Quarterly Groundwater Monitoring Report – Outside 

(Non-Tunnel) Wells 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

August 2010 

Prepared by: 

TEC Inc. 

1003 Bishop St. Suite 1550 

Pauahi Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 
1 

Table of Contents 

Table of Contents ............................................................................................................................ 1

Executive Summary ......................................................................................................................... 2

1.0 Introduction.......................................................................................................................... 3

1.1 Project Objective .............................................................................................................. 3

1.2 Previous Reports .............................................................................................................. 3

1.3 Background ...................................................................................................................... 4

1.3.1 Site Description ......................................................................................................... 4

1.3.2 Facility Information .................................................................................................. 5

1.3.3 UST Information ....................................................................................................... 6

1.4 Regulatory Updates .......................................................................................................... 6

2.0 Sample Collection and Analyses .......................................................................................... 6

2.1 Monitoring Well Purging ................................................................................................. 6

2.2 Groundwater Sample Collection ...................................................................................... 7

2.3 Groundwater Sample Analyses ........................................................................................ 7

3.0 Groundwater Sample Analytical Results ............................................................................ 6

3.1 July 2010 Sample Analytical Results ............................................................................... 7

4.0 Summary and Conclusions ............................................................................................... 9

5.0 References .......................................................................................................................... 12

List of Tables 

Table 1 Monitoring Well Information ........................................................................................6 

Table 2 Analytical Results for Quarterly Groundwater Sampling (July 8, 2010) ......................8 

List of Figures 

Figure 1 Groundwater Monitoring Well Locations ....................................................................10 

Figure 2 TPH Detected in Groundwater .....................................................................................11 

List of Appendices 

Appendix A – Laboratory Analytical Reports 
2 

Executive Summary 

There are 18 active and 2 inactive, 12.5 million gallon, field-constructed underground storage 

tanks (USTs) located at the Red Hill Fuel Storage Facility (the Facility). Previous environmental 

site investigations indicated a release had occurred and contaminated the groundwater underlying 

the Facility. 

The United States (US) Navy implemented a groundwater monitoring program, which includes 

collecting groundwater samples quarterly from US Navy Well 2254-01 (RHMW2254-01) and 

four wells installed in the Facility lower access tunnel (RHMW01, RHMW02, RHMW03, and 

RHMW05). The US Navy Well 2254-01 is located approximately 3,000 feet downgradient from 

the Facility and provides approximately 24 percent of the potable water to the Pearl Harbor 

Water System (PHWS). The groundwater samples are analyzed for petroleum constituents and 

compared against State of Hawaii Department of Health (HDOH) Drinking Water 

Environmental Action Levels (EALs) (HDOH, 2008). 

In response to increasing concentrations of contaminants of potential concern in the groundwater 

monitoring wells within the facility (specifically RHMW02) during 2008, plans were made to 

conduct four rounds of quarterly sampling at the following outside monitoring well locations: 

 RHMW04; 

 Oily Waste Disposal Facility monitoring well 01 (OWDFMW01); and 

 Halawa Deep Well 2253-03 (referred to as HDMW2253-03 in this report). 

Since four quarterly sampling events at RHMW04 and OWDFMW01 have already been 

completed (during August 2009 through April 2010), this groundwater monitoring report 

presents the analytical results for samples collected on July 8, 2010 at HDMW2253-03. 

Laboratory analytical results indicate that only naphthalene was detected above the laboratory 

method detection limit (MDL) via United Stated Environmental Protection Agency (USEPA) 

Method 8279C SIM at 0.0596F μg/L [F indicates that the compound was identified, with the 

concentration above the laboratory MDL, but below the reporting limit (RL), therefore it is 

considered an estimate] in HDMW2253-03. No other compounds were detected above the MDL 

during July 2010. 
3 

1.0 Introduction

This report presents the results of the fourth groundwater sampling event at HDMW2253-03, 

conducted in July 2010. The first, second, and third sampling events at HDMW2253-03 were 

conducted in October 2009, January 2010, and April 2010, respectively. Four quarterly 

sampling events at two other monitoring wells (RHMW04 and OWDFMW01) were completed 

during August 2009, October 2009, January 2010, and April 2010. An August 2009 sampling 

event for HDMW2253-03 was not conducted due to access issues. 

These three wells surround the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred 

to as “the Facility”). This groundwater sampling and analysis is considered supplemental to the 

quarterly groundwater monitoring program conducted within the Facility. This supplemental 

sampling was conducted in response to increasing concentrations of contaminants of potential 

concern in a groundwater monitoring well within the Facility, specifically RHMW02 during 

2008. 

1.1 Project Objective 

This groundwater sampling project was performed to evaluate the presence of chemicals of 

potential concern in groundwater surrounding the Facility. The project was conducted to ensure 

the Navy remains in compliance with Hawaii Department of Health (HDOH) UST release 

response requirements. The groundwater sampling program followed the procedures described 

in Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan [TEC Inc. (TEC), 2008 

updated in 2009], also referred to as “the Plan”. 

This groundwater sampling event was conducted by TEC under United States (US) Navy 

Contract Number N47408-04-D-8514, Task Order No. 54, Modification No. 01. 

1.2 Previous Reports 

As indicated earlier, this outside well sampling supplements the quarterly groundwater 

monitoring of wells within the Facility, which began in 2005. The following groundwater 

monitoring reports were previously submitted to the HDOH, for groundwater monitoring wells 

within the Facility: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 
4 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 

12. Groundwater Monitoring Results, July 2008 (submitted October 2008); 

13. Groundwater Monitoring Results, October and December 2008 (submitted February 

2009); 

14. Groundwater Monitoring Results, February 2009 (submitted May 2009); 

15. Groundwater Monitoring Results, May 2009 (submitted July 2009); 

16. Groundwater Monitoring Results, July 2009 (submitted September 2009); 

17. Groundwater Monitoring Results, October 2009 (submitted December 2009); 

18. Groundwater Monitoring Results, January, February, and March 2010 (submitted April 

2010); 

19. Groundwater Monitoring Results, April 2010 (submitted May 2010); and 

20. Groundwater Monitoring Results, July 2010 (submitted August 2010). 

The following groundwater monitoring reports were previously submitted to the HDOH for 

groundwater monitoring wells outside the Facility: 

1. Groundwater Monitoring Results, August 2009 (submitted September 2009); 

2. Groundwater Monitoring Results, October 2009 (submitted December 2009); 

3. Groundwater Monitoring Results, January 2010 (submitted April 2010); and 

4. Groundwater Monitoring Results, April 2010 (submitted May 2010). 

1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Red Hill, Oahu, Hawaii. Land adjacent to the north of the Facility is 

occupied by the Halawa Correctional Facility and private businesses. Land to the south and west 

of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east of the 

Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet from the Facility (Dawson, 2006). The US Navy Well 2254-01 is located 

approximately 3,000 feet west of the Facility and provides approximately 24% of the potable 

water to the Pearl Harbor Water System, which serves approximately 52,200 military consumers 

(TEC, 2008). 
5 

1.3.2 Facility Information 

The Facility consists of 18 active and two inactive USTs operated by Navy Fleet and Industrial 

Supply Center (FISC) Pearl Harbor. Each UST has a capacity of 12.5 million gallons. The 

Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006). 

In 2002, the US Navy installed a groundwater monitoring well (currently named RHMW01) into 

the basal aquifer, directly down-gradient from the Facility, within the lower access tunnel. 

Groundwater samples from this well indicated that petroleum from the Facility has migrated to 

the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the 

aquifer to protect their down-gradient drinking water resource associated with the US Navy Well 

2254-01. 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility UST system, a groundwater monitoring well 

(RHMW04) north of the Facility adjacent to the US Navy Firing Range, and a groundwater 

monitoring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). Since 

2005, RHMW01, RHMW02, RHMW03, and RHMW2254-01 have been sampled quarterly for 

TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. 

Due to increasing concentrations of contaminants of potential concern at the groundwater 

monitoring wells within the Facility (specifically RHMW02) during 2008, response measures 

were warranted. In April 2009, another groundwater monitoring well (RHMW05) was installed 

within the lower access tunnel between RHMW01 and RHMW2254-01. It was installed to 

identify the extent of contaminant migration before it reaches the infiltration gallery at 

RHMW2254-01. 

