**.~:.:** " 

### .. , . .' .'-'

.**~.** . 

## . ; 

# .;,""',**~.o:.,~"** 

# ":",:.::"'**""~'~~r~~~~~~~.~"** 

# "

.. .. ,... , 

### .. "

" 

# - ,'. ':'" :



### RMCEINC Project

### #2005-13084

ENCHRO PLATING, INC. 

### MELROSE PARK, ILLINOIS

PREPARED FOR: ENCHRO PLATING, INC. 

### BY: RMC ENVIRONMENTAL, 

### INc.
- ClUCAGO OmCE

### ENCHRO PLATING, INC. Melrose Park, IT.



### TABLE OFCONTENTS RMCE INC-EAsTCOASl' OmCE Project 

### #2005-13084



### 1.0 PRo.JE.Cr SUMMAR.Y .•-.........................._............................................................................................1 1.1 CompBDY Info.rmatiOD•••••..•••••••.•••••.••••.•••••••.•.••.•••••••••.•••••.••..•••••.•••...•••••••••.••••..•••..•••••••••.•.•••.••..•.•.•.••.•.••••. 

### 1 

### 1.2 TestiDgFirm 

## Information

........................................................................................................................... 1 1.3 Test 

## Information

........................................................................................................................................ 1 1.0 SUMMARY OF RESULTS••

___•••_.__................_ ..........................**~**

### ••

__--..._........................_....

### ...2


### 3.0 TEST EQV'lPMENT AND PROCEDURES

..........................................."

.........................._...................3 

### 3.1 Total Chromium

- Emissions Testing

............................................................................. 3
4.0 EQUIPMENT CALIBRATION AND QUALITY ASSURANCE

......................................... 4 

### AppeDdix 

## A - Reference Measurement Data With Emission Rate Calculations AppeDcIh 

## B - Field Data Sheets ForTotal Chromium AppeDdix C - Analytical Data For Total Chromium Analysis AppeDdix D - Facility Scrobber Data AppeDdh 

### E • 

## Reference Measurement Performance Checks and Calibration, Chain Of

### Custody 

## and QAlQC 

## Documentation

### ENCHRO PLATING, INC. Melrose Park, 

# n.

1.0 PROneI'SUMMARY

1.1 Company Information Name and Address:



# contact: Telephone Number: Sources to 

### be 

### tested: Permit Number:
1.1 Testing Firm Information 

### Name and Address:

ContactIProject 

### Manager: 

### Telephone Number:



### t.3 Test Information Test Requested by:
Source Contact: 

### Telephone Number:


### Test Objective:



### Test Methods:
Test 

### Dates: Source Test 

### Coordinators:
Test 

### Personnel: Agency Personnel: 

# . RMCE INC-EAsT COASTOmCE Project

### #2005-13084



### EnCbro Plating, 

### Inc. 2755 

### West Lake 

### Street 

### Melrose Park, IlliDois 60160 Josepb ViuareaI 

### 708-456-1250 Newly Installed 

### Chromium SCNbber

- 

### #2 

### IEPA Permit # 

### 031 

### 1 86AGQ

RMC ENvIRONMENTAL, 

### INc 

### 9226 North 21!d Street Machesney 

### Park, Dlinois 6111S 

### Gregory Chleborowicz 815-378-6150 

### Voice 815-425-1102 

### Fax

EnCbro Plating. Inc. Joseph VHlareal 108-456-1250 CompUaru:elPerformaace testing 

### in 

### acc:ordance with 40 CPR. 

### 63, SubpartN - 

### National Emissions Scandards for Chromium Emissions fiom Hard 

### and 

### Decorative Chrome Electroplating and Chromium Aaodizing 

### Taub

EPA Methods 1-4 and 306 September 21, 2005 

### Joseph Villareal Gregory Chleborowicz

-**Proj~** 

### manager 

### Mr. Marcus Hatc:b -lEPA

### ENCBRO PLATING, INC. 

### Melrose Park, IL

1.0 SUMMARY OF RESULTS 

### RMCE INC-EAsT COAST 

### Oma Ploject#200S-13084



### The results 

### ofthe emissions retesting 

### performed on the large chrome tank 

### S1aCks 

### are presented 

### in Table 2-1. Detailed results of aU 

### of

### the testing 

### compJeted on 

### this location 

### are located 

### in Appendis A. 

### The field data and 

### the analytical results are presented 

### in Appendix B and C, respectively. 

### Calibration sheets and 

### equipment performance checks 

### are presented in Appendb 

### D, alons 

### with the chain ofcustody. 

### A cyclonic flow check 

## was performed at 

### the sampling 

### location to 

### detenn.iJle the existence ofabnormal flow. The observed average yaw 

### angle for scrubber 2 

### was 1.2°. 

### Section 2.S 

### ofEPA Method 1 

### indicates that 

### a 

### sampliDg location with 

### an average yaw 

### angle of

### S 20° is 

### acceptable. As 

### indicated by 

### the average of

### the three test 

### runs, 

### the concentrations of

### the chromium emissions 

## were below the MACT regulation standards 

### ofO.OU 

### mgIDSCM for composite 

### mesh pad scrubber 

### systems 

### on hard chrome plating tanks.



### Loeatfoa' Scrubber 2 

### TABLE 2-1 SUMMARY OFTOTAL CHROMIUM RESULTS ENCBRO PLATING, INC. September

### 21, 2005 

## Teat'Pmmeter 

## RalaJt" " .',', " 

## . SiM:dffatii)lt ' .. - \ 

### mglDSCM 

### 0.006 

### S 0.015 mglDSCM 

### for 

### bard chrome plating 

### Flow rate DSCFM 

### 18)67 

## sources

### ENCHRO PLATING, INC. 

### Melrose Parle, 

# n.

3.0 TEST EQUIPMENTAND PROCEDURES 

### RMCE INC-EAsT COASTOmCE 

### Project #2005-13084



### The test program includes the 

### measurement oftotal 

### chromium stack

### emissions. This testing 

### will 

### be conducted for 

### verification of compliance status 

### with 

### 40 CFR 63, SubpartN -thespecification is 

### O.OlS mgIDSCM of total 

### cbromimn for each plating tank. The 

### methods to be 

### preformed conform to 

### the requirements ofCFR; Title 40 Part 

### 60, Appendix A and EPA Test Methods 1.2, 3, 4, and 306 (CFR; 

### Title 40 

### Part 60. 

### Appendix A). The 

### equipment and procedures 

### RMCEINC uses 

### in meeting these requirements 

### are 

### described below.
3.1 Total Chromium

- EmJssioDS Testing 

### Sample Collection. Samples 

### are withdrawn isokinetically 

### from the 

### source using 

### a modified EPA Method 5 sampling train. 

### The sampling ttain 

### consists ofa glass 

### nozzle. an unheated Teflon probe with a Type 

### S Pitot 

### tube attached, Teflonjumper, four chiDed impingers, and a 

### metering console. The first and 

### second impinger 

### contain 100 ml 

### of a 0.1 N 

### sodium hydroxide (NaOH) solution, the tirlrd remains 

### empty 

### and the fourth contains pmvcighed silica gel.
Each run is a minimum 

### oftwo 

### houn in 

### duration 

### with a 

### minimum sample 

### volume of60 dIy 

### standard cubic 

### feet. Each ofthe points is 

### sampled for the 

### appropriate times, resultiDg 

### in 

### net nm times of 

### 120 minutes. 

### RUDJ 

### will be numbers consecutively 

### with the 

### unit designation, method and run number (ex. 

### Stl-M306-01 and Sa-M306-01). 

### Field blanks and a reagent blank will be 

### coUected and aualyzed per

### EPA Method 306. 

### Since each set oftwo 

### scrubbers vent through one duct to 

### the atmosphere. aU 

### the scrubbers and 

### aU ofthe tanks 

### will be 

### operated simultaneously but each ofthctwo ducts/stacks is tested 

### individually to filcilltate 

### as close to

### normal I 

### maximum production as possible. Sample Recoyery. The 

### reagents are returned 

### to the original bottles,**weigh~** 

### the weights recorded on the labels, and the 

### liquid levels, marked. 

### The silica gel 

### is retmned 

### to the original container. weighed, 

### and the weight 

### recorded on the 

### label. The volume ofwater 

### vapor condensed in 

### the impingers and the volume ofwater vapor collected in the silica gol is 

### summed and entered into 

### moisture content 

### calculations. The nozzle. probe 

### and connecting tetIon is rinsed with

### NaOH 

### into the original 

### container. The first, 

### second and 

### third impingen 

### are 

## alSo rinsed with

### 0.1 N NaOH andadded to 

### the original reagent

### jar.

. 

### Sample Analyses. The 

### amount ofcondensate collected in 

### each train is

### used to 

### determine the moisture content ofthe flue gas. The sampJe (container 1) is 

### analyzed 

### for total chromium 

### utilizing inductively

- coupled plasma

- mass spectroscopy (lCPMS). Samples are 

### collected, a chain 

### ofcustody tilled out, and the 

### samples shipped or 

### driven directly to 

### Environmental 

### Monitoring & 

### Tecbnology, Inc. (EMT. 

### Inc.) after the test project is complete. All QAlQC 

### data from this 

### analysis 

### will be 

### provided by 

### EMT, Inc. (8 

### NELAP Certified Laboratory). 4.0 EQUIPMENT CALIBRATION AND QUALITY ASSURANCE 

### RMC Environmental. Inc. observes cahDration and quality 

### assurance (QA) programs for aU equipment used in emissions measurement. Calibrations are conducted in 

### a manner and at 

### a frequency which meet or exceed U.S. EPA QA specifications. The Meterbox, Pitot and nozzle calibrations are included 

### in Appendix

. Specific quality 

### control (QC) 

### procedures are 

### followed to 

### ensure the continuous production ofusetW and valid data throughout the course of this 

### test program. The QC 

### checks and procedures described in 

### this 

### section represent an 

### intep

# nart ofthe overall sampling and analytical scheme. Strict adherence to 

### prescribed procedures is quite often the 

### most applicable QC 

### check.
The 

### cah'bntion and quality assurance procedures ofEPA Methods 1-5 

### will be followed throughout the test program.

### ENCBRO PLATING, 

### INC. Melrose Park, 

## n. RMCE 

### INC·EABrCOABl' Oma Project #2005-13084



## Appendix A - Reference Measurement Data With Emission Rate Calculations

### RMC Environmental, Inc. Em issions Testing 

### & Consulting

Plant: EnChro Plating Date: 10108105 Project 

### #: 200&-13064 

### location:**SCiij~** 

### Sample Identification 2·M3Q6-1 

### Test Date 09121 / 05
Start 835 

### Finish 1037 

### Total 120 Cp 

### Pitot Coefficient (C F) 0.64 A 

### Area of stack 

### sq. Inches 1017.9 

### Pbar Barometric Pressure (in HG) 30.08 Wm 

### Volume of Condensate (mg) 24.6 Ts 

### Temperature of Effluent 

### (F) 86

.5 

### Pavg Average Delta P 0

.640 Pg 

### Static Pressure (i n H2O) 1

. 10 OH 

### Delta H, Orifice pressure different (in H2O) 0.89 Tm 

### Meterbox Temperature (F) 79

. 1 Vm 

### Volume of sample metered (C F) 63

.212 

### Y Meter correction factor 1

.036 On 

### Nozzle Dlamater (In) 0.195
CO2 

### Percent Carbon Dioxide (%) 1 .00 02 

### Percent Oxygen (%) 21

.00 CO 

### Percent Carbon Monoxide (%) 0 N2 

### Percent Nillogen ('''') 78

.00 Ms 

### Molecular Weight (wet) (Ibflb-m) 28

.81 

### Laboratory Resultl
Total Chrome (mg) 1.33E-02

Ps 

### Absolute pressure of Flue Gas (I n HG) 

### 30.16 Vwstd Volume of Water Vapor (SCF) 1

. 16 

### Vmstd Voluma of Metered Gas (DSCF) 64

.597 M 

### Moisture (%) 1

.76 Vs Velocity (FPS) 45.56 

### Daw Volumetirc Flow (ACFM) 19

.324 

### Dsd Volumetric Flow (DSCF) 18.488 

### Chrom ium Concentration (mglOSCM) 0

.0073 

### Chromium Concentration (lblHr) 5.05E-D4



### Isokenetic (%) 99

.24 2·M306-2 2·M306-3 

### 09121105 09121105
1055 1315 

### 1257 1518

120 120
0

.64 0

.64 1017

.9 1017

.9 30.08 30.08

29.4 29

.2

88 92.1 0

.620 0

.650

1

. 10 

### 1.02 0

.87 0.90 83

.0 85.8 63.421 65.196

1

.036 1

.036 0.195 0

. 195
1

.00 1

.00 21

.00 21

.00 0 0 78

.00 78

.00 

### 28,n 28

.77

1

.29E-02 1.11E-02
AVERAGES 30

. 16 30

. 16

1.39 1

.38 64.342 65

.808 2.11 2

.05 

### 44

.94 46.18 19.058 19.587 18.120 18.492 18

.367
0

.0071 0

.0060 0.00596 4

.79E-D4 4.13E-D4 4.66E-D4

100

.85 101

.08

### ENCHRO PLATING, INC. 

### Melrose Park, IL RMCE lNC-EASTCOASTOFAa 

### Project #200.5-13084

Appendix B
- Field Data Sheets For Total Chromium

### METHOD 1 - SAMPLE AND VELOCllY TRAVERSES FOR CIRCULAR SOURCES

Plant Name En Chro Plating

. Date 

### 09121105 SampUna LocatIon Unit 2 Scrubber 

### Project. 2005-13084 Operator Gac , of Ports Avallable 2 8tackType 

### CirGuJar • ofPorts Used 2 8tacilSize 

### llarae Port inside Dlamemr 4 

## L

fw Circular Staclt or Duct Diameter 

### DIstance to Far Wall ofStack (Lt.) 

### 39.50 in 

### f--LnW

# V**~** DIstance to NHI'Wall of Stack (L",,) 

### 3.50 in 

# ! 

# \

- {-t.1w.WI DIameter of 

### 8tacJr (D) 

### 36.00 in 

# v-\**{-3.t~J2IArea** of Stack (A.) 

### 7.07 ft'" 

### r-- 

### DIstancefrom 

### Portto 

### DIsturtIances 

### 0 DIstance U...-

......... 

### (8) 76.00 in

# ~**~~** ('8.01 

### DIameters U (So) 

### 2.11 diametans Distance Downstream 

### jAl 40.00 in (-MIl Dlamellln Downstream (Ao) 

### 1.11 dlametare 

# T ,--- 

### Down streom Number ofTraverse PoInts Required Mlnlmwn Number 

### of' 

# t Disturbance Dlametento 

## A Flow Disturbance Traverse PoInts

Up Down PartIculate Velocity 

# , P Measurement Stream Strum Points PoInts**~** 

### Site 

### 2.Q0...4.99 0.50-1.24 24 16 5.00-5.99 1.25-1.49 20 16 

# t**6.0~.99** 

### 1.50-1.74 16 12 7.00-7.99 1.75-1.99 12 12 

## B

>-= 8.00 >=2.00**8or1~ 8or1~_**  Upstream Spec 

### 24 16

## ~ceo,," Downstream Spec 

### 24 16 Traverse Pta Raqulr.d 

### 24 16 "-..

### D;st~bon-ce .' Chock MInimum Numb«rA PoInts for the Upslnlem

and Downstream concfiIfans. then &ISO IfIo

### /artest. Number ofTraverse PoInts Used2 8 for Circular Stadca 12 to z.41nchas 

### 2 Parts by 

### 12 Across

12 far Clrc;uIat Stadia CMIt24 Inches 

### 24 PlaUsell 

## 24 Required 

## [.,J ParClculate 

### [J Velocity


### Traverse PoInt 

### locations Leadoa afT_neP

......CIrcaIar

.... Fraction DIstance 

### DIstance 'navcno**rP_licooISlacft~&_:racid**.. WallIDT_PW.) Traverse of from 

### Incfudlng

POInt Numl

.. r**alT~** Pod. 011 aI>iams:W Point Stacir Inside Nipple Numb

... 2 4 Ii II t. II 1 .146 .06'7 .04-t .031 .026 .0%1 Number DIameter 

### Wall Length 

### z .854 .150 

# .1'" .1115 .1J8Z .067- In 

### in J .750 .l96 .194 .1-46 .Jl8 

### 1 0.021 6/8 4218 J .!J,u**.7~** ..121 .UAi .177 5 

### .•s. .677 ..J.U .l5O 

### 2 0.067 23/8 5718 6 .95 .1106 .691 ..156 

### 3 0.118 42/8 76/8 7 .8H .77-4 ,6.U 

### 4 0.1n 6318 

### 97/8 

# • .9Ci8 .854 .750 

# , .918 JI2.J 

### 5 0.250 9 124/8 10 .97-4 .lSI 

### 8 0.356 127/8 16318 11 3» U 979 

### 7 0.644 231/8 

### 265/8 8 0.750 27 304/8 

### 9 0.823 29518 331/S 

### 10 0.S82 316/8 35218 

### 11 0.933 335/8 371/8 

### 12 0.979 35218 

### 386/8

Enchro Plating

- M1

- Circular Page 

### 1 Printed 

### 1018/2005 V1.1S

### METHOD 2· DETERMINATION OF STACK GAS VELOCITY AND VOLUMETRIC FLOW RATE
PfantName En Chro Plating Date 

### 09fl1Al5 8amDUna Location Unit 2 

### Saubber 

### Project. 2005-13084 Operator Gee " or 

### Ports Used 2**Stack~** 

### CiR:u1ar PItOIldentlflcatlon M5-11-02 Pilot Leak Check 

## 0 

## I PreTest 

## L [,,] 

## 1 POlitTest PIlot Coeftk:lent (CJ 0.84
8tact Dtmenstons Velocray Traverse Data Diameter or

## i.enath or

### Stack (D) 

### 36.00 in Run Number U2·M3Q6.V1 lMdth orStIM:k (W) in 

### Runnme Area orstack (As) 

### 7.07 

# nz Traverse Velocfty Stack Local Point Head Temp Velocity Pressuru**(~)** (t.) (vsll Barometrtc 

### Pressun (P.,) 

### 24.68 inHg**ln~ ~**  ftIaec StaIIc Pressure 

### (P..J 1.10 

### InHzO A-1 0.60 

### 84 48.6 ADsoCute stack PnssUre (P.) 

### 24.78 InHg 

### A-2 0.82 

### 84 49.4 

### A-3 0.58 84 

### 47.8 8tac:k Gas Composblon 

### A-4 0.80 84 

### 48.6 Composlllon

## Data:1 AdUaI 

### [,,] EstImated 

## 11 A-5 0.63 84 49.8 Carbon Dtoxlde Conc.ntndlon (%CO,) 

### 1.0 % 

### A-6 0.61 84 

### 49.0 OXygen Concentrallon (%O:r) 

### 20.0 %**~7** 

### 0.65 

### 84 SO.6 Carbon MonoJdde Concentralion (%CO) 

### 0.0 % 

### M 0.64 

### 84 SO.2 Nitrogen Conctrdndfon (IWoNz) 

### 79.0 % 

### A-9 0.67 

### 84 51.4 Stac:t Moisture Content 

## (a..> 2.000 A-10 0.62 84 

### 49.4 Stack Dry MofecuJar Welght CM.t) 

### 28.96 lb.1b-moIe 

### A-11 0.60 84 

### 48.6 Stack Wet MolecUlarWelght (M.) 

### 28.74 IbAb-moIe 

### A-12 0.59 84 

### 48.2 8-1 0.59 84 

### 48.2 R.esuIts 

### B-2 0.61 84 

### 49.0 Avg8tadc Gas Velocity (va) 

### 49.6 ftIsec 

### B-3 0.63 85 49.9 Avg Stack Dry S1d Flow Rate 

### (Clad) 

### 993688 dscMu' B-4 

### 0.80 85 48.7 Avg Stack Dry Std Flow 

### Rate CQ.) 

### 18561 dscfhni'l 

### B-5 0.87 ·84 

### 51.4 Ava 

### StackWet Flow 

### Rate (a..) 

### 21046 ascfhnin 

### B-6 0.68 84 

### 51.0 8-7 0.65 84 

### 50.6 Stack Cross 8edfon 8dtemaIJc 

### B-8 0.64 

### 84 50.2



### PI. =DWfr<u 

### hlr RedangUIar Stadca 

### As = (K(OlZ)2)JK., for Circular Stacks wh."., 

## Ku :: 1 for metric units wh."., K.,:: 144 (,,"2m; for English units p. :: 

### Pilar + 

### P.J13.6 %N2

# = 100· %C02· %02 • %CO Md:: .44{%CO:z) + .32(%02 ) + .28(%Nz+ %CO) M. 

# = Md(1 • Bw.) 

### + 18Bw. (.lP)112**~_**'" 1/,,E(.lpIa,
Enchro Plating

- M2 B-9 

### 0.68 

### 84 51.0 8-10 0.58 

### 84 47.8 8-11 0.57 

### 85 47.4 8-12 0.57 85 47.4

Average' 

### 0.79 84 PI_ "'porttho 8VIf1tG. 01 the 5qW1l'& toOCs of .lP.or, (,»)"l_o**,,~I'i** Formulas Used 

### TI(,,'

### =lInD. +Tu whent T u

### =273 

### OK for metric units wh."., 

### Tu:= 460 

### OR for 

### Eng/ish units 

### v." K"Cp(.lp)IIl.,g (f

..**WI'I~.MJ)11l** wh."., 

### Kp 

### =34.97fer 

### metric units whete 

### Kp

.. 85.49 for EngIitIh units QId" 3600(1 • 

### B..)vsA.(T

### sJT1(1YII1)(PslPs1d) wh."., T sill 

### =293 

### OK, Pili! 

# = 760 mm Hg, for metric units wh."., T sat 

### =528 

### DR. P

### I1d :: 29.92 in Hg, for Engl18h units 

# I

Page 

### 1 Printed 10/812005 V1.1S

### METHOD 3 - GAS ANALYSIS FOR THE DETERMINATION OF DRY MOLECULAR WEIGHT
Plant Name 

### En ChIo Platina Date 09121105 Samplll'lfl Locallon Unit 2 Scrubber Project" 2COS-1301W ()per@tor Gac tIof Porta Used 2 Fue'Type N/A 

### I MInImum FU1II Factor 1.600 I Maximum Fuel FactorI1.800 OrsatLeak Check [-!I I PreTest I

Run Number 

### U2-M306a-01 Sample Carbon Carbon Analyals Dioxide Oxygen Monoxide

Time Volume Volume Volume 

### (Vcaa> (Vm) (Veo) hh:mm ml mJ mI 

### FYRITE 1.0 21.0 1.0 21.0 1.0 21.0 Result. 

### [,,-wrages Average Calculated Fuel Factor (F.)

.... Averaoe Excess Air (%EA)_

Run Number 

### U2-MS06-2 Sample carbon carbon Analysis Dioxide Oxygen Monoxide

Time Volume Volume Volume 

### (Vcaa> (Ve»,) 

### (vcol hh:mm mJ mJ 

### mI 

### FYRITE 1.0 21.0 1.0 21.0 1.0 21.0 

# Resu'" IAverages Average Calculated Fuel Factor 

## CFJ.., Average Exceu Air ("EA)_

Run Number 

### U2-M306-3 Sample Carbon Carbon Analyal. DioxIde Oxygen MonoxIde

Time Volume Volume Volume 

### (Vee»> (Voz) (Vco) hh:mm ml mJ ml 

### FYRITE 1.0 21.0 1.0 21.0 1.0 21.0 Results 

### Averages Average Calculated Fuel Factor**(F.)~** Average 

### Excess Air ('I&EA)...,
Fuel FactorFo Fuel Type Minimum Maximum Coal, Anthracite 

### 1.018 1.130 Coal, Ugnlte 

### 1.018 1.130 Coal, Bltumlnoua 

### 1.083 1.230 

### 011, Distillate 

### 1.260 1.413 Oil, Residual 

### 1.210 1.370 

### Ga., Natural 

### 1.800 1.838 Gas, PropaJ\a 

### 1.434 1.588 Gas, Butane 

### 1.405 1.553 Wood 

### 1.000 1.120 Wood Bark 

### 1.003 1.130

Enchro Plating

- M3

- Orsat**~** I PostTest Oraat identificationI
Oaa Analyals Data Run StartTime 

### .8:35 Run Stop Time 

### 10:37 Carbon Carbon DIy Molecular Dioxide Oxygen Monoxide Nitrogen MolfICUlar Weight Cone. Cone. Cone. Cone. Weight Deviation**~** (%Oz) (%00) ("'Nz) (M..) (.1M..) 

### fIM*'It peRent pen:ert percent Ib.1IHnoIe IbIItHnoIe



### 1.0 20.0 0.0 79.0 28.96 0.00 1.0 20.0 0.0 79.0 28.96 0.00 1.0 20.0 0.0 79.0 28.96 0.00 1.0 20.0 0.0 79.0 28.98 0.900 Mo'flCUlarWI Deviation c 0.3? 

### Itl_ 2338.4 percent Fuel FactorIn Handbook Range? 

### ItJ
Oaa Analy_sls Data 

### RLm StartTime 

### 10:55 Run StopTime 

### 12:57 carbon Dioxide Oxygen Cone. Cone. (%COz) ("'Oz) pen:ent percent



### 1.0 20.0 1.0 20.0 1.0 20.0 1.0 20.0 0.900 2338.4 pen:ent
Gaa Analysl. Data 

### Run StartTime Carbon DIOXIde Oxygen Cone. Cone. (%COz) (%Oz) percent pen:ent.



### 1.0 20.0 1.0 

### 20.0 1.0 20.0 1.0 20.0 0.900 2338.4 pen:ent

Page 1 Carbon Dry Molecular Monoxide Nitrogen Molecular

Cone. Cone. Weight (%CO) ("'Nz) (M..) pen:ent pen:ent IIktIHnole



### 0.0 79.0 28.98 0.0 79.0 28.98 0.0 79.0 28.98 0.0 79.0 28.98 MolecularWI DevIation c 0.31 Fuel Factor In Handbook Range?



### 13:15 

### Run Stop Time cartIon DJy MonoxIde Nitrogen Molecular

Cone. Cone. Weight (%CO) ("'Nz)**(~** pen:ent**~.** IbIIb-moIe



### 0.0 79.0 28.98 0.0 79.0 28.98 0.0 79.0 28.98 0.0 79.0 28.98 MolecularWI DeviatIon <0.3? Fuel FactorIn Handbook Range?
Formulas Used**%~=Vcoz** "40z sa VOl

- Vcoz 'l6CO 

# = Veo

- VOl "'Nz 

### = 100

-**'l6~** - 

### 'l60z

- "'CO WeIght Deviation

(AM..) IbmHnoIe



### 0.00 0.00 0.00 

### Itl [of]



### 15:18 MolfICUllllr

WeIght Deviation

(AM..) IbAb-moIe



### 0.00 0.00 0.00 

### [] [J

Mof:: .44('l6COz.)+ .32(%0z)+ .28(e"Nz+ %CO) 

