Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

10670 AES Deepwater Unit 1 petroleum cokeFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

10670 AES Deepwater Unit 1 As Received Higher Heating Value 10670 AES Deepwater Unit 1 As Received % Moisture 10670 AES Deepwater Unit 1 As Received % Ash 10670 AES Deepwater Unit 1 As Received % Sulfur 10670 AES Deepwater Unit 1 Dry basis Higher Heating Value 10670 AES Deepwater Unit 1 Dry basis % Ash 10670 AES Deepwater Unit 1 Dry basis % Sulfur 10670 AES Deepwater Unit 1 Dry basis Antim ony 10670 AES Deepwater Unit 1 Dry basis Arsenic 10670 AES Deepwater Unit 1 Dry basis Beryllium 10670 AES Deepwater Unit 1 Dry basis Cadmium 10670 AES Deepwater Unit 1 Dry basis Chlorine 10670 AES Deepwater Unit 1 Dry basis Chromium 10670 AES Deepwater Unit 1 Dry basis Cobalt 10670 AES Deepwater Unit 1 Dry basis Fluorine 10670 AES Deepwater Unit 1 Dry basis Lead 10670 AES Deepwater Unit 1 Dry basis Manganese 10670 AES Deepwater Unit 1 Dry basis Mercury 10670 AES Deepwater Unit 1 Dry basis Nickel 10670 AES Deepwater Unit 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) D4809 160.3 MOD D482 D1552 D5865 D3174 D4239 6020 6020 6020 6020 9056 6020 6020 9056 6020 6020 7471A 6020 6020EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10670 AES Deepwater Unit 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units PM-R1 8/3/2010 8/3/2010 14811 Btu/lb PM-R2 8/3/2010 8/3/2010 14527 Btu/lb PM-R3 8/4/2010 8/4/2010 14752 Btu/lb HG-R1 7/25/2010 7/25/2010 14704 Btu/lb HG-R2 7/25/2010 7/25/2010 14854 Btu/lb HG-R3 7/25/2010 7/25/2010 14593 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 4.2 0.53 15460 Btu/lb 0.55 4.471 5.5 1.57 15373 Btu/lb 1.66 4.554 4.5 0.46 15447 Btu/lb 0.48 4.436 4.7 2.78 15429 Btu/lb 2.92 4.779 4 1.68 15473 Btu/lb 1.75 4.717 5.4 2.91 15426 Btu/lb 3.08 4.979Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) [<7.5] ppm [<0.0009] mg/Kg [<0.3] mg/Kg [<0.13] mg/Kg [<0.11] [<7.5] ppm 0.019 mg/Kg [<0.3] mg/Kg [<0.13] mg/Kg [<0.11] [<7.5] ppm 0.0214 mg/Kg [<0.3] mg/Kg [<0.13] mg/Kg [<0.11] [<7.5] ppm [<7.5] ppm [<7.5] ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg [<0.15] mg/Kg [<0.2] mg/Kg [<0.09] mg/Kg [<0.10] mg/Kg mg/Kg [<0.15] mg/Kg [<0.2] mg/Kg [<0.09] mg/Kg [<0.10] mg/Kg mg/Kg [<0.15] mg/Kg [<0.2] mg/Kg 1.4 mg/Kg [<0.10] mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 314 mg/Kg [<0.6] mg/Kg [<0.08] mg/Kg 4.2 313 mg/Kg [<0.6] mg/Kg [<0.08] mg/Kg 5.5 318 mg/Kg [<0.6] mg/Kg [<0.08] mg/Kg 4.5 4.7 4 5.4 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 10.9 0.55 88.55 90.22 3.93 2.02 4.471 11.35 1.66 86.99 90.82 3.47 2.01 4.554 11.08 0.48 88.43 90.59 3.34 1.77 4.436 11.14 2.92 85.94 90.38 3.34 2.08 4.779 13 1.75 85.26 90.93 3.31 2.06 4.717 13.12 3.08 83.8 90.41 2.79 2.17 4.979 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen1