Additionally, plans were made to sample three monitoring wells surrounding and outside of the 

Facility, RHMW04, OWDFMW01, and HDMW2253-03. RHMW04 was installed to provide 

contaminant chemistry data for water moving through the basal aquifer beneath the Facility. 

OWDFMW01 (originally known as MW08) was installed into the basal aquifer in 1998 for a 

Phase II Remedial Investigation/ Feasibility Study for the Red Hill Oily Waste Disposal Facility 

(Earth Tech Inc., 2000). It is located geographically down-gradient of the USTs and US Navy 

Well 2254-01. HDMW2253-03 is controlled by the State of Hawaii Commission on Water 

Resource Management. It is located between the Facility and the municipal drinking water 

supply well run by the City and County of Honolulu Board of Water Supply (Halawa Shaft 

pumping station 2354-01). 

Table 1 summarizes basic groundwater monitoring well information, Figure 1 shows 

groundwater monitoring well locations and Appendix A provides the laboratory data. 
6 

Table 1. Monitoring Well Information 

Groundwater Well TOC Elevation 

(ft msl) 

DTW (ft) TD (ft) 

RHMW04 313.03 293 320 

OWDFMW01 138.94 120 142.8 

HDMW2253-03 225 210 1,575 

Notes: 

 DTW - Distance to water 

 TD - Total depth of well 

 TOC - Top of casing 

ft – Feet 

ft msl - Feet from mean sea level 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel, JP-8, and F-76 (diesel marine fuel). Previously, several tanks 

stored Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Regulatory Updates 

During the summer and fall of 2008, HDOH updated their EALs, which resulted in significant 

changes to the action levels associated with methylnaphthalenes. The drinking water toxicity 

EAL for these compounds was 240 g/L. This concentration presumed that methylnaphthalenes 

were non-carcinogenic. Evidence that they are human carcinogens has now been accepted by the 

US Environmental Protection Agency (USEPA). As a result, HDOH adopted more rigorous 

EALs of 4.7 g/L for 1-methylnaphthalene and 24 g/L for 2-methylnaphthalene, corresponding 

to a residential tap water scenario, and a 1 in a million cancer risk (HDOH, 2008). 

Also, the drinking water EAL for naphthalene was increased from 6.2 g/L to 17 g/L (HDOH, 

2008). Finally, the HDOH Drinking Water EAL for TPH-DRO was increased from 100 g/L to 

210 g/L, although the HDOH Groundwater Gross Contamination EAL for TPH-DRO remains 

100 g/L. 

2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on July 8, 2010. 

Groundwater samples were collected from one monitoring well, HDMW2253-03. Sampling and 

analysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater 

Protection Plan (TEC, 2008). 

2.1 Monitoring Well Purging

Due to the well construction characteristics of HDMW2253-03, the well was not purged prior to 

sampling, but field parameters were recorded. Rather than purging, a grab sample was collected 

at a depth below the solid casing (which extends about 50 feet below the water table) and within 

the open-holed portion of the well. Field parameters included pH, temperature, specific 

conductivity, dissolved oxygen, and turbidity. 
7 

2.2 Groundwater Sample Collection 

HDMW2253-03 was sampled using a disposable bailer designed to collect samples at desired 

depths. Samples were placed into sampling containers with appropriate preservatives [i.e., 

hydrochloric acid (HCl) for volatile organic analysis, nitric acid (HNO3) for dissolved lead]. The 

dissolved lead sample was filtered in the field and placed in a preserved bottle. Sample 

containers were labeled with the date, sample identification number, type of analysis, and 

sampler’s name. The containers were placed on ice in a sample cooler and transported under 

chain-of-custody procedures to the certified laboratory for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, VOCs by EPA Method 8260B, PAHs by 

EPA Method 8270C SIM, and dissolved lead by EPA Method 6020. 

3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

HDMW2253-03. A summary of groundwater analytical results for TPH-DRO and TPH-GRO, 

VOCs, PAHs, and dissolved lead is included in Table 2. Complete analytical laboratory reports 

are provided in Appendix A. 

3.1 July 2010 Sample Analytical Results 

Groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. The results are discussed below. 

HDMW2253-03

Naphthalene was analyzed by USEPA Method 8270C SIM and USEPA Method 8260B. Trace 

concentrations of naphthalene was detected at 0.0596F μg/L [F indicates that the compound was 

identified, with the concentration above the laboratory method detection limit (MDL), but below 

the reporting limit (RL), therefore it is considered an estimate] in HDMW2253-03, via USEPA 

Method 8270C SIM. This concentration is significantly below the HDOH Drinking Water EAL 

for this constituent (i.e., 17 μg/L). No other potential chemical of concern was detected above 

the laboratory MDL in HDMW2253-03 (Table 2). 
Page 

Table . Analytical Results for Quarterly Groundwater Monitoring Release Response Report (July 8, 2010)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL

TPH as DIESEL RANGE ORGANICS 210 100 ND U 160 426

TPH as GASOLINE RANGE ORGANICS 100 100 ND U 30 100

1-METHYLNAPHTHALENE 4.7 10 ND U 0.0174 0.0581

2-METHYLNAPHTHALENE 24 10 ND U 0.0174 0.0581

ACENAPHTHENE 370 20 ND U 0.0174 0.0581

ACENAPHTHYLENE 240 2000 ND U 0.0174 0.0581

ANTHRACENE 1800 22 ND U 0.0174 0.0581

BENZO(a)ANTHRACENE 0.092 4.7 ND U 0.0174 0.0581

BENZO(a)PYRENE 0.2 0.81 ND U 0.0174 0.0581

BENZO(b)FLUORANTHENE 0.092 0.75 ND U 0.0174 0.0581

BENZO(g,h,i)PERYLENE 1500 0.13 ND U 0.0174 0.0581

BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.0174 0.0581

CHRYSENE 9.2 1 ND U 0.0174 0.0581

DIBENZ(a,h)ANTHRACENE 0.0092 0.52 ND U 0.0174 0.0581

FLUORANTHENE 1500 130 ND U 0.0174 0.0581

FLUORENE 240 950 ND U 0.0174 0.0581

INDENO(1,2,3-c,d)PYRENE 0.092 0.095 ND U 0.0174 0.0581

NAPHTHALENE 17 21 0.0596 F 0.036 0.116

PHENANTHRENE 240 410 ND U 0.0174 0.0581

PYRENE 180 68 ND U 0.0174 0.0581

1,1,1,2-TETRACHLOROETHANE 0.52 50000 ND U 0.15 0.5

1,1,1-TRICHLOROETHANE 200 970 ND U 0.31 1

1,1,2,2-TETRACHLOROETHANE 0.067 500 ND U 0.15 0.5

1,1,2-TRICHLOROETHANE 5 50000 ND U 0.31 1

1,1-DICHLOROETHANE 2.4 50000 ND U 0.31 1

1,2,3-TRICHLOROPROPANE (TCP) 0.6 50000 ND U 0.31 1

1,2,4-TRICHLOROBENZENE 70 3000 ND U 0.31 1

1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 0.04 10 ND U 0.62 2

1,2-DIBROMOETHANE (EDB) 0.0065 50000 ND U 0.31 1

1,2-DICHLOROBENZENE 600 10 ND U 0.31 1

1,2-DICHLOROETHANE 0.15 7000 ND U 0.15 0.5

1,2-DICHLOROPROPANE 5 10 ND U 0.31 1

1,3-DICHLOROBENZENE 180 50000 ND U 0.31 1

1,4-DICHLOROBENZENE 75 5 ND U 0.15 0.5

ACETONE 22000 20000 ND U 3.1 10

BENZENE 5 170 ND U 0.12 0.4

BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5

BROMOFORM 100 510 ND U 0.31 1

BROMOMETHANE 8.7 50000 ND U 0.94 3

CARBON TETRACHLORIDE 5 520 ND U 0.31 1

CHLOROBENZENE 100 50 ND U 0.15 0.5

CHLOROETHANE 8600 16 ND U 0.31 1

CHLOROFORM 70 2400 ND U 0.3 1

CHLOROMETHANE 1.8 50000 ND U 0.31 1

cis-1,2-DICHLOROETHYLENE 70 50000 ND U 0.31 1

cis-1,3-DICHLOROPROPENE 0.43 50000 ND U 0.15 0.5

DIBROMOCHLOROMETHANE 0.16 50000 ND U 0.15 0.5

ETHYLBENZENE 700 30 ND U 0.31 1

HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1

M,P-XYLENE (SUM OF ISOMERS) 10000 20 ND U 0.62 2

METHYL ETHYL KETONE (2-BUTANONE) 7100 8400 ND U 3.1 10

METHYL ISOBUTYL KETONE (4-METHYL-2-PENTANONE) 2000 1300 ND U 3.1 10

METHYLENE CHLORIDE 4.8 9100 ND U 1 5

NAPHTHALENE 17 21 ND U 0.62 2

STYRENE 100 10 ND U 0.31 1

TETRACHLOROETHYLENE(PCE) 5 170 ND U 0.31 1

TOLUENE 1000 40 ND U 0.31 1

trans-1,2-DICHLOROETHENE 100 260 ND U 0.31 1

TRICHLOROETHYLENE (TCE) 5 310 ND U 0.31 1

VINYL CHLORIDE 2 3400 ND U 0.31 1

XYLENES, TOTAL 10000 20 ND U 0.94 3

6020 LEAD 15 50000 ND U 0.31 1

PAHs - Polynuclear aromatic hydrocarbons

VOCs - Volatile organic compounds

UG/L - Micrograms per Liter

Q - Data qualifier

U - Indicates that the compound was analyzed for but not detected at or above the stated limit

MDL - Method detection limit

RL - Reporting limit

TPH - Total petroleum hydrocarbons 

ND - Indicates that the compound was not detected above the stated method detection limit

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EALs

1

2

HDMW2253-03

UG/L

8015B (Petroleum)

8270C SIM 

(PAHs)

8260B 

(VOCs)

Final Drinking Water Action Levels for Human Toxicity, Table D-3a, Screening for Environmental Concerns at Sites 

with Contaminated Soil and Groundwater, HDOH, 2009

Groundwater Gross Contamination Action Levels, Table G-1, Screening for Environmental Concerns at Sites with 

Contaminated Soil and Groundwater, HDOH, 2009

July 8, 2010 Method

HDOH Drinking Water 

EALs1

for Human Toxicity 

UG/L

HDOH Groundwater 

Gross Contamination 

EALs2

UG/L

Chemical

200
9 

4.0 Summary and Conclusions 

Summary

In HDMW2253-03, trace naphthalene was detected at 0.0596F μg/L. This concentration is 

below the HDOH Drinking Water EAL, and the HDOH Gross Contamination EAL. No other 

potential chemicals of concern were detected above the laboratory MDLs in HDMW2253-03 

during the July 2010 sampling event. 

This is the first time naphthalene was detected at HDMW2253-03 during the four quarterly 

sampling events. Previously, only TPH-DRO has been detected at HDMW2253-03 and 

OWDFMW01. TPH-DRO has not been detected above the laboratory MDL in HDMW2253-03 

since January 2010. Figure 2 summarizes TPH results for three wells outside of the Facility 

during all four quarterly sampling events. 

Conclusions/Recommendations

No compounds were detected above the MDLs during the August 2009 sampling event at 

OWDFMW01 and RHMW04 (HDMW2253-03 was not sampled in August 2009 due to access 

issues); or during the October 2009 sampling event at OWDFMW01, RHMW04, or 

HDMW2253-03. 

Despite the detection of TPH-DRO at HDMW2253-03 during January 2010, TPH-DRO was not 

detected above the laboratory MDL during the April 2010 and July 2010 sampling events. Since 

two or more consecutive sampling events of increasing (or decreasing) concentrations of TPHDRO at HDMW2253-03 have not occurred, no trend for TPH-DRO has been established at this 

location. 

TPH-DRO detected at OWDFMW01 during January 2010 significantly decreased in April 2010 

(i.e., from 1,490 μg/L in January 2010 to 288F μg/L in April 2010). 

 

TPH-DRO (detected at both HDMW2253-03 and OWDFMW01 in January 2010 and only at 

OWDFMW01 in April 2010) has been the only parameter detected above HDOH Drinking 

Water EALs during all four outside well sampling rounds. For the three wells surrounding the 

Facility (i.e., RHMW04, OWDFMW01, and HDMW2253-03), no more sampling event remains 

tasked under Contract Number N47408-04-D-8514, Task Order No. 54, Modification No. 01. 

Consequently, consideration should be given to conducting follow-on, periodic (perhaps semiannually), targeted monitoring of these outside wells for TPH-DRO. 

RHMW04 (ug/L)

Compound

August 4, 2009 October 13, 2009 January 26, 2010 

Result Q MDL RL Result Q MDL RL Result Q MDL R

TPH-DRO ND U 157 419 ND U 169 452 ND U 167 44

TPH-GRO ND U 30 100 ND U 30 100 ND U 30 10

HDMW2253-03 (ug/L)

Compound

October 13, 2009 January 26, 2010 April 26, 2010 July 8, 2010

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL

TPH-DRO ND U 185 494 322 F 172 460 ND U 176 471 ND U 160 426

TPH-GRO ND U 30 100 ND U 30 100 ND U 30 100 ND U 30 100

TPH-GRO ND U 30 100 ND U 30 100 ND U 30 10

RHMW04D (ug/L)

Compound

August 4, 2009 October 13, 2009 January 26, 2010 

Result Q MDL RL Result Q MDL RL Result Q MDL R

TPH-DRO ND U 161 430 ND U 174 465 ND U 165 44

OWDFMW01 (ug/L)

TPH-GRO ND U 30 100 ND U 30 100 ND U 30 100 ND U 30 100 TPH-GRO ND U 30 100 ND U 30 100 ND U 30 10

Compound

August 4, 2009 October 13, 2009 January 26, 2010 April 26, 2010

Result Q MDL RL Result Q MDL RL Result Q MDL RL Result Q MDL RL

TPH-DRO ND U 171 457 ND U 167 444 1490 165 440 288 F 176 471

TPH-GRO ND U 30 100 ND U 30 100 ND U 30 100 ND U 30 100

Notes:F - Estimated result betwDRO - Diesel Range OrgGRO - Gasoline Range OMDL - Method Detection ND - Not DetectedQ - Data QualifierRL - Reporting LimitTPH - Total Petroleum HyU - Result not detectedug/L - Micrograms per lite

200 200 - Result exceeded on

•TPH-DRO Residential Tap •TPH-GRO Residential Ta(HDOH, 2008).
12 

5.0 References 

AMEC. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Earth Tech, Inc. Remedial Investigation Phase II, Volume I, Technical Report, Red Hill Oily 

Waste Disposal Facility, Halawa, Oahu, Hawaii. September 2000. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

HDOH. Screening for Environmental Concerns at Sites with Contaminated Soil and 

Groundwater, Summary Lookup Tables. March 2009. 

HDOH. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underground 

Storage Tank Sites. Memo. July 2005. 

HDOH. Evaluation of Environmental Hazards at Sites with Contaminated Soil and 

Groundwater. Summer 2008 (updated October 2008). 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, Pearl 

Harbor, Hawaii. May 2006. 

TEC, Inc. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January 2008 revised in December 2009. 
Appendix A 

Laboratory Analytical Reports 
SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1103364

1 of 43
CASE NARRATIVE Print Date: 7/30/2010

Workorder No.: 1103364

Project Name: 3354-003 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

1103364001

8270D SIM – The corrected CCV recovery for naphthalene does not meet QC criteria (biased high). The results for this 

analyte may be estimated in the associated samples.

8270D SIM Corrected Report - Results for this analysis are being resubmitted based on a correction to the initial calibration.

PS HDMW2253-03-WG-05

972723

8270D SIM - LCSD recovery for napthalene is outside of QC criteria (biased high). The results for this analyte may be 

estimated in the associated samples.

8270D SIM - LCS/LCSD RPD for napthalene is outside of QC criteria (biased high). The results for this analyte may be 

estimated in the associated samples.

* LCSD LCSD for HBN 515780 [XXX/23016

973529

8260B - LCS recovery for acetone does not meet QC criteria (biased high). This analyte was not detected above the LOQ in 

the associated samples.

