form of a phone plug-in jack. Do not 

grasp the circuit board. Rest the control panel on the PVC case by slipping the triangular 

mount stand over the lip of the casing. This is not a firm support, so be careful! Standing 

the instrument against a structure can provide additional support, and is highly recommended. 
14

 

3.1 FEATURES 

Battery-Operation: The rechargeable, 12-volt lead-acid batteries provide 24 hours of 

sampler operation (when fully charged). The U.S. Army has had good success operating the 

samplers by battery in SW Asia. Some special notes: 

3⁄4 A green LED on top of the battery illuminates while the battery is charging. The light will 

turn off to indicate a full charge. 

3⁄4 A fully discharged battery may require 14-18 hours of recharging. If it is to be used 

frequently, leave it plugged into the charging transformer where it will continue to receive a 

trickle charge. To prevent damage: 

3⁄4 do not store the battery for extended periods while being charged 

3⁄4 do not store the battery while 

connected to the sampler 

3⁄4 The instrument will also operate from an AC 

power source by simply connecting the 

transformer/recharge cord from the power 

source to the battery. In this configuration, 

the AC overrides the battery (while it provides 

a trickle charge to the battery). 

3⁄4 Should the batteries fail to supply sufficient 

voltage (below 10.3 volts), the instrument will 

shut down. A LLLOOOWWWBBBAAATTTTTTEEERRRYYY indicator will 

illuminate on the control panel if the 

instrument ceases operation for this reason. 

3⁄4 Connect the battery to the bottom of the 

sampler by inserting the three pins on the 

sampler into the receptacles on top of the 

battery (the battery can only fit one way). 
15

Lock the side latches. 

Programmable Timer: A timer on the control panel can actuate the pump manually, or 

in the timer mode. The timer can be set up to initiate six separate runs within any period of 

up to seven days (normally, the unit will be programmed to make one run over a single period 

of 24 hours). The timer is powered separately by the AA alkaline battery located above it. It 

is under a constant drain. Replace this battery at 6-month intervals—observe the correct 

polarity when installing! Refer to Page 11 of this manual for instructions on turning the 

sampler on and off, setting the real-time clock, and setting the timer. Practice setting and 

clearing the timer before attempting to sample for the first time. This feature is probably 

the most difficult to fully grasp. 

Elapsed Time Totalizer (ETT): Located at the top of the control panel, this feature 

displays the total number of hours the unit has operated. The totalizer accumulates time only 

when the pump is running. It cannot be reset to zero. Although the manual indicates the 

totalizer reads in hundredths of hours, it actually reads in tenths of hours. So there is a sixminute interval between each incremental change. This feature should not be used for 

timing purposes. However, ETT readings are to be recorded before and after each run 

for QC and troubleshooting purposes. 

Constant Flow: The instrument is designed to maintain a constant flow rate despite 

increased resistance, such as from filter loadings. The pump will automatically shut off if the 

flow rate drops below an established threshold of between 10% and 20% below 5 lpm (4.5 

and 4.0 lpm, respectively). LLLOOOWWWFFFLLLOOOWWWAAADDDJJJUUUSSSTTT and LLLOOOWWWFFFLLLOOOWWWZZZEEERRROOO adjustment 

screws are located on the front panel. AFIERA has already adjusted this threshold to 

10%. No further adjustment should be necessary. An indicator labeled TTTHHHRRREEESSSHHHOOOLLLDDD on 

the front panel will illuminate any time the flow drops below the set threshold. However, this 

indicator is used only when making the threshold adjustments as described on Page 15 of the 

technical manual. Don’t confuse this with the LLLOOOWWWFFFLLLOOOWWWindicator, which will illuminate 

if the pump remains below the threshold for more than a few seconds, initiating premature 

pump shut down and an invalid sampling run. When a low flow condition shuts down the 

sampler, press the RRREEESSSEEETTTbutton on the control panel to restart the sampler.

Flow Adjust: The FFFLLLOOOWWWAAADDDJJJUUUSSSTTT knob is used to regulate the flow to 5.0 lpm 

(actual/ambient conditions) during calibration. Do not deviate from a setting of 5.0 lpm. 

The PM2.5 and PM10 impactor design requires this actual flow rate for proper particle size 

separations. 

