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# AppendixE Calibration DataControl Module Project: Date: 

### Technician:

M5APR.WQ1 

### C-4 Routine 3/15/2005 NRS Leak checks Negative- ok Positive -- ok 

### >SW.C. > in.Hg 

### Barometric Pressure Previous Y -- Previous Delta H --- 29.31 1.0040 2.2168

### Routine 

### Dry Gas Meter Calibration Control Module Number: 

### _C."· 

# :...·_'1'--- Date: 3 

### -!S:-Cl'S

**Techrudan:-L~~~s~-------------** leal< Checks Positive cit_ Negative 

## "k Bammetlic Press.: ., 5 in. W.C. Previous Y: L00'-!0 15in.Hg Previous&i: 

### -z_.z_\.1.!;\i

### Control Module Project: 

### Dale: Technician: C-3 Routine 

### 41212005 NRS Leak checks

### NegativePositiveok ok Barometric Pressure 

### Previous Y- >5 W.C. Previous Delta H - 

### > in.Hg



### 1.0024

1.0024

1.0020 29.22 0.9999 1.8261

1.8568

1.8655

### Routine 

# BARR Dry Gas Meter Calibration Control Module Number: 

# t · 3 Date: 

## 7£<1-2. 

# -osTechn?cian:



# ~At:'>..L)/l.=S'------- Orifice Dry gas WetTest Leak Checks Positive 

## •'k. Negative oiz_ WetTest 

### Barometric Press.: 

# 2 <J, 2 2_ 

### 5 in. W.C. Previous Y: • 

### 'i''t 9 "( 15 in.Hg Previous Ll.H: Elapsed Meter Orifice

### Project Name: 

### MiiUltac Module Number: .;;;C:..;-4'-::-:;-:---:::::- Date: 26-Apr-05 Tech:.;;;JMM==---- 

### EPA M5 POST TEST METER CALffiRATION

Nominal sample conditions

Delta H: L65 W.C. Vacuum: 5 in. Hg 

### Project No.: 23/69-927-002 Barometric 

### Pressure: --:-;:c;?:2;:8-:::6c.4 Previous Y : 

### 1.0055 Previous Delta H : --::-2. 7 

### 197::;:::4-

Pre cal +5% 

### Pre cal- 5% Within 

### 5% YIN 1.0558 0.9552 YES 

### 2.3073 

### 2.0875 YES

# ··:cBARR EPA MS POST TEST METER CALIBRATION

Project Name: _,!"->/)L-'-'"''-'"'--'-''kc:. w<c..'
__ _ 

### vlodule Number: _G
__ -_'-_,_{ ____ _ Date:



# ---~.1"-'f"-'J t.,_< ,_,/o'--' 

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PTC Template Nominal sample conditions Dl

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### e 

### ta H:
. ..,. -· • 

## w.c. Vacuum:

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### in. 

### Hg Project No.: Barometric Pressure: )'revious 

### Y : 

# :) 3/r, '1- 

# 1) 7-t:cCL 

## ' 

# """" ,J ,) '\t"-' L 

### I C[J 

# s-.._) Previous Delta H : 

## .J , 

## I 

# ? 7 

## t--/Project Name: Minntac 

### Module Number:..:C:...-=,3::7-:---::--oDate: 26-Apr-05 Tech: JMM 

### EPA MS POST TEST METER CALIDRATION

Nominal sample conditions

Delta H: 1.05 W.C. Vacuum:
_ _::2c::2
__ in. Hg Project No.: 23169-927-002 Barometric Pressure: 28.64 Previous Y : 

### _...:1.::.0:..:0col.::6_ Previous Delta H : _...:1.::.8e.:3col.::8_

Pre cal+ 5% 

### Pre cal- 5% 

### Within 5% Y !N 

### 1.0517 0.9515 YES 

### 1.9234 1.7402 YES

## EPA M5 POST TEST METER CALIDRATION 

# BARR

v!odule Number: 

### _.._'_-_7;;>..-
__ _
Tech:



### J~

PTC Template Nominal sample conditions I -·- 

### Delta H: I ' 

# a J 

## w.c. Project No.:

# BARR Engineering Company

Pitot Tube Number:



## ~ 

## 7- 

# I \ 

### Length: Function: M-5 Probe 

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### ~ES (go to 2) D NO (go to Ia) 

## '

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# *

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# ffil.._:rES (go to 3) D NO (go to 2a)

3. Are legs of equaJ length?



## ~'.YES (go to 4) 

## D NO (go to 3a) 

# f

**---,-~-.---=<--?----**

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## ~S (goto5) 

## 0 NO (goto4a)



### f----~<~---=<--?-----

5. Does this pitot -tube pass an of the above criteria?
T ectinidan Signature: 

### S-Type Pitot Tube Geometry Check Inspection Date: Technician,_: '-'-'-""'--"'-'""---------

1a. If NO, is ang"Je less than· 10°? D YES(goto2) 

## 0_ NO (discontinue use)



# ....

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3a. If NO, is difference less than 1/8 inch? DYES (goto4) 

## · 0 NO (discontinue use}

4a. If_ NO, are center-lines of face openings less than 1132 inch? D YES(goto5) 

## 0 NO (discontinue use)



# lizJ YES 0NO

. 

# ---

# BARR Engineering Company

Pitot Tube Number: 

# l-Z. lenglh: 

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### Function( M-5 ProbE7 

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## 0 NO (go to 1a)

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## l>lJ YES ( go 10 3) 0 NO {go to Za)

3. Are 11J9S of equal length? 

# D YES(go!o4) 

### ri;j NO (go to3a)**~---;;w~ ~-)-----** 

4. Are center-fines of legs coincident? 

# !2!J YES (go 

### to 5) 

## 0 NO (go to 4a)

### ~----~~**~-)-----**



# s. Does 

# !his pitot 

# tube pass**a~~Aot;e!Ti,·~?** Technician Signature:

# ~f_L_ "" I j S-Type Pitot Tube Geometry Check Inspection Date:

1a. If NO, is angle less 1han 10•7 0 YES(goto2) 

## 0 NO (discontinue use)

I , l I I 

# .... w· ... 

# --J8E3---· _;,.•**~-** 

# .., .. --· I I I - I 

# . - 

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### Use) 

# -V

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# -- --- 

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---- .:::r_

3a If NO, is dilference less U1an 1/8 inch? 

## fil YES (go 

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## 0 NO (discontinue use) IV -£-- 

### d '.

4a lfNO, 

### are cenb,4ines of 

### face openings less U1an 1/32 inc!1? DYES (go to 5) 

## D NO (discontinue use)



# i?3- YES ONO

# BARR PYROMETER CALIBRATION
Pyrometer Number. 

# c:-""

- 

# 'f Date: 

# 0 

# );J:; 

# /o 'f Pyrometer Reference: 

### CL 3C•c 

## -1'-- (t'l?•' 

### F Technician: .I fVV'-- 

## "3 

## o7..:7'ifs
Reference (•F) Reference ("C) Pyrometer 

### L__) 

### 1000 538 

# 1 

# ool 950 510 

## OJ**~I** 900 482 

## Cf 

# o I 850 454**~s** 

## i 800 427**~ul** 

### 750 399 

# 7s-l 700 371 

## /C>i 650 343 

### f., 

# s-> 600 316 

# looi 550 288 

# -ssl 500 260 

# so i 450 232 

## '-1 

# so 400 204 

# 'iol 350 

### 177 

# 3s-o 300 149 

## "3o I 250 121**~** 

## ,;;;-/ 200 93 

## )C 

## I 150 67**/~::,** 

### 100 38 

# i 0 I 50 10 -J_ 

## 2:> 

## ' 0 

### -18 I 

### -50 -46 

# -lit
Notes:

### Pyrometer Number: {_ 

# -3 PYROMETER CALIBRATION

Pyrometer Reference: 

# ll- -]co**-{CkL,~** Date: 

# L)_- .).. 'f- -c'-( Technician:

## --::'r~SL ·

Reference ("F) Reference ("C) Pyrometer 

## C'.f:_) 1000 538 

# qqcr 950 510 

# q 

# so 900 482 

## tfoo 850 454 

# "'f"**~** 

## c:? 800 427 

## 1(-uo 750 399 

# )s;o 700 371 

# 7oo 650 343 

# G)O 600 316 

## c:;CXJ 550 288 

# 5 

# >I 500 260 

### 5o0 450 232 

# 4<;o 400 204 

# Lfoo 350 177 

# 3Y1 300 149 

# > oj 250 121 

# 'Z _')J 200

. 

### 93 

## ')_g.U 150 67 

# i<.J
... 100 38 LO 

# I 50 10 

# -YI 0 -18 

# I -50 -46 .

## -4~

.



### · Notes:

# BARR

REFERENCE STANDARDS Hart Scientific 91 03-A sin A1 8289 Hart Scientific 9140 sin A18086 

### Temperature Calibraion Points Reference Deg F (To} Probe Temp (deg F) Reference Temp (deg R) deg F + 

### 460 Probe Temp (deg R), deg F + 

### 460 Difference (degrees) % DiffAbs. T Is difference less than 1.5% at all measured points?
1700. 1600. 1500 

# "' g. 1400. 

# "**~** 

### 1300. 

# "

.**~** 

### 1200. w 

### !:; 1100 w 

### :;; 1000**~** 

# .. :l 

### 900 : 

## 8**~** BOO • 

# "' w 

## i= 700 600 500 400 

# THERMOCOUPLE CALIBRATION
THERMOCOUPLE ID C-4-0 Cai;Date: 12i22i2004 

# Meter In or Out CALIBRATION TECHNICIAN: JMM TRACEABILITY Report No. A1 80718 Report No. A1 82024 

## 32 212 32 212 32 211 492 672 492 671

0 1 0.0% 0.1% YES DATE LABORATORY 12i11i2003 Hart Scientific 12111i2003 Hart Scientific 400 650 70 400 650 70 

### 398 648 

### 69 860 1110 530 858 1108 529

2 2 1 0.2% 0.2% 0.2%

400 500 600 700 BOO 

### 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Are extrapolated limits less than 1.5%? YES If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR Engineering Company
Thermocouple Number: 

# ..f::r ( <-/- 0 

# f.,+ i e 

# f

Media Sld Used

**D-~** 

### Reference DeaF 

### ITol Reference CorrTemp ldeg 

### Rl deo F 

### + 460 Probe Temo Ideo R Probe Temo Ideo 

### Rl, deg F + 460 Difference (cteoreesl 

### % Diff Abs. T 

### (Renkin)
Diff. less than 1.5"A> 

### at all 

### points Graph Attached E.ldrnpolated Range with Di!f. <= 1.5%

-·Description of the thetrnocouple's function: . 

### 32
. 212 

# ;\) .c ';:) I ;\. 

## i../•1 '} {:,7),



## ""ii ,o 

## 1 I 

# 4'1 '\

. I' 

## t, '7/ 

## 6 

## . I 6.c Q:;' ( 

## THERMOCOUPLE CAUBRATION

T echnichian: 

### _...:<l__:__:.c""'""'c.:.:.
__


### 400



# -
- 

# 4oo

**•·1~o**

**-J-1~-** '.(:<.:.- 

# ¥

,,l 0.?.. ®JNo) @No) 

### 650 Other 

# G 

# s:c .J 

### 70 

### ,b 111o

**S~G** 

### {,!-{ 

# ¥' c,c; II C 

### R" 

# 9'1 -2. 

# I c.<- 0. 

### "2..



### to


# c ... h{

**f!ed~l,** 

## 'i

**/)~!'{ o~+!...+**  **hv~<><o~l'4-**

If not acceptable, desaibe corrective procedures undertaken:

P:\00\02\0EM\Oatasheets\calitmatioo.xls

# BARR

REFERENCE STANDARDS Hart Scientific 91 03-A sin A1 8289 Hart Scientific 9140 sin A1 8086 Temperature Calibraion Points Reference Deg F (To) Probe Temp ( deg F) Reference Temp (deg 

### R) deg F 

### + 460 Probe Temp (deg R), deg F + 

### 460 Difference (degrees) % Diff Abs. T Is difference less than 1 .5% at all measured points?
1700 1600 1500

### ~ 1400 

## •**~** 

# ::! 1300 ::>

### ~ 

### 1200 w 

### §; 

### 1100 w

### ~ 1000**~** n. 

# 5 900 

# " 0**~** 

### 800 w 

### i!: 700 600 500 400 

# THERMOCOUPLE CALIBRATION
THERMOCOUPLE ID C-4-1 Cal; Date: 12i22i2004 Meter 

## In or Out CALIBRATION TECHNICIAN: JMM TRACEABILITY Report No. A1 80718 Report No. A1B2024 

## 32 212 32 212 34 

### 211 492 672 494 671

-2 1 0.4% 0.1% YES DATE LABORATORY 12i11i2003 Hart Scientific 12i11i2003 Hart Scientific 400 650 70 400 650 70 

### 399 650 69 

### 860 1110 530 859 1110 529

1 0 1 0.1% 0.0% 0.2%

400 500 600 700 800 900 1000 11 00 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Are extrapolated limits less than 1.5%? YES If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR Engineering Company
Thermocouple Number: 

## r' 

# L/

- ; '/"\ 

# I r 

# +

1\ile<fia Std Used 

## .D-8' Reference Deg 

### F (To) Reference Corr Temp ( deg R) deq F 

### + 460 Probe Temp (deg F) Probe Temp (deg R), deq F + 460 Difference (degrees) 

### % Diff Abs. T (Renkin)
Oilf. less !han 1.5% at all poinls Graph Atlached Extrapolated Range with Oi!f. 

## = 1.5%

\"L bescription of the thennocouple's function: 

# . 32 

### 212**s.::~-t**

## ~ 

## Lj"/). 

# (..;:17::



# 3'1 :TIT 

# 'i"i t.-f

## ~



# •.1- ·. >fD 

## .<.f 0.( 

## THERMOCOUPLE CAUBRAT!ON

400



## -- 

## '-(CO 

# 'f{., 6 ?>'1'7 

# ¥5t.(

I 6. 