### lM.. :: Mel

- MdIoV Fo 

# = (20.9

- 

### %Oz

- .5'l6CO)/('W.CO-z + %CO)**%EAa100~Or.s'loCO)l(.264'l6NOr("0r.S%CO)** 

## I 

## J

Printed 10/812005 V1.1S

### METHOD 4 - DETERMINATION OF MOISTURE CONTENT IN STACK GASES

Plant Name sampllna LocaIIon**O~rato,** 81ackJDe Train Leak Check

Run Number Total MeterVolume Avg Meter Temp Avg 

### Stack Temp

Contents final Value lnIIfal Value

Net Value
Total VolUme TotalWeIgh! Std Meter Volume Calc Moisture Content

RunNumller Total Meter Volume AY8 Meter Temp Avg 

### StackTemp

Contents FJnaJVaJue InHfaJ Value

Net V

..... Total Volume Tocal WeIght SId MeterVolume Calc MoistureContent



## . Run Number Total Meter Vorume AVO MeterTemp 

## Ava Stack Temp

Contents FJnalVaJue Initial Value

NetValue
Total Volume 

### Total Wefght Ski MeterVolume 

### caJc Moisture Content
Enchro Plating

- M4 En Chro 

### Platina Dale 

### 09TJ1JD5 Unit 2 Scrubber**P~ect#** 

### 2005-13084 Gac 

### " of Ports Used 2 Circ:uJar Miler 

### 80. Number 

### 05 ["'] 

## I PreTest 

## I ["'] 

## I PosITest Meter Cal Factor

# m 1.038

U2-M306-1 

### (VnJ 63.212 (tn.>- 79**(t.~** 87 bnplnpr1 mI 01 (V,).(W,) 108.00 <V!).(W,) 100.00 (v,J.(W,J 8.0

(Vi} 13.00 (Wi} 11.60 

### lVllltsW 64.622**~calr:Jl** 1.8

U2-M306-2 (V",) 63.421**~** 83 

## <t.>av 88 Impllller1 mI 01 (V,).(W,) 108.00**(V~.(W,)** 100.00 

### NJ.cWn) 8.0 !VI) 18.00 (We) 11.40**(V~aol** 64.370 (BwJ 2.1

U2-M308-3 (Vm) 65.196 

## ttn.>- 86 (t.)wg 

### 92 Impfnger1 mI 

### OJ**(V,).~,)** 109.00**(vJ.~,)** 100.00 

### NJ.fNn> 9.0

(ViJ 16.00**~~** 13.20 (VmrSfIIJ) 65.833



### Ce...) 2.0 Moisture ContenI 

### Data Run 

### stall11me1 8:35 

### Run Stop TIme 10:37 dcf BaromeCrtc Press. (Pb) 

### 30.08 In Hg 

### OF StacIe Stade Press. (P..J 1.10**inH~** "F Avg 

### Ortllce 

### Press. (Mi).,g 0.89 in H20 Implnge,Z Imlllnler3 Implnfer4 fmplnger' Implnger.**fm~naer7** mf 

# m 9 mJ 

### mI mI 01 Sil Gel 105.00

. 161.60 100.00 150.00

5.0 11.6 

### RuuIts mI WaterVol ContIMaStId (V.,.w 0.612 

### ad 9 waterVol

### w.lthed 

## tv

.. an) 

### 0.547 ad dad Sat. Moisture ContenI IA .\ 

## 4.2 %

% final Moislure Content (B..) 1.8 %
MoistureConleld 

### Data Run 

### StallTbne 10:55**Run~TIme** 12:57 del Barometric Press. (I\) 30.08 inHg 

### OF 818ck 8taIIc 

### Press. 

## (P..J 1.10 InHzO 

### "F Avg 

## ormce PIUs.**(~>.w,** 0.87 InHzO ImplngerZ Implnaer3 ImPinaer4 Implnaer' ImJ)lnlle,• Implnger7 

### mI ml 9 

### ml mJ ml 01 

### SIIGeJ 110.00 161.40 100.00 150.00

10.0 11.4 Results 

### mI WIder Vol Condensed**(\[~~)** 0.847 

### ecf 9 WillerVol WeIghed (V

... 

### Anl 0.538 

### ad dscf 

### sat. MoIstUre Content IA 

### 4.4 %

% 

### FInII Moisture Content 

### Ca.) 2.1 %
Moisture Content DaIa Run Start TIme 13:15 Run Stop TIme 15:18 dcf Barometrfc 

### Press. (P,) 30.08 inHg 

### OF Stack

### StaIIc Press. (P..J 1.02 in H20 

### UF Avg OrUlce 

### Press. (Milwt 0.90 inHzO Impfn,erZ Implnger3 impinge," ImMerS Im"",er. fmplnaer7 mI 

### mI 

### Jl 01 

### Sil Gel 107.00 163.20 100.00 150.00

7.0 13.2 Results 

### ml Water Vol Condensed 9 Water Vol WeIghed 

### dacf 

## sat. Moisture Content

% FInal Moisture Content

Page 1 

### mI 

### rri

(VWC(aI) 0.753 

### N

... IIIIl) 0.622 

# (a._,) 5.0



### (e...) 2.0 mI

I

sc:f 

### sc:f % %

Printed 

### 101812005 V1.1S

### rSOKrNETIC SAMPUNG DATA

PlanlName En CM 

### Platina Sampling Locctlon Unit 2 Serubber Operator Gac tI 01 Polnb Actosa 12 Ideal Nozzle Dlametv and lsal<lMtlc Feetor Setup PItaC Tube Coeftlclent (c,) 0.840 Ava Stack Temp (IJ 84 