Flow Meter: The flow meter (rotameter) on the control panel is not to be used for 

calibration or for recording the flow rate at the end of a run, as indicated in the 

Airmetrics® technical manual. However, it can be used to aide in identifying flow problems 

(i.e., troubleshooting). Instrument calibration is discussed in Section 4.2. 

 

Filter Holder/Pre-Separator Assembly: The apparatus shown below can be 

configured three ways to sample for either TSP, PM10, or PM2.5. It is assembled from left to 

right in a cascade fashion: 

 

(1) Filter Holder w/Cassette 
16

(2) Preseparator Adapter w/PM2.5 Impactor 

(3) Preseparator Adapter w/PM10 Impactor 

(4) Rain Hat 

A complete assembly is shown in the background. Note that the inlet for the PM10 impactor on the 

right is larger than the PM2.5 impactor on the left. These impactors easily slide in and out of the 

adapters by pressing them from their bottom with your thumbs. The impactors must be situated 

flush with the tops of the adapters. 

4.0 PM SAMPLING PROCEDURES: 

Note: New sampling locations require proper siting. Refer to Section 4.4, “SITING” prior to 

initial sampling. 

 

4.1 PRECALIBRATION 

Note: New Nitrile protective gloves should be worn when handling filters, filter holders 

and impactors. Very small artifacts and even body oils can adversely affect results. 

4.1.1 Filter/Pre-separator Configuration: Select the appropriate configuration: 

PM2.5 – The PM2.5 configuration is shown below. It first requires the filter holder, then the 

screw-on adapter with PM2.5 impactor insert, and finally a slide-on adapter with PM10 impactor 

insert. Ensure the impactors are inserted with their tops flush with the tops of the adapters.

PM10 – The PM10 configuration requires the filter holder attached to the screw-on adapter. 

The PM10 impactor is inserted into the adapter. 

TSP – The TSP configuration will not normally be used. However, specially directed surveys 

may require this setup when sampling for specific PM species. It requires only the filter 

holder attached to the screw-on adaptor. No impactors are used. 
17

 PM2.5 Configuration PM10 Configuration 

4.1.2 Filter Assembly and Impactor Preparation 

Initially, and after every two sampling events (recommended for desert conditions), the 

impactor targets must be cleaned and re-greased. The cleaning/greasing frequency should 

be increased or decreased as needed, depending on ambient loadings and degree of soiling 

observed on the target disks. Note that the disks easily pull away from the impactor standoffs. 

1. Inspect the O-rings on the impactor for serviceability. If necessary, use another impactor 

or replace the O-rings. 

2. The impactors can be cleaned by rinsing from top to bottom with a locally obtained 

solvent; a polyethylene squeeze bottle is recommended. Use a clean soft bristle brush if 

necessary. Hexane is preferred; however, unleaded mogas, lighter fluid, white gas or 

lantern gas are acceptable solvents. Let air-dry. 
18

3. Grease the impactor target cup/plate as shown above. Prepare a mixture of the solvent 

and impactor grease in the dropper bottle by mixing a one-inch length of grease to 30 ml 

of solvent. Vigorously shake the mixture before each use until an opaque, uniform 

suspension, free from grease globs, is obtained. 

4. Put two or three drops of the solution on the target plate. The drops should saturate the 

plate, flowing freely to the edge. 

5. Let the target plate dry by allowing the solvent to volatilize, leaving a thin film of grease on 

the plate. 

6. Sparingly, use a very thin film of grease (if needed) to lubricate the O-rings prior to 

inserting the reassembled impactor into a clean adapter. Ensure the exterior of the 

impactor is clean and free of any artifacts that could deposit onto the filter. 

7. The adapter should be clean inside and out, free of any dust, residues or other artifacts. 

The adapters can be cleaned with warm soapy water and allowed to air dry. Do not wipe 

down with materials that can leave lint. 

