Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-001Date Collected:11/11/2013Date Received:11/12/2013 

### Field Blank

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg < 0.2 0.5 JAB EPA 1631E 0.2 11/20/2013 U



### Sample Number:134582-002Date Collected:11/11/2013Date Received:11/12/2013 

### CPS Influent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.87 0.5 DPC EPA 200.8 0.1 11/15/2013 13:36 ug/L Arsenic, As 105 1 DPC EPA 200.8 0.3 11/15/2013 13:36 ug/L Barium, Ba 67.4 1 DPC EPA 200.8 0.2 11/15/2013 13:36 ug/L Beryllium, Be < 5 20 DAM EPA 200.7 5 11/15/2013 13:39 U ug/L Cadmium, Cd 26.5 0.5 DPC EPA 200.8 0.1 11/15/2013 13:36 ug/L Chromium, Cr 29.5 2 DPC EPA 200.8 0.4 11/15/2013 13:36 ug/L Cobalt, Co 29.1 0.2 DPC EPA 200.8 0.04 11/15/2013 13:36 ug/L Copper, Cu 29.6 0.5 DPC EPA 200.8 0.1 11/15/2013 13:36 ug/L Lead, Pb 9.32 0.1 DPC EPA 200.8 0.02 11/15/2013 13:36 ng/L Mercury, Hg 202000 5000JAB EPA 1631E 2000 11/20/2013 ug/L Molybdenum, Mo 64.2 0.5 DPC EPA 200.8 0.1 11/15/2013 13:36 ug/L Nickel, Ni 269 2 DPC EPA 200.8 0.5 11/15/2013 13:36 ug/L Selenium, Se 105 5 DPC EPA 200.8 2 11/15/2013 13:36 ug/L Silver, Ag 0.06 0.1 DPC EPA 200.8 0.02 11/15/2013 13:36 J ug/L Thallium, Tl 1.66 0.5 DPC EPA 200.8 0.02 11/15/2013 13:36 ug/L Tin, Sn < 100 500 DAM EPA 200.7 100 11/15/2013 13:39 U ug/L Titanium, Ti 103 100 DAM EPA 200.7 20 11/15/2013 13:39 ug/L Zinc, Zn 309 5 DPC EPA 200.8 1 11/15/2013 13:36 mg/L Aluminum, Al 0.615 0.01 DPC EPA 200.8 0.003 11/15/2013 13:36 mg/L Boron, B 489 1 DAM EPA 200.7 0.2 11/15/2013 13:39 mg/L Calcium, Ca 3790 1 DAM EPA 200.7 0.2 11/15/2013 13:39 mg/L Iron, Fe 50.3 2 DAM EPA 200.7 0.5 11/15/2013 13:39 mg/L Magnesium, Mg 4300 0.5 DAM EPA 200.7 0.1 11/15/2013 13:39 mg/L Manganese, Mn 74.1 0.02DAM EPA 200.7 0.005 11/15/2013 13:39 mg/L Potassium, K 82.0 2 DAM EPA 200.7 0.4 11/15/2013 13:38 mg/L Sodium, Na 447 2 DAM EPA 200.7 0.4 11/15/2013 13:37 mg/L Strontium, Sr 31.5 0.05DAM EPA 200.7 0.02 11/15/2013 13:37 mg/L Ammonia, NH3, as N 0.72 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N12.3 5 DMM EPA 351.2 1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N44.7 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 1 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-002ADate Collected:11/11/2013Date Received:11/12/2013 

### CPS Influent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.64 0.5 DPC EPA 200.8 0.1 11/15/2013 13:41 ug/L Arsenic, As 7.96 1 DPC EPA 200.8 0.3 11/15/2013 13:41 ug/L Barium, Ba 7.30 1 DPC EPA 200.8 0.2 11/15/2013 13:41 ug/L Beryllium, Be < 5 20 DAM EPA 200.7 5 11/15/2013 13:43 U ug/L Cadmium, Cd 22.8 0.5 DPC EPA 200.8 0.1 11/15/2013 13:41 ug/L Chromium, Cr 1 2 DPC EPA 200.8 0.4 11/15/2013 13:41 J ug/L Cobalt, Co 23.0 0.2 DPC EPA 200.8 0.04 11/15/2013 13:41 ug/L Copper, Cu 1.43 0.5 DPC EPA 200.8 0.1 11/15/2013 13:41 ug/L Lead, Pb 0.04 0.1 DPC EPA 200.8 0.02 11/15/2013 13:41 J ng/L Mercury, Hg 21200 500 JAB EPA 1631E 200 11/20/2013 ug/L Molybdenum, Mo 53.7 0.5 DPC EPA 200.8 0.1 11/15/2013 13:41 ug/L Nickel, Ni 225 2 DPC EPA 200.8 0.5 11/15/2013 13:41 ug/L Selenium, Se 62.8 5 DPC EPA 200.8 2 11/15/2013 13:41 ug/L Selenite, Se+4 (Hydride) 348 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag < 0.02 0.1 DPC EPA 200.8 0.02 11/15/2013 13:41 U ug/L Thallium, Tl 1.39 0.5 DPC EPA 200.8 0.02 11/15/2013 13:41 ug/L Tin, Sn < 100 500 DAM EPA 200.7 100 11/15/2013 13:44 U ug/L Titanium, Ti < 20 100 DAM EPA 200.7 20 11/15/2013 13:44 U ug/L Zinc, Zn 113 5 DPC EPA 200.8 1 11/15/2013 13:41 mg/L Aluminum, Al 0.0110 0.01 DPC EPA 200.8 0.003 11/15/2013 13:41 mg/L Boron, B 514 1 DAM EPA 200.7 0.2 11/15/2013 13:43 mg/L Calcium, Ca 673 1 DAM EPA 200.7 0.2 11/15/2013 13:43 mg/L Iron, Fe < 0.5 2 DAM EPA 200.7 0.5 11/15/2013 13:44 U mg/L Magnesium, Mg 4510 0.5 DAM EPA 200.7 0.1 11/15/2013 13:43 mg/L Manganese, Mn 75.5 0.02DAM EPA 200.7 0.005 11/15/2013 13:43 mg/L Potassium, K 83.9 2 DAM EPA 200.7 0.4 11/15/2013 13:42 mg/L Sodium, Na 475 2 DAM EPA 200.7 0.4 11/15/2013 13:42 mg/L Strontium, Sr 9.62 0.05DAM EPA 200.7 0.02 11/15/2013 13:42