* LCS LCS for HBN 533980 [VXX/20930]

973530

8260B - LCSD recovery for acetone and 2-hexanone does not meet QC criteria (biased high). These analytes were not 

detected above the LOQ in the associated samples.

8260B - LCS/LCSD RPD for acetone does not meet QC criteria. This analyte was not detected above the LOQ in the 

associated samples.

* LCSD LCSD for HBN 533980 [VXX/20930

973543

8260B - CCV recovery for several analytes does not meet QC criteria (biased high). These analytes were not detected 

above the LOQ in the associated samples.

* CCV CCV for HBN 534280 [VMS/11383]

976463

8270D SIM – The corrected CCV recovery for naphthalene does not meet QC criteria (biased high). The results for this 

analyte may be estimated in the associated samples.

* CCV CCV for HBN 599080 [XMS/5543]

* QC comments may be associated with the field samples found in this report. When applicable, comments will be applied to

 associated field samples.

SG S N o rth A m eric a Inc . En vir onm enta l D ivision 200 W e st Potter D rive A nc hora ge A K 99518 t(907 )562.2343 f( 907)561 .5301 w w w .us.sgs.com M em ber of SG S Group

2 of 43
Report of Manual Integrations Print Date: 7/30/2010 4:34 pm

Laboratory ID Client Sample ID Analytical Batch Method Analyte Reason

972722 LCS for HBN 515780 [XXX/23016] XMS5511 8270D SIMS Benzo[k]fluoranthene RP

972723 LCSD for HBN 515780 [XXX/23016 XMS5511 8270D SIMS Benzo[k]fluoranthene RP

Manual Integration Reason Code Descriptions

Code Description

O Original Chromatogram

M Modified Chromatogram

SS Skimmed surrogate

BLG Closed baseline gap

RP Reassign peak name

PIR Pattern integration required

IT Included tail

SP Split peak

RSP Removed split peak

FPS Forced peak start/stop

BLC Baseline correction

PNF Peak not found by software

All DRO/RRO analysis are integrated per SOP.

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

3 of 43
3354-003 Red Hill BFSF

Project Manager

jennifer.serna@sgs.com

Jennifer Serna

T: (808)528-1445 F:(808)528-0768

Attn: Rick Adkisson

1003 Bishop Street,

Pauahi Tower Suite 1550

Honolulu, HI 96813

Certification:

This data package is in compliance with the terms and conditions of the contract, both 

technically and for completeness, unless otherwise noted on the sample data sheet(s) and/or 

case narrative. This certification applies only to the tested parameters and the specific 

sample(s) received at the laboratory. If you have any questions regarding this report, or if we 

can be of further assistance, please contact your SGS Project Manager.

1103364

The Environmental Company, Inc. (TEC)

Workorder No.:

Client:

Project:

Laboratory Analytical Report

Contents (Bookmarked in PDF):

Cover Page

Glossary

Sample Summary Forms

Case Narrative

Sample Results Forms

Batch Summary Forms (by method)

Quality Control Summary Forms (by method)

Chain of Custody/Sample Receipt Forms

Attachments (if applicable)

SGS No rth Americ a Inc . En vir onmenta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com Member of SG S Group

4 of 43
Enclosed are the analytical results associated with the above work order. All results are intended to be used in their entirety and SGS is not 

responsible for use of less than the complete report. If you have any questions regarding this report, or if we can be of any other assistance, please 

contact your SGS Project Manager at 907-562-2343. All work is provided under SGS general terms and conditions 

(<http://www.sgs.com/terms_and_conditions.htm>), unless other written agreements have been accepted by both parties.

SGS maintains a formal Quality Assurance/Quality Control (QA/QC) program. A copy of our Quality Assurance Plan (QAP), which outlines this 

program, is available at your request. The laboratory certification numbers are AK00971 (DW Chemistry & Microbiology) & UST-005 (CS) for 

ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 3010A, 3050B, 3520C, 3550C, 5030B, 5035B, 6010B, 6020, 7470A, 7471B, 

8021B, 8081B, 8082A, 8260B, 8270D, 8270D-SIM, 9040B, 9045C, 9056A, 9060A, AK101 and AK102/103). Except as specifically noted, all 

statements and data in this report are in conformance to the provisions set forth by the SGS QAP and, when applicable, the National Environmental 

Laboratory Accreditation Program and other regulatory authorities. The following descriptors or qualifiers may be found in your report:

* The analyte has exceeded allowable regulatory or control limits.

! Surrogate out of control limits.

B Indicates the analyte is found in a blank associated with the sample.

CCV Continuing Calibration Verification

CL Control Limit

D The analyte concentration is the result of a dilution.

DF Dilution Factor

DL Detection Limit (i.e., maximum method detection limit)

E The analyte result is above the calibrated range.

F Indicates value that is greater than or equal to the DL

GT Greater Than

ICV Initial Calibration Verification

J The quantitation is an estimation.

JL The analyte was positively identified, but the quantitation is a low estimation.

LCS(D) Laboratory Control Spike (Duplicate)

LOD Limit of Detection (i.e., 2xDL)

LOQ Limit of Quantitation (i.e., reporting or practical quantitation limit)

LT Less Than

M A matrix effect was present.

MB Method Blank

MS(D) Matrix Spike (Duplicate)

ND Indicates the analyte is not detected.

Q QC parameter out of acceptance range.

R Rejected

RL Reporting Limit

RPD Relative Percent Difference

U Indicates the analyte was analyzed for but not detected.

Note: Sample summaries which include a result for "Total Solids" have already been adjusted for moisture content.

All DRO/RRO analyses are integrated per SOP.

Print Date: 7/30/2010

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

5 of 43
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-003 Red Hill BFSF

Workorder No.: 1103364

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015C (W) SW8015C

GRO (W) SW8015C

Print Date: 7/30/2010 4:34 pm

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1103364001 HDMW2253-03-WG-05

1103364002 TB01-WG-05

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

6 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

DL DF

Lead 0.620 U 1.00 0.310 ug/L 5 MMS6543 MXX23243

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6543

Analytical Method: SW6020

Analysis Date/Time: 07/21/10 19:48

Prep Batch: MXX23243

Prep Method: SW3010A

Prep Date/Time: 07/16/10 18:10 Container ID:1103364001-G

Dilution Factor: 5 Analyst: KDC

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

7 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10031 VXX20961

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC10031 VXX20961

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10031

Analytical Method: SW8015C

Analysis Date/Time: 07/20/10 15:09

Prep Batch: VXX20961

Prep Method: SW5030B

Prep Date/Time: 07/20/10 12:00 Container ID:1103364001-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

8 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

DL DF

Diesel Range Organics 0.320 U 0.426 0.160 mg/L 1 XFC9357 XXX23023

5a Androstane <surr> 83.7 50-150 % 1 XFC9357 XXX23023

Batch Information

Initial Prep Wt./Vol.: 940 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC9357

Analytical Method: SW8015C

Analysis Date/Time: 07/20/10 05:12

Prep Batch: XXX23023

Prep Method: SW3520C

Prep Date/Time: 07/13/10 10:10 Container ID:1103364001-K

Dilution Factor: 1 Analyst: LCE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

9 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11383 VXX20930

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11383 VXX20930

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11383 VXX20930

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11383 VXX20930

Acetone 6.20 U 10.0 3.10 ug/L 1 VMS11383 VXX20930

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11383 VXX20930

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11383 VXX20930

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

10 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11383 VXX20930

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11383 VXX20930

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11383 VXX20930

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11383 VXX20930

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11383 VXX20930

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11383 VXX20930

1,2-Dichloroethane-D4 <surr> 104 73-120 % 1 VMS11383 VXX20930

4-Bromofluorobenzene <surr> 109 76-120 % 1 VMS11383 VXX20930

Toluene-d8 <surr> 97 80-120 % 1 VMS11383 VXX20930

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

11 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11383

Analytical Method: SW8260B

Analysis Date/Time: 07/14/10 14:40

Prep Batch: VXX20930

Prep Method: SW5030B

Prep Date/Time: 07/13/10 11:31 Container ID:1103364001-A

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

12 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: HDMW2253-03-WG-05

SGS Ref. #: 1103364001 Collection Date/Time: 07/08/10 10:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