4.1.3 Filter Handling and Processing 

Filter handling presents the greatest opportunity to introduce error. The lower volumes (and 

therefore less matter) encountered with the MinivolTM versus FRM samplers amplifies the 

significance of accurate filter weights. Accumulation of matter on the filter from other than the 

actual sample collection itself must be prevented. On the other hand, care must be taken to 

ensure PM collected during sampling is not lost afterward, or that material from the filter itself is 

not lost during handling. The 47mm quartz or teflon-coated glass fiber filters provided are 

delicate and easily damaged. Standard precautions: 

3⁄4 Wear new Nitrile, no-powder gloves each time 

3⁄4 Load filters just before sampling, not hours/days prior 

3⁄4 Handle filters in clean area, away from air disturbances 

3⁄4 Use only non-serrated forceps, preferably teflon coated 

3⁄4 Handle filters by the filter edges only; never bend or fold 

3⁄4 Keep filters covered and protected when not actually handling

3⁄4 Do not use any filter damaged, dropped, or otherwise contaminated

Filter Cassette: exploded view 

and as loaded in Filter Holder 

1. Open a clean Filter Cassette (FC). 

2. Select a filter and carefully remove from petri dish by using the precut forceps groove in 

the side of the dish. Do not attempt to “dig” the filter out of the dish. 

3. Inspect filter. It must not be bent, torn, contain perforations, or be otherwise damaged. 

4. Place filter on the FC drain disk, rough side up! Reassemble the FC and place into the 

filter holder (as shown below). Screw the adapter on snugly. 

5. Record the filter, filter holder, and sample numbers on the Field Datasheet. 

6. Opening FC: Upon retrieval of sample or field blank, always use the Cassette Shoe to open 

FC to prevent loss of particulate matter. Never pull apart the cassette to retrieve filter. 
19

Grasp cassette shoe with one hand; use thumb and forefinger 

of other hand to maintain grip of cassette edges while 

sliding, to prevent cassette from flying apart and 

disrupting PM deposits. Practice technique before actual 

sampling. 

Field Blanks (FBs): Process one FB for every nine sampling events (unless 

instructed otherwise). FBs are loaded into a clean filter holder with appropriate 

impactors and carried to the site in a clean ziplock bag. Momentarily attach to 

sampler, remove, and immediately bring back to clean process area. Handle and 

process as a normal sampling event—except FB’s are not exposed to 

calibrations or the 24-hour sampling run. Complete a datasheet for each FB. 

Trip Blanks (TBs): Include one completely unused/unopened filter as a trip blank when 

shipping sampling filters and field blanks. Ensure it is appropriately labeled “Trip Blank”. 

Shipping Filters: All samples and blanks should be stored/shipped upright in their 

original, appropriately marked petri dishes. Secure dish covers with a rubber band and place 

in individual 3” x 5” zip lock bags. When shipping, include enough packing material to 

prevent movement during shipment. Include Field Datasheets and Meteorology Datasheets. 

Mark box “FRAGILE” and “UP⇑”. Priority mail to appropriate lab as instructed. 

4.2 CALIBRATION 

Calibrate the instrument to sample at 5 liters per minute in the field (actual 

conditions) prior to all sampling runs. Because air density does not affect the 

flow rate readings of the BIOSTM flow meter (vs. rotameter), no corrections are 

required to ensure 5 lpm, actual conditions. Varying air densities also are not a 

significant factor in toxicological exposures to PM, so unlike gaseous 

pollutants, the EPA requires no STP corrections for particulate matter sample 

results (however, meteorological conditions will still need to be recorded for 

each sampling event). 

Airmetrics typically supplies a calibration curve for the instrument’s rotameter. 

The company also sells a digital manometer that reads in static pressure, and a 

blue calibration orifice with a calibration curve and associated equations for 

conversions and corrections. These will not be necessary for calibrations or for 

calculating final flow rates. These procedures have been greatly simplified by 

the application of a BIOSTM DryCal® flow meter—a field-portable primary flow 

standard that provides direct calibrations in lpm. The Airmetrics’ blue 

calibration orifice has been modified to interface with, and act as the instrument 

adapter for, the BIOSTM flow meter. 
20

Operational Check: Prior to each sampling run, the 

instrument should be checked out for leaks and 

given an initial calibration in a clean area. This will 

confirm the sampler is performing properly and will 

reduce any “tweaking” needed when calibrating in 

the field. Follow the procedures below. 

 

3⁄4 Setup: Ensure sampling filter and appropriate 

impactors (greased) are in place. The hose to the 

calibrator should be attached to the bottom port. Inspect 

for kinks in the lines or any other obstruction in the 

calibration train. 

 

3⁄4 Leak Test: Upon train setup: 

Press the calibrator’s OOONNN button. 

Press OOONNN///AAAUUUTTTOOO///OOOFFFFFFon the Minivol’s control panel to 

manually turn on the pump. Check for any restrictions. 