### I**~No)** 

## (9rNo) Date:

# I.J../~ ;;_ 

# /t<j T echnichian: ': 

## t f'v'I.AA

### 650 Other**[:,~** 

# -o 1 (J ,() 

## tqo .:;,-?,15 (;;, !> 

# --e 

# tao/ I I 

### i 

## o 

# 01 0 

## I O.cl O·"Lto


# C-J.,.,I Mod.,/.._ '1 !:>(J,M "X

### ~le.±**ft..._,....,.,,o~r\.o..**

ft not acceptable. describe corrective procedures undertaken:

P:\00102\0EM\Dafasheets\calibrntion.xls

### REFERENCE STANDARDS Hart Scientific 91 03-A s/n A1 B289 Hart Scientific 9140 s/n A1 B086 Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg 

### F) Reference Temp (deg R) deg 

### F + 460 Probe Temp ( deg R), deg 

### F 

### + 460 Difference (degrees) % Diff Abs. T Is difference less than 1 .5% at all measured points? 1700 1600 "' 1500



# ~ 1400 w 

## !§ 1300 >-



### ~ 1200 w



### ~ 1100 w



### ~ 

### 1000 ...J 

## §; 900 

# § 800 il1 

### 700 w I 

### >- 

### 600 500 400 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE ID 

## C-3-0 Cal Date: 12/27/2004 Meter In or Out CALIBRATION TECHNICIAN: NRS TRACEABILITY Report No. A 1 B0718 Report No. A1B2024 

## 20 70 20 70 20 

### 69 480 530 480 529

0 1 0.0% 0.2% 

## YES DATE 12/11/2003 12/11/2003 

## 150 150 148 610 608



### 2 0.3% LABORATORY Hart Scientific Hart Scientific

400 500 600 700 800 900 1000 11 00 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Are extrapolated limits less than 1.5%? 

## YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 

### -20 1200

# BARR Engineering Company
Thennocouple Number: 

# ·tc..**~'-3-D**

Media Sid Used 

## b-ll Reference Deq F (To) ReferenceGorr Temp (deq R) deq F + 460 Probe Temp (deq Fl Probe Temo (deo R), deg F +460 Difference (degrees) % DfffAbs. T (Renl<in)
Diff. less than 1.5% at all points 

### Graph Attached Extrapolated Range with Diff. <= 1.5%
Description of the thermocouple"'s.function: 

### 20


## z.o '-j 

### l?O



## 2..0 "ff{CJ

0 

## o.o 70


### ;c S3Ci 

## to"' 

## s-2'7



## -I D· 

### 2. 

## THERMOCOUPLE CALIBRATION

150
jS() 

### (olD 

## I 

## "l 

## \? ccol? 

## -"2 0-3 

# ((i;) No) 

### ®No) Techniclan:**-<>N<.J·~,.,_"'-)** 

### __ _

to


# C:....,bl 

# t\,J..\..,**~** 

# fi>t;M**0-.~\£:\·** tl...m•"hf'k

If 

### not acceptable, describe corrective procedures undertaken:

# BARR

REFERENCE STANDARDS Hart Scientific 91 03-A s/n A1 B289 Hart Scientific 9140 sin A1B086 

## Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F + 

### 460 Probe Temp ( deg R), deg F + 

### 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points? 1700 1600 ct;1500 

## "' {!:_1400 w 

### !;§1300 

# ,_ ;:;1200 w

### ~1100 w 

### :;;1 000 -' 

# !5 900 0 

# g BOO :;; 

### "' 700 w

## ~ 600 500 400 

# THERMOCOUPLE CALIBRATION
THERMOCOUPLE ID C-3-1 Cal Date: 12/27/2004 

## Meter In or Out CALIBRATION TECHNICIAN: NRS TRACEABILITY DATE LABORATORY Report No. A1 B0718 12/11/2003 Hart Scientific Report No. A1B2024 12/11/2003 Hart Scientific 20 70 150 20 70 150 21 

### 69 148 4BO 530 610 4B1 529 60B

-1 1 2 0.2% 0.2% 0.3% YES

400 500 600 700 BOO 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Are extrapolated limits less than 1.5%? xtrapolation limit of calibration from graph: If not acceptable, describe corrective action: NO Enter Upper FAHRENHEIT Limit CALIBRATION RANGE -20 1200

# BARR Engineering Company
Thermocouple Number: 

# '<:- C.-::!>- 

## L

Media Std Used**!)-~** Reference Deo F (To) . Reference Carr Temp ( deg R) deg F 

### + 460 Probe Temp (deg F) 

### Probe Temp (deg R). deg F + 460 Difference (degrees) 

### % Diff 

### Abs. T (Renkin)
Diff. less than 1.5% at all points 

### Graph Attached Extrapolaled Range 

### with Diff. 

## = 1.5%

Description of the thermocouple"'s, function: 

### 20
20 

### '"ili'D



# ·z.l <.j 

### 'i? ( 

## +I 0,2_ 70 

### tO :>:So**~.c~9.** 

### SZ"'r



## -I e>- 

## <- THERMOCOUPLE CALIBRATION

150 (SQ 

## (., l 0 

## I**'I~** 

### (oCy 

### -2. 

## 0-3**(~/No)** ((£;;;1 No) Date:. i7 

### -1- "'t

- o"' 

### Technician:
__ rv:;c·**"-~"'------**



### to


# C..,.,J,..
... \**f{.,J~\.,_** 

## 3 b G.M 

# :r. .... l
.. 

# + fu,.....,..<O**~r\~**

If not acceptable, describe corrective procedureS undertaken:

# BARR

REFERENCE STANDARDS Hart Scientific 91 03-A s/n A1 8289 Hart Scientific 9140 s/n A1 8086 

## Temperature Calibraion Points Reference Deg F {To) Probe Temp ( deg F) Reference Temp {deg R) deg F 

### + 460 Probe Temp {deg R), deg F 

### + 460 Difference {degrees) % DiffAbs. T Is difference less than 1.5% at all measured points? 

## ,-- 1700 1600 1500**~** 

### 1400 

## •**~ ~**  

### 1300 ::>**~** 

### 1200 w 

### !:; 1100 w 

### :;; 1000**~** 

# .. ::> 

### 900 

# i BOO w 

## i!: 700 600 500 400 

# THERMOCOUPLE CALIBRATION
THERMOCOUPLE ID TC7-1 Cai;Date: 1/3/2005 

## M-5 Probe CALIBRATION TECHNICIAN: JMM TRACEABILITY Report No. A180718 Report No. A1 82024 

## 32 212 32 212 

### 32 209 492 672 492 669

0 3 0.0% 0.4% YES DATE LABORATORY 12/11/2003 Hart Scientific 12/11/2003 Hart Scientific 400 650 

## Ambient 400' 650 70 

### 395 642 

### 70 860 1110 530 855 1102 530

5 8 0 0.6% 0.7% 0.0%

400 500 600 700 BOO 

### 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Are extrapolated limits less than 1.5%? YES If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 950 -20 490

# BARR Engineering Company



# ·rr-. Thermocouple Number: _;_i_-'-------

Media Std Used Reference Deg F (To) Reference Carr Temp (deg R) deg F + 460 Probe Temp ldeg_F] Probe Temp (deg R), deg F + 460 Difference (degrees) % Diff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's function: 

### VI{}!,,)

## -~ 

## !r.,.j.e,_ 

# ' 32 

# <)- ,_) . 

## 4"'1 (_ 

# sJ- '-19 (__

0 

# o.o

If 

### not acceptable, describe corrective procedures undertaken: 70 

# '76 s-30 "'70 s-30

0 

# o.o THERMOCOUPLE CALIBRATION

212 

## ;) 1-2 ' (o 

## 7?.. ;)0 

# '1

(., <.'1**~:,** 

## 0·'1**~No) (~/No)**  Date: 

# I - < 

# -o c;- Technician: , J f"w"'V\/'-

400 650 

### f.)bO 

## (o.>() '1((,0 

### l I I<> 

# 515- 

# 0•1 )_ Ss-s- ( 10<... 

# -r**-~** 

# "'·"' 0-/

to

# BARR

REFERENCE STANDARDS Hart Scientific 9103-A s/n A1 B289 Hart Scientific 9140 s/n A 1 B086 Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F + 460 Probe Temp (deg R), deg F + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points?
1700 1600. 1500**~** 

### 1400 

## •**~** 

### ::1" 

### 1300 

# "**~** 

### 1200 w 

### !I; 1100 w 

### :;; 1000**~** 

# .. 5 900 u

### ~ 800 It: w 

## i!: 700· 600 500 400 

# THERMOCOUPLE CALIBRATION
THERMOCOUPLE ID TC 7-2 Cai;Date: 1/7/2005 

## M-5 Probe CALIBRATION TECHNICIAN: NRS TRACEABILITY Report No. A1B0718 Report No. A1B2024 

## 32 212 32 212 

### 32 209 

### 492 672 492 669

0 3 0.0% 0.4% YES DATE LABORATORY 12/11/2003 Hart Scientific 12/11/2003 Hart Scientific 400 650 Ambient 400 650 70 394 643 

### 69 860 1110 530 854 1103 529

6 7 1 0.7% 0.6% 0.2%

400 500 600 700 800 900 1000 11 00 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR Engineeling Company 

### Thermocouple Number: IC 

# 'l- 2 ·

Media Std Used 

## .t:H? Reference 

### Deg 

### F (To)

. 

### .

Reference Corr Temp ( deq 

### R) deq 

### F + 

### 460 Probe Temp (deg F) 

### Probe Temp (deq R). 'cteq 

### F + 

### 460 Difference (degrees) 

### % Diff 

### Abs. T (Renl<inJ
Oil!' less {han 1.5% 

### at all poinls 

### Graph Attached Extrapolated Range with Oiff. 

# = 1.5"/o

If 

### not acceptable, describe corrective procedures Wlderta.ken::

P:\00\02\0EM\Datasheets\cautas!ion.:ds 

### 32 212 

## '32. 2.12 

### 4"1'"t 

## "' ( "2.. 

## 32... 

# Z09 'I 'f 

## Z, <oG>"j

0 

## -3 o.c) C?."f THERMOCOUPLE CALIBRATION

Date: i-1-0'> Tec:.'lnichian: 

### --'-="'----


### 400 650 Other 

### ' "!OC 

### (.,'51:1 

# 10 '<;rc,o I\ (o 

### <;'"3<:::>



## 3'1'-/ G:.>'i3 

# G'l 'il'S'<f It o"3 

## s-2. 

## 9 -(o 

## -l -(

**~·l** 

# o.c:o 

# I o.z..

to;;;&BARRProjectJlS)II''>:Y!"=\-'<1(_Srnp!Loc(.,"\A"t.1Sbc.b:-TestNo.3Runsl·Date..7;!:::.-c::>$Pita!No.J::.=.l__Operotor'J'1<,.j(\J"1'CM'{SM'(IMeteryI,l><>)j•H@'2,1q1'fcpo.'iS'fpv'-'-,.,MET,avu5FIELDDATASHEETBar.Pres?9.,'ifInHgStat.Pres..0.4fZ.inH20ProbeLnglh3:flLinerType:08.8,OOtherSamgleTrainLeakRate(elm)Run1IRun2at15inHgPretestat15inHgPastiest0..0atGfInHPosHest0.DatI0InHgPitol(3in.)Pos.Pilot(31n.LPos.(jweg,\QTESTAUf\SampleISampleMeterVelocityOrificeTrainStackSamleTrainTemp,"FMeterMeter MeterVelocityOrificeTrainStackSam1eTrainTern_&"fMeterMeterPointTimeVolume.t.P,t.H,VacuumTemp.lmpngrInletGulletVolumflt.P,t.H,VacuumTemp.lmpngrInletOutletATVm,InHaOInH20in.HgTs,"FProbeFillerOutletTemp,"FTemp,"FVm,InH20inH20ln.HgTs,"FProbeFillerGulletTemp,"FTemp,"F'"'"''"..,'""""·..·,.'""',..,,..,,,,,,,,,,,.,,.,,.•,,..·'·,,··''"''''''·:,.,,,,'""'''"''"'''"''W''1'''"..,..,....,p,....,·='"'..,,..,.,.,,.,:::l.f!·(,'ZS1'13.11.O.'}L1.1&t.5"\1'1'Z1Lt'\YSl,tj,_t;J,!'f_O."!.S"·t_:q-(o1..\I'l0?.'I/L'{"J'1'11-)C:.<&<.;,.,11%,.,o....,,.1-5!!1"111"q'1,c.,cS'>r::.."fo1,-;6'J,o\1'\-z.z.'lt..Y/'-ltz.<a'iiYr.)lti..EG.'-{"{1.c.II'\'tlt-'f7-!..1f>30110·"11..I.'S"'J.o11q'231'Z.,E_l'i'S''ill"'c..,o1...I111In'lt'HI'-1<..IC.rIrrlimL"t_Lu8yknIJ.f1119.L2HI<'-I'llIItoLl'ullt1C!RJluyI''$1111ltv'bI'!C..IC.l..I.n..lt1\fi<>'"'1,cu.'II..,:u'>.s-:-111-1.n-2..-1....r..1-s':l-••..-v-Ju.f-112or..o1fi)."3'\13."'I1.,,,12-Y'i>I'f"7IIStlhw.<sllo.'JC.:11.1'11-z..'('11·,·-:r12>}I'1'1I<;:t11-1Inc;,:r'rtI1.1"-'"'Jl..ll....)lb.•itIJ.l,'LI't'bIltI5'611'2'11.'3Yilt.'-'1-I'Z..')Ill&mI'2HI2f'Iyq11z.£1Pz'1.'f£1b..t'\IJ./1......11·..01i''b1'tHI'VI1"n1tsIc.,..5y;,uC>.:JZ,.!.'Z.J,3.0ll"b2'ZY'r'f'b}L)0I[}yJlgy<..lrz.\'h•9..1"1lt:t.'lD11.\lol-:1.0lltrln'tl'lv1IYt-IJ1.1<.,1112r:t:t'fiD.'/l.lt&1>1'3..5"ll1l3l>tIlr'S'1'1-Y1I'lL"'111'1-12..1'6lntlYll1t.Ic.,,IIZS'!,"Ilo.Yt-[1.1..(,lls-Itt""ln'r[zri.-I$7'-Ti:?-liYl.:oit<.\rz.v'l.Ql1i'l-1.1'7to'l'fil.,-z;;'Z..o.'l<..11'r2:>"\HJKlir\It::•·"''21l.f(D.'(LJ.lp'l...].\II'<'2.3+2.'{"1,'{V,f.'!.(.Jl?lo'Z.tLO.'i'i1.1'1h.S11'6'2>1'-S'C..SyKVl->'{:ilSU'I·'Z.I'·'f1lv.•It'\11.3'\1Y¥V'61YC.3•.2."":1-'1.03h<£tfc.S>!S'<"1-rS{P1lt.1{b.'f'l'/.<>h'tI1Y1'"'\11-ll>fo)tl.!-.•}o.o;l,.z.n'f.'l1•"617)1._'t>1>lltt1.'!.1IO.S'IlVI?.l'fSIll'1>1'1.\l.z.h.r•IY&"'"Il.t>ilr.oIll"I"Z.')I.Izsc...l.!'1-1r11-:s-,,-gr,:J{o·..-'"'MOISTUREFlEGOVEFIYRUNflmolnaer1Total1I,171.I1...II--=tII't.Vo>II)-=-lo'-6I''tO'1....II...3-,LnHoHLt..finalWI-,g_lnm!!!wl.gII•"OiJferenceI-t;;<612Runs1·2PltotNo.)•'"lSM?Me<ery1.oO)bAli@Cp•pProjectSmplLoc3\&C...,TestNo.__Z:_Date'1·tOperatorV\1'\O:t"CM<,IEiPAMETHODsr'.>DFIELDDATASHEETlnHg........lnH20'.UnerType:OGfassDS.S,OOther__t:!:-o,vlll..'lHgProject·h'-Smplloc(;!!!'<-1-I..VC..Tes!No.LfOate1.(-I<>-"rRuns1-2OperatorIY'IT;IJ,A'ffCM3SM2,.MeteryAH@>IEPAMETHODlP13>f}FIELDDATASHEETBar.Pres2?,.1./S"InHgSlatPres..Q;,'/t.inProbeLng!hJ..ftUnarType:(l.GiassOS.S,OOiher

## ANEROID BAROMETER CALIBRATION

Barometer 

### I.D. Number:

# p~Jt 06 Barometer Reference: · 

## N L 

### 0

Pretest Calibration:

Before Adjustment After Adjustment

Posttest Check:

Notes:

Barr Engineering Co. 4700 

## w. 77th St Minneapolis. MN 55437 (952) 832·2600 

### Reference ("Hg)

### c-:Jq~ 

# g, 

# 'I

Reference f'Hg) 

### 2''!.00 Project Name: 

# u,,4J -,...,'**<~:-k** Project Number: 

# :?3/id1- "/;rt"

Barometer ("Hg) 

### Date Technician**~Cf.3** 

# ,, l.f- I 5 

# -c.;' 

# foL 

# v . .k:""

Barometer ("Hg) Date Technician 

### 2"!.06 

## "0/7/0'>**N~S:**

### Project Sample Loc. Date Operators US Steel - Minntac Line 6 Waste Gas (SV144) 4/19/2005 MTP, DJK, APP Analyzer Model/ SN Analyzer Range (span) Stripchart Speed (units): Cal. Anai./Model 200 25 % 20 cm/hr ANALYZER CALIBRATION DATA Note: Difference must be less than +/- 2 percent of span Test Runs : _1!__::__,3,__ Zero Gas Mid-rage High-range:
SYSTEM CALIBRATION BIAS AND DRIFT DATA: Cylinder Value 

### EPA METHOD 3A ANALYZER CALIBRATION (Oxygen)

Zero Gas Mid-ranQe Hi!:lh-ranQe

Analyzer Calibration Resoonse 0.0 9.1 20.0 Cylinder Serial No. Nitrogen CC12898 CC67233

Absolute Difference Difference, %of Span

Note: System Cal bias cannot exceed 

### +/- 5 percent of span. Drift cannot exceed 

### +/- 3 percent of span Certified Value 0.0 9.1 20.0

### Project Sample Loc. Date Operators US Steel - Minntac Line 6 Waste Gas (SV144) 4/19/2005 MTP, DJK, APP Analyzer Model/ SN Analyzer Range (span) Stripchart Speed (units): Cal. Anai./Model 200 10 % 20 cm/hr ANALYZER CALIBRATION DATA Note: Difference must be less than 

### +/- 2 percent of span Cylinder Test Runs: 1 3 Value Zero Gas 

# I •·. :.::.··· Mid-rage 

# 1:··,····· ; i'h·: High-range: 

# I· : ... '<·''
SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

### EPA METHOD 3A ANALYZER CALIBRATION

·:,, 

# <:

······· 

### (Carbon Dioxide)



### Zero Gas Mid-range High-range

Analyzer Calibration Response 0.0 5.0 9.1 Cylinder Serial No. Nitroaen CC67233 CC12898

Absolute Difference Difference, %of Span

Note: System Cal bias cannot exceed +/- 5 percent of span. Drift cannot exceed +/- 3 percent of span
Response

Bias= Drift= [(Final System Cal. Response -Initial System Cal Response) 

### I Span] x 100 Certified Value 0.0 5.0 9.1



### C02

### Project Sample Loc. Date Operators US Steel - Minntac Line 6 Waste Gas (SV144) 411912005 MTP,DJK,APP APi!Model 1 OOAH Analyzer Model 

### I SN Analyzer Range (span) Stripchart Speed (units): 50 ppm 20 cm/hr ANALYZER CALIBRATION DATA Note: Difference must be Jess than +I- 

### 2 percent of span

Test Runs: _1L_.::...__,3,__ Zero Gas

SYSTEM CALIBRATION BIAS AND DRIFT DATA: Cylinder Value 

### EPA METHOD 6C ANALYZER CALl BRA TION (Sulfur Dioxides)

Zero Gas Mid-range High-range

Analyzer Calibration Cylinder Serial No. CC146372 (Zero Air) CC68786 CC121446

Absolute Difference Difference, %of Span

Note: System Cal bias cannot exceed 

### +1- 5 percent of span. Drift cannot exceed 

### +1- 3 percent of span Analyzer Cal

System Calibration Bias= [(System Cal. Response- Analyzer Cal. Response) 

### I Span] x 100 Drift= [(Final System Cal. Response -Initial System Cal Response) 

### I Span] x 100 Certified Value 0.0 50.5 93.1

Drift, Percent of



### 502

### Project Sample Lac. Date Operators US Steel - Minntac Line 6 Waste Gas {SV144) 4/19/2005 MTP, DJK, APP TE Model 48/C0-1 Analyzer Model 

### f SN Analyzer Range (span) Stripchart Speed (units): 100 ppm 20 cmfhr ANALYZER CALl BRA TION DATA Note: Difference must be less than +/- 2 percent of span

Test Runs ;**_1~....-.:..__,3<--**



### SYSTEM CALIBRATION BIAS AND DRIFT DATA: Cylinder Value 

### EPA METHOD 10 ANAL VZER CALIBRATION (Carbon Monoxide)

Zero Gas Mid-range High-range

Analyzer Calibration Cvlinder Serial No. CC146372 (Zero Air) CC78171 CC117979

Absolute Difference Difference, %of Span

Note: System Cal bias cannot exceed 

### +/- 5 percent of span. Drift cannot exceed 

### +/- 3 percent of span
Analyzer Cal

System Calibration Bias= [{System Cal. Response- Analyzer Cal. Response) 

### f Span] x 100 Drift= [(Final System Cal. Response -Initial System Cal Response) 

### I Span] x 100 Certified Value 0.0 34.1 60.2

Drift, Percent of



# co

### Project ..:U:.:.·..:S:.:.·..:S:.:te::.:e:::.l
______ _ Sample Loc. Line 6 Waste Gas (SV144) Date 4/19/05 revised February 6 2006 Operators MTP, DJK, APP API/Model 1 

### OOAH Analyzer Model/ SN Analyzer Range (span) Stripchart Speed (units): 100 ppm 20 cm/hr ANALYZER CALIBRATION DATA Note: Difference must be less than +/- 2 percent of span Cylinder Test Runs: 1 

## - 3 Value Zero Gas 0.0 Mid-raqe 

### 50.5 • Hiqh-range: .· . 

### 93.1

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

### EPA METHOD GC ANALYZER CALIBRATION (Sulfur Dioxides)



### Cylinder Serial No. Zero Gas CC146372 (Zero Air) Mid-range CC68786 High-range CC121446

Analyzer Absolute Difference, Calibration Difference %of Span Response 0.0 . 

### 0.0 .· 

### 0,00% 51.3

. 