DL DF

1-Methylnaphthalene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

2-Methylnaphthalene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Acenaphthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Acenaphthylene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Anthracene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Benzo(a)Anthracene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Benzo[a]pyrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Benzo[b]Fluoranthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Benzo[g,h,i]perylene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Benzo[k]fluoranthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Chrysene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Dibenzo[a,h]anthracene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Fluoranthene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Fluorene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Indeno[1,2,3-c,d] pyrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Naphthalene 0.0596J 0.116 0.0360 ug/L 1 XMS5543 XXX23016

Phenanthrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Pyrene 0.0348 U 0.0581 0.0174 ug/L 1 XMS5543 XXX23016

Terphenyl-d14 <surr> 118 50-135 % 1 XMS5543 XXX23016

Batch Information

Initial Prep Wt./Vol.: 860 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5543

Analytical Method: 8270D SIMS

Analysis Date/Time: 07/13/10 15:37

Prep Batch: XXX23016

Prep Method: SW3520C

Prep Date/Time: 07/12/10 11:00 Container ID:1103364001-H

Dilution Factor: 1 Analyst: CDE

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

13 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: TB01-WG-05

SGS Ref. #: 1103364002 Collection Date/Time: 07/08/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Fuels Department

DL DF

Gasoline Range Organics 60.0 U 100 30.0 ug/L 1 VFC10031 VXX20961

4-Bromofluorobenzene <surr> 103 50-150 % 1 VFC10031 VXX20961

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC10031

Analytical Method: SW8015C

Analysis Date/Time: 07/20/10 15:48

Prep Batch: VXX20961

Prep Method: SW5030B

Prep Date/Time: 07/20/10 12:00 Container ID:1103364002-B

Dilution Factor: 1 Analyst: EAB

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

14 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: TB01-WG-05

SGS Ref. #: 1103364002 Collection Date/Time: 07/08/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 1 VMS11383 VXX20930

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 1 VMS11383 VXX20930

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 1 VMS11383 VXX20930

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 1 VMS11383 VXX20930

Acetone 3.43J 10.0 3.10 ug/L 1 VMS11383 VXX20930

Benzene 0.240 U 0.400 0.120 ug/L 1 VMS11383 VXX20930

Bromobenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Bromochloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

Bromoform 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Bromomethane 1.88 U 3.00 0.940 ug/L 1 VMS11383 VXX20930

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Chlorobenzene 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

15 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: TB01-WG-05

SGS Ref. #: 1103364002 Collection Date/Time: 07/08/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Chloroethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Chloroform 0.600 U 1.00 0.300 ug/L 1 VMS11383 VXX20930

Chloromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 1 VMS11383 VXX20930

Dibromomethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Ethylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Methylene chloride 2.00 U 5.00 1.00 ug/L 1 VMS11383 VXX20930

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 1 VMS11383 VXX20930

Naphthalene 1.24 U 2.00 0.620 ug/L 1 VMS11383 VXX20930

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

o-Xylene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

P & M -Xylene 1.24 U 2.00 0.620 ug/L 1 VMS11383 VXX20930

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Styrene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Toluene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Trichloroethene 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Vinyl chloride 0.620 U 1.00 0.310 ug/L 1 VMS11383 VXX20930

Xylenes (total) 1.88 U 3.00 0.940 ug/L 1 VMS11383 VXX20930

1,2-Dichloroethane-D4 <surr> 101 73-120 % 1 VMS11383 VXX20930

4-Bromofluorobenzene <surr> 107 76-120 % 1 VMS11383 VXX20930

Toluene-d8 <surr> 98.6 80-120 % 1 VMS11383 VXX20930

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

16 of 43
The Environmental Company, Inc. (TEC) Print Date: 7/30/2010 4:34 pm

Client Sample ID: TB01-WG-05

SGS Ref. #: 1103364002 Collection Date/Time: 07/08/10 08:05

Project ID: 3354-003 Red Hill BFSF Receipt Date/Time: 07/09/10 11:30

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result LOQ/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

DL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS11383

Analytical Method: SW8260B

Analysis Date/Time: 07/14/10 13:47

Prep Batch: VXX20930

Prep Method: SW5030B

Prep Date/Time: 07/13/10 11:31 Container ID:1103364002-A

Dilution Factor: 1 Analyst: SCL

SGS No rth Am eric a Inc . En vir onm enta l Division 200 W e st Potter D rive Anc hora ge AK 99518 t(907 )562.2343 f( 907)561 .5301 w ww.us.sgs.com M ember of SG S Group

17 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972721 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23016

SW3520C

07/12/2010

QC results affect the following production samples:

1103364001

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

1-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

2-Methylnaphthalene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Acenaphthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Acenaphthylene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Anthracene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo(a)Anthracene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[a]pyrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[b]Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[g,h,i]perylene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Benzo[k]fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Chrysene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Dibenzo[a,h]anthracene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Fluoranthene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Fluorene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Indeno[1,2,3-c,d] pyrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 07/13/10

Naphthalene 0.0620 U 0.100 0.0310 ug/L 07/13/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Phenanthrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

Pyrene 0.0300 U 0.0500 0.0150 ug/L 07/13/10

18 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972721 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23016

SW3520C

07/12/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Polynuclear Aromatics GC/MS

Surrogates 

Terphenyl-d14 <surr> 120 50-135 % 07/13/10

Terphenyl-d14 <surr> 114 50-135 % 07/13/10

Instrument

Method

Batch XMS5543

8270D SIMS

HP 6890/5973 MS SVQA

19 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972948 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23023

SW3520C

07/13/2010

QC results affect the following production samples:

1103364001

Parameter Results LOQ/CL Units

Analysis

DL Date

Semivolatile Organic Fuels Department

Diesel Range Organics 0.300 U 0.400 0.150 mg/L 07/20/10

Surrogates 

5a Androstane <surr> 83.6 60-120 % 07/20/10

Instrument

Method

Batch XFC9357

SW8015C

HP 7890A FID SV E R

20 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973528 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

QC results affect the following production samples:

1103364001, 1103364002

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

21 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973528 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 07/14/10

1,1,1-Trichloroethane 0.620 U 1.00 0.310 ug/L 07/14/10

1,1,2,2-Tetrachloroethane 0.300 U 0.500 0.150 ug/L 07/14/10

1,1,2-Trichloroethane 0.620 U 1.00 0.310 ug/L 07/14/10

1,1-Dichloroethane 0.620 U 1.00 0.310 ug/L 07/14/10

1,1-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/14/10

1,1-Dichloropropene 0.620 U 1.00 0.310 ug/L 07/14/10

1,2,3-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 07/14/10

1,2,3-Trichloropropane 0.620 U 1.00 0.310 ug/L 07/14/10

1,2,4-Trichlorobenzene 0.620 U 1.00 0.310 ug/L 07/14/10

1,2,4-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

1,2-Dibromo-3-chloropropane 1.24 U 2.00 0.620 ug/L 07/14/10

1,2-Dibromoethane 0.620 U 1.00 0.310 ug/L 07/14/10

1,2-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 07/14/10

1,2-Dichloroethane 0.300 U 0.500 0.150 ug/L 07/14/10

1,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 07/14/10

1,3,5-Trimethylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

1,3-Dichlorobenzene 0.620 U 1.00 0.310 ug/L 07/14/10

1,3-Dichloropropane 0.240 U 0.400 0.120 ug/L 07/14/10

1,4-Dichlorobenzene 0.300 U 0.500 0.150 ug/L 07/14/10

1-Chlorohexane 0.620 U 1.00 0.310 ug/L 07/14/10

2,2-Dichloropropane 0.620 U 1.00 0.310 ug/L 07/14/10

2-Butanone (MEK) 6.20 U 10.0 3.10 ug/L 07/14/10

2-Chlorotoluene 0.620 U 1.00 0.310 ug/L 07/14/10

4-Chlorotoluene 0.620 U 1.00 0.310 ug/L 07/14/10

4-Isopropyltoluene 0.620 U 1.00 0.310 ug/L 07/14/10

4-Methyl-2-pentanone (MIBK) 6.20 U 10.0 3.10 ug/L 07/14/10

Acetone 6.20 U 10.0 3.10 ug/L 07/14/10

Benzene 0.240 U 0.400 0.120 ug/L 07/14/10

Bromobenzene 0.620 U 1.00 0.310 ug/L 07/14/10

Bromochloromethane 0.620 U 1.00 0.310 ug/L 07/14/10

Bromodichloromethane 0.300 U 0.500 0.150 ug/L 07/14/10

Bromoform 0.620 U 1.00 0.310 ug/L 07/14/10

Bromomethane 1.88 U 3.00 0.940 ug/L 07/14/10

Carbon tetrachloride 0.620 U 1.00 0.310 ug/L 07/14/10

Chlorobenzene 0.300 U 0.500 0.150 ug/L 07/14/10

Chloroethane 0.620 U 1.00 0.310 ug/L 07/14/10

Chloroform 0.600 U 1.00 0.300 ug/L 07/14/10

Chloromethane 0.620 U 1.00 0.310 ug/L 07/14/10

22 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973528 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Gas Chromatography/Mass Spectroscopy