Place your thumb or other seal over the open end of the 

calibrator’s intake. The sampler should stop operating 

within 5-10 seconds. If it does not, check the seal and, if 

necessary, the sampling train for leaks. To isolate leaks, 

disassemble the train at each connection, starting with 

the calibrator, and perform a leak check at each step as 

you work your way back. Example: pull the hose off the 

BIOS calibrator and seal the hose opening. Restart the 

sampler. If the leak check passes, the problem is the 

hose/calibrator connection or the calibrator itself. If it 

fails, continue moving through the train, sealing off each 

connection until you isolate the leak. 

Calibration Procedure: You should familiarize yourself 

with the BIOS DryCal DC-Lite calibrator (starting on page 5 of the calibrator instruction 

brochure provided). Once the leak test

passes: 

1. Press the “READ” button on the BIOSTM

calibrator to read the sampling rate in lpm 

(observe the FLOW, not the AVERAGE). 

The “RRREEEAAADDD” button must be pushed once 

each time to observe an instantaneous flow 

reading (or, press and hold the button to 

iniate the “AUTO” mode, which provides a 

new reading every few seconds). 

2. Adjust sampler flow rate by turning the 

FFFLLLOOOWWWAAADDDJJJUUUSSSTTT knob on the sampler 
21

control panel. Adjust to 5 lpm +/- 2% (+/- 0.1 lpm). This equates to an acceptable range 

of 4.90 – 5.10 lpm. Disregard the indicated rotameter reading. 

3. Once individual readings indicate 5 lpm (+/- 0.1 lmp), press the “READ” button 10 

consecutive times (or allow the “AUTO” mode to sequence through 10 readings). Observe

the average for all 10 readings. If the average is within the acceptable range, calibration is 

successful. 

 

4. For official field calibrations, record the average as the initial flow rate. If the average is 

outside the threshold, readjust the flow rate accordingly until the average of 10 consecutive 

readings is within 4.9 – 5.1 lpm. 

4.3 SAMPLING ROUTINE 

24-hour sampling runs will generally be conducted at 6-day intervals. AFIERA will provide 

instructions regarding any changes to sampling routine. 

4.3.1 Pre-sampling 

If the sampler is to be operated by battery, the Minivol battery must be fully charged prior to 

sampling. The calibrator should also be charged. Once the instrument passes the operational 

and calibration checks in a clean area: 

1. Record preliminary information on the Field Datasheet (i.e., date, location, sample no., etc.). 

2. Detach calibration train and the filter assembly from the sampler. 

3. Place filter/impactor assembly in a clean plastic bag (e.g., zip lock) with a clean rain cap. 

4. Reinsert control panel into the instrument housing for transport. 

5. Transport filter/impactor assembly and calibration train in a suitable protective carrier, e.g., 

carrier cases that accompanied the new instrument. Bring Field Datasheet. 

4.3.2 Field Procedures 

At field location, carry out the steps below before sampling. Procedures should be performed 

in an area relatively free from the elements. If necessary, carry them out within a vehicle. 

Remove control panel from instrument housing. Do not detach power cord. Grasp unit by 

top cap, not circuit board; place panel on lip edge, and support against wall/structure.

Attach filter/impactor assembly and calibration train to the instrument. 

Start pump by pressing the OOONNN///AAAUUUTTTOOO///OOOFFFFFF button on the control panel. 

Leak check sampler. 

Calibrate to 5 lpm +/- 2% (avg. over ten consecutive readings) under ambient conditions 

Record average (AVG) flow rate on the Field Datasheet. 
22

Turn off sampler, record reading from Elapsed Time Totalizer LED (next to AA battery). 

Set Real Time Clock (if necessary): Personnel should 

synchronize their watch with the instrument clock. 

• DAY SET: While holding down CCCLLLOOOCCCKKKbutton, press

WWWEEEEEEKKK button until correct day appears at top. 

• TIME SET (Hour): Hold down CCCLLLOOOCCCKKK and press HHHOOOUUURRR

until display indicates correct hour (you may need to cycle 

through hours to obtain proper AM/PM). 

• TIME SET (Minutes): Hold down CCCLLLOOOCCCKKK and press MMMIIINNN

until the display indicates correct minutes. Seconds will 

automatically reset to zero. 