### 0.8
. 0.80% 93.0 0.1. 0.10%

Note: System Cal bias cannot exceed +/- 5 percent of span. Drift cannot exceed+/- 3 percent of span Initial Values Final Values Analyzer Cal System Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response. Cal. Bias TEST RUN 1 

### Time (sec) PPM PPM %of Span PPM %of Span Zero Gas 0.0 -0.1 

### ·.·•· cb.10%) 0.5 •0:50% • Upscale Gas 51.3 51.3
1 

### L.o.oo% • 50.4 •..**~0.90%** 

### ·. TEST RUN 2 Zero Gas 

### LO ·:·: 0.5**o.5a%····.~·** 

### 0.1 Upscale Gas 

# I :•• 

# .. 50.4 

### .**-0.90"1~** 

### •.· 50.0 TEST RUN 3 Zero Gas 

## o:o'/ ··.·· 0.1 0.10% . 

### 0.2 Upscale Gas

.. 

## 51.3 50.0 -1.30% 50.2 TESTRUN4 Zero Gas ·.·.·

. 

### ··.·· 

# ...... Upscale Gas 

# •

·. 

# ····· · .. 

# . · .. 

### System Calibration Bias = [(System Cal. Response- Analyzer Cal. Response) I Span] x 100 Drift= [(Final System Cal. Response- Initial System Cal Response) I Span] x 100 · .. \ 0.10%. -1.30%

.·. 

### 0.20%. -1.10%

. .

.. 

### Certified Value 0.0 50.5 93.1

Drift, Percent of span

. ··.···.:o.6b%

. • -0.90% -0.40%. .' 

### '0.40% 0.10%
. 0.20%



### 502

# BARR Project Sample Location Date Operators U.S. Steel Line 6 Waste Gas (SV144) 4/19/05 revised February 6 2006 MTP,DJK,APP Analyzer Model/ Serial No. Calibration Range, PPM: 0 to VIG/Model 20 100 Calibration Gas: Chart Speed: Propane in air 20 cm/hr PRETEST CALIBRATION DATA 

### EPA METHOD 25A ANALYZER CALl BRA TION (Total Hydrocarbons)

High-Range Mid-range Low-range Cylinder Serial No. CC93373 CC12353 CC98726 Zero Gas CC146372 (Zero Air)
Note: Calibration error must be less than +/- 5% of span gas value. Cylinder Analyzer Absolute Allowable Test Runs: 1

- 

### 3 Value, Response, Difference Difference PPM PPM PPM PPM**Hi~h-range:** 

### 88.8 88.5 0.3 4.4 Mid-rage 46.3 46.3 0.0 2.3 Low-range 30.4 30.1 0.3 1.5 Zero Gas 0.0 0.1 0.1 3.0 PRETEST RESPONSE TIME Note: Time to register 95% stepchange with high level gas. 

# I Response 

# I 1 Time (secj 

### 2 3 Average:
POST RUN DRIFT DETERMINATION Note: Zero drift must be less than +/- 3% of span Calibration drift must be less than+/- 3% of span. Initial Final System System Drift, Response, Response, Percent of RUN 1 PPM PPM span Zero Gas 0.1 0.1 0.0 Upscale Gas 30.1 31.0 0.9 RUN2 Zero Gas 0.1 0.5 

## I 0.4 Upscale Gas 31.0 31.4 

## I 0.4 RUN3 Zero Gas 0.5 0.1 

# I -0.4 Upscale Gas 31.4 31.7 

# I 0.3 RUN4 Zero Gas 

## I Upscale Gas 

# I Drift= [(Final System Cal. Response- Initial System Cal Response) I 

### Span] x 100 Cert. PPM 88.8 46.3 30.4 0.0

Calibration Error% of Cal Gas Value 0.3 0.0 1.0 0.1

THC

### Project _;;U:.;. ..;;S.:... S;:.t::::ee..::;l:_..
_____ _ Sample Loc. Line 7 Waste Gas (SV151) Date 4/20/05 revised February 6 2006 Operators MTP. DJK. APP API/Model 1 OOAH Analyzer Model/ SN Analyzer Range (span) Stripchart Speed (units): 100 ppm 20 cmlhr ANALYZER CALl BRA TION DATA Note: Difference must be less than +/- 2 percent of span Cylinder Test Runs: j 

# - 3 Value Zero Gas 0.0 Mid-raQe 50.5 ·. 

### EPA METHOD GC ANALYZER CALIBRATION (Sulfur Dioxides)

Cylinder Serial No. Zero Gas CC146372 (Zero Air) Mid-ranqe CC68786 High-range CC121446

Analyzer Absolute Difference, Calibration Difference %of Span Response 0.0 •' 

### 0.0 : 

### 0.00% 51.5 ... 1.0 1.00% HiQh-ranqe: .·. 

### 93:1 93.0 : . : 0.)


## .. < 0.10% ·· ... ···


### SYSTEM CALIBRATION BIAS AND DRIFT DATA: Note: System Cal bias cannot exceed 

### +/- 5 percent of span. Drift cannot exceed 

### +/- 3 percent of span Initial Values Final Values Analyzer Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response, TEST RUN 1 Time (sec) PPM PPM %of Span PPM Zero Gas 0.0 0.3 0.30%: 0.4 Upscale Gas 51.5 50.6 

## :·- '.0.90.%

- 49.5 TEST RUN 2 Zero Gas 

## ,-_.':
.. ·M···-
.. 0.4 . 0.40%c:< 0.6 Upscale Gas .·-- <51.5:.-···_: 495 

### I• -2.00%: _· 50.5 TEST RUN 3



## ~oGas ····- ...



## "(10''~: 0.6 I
. 0.60% -· . 0.6 scale Gas
.. •.··_····51.5 50.5 I 

## '-LOO% ·· 49.8 TESTRUN4 Zero Gas 

### ·.·.···-·.. ' 

# .· ....•. · 

### .. · 

## .. - 

# ....... •.• 

### Upscale Gas 

# -: 

# ·.· 

# ...... : 

# . I•
.. 

# \C•:
..... ·. System Calibration Bias= [(System Cal. Response- Analyzer Cal. Response) I Span] x 100 Drift= [(Final System Cal. Response- Initial System Cal Response) I 

### Span] x 100 System Cal Cal. Bias %of Span



### 0.40% •2.00% .· 

## i 

# "6.60o/o ·

'1.00% ·. 0:60%



### . -1:70%

-

.

. 

## ·• -·-·· 

# .. _.,_.· .·. 

### Certified Value 0.0 50.5 93.1

Drift, Percent of span 0.10% -1.10% .·

. 0.20% 1.00% : 

### 0.00%. -0.70%



## .. · .. .• ..


### S02

### Project Sample Location Date Operators U.S. Steel Line 7 Waste Gas (SV151) 4/20/05 revised February 6 2006 

## ' MTP, DJK, APP Serial No. Analyzer Model/ Calibration Range Calibration Gas: VlG/Model 20

, PPM: 0 to 100 Propane in air Chart Speed: 20 cmlhr PRETEST CALIBRATION DATA 

## EPA METHOD 25A ANAL VZER CALIBRATION {Total Hydrocarbons)

High-Range Mid-range Low-range Cylinder Serial No. CC93373 CC12353 CC98726 Zero Gas CC146372 (Zero Air)
Note: Calibration error must be less than +/- 5% of span gas value. Cylinder Analyzer Absolute Allowable Test Runs: 1 

# - 3 Value, Response, Difference Difference PPM PPM PPM PPM High-range: 

### 88.8 88.8 0.0 4.4

Mid-raQe 46.3 46.5 0.2 

### 2.3 Low-range 30.4 30.4 0.0 1.5 Zero Gas 0.0 

### 0.0 0.0 3.0 PRETEST RESPONSE TIME Note: Time to register 95% stepchange with high level gas. 

# I Response 

# I 1 

### 2 

### 3 Average:
POST RUN DRIFT DETERMINATION Note: Zero drift must be less than +/- 3% 

### of span Calibration drift must be less than+/- 3% 

### of span. Initial Final System System Drift, Response, Response, Percent of RUN 1 PPM PPM span Zero Gas 0.0 0.2 0.2 Upscale Gas 30.4 31.1 0.7 RUN2 Zero Gas 0.2 

## I 0.1 

# I -0.1 Upscale Gas 31.1 

# I 31.0 

# I -0.1 RUN 

### 3 Zero Gas 

## I 0.1 

## I -0.1 

## I -0.2 Upscale Gas 31.0 

## I 30.9 

## I -0.1 RUN4 Zero Gas 

## I I I Upscale Gas 

## I I I Drift= [(Final System Cal. Response -Initial System Cal Response) I 

### Span] x 100 Cert. PPM 

### 88.8 46.3 304 0.0

Calibration Error% of Cal Gas Value 

### 0.0 0.4 0.0 0.0

THC

### Project Sample Location Date Operators US Steel - Minntac Line 6 Waste Gas (SV144) 4/19/2005 MTP, DJK, APP Serial No. Analyzer Model/ Calibration Range Calibration Gas: VIG/Model 20

, PPM: 0 to 100**Pro~ane** 

### in air Chart Speed: 20 cm/hr PRETEST CALIBRATION DATA 

### EPA METHOD 25A ANAL VZER CALIBRATION (Total Hydrocarbons)

High-Range Mid-ranQe Low-range Cylinder Serial No. CC93373 CC12353 CC98726 Zero Gas CC146372 (Zero Air)
Note: Calibration error must be less than +/- 5% of span gas value. Cylinder Analyzer Absolute Allowable Test Runs: 1 

# - 3 Value, Response, Difference Difference PPM PPM PPM PPM HiQh-ranQe: 88.8 88.5 0.3 4.4

Mid-rage 46.3 46.3 0.0 2.3 Low-range 30.4 30.1 0.3 1.5 Zero Gas 0.0 0.1 0.1 3.0 PRETEST RESPONSE TIME Note: Time to register 95% stepchange with high level gas. 

# I**Res~onse** 

# I 1 2 

### 3 Average: Time (sec) #DIV/0! POST RUN DRIFT DETERMINATION Note: Zero drift must be less th 

### I 3"A f an+· 0 0 

### span. 

# c l'b 

### t' d 'ft al ra 1on 

### n mus t b I th e ess 

### an+- 

### I 3% of span. Initial Final System System Drift, Response, Response, Percent of RUN 1 PPM PPM span Zero Gas 0.1 0.1 0.0 Upscale Gas 30.1 31.0 0.9 RUN2 Zero Gas 0.1 

## I 0.5 0.4 Upscale Gas 31.0 

## I 31.4 0.4 RUN3 Zero Gas 0.5 

## I 0.1 

## I -0.4 Upscale Gas 31.4 

## I 34.7 

## I 3.3 RUN4 Zero Gas 

## I I Upscale Gas 

# I I Drift= [(Final System Cal. Response- Initial System Cal Response) 

### I Span] x 100 Cert. PPM 88.8 46.3 30.4 0.0

Calibration Error% of Cal Gas Value 0.3 0.0 1.0 0.1

THC

### Project Sample Loc. Date Operators US Steel - Minntac Line 7 Waste Gas (SV151) 4/2012005 MTP, DJK, APP Analyzer Modell SN Analyzer Range (span) Slripchart Speed (units): ANALYZER CALIBRATION DATA Note: Difference must be less than +/- 2 percent of span Test Runs: 1 - 

### 3

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

### i Value 

## EPA METHOD 3A ANALYZER CALl BRA TION (Oxygen)



### Analyzer Calibration Difference 

### i %of Span

Note: System Cal bias cannot exceed+/- 5 percent of span. Drift cannot exceed 

### +/- 3 percent of span



### i i Drift= [(Final System Cal. Response- Initial System Cal Response) I Span] x 100 

### 02

### Project Sample Loc. Date Operators US Steel • Minntac Line 7 Waste Gas (SV151) 4/20/2005 MTP, DJK, APP Analyzer Modell SN Analyzer Range (span) Stripchart Speed (units): Cal. Anai.IModel 200 10 % 20cm/hr ANALYZER CALIBRATION DATA Note: Difference must 