Mountaineer Plant, 134582 Page 2 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-003Date Collected:11/11/2013Date Received:11/12/2013 

### Primary Clarifier Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 4.88 0.05DPC EPA 200.8 0.01 11/15/2013 14:32 ug/L Arsenic, As 5.48 0.1 DPC EPA 200.8 0.03 11/15/2013 14:32 ug/L Barium, Ba 60.3 0.1 DPC EPA 200.8 0.02 11/15/2013 14:32 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 13:48 U ug/L Cadmium, Cd 95.2 0.05DPC EPA 200.8 0.01 11/15/2013 14:32 ug/L Chromium, Cr 10.5 0.2 DPC EPA 200.8 0.04 11/15/2013 14:32 ug/L Cobalt, Co 153 0.02DPC EPA 200.8 0.004 11/15/2013 14:32 ug/L Copper, Cu 8.57 0.05DPC EPA 200.8 0.01 11/15/2013 14:32 ug/L Lead, Pb 1.65 0.01 DPC EPA 200.8 0.002 11/15/2013 14:32 ng/L Mercury, Hg 5090 50 JAB EPA 1631E 20 11/20/2013 ug/L Molybdenum, Mo 556 0.05DPC EPA 200.8 0.01 11/15/2013 14:32 ug/L Nickel, Ni 1370 0.2 DPC EPA 200.8 0.05 11/15/2013 14:32 ug/L Selenium, Se 544 0.5 DPC EPA 200.8 0.2 11/15/2013 14:32 ug/L Silver, Ag 0.034 0.01 DPC EPA 200.8 0.002 11/15/2013 14:32 ug/L Thallium, Tl 9.28 0.05DPC EPA 200.8 0.002 11/15/2013 14:32 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 13:48 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 13:48 U ug/L Zinc, Zn 265 0.5 DPC EPA 200.8 0.1 11/15/2013 14:32 mg/L Aluminum, Al 0.350 0.001DPC EPA 200.8 0.0003 11/15/2013 14:32 mg/L Boron, B 441 0.2 DAM EPA 200.7 0.04 11/15/2013 13:48 mg/L Calcium, Ca 630 0.2 DAM EPA 200.7 0.04 11/15/2013 13:48 mg/L Iron, Fe 1.17 0.5 DAM EPA 200.7 0.1 11/15/2013 13:48 mg/L Magnesium, Mg 3980 0.1 DAM EPA 200.7 0.02 11/15/2013 13:48 mg/L Manganese, Mn 63.4 0.005DAM EPA 200.7 0.001 11/15/2013 13:48 mg/L Potassium, K 71.7 0.5 DAM EPA 200.7 0.07 11/15/2013 13:46 mg/L Sodium, Na 422 0.3 DAM EPA 200.7 0.08 11/15/2013 13:46 mg/L Strontium, Sr 7.88 0.01 DAM EPA 200.7 0.003 11/15/2013 13:46 mg/L Ammonia, NH3, as N 2.84 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N6.17 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N36.7 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 3 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-003ADate Collected:11/11/2013Date Received:11/12/2013 

### Primary Clarifier Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 4.35 0.05DPC EPA 200.8 0.01 11/15/2013 14:37 ug/L Arsenic, As 4.03 0.1 DPC EPA 200.8 0.03 11/15/2013 14:37 ug/L Barium, Ba 53.0 0.1 DPC EPA 200.8 0.02 11/15/2013 14:37 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 14:17 U ug/L Cadmium, Cd 85.0 0.05DPC EPA 200.8 0.01 11/15/2013 14:37 ug/L Chromium, Cr 3.0 0.2 DPC EPA 200.8 0.04 11/15/2013 14:37 ug/L Cobalt, Co 137 0.02DPC EPA 200.8 0.004 11/15/2013 14:37 ug/L Copper, Cu 4.69 0.05DPC EPA 200.8 0.01 11/15/2013 14:37 ug/L Lead, Pb 0.022 0.01 DPC EPA 200.8 0.002 11/15/2013 14:37 ng/L Mercury, Hg 2580 50 JAB EPA 1631E 20 11/20/2013 ug/L Molybdenum, Mo 496 0.05DPC EPA 200.8 0.01 11/15/2013 14:37 ug/L Nickel, Ni 1240 0.2 DPC EPA 200.8 0.05 11/15/2013 14:37 ug/L Selenium, Se 496 0.5 DPC EPA 200.8 0.2 11/15/2013 14:37 ug/L Selenite, Se+4 (Hydride) 393 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.015 0.01 DPC EPA 200.8 0.002 11/15/2013 14:37 ug/L Thallium, Tl 8.41 0.05DPC EPA 200.8 0.002 11/15/2013 14:37 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 14:17 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 14:17 U ug/L Zinc, Zn 222 0.5 DPC EPA 200.8 0.1 11/15/2013 14:37 mg/L Aluminum, Al 0.0294 0.001DPC EPA 200.8 0.0003 11/15/2013 14:37 mg/L Boron, B 456 0.2 DAM EPA 200.7 0.04 11/15/2013 14:17 mg/L Calcium, Ca 649 0.2 DAM EPA 200.7 0.04 11/15/2013 14:17 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/15/2013 14:17 U mg/L Magnesium, Mg 4070 0.1 DAM EPA 200.7 0.02 11/15/2013 14:17 mg/L Manganese, Mn 65.3 0.005DAM EPA 200.7 0.001 11/15/2013 14:17 mg/L Potassium, K 72.3 0.5 DAM EPA 200.7 0.07 11/15/2013 14:15 mg/L Sodium, Na 428 0.3 DAM EPA 200.7 0.08 11/15/2013 14:15 mg/L Strontium, Sr 8.01 0.01 DAM EPA 200.7 0.003 11/15/2013 14:15

Mountaineer Plant, 134582 Page 4 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-004Date Collected:11/11/2013Date Received:11/12/2013 

### CPS Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 3.77 0.05DPC EPA 200.8 0.01 11/15/2013 14:42 ug/L Arsenic, As 3.92 0.1 DPC EPA 200.8 0.03 11/15/2013 14:42 ug/L Barium, Ba 58.9 0.1 DPC EPA 200.8 0.02 11/15/2013 14:42 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 14:26 U ug/L Cadmium, Cd 4.62 0.05DPC EPA 200.8 0.01 11/15/2013 14:42 ug/L Chromium, Cr 1.9 0.2 DPC EPA 200.8 0.04 11/15/2013 14:42 ug/L Cobalt, Co 95.2 0.02DPC EPA 200.8 0.004 11/15/2013 14:42 ug/L Copper, Cu 1.14 0.05DPC EPA 200.8 0.01 11/15/2013 14:42 ug/L Lead, Pb 0.140 0.01 DPC EPA 200.8 0.002 11/15/2013 14:42 ng/L Mercury, Hg 254 20 JAB EPA 1631E 8 11/20/2013 ug/L Molybdenum, Mo 414 0.05DPC EPA 200.8 0.01 11/15/2013 14:42 ug/L Nickel, Ni 967 0.2 DPC EPA 200.8 0.05 11/15/2013 14:42 ug/L Selenium, Se 458 0.5 DPC EPA 200.8 0.2 11/15/2013 14:42 ug/L Silver, Ag 0.005 0.01 DPC EPA 200.8 0.002 11/15/2013 14:42 J ug/L Thallium, Tl 3.06 0.05DPC EPA 200.8 0.002 11/15/2013 14:42 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 14:27 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 14:27 U ug/L Zinc, Zn 165 0.5 DPC EPA 200.8 0.1 11/15/2013 14:42 mg/L Aluminum, Al 0.0728 0.001DPC EPA 200.8 0.0003 11/15/2013 14:42 mg/L Boron, B 388 0.2 DAM EPA 200.7 0.04 11/15/2013 14:26 mg/L Calcium, Ca 536 0.2 DAM EPA 200.7 0.04 11/15/2013 14:26 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/15/2013 14:27 U mg/L Magnesium, Mg 3490 0.1 DAM EPA 200.7 0.02 11/15/2013 14:26 mg/L Manganese, Mn 58.2 0.005DAM EPA 200.7 0.001 11/15/2013 14:26 mg/L Potassium, K 61.6 0.5 DAM EPA 200.7 0.07 11/15/2013 14:25 mg/L Sodium, Na 356 0.3 DAM EPA 200.7 0.08 11/15/2013 14:25 mg/L Strontium, Sr 6.73 0.01 DAM EPA 200.7 0.003 11/15/2013 14:25 mg/L Ammonia, NH3, as N 3.22 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N5.52 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N34.7 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 5 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-004ADate Collected:11/11/2013Date Received:11/12/2013 

### CPS Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 3.64 0.05DPC EPA 200.8 0.01 11/15/2013 14:47 ug/L Arsenic, As 3.71 0.1 DPC EPA 200.8 0.03 11/15/2013 14:47 ug/L Barium, Ba 55.7 0.1 DPC EPA 200.8 0.02 11/15/2013 14:47 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 14:36 U ug/L Cadmium, Cd 2.88 0.05DPC EPA 200.8 0.01 11/15/2013 14:47 ug/L Chromium, Cr 1.4 0.2 DPC EPA 200.8 0.04 11/15/2013 14:47 ug/L Cobalt, Co 89.1 0.02DPC EPA 200.8 0.004 11/15/2013 14:47 ug/L Copper, Cu 0.72 0.05DPC EPA 200.8 0.01 11/15/2013 14:47 ug/L Lead, Pb 0.560 0.01 DPC EPA 200.8 0.002 11/15/2013 14:47 ng/L Mercury, Hg 9.0 2 JAB EPA 1631E 0.8 11/20/2013 ug/L Molybdenum, Mo 395 0.05DPC EPA 200.8 0.01 11/15/2013 14:47 ug/L Nickel, Ni 918 0.2 DPC EPA 200.8 0.05 11/15/2013 14:47 ug/L Selenium, Se 431 0.5 DPC EPA 200.8 0.2 11/15/2013 14:47 ug/L Selenite, Se+4 (Hydride) 375 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.003 0.01 DPC EPA 200.8 0.002 11/15/2013 14:47 J ug/L Thallium, Tl 2.69 0.05DPC EPA 200.8 0.002 11/15/2013 14:47 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 14:36 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 14:36 U ug/L Zinc, Zn 155 0.5 DPC EPA 200.8 0.1 11/15/2013 14:47 mg/L Aluminum, Al 0.0242 0.001DPC EPA 200.8 0.0003 11/15/2013 14:47 mg/L Boron, B 392 0.2 DAM EPA 200.7 0.04 11/15/2013 14:36 mg/L Calcium, Ca 545 0.2 DAM EPA 200.7 0.04 11/15/2013 14:36 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/15/2013 14:36 U mg/L Magnesium, Mg 3540 0.1 DAM EPA 200.7 0.02 11/15/2013 14:36 mg/L Manganese, Mn 58.9 0.005DAM EPA 200.7 0.001 11/15/2013 14:36 mg/L Potassium, K 63.5 0.5 DAM EPA 200.7 0.07 11/15/2013 14:34 mg/L Sodium, Na 362 0.3 DAM EPA 200.7 0.08 11/15/2013 14:34 mg/L Strontium, Sr 6.86 0.01 DAM EPA 200.7 0.003 11/15/2013 14:34

Mountaineer Plant, 134582 Page 6 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-005Date Collected:11/11/2013Date Received:11/12/2013 

### Landfill Leachate

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 10.5 0.05DPC EPA 200.8 0.01 11/15/2013 14:52 ug/L Arsenic, As 29.4 0.1 DPC EPA 200.8 0.03 11/15/2013 14:52 ug/L Barium, Ba 37.8 0.1 DPC EPA 200.8 0.02 11/15/2013 14:52 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 14:45 U ug/L Cadmium, Cd 51.2 0.05DPC EPA 200.8 0.01 11/15/2013 14:52 ug/L Chromium, Cr 1.4 0.2 DPC EPA 200.8 0.04 11/15/2013 14:52 ug/L Cobalt, Co 63.3 0.02DPC EPA 200.8 0.004 11/15/2013 14:52 ug/L Copper, Cu 2.42 0.05DPC EPA 200.8 0.01 11/15/2013 14:52 ug/L Lead, Pb 0.241 0.01 DPC EPA 200.8 0.002 11/15/2013 14:52 ng/L Mercury, Hg 276 10 JAB EPA 1631E 4 11/20/2013 ug/L Molybdenum, Mo 5710 0.05DPC EPA 200.8 0.01 11/15/2013 14:52 ug/L Nickel, Ni 522 0.2 DPC EPA 200.8 0.05 11/15/2013 14:52 ug/L Selenium, Se 399 0.5 DPC EPA 200.8 0.2 11/15/2013 14:52 ug/L Silver, Ag 0.006 0.01 DPC EPA 200.8 0.002 11/15/2013 14:52 J ug/L Thallium, Tl 5.70 0.05DPC EPA 200.8 0.002 11/15/2013 14:52 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 14:46 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 14:45 U ug/L Zinc, Zn 146 0.5 DPC EPA 200.8 0.1 11/15/2013 14:52 mg/L Aluminum, Al 0.154 0.001DPC EPA 200.8 0.0003 11/15/2013 14:52 mg/L Boron, B 206 0.2 DAM EPA 200.7 0.04 11/15/2013 14:45 mg/L Calcium, Ca 485 0.2 DAM EPA 200.7 0.04 11/15/2013 14:45 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/15/2013 14:46 U mg/L Magnesium, Mg 1660 0.1 DAM EPA 200.7 0.02 11/15/2013 14:45 mg/L Manganese, Mn 23.3 0.005DAM EPA 200.7 0.001 11/15/2013 14:45 mg/L Potassium, K 116 0.5 DAM EPA 200.7 0.07 11/15/2013 14:44 mg/L Sodium, Na 1650 0.3 DAM EPA 200.7 0.08 11/15/2013 14:44 mg/L Strontium, Sr 6.90 0.01 DAM EPA 200.7 0.003 11/15/2013 14:44 mg/L Ammonia, NH3, as N 1.88 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.52 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N18.5 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 7 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-005ADate Collected:11/11/2013Date Received:11/12/2013 

### Landfill Leachate Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 9.77 0.05DPC EPA 200.8 0.01 11/15/2013 14:57 ug/L Arsenic, As 26.2 0.1 DPC EPA 200.8 0.03 11/15/2013 14:57 ug/L Barium, Ba 33.9 0.1 DPC EPA 200.8 0.02 11/15/2013 14:57 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 14:55 U ug/L Cadmium, Cd 48.8 0.05DPC EPA 200.8 0.01 11/15/2013 14:57 ug/L Chromium, Cr 0.9 0.2 DPC EPA 200.8 0.04 11/15/2013 14:57 ug/L Cobalt, Co 59.4 0.02DPC EPA 200.8 0.004 11/15/2013 14:57 ug/L Copper, Cu 1.81 0.05DPC EPA 200.8 0.01 11/15/2013 14:57 ug/L Lead, Pb 0.010 0.01 DPC EPA 200.8 0.002 11/15/2013 14:57 ng/L Mercury, Hg 53.2 2 JAB EPA 1631E 0.8 11/20/2013 ug/L Molybdenum, Mo 5460 0.05DPC EPA 200.8 0.01 11/15/2013 14:57 ug/L Nickel, Ni 495 0.2 DPC EPA 200.8 0.05 11/15/2013 14:57 ug/L Selenium, Se 377 0.5 DPC EPA 200.8 0.2 11/15/2013 14:57 ug/L Selenite, Se+4 (Hydride) 317 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.003 0.01 DPC EPA 200.8 0.002 11/15/2013 14:57 J ug/L Thallium, Tl 5.55 0.05DPC EPA 200.8 0.002 11/15/2013 14:57 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 14:55 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 14:55 U ug/L Zinc, Zn 131 0.5 DPC EPA 200.8 0.1 11/15/2013 14:57 mg/L Aluminum, Al 0.0506 0.001DPC EPA 200.8 0.0003 11/15/2013 14:57 mg/L Boron, B 205 0.2 DAM EPA 200.7 0.04 11/15/2013 14:55 mg/L Calcium, Ca 485 0.2 DAM EPA 200.7 0.04 11/15/2013 14:55 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/15/2013 14:55 U mg/L Magnesium, Mg 1660 0.1 DAM EPA 200.7 0.02 11/15/2013 14:55 mg/L Manganese, Mn 23.1 0.005DAM EPA 200.7 0.001 11/15/2013 14:55 mg/L Potassium, K 115 0.5 DAM EPA 200.7 0.07 11/15/2013 14:54 mg/L Sodium, Na 1640 0.3 DAM EPA 200.7 0.08 11/15/2013 14:54 mg/L Strontium, Sr 6.84 0.01 DAM EPA 200.7 0.003 11/15/2013 14:54

Mountaineer Plant, 134582 Page 8 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-006Date Collected:11/11/2013Date Received:11/12/2013 

### 1st Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 7.03 0.05DPC EPA 200.8 0.01 11/15/2013 15:02 ug/L Arsenic, As 15.8 0.1 DPC EPA 200.8 0.03 11/15/2013 15:02 ug/L Barium, Ba 51.1 0.1 DPC EPA 200.8 0.02 11/15/2013 15:02 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 15:04 U ug/L Cadmium, Cd 27.1 0.05DPC EPA 200.8 0.01 11/15/2013 15:02 ug/L Chromium, Cr 1.9 0.2 DPC EPA 200.8 0.04 11/15/2013 15:02 ug/L Cobalt, Co 82.5 0.02DPC EPA 200.8 0.004 11/15/2013 15:02 ug/L Copper, Cu 1.87 0.05DPC EPA 200.8 0.01 11/15/2013 15:02 ug/L Lead, Pb 0.142 0.01 DPC EPA 200.8 0.002 11/15/2013 15:02 ng/L Mercury, Hg 275 10 JAB EPA 1631E 4 11/20/2013 ug/L Molybdenum, Mo 2950 0.05DPC EPA 200.8 0.01 11/15/2013 15:02 ug/L Nickel, Ni 790 0.2 DPC EPA 200.8 0.05 11/15/2013 15:02 ug/L Selenium, Se 445 0.5 DPC EPA 200.8 0.2 11/15/2013 15:02 ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 11/15/2013 15:02 J ug/L Thallium, Tl 4.26 0.05DPC EPA 200.8 0.002 11/15/2013 15:02 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 15:05 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 15:05 U ug/L Zinc, Zn 164 0.5 DPC EPA 200.8 0.1 11/15/2013 15:02 mg/L Aluminum, Al 0.135 0.001DPC EPA 200.8 0.0003 11/15/2013 15:02 mg/L Boron, B 309 0.2 DAM EPA 200.7 0.04 11/15/2013 15:04 mg/L Calcium, Ca 515 0.2 DAM EPA 200.7 0.04 11/15/2013 15:04 mg/L Iron, Fe 0.2 0.5 DAM EPA 200.7 0.1 11/15/2013 15:05 J mg/L Magnesium, Mg 2690 0.1 DAM EPA 200.7 0.02 11/15/2013 15:04 mg/L Manganese, Mn 43.4 0.005DAM EPA 200.7 0.001 11/15/2013 15:04 mg/L Potassium, K 84.8 0.5 DAM EPA 200.7 0.07 11/15/2013 15:03 mg/L Sodium, Na 911 0.3 DAM EPA 200.7 0.08 11/15/2013 15:03 mg/L Strontium, Sr 6.79 0.01 DAM EPA 200.7 0.003 11/15/2013 15:03 mg/L Ammonia, NH3, as N 2.36 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N5.01 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N32.1 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 9 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-006ADate Collected:11/11/2013Date Received:11/12/2013 

### 1st Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 6.44 0.05DPC EPA 200.8 0.01 11/15/2013 15:08 ug/L Arsenic, As 12.6 0.1 DPC EPA 200.8 0.03 11/15/2013 15:08 ug/L Barium, Ba 44.4 0.1 DPC EPA 200.8 0.02 11/15/2013 15:08 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 15:14 U ug/L Cadmium, Cd 23.7 0.05DPC EPA 200.8 0.01 11/15/2013 15:08 ug/L Chromium, Cr 1.2 0.2 DPC EPA 200.8 0.04 11/15/2013 15:08 ug/L Cobalt, Co 73.7 0.02DPC EPA 200.8 0.004 11/15/2013 15:08 ug/L Copper, Cu 1.19 0.05DPC EPA 200.8 0.01 11/15/2013 15:08 ug/L Lead, Pb 0.038 0.01 DPC EPA 200.8 0.002 11/15/2013 15:08 ng/L Mercury, Hg 22.7 2 JAB EPA 1631E 0.8 11/20/2013 ug/L Molybdenum, Mo 2660 0.05DPC EPA 200.8 0.01 11/15/2013 15:08 ug/L Nickel, Ni 717 0.2 DPC EPA 200.8 0.05 11/15/2013 15:08 ug/L Selenium, Se 395 0.5 DPC EPA 200.8 0.2 11/15/2013 15:08 ug/L Selenite, Se+4 (Hydride) 361 20 TLT AEP Method 4 12/04/2013 AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 11/15/2013 15:08 J ug/L Thallium, Tl 3.82 0.05DPC EPA 200.8 0.002 11/15/2013 15:08 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 15:14 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 15:14 U ug/L Zinc, Zn 142 0.5 DPC EPA 200.8 0.1 11/15/2013 15:08 mg/L Aluminum, Al 0.0359 0.001DPC EPA 200.8 0.0003 11/15/2013 15:08 mg/L Boron, B 305 0.2 DAM EPA 200.7 0.04 11/15/2013 15:14 mg/L Calcium, Ca 509 0.2 DAM EPA 200.7 0.04 11/15/2013 15:14 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 11/15/2013 15:14 U mg/L Magnesium, Mg 2660 0.1 DAM EPA 200.7 0.02 11/15/2013 15:14 mg/L Manganese, Mn 42.7 0.005DAM EPA 200.7 0.001 11/15/2013 15:14 mg/L Potassium, K 83.7 0.5 DAM EPA 200.7 0.07 11/15/2013 15:13 mg/L Sodium, Na 896 0.3 DAM EPA 200.7 0.08 11/15/2013 15:13 mg/L Strontium, Sr 6.69 0.01 DAM EPA 200.7 0.003 11/15/2013 15:13

Mountaineer Plant, 134582 Page 10 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-007Date Collected:11/11/2013Date Received:11/12/2013 

### 2nd Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.40 0.05DPC EPA 200.8 0.01 11/15/2013 15:13 ug/L Arsenic, As 15.4 0.1 DPC EPA 200.8 0.03 11/15/2013 15:13 ug/L Barium, Ba 36.2 0.1 DPC EPA 200.8 0.02 11/15/2013 15:13 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 15:37 U ug/L Cadmium, Cd 1.17 0.05DPC EPA 200.8 0.01 11/15/2013 15:13 ug/L Chromium, Cr 1.0 0.2 DPC EPA 200.8 0.04 11/15/2013 15:13 ug/L Cobalt, Co 41.4 0.02DPC EPA 200.8 0.004 11/15/2013 15:13 ug/L Copper, Cu 0.34 0.05DPC EPA 200.8 0.01 11/15/2013 15:13 ug/L Lead, Pb 0.029 0.01 DPC EPA 200.8 0.002 11/15/2013 15:13 ng/L Mercury, Hg 79.3 2 JAB EPA 1631E 0.8 11/20/2013 ug/L Molybdenum, Mo 4190 0.05DPC EPA 200.8 0.01 11/15/2013 15:13 ug/L Nickel, Ni 200 0.2 DPC EPA 200.8 0.05 11/15/2013 15:13 ug/L Selenium, Se 11.7 0.5 DPC EPA 200.8 0.2 11/15/2013 15:13 ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 11/15/2013 15:13 J ug/L Thallium, Tl 0.43 0.05DPC EPA 200.8 0.002 11/15/2013 15:13 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 15:38 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 15:38 U ug/L Zinc, Zn 6.1 0.5 DPC EPA 200.8 0.1 11/15/2013 15:13 mg/L Aluminum, Al 0.507 0.001DPC EPA 200.8 0.0003 11/15/2013 15:13 mg/L Boron, B 211 0.2 DAM EPA 200.7 0.04 11/15/2013 15:37 mg/L Calcium, Ca 492 0.2 DAM EPA 200.7 0.04 11/15/2013 15:37 mg/L Iron, Fe 1.05 0.5 DAM EPA 200.7 0.1 11/15/2013 15:38 mg/L Magnesium, Mg 1700 0.1 DAM EPA 200.7 0.02 11/15/2013 15:37 mg/L Manganese, Mn 25.5 0.005DAM EPA 200.7 0.001 11/15/2013 15:37 mg/L Potassium, K 120 0.5 DAM EPA 200.7 0.07 11/15/2013 15:36 mg/L Sodium, Na 1620 0.3 DAM EPA 200.7 0.08 11/15/2013 15:36 mg/L Strontium, Sr 6.84 0.01 DAM EPA 200.7 0.003 11/15/2013 15:36 mg/L Ammonia, NH3, as N 0.62 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N5.51 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N1.22 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 11 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-007ADate Collected:11/11/2013Date Received:11/12/2013 