Set Timer: (It is recommended that the timer be set up at 

the field location) 

9.1 Set new on/off times. 

9.1.1 Press PPPRRROOOGGG once. 1on will appear in the lower left corner. 

9.1.2 Press HHHOOOUUURRR and MMMIIINNN to set desired start time. Note the correct AM/PM. 

9.1.3 Press WWWEEEEEEKKK to select day of the week (i.e., Mo, Tu, We, Th, Fr, Sa or Su). When 

more than one day is displayed, these days will all have the same power-on time. 

9.1.4 Once the program-on time is set for the first cycle, press PPPRRROOOGGG again to set 

program-off. 1off will now appear. Again press HHHOOOUUURRR, MMMIIINNN, and WWWEEEEEEKKK buttons in 

sequence to set those parameters and complete the first cycle. Note the correct 

AM/PM. 

Normally, only one cycle will be necessary. All subsequent cycles (2 – 6) should be clear. 

9.2 Clear unwanted entries. 

9.2.1 Once Cycle 1 is set up, press PPPRRROOOGGGto toggle through each of the remaining cycles (2 

- 6). If a start or stop time is observed in these cycles, press RRREEESSSEEETTTonce to clear the 

entry (a cleared entry is signified by four dashes in place of the time). (Note: 

Pressing the RESET button again will recall, or reinsert the time just cleared!)

9.2.2 Verify correct program entries for all 12 entry locations by pressing PPPRRROOOGGGto toggle 

through the 6 on/off cycles. 

Your entries for cycle 1 should look similar to the following example: 
23

AM Mo 

 8:00 00

1on

 

AM Tu 

 8:00 00

1off

 Press CCCLLLOOOCCCKKK to return to the real-time clock display. 

11. Press OOONNN/

//AAAUUUTTTOOO///OOOFFFFFF button until the bar on the lower edge of the display is above the 

 “AUTO” legend. The timer is now set. 

12. Reinsert Control Panel into the instrument housing. The instrument is now ready to 

 sample. (Placement/mounting instructions can be found in Section 4.4, SITING) 

4.3.3 Post-sampling 

Potential for change in sample mass due to particle loss, passive PM deposition, and 

damage to the filter increases between end of sample run and processing of filter. Therefore, 

personnel should arrive at the sample location before the end of the sample run so 

that the filter can be processed immediately after sampling. At the completion of the 

sampling run: 

1. Remove sampler from mounting pole to a relatively clean, nearby area out of the 

elements. Maintain the sampler/filter assembly in an upright position at all times. Place 

on a firm, level surface. 

2. Gently lift pump/timer assembly out of the unit and mount on the edge of the housing, 

preferably against a support structure such as a wall. 
24

3. Check control panel for the Error Conditions below. Either condition results in premature 

pump shutdown. If an error condition exists, refer to the “Error Conditions” discussion at 

the end of this section for troubleshooting assistance. 

• LLLOOOWWWFFFLLLOOOWWW Indicator 

• LLLOOOWWWBBBAAATTTTTTEEERRRYYY Indicator 

4. Verify elapsed time as shown on the Elapsed Time Totalizer at the top of the control 

panel to validate sampling event. If the time lapse is less than 24 hours, refer to the “Error 

Conditions” discussion at the end of this section. 

5. Verify correct time and day on the time LCD to validate sampling event. 

6. Record ending flow rate on Field Datasheet: remove rain cap, attach calibration train, and 

press OOONNN///AAAUUUTTTOOO///OOOFFFFFF twice to start pump. Record the average (AVG) of 10 consecutive 

readings. 

7. Detach Filter Assembly and carefully place into a clean zip lock bag for transport to filter 

processing area (clean area). Every attempt should be made to keep the assembly in 

an upright position throughout the handling, transportation, and processing steps. 

Filter Recovery 

8. In a clean area, carefully remove filter and place in appropriately numbered petri dish, 

rough side up. Close the dish immediately and secure with rubber band. Store upright. 

Refer to Section 4.1.3, “Filter Handling”, for handling procedures, precautions, and 

packing/shipping instructions. 

9. Complete Field Datasheet and Meteorological Records as described in section 4.5, 

“RECORDKEEPING”. 

