.~:.: " .. , . .' .'-' . ~. . . ; .; ," "', ~.o:.,~" ": ",:.::"' ""~'~~r~~~~~~~.~" " .. .. , ... , .. " 

" - ,'. ':'" : 

RMCEINC Project #2005-13084 

ENCHRO PLATING, INC. 

MELROSE PARK, ILLINOIS 

PREPARED FOR: 

ENCHRO PLATING, INC. 

BY: 

RMC ENVIRONMENTAL, INc. - ClUCAGO OmCE 
ENCHRO PLATING, INC. 

Melrose Park, IT. 

TABLE OF CONTENTS 

RMCE INC-EAsT COASl' OmCE 

Project #2005-13084 

1.0 PRo.JE.Cr SUMMAR.Y .• -.. ........................ _ ............................................................................................ 1 

1.1 CompBDY Info.rmatiOD •••••..•••••••.•••••.••••.•••••••.•.••.•••••••••.•••••.••..•••••.•••...•••••••••.••••..•••..•••••••••.•.•••.••..•.•.•.••.•.••••. 1 

1.2 TestiDgFirm Information ........................................................................................................................... 1 

1.3 Test Information ........................................................................................................................................ 1 

1.0 SUMMARY OF RESULTS •• ___ ••• _. __ ................ _ .......................... ~ •• __ --..._ ........................ _ .... ...2 

3.0 TEST EQV'lPMENT AND PROCEDURES ........................................... " .......................... _ .................. .3 

3.1 Total Chromium - Emissions Testing ............................................................................. 3 

4.0 EQUIPMENT CALIBRATION AND QUALITY ASSURANCE ......................................... 4 

AppeDdix A - Reference Measurement Data With Emission Rate Calculations 

AppeDcIh B - Field Data Sheets For Total Chromium 

AppeDdix C - Analytical Data For Total Chromium Analysis 

AppeDdix D - Facility Scrobber Data 

AppeDdh E • Reference Measurement Performance Checks and Calibration, Chain Of Custody and 

QAlQC Documentation 
ENCHRO PLATING, INC. 

Melrose Park, n. 

1.0 PROneI' SUMMARY 

1.1 Company Information 

Name and Address: 

contact: 

Telephone Number: 

Sources to be tested: 

Permit Number: 

1.1 Testing Firm Information 

Name and Address: 

ContactI Project Manager: 

Telephone Number: 

t.3 Test Information 

Test Requested by: 

Source Contact: 

Telephone Number: 

Test Objective: 

Test Methods: 

Test Dates: 

Source Test Coordinators: 

Test Personnel: 

Agency Personnel: 

. RMCE INC-EAsT COASTOmCE 

Project #2005-13084 

EnCbro Plating, Inc. 

2755 West Lake Street 

Melrose Park, IlliDois 60160 

Josepb ViuareaI 

708-456-1250 

Newly Installed Chromium SCNbber - #2 

IEPA Permit # 031 1 86AGQ 

RMC ENvIRONMENTAL, INc 

9226 North 21!d Street 

Machesney Park, Dlinois 6111 S 

Gregory Chleborowicz 

815-378-6150 Voice 

815-425-1102 Fax 

EnCbro Plating. Inc. 

Joseph VHlareal 

108-456-1250 

CompUaru:elPerformaace testing in acc:ordance with 40 CPR. 63, Subpart N -

National Emissions Scandards for Chromium Emissions fiom Hard and 

Decorative Chrome Electroplating and Chromium Aaodizing Taub 

EPA Methods 1-4 and 306 

September 21, 2005 

Joseph Villareal 

Gregory Chleborowicz - Proj~ manager 

Mr. Marcus Hatc:b -lEPA 
ENCBRO PLATING, INC. 

Melrose Park, IL 

1.0 SUMMARY OF RESULTS 

RMCE INC-EAsT COAST Oma 

Ploject#200S-13084 

The results of the emissions retesting performed on the large chrome tank S1aCks are presented in Table 2-1. Detailed results 

of aU of the testing compJeted on this location are located in Appendis A. The field data and the analytical results are 

presented in Appendix B and C, respectively. Calibration sheets and equipment performance checks are presented in 

Appendb D, alons with the chain of custody. 

A cyclonic flow check was performed at the sampling location to detenn.iJle the existence of abnormal flow. The observed 

average yaw angle for scrubber 2 was 1.2°. Section 2.S of EPA Method 1 indicates that a sampliDg location with an average 

yaw angle of S 20° is acceptable. As indicated by the average of the three test runs, the concentrations of the chromium 

emissions were below the MACT regulation standards ofO.OU mgIDSCM for composite mesh pad scrubber systems on hard 

chrome plating tanks. 

Loeatfoa' 

Scrubber 2 

TABLE 2-1 

SUMMARY OF TOTAL CHROMIUM RESULTS 

ENCBRO PLATING, INC. 

September 21, 2005 

Teat'Pmmeter RalaJt" " 

' .. -

.',', \ " . SiM:dffatii)lt 

mglDSCM 0.006 S 0.015 mglDSCM for bard chrome plating 

Flow rate DSCFM 18)67 sources 
ENCHRO PLATING, INC. 

Melrose Parle, n. 