### 2nd Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.38 0.05DPC EPA 200.8 0.01 11/15/2013 15:48 ug/L Arsenic, As 13.5 0.1 DPC EPA 200.8 0.03 11/15/2013 15:48 ug/L Barium, Ba 32.8 0.1 DPC EPA 200.8 0.02 11/15/2013 15:48 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 15:47 U ug/L Cadmium, Cd 0.57 0.05DPC EPA 200.8 0.01 11/15/2013 15:48 ug/L Chromium, Cr 0.9 0.2 DPC EPA 200.8 0.04 11/15/2013 15:48 ug/L Cobalt, Co 39.0 0.02DPC EPA 200.8 0.004 11/15/2013 15:48 ug/L Copper, Cu 0.20 0.05DPC EPA 200.8 0.01 11/15/2013 15:48 ug/L Lead, Pb 0.017 0.01 DPC EPA 200.8 0.002 11/15/2013 15:48 ng/L Mercury, Hg 14.2 1 JAB EPA 1631E 0.4 11/20/2013 ug/L Molybdenum, Mo 3940 0.05DPC EPA 200.8 0.01 11/15/2013 15:48 ug/L Nickel, Ni 188 0.2 DPC EPA 200.8 0.05 11/15/2013 15:48 ug/L Selenium, Se 5.9 0.5 DPC EPA 200.8 0.2 11/15/2013 15:48 ug/L Selenite, Se+4 (Hydride)< 0.4 2 TLT AEP Method 0.4 12/04/2013 U AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 11/15/2013 15:48 U ug/L Thallium, Tl 0.38 0.05DPC EPA 200.8 0.002 11/15/2013 15:48 ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 15:47 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 15:47 U ug/L Zinc, Zn 9.4 0.5 DPC EPA 200.8 0.1 11/15/2013 15:48 mg/L Aluminum, Al 0.455 0.001DPC EPA 200.8 0.0003 11/15/2013 15:48 mg/L Boron, B 202 0.2 DAM EPA 200.7 0.04 11/15/2013 15:47 mg/L Calcium, Ca 469 0.2 DAM EPA 200.7 0.04 11/15/2013 15:47 mg/L Iron, Fe 0.979 0.5 DAM EPA 200.7 0.1 11/15/2013 15:47 mg/L Magnesium, Mg 1620 0.1 DAM EPA 200.7 0.02 11/15/2013 15:47 mg/L Manganese, Mn 24.2 0.005DAM EPA 200.7 0.001 11/15/2013 15:47 mg/L Potassium, K 114 0.5 DAM EPA 200.7 0.07 11/15/2013 15:46 mg/L Sodium, Na 1540 0.3 DAM EPA 200.7 0.08 11/15/2013 15:46 mg/L Strontium, Sr 6.53 0.01 DAM EPA 200.7 0.003 11/15/2013 15:46

Mountaineer Plant, 134582 Page 12 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-008Date Collected:11/11/2013Date Received:11/12/2013 

### Bioreactor Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.17 0.05DPC EPA 200.8 0.01 11/15/2013 15:53 ug/L Arsenic, As 0.70 0.1 DPC EPA 200.8 0.03 11/15/2013 15:53 ug/L Barium, Ba 35.2 0.1 DPC EPA 200.8 0.02 11/15/2013 15:53 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 15:57 U ug/L Cadmium, Cd 0.23 0.05DPC EPA 200.8 0.01 11/15/2013 15:53 ug/L Chromium, Cr 0.8 0.2 DPC EPA 200.8 0.04 11/15/2013 15:53 ug/L Cobalt, Co 0.096 0.02DPC EPA 200.8 0.004 11/15/2013 15:53 ug/L Copper, Cu 0.14 0.05DPC EPA 200.8 0.01 11/15/2013 15:53 ug/L Lead, Pb 0.015 0.01 DPC EPA 200.8 0.002 11/15/2013 15:53 ng/L Mercury, Hg 15.2 1 JAB EPA 1631E 0.4 11/20/2013 ug/L Molybdenum, Mo 563 0.05DPC EPA 200.8 0.01 11/15/2013 15:53 ug/L Nickel, Ni 4.81 0.2 DPC EPA 200.8 0.05 11/15/2013 15:53 ug/L Selenium, Se 2.2 0.5 DPC EPA 200.8 0.2 11/15/2013 15:53 ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 11/15/2013 15:53 J ug/L Thallium, Tl 0.02 0.05DPC EPA 200.8 0.002 11/15/2013 15:53 J ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 15:57 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 15:57 U ug/L Zinc, Zn 1.3 0.5 DPC EPA 200.8 0.1 11/15/2013 15:53 mg/L Aluminum, Al 1.33 0.001DPC EPA 200.8 0.0003 11/15/2013 15:53 mg/L Boron, B 203 0.2 DAM EPA 200.7 0.04 11/15/2013 15:57 mg/L Calcium, Ca 491 0.2 DAM EPA 200.7 0.04 11/15/2013 15:57 mg/L Iron, Fe 1.23 0.5 DAM EPA 200.7 0.1 11/15/2013 15:57 mg/L Magnesium, Mg 1680 0.1 DAM EPA 200.7 0.02 11/15/2013 15:57 mg/L Manganese, Mn 24.0 0.005DAM EPA 200.7 0.001 11/15/2013 15:57 mg/L Potassium, K 125 0.5 DAM EPA 200.7 0.07 11/15/2013 15:55 mg/L Sodium, Na 1570 0.3 DAM EPA 200.7 0.08 11/15/2013 15:55 mg/L Strontium, Sr 6.81 0.01 DAM EPA 200.7 0.003 11/15/2013 15:55 mg/L Ammonia, NH3, as N 0.48 0.05DMM EPA 350.1 0.02 11/15/2013 mg/L Total Kjeldahl Nitrogen, TKN as N7.28 0.5 DMM EPA 351.2 0.1 10/29/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N2.21 0.1 DMM SM20 4500NO3 H 0.02 11/19/2013

Mountaineer Plant, 134582 Page 13 of 14

### Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number:134582-008ADate Collected:11/11/2013Date Received:11/12/2013 

### Bioreactor Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.14 0.05DPC EPA 200.8 0.01 11/15/2013 15:58 ug/L Arsenic, As 0.65 0.1 DPC EPA 200.8 0.03 11/15/2013 15:58 ug/L Barium, Ba 32.2 0.1 DPC EPA 200.8 0.02 11/15/2013 15:58 ug/L Beryllium, Be < 1 5 DAM EPA 200.7 1 11/15/2013 16:06 U ug/L Cadmium, Cd 0.16 0.05DPC EPA 200.8 0.01 11/15/2013 15:58 ug/L Chromium, Cr 0.8 0.2 DPC EPA 200.8 0.04 11/15/2013 15:58 ug/L Cobalt, Co 0.104 0.02DPC EPA 200.8 0.004 11/15/2013 15:58 ug/L Copper, Cu 0.06 0.05DPC EPA 200.8 0.01 11/15/2013 15:58 ug/L Lead, Pb 0.022 0.01 DPC EPA 200.8 0.002 11/15/2013 15:58 ng/L Mercury, Hg 5.5 0.5 JAB EPA 1631E 0.2 11/20/2013 ug/L Molybdenum, Mo 500 0.05DPC EPA 200.8 0.01 11/15/2013 15:58 ug/L Nickel, Ni 4.67 0.2 DPC EPA 200.8 0.05 11/15/2013 15:58 ug/L Selenium, Se 1.8 0.5 DPC EPA 200.8 0.2 11/15/2013 15:58 ug/L Selenite, Se+4 (Hydride)< 0.08 0.4 TLT AEP Method 0.08 12/04/2013 U AEP Method for Se speciation is not accredited through any agency. Results are for internal use only. ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 11/15/2013 15:58 U ug/L Thallium, Tl 0.02 0.05DPC EPA 200.8 0.002 11/15/2013 15:58 J ug/L Tin, Sn < 20 100 DAM EPA 200.7 20 11/15/2013 16:06 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 11/15/2013 16:06 U ug/L Zinc, Zn 3.3 0.5 DPC EPA 200.8 0.1 11/15/2013 15:58 mg/L Aluminum, Al 1.22 0.001DPC EPA 200.8 0.0003 11/15/2013 15:58 mg/L Boron, B 206 0.2 DAM EPA 200.7 0.04 11/15/2013 16:06 mg/L Calcium, Ca 498 0.2 DAM EPA 200.7 0.04 11/15/2013 16:06 mg/L Iron, Fe 1.15 0.5 DAM EPA 200.7 0.1 11/15/2013 16:06 mg/L Magnesium, Mg 1710 0.1 DAM EPA 200.7 0.02 11/15/2013 16:06 mg/L Manganese, Mn 24.3 0.005DAM EPA 200.7 0.001 11/15/2013 16:06 mg/L Potassium, K 126 0.5 DAM EPA 200.7 0.07 11/15/2013 16:05 mg/L Sodium, Na 1580 0.3 DAM EPA 200.7 0.08 11/15/2013 16:05 mg/L Strontium, Sr 6.83 0.01 DAM EPA 200.7 0.003 11/15/2013 16:05

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224

Fax 614-836-4168Audinet 210-4224

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