cis-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/14/10

cis-1,3-Dichloropropene 0.300 U 0.500 0.150 ug/L 07/14/10

Dibromochloromethane 0.300 U 0.500 0.150 ug/L 07/14/10

Dibromomethane 0.620 U 1.00 0.310 ug/L 07/14/10

Dichlorodifluoromethane 0.620 U 1.00 0.310 ug/L 07/14/10

Ethylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

Hexachlorobutadiene 0.620 U 1.00 0.310 ug/L 07/14/10

Isopropylbenzene (Cumene) 0.620 U 1.00 0.310 ug/L 07/14/10

Methylene chloride 2.00 U 5.00 1.00 ug/L 07/14/10

Methyl-t-butyl ether 3.00 U 5.00 1.50 ug/L 07/14/10

Naphthalene 1.24 U 2.00 0.620 ug/L 07/14/10

n-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

n-Propylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

o-Xylene 0.620 U 1.00 0.310 ug/L 07/14/10

P & M -Xylene 1.24 U 2.00 0.620 ug/L 07/14/10

sec-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

Styrene 0.620 U 1.00 0.310 ug/L 07/14/10

tert-Butylbenzene 0.620 U 1.00 0.310 ug/L 07/14/10

Tetrachloroethene 0.620 U 1.00 0.310 ug/L 07/14/10

Toluene 0.620 U 1.00 0.310 ug/L 07/14/10

trans-1,2-Dichloroethene 0.620 U 1.00 0.310 ug/L 07/14/10

trans-1,3-Dichloropropene 0.620 U 1.00 0.310 ug/L 07/14/10

Trichloroethene 0.620 U 1.00 0.310 ug/L 07/14/10

Trichlorofluoromethane 0.620 U 1.00 0.310 ug/L 07/14/10

Vinyl chloride 0.620 U 1.00 0.310 ug/L 07/14/10

Xylenes (total) 1.88 U 3.00 0.940 ug/L 07/14/10

Surrogates 

1,2-Dichloroethane-D4 <surr> 101 73-120 % 07/14/10

4-Bromofluorobenzene <surr> 109 76-120 % 07/14/10

Toluene-d8 <surr> 99.7 80-120 % 07/14/10

Instrument

Method

Batch VMS11383

SW8260B

HP 5890 Series II MS1 VJA

23 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

974420 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX23243

SW3010A

07/16/2010

QC results affect the following production samples:

1103364001

Parameter Results LOQ/CL Units

Analysis

DL Date

Metals by ICP/MS

Lead 0.620 U 1.00 0.310 ug/L 07/21/10

Instrument

Method

Batch MMS6543

SW6020

Perkin Elmer Sciex ICP-MS P3

24 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

975014 Method Blank

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20961

SW5030B

07/20/2010

QC results affect the following production samples:

1103364001, 1103364002

Parameter Results LOQ/CL Units

Analysis

DL Date

Volatile Fuels Department

Gasoline Range Organics 60.0 U 100 30.0 ug/L 07/20/10

Surrogates 

4-Bromofluorobenzene <surr> 106 50-150 % 07/20/10

Instrument

Method

Batch VFC10031

SW8015C

HP 5890 Series II PID+FID VCA

25 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972722 Lab Control Sample

972723 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23016

SW3520C

07/12/2010

QC results affect the following production samples:

1103364001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

1-Methylnaphthalene LCS 0.372 74 ( 58-114 ) 0.5 ug/L 07/13/2010

LCSD 0.475 95 24 (< 30 ) 0.5 ug/L 07/13/2010

1-Methylnaphthalene LCS 0.433 87 ( 58-114 ) 0.5 ug/L 07/13/2010

LCSD

2-Methylnaphthalene LCS 0.348 70 ( 54-105 ) 0.5 ug/L 07/13/2010

LCSD 0.408 82 16 (< 30 ) 0.5 ug/L 07/13/2010

2-Methylnaphthalene LCS 0.395 79 ( 54-105 ) 0.5 ug/L 07/13/2010

LCSD

Acenaphthene LCS 0.373 75 ( 57-110 ) 0.5 ug/L 07/13/2010

LCSD

Acenaphthene LCS 0.373 75 ( 57-110 ) 0.5 ug/L 07/13/2010

LCSD 0.395 79 6 (< 30 ) 0.5 ug/L 07/13/2010

Acenaphthylene LCS 0.398 80 ( 58-105 ) 0.5 ug/L 07/13/2010

LCSD

Acenaphthylene LCS 0.385 77 ( 58-105 ) 0.5 ug/L 07/13/2010

LCSD 0.411 82 6 (< 30 ) 0.5 ug/L 07/13/2010

Anthracene LCS 0.375 75 ( 63-120 ) 0.5 ug/L 07/13/2010

LCSD

Anthracene LCS 0.369 74 ( 63-120 ) 0.5 ug/L 07/13/2010

LCSD 0.399 80 8 (< 30 ) 0.5 ug/L 07/13/2010

Benzo(a)Anthracene LCS 0.405 81 ( 61-120 ) 0.5 ug/L 07/13/2010

LCSD 0.455 91 12 (< 30 ) 0.5 ug/L 07/13/2010

Benzo(a)Anthracene LCS 0.456 91 ( 61-120 ) 0.5 ug/L 07/13/2010

LCSD

Benzo[a]pyrene LCS 0.350 70 ( 57-120 ) 0.5 ug/L 07/13/2010

LCSD 0.380 76 8 (< 30 ) 0.5 ug/L 07/13/2010

26 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972722 Lab Control Sample

972723 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23016

SW3520C

07/12/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Benzo[a]pyrene LCS 0.378 76 ( 57-120 ) 0.5 ug/L 07/13/2010

LCSD

Benzo[b]Fluoranthene LCS 0.404 81 ( 66-130 ) 0.5 ug/L 07/13/2010

LCSD 0.454 91 12 (< 30 ) 0.5 ug/L 07/13/2010

Benzo[b]Fluoranthene LCS 0.447 89 ( 66-130 ) 0.5 ug/L 07/13/2010

LCSD

Benzo[g,h,i]perylene LCS 0.393 79 ( 60-125 ) 0.5 ug/L 07/13/2010

LCSD 0.442 89 12 (< 30 ) 0.5 ug/L 07/13/2010

Benzo[g,h,i]perylene LCS 0.443 89 ( 60-125 ) 0.5 ug/L 07/13/2010

LCSD

Benzo[k]fluoranthene LCS 0.404 81 ( 67-125 ) 0.5 ug/L 07/13/2010

LCSD

Benzo[k]fluoranthene LCS 0.396 79 ( 67-125 ) 0.5 ug/L 07/13/2010

LCSD 0.380 76 4 (< 30 ) 0.5 ug/L 07/13/2010

Chrysene LCS 0.397 79 ( 71-120 ) 0.5 ug/L 07/13/2010

LCSD 0.414 83 4 (< 30 ) 0.5 ug/L 07/13/2010

Chrysene LCS 0.415 83 ( 71-120 ) 0.5 ug/L 07/13/2010

LCSD

Dibenzo[a,h]anthracene LCS 0.387 78 ( 56-125 ) 0.5 ug/L 07/13/2010

LCSD 0.419 84 8 (< 30 ) 0.5 ug/L 07/13/2010

Dibenzo[a,h]anthracene LCS 0.424 85 ( 56-125 ) 0.5 ug/L 07/13/2010

LCSD

Fluoranthene LCS 0.416 83 ( 63-125 ) 0.5 ug/L 07/13/2010

LCSD 0.465 93 11 (< 30 ) 0.5 ug/L 07/13/2010

Fluoranthene LCS 0.454 91 ( 63-125 ) 0.5 ug/L 07/13/2010

LCSD

Fluorene LCS 0.415 83 ( 59-120 ) 0.5 ug/L 07/13/2010

LCSD

27 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972722 Lab Control Sample