3.0 TEST EQUIPMENT AND PROCEDURES 

RMCE INC-EAsT COASTOmCE 

Project #2005-13084 

The test program includes the measurement of total chromium stack emissions. This testing will be conducted for verification of 

compliance status with 40 CFR 63, Subpart N -the specification is O.OlS mgIDSCM of total cbromimn for each plating tank. The 

methods to be preformed conform to the requirements ofCFR; Title 40 Part 60, Appendix A and EPA Test Methods 1.2, 3, 4, 

and 306 (CFR; Title 40 Part 60. Appendix A). The equipment and procedures RMCEINC uses in meeting these requirements are 

described below. 

3.1 Total Chromium - EmJssioDS Testing 

Sample Collection. Samples are withdrawn isokinetically from the source using a modified EPA Method 5 sampling train. 

The sampling ttain consists of a glass nozzle. an unheated Teflon probe with a Type S Pitot tube attached, Teflonjumper, four 

chiDed impingers, and a metering console. The first and second impinger contain 100 ml of a 0.1 N sodium hydroxide 

(NaOH) solution, the tirlrd remains empty and the fourth contains pmvcighed silica gel. 

Each run is a minimum of two houn in duration with a minimum sample volume of 60 dIy standard cubic feet. Each of the 

points is sampled for the appropriate times, resultiDg in net nm times of 120 minutes. RUDJ will be numbers consecutively 

with the unit designation, method and run number (ex. Stl-M306-01 and Sa-M306-01). Field blanks and a reagent blank will 

be coUected and aualyzed per EPA Method 306. 

Since each set of two scrubbers vent through one duct to the atmosphere. aU the scrubbers and aU of the tanks will be operated 

simultaneously but each ofthc two ducts/stacks is tested individually to filcilltate as close to normal I maximum production as 

possible. 

Sample Recoyery. The reagents are returned to the original bottles, weigh~ the weights recorded on the labels, and the 

liquid levels, marked. The silica gel is retmned to the original container. weighed, and the weight recorded on the label. The 

volume of water vapor condensed in the impingers and the volume of water vapor collected in the silica gol is summed and 

entered into moisture content calculations. 

The nozzle. probe and connecting tetIon is rinsed with NaOH into the original container. The first, second and third impingen 

are alSo rinsed with 0.1 N NaOH and added to the original reagent jar. . 

Sample Analyses. The amount of condensate collected in each train is used to determine the moisture content of the flue gas. 

The sampJe (container 1) is analyzed for total chromium utilizing inductively - coupled plasma - mass spectroscopy (lCPMS). Samples are collected, a chain of custody tilled out, and the samples shipped or driven directly to Environmental 

Monitoring & Tecbnology, Inc. (EMT. Inc.) after the test project is complete. All QAlQC data from this analysis will be 

provided by EMT, Inc. (8 NELAP Certified Laboratory). 

4.0 EQUIPMENT CALIBRATION AND QUALITY ASSURANCE 

RMC Environmental. Inc. observes cahDration and quality assurance (QA) programs for aU equipment used in emissions 

measurement. Calibrations are conducted in a manner and at a frequency which meet or exceed U.S. EPA QA specifications. 

The Meterbox, Pitot and nozzle calibrations are included in Appendix . 

Specific quality control (QC) procedures are followed to ensure the continuous production ofusetW and valid data throughout 

the course of this test program. The QC checks and procedures described in this section represent an intep nart of the 

overall sampling and analytical scheme. Strict adherence to prescribed procedures is quite often the most applicable QC 

check. 

The cah'bntion and quality assurance procedures of EPA Methods 1-5 will be followed throughout the test program. 
ENCBRO PLATING, INC. 

Melrose Park, n. 

RMCE INC·EABr COABl' Oma 

Project #2005-13084 

Appendix A - Reference Measurement Data With Emission Rate Calculations 
RMC Environmental, Inc. 

Emissions Testing & Consulting 

Plant: EnChro Plating Date: 10108105 

Project #: 200&-13064 

location: SCiij~ 

Sample Identification 2·M3Q6-1 

Test Date 09121 /05 

Start 835 

Finish 1037 

Total 120 

Cp Pitot Coefficient (CF) 0.64 

A Area of stack sq. Inches 1017.9 

Pbar Barometric Pressure (in HG) 30.08 

Wm Volume of Condensate (mg) 24.6 

Ts Temperature of Effluent (F) 86.5 

Pavg Average Delta P 0.640 

Pg Static Pressure (in H2O) 1.10 

OH Delta H, Orifice pressure different (in H2O) 0.89 

Tm Meterbox Temperature (F) 79.1 

Vm Volume of sample metered (CF) 63.212 

Y Meter correction factor 1.036 

On Nozzle Dlamater (In) 0.195 

CO2 Percent Carbon Dioxide (%) 1.00 

02 Percent Oxygen (%) 21 .00 

CO Percent Carbon Monoxide (%) 0 

N2 Percent Nillogen ('''') 78.00 

Ms Molecular Weight (wet) (Ibflb-m) 28.81 

Laboratory Resultl 

Total Chrome (mg) 1.33E-02 

Ps Absolute pressure of Flue Gas (In HG) 30.16 

Vwstd Volume of Water Vapor (SCF) 1.16 

Vmstd Voluma of Metered Gas (DSCF) 64.597 

M Moisture (%) 1.76 

Vs Velocity (FPS) 45.56 

Daw Volumetirc Flow (ACFM) 19.324 

Dsd Volumetric Flow (DSCF) 18.488 

Chromium Concentration (mglOSCM) 0.0073 

Chromium Concentration (lblHr) 5.05E-D4 

Isokenetic (%) 99.24 

2·M306-2 2·M306-3 

09121105 09121105 

1055 1315 

1257 1518 

120 120 

0.64 0.64 

1017.9 1017.9 

30.08 30.08 

29.4 29.2 

88 92.1 

0.620 0.650 

1.10 1.02 

0.87 0.90 

83.0 85.8 

63.421 65.196 

1.036 1.036 

0.195 0.195 

1.00 1.00 

21 .00 21 .00 

0 0 

78.00 78.00 

28,n 28.77 

1.29E-02 1.11E-02 

AVERAGES 

30.16 30.16 

1.39 1.38 

64.342 65.808 

2.11 2.05 

44.94 46.18 

19.058 19.587 

18.120 18.492 18.367 

0.0071 0.0060 0.00596 

4.79E-D4 4.13E-D4 4.66E-D4 

100.85 101.08 
ENCHRO PLATING, INC. 

Melrose Park, IL 

RMCE lNC-EASTCOASTOFAa 

Project #200.5-13084 

Appendix B - Field Data Sheets For Total Chromium 
METHOD 1 - SAMPLE AND VELOCllY TRAVERSES FOR CIRCULAR SOURCES 

Plant Name En Chro Plating . Date 09121105 

Sam pUna LocatIon Unit 2 Scrubber Project. 2005-13084 

Operator Gac , of Ports Avallable 2 

8tackType CirGuJar • of Ports Used 2 

8tacilSize llarae Port inside Dlamemr 4 

Lfw Circular Staclt or Duct Diameter 

DIstance to Far Wall of Stack (Lt.) 39.50 in f--LnWDIstance to NHI' Wall of Stack (L",,) 3.50 in V ~ 

! \ - {-t.1w. WI DIameter of 8tacJr (D) 36.00 in 

{-3.t~J2IArea of Stack (A.) 7.07 ft'" v-\ r--

DIstance from Port to DIsturtIances 0 

DIstance U...-......... (8) 76.00 in 

(-MIl 

('8.01 

Dlamellln 

Distance 

DIameters 

Downstream 

Downstream 

U 

(Ao) 

(So) 

jAl 40.00 

2.11 

1.11 dlametare 

diametans 

in 

~ ~~ 

T ,--- Down streom Number of Traverse PoInts Required 

Mlnlmwn Number of' t 

Disturbance Dlametento A Flow Disturbance Traverse PoInts 

Up Down PartIculate Velocity , P Measurement 

Stream Strum Points PoInts ~ Site 

2.Q0...4.99 0.50-1.24 24 16 

5.00-5.99 1.25-1.49 20 16 t 6.0~.99 1.50-1.74 16 12 

7.00-7.99 1.75-1.99 12 12 B 

>-= 8.00 >=2.00 8or1~ 8or1~_ 

Upstream Spec 24 16 

Downstream Spec 24 16 ~ceo,," Traverse Pta Raqulr.d 24 16 "-.. D;st~bon-ce 

.' Chock MInimum Numb« rA PoInts for the Upslnlem 

and Downstream concfiIfans. then &ISO IfIo /artest. Number of Traverse PoInts Used2 8 for Circular Stadca 12 to z.41nchas 2 Parts by 12 Across 

12 far Clrc;uIat Stadia CMIt 24 Inches 24 PlaUsell 24 Required 

[.,J ParClculate [J Velocity 

Traverse PoInt locations 

Leadoa afT_neP ...... CIrcaIar .... Fraction DIstance DIstance 

'navcno rP_licooISlacft~&_:racid .. WallIDT_PW.) Traverse of from Incfudlng POInt Numl .. r alT~ Pod. 011 a I>iams:W Point Stacir Inside Nipple Numb ... 2 4 Ii II t. II 

1 .146 .06'7 .04-t .031 .026 .0%1 Number DIameter Wall Length 

z .854 .150 .1'" .1115 .1J8Z .067- In in 

J .750 .l96 .194 .1-46 .Jl8 1 0.021 6/8 4218 J .!J,u .7~ ..121 .UAi .177 

5 .• s. .677 ..J.U .l5O 2 0.067 23/8 5718 

6 .95 .1106 .691 ..156 3 0.118 42/8 76/8 7 .8H .77-4 ,6.U 

4 0.1n 6318 97/8 • .9Ci8 .854 .750 

, .918 JI2.J 5 0.250 9 124/8 

10 .97-4 .lSI 8 0.356 127/8 16318 11 3» 