### be less than 

### +I· 2 percent of span Cylinder Test Runs: 

## l 

# . 3 Value Zero Gas 

# 1.'. : <: 

## 1;,'(1;;

**Mid·ra~e** 

# f:>>. )' 

## :.· 

# :: Hioh-range: 

# 1' .• : ,.• .··· ft
SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

## EPA METHOD 3A ANAL VZER CALIBRATION (Carbon Dioxide)


### Cylinder Serial No. Zero Gas Nitrogen Mid·range CC67233 High·range CC12898

Analyzer Absolute Difference, Calibration Difference %of Span Response 0.0 

### ?/}' 

# B'<·>•• 1'':·•:;;: 

# g1?] 5.0 

## !)}.:•·, .• ;,; 9.0

**5£(~?)'** 

# 1.·'';··· 1>i{ 

## 1}06•£ ,,,,

Note: System Cal bias cannot exceed 

### +I· 5 percent of span. Drift cannot exceed 

### +I· 3 percent of span



### i Certified Value 0.0 5.0 9.1

Drift= [(Final System Cal. Response- Initial System Cal Response) 

### I Span] x 100 

### C02

### Project Sample Loc. Date Operators US Steel - Minntec Line 7 Waste Gas (SV151) 4/20/2005 MTP, DJK, APP API/Model 1 OOAH Analyzer Model/ SN Analyzer Range (span) Stripchart Speed (units): 50 ppm 20 cm/hr ANALYZER CALIBRATION DATA Note: Difference must 

### be less than+/- 2 percent of span
Test Runs :

**__j1L.......::__~il,_** 

### Zero Gas Mid-raqe High-range:
SYSTEM CALIBRATION BIAS AND DRIFT DATA: Cylinder Value 

### EPA METHOD 6C ANALYZER CALIBRATION {Sulfur 

### Dioxides)

Zero Gas Mid-ran>Je High-range

Analyzer Calibration Response 

### 0.0 51.5 93.0 Cylinder Serial No. CC146372 (Zero Air) CC68786 CC121446

Absolute Difference Difference, %of Span

Note: System Cal bias cannot exceed 

### +/- 5 percent of span. Drift cannot exceed +/- 3 percent of span Analyzer Cal System Cal System Cal

System Calibration Bias= [(System Cal. Response· Analyzer Cal. Response) 

### I Span] x 100 Drift= [(Final System Cal. Response· Initial System Cal Response) 

### I Span] x 

### 100 Certified Value 0.0 50.5 93.1

Drift, Percent 

### of



### S02

### Project US Steel - Minntec Sample Loc. Line 7 Waste Gas (SV151) Date ....:.4:.=12:.::012=00::.:5=-------- 0perators MTP, DJK, APP TE Model 48/C0-1 Analyzer Model/ SN Analyzer Range (span) Stripchart Speed {units): 100 ppm 20 cm/hr ANALYZER CALIBRATION DATA Note: Difference must be less than +/- 2 percent of span

Zero Gas

SYSTEM CALIBRATION BIAS AND DRIFT DATA: Cylinder Value 

### EPA METHOD 10 ANAL VZER CALIBRATION (Carbon 

### Monoxide)

Zero Gas Mid-range High-range

Analyzer Calibration Cylinder Serial No. CC146372 (Zero Air) CC78171 CC117979

Absolute Difference Difference, %of Span

Note: System Cal bias cannot exceed 

### +I· 5 percent of span. Drift cannot exceed +/- 3 percent of span

Response Time Analyzer Cal System Cal System Cal Cal. Bias

System Calibration Bias= [(System Cal. Response- Analyzer Cal. Response) 

### I Span] 

## x 100 Drift= [(Final System Cal. Response -Initial System Cal Response) 

### I Span] 

## x 100 Certified Value 0.0 34.1 60.2

Drift, Percent of



# co

### Project US Steel - Minntac Sample Location Une 7 Waste Gas (SV151) Date 4/20/2005 Operators MTP, DJK, APP Serial No. Analyzer Model/ Calibration Range Calibration Gas: , PPM: 0 to Propane in air Chart Speed: 20 cm/hr PRETEST CALIBRATION DATA VIG/Model 20 100 

## EPA METHOD 25A ANAL VZER CALIBRATION (Total Hydrocarbons)

High-Range Mid-range Low-ranQe Cylinder Serial No. CC93373 CC12353 CC98726 Zero Gas CC146372 (Zero Air)
Note: Calibration error must be less than 

### +/- 5% of span gas value. Cylinder Analyzer Absolute Test Runs: 1 

# - 3 Value, Response, Difference PPM PPM PPM High-range: 

### 88.8 88.8 

### 0.0

Mid-rage 46.3 46.5 0.2 Low-range 30.4 30.4 0.0 Zero Gas 0.0 0.0 0.0 PRETEST RESPONSE TIME Note: Time to register 95% stepchange with high level gas. 

# I Response 

# I Time (sec) 

### 1 2 

### 3 Average: #DIV/0! POST RUN DRIFT DETERMINATION Note: Zero drift must 

### be less than 

### +/- 3% of span. Calibration drift must be less than 

### +/- 3 Initial Final System System Drift, Response, Response, Percent of RUN 1 PPM PPM span Zero Gas 0.0 0.2 0.2 Upscale Gas 30.4 31.3 0.9 RUN2 Zero Gas 

## I 0.2 

## I 0.1 

## I -0.1 Upscale Gas 

## I 31.3 

## I 31.0 

## I -0.3 RUN3 Zero Gas 

## I 0.1 

# I -0.1 

## I -0.2 Upscale Gas 

## I 31.0 

# I 30.9 

## i -0.1 RUN4 Zero Gas 

## I I Upscale Gas 

## I Drift= [(Final System Cal. Response- Initial System Cal Response) 

### I Span] x 100 Allowable Difference PPM 4.4 2.3 1.5 3.0

%of span. Cert. PPM 

### 88.8 46.3 30.4 0.0

Calibration Error% of Gal Gas Value 0.0 0.4 0.0 0.0

THC

# AppendixF Cylil'lder Gas Certifications

# Sill I

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 

### 92507 TELEPHONE (9091 653·6780 • FAX 

### (9091 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: 

### April 16 2004 Barr Engineering Co 

### 7390 OHMS Lane Edina 

### MN 55439-2330
CUSTOMER ORDER NUMBER: 

### 20040210ASMF2**----------------------------------------------------~-~-----~------ --~-,--**  .......**~~-----------------------------------------------------------** COMPONENT CONCENTRATION(v/v) REFERENCE ANALVZER EXPIRATION REPLICATE +EPA UNCERTAINTY STANDARD MAKE. MODEL, SiN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC1289B VARIAN MODEL 1860 TCD 04/12/04 Carbon Dioxide 9.05 ± 0.03% GMIS 5/N NONE 04/12/07 9.06% CYLINDER#: THERMAL CONDUCTIVITY 9 .OS% CC51112 GAS CHROMATOGRAPHY 9.05\ @17.98% LAST CAL DATE: 03/29/04 MEAN: 9.05% VARIAN MODEL 1860 TCD 04/15/04 Oxygen 9.07 ± 0.05% GMIS S/N NONE 04/15/07 9.08% CYLINDER#: THERMAL CONDUCTIVITY 9.08% 

### Nitrogen Balance CC81204 GAS CHROMATOGRAPHY 9.05\ CYLINDER PRESSURE: 2000 

### psig @ 9.88% LAST CAL DATE: 03/25/04 MEAN: 9.07%

ppm =**~ole/mole** % = mole-% The above analyses were performed in accordance with Procedure G1 of the**EPATrEtc~abiility** Protocol, Report Number EPA-600/R97/121, dated Se mber 1997. This cylinder shou d if the pressure is less than 150 psig.

The only liability of this company for gas which fails to comply with this analysis shall be replacement reanalysis thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

### BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. • RIVERSIDE. CA 92507 TELEPHONE (909) 653-6780 

### o FAX {909l 653-2430 

# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: June 

### 25 2004 

### Barr**Eng~neering** 

### Co 7390 OHMS Lane Edina MN 55439-2330
CUSTOMER ORDER NUMBER: 

### 20040420ASMF2

,...,........,.....,_,_.._,.._.._.. 

# _____ ..__ 

### ..... ...,.._. 

# ____ ,.,.,....,."·""'""" ....... ...-. ............. 

# -----"""'"'""-----

............ 

# ------ ..... ....., 

### ............ ""' 

### ..... """'""" 

# __ ,.,... 

# ______**~** 

# .. ,...""",..... 

## ..... _,..-.-.--..- 

### ..... 

# ..--- ....... ....,._..-. 

## .....**_-~** 

## .....**~-""""'"'_,......** ....... """ 

### ...**"'_"""_~-""""""---------** 

### ......**--~---** 

### ....... --""""""'"""'_"""' 

# ______ . COMPONENT CONCENTRATION(v/v) REFERENCE ANALVZER EXPIRATION REPUCATE ±EPA UNCERTAINTY STANDARD MAKE, MODaL, SiN, OETECTJON DATE ANALYSIS DATA CYLINDER NO: 

## CC67233 VARIAN MODEL 1860 TCO 06/25/04 

### Carbon Dioxide 

### s.o1 ± 

### o.os% GM1S 5/N NONE 06125/07 5.0H CYLINDER II: THERMAL CONDUCTIVITY 5.01% CC42Bl4 GAS CHROMATOGRAPHY 

## s.ou @a.on LAST CAL DATE: 06125104 MEAN: 5.0111 VARIAN MODEL 1860 TCD 06/24/04 

### Oxygen 

### 19.98 " 0.2% GMIS S/N NON:E 06/24/07 19.94% CYLINDER#: THERMAL CONDUCTIVITY :20.05% 

### Nitrogen Balance CA0320l GAS CRROMATOGRAPlif 19.96% CYLINDER PRESSURE: 2000 

### psig @ 24-82% LAST CAL DATE: 06/23/04 MEAN: 19.98%

ppm •**~le/mole** \ = mole-\ The above analyses were performed in accordance wilh Procedure G1 of the EPA Traceability Protocol, Report Number 

### EPA-600IR97/121, .tad 

### e ember 

### 1997. This cylinder 

# snot ,d lithe pressure is less than 150 psig. 

# n
ANALYST:

# ~v t

# APPROVED:._,c_~.....:C-A-~""If1_;_,+ 

# o

________ _ M. S. CALHOUN 

# 61J!{ J, T. MAIUUN 

# ==e--
The O!liy !iabUity of this company for gas Which fais to comply with this anatysls shall be**r~laf.:emenl** or rea.naiysls thereof by the company without extra CQSI. STANDARD CALIBRATION GASES IN IILUMINUM CYLINDERS

# II

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 

### 92507 TELEPHONE (909) 653-6780 • FAX 

### (909) 653·2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: John Stock DATE: August 27 2003 

### Barr 

### Engineering Co 7 3 90 OHMS Lane 

### Edina MN 55439-2330
CUSTOMER ORDER NUMBER: 20030707A**~~--~---------~~----------~-------------------~------------~---­ -~----~---~---------------~--~-------------~-~~--~-------------~**  COM!'ONENT CONCENTRATION(v!V) REFERENCE ANALVZER EXPIRATION REPLICATE :EPA UNCERTAINTY STANDARD MAKE. MODEL, SJN, DETECTION DATE ANALYSIS DATA cYLINDER NO: 

## CC68786 BOVAR MODEL .922M OB/12/03 Sulfur Dioxide 50.5 " 0.6 

### ppm GMIS S/N VD92284844 OB/19/05 50.4 ppm CYLINDER#: CONTINUOUS 

## so.s pp1U 

### Nitrogen Balance CC12643 UV PHOTOMETRY 

### 50.5 ppm CYLINDER PRESSURE: 2000 psig @ 

## ss.a ppm LAST CAL DATE: OB/07/03 MEAN: 50.5 ppm

ppm =**~ole** /tnole The above analyses were performed in accordance wfih Procedure G1 of !he EPA Trac ability Protocol, Report Number EPA-600/R97 /1 21 , daled September 1997. This cylinder should not be used 

### if !he pressure is less than 150 psig.

# ANALYST:~ M.J .MONSON The only l.iablli\y of this company tor gas Whteh 1alis to comply with U'll$ analysis shall be replacement or reanalysis thereof by the company without extra cost STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 08{19/03 50.5 ppm 

### so.s ppm 50.6 ppm 50.5 ppm

# 1111

BAR:ROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (909) 653-6760 • FAX (909) 653-2430 

# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: July l3 2004 

### Barr Engineering Co 

### 73!!0 OHMS Lane 

### Edina MN 55439-2330
CUSTOMER ORDER NUMBER: Vbl/S FOSS ----"""""""'""""_.....,
............... _... 

### ............ ,..... 

# ______ ..__....., 

# ______ .... 

# _____**~-----....,-----......-** 

### ................. 

# __**~-----** 

### ..... 

# ---·--**,-~-~--~~~-~----------------~--------~~-----~--~~~~~----------~~-** COMPONENT CONCENTRATION(v/v) REFERENCE ANALVZER EXPIRATION REPLICATE ±EPA UNCERTAINTY STANDARD MAKE, MODEL. SIN, DETECTIOH DATE ANALYSIS DATA CYLINDER NO: 

## CC121446 BOVAR MODEL 922M 07/12/04 

### Sulfur llioxide 93.1 :t 0.9 

### ppm GMIS S/N VD922.048U 07/12/06 93.1 ppm**CY~INDERII:** CONTINUOUS 93.1 ppm 

### Nitrogen 

### Balance CCl2025 UV PHOTOME:TRY 93.3 ppm CYLINDER PRESSURE: 1150 psig @ lll.8 ppm I.AST CAL DATE: 06/14/04 MEAN: 93.2 ppm

ppm ..,**~l.e/rnole** % ,. mole-\ The above analyses were performed In accordance with Procedure G1 otlhe EPA Trace !lily Protocol, Report Number EPA-600/R97/121, dated September 1997. This cylinder should not be used if the pressure Is less !han 150 psig.