0.73 0.79 0.67 0.78 0.56EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10670 AES Deepwater Unit 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units AG-R1 8/18/2010 8/18/2010 14847 Btu/lb AG-R2 8/19/2010 8/19/2010 14677 Btu/lb AG-R3 8/19/2010 8/19/2010 14430 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 3 0.88 15306 Btu/lb 0.91 4.493 5 0.89 15450 Btu/lb 0.94 4.772 6 0.84 15351 Btu/lb 0.9 4.827Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) [<7.5] ppm [<7.5] ppm [<7.5] ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units [<3] ppm [<3] ppm [<3] ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

3 10.34 0.91 88.43 89 3.24 2.03 4.493 5 10.96 0.94 87.53 89.5 3.28 2.33 4.772 6 12.33 0.9 85.98 88.34 3.78 2.45 4.827 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 0.32 <0.05 <0.05EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10670 AES Deepwater Unit 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units ORG-R1 7/23/2010 7/23/2010 14793 Btu/lb ORG-R2 7/23/2010 7/23/2010 14840 Btu/lb ORG-R3 7/23/2010 7/23/2010 14744 Btu/lb HCHO-R1 7/24/2010 7/24/2010 14854 Btu/lb HCHO-R2 7/24/2010 7/24/2010 14716 Btu/lb HCHO-R3 7/24/2010 7/24/2010 14734 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 3.8 0.52 15378 Btu/lb 0.54 4.584 3.9 1.85 15443 Btu/lb 1.92 4.74 4.3 1.99 15406 Btu/lb 2.08 4.693 3.8 1.1 15441 Btu/lb 1.14 4.549 4.7 0.75 15442 Btu/lb 0.79 4.413 4.1 1.71 15364 Btu/lb 1.79 4.407Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) [<7.5] ppm mg/Kg mg/Kg mg/Kg [<7.5] ppm mg/Kg mg/Kg mg/Kg [<7.5] ppm mg/Kg mg/Kg mg/Kg 52 ppm mg/Kg mg/Kg mg/Kg [<7.5] ppm mg/Kg mg/Kg mg/Kg [<7.5] ppm mg/Kg mg/Kg mg/KgBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture mg/Kg mg/Kg ppm mg/Kg 3.8 mg/Kg mg/Kg ppm mg/Kg 3.9 mg/Kg mg/Kg ppm mg/Kg 4.3 mg/Kg mg/Kg ppm mg/Kg 3.8 mg/Kg mg/Kg ppm mg/Kg 4.7 mg/Kg mg/Kg ppm mg/Kg 4.1 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 10.92 0.54 88.54 90.43 3.12 1.97 4.584 0.8 11.65 1.92 86.43 90.93 2.93 2.13 4.74 0.76 11 2.08 86.46 90.69 3.46 1.82 4.693 0.83 11.68 1.14 87.19 90.26 3.27 2.09 4.549 0.65 11.05 0.79 88.16 89.72 2.99 1.81 4.413 0.68 11.91 1.79 86.31 91.01 3.22 1.97 4.407 0.76 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10670 AES Deepwater Unit 1 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units DF R1 (HCHO R1-3) 7/24/2010 7/24/2010 14768 Btu/lb DF R2 (Hg R1-3) 7/25/2010 7/25/2010 14717 Btu/lb DF R3 7/26/2010 7/26/2010 14876 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 4.2 1.19 15416 Btu/lb 1.24 4.456333 4.7 2.46 15443 Btu/lb 2.58 4.825 3.8 0.63 15463 Btu/lb 0.66 4.696Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 52 ppm [<7.5] ppm [<7.5] ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 4.2 4.7 3.8 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 11.55 1.24 87.22 90.33 3.16 1.96 4.456 0.70 12.42 2.58 85.00 90.57 3.15 2.10 4.825 0.67 11.34 0.66 84.66 91.55 2.50 1.97 4.696 0.77 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm