Data Collection Quality 

Assurance Plan 

BWX Technologies, Inc. 

Mt. Athos Site 

Lynchburg, Virginia 

Prepared by: 

BVVX 

- 

Technologies, Inc. 

PR\ APPROVED June 2004 

JUN 1 fi :::'1

ADMINISTRATIVE REV IM - DATE 
APPENDIX F 

DATA COLLECTION QUALITY ASSURANCE PLAN 

BWX Technologies, Inc. 

Nuclear Products Division 

Mt. Athos Site, Lynchburg, Virginia 

Revised June 2004 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Table of Contents 

Page 

... List of Tables ......................................................................................................................... 111 

... List of Figures .......................................................................................................................... 111 

... List of Attachments .................................................................................................................. 111 

List of Acronyms ..................................................................................................................... iv 

I ................................................................................................................. . Introduction I- 1 

A . Data Quality Levels ........................................................................................ 1-1 

B . Data Precision, Accuracy, Representativeness, and Completeness ................ 1-2 

C ......................................................................................... . Data Comparability 1-3 .................................................................................................. I1 . Project Management I 1-3 

A ...................................................................................... . Project Organization I 1-3 

A . 1 BWXT Personnel ............................................................................... I 1-3 

A.2 Shaw Personnel .................................................................................. I 1-4 

B . Training, Certification, and Qualification ...................................................... 11-6 

I11 . Sampling Procedures .............................................................................................. 111-6 

A . General ......................................................................................................... 111-6 

B . Field Documentation .................................................................................... 111-7 

B.l Field Activity Daily Logs ................................................................ 111-7 

B.2 Sample Collection Logs ................................................................... 111-8 

B.3 Chain of Custody ............................................................................. 111-8 

C . Field Measurements ..................................................................................... 111-9 

D . Soil Borings and Sampling ........................................................................ 111-10 

E ............................................................................. . Borehole Abandonment 111- 1 1 . . F . Monitonng Well Lnstallation ...................................................................... 111-1 1 

F ............................................................................ . 1 Drilling Methods 111- 1 1 

F.2 Well Completion ............................................................................ 111- 12 

F.3 Well Development ......................................................................... 111- 13 

F.4 Aquifer Testing .............................................................................. 111- 13 

F.5 Monitoring Well Surveying ........................................................... 111-14 

G . Water Sampling ......................................................................................... 111-14 

G.l Groundwater Sampling of Monitoring Wells ................................ 111-14 

G.2 Water Supply Well Sampling ........................................................ 111-14 

G.3 Surface Water Sampling ................................................................ 111-14 

H .................................................................................... . Sediment Sampling 111- 15 

I . Collection of Quality Control Samples ...................................................... 111-1 5 

I . 1 Trip Blanks ..................................................................................... 111- 15 

1.2 Equipment Rinsate Samples .......................................................... 111- 15 

1.3 Field Blanks ................................................................................... 111- 16 

1.4 Field Duplicates ............................................................................. 111- 16 

1.5 Matrix Spike and Matrix Spike Duplicate Samples ....................... 111-16 

J ........................................................................................ . Sample Handling 111- 16 

J . 1 Order of Sample Collection ........................................................... 111- 16 

J.2 Sample Container, Preservation, and Holding Time RequirementsIII- 17 
BU'XT FEP Data Collection Quality Assurance Plan 6/10/04 

J.3 Sample Labels ................................................................................ 111-1 7 

J.4 Sample Packaging and Shipping .................................................... 111-1 7 

K . Cleaning Procedures .................................................................................. 111- 1 7 

IV . Contractor Project Documentation ........................................................................ IV- 18 

A . Record of Telephone Conferences and Meetings ...................................... IV- 18 

B ........................................................................................... . Record Storage IV- 19 

V ............................................................................................... . Laboratory Analyses V-19 

A . Laboratory Sample Receipt ......................................................................... V- 19 

B . Laboratory Instrument Calibration ............................................................. V-20 

C . Analytical Methods for Soil, Groundwater, Surface Water. and Sediment 

Samples ....................................................................................................... V-21 

D . Laboratory Quality Control Checks ............................................................ V-21 

E . Documentation of Data ............................................................................... V-21 

E.l Laboratory Sample Receipt Logbook ............................................. V-21 

E.2 Laboratory Worksheets ................................................................... V-22 

E.3 Laboratory Method Logbooks ........................................................ V-22 

E.4 Calibration Standards Logbook ..................................................... V-22 

E.5 Instrument Computer Data System Files ........................................ V-22 

F . Data ReductionIValidation Reporting ........................................................ V-22 

F . 1 Data Assessment Protocol ............................................................... V-23 

F.l.l Method Blank Evaluation ................................................... V-23 

F . 1.2 Field and Trip Blank Evaluation ......................................... V-23 

F.1.3 Method Calibration Evaluation ........................................... V-23 

F.1.4 Evaluation of Analytical Precision ..................................... V-23 

F . 1.5 Evaluation of Analytical Accuracy ..................................... V-24 

F . 1.6 Matrix Spike Evaluation ..................................................... V-24 

F . 1.7 Reference Standard Evaluation ........................................... V-24 

F.1.8 Surrogate Spike Response Evaluation ................................ V-25 

F.2 Data Reporting Format ................................................................... V-25 

F.3 Laboratory Turnaround Time ......................................................... V-26 

VI . Performance Monitoring ........................................................................................ VI-26 

A . Nonconfomance and Corrective Action ................................................... VI-26 

B . Variances .................................................................................................... VI-27 

C . Audits ......................................................................................................... VI-27 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

List of Tables 

Table 

F- 1 

List of Figures 

Figure 

F- 1 

List of Attachments 

Attachment 

A 

Title 

Analytical Data Quality Levels 

Title 

Project Organization 

Title 

Forms 

Certificates of Accreditation for Laboratories 

BWXT Services Nuclear Environmental 

Laboratory 

(all parameters except dioxinslfurans and oil 

and grease) 

Certifications by Florida and Utah 

Eno River Laboratories (dioxinslfurans) 

Sevem Trent Laboratory St. Louis (oil and 

grease) - Certification by Florida 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

List of Acronyms 

BWXT 

COC 

DCQAP 

DI 

EPA 

FADL 

MS 

MSD 

N&EO 

NEL 

NPD 

%R 

PM 

Q A 

Q AP 

QC 

RCRA 

RPD 

SAP 

SCL 

SDG 

Shaw 

SOP 

TP 

VOC 

BWX Technologies, Inc. 

chain-of-custody 

data collection quality assurance plan 

deionized 

U.S. Environmental Protection Agency 

Field Activity Daily Log 

matrix spike 

matrix spike duplicate 

Nuclear & Environmental Operations 

Nuclear Environmental Laboratory 

Nuclear Products Division 

percent recovery 

project manager 

quality assurance 

quality assurance plan 

quality control 

Resource Conservation and Recovery Act 

relative percent difference 

sampling and analysis plan 

sample collection log 

sample delivery group 

Shaw Environmental Inc. 

standard operating procedure 

technical procedure 

volatile organic compounds 
BWXT FEP Data Collection Qualitv Assurance Plan 611 0104 

DATA COLLECTION 

QUALITY ASSURANCE PLAN 

I. Introduction 

This data collection quality assurance plan (DCQAP) applies to sampling and analysis of 

environmental media at the BWX Technologies, Inc. (BWXT) Mt. Athos site. However, its 

current use is to support a task-specific Sampling and Analysis Plan for characterization of 

sludge from two Final Effluent Ponds. 

The principal data collection goals are: 

Gather and develop data in accordance with procedures appropriate for the intended use 

of the data 

Generate scientific data that will withstand scientific, regulatory, and legal scrutiny 

Generate data that are precise, accurate, representative, complete, and comparable. 

To accomplish these goals, this DCQAP provides general guidance on project management, 

field procedures, analytical procedures, and documentation. The DCQAP guidance applies to 

BWXT and its contractors during the course of sampling events conducted at the BWXT Mt. 

Athos site. 

A task-specific sampling and analysis plan (SAP) will be prepared to detail the data quality 

objectives for each sampling activity or event. The SAP will specify the sampling procedures 

and analytical methods for accomplishing the particular objectives. The SAP may vary 

procedures as needed to accomplish the objectives. Where the SAP differs from this DCQAP, 

the SAP will take precedence. 

Laboratory quality assurance (QA) at BWXT Services, Inc. Nuclear & Environmental 

Operations (N&EO) Nuclear Environmental Laboratory (NEL) is documented in the NEL 

quality assurance plan (QAP), N&EO quality implementing procedures, and the NEL technical 

procedures (TP). BWXT has also used outside laboratories to provide confirmatory and 

support analyses. 

A. Data Quality Levels 

The general levels of data quality for environmental measurements and analyses at the Mt. 

Athos site are listed in Table F-1. The table shows the intended uses of the data for the various 

analytical techniques and sample matrices, together with the appropriate analytical levels. 

These levels are: 

Level I - Field screening or analysis using portable instruments 

Level I1 - Field analysis using more sophisticated portable analytical instruments 

(possibly in a mobile laboratory) 

Level I11 - Analyses performed in an analytical laboratory. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

The SAP will select the data quality levels appropriate for the specific task. 

B. Data Precision, Accuracy, Representativeness, and Completeness 

Laboratory QA objectives for precision, accuracy, representativeness, completeness, and 

comparability are documented in the laboratory quality assurance/quality control (QNQC) 

manuals and in this DCQAP. The selection of specific laboratory analytical methods and 

detection limits will be addressed in the task-specific SAP. 

Analytical results will be calculated and reported in units consistent with the analytical 

procedures in the U.S. Environmental Protection Agency's (EPA) Test Methods for tlze 

Evaluation of Solid Waste, Physical/Clzernical Methods, SW-846, Update 111 (or latest edition) 

or other published EPA method, to allow comparability. Definitions for and means of 

assessing precision, accuracy, representativeness, and completeness are described below: 

Precision. A measure of agreement among replicate measurements of a sample. 

Comparison of replicate values is expressed as the relative standard deviation. 

Field duplicate samples and matrix spike duplicates are used to assess precision. 

Bias. Consistent deviation of a measured value from the true value, caused by a 

systematic error in procedure. Matrix spike samples are used to assess bias. 

Accuracy. The degree of agreement of a measurement X (or an average of 

replicate measurements) with an accepted reference or true value, T, usually 

expressed as the difference between the two values, X-T, or the difference as a 

percentage of the reference or true value, 100*(X-T)/T, and sometimes expressed 

as a ratio, X/T. Accuracy is a measure of bias and precision. Analytical 

accuracy is assessed through the analysis of spiked samples, known standards, 

and reference samples. 

Representativeness. Expresses the degree to which data accurately and precisely 

represent a characteristic of a population, parameter variations at a sampling 

point, a process condition, or an environmental condition. Representativeness is 

a qualitative criterion that is associated with the proper design of the sampling 

program. Representative site data will be obtained by proper preparation and 

implementation of task-specific SAPS. 

Completeness. Completeness is calculated as the percent of total usable data 

points out of the set of total data points collected, analyzed, and available. Data 

points may not be usable if sample analysis time exceeded holding times, if QC 

sample criteria were not met and reanalysis of samples is not possible, or if 

sample containers were damaged during shipping or in the laboratory. The goal 

for completeness of sample collection and analyses will typically be 90 percent or 

better. 

If it is determined that previous sampling, analytical, or QAIQC procedures did not confonn to 

currently accepted requirements, the discrepancies will be noted and the data from the previous 

investigations will be qualified accordingly. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

C. Data Comparability 

One of the data collection objectives is to provide analytical data of comparable quality 

between sample locations and with data from previous investigations. Comparability is a 

qualitative criterion measuring the confidence with which one set of data can be compared to 

another. For this project, data comparability will be achieved by the following: 

Sampling will be performed using widely recognized, well-documented procedures. 

Analyses will be performed using standardized methods and reported in appropriate 

units: micrograms per liter and milligrams per liter for aqueous samples, and 

milligrams per kilogram for soil samples. 

Additionally, to enhance comparability between samples, consideration will be given to 

seasonal conditions, stream flow, or other fluctuating environmental conditions that could 

influence the results. 

11. Project Management 

This section provides an overview of the project organization and responsibilities for 

environmental investigations at the BWXT Mt. Athos site. 

A. Project Organization 

The responsibilities of the members of the BWXT team who are involved in environmental 

investigations at the Mt. Athos site are presented below. Section A. 1 discusses BWXT 

personnel. Section A.2 discusses the personnel of Shaw Environmental, Inc. (Shaw), one of 

BWXT's prime contractors. 

A.l BWXT Personnel 

B WXTProject Manager. The BWXT project manager (PM) is responsible for representing the 

client and providing technical oversight to the contractor throughout project execution, 

approving in-scope changes, advising BWXT contracting personnel of changes that may affect 

cost andlor schedule, and issuing technical direction. The BWXT PM may designate a BWXT 

environmental engineer to coordinate work activities with the contractor PM on individual 

work tasks. BWXT may assign different PMs for various tasks under the Resource 

Conservation and Recovery Act (RCRA) environmental program depending on the nature of 

the work to be completed. 

B WXT Quality Assul-ance / Quality Control Manager. The BWXT QNQC manager will 

coordinate with the BWXT PM to establish the aspects of BWXT QNQC procedures that will 

be applied to the environmental program. 

B WXT Health and Safety Manager. The BWXT health and safety manager will coordinate 

with the BWXT PM to ensure that BWXT health and safety procedures are followed on RCRA 

environmental projects at the site. This includes providing facility-specific training for 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

contractors before they begin work at the site and maintenance of training records. The health 

and safety manager will also review project-specific health and safety plans prepared by the 

contractor and provide health physics technicians as necessary to monitor work activities or 

assist in decontamination procedures. 

3 WXT Envirorznzerztal Erzgirzeer. The BWXT environmental engineer will assist the B WXT 

PM in coordinating the activities of contractors involved in environmental work. At the 

discretion of the BWXT PM, the BWXT environmental engineer may scope work activities, 

review and approve reports, monitor field activities, and provide any assistance that the BWXT 

PM requests. 

B WXT Laboratory Project Manager. The BWXT laboratory PM will work with the contractor 

PM and project chemist on designing and implementing each task-specific analysis program. 

The laboratory PM will also: 

Verify that the laboratory achieves and maintains EPA Region 3 and Virginia 

Department of Environmental Quality approval for applicable analyses. 

Verify that the laboratory can quantify the planned parameters and routinely achieve the 

reporting limits using the methods specified in task work plans. 

Coordinate sample receipt, processing, analysis, and data reporting with members of the 

laboratory technical staff to ensure accurate and on-time deliverables. Prepare 

electronic data format for analytical files so that they can be efficiently utilized. 

Review the deliverables for completeness, accuracy, and compliance with the analysis 

program. 

B WXT Waste Treatment Manager. The BWXT waste treatment manager will manage the 

storage, transportation, and treatmentldisposal of investigative-derived waste generated during 

environmental activities at the facility. 

3 WXTLegal Counsel. The BWXT legal counsel will provide legal expertise to the BWXT 

environmental project team and coordinate efforts with outside legal counsel. 

A.2 Shaw Personnel 

Shaw personnel associated with the environmental activities at BWXT may include various 

engineering and scientific disciplines, such as geologists; hydrogeologists; chemists; 

microbiologists; civil, electrical, mechanical, and chemical/process engineers; sampling 

technicians; QAJQC coordinators; health and safety professionals; and subcontractor personnel. 

Figure F-1 shows the organization of the Shaw project team as it relates to QA responsibilities 

and lines of communication. 

Shaw Project Manager The Shaw PM is responsible for the effective execution of contracted 

environmental work. The Shaw PM oversees the activities of all Shaw personnel, ensures 

compliance with the scope of work, and controls project consistency. The Shaw PM is 

responsible for ensuring that all work activities on the project are completed in compliance with 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

the QAIQC procedures established for the project. The Shaw PM provides the BWXT PM with 

a Shaw point-of-contact for the project. 

Shaw Geo-Environmental Engineer. The Shaw geo-environmental engineer is responsible for 

supervising and issuing major task work plans and reports. The geo-environmental engineer is 

a technical specialist, providing technical expertise in the areas of investigative methods, 

hydrogeology, and risk assessment. The Shaw geo-environmental engineer will coordinate with 

the PM and other team members in the preparation of task-specific work plans to ensure project 

consistency. 

Shaw Field Coordinator. The Shaw field coordinator will be the coordinator/liaison to BWXT 

personnel and will oversee on-site activities, including site investigation, remediation and 

treatment support, long-term monitoring, utility clearances, and site maintenance. The field 

coordinator's responsibilities include ensuring that planned project objectives are met and that 

on-site activities are executed in a technically sound way and with regard to quality and health 

and safety. 

Shaw Project Chemist/Data Coordinator. The project chemist will work with the project team 

in formulating plans and approaches and will help to assess sampling, analytical, and QNQC 

requirements for each project task. The project chemist will help to ensure consistency of 

approach among the various tasks regarding these areas. The project chemist will review 

analytical data and assist in the interpretation and use of sampling and QNQC data. The 

project chemist will also serve as the data coordinator for this project. 

The data coordinator will support the field team's sample collection and documentation efforts 

by preparing project forms, labels, and logs as needed. The data coordinator will work with the 

project team and the analytical laboratory to ensure the complete and accurate transfer of 

samples and information from the field into the laboratory. This individual also receives and 

reviews analytical data. The data coordinator verifies the receipt of incoming field data and 

analytical data from the laboratory in both hard copy and electronic formats. The data 

coordinator will oversee and track the data review process and the preparation and submittal of 

the database deliverables. The data coordinator and project chemist will work together to 

identify and resolve analytical issues and nonconformances. Other responsibilities of the 

project chemistldata coordinator include: 

Interfacing with the laboratory PM to ensure the laboratory is aware of the project data 

quality objectives, program goals, and analytical QNQC objectives. 

Monitor the QNQC deliverables from the laboratory; ensure conformance with 

policies, procedures, and sound practices; and assist in identifying and resolving 

nonconfonnances. 

Ensure that all records, logs, standard procedures, and plans are distributed to the 

laboratory PM and Shaw field coordinator. 

Ensure that sampling is conducted in a manner consistent with the QA program through 

ongoing communication with field personnel. 

Review all laboratory data before those data are transferred to permanent storage or 

reported to other project participants. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Coordinate validation of laboratory data and provide a data quality summary report for 

data presentation in reports on an as-needed basis. 

Shaw Regulatory Specialist. The Shaw regulatory specialist will provide the BWXT 

environmental project team members with expertise on the RCRA regulatory process and assist 

in the preparation of reports as needed. 

B. Training, Certification, and Qualification 

Training requirements are identified during the work planning phase at the beginning of a 

project or task and include training regarding standard operating procedures (SOP) referenced 

by the respective work plan. SOPS may be used to address specific field procedures, such as 

low-flow groundwater sampling and equipment decontamination. Other required training may 

relate to health and safety, quality, or specific administrative procedures that need to be 

followed. 

Some activities require performance of work by individuals who have completed specialized 

health and safety training (e.g., hazardous waste operations and emergency response) and have 

demonstrated their knowledge of core requirements through a certification process. The 

requirements for certification will be identified in specific work plans, along with any 

requirements for recertification and/or refresher training. 

Training and qualification records are maintained for each employee. Traininglcertification 

records are referred to prior to assignment of work to verify that the individual has the 

appropriate training, certifications and/or qualifications. 

111. Sampling; Procedures 

A. General 

This section outlines activities that may be conducted as part of field operations. Additional 

activities may be required during future tasks and will be discussed in the task-specific work 

plans. Potential field operations include: 

Drilling, sampling, and abandoning boreholes in soil and unconsolidated sediments 

Installing and developing monitoring wells, piezometers, and extraction wells 

Redevelopment of monitoring wells 

Purging and sampling groundwater from monitoring wells 

Measuring static water levels and free product levels in monitoring wells 

Conducting aquifer pumping tests 

Conducting in situ permeability tests in selected monitoring wells 

Geophysical surveys 

Surveying and locating sampling points 

Performing direct-push soil and groundwater investigations 

Membrane Interface Probe sunrey 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Surface soil pH readings 

Performing soil gas surveys 

Surface soil and sediment sampling 

Surface water sampling 

Sludge sampling in surface impoundments 

Collecting samples of investigation-derived waste. 

Brief descriptions of the most widely used field procedures are provided in this section. This 

chapter provides general procedures for sampling soil, sludge, sediment, and water at the Mt. 

Athos site. Groundwater samples may be collected from groundwater monitoring wells or 

water supply wells. Surface water samples may be collected from creeks that originate on the 

facility property and flow into the James River, as well as from the river itself. Soil samples 

may be collected from borings. Sediment samples may be collected from selected ponds and 

creeks at the facility. Sludge and pond water samples may be collected from current and 

historical waste disposal sites at the facility. 

A task-specific SAP will be prepared prior to conducting field sampling. The SAP should 

address the following details: 

Selection of sampling locations, sample depths, and numbers of samples. 

Screen lengths and placement for monitoring wells. 

Specifics about sample collection methods. 

Analytical parameters, desired analytical detection limits, sample containers, sample 

preservation, and maximum holding times. 

In cases where the SAP specifies different requirements than in this DCQAP, the SAP will take 

precedence. 

B. Field Documentation 

Field data collection activities will be recorded on a number of field logs. Entries will be 

described at an appropriate level of detail so that the situation can be accurately reconstructed. 

All entries will be made in permanent ink; no erasures will be allowed. If an incorrect entry is 

made, the information will be crossed out and initialed. All log sheets will be kept in the 

project files or the NEL files, as appropriate. 

B.l Field Activity Daily Logs 

General field activities will be recorded on a field activity daily log (FADL). Attachment A 

shows an example of a FADL. At least one FADL will be filled out each day in the field. The 

FADL will supplement but not duplicate the information recorded on the Sample Collection 

Logs. Information to be recorded on the FADL includes: 

Project identification 

Field activity subject 

General work activity 

Work progress that day 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Calibration of field measurement equipment 

Variances from project plans and procedures 

Personnel on site 

Communication with the client or others 

Weather conditions 

o Accomplishment of sampling equipment decontamination 

Photographs and identification numbers. 

B.2 Sample Collection Logs 

The collection of each field sample will be documented on a sample collection log (SCL). 

Attachment A shows an example of a generic SCL. Substitutes for the generic SCL include a 

groundwater sampling form or a boring log. The following types of information will be 

recorded on the SCL, as applicable: 

Project name and number 

Date 

Time of sample collection 

Unique sample number 

Sample location 

Sample type (matrix, QC type) 

Compositing information 

Weather 

Sampling depth 

Description of the sampled material 

Types and volumes of sample containers filled 

Field measurements 

Layout of the sampling area 

Other pertinent field observations. 

B.3 Chain of Custody 

The criteria for maintaining custody requires that, throughout the sampling and analysis 

process, the samples and associated paper work are controlled in a manner designed to prevent 

unauthorized tampering that could affect reported results while providing a traceable record of 

sample handling. 

Sample possession from the time of collection to disposal will be tracked with a chain-ofcustody (COC) form. When sample custody changes, signatures of personnel relinquishing and 

accepting the sample will be put on the form accompanied by date and time. Attachment A 

shows an example COC form. A COC form will be prepared for each sample container set. 

The following information will be recorded on the COC form: 

Project nameinumber 

Lab destination 

Sample team members 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

The sample number, location, and description; date and time collected; sampling type; 

container type; and condition on receipt 

Requested laboratory analyses 

Any special instructions andlor sample hazards 

Signatures of samplers in the designated blocks, along with their company, name, date, 

and time. 

The COC form will indicate the analyses required for each sample as specified by the project 

plan. The request for analysis will either state in detail the specific test methods and 

parameters to be tested or reference a specific document that is readily available for reference at 

the laboratory. 

The original COC form will be placed in a plastic bag inside the secured shipping container if 

samples are shipped. A copy of the record will be retained by the sampling team leader. The 

original record will be transmitted to the project staff after samples are accepted by the 

laboratory. This original record will become part of the project file. 

If the sampling team is not in possession of the samples until they are delivered to the 

laboratory, then custody seals will be used to ensure against tampering. For example, custody 

seals are necessary when the samples are shipped by another carrier or when the samples are 

held overnight before delivery to the laboratory. Custody seals may be used either on each 

sample container or on the cooler that holds the samples. 

The laboratory report will include a copy of the signed and completed COC form. 

C. Field Measurements 

Field measurements typically include measurements of temperature, pH, specific conductance, 

and turbidity performed on water samples at the time of sample collection, water level 

measurements in wells, and organic vapor screening of soils. Groundwater samples may also 

be measured in the field for dissolved oxygen and oxidation-reduction potential. Testing and 

monitoring equipment may include hand-held organic vapor monitors used for health and 

safety air monitoring or screening soil vapors, combination pHItemperaturelspecific 

conductivity meters, dissolved oxygen meters, oxidation-reduction potential meters, and 

turbidity meters. 

Field measurements of groundwater collected from monitoring wells are addressed in the 

Standard Operating Procedure for Low-Flow Groundwater Samnpling. 

Water level measurements in monitoring wells will be performed before purging, immediately 

before groundwater samples are collected. 

For water-level mapping, water level measurements of multiple monitoring wells in a given 

area will be made in a one-day period. This will ensure that comparable water levels will be 

collected from each well and will represent an "instant" in time. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Field measurements will be recorded on an SCL or boring log. 

Field testing and monitoring equipment will be inspected and calibrated before use each day. If 

calibration experience shows that an instrument has significant calibration drift from one day to 

the next, then a mid-day calibration will also be added. 

Calibration standards for field instruments will be representative of the parameter 

concentrations observed on site, will be in good condition, and will be replaced when expired. 

Each day an instrument is used, its calibration will be checked against at least one of these 

certified standards. 

Calibrated equipment will be uniquely identified using the manufacturer's serial number or 

other unique identification. Instruments will be calibrated according to manufacturer 

recommendations. 

The calibration date, time, and results will be noted in the field records, whether in an 

instrument calibration log, a FADL, an SCL, or a groundwater sample collection log, as 

appropriate. If an instrument is out of calibration, it will be recalibrated and noted in the log. 

Preventive maintenance of field measuring equipment will be performed prior to sampling to 

ensure equipment is operating properly. Spare parts will be brought to the field as appropriate. 

D. Soil Borings and Sampling 

Soil borings may be advanced using hollow-stem augers or a direct-push rig, although a hand 

auger may be used for borings only a few feet deep. Soils will be logged using the Unified Soil 

Classification System. The entire length of retrieved soil samples will be described for visual 

classification of the soil. Soil samples will be retained until the boring is completed. The 

criteria for selecting which soil samples are submitted for laboratory analysis will be 

documented on the boring log or SCL. Samples not selected for laboratory analysis will be 

disposed of with the drill cuttings. 

The site geologist will maintain a detailed boring log during the drilling of each borehole. The 

log will serve as a record of sample collection, sample location and depth, and drilling methods. 

The boring log will include: 

Heading information including project number, site number, boring number, personnel 

responsible for logging the hole, ground elevation and coordinates, and date boring was 

started and completed 

Depths of samples, recorded in feet and tenths of feet 

Detailed soil descriptions, including: 

- Major soil component - Secondary components and estimated percentages 

- Classification - Unified Soil Classification System symbol 

- Color 
BWXT FEP Data Collection Qualitv Assurance Plan 611 0104 

- Consistency or density - Moisture content - listed as an adjective (e.g., dry, damp, wet) 

- Texture 

- Depositional origin 

- Visual observation of contamination 

0 Depthlelevation of stratigraphic changes 

Water table information and method of determination 

Sample drive depth and recovery percentages 

Drilling and sampling equipment details 

Drilling sequence and comments. 

If field screening of soils for volatile organic compounds (VOC) is deemed necessary, the 

entire length of the sample will then be scanned with an organic vapor meter. The depth 

interval and reading in units of parts per million will be recorded for any portion of the sample 

where organic vapors are detected. Negative (zero or background) readings will also be 

recorded. The sample will also be visually observed for any signs of alteration or 

contamination and the observations noted. The measurement of volatile emissions or 

significant visual observations will serve as a qualitative indication of potential contamination. 

In areas of known or suspected acid releases, soil samples will be collected and submitted for 

laboratory measurement of pH. Low pH readings will serve as a qualitative indicator of acidimpacted soils. 

The SAP should address whether it is necessary to survey soil boring locations. 

Soil cuttings generated during the drilling of soil borings will be drummed, unless returned to 

the borehole in the case of shallow borings as described in Section 1II.E. Upon receiving the 

laboratory analytical results from the samples collected from the borings, the disposition of the 

soils will be determined. 

E. Borehole Abandonment 

Boreholes not used for the installation of monitoring wells will be backfilled with cement grout 

with 3 to 5 percent bentonite (percent by dry weight). However, very shallow boreholes, less 

than about six feet deep (such as drilled by hand auger), may be filled with soil cuttings. 

Grouted boreholes will be filled with grout from the bottom to the top of the borehole using a 

tremie pipe method as the hollow-stem augers are being removed from the borehole. The grout 

will be allowed to settle overnight and will be topped off the following day, if necessary, to 

compensate for any settling that may have occurred. 

F. Monitoring Well Installation 

F.l Drilling Methods 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Shallow monitoring wells may be drilled with l-lollow-stem augers, air hammer, or air rotary. 

Tasks that require drilling to the top of bedrock must include the capability to drill by either air 

hammer or air rotary techniques, because hollow-stem augers often meet refusal due to cobbles 

in the lower portion of the overburden soil. 

Borings for the installation of bedrock monitoring wells will be drilled using an air rotary 

drilling rig. Upon encountering bedrock, a temporary casing will be placed in the boring to 

prevent the sidewalls from collapsing. Deep wells to be completed in bedrock will be drilled 5 

to 10 feet into the competent bedrock, and a surface casing will be installed and grouted into 

place. The grout will be allowed to solidify for no less than 24 hours. This procedure will be 

followed to prevent potential mixing of the surficial and bedrock aquifer waters. After 24 

hours, the well will be drilled to total depth. 

A boring log will be prepared for each well to describe the lithology encountered. 

Cuttings generated during the drilling of borings for the installation of monitoring wells may be 

field screened for the presence of organic vapors using an HNu photoionization device. Those 

cuttings exhibiting organic vapors will be stockpiled on plastic sheeting, bermed, and covered 

with plastic sheeting. 

All water and fluids generated during the drilling and completion of the wells will be contained 

and disposed of by being pumped into the industrial wastewater treatment system at the 

Nuclear Products Division (WD) plant. 

F.2 Well Completion 

Well screen lengths and placement will be addressed by a task-specific SAP that will take into 

account the aquifer characteristics and investigation goals. 

All polyvinyl chloride screen and casing construction joints shall be flush threaded. No glued 

or solvent-welded joints shall be permitted. 

Shallow monitoring wells installed above bedrock, or to a maximum depth of 100 feet below 

the bedrock surface, will be completed with 2-inch Schedule 40 polyvinyl chloride solid riser 

and machine-cut screen with 0.010-inch slots. The annulus around each well screen will be 

backfilled with clean, well-graded silica sand using a tremie pipe. The sand pack will extend to 

approximately 2 feet above the well screen. A 2-foot layer of bentonite pellets will be placed 

directly above the sand pack. Bentonite pellets will be emplaced with a tremie pipe in wells 

deeper than 30 feet, and a tamping device will be used to pack the pellets in wells less than 30 

feet deep. The remainder of the annulus will be filled with a bentonitelcement grout. The 

wells will be finished with concrete pads and locking caps. 

Monitoring wells drilled to depths greater than 100 feet below the bedrock surface will be 

completed as open holes below the surface casing without well casing. All shallower wells will 

be completed with well casing as specified above. The wells will be finished with concrete 

pads and locking well caps. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

F.3 Well Development 

Each newly installed groundwater monitoring well will be developed no sooner than 24 hours 

after completion. The wells will be developed by pumping. Surging of the pump will be 

performed during well development to prevent bridging. The well pump shall be properly 

cleaned before it is inserted in any well, as specified in Section 1II.K. Development water will 

be pumped into 55-gallon drums and labeled. The drums will be identified as to the well the 

purge water came from. Purge water will be disposed of by pumping it into the NPD industrial 

wastewater treatment system. 

Development of water from the well will continue until the water is visibly clear or until three 

successive readings of pH, conductivity, and temperature of the development water stabilize 

within 10 percent. Readings of the above parameters will be taken at approximately 15-minute 

intervals. Wells with low water yields will be developed until at least three boring volumes are 

removed or until the well is pumped dry. 

F.4 Aquifer Testing 

Permeability tests may be run on newly constructed monitoring wells. The method used to run 

the tests in wells installed in the surficial aquifer will involve placing an electric submersible 

pump into the well, measuring the static water level, and pumping the well at a known and 

constant rate while measuring the dropping water level. When the water level in the well drops 

below the pump, the pump will be disconnected from the power source and the recovering 

water level will be measured at recorded time increments until the level reaches its static 

elevation. A semilogarithmic plot will be prepared for each well data set to graph the change in 

head in the water level versus the elapsed time since the pump was started and the time since 

the pump was disconnected. From these plots, the hydraulic conductivity of the aquifer will be 

calculated. For deep bedrock aquifer wells with open-hole completions, an inflatable packer 

will be used if determined necessary by the field geologist to isolate individual water-bearing 

zones as identified from the borehole drilling logs. The specific water-bearing zones to be 

tested and the number of tests will be determined by the geologist in the field based on the data 

collected during the drilling and testing of the boring. As with the shallow aquifer wells, an 

electric pump will be used to draw the water level down. The water level drawdown and 

recovery rates will be measured and utilized to determine the hydraulic conductivity of the 

specific water-bearing zones. All water removed from the well during aquifer testing will be 

disposed of as discussed in Section III.F.3. All aquifer testing equipment will be thoroughly 

decontaminated between wells. 
BWXT FEP Data Collection Oualitv Assurance Plan 611 0104 

F.5 Monitoring Well Surveying 

Once monitoring wells have been installed, final locations and elevations will be surveyed by a 

registered Virginia surveyor. Horizontal coordinates for all new monitoring wells will be 

measured to the nearest 0.1 foot and referenced to the 1929 National Geodetic Vertical Datum. 

Surface elevations for soil borings will be determined to the nearest 0.1 foot. Elevation 

measurements will be made at the top of the well casing and at the ground surface at each well. 

Elevations at wells will be measured to the nearest 0.01 foot. The measurement point on the 

casing will be clearly and permanently marked for future water level measurements. The 

locations will also be marked on the pad. The unique monitoring well identification number 

will be permanently mounted to the protective cover. 

G. Water Sampling 

G.l Groundwater Sampling of Monitoring Wells 

Groundwater samples for laboratory analysis will be collected at a slow flow rate to minimize 

agitation and aeration. Groundwater sampling from monitoring wells will be performed using a 

bailer, a low-flow purging technique (particularly where metals are the principal constituents of 

concern), or passive diffusion bag samplers (for samples requiring only VOC analyses). Site 

experience has shown that groundwater sampling for VOCs with bailers, passive diffusion 

bags, and low-flow purging all produce comparable results (RCRA Comprehensive Baseline 

Monitoring Report by BWXT, 2002, and 2003 Annual Monitoring Report for the RCRA 

Corrective Measure Stud}) by BWXT, 2003). 

Wastewater produced during purging and sampling operations shall be stored on site in 

dedicated drums that are properly labeled with the well the purge water came from. All purge 

waters will be disposed of as stated in Section III.F.3. 

G.2 Water Supply Well Sampling 

For water supply wells, including potable water wells, samples will be collected from a faucet 

or valve near the well discharge point. If possible, samples will be collected before the water 

goes through any type of filter system that maybe in use at that location. Before any samples 

are collected from domestic wells, the pump will be permitted to run for approximately 15 

minutes to ensure that a fresh groundwater sample is collected. 

G.3 Surface Water Sampling 

Sampling of surface water shall be performed using the following procedures. Grab samples 

from the surface of the water may be obtained using a beaker, sample vial, or Kemmerer 

sampler. Sampling devices will be thoroughly cleaned before use and after each sample point 

with a ~i~uinox' and potable water wash and deionized (DI) water rinse. Samples collected 

with beakers will be transferred to the sample container with minimal agitation and aeration. 

Field measurements for pH, conductivity, and temperature will be made at each sample 

location. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

H. Sediment Sampling 

Sediment samples obtained from streams will be collected with a stainless steel trowel or scoop 

sampling device. Any excess liquid will be decanted from the sediment sample before placing 

it in the appropriate sample container. Physical parameters of the sediment (e.g., color, grain 

sizes, presence of organic matter) will be described on an SCL. 

Sampling methods for pond sludges will be addressed in the task-specific SAP, taking into 

account the means of accessing the pond, the depth of overlying water, and the thickness and 

material consistency of the sludge. 

I. Collection of Quality Control Samples 

To ensure the reliability of field sampling procedures and materials, field QC samples will be 

collected or prepared for each medium sampled, each sample shipment, and each sampling 

event. Each field investigation will be considered one event unless field personnel leave the 

site for more than 24 hours during the course of the investigation. 

The following information defines and describes how to identify and document QC samples. 

All field samples will be given unique sample numbers. 

1.1 Trip Blanks 

Trip blanks are samples that originate from laboratory-grade DI water taken from the 

laboratory to the sampling site and returned to the laboratory with aqueous volatile organic 

samples. 

The trip blank monitors potential cross-contamination of the samples for volatiles during 

handling and shipment. One trip blank shall accompany each cooler containing aqueous 

samples to be analyzed for VOCs, shall be stored at the laboratory with the samples, and shall 

be analyzed by the laboratory. Trip blanks only need to be analyzed for VOCs. Trip blanks 

shall be identified with a unique number and the prefix "TB" on the sample bottle and COC. 

1.2 Equipment Rinsate Samples 

Equipment rinsate samples will be collected during soil and groundwater sampling to verify the 

effectiveness of sampling equipment cleaning and to monitor for potential cross-contamination 

between samples. Equipment rinsate samples are collected from the final DI water rinses of the 

equipment cleaning process. Equipment rinsate samples will be collected at a minimum 

frequency of 1 per 20 samples per sampling medium or sampling event, whichever is more 

frequent. The rinsates will be analyzed for the same analytes as the samples collected that day. 

Equipment rinsates will be identified with a unique number and the prefix "ER" on the sample 

bottle and COC. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

1.3 Field Blanks 

Field blanks are prepared from the laboratory-grade DI water used for cleaning. Analysis of 

field blanks will ensure that all water sources used during cleaning of sampling equipment are 

free of the parameters of interest. Only water field blanks are required. At a minimum, one 

sample will be collected for each source of water used for cleaning, per sampling event. Field 

blanks will be analyzed for all parameters. Field blanks will be identified by a unique number 

and the prefix "FB" on the sample bottle and COC. 

1.4 Field Duplicates 

Duplicates for samples will be collected simultaneously with the original samples. Field 

duplicates will be collected at a frequency of 10 percent (1 per 10) of water samples and 5 

percent (1 per 20) of soil samples, or one per sampling event, whichever is more frequent. 

Field duplicates will be used as confirmation samples. 

1.5 Matrix Spike and Matrix Spike Duplicate Samples 

A matrix spike (MS) is an aliquot of a sample that is spiked with a known concentration of 

target analyte(s). The spiking occurs in the laboratory prior to sample preparation and analysis. 

A matrix spike is used to document the bias of a method in a given sample matrix by measuring 

the recovery of the analytes of interest. A matrix spike duplicate (MSD) is a duplicate of the 

MS, a second aliquot of the sample spiked with identical concentrations of target analytes. The 

MSD data are used to verify the results of the MS and to evaluate the analytical precision of the 

spiked samples. 

Extra field QC samples will be collected for the MSIMSD analyses. One pair of MSIMSD 

samples will be collected and analyzed for every 20 site samples of a given matrix, or one pair 

matrix per sampling event, whichever is more frequent. 

J. Sample Handling 

J.l Order of Sample Collection 

Water samples will be collected and containerized in the order of volatilization sensitivity of 

the analytical parameters as follows: 

VOCs 

Baselneutral and acids 

Total metals 

Dissolved metals 

Inorganics. 

For soil, sediment, and sludge samples, the VOC aliquot will be collected first, before any 

sample homogenization is performed. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

5.2 Sample Container, Preservation, and Holding Time Requirements 

The task-specific SAP will determine the requirements for sample containers, preservatives, 

and holding times. These requirements will generally follow those specified in SW-846, unless 

a method published elsewhere is used. 

Containers will not be overfilled, as this will dilute preservatives. 

5.3 Sample Labels 

A sample label will be securely affixed to each sample container. Attachment A shows an 

example of a sample container label. Each sample will be assigned a unique identification 

number. Samples will be labeled and identified with the following minimum information: 

Project name and project number 

Sample location 

Sample number 

Name of sampler and sample date 

Parameters and preservation. 

The information on the label should be consistent with that recorded on the COC form. 

5.4 Sample Packaging and Shipping 

Samples will be packaged and shipped in a way to best preserve the integrity of the samples 

and in accordance with shipping guidance and requirements. Ice chests (coolers) will be used 

as shipping containers. Sample containers will be custody sealed in a plastic bag, placed in ice 

chests, cooled with ice and surrounded with packing material. Required documents will be 

hand carried by same-day courier or included in the ice chest for overnight service. After 

securing the ice chest, custody seals will be applied to warn of tampering. Sample containers 

shall remain in the custody of the sampling crew or designated person and secure location prior 

to courier pickup. Shipment of samples will be by local same-day courier or overnight service. 

Samples shall be stored in the coolers at 4'Celsius. The COC forms will be copied, and the 

original will be sent with the samples with the bill of lading. Custody will be maintained by the 

shipper for NEL and shipped overnight. Copies of the COC will be placed in the BWXT NPD 

project files and the NEL project files. The completed COC will be returned to NPD with the 

analysis results package. 

K. Cleaning Procedures 

Drilling equipment will be thoroughly decontaminated and inspected before each drilling 

location and after the last location. All drilling equipment that may contact the interior of the 

borehole and all well completion materials shall be thoroughly steam-cleaned in an area 

designated by the field coordinator that is clean and free of contamination. All equipment used 

for groundwater and soil sampling, well purging, and well development (including aquifer 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

testing) will be washed with laboratory-grade detergent, rinsed with tap water, rinsed with DI 

water, and allowed to air dry. The cleaning area shall be lined with plastic and shall have 

raised edges to contain all cleaning solutions and material dislodged from equipment during 

cleaning operations. The materials collected at the cleaning area (drill cuttings, soil sample 

debris, and other potentially hazardous solid waste) shall be placed in labeled drums and 

disposed of in accordance with state and federal guidelines. 

Precleaned bottles will be used for all analyses. Sample bottles will be cleaned according to 

standard EPA procedures for each analysis type. 

IV. Contractor Project Documentation 

In the performance of BWXT project tasks, contractor personnel will be required to complete 

the necessary documentation to record such events as nonconformances, variances, and 

decisions and action items from meetings held with BWXT and regulatory agencies. This 

project documentation will supplement basic documentation that consists of field investigation 

data, sample collection information, and analytical data records. To assist in the collection of 

information, project documentation procedures have been developed and specialized forms 

designed. 

Field documentation was discussed in Section 111. Nonconformance and variance 

documentation is discussed in Section VI. The following sections discuss communication 

records and record storage. 

A. Record of Telephone Conferences and Meetings 

Meetings are frequently held via telephone or in person among members of the contractor 

project team, BWXT, and/or the regulatory agencies. During these meetings, often critical 

decisions are made and action items assigned. Some of these decisions include scope and 

schedule changes that may impact project objectives and budgets. These decisions must be 

carefully documented and distributed to all team members who will participate in or implement 

the decisions. The primary form to record these decisions is via meeting minutes; however, the 

Record of Teleconference/Meeting can also be used. An example of this form is included in 

Attachment A. A blank version of this form may be used by at least one designated person 

during the meeting to record project decisions and assigned action items. 

This completed record form or meeting minutes would be circulated as a draft and reviewed by 

other participants in the meeting. Comments would be added as needed based on their meeting 

notes, and a final typewritten version of the form or minutes would be completed and signed by 

the preparer. The preparer is then responsible for distributing the form or minutes to the 

appropriate team personnel. The preparer will work with the contractor PM in determining the 

distribution. The original of all completed Record of TeleconferenceIMeeting forms or 

meeting minutes will be sent to the project central files for storage and reference. 

IV- 18 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

B. Record Storage 

Project documentation includes field activity data, sample collection information, and 

analytical data records (hard copy analytical reports and electronic data deliverables). 

Supplemental documentation such as nonconformance reports, variance logs, record of 

teleconferencelmeeting forms, letters of transmittal, general correspondence, project 

proposals/plans, drawings, and reports, along with the project documentation will comprise the 

project files. Copies of these documents may exist elsewhere, but the originals shall be kept in 

the project file. The project files will be kept in a secure, central location and indexed by 

project number and the type of record for easy cross-referencing. 

The Shaw PM will designate an individual to assume overall responsibility for maintaining 

project files using file tracking forms for inventory and control. The project files will be a focal 

point for project audits and must be kept current at all times. While the project is active, 

project files will be kept in the Shaw Knoxville office. Original documents produced in the 

field will be copied, the copies filed in the field, and the original forwarded to the Knoxville 

office in a timely manner. Task managers will be responsible for verifying that original project 

plans, field forms, and reports are transferred to the project file for long-term storage. Updated 

information will be noted and added to the file as appropriate. 

V. Laboratorv Analvses 

The samples collected during the course of investigation will be controlled and analyzed at 

BWXT Services, 1nc.-NEL in accordance with the NEL QAP and applicable NEL TP. The 

SOPS for this plan represent industry-recognized analytical methods from source documents 

established by EPA, including SW-846 (3rd or most recent edition). Other than for 

emergencies, analysis at any off-site lab will be preceded by an audit to assure compliance with 

acceptable EPA procedures and protocols. 

A. Laboratory Sample Receipt 

Upon sample receipt, the sample custodian or designee shall: 

Confirm that samples have been stored correctly in an iced container. If samples have 

been damaged during delivery, the remaining samples shall be visually inspected to 

determine their integrity. Any samples suspected of being affected shall also be 

considered damaged. It will be noted on the COC record what specific samples were 

damaged and that the samples were removed from the sampling program. Field 

personnel will be notified as soon as possible that samples were damaged and are 

unusable. 

Compare samples received against those listed on the COC. 

Verify that sample holding times have not been exceeded. If the sample holding time 

has been exceeded, the sample custodian or designee will notify the project manager 

and the field personnel as soon as possible and prepare a nonconformance report 

(Section V1.A.). 

Place the samples in appropriate laboratory storage. 
BWXT FEP Data Collection Oualitv Assurance Plan 611 0104 

Log the samples into the sample tracking system with the following information: 

- Laboratory sample delivery group (SDG) number 

- Project identification number or name 

- Sample numbers 

- Type of samples 

- Date received in laboratory 

- Sampling date. 

Note the laboratory SDG number on the COC form. 

If collected samples arrive without COC or with incorrect COC records, the sample custodian 

shall do the following: 

If the COC form is incorrect or incomplete, the NEL sample custodian shall note each 

discrepancy or missing item and relay the information to the NEL project manager. The 

NEL project manager shall contact the BWXT project manager and reach agreement on 

the method to resolve the deficiencies. All correspondence shall be documented. If the 

deficiencies cannot be resolved, the affected samples shall be removed from the 

sampling program and a nonconformance report issued. 

If the COC form is not included with the samples, the field personnel responsible for 

collecting and transporting or shipping the samples shall be contacted. The COC form 

will be prepared with the help of field personnel and initialed by field personnel as soon 

as possible. The COC form (remarks) will note this deviation. 

B. Laboratory Instrument Calibration 

Instruments and equipment used in the laboratory are controlled by a formal calibration 

program defined in the laboratory QA plan. The program verifies that equipment is of the 

proper type, range, accuracy, and precision to provide data compatible with specified 

requirements. Calibration may be performed using reference standards or externally by 

calibration agencies or equipment manufacturers that have been audited by the laboratory QA 

administrator for acceptability. 

Two types of calibration utilized in the laboratory are: 

Operational calibration: Routinely performed as part of instrument usage, such as the 

development of a standard curve for use with an atomic absorption spectrophotometer. 

Operational calibration is generally performed for instrument systems as part of the 

SOP. 

Periodic calibration: Performed at prescribed intervals for equipment such as balances 

and ovens. In general, equipment items that can be calibrated periodically are distinct, 

single-purpose units and are relatively stable in performance. 

Procedures published by the American Society for Testing and Materials or the EPA, or 

procedures provided by manufacturers, will be utilized. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

At a minimum, the procedures shall include: 

Calibration technique and sequential actions 

Calibration documentation format 

Reference standards used for calibration 

Acceptable performance tolerances 

Frequency of calibration. 

Documentation of calibration shall be kept with project files or laboratory equipment files for 

each equipment item. 

C. Analytical Methods for Soil, Groundwater, Surface Water, and Sediment 

Samples 

Analyses will be performed by the methods specified in the task-specific SAP. Analytical 

methods from SW-846, latest edition, will typically be used, but other EPA-published methods 

may be used if appropriate. 

D. Laboratory Quality Control Checks 

Laboratory QC checks are used to validate data integrity. Analytical quality controls are 

related to batches of samples as specified in the published EPA methods (e.g., SW-846) and the 

NEL QAP. These controls include reagent blanks, QC check samples, duplicate samples, and 

spiked duplicates for each batch or every 20 samples. Initial and continuing calibrations shall 

be performed at intervals as referenced in the published methods and NEL TPs. Calibration 

standards must be reference quality, traceable to the National Institute for Standards and 

Technology, and purchased from an approved supplier. QC check samples shall be evaluated 

against the acceptance limits as specified in the appropriate SW-846 methods and the NEL TPs. 