U 979 7 0.644 231/8 265/8 

8 0.750 27 304/8 

9 0.823 29518 331/S 

10 0.S82 316/8 35218 

11 0.933 335/8 371/8 

12 0.979 35218 386/8 

Enchro Plating - M1 - Circular Page 1 Printed 1018/2005 

V1.1S 
METHOD 2· DETERMINATION OF STACK GAS VELOCITY AND VOLUMETRIC FLOW RATE 

PfantName En Chro Plating Date 09fl1Al5 

8amDUna Location Unit 2 Saubber Project. 2005-13084 

Operator Gee " or Ports Used 2 

Stack~ CiR:u1ar PItOIldentlflcatlon M5-11-02 

Pilot Leak Check 0 I PreTest L [,,] 1 POlitTest PIlot Coeftk:lent (CJ 0.84 

8tact Dtmenstons Velocray Traverse Data 

Diameter or i.enath or Stack (D) 36.00 in Run Number U2·M3Q6.V1 

lMdth or StIM:k (W) in Runnme 

Area or stack (As) 7.07 nz Traverse Velocfty Stack Local 

Point Head Temp Velocity 

Pressuru (~) (t.) (vsll 

Barometrtc Pressun (P.,) 24.68 inHg ln~ ~ ftIaec 

StaIIc Pressure (P..J 1.10 InHzO A-1 0.60 84 48.6 

ADsoCute stack PnssUre (P.) 24.78 InHg A-2 0.82 84 49.4 

A-3 0.58 84 47.8 

8tac:k Gas Composblon A-4 0.80 84 48.6 

Composlllon Data:1 AdUaI [,,] EstImated 11 A-5 0.63 84 49.8 

Carbon Dtoxlde Conc.ntndlon (%CO,) 1.0 % A-6 0.61 84 49.0 

OXygen Concentrallon (%O:r) 20.0 % ~7 0.65 84 SO.6 

Carbon MonoJdde Concentralion (%CO) 0.0 % M 0.64 84 SO.2 

Nitrogen Conctrdndfon (IWoNz) 79.0 % A-9 0.67 84 51.4 

Stac:t Moisture Content (a..> 2.000 A-10 0.62 84 49.4 

Stack Dry MofecuJar Welght CM.t) 28.96 lb.1b-moIe A-11 0.60 84 48.6 

Stack Wet MolecUlar Welght (M.) 28.74 IbAb-moIe A-12 0.59 84 48.2 

8-1 0.59 84 48.2 

R.esuIts B-2 0.61 84 49.0 

Avg8tadc Gas Velocity (va) 49.6 ftIsec B-3 0.63 85 49.9 

Avg Stack Dry S1d Flow Rate (Clad) 993688 dscMu' B-4 0.80 85 48.7 

Avg Stack Dry Std Flow Rate CQ.) 18561 dscfhni'l B-5 0.87 ·84 51.4 

Ava Stack Wet Flow Rate (a..) 21046 ascfhnin B-6 0.68 84 51.0 

8-7 0.65 84 50.6 

Stack Cross 8edfon 8dtemaIJc B-8 0.64 84 50.2 

PI. = DWfr<u hlr RedangUIar Stadca 

As = (K(OlZ)2)JK., for Circular Stacks 

wh."., Ku :: 1 for metric units 

wh."., K.,:: 144 (,,"2m; for English units 

p. :: Pilar + P.J13.6 

%N2 = 100· %C02· %02 • %CO 

Md:: .44{%CO:z) + .32(%02) + .28(%Nz + %CO) 

M. = Md(1 • Bw.) + 18Bw. 

(.lP) 112 ~_ '" 1/,,E(.lp Ia, 

Enchro Plating - M2 

B-9 0.68 84 51.0 

8-10 0.58 84 47.8 

8-11 0.57 85 47.4 

8-12 0.57 85 47.4 

Average' 0.79 84 

PI_ "'port tho 8VIf1tG. 01 the 5qW1l'& toOCs of 

.lP.or, (,»)"l_o ,,~I'i 

Formulas Used 

TI(,,' = lInD. + Tu 

whent T u = 273 OK for metric units 

wh."., Tu:= 460 OR for Eng/ish units 

v." K"Cp(.lp)IIl.,g (f .. WI'I~.MJ)11l 

wh."., Kp = 34.97 fer metric units 

whete Kp .. 85.49 for EngIitIh units 

QId" 3600(1 • B..)vsA.(T sJT 1(1YII1)(PslPs1d) 

wh."., T sill = 293 OK, Pili! = 760 mm Hg, for metric units 

wh."., T sat = 528 DR. PI1d :: 29.92 in Hg, for Engl18h units 

I 

Page 1 Printed 10/812005 

V1.1S 
METHOD 3 - GAS ANALYSIS FOR THE DETERMINATION OF DRY MOLECULAR WEIGHT 

Plant Name En ChIo Platina Date 09121105 

Samplll'lfl Locallon Unit 2 Scrubber Project" 2COS-1301W 

()per@tor Gac tI of Porta Used 2 

Fue'Type N/A I MInImum FU1II Factor 1.600 I Maximum Fuel FactorI1.800 

Orsat Leak Check [-!I I PreTest I 

Run Number U2-M306a-01 

Sample Carbon Carbon 

Analyals Dioxide Oxygen Monoxide 

Time Volume Volume Volume 

(Vcaa> (Vm) (Veo) 

hh:mm ml mJ mI 

FYRITE 1.0 21.0 

1.0 21.0 

1.0 21.0 

Result. [,,-wrages 

Average Calculated Fuel Factor (F.) .... 

Averaoe Excess Air (%EA)_ 

Run Number U2-MS06-2 

Sample carbon carbon 

Analysis Dioxide Oxygen Monoxide 

Time Volume Volume Volume 

(Vcaa> (Ve»,) (vcol 

hh:mm mJ mJ mI 

FYRITE 1.0 21.0 

1.0 21.0 

1.0 21.0 

Resu'" I Averages 

Average Calculated Fuel Factor CFJ.., 

Average Exceu Air ("EA)_ 

Run Number U2-M306-3 

Sample Carbon Carbon 

Analyal. DioxIde Oxygen MonoxIde 

Time Volume Volume Volume 

(Vee»> (Voz) (Vco) 

hh:mm ml mJ ml 

FYRITE 1.0 21.0 

1.0 21.0 

1.0 21.0 

Results Averages 

Average Calculated Fuel Factor (F.)~ 

Average Excess Air ('I&EA)..., 

Fuel Factor Fo 

Fuel Type Minimum Maximum 

Coal, Anthracite 1.018 1.130 

Coal, Ugnlte 1.018 1.130 

Coal, Bltumlnoua 1.083 1.230 

011, Distillate 1.260 1.413 

Oil, Residual 1.210 1.370 

Ga., Natural 1.800 1.838 

Gas, PropaJ\a 1.434 1.588 

Gas, Butane 1.405 1.553 

Wood 1.000 1.120 

Wood Bark 1.003 1.130 

Enchro Plating - M3 - Orsat 

~ I PostTest Oraat identification I 

Oaa Analyals Data 

Run Start Time .8:35 Run Stop Time 10:37 

Carbon Carbon DIy Molecular 

Dioxide Oxygen Monoxide Nitrogen MolfICUlar Weight 

Cone. Cone. Cone. Cone. Weight Deviation 

~ (%Oz) (%00) ("'Nz) (M..) (.1M..) 

fIM*'It peRent pen:ert percent Ib.1IHnoIe IbIItHnoIe 

1.0 20.0 0.0 79.0 28.96 0.00 

1.0 20.0 0.0 79.0 28.96 0.00 

1.0 20.0 0.0 79.0 28.96 0.00 

1.0 20.0 0.0 79.0 28.98 

0.900 Mo'flCUlar WI Deviation c 0.3? Itl_ 

2338.4 percent Fuel Factor In Handbook Range? ItJ 

Oaa Analy_sls Data 

RLm Start Time 10:55 Run Stop Time 12:57 

carbon 

Dioxide Oxygen 

Cone. Cone. 

(%COz) ("'Oz) 

pen:ent percent 

1.0 20.0 

1.0 20.0 

1.0 20.0 

1.0 20.0 

0.900 

2338.4 pen:ent 

Gaa Analysl. Data 

Run Start Time 

Carbon 

DIOXIde Oxygen 

Cone. Cone. 

(%COz) (%Oz) 

percent pen:ent. 

1.0 20.0 

1.0 20.0 

1.0 20.0 

1.0 20.0 

0.900 

2338.4 pen:ent 

Page 1 

Carbon Dry Molecular 

Monoxide Nitrogen Molecular 

Cone. Cone. Weight 

(%CO) ("'Nz) (M..) 

pen:ent pen:ent IIktIHnole 

0.0 79.0 28.98 

0.0 79.0 28.98 

0.0 79.0 28.98 

0.0 79.0 28.98 

Molecular WI DevIation c 0.31 

Fuel Factor In Handbook Range? 

13:15 Run Stop Time 

cartIon DJy 

MonoxIde Nitrogen Molecular 

Cone. Cone. Weight 

(%CO) ("'Nz) (~ 

pen:ent ~. IbIIb-moIe 

0.0 79.0 28.98 

0.0 79.0 28.98 

0.0 79.0 28.98 

0.0 79.0 28.98 

Molecular WI DeviatIon < 0.3? 

Fuel Factor In Handbook Range? 

Formulas Used 

%~=Vcoz 

"40z sa VOl - Vcoz 

'l6CO = Veo - VOl 

"'Nz = 100 - 'l6~ - 'l60z - "'CO 

WeIght 

Deviation 

(AM..) 

IbmHnoIe 

0.00 

0.00 

0.00 

Itl 

[of] 

15:18 

MolfICUllllr 

WeIght 

Deviation 

(AM..) 

IbAb-moIe 

0.00 

0.00 

0.00 

[] 

[J 

Mof:: .44('l6COz.)+ .32(%0z)+ .28(e"Nz + %CO) 

lM.. :: Mel - MdIoV 

Fo = (20.9 - %Oz -.5'l6CO)/('W.CO-z + %CO) 

%EAa100~Or.s'loCO)l(.264'l6NOr("0r.S%CO) 

I 

J 

Printed 10/812005 

V1.1S 
METHOD 4 - DETERMINATION OF MOISTURE CONTENT IN STACK GASES 

Plant Name 

sampllna LocaIIon 

O~rato, 

81ackJDe 

Train Leak Check 

Run Number 

Total Meter Volume 

Avg Meter Temp 

Avg Stack Temp 

Contents 

final Value 

lnIIfal Value 

Net Value 

Total VolUme 

Total WeIgh! 

Std Meter Volume 

Calc Moisture Content 

RunNumller 

Total Meter Volume 

AY8 Meter Temp 

Avg Stack Temp 

Contents 

FJnaJVaJue 

InHfaJ Value 

Net V ..... 

Total Volume 

Tocal WeIght 

SId Meter Volume 

Calc Moisture Content 

. 

Run Number 

Total Meter Vorume 

AVO Meter Temp 

Ava Stack Temp 

Contents 

FJnalVaJue 

Initial Value 

Net Value 

Total Volume 

Total Wefght 

Ski Meter Volume 

caJc Moisture Content 

Enchro Plating - M4 

En Chro Platina Dale 09TJ1JD5 

Unit 2 Scrubber P~ect# 2005-13084 

Gac " of Ports Used 2 

Circ:uJar Miler 80. Number 05 

["'] I PreTest I ["'] I PosITest Meter Cal Factor m 1.038 

U2-M306-1 

(VnJ 63.212 

(tn.>- 79 

(t.~ 87 

bnplnpr1 

mI 

01 

(V,).(W,) 108.00 

<V!).(W,) 100.00 

(v,J.(W,J 8.0 

(Vi} 13.00 

(Wi} 11.60 

lVllltsW 64.622 

~calr:Jl 1.8 

U2-M306-2 

(V",) 63.421 

~ 83 

<t.>av 88 

Impllller1 

mI 

01 

(V,).(W,) 108.00 

(V~.(W,) 100.00 

NJ.cWn) 8.0 

!VI) 18.00 

(We) 11.40 

(V~aol 64.370 

(BwJ 2.1 

U2-M308-3 

(Vm) 65.196 

ttn.>- 86 

(t.)wg 92 

Impfnger1 

mI 

OJ 

(V,).~,) 109.00 

(vJ.~,) 100.00 

NJ.fNn> 9.0 

(ViJ 16.00 

~~ 13.20 

(VmrSfIIJ) 65.833 

Ce...) 2.0 

Moisture ContenI Data 

Run stall11me1 8:35 Run Stop TIme 10:37 

dcf BaromeCrtc Press. (Pb) 30.08 In Hg 

OF StacIe Stade Press. (P..J 1.10 inH~ 

"F Avg Ortllce Press. (Mi).,g 0.89 in H20 

Implnge,Z Imlllnler3 Implnfer4 fmplnger' Implnger. fm~naer7 

mf m 9 mJ mI mI 

01 Sil Gel 

105.00 . 161.60 

100.00 150.00 

5.0 11.6 

RuuIts 

mI Water Vol ContIMaStId (V.,.w 0.612 ad 

9 water Vol w.lthed tv .. an) 0.547 ad 

dad Sat. Moisture ContenI IA .\ 4.2 % 

% final Moislure Content (B..) 1.8 % 

Moisture Conleld Data 

Run Stall Tbne 10:55 Run~TIme 12:57 

del Barometric Press. (I\) 30.08 inHg 

OF 818ck 8taIIc Press. (P..J 1.10 InHzO 

"F Avg ormce PIUs. (~>.w, 0.87 InHzO 

ImplngerZ Implnaer3 ImPinaer4 Implnaer' ImJ)lnlle, • Implnger7 

mI ml 9 ml mJ ml 

01 SIIGeJ 

110.00 161.40 

100.00 150.00 

10.0 11.4 

Results 

mI WIder Vol Condensed (\[~~) 0.847 ecf 

9 Willer Vol WeIghed (V ... Anl 0.538 ad 

dscf sat. MoIstUre Content IA 4.4 % 

% FInII Moisture Content Ca.) 2.1 % 

Moisture Content DaIa 

Run Start TIme 13:15 Run Stop TIme 15:18 

dcf Barometrfc Press. (P,) 30.08 inHg 

OF Stack StaIIc Press. (P..J 1.02 in H20 UF Avg OrUlce Press. (Milwt 0.90 inHzO 

Impfn,erZ Implnger3 impinge," ImMerS Im"",er. fmplnaer7 

mI mI Jl 

01 Sil Gel 

107.00 163.20 

100.00 150.00 

7.0 13.2 

Results 

ml Water Vol Condensed 

9 Water Vol WeIghed 

dacf sat. Moisture Content 

% FInal Moisture Content 

Page 1 

mI rri 

(VWC(aI) 0.753 

N ... IIIIl) 0.622 

(a._,) 5.0 

(e...) 2.0 

mI 

I 

sc:f 

sc:f 

% 

% 

Printed 101812005 

V1.1S 
rSOKrNETIC SAMPUNG DATA 

PlanlName En CM Platina 

Sampling Locctlon Unit 2 Serubber 

Operator Gac 

tI 01 Polnb Actosa 12 

Ideal Nozzle Dlametv and lsal<lMtlc Feetor Setup 

PItaC Tube Coeftlclent (c,) 0.840 

Ava Stack Temp (IJ 84 ·F 

Ava au Meter Temp (W 70 OF 

DH • 0.76 SCFM (~O) 1.70 InHP 

Avg PItot Tube Dtff. Preuure (~ 1.70 InHp 

StacIe MGlstura Contw1t (8..) 1.8 ~ 

SbIck Dry MoIec:u .... WeIght (M..) 28.96 IbIIHnalo 

EstImated Oriftce Flow Rate (Q.) 0.750 acfm 

DP 10 DH Isoldnedc Factor . (I<) 1.39 

Pressures 

Barometric Pressure (f\) 30.08 In HI 

SI.etc Static Pressure (PoIIIIJ 1.10 In Hz{) 

Abaolute S18ck Prosun CPS> 30.18 In HI 

Abaol_ Meter Pressure (P.,.) 30.21 In HI 

DlyGu De:Itnd Ar:tuIII 

Traverse Sampling Clock MfIter VeIac:Ity OrIfIce 0Iffice 

PoInt. TIme nme Readfng Held .Uf ~ 

(8) (V.) ("P) (~ (.Uf) 

min hh:mm:ss rr In Hz{) In Hz{) In Hz{) 

A-1 0.0 8:35:00 538.900 0.580 0.808 0.810 

A-2 5.0 8:410:00 539.400 0.820 0.864 0.860 

A-3 10.0 8:45:00 542.000 0.810 0.850 0.850 

A-4 15.0 8:50:00 544.560 0.820 0.884 0.880 

A-5 20.0 8:55:00 547.160 0.820 0.884 0.880 

A-8 25.0 9:00:00 549.850 0.830 0.878 0.880 

A-7 30.0 9:05:00 552.450 0.820 0.884 0.880 

A-8 35.0 9:10:00 555.000 0.84D 0.892 0.890 

A-9 40.0 9:15:00 557.600 0.830 0.878 0.880 

A-10 45.0 9:20:00 560.350 0.810 0.850 0.850 

A-11 50.0 9:25:00 583.000 0.860 0.919 0.920 

A-12 55.0 9:30:00 585.420 0.850 0.905 0.900 

B-1 60.0 9:37:00 588.210 0.830 0.878 0.880 

B-2 85.0 9:42:00 571.110 0.840 0.892 0.890 

B-3 70.0 9:47:00 513.340 0.860 0.919 0.920 

B-4 75.0 9:52:00 578.520 0.870 0.933 0.930 

B-5 SO.O 9:57:00 578.890 0.860 0.919 0.920 

8-8 85.0 10:02:00 581.850 0.680 0.947 0.940 

8-7 90.0 10:07:00 584.200 0.870 0.933 0.930 

B-8 95.0 10:12:00 587.850 0.680 0.947 0.940 

8-9 100.0 10:17:00 590.000 0.870 0.933 0.930 

8-10 105.0 10:22:00 593.~ 0.660 0.919 0.920 

8-11 110.0 10:21:00 595.450 0.820 0.864 0.860 

8-12 115.0 10:32:00 591.880 0.810 0.850 0.850 

LastPt 120.0 10:37:00 600.112 

LasIPl 120.0 10:37:00 600.112 

Average Values 0.64 I 0.89 I 

Enchro Plating - M5 - Run 1 Page 1 

DGe 8121121lO5 

ProJect. 2005-130&4 

Run. U2-M308-1 

tI 01 Pwta Used 2 

Samplln, E~ulpment 

Meter. 05 

MeterbOlI CaL FacCDr (Y) I 1.036 I 

Nozzle. 

Actual Nozzle Dt.meIer (D,.) 0.1950 In 

Req. Nozzle DIameter ~ 0.1799 In 

Prabe ., Langth 40.00 It 

Unar IIatertII Teftan 

Sample cae I Oven. 

ImJIlnaer cae. 

.1V. lKkChecks 

Pre 0 tt'/mln (I 15 In Hg 

MId rlmln .. InHg 

Post 0 tt'lmln CD 10 InHO 

.1V. < 0.020 ft-/min 1tJ LHk Check OK? 

PlIDtOK? 

Iktcr 

Stack Inlet 

Temp Temp 

(tJ <Y 

"F DF 

84 72 

85 72 

B5 75 

B5 75 

85 77 

88 78 

88 79 

88 80 

88 81 

88 81 

88 82 

~ 83 

~ 84 

88 84 

88 85 

87 88 

87 88 

87 87 

87 88 

87 88 

88 88 

89 88 

89 90 

89 91 

87 I 83 

1 79 

21 OrsatOK? iii 

..... 1mplngM' 

Cutlet Fl1ter Exit Pump 

Temp Temp Temp Vacuum 

(~ 

"F "F "F InHg 

12 45 3.0 

12 42 3.0 

13 42 3.0 

74 43 3.0 

75 43 3.0 

75 43 3.0 

75 43 3.0 

75 43 3.0 

75 43 3.0 

75 43 3.0 

75 43 3.0 

78 44 3.0 

78 44 3.0 

78 44 3.0 

78 44 3.0 

78 44 3.0 

77 45 3.0 

77 45 3.0 

77 45 3.0 

77 45 3.0 

77 45 3.0 

78 45 3.0 

78 45 3.0 

79 45 3.0 

Maximum Vacuum 3.0 

78 I 44 

Prin1Bd 1018l2D05 

V1.15 
ISOKINEnC SAMPUNG DATA 

Ptanttwne EnCltf1)_~ 

Locdon Unit 2 Sc:rubbor 

Operator Gac 

• of Paints Acfou 12 

ldul Nozzle Dkmetar ~ Isot<lntdlc Factor Setup 

PIlat Tube CoeftlcJent (c..> 0.840 

Ava Stack Temp ll.) 84 ~ 

Avg Gu Meter Temp t\,) 70 of 

DH e 0.75 SCFM WIG> 1.70 InH~ 

Ava Pltot Tube Dtfr. Preuw. (4P..g) 1.70 InHP 

StKtt MoIWn Conant (8.,J 1.8 'K 

Steck Dry Molecu .. WIlfaht <M.) 28.98 IbIIHnaIo 

EatImIded 0rffIce Flow Rate (0.,) 0.527 acfrn 

DP to DH laoldnellc r:.:tor 00 1.39 

PnIssunIs 

BanImetJfc Pressure (P.,) 30.08 InHg 

Stack Static Pressure (P.-)- 1.10 InH~ 

AbaoIuw Stack Pres .... (PJ 30.18 InHo 

Absolute M .... Preaauro (P~ 30.21 In HI 

DryGu Dahd Actual 

Traverse Samplfng Clode Metar Velocily Ortftce 0riIIc:e 

PoInt. nme TIme Reacllng Had .iH .1H 

(9) (Ve) (4p) (Mf) (Mf) 

min hh:mm:ss It" InHP InHP InHzO 

A·1 0.0 10:55:00 600.900 0.S90 0.822 0.820 

~2 5.0 11:00:00 603.440 0.630 0.878 0.880 

A-3 10.0 11:05:00 605.950 0.830 o.m 0.880 

M 15.0 11:10:00 808.850 0.850 0.905 0.910 

M 20.0 11:15:00 811.500 0.820 0.884 0.880 

MJ 25.0 11:20:00 814.000 0.650 0.905 0.800 

A·7 30.0 11:25:00 817.000 0.660 0.919 0.920 

MJ 35.0 11:30:00 819.550 0.870 0.933 0.930 

A-8 40.0 11:35:00 822.320 0.660 0.919 0.920 

A-10 45.0 11:40:00 625.000 0.870 0.933 0.930 

A-11 50.0 11:45:00 671.750 0.820 0.884 0.860 

A·12 55.0 11:50:00 830.200 0.S90 0.822 0.820 

8-1 60.0 11:57:00 633.000 0.510 0.794 0.790 

8-2 85.0 12:02:00 835.860 0.530 0.738 0.740 

a.3 70.0 12:07:00 838.050 0.600 0.838 0.840 

s.4 75.0 12:12:00 640.860 0.830 0.878 0.880 

8-5 80.0 12:17:00 843.000 0.640 0.892 0.890 

~ 85.0 12:22:00 646.320 0.870 0.933 0.930 

B·7 90.0 12:27:00 848.780 0.640 0.892 0.890 

B-8 95.0 12:32:00 651.350 0.850 0.905 0.910 

8·9 100.0 12:37:00 654.000 0.820 0.884 0.880 

8-10 105.0 12:42:00 668.870 0.600 0.836 0.840-

8-11 110.0 12:47:00 659.320 0.590 0.822 0.820 

8-12 115.0 12:52:00 862.000 0.600 0.838 0.840 

last Pt 120.0 12:57:00 684.321 

Final Value 120.0 12:57:00 664.321 

Average Values 0.82 I I 0.87 I 

Enc;hro Plating· M5 • Run 2 Page 1 

o.t. 81211ZOO5 

Pro~' 2DDS-130&4 

Run. U2-M306-2 

f# 01 Parts Uaed 2 

Sampllnt E 

Meter. 05 

IIeCerbox Cal. Fector (Y) 1.038 

Nozzle. 

Actual Nozzle Dtanet8r (D"J I 0.1950 In 

Req. Noule DfMIeCer COn) I 0.1508 In 

Pralle tI' Length 40.00 It 

LIner ........ Teftcn 

Sample Cae/OwM. 

Cue. 

.1V .. LHkCbecb 

Pre 0.001 ~lmln • 1S In HI 

Mid 0 ft"1mIn _0- 10 In HI 

Post 0.002 It"Imln • 10 InHo 

AV"" < 0.020 n*/mIn I2J LeU Check OK? 

PltatOK? 

.... 

Stack InJeI 

Temp Temp 

(IJ ty 

~ of 

81 80 

88 81 

88 83 

88 83 

88 85 

88 88 

85 87 

81 88 

87 88 

88 88 

88 89 

88 89 

88 89 

89 89 

89 90 

87 90 

88 91 

90 91 

91 91 

91 92 

91 92 

91 92 

91 92 

91 92 

88 I 88 

I 83 

~ orsatoK?1 ~ 

.... IInpllluw 

0UtI8t FIlter ExIt Pump 

Temp Temp Temp Vcuum 

tt-) 

~ ~ ~ In H, 

75 47 3.0 

78 45 3.0 

76 44 3.0 

78 44 3.0 

78 43 3.0 

71 43 3.0 

71 44 3.0 

7B 44 3.0 

7B 44 3.0 

71 43 3.0 

71 43 3.0 

71 43 3.0 

77 44 3.0 

7B 44 3.0 

78 42 3.0 

18 41 3.0 

78 42 3.0 

79 43 3.0 

79 43 3.0 

79 44 3.0 

79 44 3.0 

80 43 3.0 

80 44 3.0 

80 43 3.0 

Maximum Vacuum 3.0 

.78 I I 

I 

44 

Printed 10I8l2005 

V1.1S