972723 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23016

SW3520C

07/12/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Fluorene LCS 0.408 82 ( 59-120 ) 0.5 ug/L 07/13/2010

LCSD 0.422 84 4 (< 30 ) 0.5 ug/L 07/13/2010

Indeno[1,2,3-c,d] pyrene LCS 0.393 79 ( 59-125 ) 0.5 ug/L 07/13/2010

LCSD 0.435 87 10 (< 30 ) 0.5 ug/L 07/13/2010

Indeno[1,2,3-c,d] pyrene LCS 0.431 86 ( 59-125 ) 0.5 ug/L 07/13/2010

LCSD

Naphthalene LCS 0.376 75 ( 56-108 ) 0.5 ug/L 07/13/2010

LCSD 0.546 109 * 37 (< 30 ) 0.5 ug/L 07/13/2010 *

Naphthalene LCS 0.502 100 ( 56-108 ) 0.5 ug/L 07/13/2010

LCSD

Phenanthrene LCS 0.412 83 ( 60-115 ) 0.5 ug/L 07/13/2010

LCSD 0.457 91 10 (< 30 ) 0.5 ug/L 07/13/2010

Phenanthrene LCS 0.427 85 ( 60-115 ) 0.5 ug/L 07/13/2010

LCSD

Pyrene LCS 0.380 76 ( 62-130 ) 0.5 ug/L 07/13/2010

LCSD 0.400 80 5 (< 30 ) 0.5 ug/L 07/13/2010

Pyrene LCS 0.391 78 ( 62-130 ) 0.5 ug/L 07/13/2010

LCSD

Surrogates 

Terphenyl-d14 <surr> LCS 115 ( 50-135 ) 07/13/2010

LCSD 105 9 07/13/2010

Terphenyl-d14 <surr> LCS 109 ( 50-135 ) 07/13/2010

LCSD

Batch

Method

Instrument

XMS5543

8270D SIMS

HP 6890/5973 MS SVQA

28 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

972950 Lab Control Sample

972952 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX23023

SW3520C

07/13/2010

QC results affect the following production samples:

1103364001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.60 92 ( 75-125 ) 5 mg/L 07/20/2010

LCSD 4.80 96 4 (< 20 ) 5 mg/L 07/20/2010

Surrogates 

5a Androstane <surr> LCS 86 ( 60-120 ) 07/20/2010

LCSD 88 3 07/20/2010

Batch

Method

Instrument

XFC9357

SW8015C

HP 7890A FID SV E R

29 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

QC results affect the following production samples:

1103364001, 1103364002

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

30 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,1,1,2-Tetrachloroethane LCS 30.1 100 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 29.2 97 3 (< 20 ) 30 ug/L 07/14/2010

1,1,1-Trichloroethane LCS 30.7 102 ( 80-122 ) 30 ug/L 07/14/2010

LCSD 31.3 104 2 (< 20 ) 30 ug/L 07/14/2010

1,1,2,2-Tetrachloroethane LCS 31.7 106 ( 76-123 ) 30 ug/L 07/14/2010

LCSD 31.3 104 1 (< 20 ) 30 ug/L 07/14/2010

1,1,2-Trichloroethane LCS 33.5 112 ( 77-120 ) 30 ug/L 07/14/2010

LCSD 31.2 104 7 (< 20 ) 30 ug/L 07/14/2010

1,1-Dichloroethane LCS 29.6 99 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.5 102 3 (< 20 ) 30 ug/L 07/14/2010

1,1-Dichloroethene LCS 27.8 93 ( 76-130 ) 30 ug/L 07/14/2010

LCSD 28.6 96 3 (< 20 ) 30 ug/L 07/14/2010

1,1-Dichloropropene LCS 30.4 101 ( 80-122 ) 30 ug/L 07/14/2010

LCSD 30.5 102 0 (< 20 ) 30 ug/L 07/14/2010

1,2,3-Trichlorobenzene LCS 30.9 103 ( 77-120 ) 30 ug/L 07/14/2010

LCSD 31.1 104 1 (< 20 ) 30 ug/L 07/14/2010

1,2,3-Trichloropropane LCS 31.9 106 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 32.1 107 1 (< 20 ) 30 ug/L 07/14/2010

1,2,4-Trichlorobenzene LCS 33.6 112 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 34.0 113 1 (< 20 ) 30 ug/L 07/14/2010

1,2,4-Trimethylbenzene LCS 31.6 105 ( 80-125 ) 30 ug/L 07/14/2010

LCSD 31.5 105 0 (< 20 ) 30 ug/L 07/14/2010

1,2-Dibromo-3-chloropropane LCS 32.9 110 ( 73-130 ) 30 ug/L 07/14/2010

LCSD 34.0 113 3 (< 20 ) 30 ug/L 07/14/2010

1,2-Dibromoethane LCS 32.3 108 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 31.6 105 2 (< 20 ) 30 ug/L 07/14/2010

1,2-Dichlorobenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.4 101 1 (< 20 ) 30 ug/L 07/14/2010

31 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichloroethane LCS 29.8 99 ( 80-129 ) 30 ug/L 07/14/2010

LCSD 30.6 102 3 (< 20 ) 30 ug/L 07/14/2010

1,2-Dichloropropane LCS 30.7 102 ( 80-121 ) 30 ug/L 07/14/2010

LCSD 31.7 106 3 (< 20 ) 30 ug/L 07/14/2010

1,3,5-Trimethylbenzene LCS 31.7 106 ( 80-128 ) 30 ug/L 07/14/2010

LCSD 31.1 104 2 (< 20 ) 30 ug/L 07/14/2010

1,3-Dichlorobenzene LCS 30.7 102 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.2 101 2 (< 20 ) 30 ug/L 07/14/2010

1,3-Dichloropropane LCS 32.4 108 ( 80-121 ) 30 ug/L 07/14/2010

LCSD 31.1 104 4 (< 20 ) 30 ug/L 07/14/2010

1,4-Dichlorobenzene LCS 31.0 103 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 31.0 103 0 (< 20 ) 30 ug/L 07/14/2010

1-Chlorohexane LCS 50.4 112 ( 70-125 ) 45 ug/L 07/14/2010

LCSD 47.0 104 7 (< 20 ) 45 ug/L 07/14/2010

2,2-Dichloropropane LCS 34.0 113 ( 80-132 ) 30 ug/L 07/14/2010

LCSD 34.5 115 1 (< 20 ) 30 ug/L 07/14/2010

2-Butanone (MEK) LCS 108 120 ( 66-136 ) 90 ug/L 07/14/2010

LCSD 121 135 12 (< 20 ) 90 ug/L 07/14/2010

2-Chlorotoluene LCS 30.6 102 ( 80-125 ) 30 ug/L 07/14/2010

LCSD 30.5 102 0 (< 20 ) 30 ug/L 07/14/2010

4-Chlorotoluene LCS 31.2 104 ( 79-128 ) 30 ug/L 07/14/2010

LCSD 30.9 103 1 (< 20 ) 30 ug/L 07/14/2010

4-Isopropyltoluene LCS 31.5 105 ( 80-125 ) 30 ug/L 07/14/2010

LCSD 31.3 104 1 (< 20 ) 30 ug/L 07/14/2010

4-Methyl-2-pentanone (MIBK) LCS 92.1 102 ( 69-134 ) 90 ug/L 07/14/2010

LCSD 95.8 106 4 (< 20 ) 90 ug/L 07/14/2010

Acetone LCS 136 151 ( 50-135 ) * 90 ug/L 07/14/2010

32 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 167 186 * 21 (< 20 ) 90 ug/L 07/14/2010 *

Benzene LCS 29.3 98 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 29.7 99 1 (< 20 ) 30 ug/L 07/14/2010

Bromobenzene LCS 30.7 102 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 29.6 99 4 (< 20 ) 30 ug/L 07/14/2010