Surrogate spikes for organics shall also be evaluated against the acceptance limits as specified 

in the appropriate methods and the NEL TPs. 

E. Documentation of Data 

Documentation measures encompass all analytical and QC activities ensuring the integrity and 

validity of sample analysis results and providing a traceable history of each sample analysis. 

Information is recorded on worksheets, analytical logbooks, or computer data systems. System 

support infornlation such as instrument maintenance and equipment calibration records is kept 

in laboratory files. Component analytical documentation measures included are summarized in 

the following sections. 

E.1 Laboratory Sample Receipt Logbook 

All samples submitted to NEL for laboratory analysis are assigned a unique SDG number, and 

each containerbottle is labeled with a unique identifier. All relevant information regarding the 

origination and receipt of the samples is recorded in the NEL's electronic sample tracking 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

system. Examples of the types of individual entries include: analyses requested, dateltime of 

collection, receipt conditions, and the field identification number. 

E.2 Laboratory Worksheets 

The analytical specifications and subsequent results of each sample submitted to the laboratory 

are recorded on various laboratory worksheets included in SOPS. Pertinent information on the 

worksheets includes laboratory sample identification, requested analytical parameters, 

maximum holding times and turnaround requests, and analytical results. Laboratory 

worksheets will be kept on file at the laboratory. 

E.3 Laboratory Method Logbooks 

Data generated during the analysis of samples by NEL is recorded and documented according 

to the NEL QAF' and governing technical procedures. The systems of documentation employed 

by NEL allow complete traceability of all the data generated during the course of analysis. 

E.4 Calibration Standards Logbook 

All laboratory primary standard data are maintained in a laboratory standards logbook. 

Working standards are documented in analysis records with traceability to the primary 

standards. 

E.5 Instrument Computer Data System Files 

Chromatography and atomic absorption spectroscopy data files are maintained according to 

sample log number. The data files include instrument parameters, calibration data, date of 

analysis, analyst, and QC results. 

I?. Data Reduction/Validation Reporting 

Validation is the process of determining whether a measurement system provides useful 

analytical data. Adequate sample identification and COC procedures verify the integrity of the 

sample. Validation of the analytical method is accomplished through instrument calibration 

with traceable standards and collaborative testing such as blind performance evaluation and 

daily QC samples. Raw data entries are validated by the analyst with a signature, date, and 

time of analysis. The sample data packages include relevant information such as sample 

identification, COC, measurement methodology, instrument identification, calibration data, 

analyst signature (with date and time of analysis), and demonstration of statistical control with 

method blanks, field and trip blanks, replicates, QC samples, and spikes (surrogates for 

organics). The laboratory supervisor or designee oversees data collection and reduction to 

verify that data are converted to meaningful reporting values. Consideration in data reduction 

must be given to significant figures for each analysis, method detection limits, precision of 

duplicate results, and the accuracy of QC data. Reporting of lab data by computer is validated 

by signature of a cognizant individual. Reports will include sample identification, final sample 

results, and QC information. 
BWXT FEP Data Collection Oualitv Assurance Plan 611 0104 

F.l Data Assessment Protocol 

When the analyses of a sample set are completed, the results are reviewed and evaluated to 

assess the validity of the data set. Review is based on the following criteria. 

F.l.l Method Blank Evaluation 

When appropriate for the method, a reagent and/or method blank should be analyzed with each 

batch of samples processed to assess contamination levels in the laboratory. The results of the 

blank should be less than the laboratory's reporting limit for the analyte. If the blank results do 

not meet the acceptance criteria above, then the laboratory should take corrective action to 

locate and reduce the source of the contamination and re-extract and reanalyze any samples 

associated with the contaminated blank. 

F.1.2 Field and Trip Blank Evaluation 

Field and trip blank results are evaluated for high readings similar to the reagent and/or method 

blanks described above. If high field blank readings are encountered, the procedures for 

sample collection, shipment, and laboratory analysis should be reviewed. If both the reagent 

and/or method blanks and the field blanks exhibit significant background contamination, the 

source of contamination is probably within the laboratory. High field blank readings may also 

be due to airborne contamination or cross-contamination due to sample leakage and poorly 

sealed sample containers. 

F.1.3 Method Calibration Evaluation 

When evaluating calibration standards, the calibration curve is evaluated to determine linearity 

through its full range and to verify that sample values are within the range defined by the low 

and high standards. If the curve is not linear, sample values must be corrected for nonlinearity 

by deriving sample concentrations from a graph or by using an appropriate algorithm to fit a 

nonlinear curve to the standards. 

Calibrations are verified using both initial and continuing calibration check standards. 

Acceptability of the calibration is based on the criteria set for each analytical method. 

F.1.4 Evaluation of Analytical Precision 

Duplicate sample analysis for the sample set is used to determine the precision of the analytical 

method for the sample matrix. Precision limits are derived statistically by the laboratory. If the 

measure of precision is outside the acceptance range for the given parameter in question, the 

reason for the nonconformance must be determined; corrective action may include reanalysis. 

MSIMSD pairs may also be assigned. The results of the duplicate analyses are used to 

calculate the relative percent difference (RPD), which is the governing QC parameter for 

precision. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

The RPD for replicate analyses is defined as the absolute difference (range) of each replicate 

pair, divided by the average value (mean) of the replicate pair, times 100. For replicate results 

Dl and D2, the RPD is calculated as follows: 

F.1.5 Evaluation of Analytical Accuracy 

In addition to the evaluation of analytical precision, the laboratory will evaluate accuracy. To 

determine the accuracy of an analysis, the results of MS, MSD, and blank spikes are used to 

calculate the QC parameter for accuracy evaluation, the percent recovery (%R). 

The %R is defined as the observed concentration minus the sample concentration, divided by 

the true concentration of the spike, times 100: 

where: 

%R = Percent recovery 

01 = Laboratory-determined concentration of the spiked sample 

O2 = Sample concentration prior to spike 

Ti = True concentration of the spike. 

F.1.6 Matrix Spike Evaluation 

To evaluate the matrix effect of the sample upon the analytical methodology, samples are 

spiked with compounds appropriate for the method. The %R of those compounds from the 

sample is monitored. Recovery limits are statistically established for each method. If the %R 

is outside the acceptance range, an evaluation of the cause of the deviation is undertaken. If it 

is determined that the analytical system was out of control, then the samples will be reanalyzed. 

F.1.7 Reference Standard Evaluation 

Standard reference material analyses are compared with true values and acceptable ranges. 

Values outside the acceptable ranges require corrective actions to determine the source of error 

and to provide corrective action. All sample analyses should be halted pending this evaluation. 

Following correction of the problem, the standard reference material should be reanalyzed. 
BWXT FEP Data Collection Oualitv Assurance Plan 611 0104 

F.1.8 Surrogate Spike Response Evaluation 

Surrogate standard determinations are performed on samples and blanks. Samples and blanks 

are fortified with surrogate spiking compounds before purging or extraction to monitor 

preparation and analysis of samples. 

Surrogate spike recovery must be evaluated for acceptance by determining whether the 

concentration (measured as %R) falls within the required recovery limits. 

If recovery is not within surrogate recovery limits, the following actions are taken: 

Check for errors in the calculations, internal standard or surrogate spiking solutions. 

Examine chromatograms for interfering peaks and integrated peak areas. 

Check instrument performance. Correct any problems and reanalyze the extract. 

If no instrument problem is found, the sample should be re-extracted and reanalyzed. 

If, upon reanalysis, the recovery is again not within limits, the data will be qualified 

accordingly. If the recovery is within the limits in the reanalysis, provide the reanalysis 

data to the data user. 

If the measures listed above fail to correct the problem, the analytical system must be 

considered out of control. The problem must be corrected before continuing. This may mean 

recalibrating the instrumentation, but it may also mean more extensive action. The specific 

corrective action should be defined by the gas chromatograph operator with the concurrence of 

the laboratory supervisor and/or instrument maintenance specialist. Report the surrogate spike 

recovery data and the sample data from both extractions when reanalysis substantiates a matrix 

effect. 

F.2 Data Reporting Format 

Final review of the data to be reported is performed by the appropriate laboratory personnel. 

Reports are reviewed for: 

Completeness - Results for all requested parameters are present; detection limits, units, 

dates, and sample descriptions are complete and correct. 

Consistency -All parameters are reviewed for internal consistency. 

Accuracy of data entries. 

The laboratory supervisor or project manager is responsible for ensuring that the final report is 

reviewed prior to release. 

Preliminary or draft analytical reports may be provided for those projects requiring rapid 

analytical turnaround times. These abridged materials primarily contain analytical results. 

Additional supporting materials may be provided if prearranged. Preliminary reports will be 

followed by final reports. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

Laboratory analytical final reports may include appropriate introductory comments, analytical 

method summaries, and QC reports in addition to listing sample analytical results and 

associated QC data. Sample analytical result report sheets are generated in hard copy andlor 

appropriate computer format. Additional technical narratives, along with supporting raw data, 

may also be included as warranted by special circumstances (e.g., atypical analyses, matrix 

interferences). 

F.3 Laboratory Turnaround Time 

The laboratory analysis turnaround time, for scheduling purposes, is estimated to be 2 months 

Expedited turnaround times may be utilized if deemed necessary. 

VI. Performance Monitoring 

This chapter addresses nonconformances and corrective action, variances, and audits. 

A. Nonconformance and Corrective Action 

Each nonconformance affecting quality will be documented by the personnel identifying the 

nonconformance. The nonconformance report may be an audit report, an inspection report, an 

internal memorandum, or other document as appropriate. A form developed specifically for 

nonconformance report is included in Attachment A. The nonconformance report must 

document: 

Date of the nonconformance 

Identification of the individual(s) identifyng or originating the nonconformance report 

Description of the nonconformance 

Method(s) for correcting the nonconformance (corrective action) to ensure that it is not 

repeated 

Schedule for completing corrective action 

Description of cause of nonconformance, including steps taken to identify these causes. 

The responsibility for tracing the cause of the nonconformance rests with the supervisor or the 

project leader of the affected area. Analysis nonconformance will be addressed by the 

laboratory supervisor and the laboratory QA administrator. The predetermined criteria for data 

acceptability for laboratory analyses are defined in specific SOPS written to comply with 40 

Code of Federal Regulations 136 or 40 Code of Federal Regulations 261. These criteria are 

summarized in Section V of this DCQAP. 

Recurring nonconformance will be evaluated by project management, laboratory management, 

and/or the BWXT QA administrator to determine its cause and to prevent recurrence if 

possible. When such an evaluation is performed, the results will be documented. The BWXT 

project manager is authorized to stop work on the project pending resolution. 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

B. Variances 

Variances from standard, approved operational procedures and plans will be documented. It is 

recognized that procedures and work plans cannot adequately foresee all possible conditions to 

be encountered. 

An example project variance form is included in Attachment A. This form has been designed 

to ensure key information is recorded by the personnel who identify variances, review the 

documentation, assess the impact on task objectives, and consider alternative strategies for 

ensuring compliance with work-controlling documents. 

The variance record will contain date and nature of the variance, applicable document (i.e., 

procedure or plan), and the person initiating the variance. Items recorded as a variance require 

the approval of the project manager or designee that is overseeing the task (the responsible PM, 

whether BWXT or contractor). Approval by the project manager can be initiated verbally via 

telephone, provided the conversation is documented and submitted to the project files. 

Formal approval of the variance will be in writing. The project manager will be provided with 

a copy of all variance requests. Upon receipt, the project manager will review the variance and, 

when in agreement, indicate approval with signature and date. The original of the variance will 

be kept in the project files. 

C. Audits 

To verify compliance with DCQAP requirements, the BWXT QA program administrator or 

designee will perform audits of project activities. Audit results will be formally documented 

and sent to the BWXT project manager. 

Audits may include, but are not limited to, the following areas: 

Field operation work procedures and records 

Laboratory testing and records 

Equipment calibration and records 

Identification and control of samples 

Numerical analyses 

Computer program documentation and verification 

Transmittal of information 

Record control and retention. 

Audits will be scheduled to coincide with appropriate project activities and at other times as 

deemed necessary. 

Audits will be performed in accordance with written checklists and applicable requirements of 

this DCQAP. A checklist shall be developed to provide a basis for each audit, identifying the 

audit scope, activities to be audited, audit personnel, any applicable documents, and the 
BWXT FEP Data Collection Quality Assurance Plan 611 0104 

schedule. The checklist shall be consistent with the project scope of work, schedule, and 

requirements. 

During an audit and upon its completion, the auditors will discuss with the responsible parties 

any findings, observations, and proposed corrective actions. Observations that can be resolved 

to the satisfaction of the auditors during an audit are not required to be cited as items requiring 

corrective action. All findings that are not resolved during the course of the audit and findings 

affecting the overall quality of the project, regardless of when they are resolved, shall be noted 

on the audit checklists. 

Following completion of an audit, the auditors shall prepare and submit an audit report to the 

appropriate project personnel. This report shall serve to notify BWXT management of audit 

results. The report may also be sent to the management of any affected subcontractor. 

The report shall be prepared as soon as possible after the audit and shall contain, as appropriate: 

Date(s) of the audit 

Identification of audit participants 

Identification of activities audited 

Audit results 

Description of items requiring corrective action and, if possible, the means of correction 

Due date for audit response 

Means for audit response (in writing). 

The individuals audited shall respond to the audit report in writing. The response shall clearly 

state the corrective action taken or planned. If all corrective actions have not been completed 

prior to issuance of the audit response, a scheduled date for completion shall be provided. 

Proposed corrective action must be approved by the QA officer and the BWXT project 

manager. Corrective action shall be handled in accordance with Section V1.A of this 

document. After acceptance and verification of all corrective actions, an audit closure report is 

issued by the QA officer. 
TABLES 
Table F-1 

Analytical Data Quality Levels 

BWX Technologies, Inc. 

Data Use Measurement or Analysis Appropriateness Analytical Level 

Health and safety, PID screening Surface soil and Level I 

field personnel cuttings from borings 

protection 

Additional 

physicalichernical 

characterization of 

surface water and 

groundwater during 

the sampling process 

pH, Specific 

Conductance, 

Temperature, Dissolved 

Oxygen, OxidationReduction Potential, 

Turbidity 

Groundwater and 

Surface water 

Level I 

I 

Determination of PID screening Field screening Level I 

vertical and horizontal measurements using 

extent of VOCs in PID 

soils and water in 

selected areas 

Further Volatile organics, Surface water, Pond water Level I11 

characterization of site Semivolatile organics, Metals 

Further Volatile organics, Groundwater Level I11 

characterization of site Semivolatile organics, Metals 

Further Volatile organics, Soil, Sediment, Sludge Level I11 

characterization of site Semivolatile organics, 

Metals, 

TCLP-extractable 

TCLP - Toxicity Characteristic Leaching Procedure. 

PID - Photoionization detector. 

VOC - Volatile organic compound. 

Level I - Field screening or analysis using portable instruments. 

Level I1 - Field analysis using more sophsticated portable analytical instruments (not shown) 

Level I11 - Analyses performed in an analytical laboratory. 

KN4\BWXT\ColdPond\GWMP\FEP DCQAP Table F-I (5-19-04).doc\6/10/2004(10:55 AM) 
FIGURES 

ATTACHMENT A 

FORMS 

KN4\BWXT\FEP\Exh7\APFFEP DCQAP( 6-4-04).doc\6/1012004(5:03 PM) 
Shaw E & l, Inc. 

SHEET 

FIELD ACTIVITY DAILY LOG 

OTHER SPECIAL ORDERS AND IMPORTANT DECISIONS: 
Shaw- A 

Shaw E & l, fnc. 

Pnge 1 of 1 

Sample Collection Log 

408486 Mt Athos 

Manager: 

Location Code: MWA-2 

SanipIe Number: AA3012 

Sample Name: MWA-2-GW-AA3012-REG 

Sampling Method: LF 

Sample Twe: GW Sample Purpose: REG 

Containers 

Anaiytiral Suite Ftt Frtn OW Size Units Type 

RFA 1 COC Number: 062403-NELS 

Task: Mt Athos 

Collection Date: 24JUN-03 

Collection Time: 10:16 

Start Depth: 

End Depth: 

Sample Matrix: WATER 

Sample Team: CVL 

1 NITRATE N a 1 25 m~ HDPE I I 

/SULFATE N a 1 25 mL HDPE 1 

Comments: 

Sketch Location: 

ERPIMS C'a1ue.s~ 

Srrcodr: 

Lot Carrvl#; 

Logged BY / Date: Reviewed BY / Date: 

Mt Athos 

Shaw Environmental Project Number 408486 I Sample No: 301 2 Lation: MA-2 

Preseruation: None except ml hD 4 C 

Require4C: Y Fibred: N 
she Shaw Environmental, Inc 
Noncunfonnance No: 

Shwa Shaw En-, Inc 
" Shaw Environmental, Im: 

Orher Participants: Call: '1.0 or From (circle me) 

Call: To or From (circle one) 

1. Summary fDecisidAction Item Requ~red): 

II. Summary of Action Items: 

Distribution List: Other Distfibution 
Table F-1 

Analytical Data Quality Levels 

BWX Technologies, Inc. 

surface water and 

groundwater during 

the sampling process 

vertical and horizontal 

erization of site 

TCLP - Toxicity Characteristic Leaching Procedure. 

PID - Photoionization detector. 

VOC - Volatile organic compound. 

Level I - Field screening or analysis using portable instruments. 

Level I1 - Field analysis using more sophisticated portable analytical instruments (not shown) 

Level I11 - Analyses performed in an analytical laboratory. 

KN4\BWXT\ColdPond\GWMP\FEP DCQAP Table F-1 (5-19-04).doc\611012004(1:18 PM) 
ATTACHMENT A 

FORMS 

KN4\BWXnFEP\Exh7\APnFEP DCQAP( 6-4-04).doc\6/1012004(5:03 PM) 
A 

S haw rtc 

Shaw E & 1, I~G. 

FIELD ACTIVITY DAILY LOG 

E 

t I 

SHAW ENVI WONMERdTAL PERSOFJNEC 063 SITE 
Page 1 of 1 

Shaw E & I, lnc. 

Sample Collection Log 

408486 Mt Athos 

Manager: 

Location Code: MWA-2 

Sample Number: hi3012 

Sample Name: MWA-24W-AA3012-REG 

Sampling Method: LF 

Sample Type: Gw Sample Purpose: REG 

RFA 1 COC Number: 062903-NELS 

Task: Mt Atbos 

Collection Date: 2dJUN-03 

Collection Time: 10:16 

Start Depth: 

End Depth: 

sample Mtrix: WATER 

Sample Team: CVL 

Containers 

Analytical Suite FIt FrtnQty Size Units Type 

NITRATE N a 1 25 mL HDPE 

SULFATE N a 1 25 mL HDPE - -- - TOC N b 2 40 mL VOAW -- 

VOLATILES N c 2 40 mL VOAVIAL 

-1 

Comments: 

Sketch Location: 

Logged 3 Y / Date: Reviewed BY / Date: 

Shaw Environmental Project Number 408486 

Sampie No: 301 2 Losation: MA-2 

Lab: BWX? - ON SITE LAB 

Sample Date: 24 3UN 2003 Time: 10:16 

Analysis: Nihb by USEPA 300.0, Sulfate by USEPA 300.0 

- 

Pteselvation: None except mi to 4 C 

Require 4C: Y Fibred: N 

Nonconformance No: 

Shma stww ~nvionme~, Inc 
" Shaw Emironmental, Inc. 

all: 'l'o or From (c~rcte one] 

TI. Summary &Action Items: 

Distribution List: Other Distribution 
ATTACHMENT B 

CERTIFICATIONS 
BWX Services Nuclear Environmental Laboratory 

Certifications 
oq FLORIDA DEPARTMENT OF 

State of Florida 

Department of Health, Bureau of Laboratories 

This is to certify that 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

has complied with Florida Administrative Code 64E-1, for the examination of 

Environmental samples in the following categories: 

DRINKING WATER - Radiochemistry; SOLID AND CHEMICAL MATERIALS - 

Extractable Organics, General Chemistry, Metals, Pesticides-Herbicides-PCB's, 

Volatile Organics 

Continued certification is contingent upon successful on-going compliance with the 

NEL4C Standards and FAC Rule 64E-1 regulations. Specific methods and analytes 

certified are cited on the Laboratory Scope of Accreditation for this laboratory and are on 

file at the Bureau of Laboratories, P. 0. Box 210, Jacksonville, Florida 32231. Clients 

and customers are urged to verify with this agency the laboratory's certification status in 

Florida for particular methods and analytes. 

EFFECTIVE JULY I, 2003 THROUGH JUNE 30,2004 

Bureau Chief, Bureau of Laboratories 

Florida Department of Health 

DH Form 1697, 7103 

NON-TRANSFERABLE 061161200~E87808 - 
John 0. Agwunobi, M.D., M.8A. 

-ry 

Laboratory Scope of Accreditation Page 1 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCLATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VA00058 (434) 5226150 

E87808 

BWXT Services, Inc 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Drinking Water Certification 

Analyte Methomech Category Type Effective Date 

Gamma Emitters EPA 901.1 Radiochemistry NELAP 511 212003 

Gross-alpha EPA 900 Radiochemistry NELAP 51 1 2/2003 

Gross-beta EPA 900 Radiochemistry NELAP 51 1 2/2003 

Tritium EPA 906 Radiochemistry NELAP 5/12/2003 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further NON-TRANSFERABLE 06/16/2003-E87808 

indicates certification compliant with the NELAC Standards. 
John 0, AgwunoQi, M.D., M.BA. 

Mary 

Laboratory Scope of Accreditation Page 2 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VA00058 (434) 522-6150 

a7808 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

Analyte MethodlTech Category Type Effective Date 

1,1,1,2-Tetrachloroethane EPA 8260 Volatile Organics NELAP 10/3/2002 

1.1-Dichloroethane 

I, l-Dichlorcethylene 

1.1-Dichloropropene 

1.2.3-Trichlorobenzene 

1,2,3-Trichloropropane 

1.2.4-Trichlorobenzene 

1,2,4-Trichlombenzene 

1.2,CTrimethylbenzene 

1.2-Dibromo-3-chloropropane (DBCP) 

1.2-Dibromoethane (EDB, Ethylene dibromide) 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 8270 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Extractable Organics 

NELAP 101312002 

NELAP 10/3IUH)2 

NELAP 1013/2002 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

EPA 8260 Volatile Organics NELAP 101312002 

EPA 8260 Volatile Organics NELAP 1 W3/2002 

EPA 8270 Extractable Organics NELAP 101312002 

EPA 8260 Volatile Organics NELAP 10/3/2002 

EPA 8151 Pesticides-Herbicides-PCB's NELAP 101312002 

EPA 8270 Extractable Organics NELAP 101312002 

EPA 8270 Extractable Organics NELAP 10/3/UX)2 

EPA 8151 Pesticides-Herbicides-PCB's NELAP 10/3/2002 

EPA 8151 Pesticides-Herbicides-PCB's NELAP 10/3/2002 

EPA 8270 Extractable Organics NELAP 101312002 

EPA 8270 Extractable Organics NELAP 1013/2002 

EPA 8270 Extractable Organics NELAP 101312002 

EPA 8270 Extractable Organics NELAP 10/3IUH)2 

EPA 8270 Extractable Organics NELAP 1013/2002 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further NON-TRANSFERABLE W16/2003-E87808 

indicates certification compliant with the NELAC Standards. 
John 0. Agwunobi, M.U., M.B.A. 

Secretciry 

Laboratory Scope of~ccreditatioa Page 3 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCLATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VA00058 (434) 5226150 

E87808 

B WXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

Analy te Method~Tech Category TY pe Effective Date 

2-Butanone (Methyl ethyl ketone, MEK) EPA 8260 Volatile Organics NELAP 1 W3/2002 

2-Chloroethyl vinyl ether 

2-Chlomnaphthalene 

2-Chlomphenol 

2-Chlorotoluene 

2-Cycbhexyl-4,6-dinitrophenol 

2-Hexanone 

2-Methyl-4,6-dinimphenol 

2-Methylnaphthalene 

2-Methylphenol (o-Cresol) 

2-Nitmaniline 

2-Niaophenol 

3,3'-Dichlorobenzidine 

3-Nitroaniline 

4,4 -Methylenebis(N,N-dimethyl 

4,4'-DDD 

4.4'-DDE 

4.4'-DDT 

CBrornophenyl phenyl ether 

4-Chloro-3-methylphenol 

CChloroaniline 

4-Chlorophenyl phenylether 

CChlorotoluene 

CDimethyl aminoazobenzene 

CMethyl-2-pentanone (MIBK) 

4-Methylphenol (pctesol) 

CNitroaniline 

4-Nitrophenol 

CNitrophenol 

Acenaphthene 

Acenaphthylene 

Acetone 

Acetonittile 

Acmiein (Propenal) 

Acrylonitrile 

Aldrin 

EPA 8260 

EPA 8270 

EPA 8270 

EPA 8260 

EPA 8270 

EPA 8260 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8270 

aniline) EPA 8270 

EPA 808 1 

EPA 808 1 

EPA 808 1 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8260 

EPA 8270 

EPA 8260 

EPA 8270 

EPA 8270 

EPA 8151 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 808 1 

Volatile Organics 

Extractable Organics 

Extractable Organics 

Volatile Organics 

Extractable Organics 

Volatile Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Exttactable Organics 

Volatile Organics 

Extractable Organics 

Volatile Organics 

Extractable Organics 

Extractable Organics 

Pesticides-Herbicides-PCB's 

Extractable Organics 

Exttactable Organics 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Pesticides-Herbicides-PCB's 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further 

indicates certification compliant with the NELAC Standards. 