# ANALYST:}~ M.J.MONSON Tne only liability of this**comp~ny** for gas which fails to comply wllh tn\s analysis shall be replacement , reanalysis thereof by lhe company without extra cost ST ANDAAD CAUBRATION GAsES IN AWMINUM CYLINDERS

# .., 1111

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (951) 653-6780 • FAX (951) 653-2430 

# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: 

### Nicholas Shreve Barr Engineering Co 7 3 90 OHMS Lane DATE: December 22 2004
Edina MN 55439-2330
CUSTOMER ORDER NUMBER: 20041123ANRS
COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPLICATE 

# * EPA UNCERTAINTY STANDARD MAKE, MODEL, SJH, OETECTION DATE ANALYSIS DATA CYLINDER NO: 

## CC78171 CARLE**IN$~** MOPEL 8000 12/14/04 12/21/04 

### carbon Monoxi4"G: :l4.l "' 0.3 ppm GMIS Sill 8249 12/21/07 34.0 ppm. 34..2 ppm. CYLIHDER#: ME'l'HAHA'l'ION/FlD 34.0 ppm 

## :u.l ppm 

### Nitrogen Balance CA03684 GAS (:HROMA'l'OQRAPH:! 34.1 ppm 34.1 ppm CYLINDER PRESSURE: 2000 

### psig @54.5 p,.. t.ASTCALDATE: 12/13/04 MEAN: 34.0 ppm 34,1 ppm

ppm = J}.mOle/mole The above analyses were performed In aeeordanee wlth Procedure Gt 

### of the EPA Tra:Cijl!biliity Protocol, Report Number EPA-600/R97/121, dated September 1997. This cylinder should not be used if the pressure is less than 150 psig.

# ANALYST:~ M.J.MONSON

STANDARD CALIBRATION GASES IN AWMINUM CYUNDERS

# 1111

BARROl 

# SCOTT-MARRIN, INC. 65:31 BOX SPRINGS BLVD. • RIVERSIDE. CA 92507 TELEPHONE {909) 65:3·6790 o 

### FAX {009) 653·2430 

# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: CUrt Stock 

### DATE: October l3 2003 

### Barr Engineering Co 73!10 OHMS Lane 

### Edina MN 55439-2330


### CUSTOMER ORDER NUMBER: 20030707A


### COMPONENT CONCENTRATION(v/V) REFERENCE "' EPA UNCERTAINTY STANDARD CYLINDER NO: 

## CC117979 Carbon Monoxide 60.2 ::!:: 0.5 

### ppm GMIS CYLINDER#: Nitrogen 

### Balance CCB5129 CYLINDER PRESSURE: 2000 

### psig @55.4 ppm

% "" tnole-\ 

### ANALVZER MAKE, YOOEL, S/M, OETECTION
CARLE INS':I' MODEL BODO SIN**82~9** ME!t'HAHA'l'ION/FID GAS CHROVA'l'OGRAPHY LAST CAL DATE: 10/02/03

The above analyses were performed In accordance with Procedure G1 of the 

### EPA Trace 

### EPA·600/R97/121 , dated September 

### 1997. This cylinder should not 

### be used if the pressure is less than 150 psig.

# ANALYST:~ M.J,MONSON EXPIRATION REPLICATE DATE ANALYSIS DATA 10/03/03 10/13/03 10/13/06 60.0 ppm 60.1 ppm 60.2 ppm**60~3** ppm 60.3 ppm 60.2 ppm MEAN: 60.2 ppm 60.2 ppm

lilly Protocol, Report Number

The on,y liability or thls company for gas wrnc.>; falls. to comply Wi1h this analysls shall be replacement reanalysis thereof by !he companywilhout extra cost STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# I SCOTT -MARRIN, 

# INC.

CHRONOLOGICAL RECORD OF CERTIFIED CONCENTRATIONS CGSTOMER: Barr Engineering Co 

### PORCHASE ORDER: Vbl/S Foss



### CYLINDER NUMBER: CC121446 COMPONENT so2 DATE 07/10/02 07/17/02 

### 07/12/04



### AVERAGE
NOTES: 93.0 ppm 

### 93.0 ppm 

### 93.2 ppm



### 93.1 ppm 

### COSTOMER CODE: BARROl 

### DATE: 07/13/04

# • 1111

BARROl 

# SCOTT-MARRIN, INC
. 6531 BOX SPRINGS BLVD. o 

### RIVERSIDE. CA 

### 92507 TELEPHONE (909) 653-6780 • FAX (909) 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: 

### Peter Rossmiller 

### Barr Engineering Co 7390 

### OHMS Lane DATE: 

### November 4 2003


### Edina MN 55439-2330
CUSTOMER ORDER NUMBER: 

### 2003/ 10/03/APJR**-----~------~-----~--~--~~~~--~~---~-----~~---~---~-~----------- --~~-~------~----~------~~--~-----~~---~-~~~-~~---~----~-----~--**  COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRAnON REPLICATE "'EPA UNCERTAINTY STANDARD MAKE, MODEL, SIN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

## CC98726 VARIAN MODEL 1860 FID 10/31/03 Propane 30.4 % 0.3 ppm GMIS S/H NONE 10/31/06 30.3 ppm CYLINDER#: FLA!-IE IONIZATION 30.4 ppm UltraPure Air Balance CC121986 GAS CHROMATOGRAPHY 30. 4 ppm CYLINDER PRESSURE: 2000 psi.g @ 50.6 ppm LASTCALOATE: 10/31/03 MEAN: 30.4 ppm



### ppm "" prnole/mole % "" mol.e-11; The above analyses were performed In accordance with Procedure G1 of the EPA Trac ability Protocol, Report Number EPA-600/R97/121, dated eplember 1997. This cylinder o I used 

### if the pressure is less than 150 psig.

The only**!iablli~** of this company iO! gas which falls to comply with this analysis 5hall b&**rep~acement** or reanalysis thereof by the company Without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# =1111

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (909) 653-6780 • FAX (909) 653·2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: John Stock DATE: January 29 2003 

### Barr Engineering Co 7390 OHMS Lane**Ed~na** 

### MN o5439-2330
CUSTOMER ORDER NUMBER: 2002-l2l9-AJZS2**-~-~~----~-~------~-----------~~------~---~~~--~-~----------~~~~ -~-~~-~-~~--------~----~-~-~-~~~----~------~~-~~~--------------~**  COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPLICATE " EPA UNCERTAINTY STANDARD MAKE, MODEL, &/N, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

## CC12353 VARIAN MODEL 1S60 FID 01/28/03 Propane 46.3 t; 0.4 ppm GMIS S/N NONE 01/22/06 46.4 ppm CYLINDER 1: FLAME IONIZATION**46~3** ppm 

### ultraPure Air Balance CC121986 GAS CHROMATOGRAPHY 46.1 ppm CYLINDER PRESSURE: 2000 psig @50.6 ppm !.AST CAL OATE: 01/28/03 MEAN: 46.3 ppm

ppm = pmole/mole t 

## = mole-% The above analyses were performed in accordance with Procedure G1 of the EPA Trac 

### ability Protocol, Report Number EPA-600/R97/121, ated September 1997. This cylinder**shQ~,~I** used H the pressure is less than 150 pslg.

The only llab!l!ty of 'this company far gas which 

### taas 1o compiy with this analysis shall be rep'.aoement or reana1ys1s thereof by the company wl\hout extra cost STANDARD CALIBRATION GASES IN ALUMINUM CYUNDERS

# .. 1111

BARROl 

# SCOTT-MARRIN, INC
. 6531 BOX SPRINGS BLVD. • RIVERSIDE, CA 92507 TELEPHONE (909l 653-6760 o 

### FAX (909) 653·2430 

# REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: 

### Peter Rossmiller Barr Engineering Co 7390 OHMS Lane DATE: November 4 2003


### Edina MN 55439-2330
CUSTOMER ORDER NUMBER: 2003/10/03/APJR**~---~~--~---~---------~-~--~~---~------~~-~-~--~~--~----~~-----~­ ~~--~---~~-~~--~------~~-~-~-----------~--~-~-----------~---~~--**  COMPONENT CONCENTRATION(v/V) REFERENCE ANALVZER EXPIRATION REPUCATE • EPA UNCERTAINTY STANDARD MAX£. MODEl., SiN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

## CC93373 VARlAN MODEL lB60 FlO 10/31/03 

### Propane 

## ss.s ± 

### 0.9 ppm CM!S S/N NONE 10/31/06 88.9 ppm CYLINDER#: FLAME**ION'IZA'l'lO~** 89-0 ppm 

### zero Air Balance CC83088 GAS CHROMkrOGRAPBY 88.6 ppm CYLINDER PRESSURE: 2000 

### psig @104 ppm LAST CAl. DATE: 10/31/03 MEAN:**88~8** ppm

ppm 

### = pmole/mole The above analyses were performed in accordance with Procedure G1 ofthe EPA Trac ilily Protocol, Report Number 

### EPA-600/R97/121, dat1 Segtember 

### 1997. This cylinder o ld

### )~ " ed If the pressure Is less than 150 psig. 

### i
. ANALYST: "' .-..· APPROVED: 

## -,iff\"!' ;:__ ___________ _ .s. AL'BO" 

# I ,!].',MARRIN The only liability of this company for gas whleh fails to comply wfth this analysis shall be replacement or reanalysis**lt!~rec1** by the company without e)ctre cost STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# CERTIFICATE OF CONFORMANCE

CUSTOMER: 1WIN CITY OXYGEN REFERENCE#: CYLINDER#: ORDER#: DATE REPORTED:
MATERIAL SUBMITTED: •AIR, CEM ZERO GRADE

INFORMATION REQUESTED: RATIO ANALYSIS 88-90939

. CC146372 43778 6/2/2004

• AIR IS DEFINED AS, OXYGEN= 19.5-23.5% WlTH A BALANCE OF NITROGEN COMPONENT SPECIFICATION CONCENTRATION METHOD S02 0.1 PPM < 0.10 PPM lJL TRAVIOLETANAL YZER NOX 0.1 PPM < 0.10 PPM CHEMILUMINESCENT 

# co 0.5PPM <0.50PPM GAS CHROMATOGRAPH C02 1 PPM < 1.00 PPM GAS CHROMATOGRAPH THC 0.1 PPM <0.10PPM FID H20 5PPM <5.00PPM MOISTURE ANALYZER OXYGEN 20.5%- 21.5% 20.5%-21.5% OXYGEN ANAL VZER NITROGEN BALANCE

AUTHORIZED SIGNATURE .

''THiS REPORT STATED ACCURATELY THE RESULTS OF 1lfE INVESTIGATION MADE UPON THE MATERIAl SUBMffTEO TO THE ANALYTICAL lABORATORY. EVERY EFFORT HAS BEEN MADE TO DETERMINE OBJECTIVELY THE INFORMATION REQUESTED; HOWEVER., IN CONNECTION W11lf ITS RENDERING OF 1l/IS REPORT. NATIONAL SPECIAl. TY GASES SHALL HAVE NO llABIUTY IN EXCESS OF THE ESTABUSHEO CHARGE FOR THE Sf::RVICE," NSG020149J ;>

# Appendix G Visible Emissions Evaluator Certifications

# VISIBLE EMISSIONS EVALUATOR
This is to certify that

I""Y"\l""d''"'"''= 

# specifications of Federal Reference Method 9 and qualified as a visible emissions evaluator. Maximum deviation on white and black smoke did not exceed 7.5% opacity and no single error exceeding l 5% opacity was incurred during the certification test conducted by Eastern Technical Associates of Raleigh, North Carolina. This certificate is valid for six months from date of issue.