10. Prepare for the next sampling event. Refer back to section 4.1.2, “Filter Assembly and 

 Impactor Preparation” to prepare for the next sampling event. 
25

Error Conditions 

LOW BATTERY Indicator ON 

Observe the total elapsed sampling time (Elapsed Time Totalizer) to determine the length of 

the sampling run before the sampler turned off. If the sampler operated for at least a few 

hours of time, the likely problem is the battery was not fully charged. Switch to the fully 

charged backup battery to complete the scheduled sampling event while recharging the first 

battery according to the manual’s directions. If the second sampling attempt is successful, try 

the first battery again for a 24-hour period, this time in or near the office/lab area. If the 

problem reoccurs, the battery is defective and will need to be replaced. If both batteries have 

similar problems, it could be the AC source, or the instrument’s pump is operating at an 

abnormally high rate throughout the sampling period to compensate for a restriction 

somewhere in the sampling chain. One other problem could be a pump that is drawing an 

abnormal amount of current. Determining whether the source of the problem is the battery 

power or the sampler can be accomplished by trying the batteries out in another sampler. 

LOW FLOW Indicator ON 

Do not confuse this indicator light with the THRESH indicator light, which normally lights 

whenever the sampler is attached to a power source but is not operating. 

Observe the total elapsed sampling time. If the battery is O.K., the problem may be due to an 

Air Restriction in the impactor inlets, filter holder (e.g., overloading of filter, wet filter, etc.), or 

tubing (crimps). Loose or broken tubing on the outlet side of the pump could also cause a 

low flow condition.). A Pump Malfunction could result in a low flow condition, which is 

usually caused by damaged or contaminated pump head components (valves, diaphragms). 

Determining whether the problem is within the filter assembly or the sampler can be 

accomplished by operating the sampler with the assembly both connected and disconnected. 

For pump maintenance instructions, see Section 7 of the manufacturer’s technical manual. 

Overriding Low Battery/Low Flow Indicators 

When these indicator lights are on, pressing the RESET button on the control panel can 

restart the instrument. Pressing and holding the switch provides continuos override of the 

fault circuit, when needed to troubleshoot the instrument. 

Additional Troubleshooting 

Other problems that can be encountered and their corrective actions can be found in Section 

8, page 57 of the manufacturer’s technical manual. 
26

4.4 SITING 

Do not site the instrument adjacent to obvious air emission sources, such as 

industrial processes, generators, fueling and fuel storage areas, vehicle or 

aircraft maintenance and operating areas, any type of stack or vent, refuse or 

other waste sites, etc. 

Do site the instrument: 

3⁄4 at or near the center of the base population 

3⁄4 in an area that provides easy access and security from tampering 

3⁄4 in a relatively open area in which nearby buildings/structures do not impede natural air flow 

3⁄4 with the air inlet at a height above the ground between 2 – 15 meters (6.5 – 49 ft) 

3⁄4 with the air inlet at a height above the supporting surface of 2.0 m +/- 0.2 m (6 – 7 ft) 

3⁄4 with the air inlet at least 1 m (3.25 ft) away from the nearest wall, structure, or other 

obstacle to air flow (preferably much more) 

Low-story roofs often provide an adequate measure of security and representative 

monitoring. The sampler inlet must be above the height of any wall or barrier surrounding the 

area. 

Obtain GIS coordinates of the site. Ask a local GIS-equipped unit to provide assistance. 

Sample Latitude and Longitude in both degrees and minutes. This information is required on 

PM Sampling Datasheets. Note: Check to ensure that accuracy of GIS does not make 

coordinates classified. 
27

Additional Precautions: 

3⁄4 The pole will likely require additional support in areas susceptible to high winds/tipover

• Mounting brackets are located on the bottom of each tripod leg, along with screws, to 

secure the tripod to the roof or appropriate surface once adequate siting is 

accomplished; bracing with rope or other means of support may also be considered 

 

3⁄4 The top of the inlet must remain horizontal during sampling; ensure the pole is 

straight and, if necessary, use tape to stabilize the sampler against the pole 

 

4.5 RECORDKEEPING And REPORTING 

4.5.1 Field Datasheet 

Complete a Field Datasheet for each sample and field blank (not trip blank). Review 

the sheets for completion before forwarding. The original datasheets will be placed in 

zip lock bags, packaged with the associated samples, and forwarded to the supporting 

lab, which may be CHPPM or AFIERA. Retain a copy on site and mail another copy to: 

Deployment Environmental Surveillance 

AFIERA/RSEW 

2513 Kennedy Circle, Bldg. 180 

Brooks AFB, TX 78235-5123 
28

Field Datasheet – PM Sampling 

Instructions 

Preliminary Data 

Installation: Self explanatory. Base Code: PSAB:1242 / Al Jaber:1237 / Esk Village:1235

Site Location: Describe area, e.g., “Building 28, barracks rooftop.” 

Geolocation: Original siting measurements. Provide Degrees and Minutes. 

Date: Sampling start date. 

Sample ID#: Dependent upon analytical support lab: 

For CHPPM: XXX YYYY DDDDD ZZ 

• XXX - First three letters of base/installation 

• YYYY - Method type (PM10 or PM25) 

• DDDDD - Jday code: last two digits of year and three digit Julian day (e.g., 00030 for 30 

Jan 00) 

• ZZ- Sample type: P-Primary sample; C-Collocated sample; FB-Field Blank; TB-Trip Blank 

For AFIERA: XX XX XXXX 

• First two digits: EX 

• Second two digits: Sample Year (00 for SY 2000) 

• Last four digits: Numerically sequenced sample number for that base during the 

calendar year. 

The AFIERA Lab will also require AF Form 2750 (3 samples per form) in place 

of 

the Field Datasheet. However, completion of the Field Datasheet is still required 

and must be forwarded to AFIERA/RSEW Deployment Environmental 

Surveillance. 

Sample Type: Circle one—except for metals. Metals are sampled/analyzed in conjunction with 

PM10, PM2.5, or TSP. Circle “Metals” and the appropriate PM type. 

Filter ID#: Fill in with pre-assigned numbers which accompany the filters from support Lab. 

Instrument SN: MiniVol serial number. 

Calibrator Mod/SN: Calibrator model and serial number.

Filter Assembly ID#: Fill in with pre-assigned numbers from AFIERA DES. 

Operator: Sampler’s name. 

Contact Info: Sampler’s E-mail address and Telephone number. 

SIgnature: Sampler’s signature. 
29

Field Data 

Pre-Sample 

Leak Check: Fill in block with Pass upon successfully completing leak check. If failure at start, 

fix problem before initiating sampling.

Starting Flow Rate: Calibrated flow rate, i.e., 5000mL/min +/- 100mL (avg of 10 consecutive 

readings). 

Sample Start Time: Normally the start time programmed into the timer, if used. 

El. Time Totalizer: Record start reading from control panel after calibration. 

Post Sample 

Leak Check: If leak is identified within the sampler or the attached filter/impactor assembly— 

sample is invalid. If the leak is identified within calibration train—fix and re-test.

Ending Flow Rate: Post-sampling flow rate (average over 10 readings).

Sample Stop Time: Self explanatory. 

El. Time Totalizer: Record End reading upon completion of sampling event—but before measuring 

 ending flow rate. A valid sample time is between 23 and 25 hours. 

Average Flow Rate: Average of Starting and Ending flow rates. 

Total Sample Time: Record in Minutes. (e.g., 24 hrs x 60 min = 1440) Valid sample is 23 – 25 hours. 

 Do not use the Elapsed Timer Totalizer readings for this. 

Actual Volume, Vact: Multiply the average flow rate (Qact) x Minutes sampled. 

Background Notes: Include any information that could affect sampling results for this sample. 

Notable activities would include increased aircraft/ vehicle operations, or 

other combustion processes in the area during the sampling, significant 

wind-blown dust events, or any activity or event that could affect airborne 

particulate matter concentrations. Include any unusual circumstances and 

any other helpful information associated with the sample or sample period. 

Lab Analysis To be completed by CHPPM or AFIERA, depending on support lab. 