Bromochloromethane LCS 28.7 96 ( 77-129 ) 30 ug/L 07/14/2010

LCSD 30.2 101 5 (< 20 ) 30 ug/L 07/14/2010

Bromodichloromethane LCS 29.7 99 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.6 102 3 (< 20 ) 30 ug/L 07/14/2010

Bromoform LCS 30.9 103 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 29.8 99 4 (< 20 ) 30 ug/L 07/14/2010

Bromomethane LCS 27.1 90 ( 30-140 ) 30 ug/L 07/14/2010

LCSD 29.7 99 9 (< 20 ) 30 ug/L 07/14/2010

Carbon tetrachloride LCS 30.1 100 ( 80-126 ) 30 ug/L 07/14/2010

LCSD 30.2 101 0 (< 20 ) 30 ug/L 07/14/2010

Chlorobenzene LCS 31.0 103 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 29.5 98 5 (< 20 ) 30 ug/L 07/14/2010

Chloroethane LCS 33.3 111 ( 67-133 ) 30 ug/L 07/14/2010

LCSD 32.0 107 4 (< 20 ) 30 ug/L 07/14/2010

Chloroform LCS 29.0 97 ( 80-124 ) 30 ug/L 07/14/2010

LCSD 29.7 99 2 (< 20 ) 30 ug/L 07/14/2010

Chloromethane LCS 30.6 102 ( 67-125 ) 30 ug/L 07/14/2010

LCSD 32.4 108 6 (< 20 ) 30 ug/L 07/14/2010

cis-1,2-Dichloroethene LCS 28.2 94 ( 80-125 ) 30 ug/L 07/14/2010

LCSD 29.4 98 4 (< 20 ) 30 ug/L 07/14/2010

cis-1,3-Dichloropropene LCS 31.2 104 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 32.2 107 3 (< 20 ) 30 ug/L 07/14/2010

33 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Dibromochloromethane LCS 31.0 103 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.2 101 3 (< 20 ) 30 ug/L 07/14/2010

Dibromomethane LCS 28.7 96 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 29.8 99 4 (< 20 ) 30 ug/L 07/14/2010

Dichlorodifluoromethane LCS 30.4 101 ( 62-153 ) 30 ug/L 07/14/2010

LCSD 30.9 103 2 (< 20 ) 30 ug/L 07/14/2010

Ethylbenzene LCS 31.8 106 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.0 100 6 (< 20 ) 30 ug/L 07/14/2010

Hexachlorobutadiene LCS 32.2 107 ( 77-125 ) 30 ug/L 07/14/2010

LCSD 31.9 106 1 (< 20 ) 30 ug/L 07/14/2010

Isopropylbenzene (Cumene) LCS 32.1 107 ( 80-121 ) 30 ug/L 07/14/2010

LCSD 30.5 102 5 (< 20 ) 30 ug/L 07/14/2010

Methylene chloride LCS 29.2 97 ( 63-131 ) 30 ug/L 07/14/2010

LCSD 30.6 102 5 (< 20 ) 30 ug/L 07/14/2010

Methyl-t-butyl ether LCS 45.0 100 ( 80-120 ) 45 ug/L 07/14/2010

LCSD 46.9 104 4 (< 20 ) 45 ug/L 07/14/2010

Naphthalene LCS 31.5 105 ( 75-120 ) 30 ug/L 07/14/2010

LCSD 31.2 104 1 (< 20 ) 30 ug/L 07/14/2010

n-Butylbenzene LCS 33.1 110 ( 80-124 ) 30 ug/L 07/14/2010

LCSD 32.7 109 1 (< 20 ) 30 ug/L 07/14/2010

n-Propylbenzene LCS 31.6 105 ( 80-129 ) 30 ug/L 07/14/2010

LCSD 31.2 104 1 (< 20 ) 30 ug/L 07/14/2010

o-Xylene LCS 31.6 105 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.1 100 5 (< 20 ) 30 ug/L 07/14/2010

P & M -Xylene LCS 62.9 105 ( 80-120 ) 60 ug/L 07/14/2010

LCSD 60.1 100 5 (< 20 ) 60 ug/L 07/14/2010

sec-Butylbenzene LCS 31.7 106 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 31.3 104 1 (< 20 ) 30 ug/L 07/14/2010

34 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 32.7 109 ( 80-120 ) 30 ug/L 07/14/2010

LCSD 30.9 103 6 (< 20 ) 30 ug/L 07/14/2010

tert-Butylbenzene LCS 31.3 104 ( 80-122 ) 30 ug/L 07/14/2010

LCSD 30.7 102 2 (< 20 ) 30 ug/L 07/14/2010

Tetrachloroethene LCS 30.8 103 ( 79-122 ) 30 ug/L 07/14/2010

LCSD 29.2 98 5 (< 20 ) 30 ug/L 07/14/2010

Toluene LCS 30.4 101 ( 77-120 ) 30 ug/L 07/14/2010

LCSD 29.2 97 4 (< 20 ) 30 ug/L 07/14/2010

trans-1,2-Dichloroethene LCS 28.1 94 ( 79-132 ) 30 ug/L 07/14/2010

LCSD 28.6 95 2 (< 20 ) 30 ug/L 07/14/2010

trans-1,3-Dichloropropene LCS 33.8 113 ( 80-124 ) 30 ug/L 07/14/2010

LCSD 33.2 111 2 (< 20 ) 30 ug/L 07/14/2010

Trichloroethene LCS 30.2 101 ( 80-125 ) 30 ug/L 07/14/2010

LCSD 30.8 103 2 (< 20 ) 30 ug/L 07/14/2010

Trichlorofluoromethane LCS 30.1 100 ( 68-145 ) 30 ug/L 07/14/2010

LCSD 30.9 103 3 (< 20 ) 30 ug/L 07/14/2010

Vinyl chloride LCS 28.5 95 ( 72-145 ) 30 ug/L 07/14/2010

LCSD 30.5 102 7 (< 20 ) 30 ug/L 07/14/2010

Xylenes (total) LCS 94.5 105 ( 80-120 ) 90 ug/L 07/14/2010

LCSD 90.1 100 5 (< 20 ) 90 ug/L 07/14/2010

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 07/14/2010

LCSD 102 3 07/14/2010

4-Bromofluorobenzene <surr> LCS 101 ( 76-120 ) 07/14/2010

LCSD 102 0 07/14/2010

Toluene-d8 <surr> LCS 101 ( 80-120 ) 07/14/2010

LCSD 98 3 07/14/2010

35 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

973529 Lab Control Sample

973530 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20930

SW5030B

07/13/2010

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS11383

SW8260B

HP 5890 Series II MS1 VJA

36 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

974421 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX23243

SW3010A

07/16/2010

QC results affect the following production samples:

1103364001

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1030 103 ( 80-120 ) 1000 ug/L 07/21/2010

Batch

Method

Instrument

MMS6543

SW6020

Perkin Elmer Sciex ICP-MS P3

37 of 43
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Prep

975015 Lab Control Sample

975016 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20961

SW5030B

07/20/2010

QC results affect the following production samples:

1103364001, 1103364002

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 200 100 ( 80-116 ) 200 ug/L 07/20/2010

LCSD 193 96 4 (< 20 ) 200 ug/L 07/20/2010

Surrogates 

4-Bromofluorobenzene <surr> LCS 110 ( 50-150 ) 07/20/2010

LCSD 105 5 07/20/2010

Batch

Method

Instrument

VFC10031

SW8015C

HP 5890 Series II PID+FID VCA

38 of 43
Matrix

SGS Ref.# Printed Date/Time 07/30/2010 16:34

Batch

Method

Date

Original

Prep

974422 Matrix Spike

974423 Matrix Spike Duplicate

1103478004

Water (Surface, Eff., Ground)

MXX23243

3010 H20 Digest for Metals ICP-MS

07/16/2010

QC results affect the following production samples:

1103364001

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Metals by ICP/MS

Lead MS (0.620) U 1040 104 ( 80-120 ) 1000 ug/L 07/21/2010

MSD 1020 102 1 (< 15 ) 1000 ug/L 07/21/2010

Batch

Method

Instrument

MMS6543

SW6020

Perkin Elmer Sciex ICP-MS P3

39 of 43
40 of 43
41 of 43
42 of 43
43 of 43