. .·. " _:.**~-** ' 

### . . 

## ' 328686 '**~"teaju::liay Jlinnc~.**  

## eertificC!e Number Locclion Oote 

### 01 Issue



### . . . . 

### .
President · .. ·

# )ih~dJ 

# (/).**~~/~.** Director ofTraining · 

# 'CT 

# u. .

# ~**-·~:** ·

# ~~e£ating~~~ta·**SU1n.qa~ F~·~** **~P~ricti~s;Soui"ces:** .. ·

# :·~~!~:':~~~'f~os

# .·7~§~f~,~j*~r~~M~,;~~lil~~~l~~~)i~.<6si~,~6~;~~~··.j·.~~ 

# ..•.. :.**>~f;(:;** •• ·

# ····,~~·.·· '
.. ·· .. •.

# iE"l~;~~~o~;
Test Date(s): Aprill9. 2005 Process Equipment Number/Identification: ,.,SV-'2:14::t:4,_
____ _ Company N 

### arne: U. 

### S. Steel Minnqsota Ore Operations- Cf't11NNT!illcc• 

### '-!..!A"'C"-'Ll

-------------------- Equipment & 

### Operating Data L Process Equipment Description: Step III Agglomerator Line 6 Waste Gas St&::k IPM tests 

### 2. Were the process 

### and control equipment operated consistent v.-ith normal procedures? 

### YBS[8l NOD If no, explain: 

### 3. Include 

### copy of production or instrumentation which indicates rate of production or operation of the equipment, i.e. units 

### per hour} pounds per hour, pressure. air flow, etc. 4. Date( 

### s) and procedure( s) of last maintenance/cleaning within 

### 6 months: 

## 18:1 Remains unchanged from info. provided in test plan

# ~~~~~~~;;~~~~~~~~ctl~~~;;~~~~);til~~~~gn~fuiltY~~~-- 5. Process rate (amount of raw material or finished product per hour, wet or dry basis) (list 

### fuel type(s) and**ratiosasa~~o·priaoo)** 

### _________________________________________________________________ .. _____ __**··;?'~-** 

# ····,· .....**c:::-el'Q~~s:~i'io)ru,1~~;,~'\li~ivn·.** 

### it: 

# t:;;r: .•**':T.~:;~** 

# .:"''"· ·-· · Green ball feed rate, long tons per hour (L TPH) 546,9 

### 543.7 547.3 Pellet production rate, (LTPH) 

### 487,0 480.2 

### 482.0 i 

# ' Fuel Input (list units) 

### i Heat Input (10'' British thermal units/hour) 6. Summarize 

### control equipment operating data documented during testing, Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) of APC equipment and parameters generally monitored, Mouitor as in test plan and/or approval letter. 

### (listtype ofscrubber): &'(in, 

### w.c.) and feed rate (gpm and psig) • Baghouse, Cyclone, and Multi-clone: &'(in, 

### w.c.) 

## • Incinerator :flFm ,°Fout) 

### and Thermal Incinerator: ron 

### • ESP: Number and identity of • 

### t field(s) 

## !.APC • •·**.:x~.·:** 

## .. 

# ::.<: . ·: 

# '" .:;**:'•R~n.'2'•',>.-- :<'~''"'"**  

# ·.·,

Wet llP 

### (in. w.c.) 

### 8.31 .18 Wet scrubber, feed rate (gpm) 2,999 3,000 2,998

' 

# 1'<
.. ::-· T 

## :. ;;:.**.;'f":'~** 

# f,-.·_._··r·· 1 .-··-··-· Continuous Opacity Monitor(list hourly average)

__ Monitor (list averaging basis):

__ Monitor (list averaging basis:**~·** 

# ... 'control or 

# .. per minute in. 

### ; of water column lbs.-pounds psig-pressure per square inch gauge ,;p. pressure drop


### Note: This form provides only a summary of the operating conditions during the performance test. Additional 

### and more detailed records are reqnired to meet the requirements of Minn. R. 7017.2035, subp. 3. This form is to 

### be submitted as part of the performance test report. aq-f6-ST05 Form ST-05, Page 

### J of 1

### Test Date(s): Aprill9, 2005 Process Equipment Number/Identification: "'SV-'-"l 2 

### 44:r_
_____ _ Company Name: 

### U. S. S!;le! Minnesota 

### Ore Operations (MlNNTAC) Equipment & 

### Operating Data 

### 6. Process Equipment Description: Step 

### Ill Agglornerator Line 

### 6 Waste 

### Gas Stack (Fluoride, S0 2 , 

### CO. VOC tests) 7. Were the process and control equipment operated consistent with nonnal procedures? VES[gj NO 

# 0 If no, explain: 8. 

### Include copy of production records 

### or instrumentation which indicates rate of production or operation of 

### the equipment, i.e. uuits 

### per hour, pouuds 

### per hour, pressure, air 

### flow, etc. 9. Date(s) and procedure(s) oflast maintenance/cleaning 

### within 6 months: 

## t'i5] Remains unchanged from info. provided in test 

### plan
__

## ~~--~----~~~~~~~~----~~~~~--~~~~~--~~- 10. Process rate (amount of raw material or finished product per hour, wet or dry basis) while combusting (list fuel 

### type(s) and**ratios~amJropri~e)** 

### ______________________________ ... , ...... __________ _ Green ball feed 

### rate, long tons per hour (L TPH) 

### 543.7 547.3 549.1 Pellet production 

### rate, (LTPH) 

### 480.2 482.0 489.8
Fuel Input (list units) Heat Input 

### (10" British thermal units/hour) 

### 7. Summarize control equipment operating data documented during 

### testing. Values reported should reflect 

### maxill1lliD, minimum, averages, or 

### as approved in 

### the 

### test plan. (See test plan 

### aud approval letter) Examples of 

### APC equipment and parameters generally monitored. Monitor 

### as in test plan and/or approval letter. • Scrubber (list 

### type of 

### scrubber): llP 

### (in. w.c.) and 

### feed rate (gpm and psig) • Baghouse,**Cyclone~** and Multi-clone; llP 

### (in. w.c.) • Catalytic Incinerator 

### :eFm ,°F ouJ 

### and 

### Thermal Incinerator:**°F~.err.tl':rnture)** 

### • ESP: Number and 

### identity of o 

### crating field(s)


# ,**~C'~!l!li.ll"llr:iiueter ilii!'lliior'ed''i·.c··J,~.**  <·''j; 

### if!- '.:cy'-:f,**,.,<::::t~<-:·'.** 

# '·;**;-;,;,_~:** 

# 'Rili.il' Y.··:·· I" "\:< 

## ··Rim:Z·{f,:·:•·:· 

# . ;::,:, 

# • Rlin .3:/c<' !'• 

### Wet scrubber, llP 

### (in. w.c.) 8.31 8.15 8.34 Wet scrubber, feed 

### rate (gpm) 

### 3,000 2,999 3,002 ;c,'

### .:LiS!;)i~ii:lltint:&''l!:veragirift-!J'~~;,;.shduldi:~t1ect!!emnt··**1:~::** 

# .**Rn'!i:l;\~** 

### : 

## 1\ki · ·Rllri·L 

## ,_. ;.'''> R11:U"' 

## C':/• Continuous Opacity Monitor(list hourly average)

__ Monitor (list averaging basis):

__ Monitor (list averaging basis: Abbreviations. 

### APC-air pollution control lbs.-pounds 

### gpm.-gallons per mmute psig-pressure per square inch gauge ln. w.c.-inches of water column AP- pressure drop


### Note: 

### This form provides only a sunnnary of the operating conditions during 

### the performance test. Additional and more detailed records are required to meet 

### the requirements of Minn. R. 7017.2035, subp. 3. This form is to be submitted as part of the performance test report. aq-f6-ST05 Form ST -05, Page 1 of 1

### Test Date(s): April20. 2005 Process Equipment Number/Identification: "'SV_,_,_15""!'------ Company Name: U. S. Steel Minnesota Ore Operations- (MINNTAC) Equipment & 

### Operating Data 11. Process Equipment Description: Step 

### 11! Agglornerator Line 7 Waste Gas Stack (PM. Fluoride, SO,, CO, VOC tests) 

## 12. Were the process and control equipment operated consistent 

### \Vith normal procedures? 

## YES[gJ NOD If no, 

### explain: 13. Include copy of production records or instrumentation which indicates rate of production or operation of the equipment, i.e. units per 

### hour, pounds per hour, pressure, air flow, etc. 14, Date( s) and procedure( s) of last maintenance/cleaning 

### within 6 months: 

# !2J Remains unchanged from info. provided in test

## p~n**----~----~----~~~~~--~----~------~~~~~------~~~~-------** 15. Process rate (amount of raw material or finished product per hour, wet or dry basis} while combusting (list fuel type(s) and**ratiosasa~~opriate)** 

### ________________________________________ _

8. Surnn:tarize control equipment operating data 

### documented during testing. Values reported should reflect maximum, rniniroum, 

### averages, or as approved in the test plan. (See test plan and approval letter) Examples of APC equipment and parameters generally monitored. Monitor as in test plan and/or approval letter. • Scrubber (list type of scrubber): LIP 

### (in. w.c.) 

### and feed rate (gpm and psig) • Baghouse, Cyclone, and Multi-clone: LJ.P (in. w.c.)

## ~:("F;, ,°F,,,) 

### and

## ~**-~** '"" · ' • ESJ 

### :and identity l 

### field( s)



### .... ·,,**~ ~-**  ' 

# ·, 

# ' 

# ,, :,, ., 'R••"**~** 

# ,, .'co<> 

### :. :' I;.RUU .:f;, :. 

# __ .**:c~,** 

# .,:--;,,; ;:;,_, :x:·<: _ Wet scrubber, LIP (in. w.c.) 

### 7.53 

### 7.55 7.57 

### Wet scrubber, feed rate (gpm) 

### 3,002 

### 2,997 3,002

" 

### :,,, Runli ' ·_ > I :: 

### :':'·;,';R_\Irtl .: .. :.) .RunL:' · ,.1 ·, 

### Continuous Opacity Monitor(llst hourly average}

___ Monitor (list averaging basis): I



### __ Monitor (list averaging basis: Abbreviations; APC-air 

### pollution control gpm.-gallons per minute in. w**.c.~incbes** 

### ; column 

### lbs.-pounds psig-pressure per square inch gauge**AP~** 

### pressure 

### drop
Note: This form provides only a summary of the operating conditions during the performance test. Additional and more detailed records are required to meet the requirements of Minn. 

### R. 7017.2035, subp. 3. This form is to be submitted as part of the performance test report. aq-f6-STOS Form ST -05, Page 1 of 1

### ANALYSES OF COAL SAMPLES TAKEN DURING STACK TESTING 

## Agglomerator line 6 and line 7

-- April18 & 

## 19, 2005 Dry Basis As Received Basis 

### BTU/Ib %5 % 

### H 2 

### 0 BTU/Ib % 

### S 

### line 6 11,831 0.405 29.5 9,136 0.313 

### line 7 11,483 0.426 27.2 9,027 0.335

# Appendix/ Stack Test Plan

# ~.·•·••··;·~~~"; 

# ·.······"··.·.
..**:."f~~~~~~~~.~~··~:~$~~~,!~~;~~;~:~x~~··•·······** 

# . ., '

.. ·.



### AQ#26A Facility Name: US Steel-Minnesota Ore Operations 

### Facility Contact: Ms. Chrissy Bartovich 

### Address: P.O. Box 417, 8819 Old Highway 169, Mountain lron, MN 55768 Fax: 

### (218) 749-7360 

### Emission Unit(s): Group II Agglomerator Line 6 and 7 (SV!44, SV151) and Group 13 Crusher (SV054) 

### Scheduled For: April 18, 2005, 

### at your Facility located in Mountain lron, 

### Minnesota. Your test plan submitted on March 22, 2005, and discussed on April 11, 2005, has been approved by the Minnesota Pollution Control Agency (MPCA) as follows: 

# 0 Shortened test notification approved 

# 0 Test plan approved without modification**~** 

### Test plan approved with the foiiowing provisions: PM! 0 will be determined via Method 5 plus Method 202 (dry 

## + organic condensibles 

## + inorganic condensib Jes). Equipment should be operated at maximum capacity during testing. Include process equipment and control equipment operating rates on the Operating Data Sunnnary form. Include in the fmal test report(s) 

### the 

## fuii reference method data record (strip chart and/or datalogger output) used to calculate emissions. The data record should include calibration values for any instrumental analyzer used for emissions compliance testing. Include in the fmal test report a simplified drawing of the test locations including pollution control equipment, stack orientation and test port locations.