NELAP 

NELAP 

NELAP 

NEL AP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NON-TRANSFERABLE 06/16/2003-E87808 
John 0. Agwunubi. M.D., M.BA. 

-ry 

Laboratory Scope of Accreditation Page 4 of 8 

THIS LISTLNG OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VA00058 (434) 522-6150 

E87808 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

Analyte Method/rech Category Type Effective Date 

Ally1 chloride (3-Chloropropene) EPA 8260 Volatile Organics NELAP 10/3/2002 

alpha-BHC (alpha-Hexachlorocyclohexane) EPA 8081 Pesticides-Herbicides-PCB k NELAP 1 0/3/2002 

alpha-Chlordane 

Aluminum 

Amenable cyanide 

Amenabk cyanide 

Aniline 

Anthracene 

Antimony 

Aroclor-1016 (PCB-1016) 

Arocl~r-1221 (PCB-1221) 

Aroclor-1232 (PCB-1232) 

Aroclor-1242 (PCB-1242) 

Aroclot-1248 (PCB-1 248) 

Aroclor-1254 (PCB-1254) 

Aroclor- 1260 (PCB- 1260) 

Arsenic 

Barium 

Benzene 

Benzidine 

Benzo(g,h,i)perylene 

Benzo(k)fluoranthene 

Benzoic acid 

EPA 8081 

EPA 6010 

EPA 9010 

EPA 9014 

EPA 8270 

EPA 8270 

EPA 6010 

EPA 8082 

EPA 8082 

EPA 8082 

EPA 8082 

EPA 8082 

EPA 8082 

Pesticides-Herbicides-PCB's NELAP 10/3/UX)2 

Metals NELAP 1013/2002 

General Chemistry NELAP 10/3/2002 

General Chemistry 

Extractable Organics 

Extractable Organics 

Metals . 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

EPA 8082 Pesticides-Herbicides-PCB's NELAP 10/3/2002 

EPA 60 10 Metals NELAP 10/3/2002 

EPA 6010 Metals NELAP 1 W312002 

EPA 8260 Volatile Organics NELAP 10/3/2002 

EPA 8270 Extractable Organics NELAP 10/3/2002 

EPA 8270 

EPA 8270 

EPA 8270 

Extractable Organics 

Extractable Organics 

Extractable Organics 

NELAP 10/3/2002 

NELAP 1W3/2002 

NELAP 10/3/2002 

EPA 8270 Extractable Organics NELAP 10/3/2002 

EPA 8270 Extractable Organics NELAP 10/3/2002 

EPA 8270 Extractable Organics NELAP 1 W3/2002 

Benzyl alcohol EPA 8270 

Beryllium EPA 6010 

beta-BHC (beta-Hexachlorocyclohexane) EPA 808 1 

Extractable Organics NELAP 1W3/2002 

Metals NELAP 1 W3/2002 

Pesticides-Herbicides-PCB's NELAP 1 W3/2002 

bis(2-Ch1oroethoxy)methane 

bis(2-Chloroethyl) ether 

bis(2-Chloroisopropyl) ether 

EPA 8270 Extractable Organics NELAP 10/3/UX)2 

EPA 8270 Extractable Organics NELAP 10/3/2002 

EPA 8270 Extractable Organics NELAP 10/3/UX)2 

bis(2-Ethylhexyl) phthalate (DEHP) EPA 8270 Extractable Organics NELAP 10/3/2002 

Boron EPA 6010 Metals NELAP 10/312002 

Bromobenzene EPA 8260 Volatile Organics NELAP 10/3/2002 

Bromochloromethane EPA 8260 Volatile Organics NELAP 10/3/2002 

"STATE" indicates certification for the analyte by the method specified. "NELAP further NON-TRANSFERABLE 06/16/2003-I37808 

indicates certification compliant with the NELAC Standards. 
John 0. Agwunabi, M.D., M.B.A. 

-ry 

Laboratory Scope of~ccreditation Page 5 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E878M EPA Lab Code: VA00058 (434) 522-6150 

E87808 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

Analyte MethodlTech Category TY ~e Effective Date 

Bromodichlommethane EPA 8260 Volatile Organics NELAP 10/3/2002 

Bromoform 

Buy1 benzyl phthalate 

Cadmium 

Calcium 

Carbazole 

Gubon disulfide 

Carbon tetrachloride 

Chlordane (tech.) 

Chlorobenzene 

Chloroethane 

Chloroform 

Chlomprene 

Chromium 

Chrysene 

cis-1.2-Dichloroethylene 

cis- 1.3-Dichloropmpene 

Cobalt 

copper 

Dalapon 

&I ta-BHC 

Dibenz(qh) anthracene 

Dibenzofuran 

Dibmmochlorornethane 

Dibromomethane 

Dicamba 

Dichlorodifluoromethane 

Dichloroprop (Dichlorprop) 

Dieldrin 

Diethyl ether 

Diethyl phthalate 

Dimethyl phthalate 

Di-n-butyl phthalate 

Di-n-octyl phthalate 

Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP) 

Diphenylamine 

EPA 8260 

EPA 8270 

EPA 6010 

EPA 6010 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 808 1 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 6010 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 601 0 

EPA 6010 

EPA 8151 

EPA 8081 

EPA 8270 

EPA 8270 

EPA 8260 

EPA 8260 

EPA 8151 

EPA 8260 

EPA 8151 

EPA 808 1 

EPA 8260 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8151 

EPA 8270 

Volatile Organics 

Extractable Organics 

Metals 

Metals 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Pesticides-Herbicides-PCB's 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Metals 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Metals 

Metals 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Extractable Organics 

Extractable Organics 

Volatile Organics 

Volatile Organics 

Pesticides-Herbicides-PCB's 

Volatile Organics 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Volatile Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Pesticides-Herbicides-PCB's 

Extractable Organics 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further 

indicates certification compliant with the NELAC Standards. 

NON-TRANSFERABLE 06/16/2003-E87808 
deb Bush 

Gorrsmoc 

John 0. Agwunubi, M.B., M.8.A. 

--ry 

Laboratory Scope of Accreditation Page 6 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VA00058 (434) 522-6150 

E87808 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

Analyte Methodmech Category Type Effective Date 

Endosulfan I EPA 808 1 Pesticides-Herbicides-PCB's NELAP 10/3/2002 

Endosulfan I1 EPA 808 1 Pesticides-Herbicides-PCB's NELAP 10/3P2002 

Endosulfan sulfate 

Endrin 

Endrin aldehyde 

Endrin ketone 

Ethanol 

Ethyl acetate 

Ethyl methacrylate 

Ethylbenzene 

gamma-BHC (Liidane, 

gamma-Hexachlorocyc1ohexane) 

gamma-Chlordane 

Heptachlor 

Heptachlor epoxide 

Hexachlorobenzene 

Hexachlorobenzene 

Hexachlorobutadiene 

Hexachlorobutadiene 

Hexachlorocyclopentadiene 

Hexachloroethane 

lgnitability 

Indeno(l,2,3-cd)pyrene 

lodomethane (Methyl iodide) 

Iron 

EPA 8081 Pesticides-Herbicides-PCB's NELAP 10/3/2002 

EPA 8081 Pesticides-Herbicides-PCB's NELAP 1w3m2 

EPA 8081 Pesticides-Herbicides-PCB's NELAP 1 W3/2002 

EPA 808 1 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8270 

EPA 8270 

EPA 808 1 

EPA 8081 

EPA 808 1 

EPA 808 1 

EPA 8081 

EPA 8270 

EPA 8260 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 1010 

EPA 8270 

EPA 8260 

EPA 6010 

lsobutyl alcohol (2-Methyl- I-propanol) EPA 8260 

Isodrin EPA 8081 

Isophorone EPA 8270 

lsopropylbenzene 

Lcad 

Lead 

Lithium 

Magnesium 

Manganese 

MCPA 

EPA 8260 

EPA 6010 

EPA 742 1 

Pesticides-Herbicides-PCB's NELAP 1W312002 

Volatile Organics NELAP 10/3/2002 

Volatile Organics NELAP 1W3/2002 

Volatile Organics 

Volatile Organics 

Extractable Organics 

Extractable Organics 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Pesticides-Herbicides-PCB's 

Extractable Organics 

Volatile Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

General Chemistry 

Extractable Organics 

Volatile Organics 

Metals 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

Volatile Organics NELAP 10/3/2002 

Pesticides-Herbicides-PCB's NELAP 10/3/2002 

Extractable Organics NELAP 10/3/2002 

Volatile Organics 

Metals 

Metals 

NELAP 10/3/2002 

NELAP 10/3/2002 

NELAP 1 W3/2002 

EPA 6010 Metals NELAP 1 W3R002 

EPA 6010 Metals NELAP I ~3/2002 

EPA 601 0 Metals NELAP 10/3/2002 

EPA 8151 Pesticides-Herbicides-PCB's NELAP 1 wm2 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further NON-TRANSFERABLE 06/16/2003-E87808 

indicates certification compliant with the NELAC Standards. 
John 0. Agwunobi, M.D., M.BA. 

Secretary 

Jeb Bush 

Oovamoc 

Laboratory Scope of Accreditation Page 7 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VAOOO58 (434) 522-6150 

E87808 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

 anal^ te Method/Tech Category TYW Effective Date 

MCPP EPA 8151 Pesticides-Herbicides-PCB's NELAP 10/3/2002 

Mercury 

Mercury 

EPA 7470 Metals 

EPA 7471 Metals 

NELAP 10/3/2002 

NELAP 10/3/2002 

Methoxychlor 

Methyl bromide (Bromomethane) 

Methyl chloride (Chloromethane) 

EPA 8081 

EPA 8260 

EPA 8260 

Pesticides-Herbicides-PCB's NELAP 10/3/2002 

Volatile Organics NELAP 10/312002 

Volatile Organics NELAP 10/3/2002 

Methyl tert-butyl ether (MTBE) 

Methylene chloride 

Molybdenum 

Naphthalene 

Naphthalene 

n-Butylbenzene 

Nickel 

Nitrobenzene 

n-Nitrosodi-n-propylamine 

n-Nitrosodiphenylamine 

EPA 8260 

EPA 8260 

EPA 6010 

EPA 8260 

EPA 8270 

EPA 8260 

EPA 6010 

EPA 8270 

EPA 8270 

EPA 8270 

Volatile Organics 

Volatile Organics 

Metals 

Volatile Organics 

Extractable Organics 

Volatile Organics 

Metals 

Extractable Organics 

Extractable Organics 

Extractable Organics 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

n-Nitrosomethylethylamine 

n-Propylbenzene 

Paint Filter Liquids Test 

Pentachlorophenol 

Pentachlorophenol 

pH 

pH 

Phenanhne 

EPA 8270 

EPA 8260 

EPA 9095 

EPA 8151 

EPA 8270 

EPA 9040 

EPA 9045 

EPA 8270 

Extractable Organics 

Volatile Organics 

General Chemistry 

Pesticides-Herbicides-PCB's 

Extractable Organics 

General Chemistry 

General Chemistry 

Extractable Organics 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

Phenol 

Phosphorus, total 

pIsopropyltoluene 

EPA 8270 

EPA 60 10 

EPA 8260 

Extractable Organics 

Metals 

Volatile Organics 

NELAP 10/3/2002 

NELAP 10/3/2002 

NELAP 10/3/UX)2 

Potassium 

Pyrene 

Pyridine 

EPA 6010 

EPA 8270 

EPA 8270 

Metals NELAP 10/3/2002 

Extractable Organics NELAP 10/3/2002 

Extractable Organics NELAP 10/312002 

Reactive cyanide 

Reactive sulfide 

sec-Butylbenzene 

EPA 7.3.3.2 

EPA 7.3.4.2 

EPA 8260 

General Chemistry 

General Chemistry 

Volatile Organics 

NELAP 10/3/2002 

NELAP 1013m2 

NELAP 10/3/2002 

Selenium 

Selenium 

Silica as Si02 

EPA 6010 Metals 

EPA 7740 Metals 

EPA 6010 Metals 

NELAP 1013/2002 

NELAP 30/3/2002 

NELAP 10/3/2002 

"STATE" indicates certification for the anaiyte by the method specified. "NELAP" further NON-TRANSFERABLE 06/16/200.7-E87808 

indicates certification compliant with the NELAC Standards. 
John 0. Agwunobi, M.P., M.BA. 