### ·F Ava au Meter Temp (W 70 

### OF DH • 0.76 SCFM**(~O)** 1.70 InHP Avg PItot Tube Dtff. Preuure**(~** 1.70 InHp StacIe MGlstura Contw1t (8..) 1.8**~** SbIck Dry MoIec:u

....WeIght (M..) 28.96 IbIIHnalo EstImated Oriftce Flow Rate (Q.) 0.750 acfm

DP 10 DH Isoldnedc Factor

. (I<) 1.39 Pressures Barometric Pressure (f\) 30.08 In HI SI.etc Static Pressure (PoIIIIJ 1.10 In Hz{) Abaolute S18ck Prosun 

### CPS> 30.18 In 

### HI Abaol_ Meter Pressure (P.,.) 30.21 In HI
DlyGu De:Itnd Ar:tuIII Traverse Sampling Clock MfIter VeIac:Ity OrIfIce 0Iffice 

### PoInt. TIme 

## nme Readfng Held .Uf**~** (8) 

### (V.) ("P)**(~** (.Uf) min hh:mm:ss 

### rr In Hz{) In Hz{) In Hz{) A-1 0.0 8:35:00 538.900 0.580 0.808 0.810 A-2 5.0 8:410:00 539.400 0.820 0.864 0.860 

### A-3 10.0 8:45:00 

### 542.000 0.810 0.850 0.850 A-4 15.0 8:50:00 544.560 0.820 0.884 0.880 A-5 20.0 8:55:00 547.160 0.820 0.884 0.880 A-8 25.0 9:00:00 549.850 0.830 0.878 0.880 A-7 30.0 9:05:00 

### 552.450 0.820 0.884 0.880 A-8 35.0 9:10:00 

### 555.000 0.84D 0.892 0.890 A-9 40.0 9:15:00 557.600 0.830 0.878 0.880 A-10 45.0 9:20:00 

### 560.350 0.810 0.850 0.850 A-11 50.0 9:25:00 583.000 0.860 0.919 0.920 A-12 55.0 9:30:00 585.420 0.850 0.905 0.900 B-1 60.0 9:37:00 588.210 0.830 0.878 0.880 B-2 85.0 9:42:00 571.110 0.840 0.892 0.890 B-3 70.0 9:47:00 513.340 0.860 0.919 0.920 B-4 75.0 9:52:00 578.520 0.870 0.933 0.930 B-5 

### SO.O 9:57:00 

### 578.890 0.860 0.919 0.920 8-8 85.0 10:02:00 581.850 0.680 0.947 0.940 8-7 90.0 10:07:00 584.200 0.870 0.933 0.930 B-8 95.0 10:12:00 587.850 0.680 0.947 0.940 8-9 100.0 10:17:00 590.000 0.870 0.933 0.930 8-10 105.0 10:22:00**593.~** 0.660 0.919 0.920 8-11 110.0 10:21:00 595.450 0.820 0.864 0.860 8-12 115.0 10:32:00 

### 591.880 0.810 0.850 0.850 LastPt 120.0 10:37:00 600.112

LasIPl 120.0 10:37:00 600.112 Average Values 0.64 

### I 0.89 

### I

Enchro Plating

- M5

- Run 1 Page 1 DGe 8121121lO5 ProJect. 2005-130&4 Run. U2-M308-1 tI 01 Pwta Used 2 Samplln,**E~ulpment**



# Meter. 05 MeterbOlI CaL FacCDr (Y) 

## I 1.036 

## I Nozzle. Actual Nozzle Dt.meIer (D,.) 0.1950 In

Req. Nozzle DIameter**~** 0.1799 In Prabe .,Langth 40.00 It Unar IIatertII 

### Teftan Sample

## cae I Oven. ImJIlnaer

## cae. .1V. lKkChecks

Pre 0 tt'/mln (I 15 In Hg MId rlmln 

# .. InHg Post 0 tt'lmln 

### CD 10 InHO .1V. < 0.020 ft-/min 

## 1tJ LHk Check OK? PlIDtOK? Iktcr Stack Inlet Temp Temp

(tJ 

### <Y "F 

### DF 84 72 85 72 B5 75 B5 75 85 

### 77 88 78 88 

### 79 88 80 88 81 88 81 88 82**~** 

### 83**~** 84 88 84 88 

### 85 87 88 87 88 87 87 87 88 87 88 88 88 89 

### 88 89 90 

### 89 

### 91

87 

### I 83 

## 1 79 

## 21 OrsatOK? 

## iii



# ..... 1mplngM' Cutlet Fl1ter Exit Pump Temp Temp Temp Vacuum**(~**

"F "F "F InHg 

### 12 45 3.0 

### 12 42 3.0 13 42 3.0 74 43 3.0 75 43 3.0 75 43 3.0 75 43 3.0 75 43 3.0 75 43 3.0 75 43 3.0 75 43 3.0 78 44 3.0 78 44 3.0 78 44 3.0 

### 78 44 3.0 

### 78 44 3.0 

### 77 45 3.0 

### 77 45 3.0 

### 77 45 3.0 

### 77 45 3.0 

### 77 45 3.0 78 45 3.0 

### 78 45 3.0 

### 79 45 3.0

Maximum Vacuum 3.0 78 

### I 44

Prin1Bd 1018l2D05 V1.15

### ISOKINEnC SAMPUNG DATA
Ptanttwne**EnCltf1)_~** Locdon Unit 2 Sc:rubbor Operator Gac
• of Paints Acfou 12 ldul Nozzle Dkmetar**~** Isot<lntdlc Factor Setup PIlat Tube CoeftlcJent 

## (c..> 0.840 Ava Stack Temp ll.) 84**~** Avg Gu Meter Temp t\,) 70 of DH 

# e 0.75 SCFM 

### WIG> 1.70**InH~** Ava Pltot Tube Dtfr. Preuw. (4P..g) 1.70 InHP StKtt MoIWn Conant (8.,J 1.8 'K Steck Dry Molecu

..

### WIlfaht <M.) 28.98 IbIIHnaIo EatImIded 0rffIce Flow Rate (0.,) 0.527 acfrn

DP to DH laoldnellc 

### r:.:tor 

### 00 1.39 PnIssunIs BanImetJfc Pressure (P.,) 30.08 InHg StackStatic Pressure (P.-)- 1.10**InH~** AbaoIuw Stack Pres

.... 

### (PJ 30.18 InHo Absolute M

.... Preaauro**(P~** 30.21 In HI
DryGu Dahd Actual Traverse Samplfng Clode Metar Velocily Ortftce 0riIIc:e PoInt. 

## nme TIme Reacllng Had .iH .1H (9) (Ve) (4p) (Mf) (Mf) min hh:mm:ss It" InHP InHP InHzO A·1 0.0 10:55:00 600.900 0.S90 0.822 0.820**~2** 5.0 11:00:00 603.440 0.630 0.878 0.880 A-3 10.0 11:05:00 605.950 0.830 

# o.m 0.880 M 15.0 11:10:00 808.850 0.850 0.905 0.910 M 20.0 11:15:00 811.500 0.820 0.884 0.880 

### MJ 25.0 11:20:00 814.000 0.650 0.905 0.800 A·7 30.0 11:25:00 817.000 0.660 0.919 0.920 

### MJ 35.0 11:30:00 819.550 0.870 0.933 0.930 A-8 40.0 11:35:00 822.320 0.660 0.919 0.920 A-10 45.0 11:40:00 625.000 0.870 0.933 0.930 A-11 50.0 11:45:00 671.750 0.820 0.884 0.860 A·12 55.0 11:50:00 830.200 0.S90 0.822 0.820 8-1 60.0 11:57:00 633.000 0.510 0.794 0.790 8-2 85.0 12:02:00 835.860 0.530 0.738 0.740 

### a.3 70.0 12:07:00 838.050 0.600 0.838 0.840 s.4 75.0 12:12:00 640.860 0.830 0.878 0.880 8-5 80.0 12:17:00 843.000 0.640 0.892 0.890**~** 85.0 12:22:00 646.320 0.870 0.933 0.930 B·7 90.0 12:27:00 848.780 0.640 0.892 0.890 B-8 95.0 12:32:00 651.350 0.850 0.905 0.910 8·9 100.0 12:37:00 654.000 0.820 0.884 0.880 8-10 105.0 12:42:00 668.870 0.600 0.836 0.840- 8-11 110.0 12:47:00 659.320 0.590 0.822 0.820 8-12 115.0 12:52:00 862.000 0.600 0.838 0.840 

### last Pt 120.0 12:57:00 684.321

Final Value 120.0 12:57:00 664.321 Average Values 0.82 

### I I 0.87 

### I

Enc;hro Plating· M5 • Run 2 Page 1 o.t. 81211ZOO5**Pro~'** 2DDS-130&4 

### Run. U2-M306-2 f# 01 Parts Uaed 2 Sampllnt E

Meter. 05 IIeCerbox Cal. Fector (Y) 1.038 

# Nozzle. Actual Nozzle Dtanet8r (D"J 

### I 0.1950 In

Req. Noule DfMIeCer COn) 

### I 0.1508 In Pralle

# tI'Length 40.00 It LIner

........ 

### Teftcn Sample Cae/OwM. Cue. .1V

.. LHkCbecb Pre 0.001**~lmln** 

# • 1S In HI Mid 0 ft"1mIn 

### _0- 10 In HI Post 0.002 

### It"Imln 

# • 10 InHo AV"" < 0.020 

### n*/mIn 

## I2J LeU Check OK? PltatOK?


# .... Stack InJeI Temp Temp

(IJ ty**~** of 

### 81 80 

### 88 81 88 

### 83 88 83 88 85 

### 88 88 85 87 

### 81 88 87 88 

### 88 88 

### 88 89 

### 88 89 88 

### 89 89 

### 89 89 

### 90 87 90 88 91 90 91 91 91 91 92 91 92 91 92 91 92 91 92

88 

### I 88 

## I 83**~** orsatoK?1**~** 

# .... IInpllluw 

### 0UtI8t FIlter ExIt Pump Temp Temp Temp Vcuum tt-)**~ ~** **~** In H, 75 47 3.0 78 45 3.0 76 44 3.0 78 44 3.0 78 

### 43 3.0 71 43 3.0 71 44 3.0 7B 44 3.0 7B 44 3.0 71 43 3.0 71 

### 43 3.0 71 43 3.0 

### 77 44 3.0 7B 

### 44 3.0 78 42 3.0 18 41 3.0 78 42 3.0 79 43 3.0 79 

### 43 3.0 79 

### 44 3.0 79 44 3.0 

### 80 43 3.0 

### 80 44 3.0 

### 80 43 3.0

Maximum Vacuum 3.0 

### .78 

### I I I 44

Printed 10I8l2005 V1.1S