### Attached Forms:



# 0 Operating Data Sunnnary- Combustion Sources**~** 

### Operating Data Sunnnary- Process Sources**~** 

### Certifications Form 

# 0 Operating Data Summary- Waste Combustors 

# 0 Operating Data Summary- Asphalt Plants**~** 

### Microfiche/CD-ROM Submittal Form Note: Forms are also available at: www.pca.state.mn.us/air/performancetest.html 

### Approved by:
Andrew Place Performance Test Coordinator Compliance and Enforcement Section Industrial Division 

### Date: Aprilll, 2005

### Please contact me at (651) 296-7169 if you have any questions regarding 

### this approval. Please be aware that enforcement action will be taken for performance test failures indicating emissions above applicable limits (excess actual emissions to the environment). Failures commonly result in assessment of a monetary penalty. Upon the first test failure, the Company should take immediate measures to minimize emissions. The measures taken should be documented, as they 

### will become part of the record of corrective actions. Hard Copy Performance Test Reports and Microfiche or CD Copy submittals 'Will be addressed to: Compliance Tracking Coordinator, Compliance and Enforcement Unit, Industrial Division, Minnesota Pollution Control Agency, 520 Lafayette Road North, St. Paul, Minnesota 55155-4194


### cc: Richard Berg, Barr Engineering, Minneapolis (email) Bob Beresford, MPCA, Duluth (email) AQ Correspondence File No. 26AU. S. Stee Corporation Mionesota Ore Operations 

### P.O. Box 417 Mt. Iron, 

### MN 55768



### March 18, 2005 Mr. Andrew Place North District, Major Facilities Minnesota Pollution Control Agency 520 Lafayette Road St. Paul, Minnesota 55155-3898
RE: USS- Minnesota Ore Operations (Minntac) Notification of Testing and Test Plan Dear Andrew, This document is the Notification of Testing and Test Plan for performance tests to be conducted during the week of April 

## J 8, 2005. Tests will be performed on the Agglomerator Line 6 and Line 7 waste 

### gas stacks (SV144 and SV151 respectively), and the Crusher 078-01-2501 tertiary crusher dust collector (SV054). Notification was previously given to test the Crusher dust collector, SV054. The test was to have been conducted during the week of February 14-18, but could not be completed because of a process line breakdown. An extension was granted by Andy Place of the MPCA following e-mail communications 

## with Ray Potts ofMinntac. 

# TEST PLAN Part 1. General Information (1) Name and address of the emission facility. U.S. Steel- Minnesota Ore Operations Minntac Plant P.O.Box417 8819 OldHvvy 169 Mountain Iron, Minnesota 55768 (2) Name, title and telephone number of contact person at the emission facility. Chrissy Bartovich Environmental Control Engineer Voice phone 218-749-7364 Fax phone 218-749-7360 Electronic mail: c!bru1ovichlalus.;;.com (3) Permit number or name of other applicable document.

- 1-

### Agglomerator Line 6 and Line 7 --pending Air Emissions Permit 13700005-004 (PSD Permit) Crusher dust collector-- air Emissions Permit 13700005-003 (Title V Permit) for the ( 4) Reason for testing. Agglomerator Line 6 and Line 7

-- Initial performance test Crusher dust collector-- Title V compliance for PM and Opacity of emissions 

## '/ (5) Schematic drawing of the stacks and sample ports. Enclosed herein. a) Location of Plant Within the corporate limits of the city of Mountain Iron, MN. b) Name, contact person, and telephone number for testing company Barr Engineering, Minneapolis, MN. Richard Berg (952) 832-2787 

## Part 2. Testing Requirements (1) List of pollutants to be tested, the emission limit for each pollutant and the applicable rule or regulation for the emission limit. 

### Group 11 Agglomerator Line 6 and Line 7 --PM, PM 10 , 

### Opacity, CO, S0 2 , 

### VOC, and Fluoride There are no permitted emissions limits for PM 10 

### CO, VOC and Fluoride until the PSD · permit is in effect. The following emissions limits are in effect. Particulate Matter (PM)

Opacity Minn. R 7011.0610 subp. l(A)(J) 0.30 grains per dry standard cubic foot, or the less stringent of either Minn. R 7011.0730 or Minn. R. 7011.0735
Minn. R 7011.0610 subp. l(A)(2) Less than or equal to 20% except for one six-minute period per hour of not more than 60% opacity.

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### Sulfur Dioxide (S0 2 ) 

### 4lb!MMBTU (solid fuel), Minn. R 7011.0610 subp. 2(B)(l) or Minn. R 7007.0800 subp. 2, subp. 4(B) alternative material balance detennination of SO, 

### Group 13 Crusher 078-0l-25Gl 

### dust collector-- PM and Opacity Particulate Matter (PM) Minn.R 7011.0715 subp. l(A) 0.30 grains per 

### dry standard cubic foot, or the Jess stringent of either Minn. R '/ 7011.0730 or Minn. 

### R. 7011.0735 Opacity Minn. R 7011.0610 subp. l(B) Less than or equal to 20% opacity
.

. (2) Description of procedure for fuel sampling and analysis, where applicable. Coal will be sampled during the testing and analyzed for moisture, Btu value, and sulfur content. 

## Part 3. Operating Conditions (I) List the process or operating rate and conditions of the process equipment and the air pollution control equipment for 

### the test. All tests will be performed while the associated process equipment is operating normally and all control equipment will be operated normally. Green ball feed rnte range 525 to 600 L TPH during both tests Fuel will be a blend of natural gas and western coal during both tests. The emission units associated with the SV054 collector include 4 bins that feed 8 crushers. 

### It is the operator's goal to keep the bins optimized but there are situations, feed to 

### the crushers may actually stop for short periods of time. For 

## that reason we have estimated large ranges of operating rates for the collectors. (2) Explanation of why the proposed conditions are considered to be in accordance with Part 7017.2025, Subpart 2, for required testing conditions. The statement about the assumption of worst case conditions in the cited subpart applies. (3) List the range of process or operating rates for this emission unit. The minimum process rate is zero. The maximum is approximately 600 long tons per hour of green ball feed rate.**~** 

### 3

-

### SV054 serves the inlet 

## to 4 surge bins that feed 8 third.stage crushers. It is anticipated that, during the testing, the bins will be filled at a rate of between 1600 and 4000 long tons per hour. (4) Descriptions of how air pollution control and process equipment wilt be monitored. The emission control units 

## will be monitored for pressure drop and water flow during all tests. The 078-0l-25G 1 (SV054) dust collector is a wet scrubber and will be monitored for wa:ter flow and pressure drop 

### during the tests. Scrubber water flow rates and pressure drops will be recorded at least every fifteen minutes during the testing. Process rates will be monitored during all three test runs for the stack. There are no weigh scales associated with the 078-01-25Gl (SV054). For this collector the process weight will be the average output from the four bins (the sum of the crushers being fed from the bins). The assumption is that the feed to the bins should be approximately equal to what is being discharged from them. 

## Part 4. Test Methods (I) List ofthe methods to be used to determine the emission rate of each pollutant. Test Port Location ·Determination of velocity and volumetric flow Determination of gas molecular weight Determination of moisture content Determination of PM Determination of Condensable PM Determination of CO concentration Determination of VOC concentration Determination of S0 2 

### concentration Determination of Fluoride concentration Visual Determination of the Opacity of Emissions EPA Method 1 EPAMethod2 EPA Method 3A EPAMethod4 EPA MethodS EPA Method 202 EPA Method I 0 EPA Method 25A EPA Method 6C EPA Method l3B EPA Method 9 Note- both filterable and condensable particulate matter will he measured. PM 10 

### measurements (Method 20 lA) cannot be made at the waste 

### gas stack because of high moisture content in the gas stream. PM 10 

## will be determined by adding the inorganic condensible particulates to the dry plus inorganic particulates. (2) Numher of test runs, length of the test runs, and sampling rate for each method. 3 one-hour test runs except for Methods I, 2 and 9 Method 9 will be 1 one-hour observation performed in conjunction with one Method 5 test run.

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### (3) Reference to any compliance document, federal regulation, or Minnesota rule or statute requiring use of specific methods or procedures. Not applicable 

### (4) Summary ofreasons for proposing to use alternative or equivalent method. None proposed 

### (5) For test methods other than reference methods, statement of the detection limit and the degree· of 

### accuracy of that method at the expected emission rate and under the conditions of the performance test. None applicable 

## Test Schedule and Pretest Meeting The testing is scheduled to occur during the week of April 19-22, 2005. At the preference of the l:vfPCA, we would suggest the pretest meeting could occur no less than 

## 7 days before the testing begins and be conducted via telephone. 

## Closing Remarks If there are any questions or comments on the information given in this document, please contact me at the telephone numbers listed above.

# ~ic~J Environmental Control Engineer Enclosures: STEP3 AGG WG.doc 078..01-25Gl (SV054) drawing Advance copy by email CERTIFIED MAIL# 7003 2260 0000 2381 8040
cc: Robert Beresford, l:vfPCA- Duluth Regional Office Hongming Jiang, l:vfPCA North District Major Facilities Richard Berg- Barr Engineering 

### Ray Potts

- Minntac Cory 

## Bird- Minntac



### -5-

## 16.0' Diam.
25.0'

Varies 4.0-6.0.' 

# "T--+--+---+--l: 0 :--+--Four Sample Points@ 

### 90'

// 

# ROOF

WET SCRUBBER

24.0'

Elevation View 

## 24.0'

1. Emission Source Number- Line 6 SV 144 

### & Line 7 SV 151 2. Emission Unit Number- 313, 314, 315, 316 (at SV 144) 332, 333, 

### 334,335 (at SV 151) 3. Plant Equipment Number- 242-06-1; 261..()6-1; 252-06-1; 262..06-1 (or 07-1 fur 

### the Line 7 

### equipment) 4. Stack Diameter- 16.0' 5. Stack Design Gas Velocity- 52 FPS 

### 6. Stack Diameter Ga• Volume- 555,650 

### CFM 7. Stack Design Gas Temperature- 125 

### W 150°F 8. Stack Test Ports- 4 

### ea. 8" dia. Pipe nipple 

### x 7" long 

### with 150 

### lb flange. Hanger hook 

### 5' above. 9. Stack Loading- 0.024 

### GR./ Cubic Ft.

S:\air\stacks\STEP 3 AGG WG.doc 

## 42.0'



# STEP III AGGLOMERATOR WASTEGA.S

Step 

### III Agglomerator Minnesota Ore Operations Minntac, Mt. lion, MK

REVISED 01-03..00

### ROOF LINE



## SV: 054 

# US STEEL MINNESOTA ORE OPERATIONS MOUNTAIN IRON, MINNESOTA



# . STEP 1 FINE CRUSHER**~30"** 

## .**~-----** 1 

### I

### ~35' 

# 1'**~a·** 

# ----l...L_

FAN

0



### SCRUBBER 2 TEST PORTS @ 

## 90'



# TEST PORT LOCATIONS 080 BINS 5;_8 WET SCRUBBER ROOF LINE

EU: 

## 085,086,087,088,089,090,091,092 CE: 

## 040 

# DRAWING 

# # 078 01 25G1 NOT TO SCALE GROUP: 13

# AppendixJ Project Participants

## Minnesota Pollution Control Agency Andrew Place- Performance Test Coordinator Hongming Jiang- Permit Engineer U.S. Steel Corporation- Minnesota Ore Operations 

# Project Participants

Larry Salmela- Department Manager

- Safety, Environmental and Hygiene Chrissy Bartovich- Environmental Control Engineer Ron Braski

- Agglomerator Coordination Barr Engineering Company Tim Russell- Vice President/Chemical Engineer Mark Petersen- Senior Air Quality Technician/Team Leader Dan Kaschak- Environmental Engineering Technician Richard Berg- Senior Air Quality Technician

#2369927001 

### J-1