4.5.2 AF Form 2750 

Only when the supporting analytical lab will be AFIERA, an AF Form 2750 (3 samples per form) 

will also need to be accomplished and forwarded along with the samples. In this situation, mail 

the original Field Datasheet to AFIERA/RSEW Deployment Environmental Surveillance and 

maintain a copy of each form. CHPPM lab requires only the original Field Datasheet with the 

samples—no Form 2750 is required. Mail a Field Datasheet copy to AFIERA/RSEW 

Deployment Environmental Surveillance and retain a copy. 
30

4.5.3 Meteorological Data 

Record the Meteorological Data for the beginning of the sampling period and at eight-hour 

intervals during the sampling event for a total of four readings. Include your observations 

over the event regarding visible emissions or odors. Meteorological information can be 

obtained from the local supporting Weather Station. 
31

Appendix B 

SUMMA Canister Sampling for Ambient VOCs – (TO 14A)
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

32
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

33
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

34
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

35
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

36
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

37
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

38
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

39
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

40
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

41
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

42
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

43
Excerpt Taken from USACHPPM DRAFT TG-251 

APPENDIX 6-4 

AMBIENT AIR VOLATILE ORGANIC COMPOUND (VOC) SUMMA 

CANISTER SAMPLING (TO-14A) 

44
 

45

Appendix C 

PS1 Sampling Instructions - (TO-14A)
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

46
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

47
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

48
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

49
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

50
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

51
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

52
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

53
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

54
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

55
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

56
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

57
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

58
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

59
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

60
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

61
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

62
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

63
Excerpt from USACHPPM DRAFT TG-251 – 

Appendix 6-5 PS1 Sampling Instructions 

64
65

Appendix D 

Oil Well Fire Equipment List 
66

Oil Well Fire Equipment List 

# Container Item Unit Quantity 

1 Blue Box PS1 Sampler Body ea 1 

1 Blue Box PS1 Extra motor ea 1 

1 Blue Box Power Strip ea 1 

1 Blue Box Isopropyl alcohol bottle 1 

1 Blue Box PS1 Calibrator ea 1 

2 Blue Box PS1 Sampler Hood ea 2 

2 Blue Box Sampler Heads ea 2 

2 Blue Box Sampler Feet ea 4 

2 Blue Box Nalgene Bottles ea 2 

2 Blue Box PS1Operation Instructions ea 1 

2 Blue Box 550 Cord ea 1 

2 Blue Box Aluminum Foil roll 1 

2 Blue Box Screwdriver Set ea 1 

3 

Cardboard 

Box TSP Body ea 1 

3 

Cardboard 

Box TSP Head ea 1 

3 

Cardboard 

Box TSP Motor ea 1 

3 

Cardboard 

Box TSP Filter Holder ea 2 

4 

Cardboard 

Box TSP Calibrator ea 1 

5 

Cardboard 

Box Tripod Legs ea 3 

6 Pelican Case SKC Pocket Pump ea 3 

6 Pelican Case SKC Universal Chargers ea 3 

6 Pelican Case Dry Cal Calibrator ea 1 

6 Pelican Case TO17 Calibration Tube ea 1 

6 Pelican Case SKC Pocket Pump Instructions ea 3 

6 Pelican Case Sampling tube holder and tubing ea 3 

7 Pelican Case Mini Vol Unit ea 1 

7 Pelican Case Mini-Vol Sampling Heads ea 2 

7 Pelican Case Mini-Vol Batteries ea 2 

7 Pelican Case Mounting bracket and cradle ea 1 

7 Pelican Case Mini-Cal Calibrator ea 1 

8 Pelican Case Mini Vol Unit ea 1 

8 Pelican Case Mini-Vol Sampling Heads ea 2 

8 Pelican Case Mini-Vol Batteries ea 2 

8 Pelican Case Mounting bracket and cradle ea 1 

9 

Cardboard 

Box Environmental Sampling Backpack ea 1 

 ? Sampling Media - PM10 (Mini-Vol Sampler) ea 20 

 ? Sampling Media - TSP ea 20 

 ? Sampling Media - TO13 (PS1 Sampler) ea 5 

 ? Sampling Media - TO17 (SKC Pumps) ea 21 

 ? Sampling Media - OVM ea 20 
67

Cardboard 

Box Deployment Potable Water Sampling Kit / with cooler ea 2 

 

Cardboard 

Box Deployment Soil Sampling Kit (3 containers) / with cooler ea 1 

 

Cardboard 

Box Field Notebooks ea 2 

 

Cardboard 

Box Sampling instructions and datasheet binder ea 1 

 

Cardboard 

Box Pens ea 2 

 

Cardboard 

Box Packing Tape ea 3 

 

Cardboard 

Box 1600 Watt Transformer ea 1 
AFIOH/DOBP (STINFO) 

2513 KENNEDY CIRCLE BROOKS CITY-BASE TX 78235-5116 ________________________________________________________  OFFICIAL BUSINESS