-*ry 

Laboratory Scope of~ccreditation Page 8 of 8 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87808 EPA Lab Code: VA00058 (434) 5226150 

E87808 

BWXT Services, Inc. 

2016 Mount Athos Road 

Lynchburg, VA 24504-5447 

Matrix: Solid and Chemical Materials 

Certification 

Andyte Method/Tech Category TY pe Effective Date 

Silver EPA 6010 Metals NELAP 10/3/UX)2 

Silver 

Siivex (2,4,5-TP) 

Sodium 

Strontium 

styrene 

Sulfide 

tert-Butylbenzene 

Tetrachloroethylene (Perchloroethylene) 

Thallium 

Thallium 

Tin 

Toluene 

Total cyanide 

Total cyanide 

Toxaphene (Chlorinated camphene) 

Toxicity Characteristic Leaching Procedure 

trans- 1.2-Dichloroethy lene 

trans- 1.3-Dichloropropylene 

trans-1,4-Dichlorw2-butene 

TricNoroethene (Trichloroethylene) 

Trichlorofluoromethane 

Vanadium 

Vinyl acetate 

Vinyl chloride 

Xylene (total) 

Zinc 

EPA 776 1 

EPA 8151 

EPA 6010 

EPA 6010 

EPA 8260 

EPA 903019034 

EPA 8260 

EPA 8260 

EPA 6010 

EPA 7841 

EPA 6010 

EPA 8260 

EPA 9010 

EPA 9014 

EPA 808 1 

EPA 1311 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 6010 

EPA 8260 

EPA 8260 

EPA 8260 

EPA 60 10 

Metals 

Pesticides-Herbicides-PCB's 

Metals 

Metals 

Volatile Organics 

General Chemistry 

Volatile Organics 

Volatile Organics 

Metals 

Metals 

Metals 

Volatile Organics 

General Chemistry 

General Chemistry 

Pesticides-Herbicides-PCB's 

General Chemistry 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Metals 

Volatile Organics 

Volatile Organics 

Volatile Organics 

Metals 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further NON-TRANSFERABLE 06/16/2003-E87808 

indicates certification compliant with the NELAC Standards. 
of Health 

DIVISlON OF EPIDEMIOLOGY 

AND LABORATORY SERVIC!ES 

State of Utah 

Michael 0. Leavitt 

Govenlo~ 

Rod L. Betit 

Executive Director 

Charles D. Brokopp, Dr. P.H. 

Ilirector 

BWXT Services - Lynchburg 

David.S Kohl Director 

2016 Mt. Athos Road 

Lynchburg VA 24504-5447 

ID# BWNU 

Account # 8045226000 

Director, 

On the basis of your most recent assessment, Proficiency Testing results and continuing 

compliance with the ELCP requirements, the laboratory listed is certified for environmental 

monitoring under the Resource Conservation and Recovery Act and authorized to perform the 

following methods, for the analytes and matrix listed:l 

)(onPotable Water 

Characteristics 

1010 lgnitabilii 

1311 Toxicity Characteristic Leaching Procedure Metals 

1311 Toxicity Charactehtic Leaching Procedure Semi-Volatiles 

1311 Toxicity Characteristic Leaching Procedure Vobtiles 

Sec 7.3.3 Reactive Cyanide 

lnomanics 

9010 B Cyanide Distillation Procedure 

9014 CyanMe 

9030 B Sutiide Distillation Procedure 

9034 Acid-Soiuble and Add-Insoluble Sulfides 

9040 B PH 

9045 B Soil and Wade pH 

Metals 

6010 B Aluminum 

6010 B Antimony 

6010 B Barium 

6010 B Boron 

6010 B Cadmium 

6010 B Calcium 

6010 B Chromium 

6010 B Cobalt 

6010 B Iron 

6010 B Lead 

6010 B Molybdenum 

6010 B Nickel 

6010 B Phosphorus 

6010 B Potassium 

6010 B Silver 

6010 B Sodium 

6010 B Tin 

The expiration for the laboratory's certification is 10/31/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 

Burcau of Laboratory Improvement 46 Korlh Med~c;il l)t.ivc Salt L;~lcc City, Uli~h 841 13- 1105 

'libicphonc. (801 .584-.18(il) 1";tx: 1801 I 58.1-8501 l~lt.~~:/hlunis.Iil.sL~~t.c~~~t .~~s/cls/l;il~inil) 
BWXT Services - Lynchburg 

Resource Conservation and Recovery Act 

Page 2 of 6 

- Metals 

742 1 Lead 

7740 Selenium 

7761 Silver 

Oraanic lnstrumentation 

8151 A 2,4,5-TP (Silvex) 

8260 B 1,l -Dichloroethylene (ethene) 

8270 C 4-Methylphenol (p-cresol, 4-Hydroxytoluene) 

8270 C 4-Nitroaniline 

8270 C bis(2-chloroethoxy)methane 

8270 C bis(2-Chloroethy1)ether 

8270 C bis(2-chloroisopropyl)ether 

8270 C Butyl Benzyl Phthalate 

8270 C C hrysene 

8270 C Di-n-butyl phthalate 

8270 C Di-n-octyl Phthalate 

8270 C Diethyl Phthalate 

8270 C Dimethyl Phthalate 

8270 C Indeno(1,2,3cd)pyrene 

8270 C Phenanthrene 

8270 C Phenol 

8270 C Pyrene 

8270 C Pyridine 

Solid 8 Chemical Materials 

Characteristics 

Sec 7.3.4 Reactive Sulfde 

lnoraanlcs 

9095 A Paint Filter Liquids Test 

- Metals 

6010 B Arsenic 

6010 B Beryll~um 

6010 B Copper 

6010 B Lithium 

6010 B Magnesium 

6010 B Manganese 

6010 B Selenium 

6010 B Silica 

6010 B Strontium 

6010 B Thallium 

6010 B Vanadium 

6010 B Zinc 

7470 A Mercury 

7471 A Mercury 

7841 Thallium 

Oraanic lnstrumentation 

8081 A 4,4'-DDD 

8081 A 4,4'-DDE 

8081 A 4,4'-DDT 

8081 A Aldrin 

8081 A alpha-BHC(alpha-hexachlorocyclohexane) 

8081 A alphaChlordane 

8081 A beta-BHC(beta-hexachlorocyclohexane) 

8081 A Chlordane (technical) -- - -- -. . . - - 

The expiration for the laboratory's certification is 10/31/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 
BWXT Services - Lynchburg 

Resource Conservation and Recovery Act 

Page 3 of 6 

Oraanic Instrumentation 

8081 A delta-BHC(delta-hexachlorocyclohexane) 

8081 A Dieldrin 

8081 A Endosulfan I 

8081 A Endosulfan ll 

8081 A Endosulfan sulfate 

8081 A Endrin 

8081 A Endrin Aldehyde 

8081 A Endrin Ketone 

8081 A gamma-BHC (Lindane, gamma-hexachlorocyclohexane) 

8081 A gamma-Chlordane 

8081 A Heptachlor 

8081 A Heptachlor Epoxide 

8081 A Hexachlorobenzene 

8081 A lsodrin 

8081 A Methoxychlor 

8081 A Organochlorine Pesticides 

8081 A Toxaphene [Chlorinated camphene] 

8082 Arolcor-1016 [PCB-$ 01 61 

8082 Arolcor-1221 PCB-1 2211 

8082 Arolcor-1232 [PCB-12321 

8082 Arolcor-1242 [PCB-1 2421 

8082 Arolcor-1248 [PC512481 

8082 Arolcor-1254 [PCB-1254) 

8082 Arolcor-1260 [PCB-12601 

8082 PCBs 

8151 A 2,4,5-T 

8151 A 2,4D 

8151 A 2,4-DB 

8151 A 4Nitrophenol 

8151 A Chlorinated Herbicides 

8151 A Dalapon 

8151 A Dicamba 

8151 A Dichlorprop(Dichloroprop) 

8151 A Dinoseb (DNBP, 2.sec-butyl-4,6-dinitrophenol) 

8151 A MCPA 

8151 A MCPP 

8151 A Pentachlorophenol 

8260 B 1,l ,I ,2-Tetrachloroethane 

8260 B 1 ,l ,l-Trichloroethane 

8260 B 1 ,l,2,2-Tetrachloroethane 

8260 B 1 ,I ,2-Trichloroethane 

8260 B 1 ,l-Dichloroethane 

8260 B 1,l-Dichloropropene 

8260 B 1,2,3-Trichlorobenzene 

8260 B 1,2,3-Trichloropropane 

8260 B 1,2,4Trichlorobenzene 

8260 B 1,2,4Trimethylbenzene 

8260 B 1,2-Dibromo-3-chloropropane (DBCP) 

8260 B 1,ZDibrornoethane (EDB, Ethylene dibromide) 

8260 B I ,2-Dichlorobenzene 

8260 B 1 $2-Dichloroethane 

8260 B 1,2-Dichloropropane 

The expiration for the laboratory's certification is 10/31/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 
BWXT Services - Lynchburg 

Resource Conservation and Recovery Act 

Page 4 of 6 

Omanic Instrumentation 

8260 B 1,3,5=rrimethylbenzene 

8260 B 1,s-Dichlorobenzene 

8260 B 2,2-Dichloropropane 

8260 B 2-Chloroethyl Vinyl Ether 

8260 B 2-Chlorotoluene 

8260 B 2-Hexanone 

8260 B 44hlorotoluene 

8260 B CMethyl-2-pentanone (MIBK, Isopropylacetone, Hexone) 

8260 B Acetone 

8260 B Acetonlrile 

8260 B Acrolein (Propenal) 

8260 B Acrylonitrile 

8260 B Allyl Chloride (3-Chloropropene) 

8260 B Benzene 

8260 B Brornobenzene 

8260 B Bromochlorornethane 

8260 B Brornodichloromethane 

8260 B Bromoform 

8260 B Carbon Diulfide 

8260 B Carbon Tetrachloride 

8260 B Chlorobenzene 

8260 B Chlorodibromornethane [Dibrornochlorornethane] 

8260 B Chloroethane 

8260 B Chloroform 

8260 B Chloroprene 

8260 B cis-1,2-Dichloroethene (ethylene) 

8260 B cis-1,3-dichloropropene 

8260 B Dibromornethane 

8260 B Dichlorodifluoromethane 

8260 B Diethyl Ether 

8260 B Ethanol 

8260 B Ethyl Acetate 

8260 B Ethyl Methacrylate 

8260 B Ethylbenzene 

8260 B Hexachlorobutadiene 

8260 B lodomethane (Methyl iodide) 

8260 B lsobutyl Alcohol (2-Methyl-1-propanol) 

8260 B lsopropylbenzene 

8260 B Methyl bromide [Bromornethane] 

8260 B Methyl chloride [Chlorornethane] 

8260 B Methyl Ethyl Ketone (MEK, 2-Butanone) 

8260 B Methyl-t-Butyl Ether (MTBE) 

8260 B Methylene Chloride 

8260 B Naphthalene 

8260 B p-lsopropyltoluene 

8260 B Styrene 

8260 B tert-Butylbenzene ... - 

The expiration for the laboratory's certification is 10/31/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 
BWXT Services - Lynchburg 

Resource Conservation and Recovery Act 

Page 5 of 6 

Oraanic lnstrumentatlorl 

8260 B Tetrachloroethylene (Perchloroethylene -ethene) 

8260 B Toluene 

8260 B trans-1 ,2-Dichloroethylene (-ethene) 

8260 B trans-1 .bDichloropropylene (-propene) 

8260 B trans-1,4dichloro-2-butene 

8260 B Trichloroethene (Trichloroethylene) 

8260 B Trichlorofluoromethane 

8260 B Vinyl Acetate 

8260 B Vinyl Chloride 

8260 B Volatile Organic Compounds 

8260 B Xylene 

8270 C 1,2,4-Trichlorobenzene 

8270 C 1,2-Dichlorobenzene 

8270 C 1,2-Diphenylhydrazine 

8270 C 2Chlorophenol 

8270 C 2-Cyclohexyl4,Winitrophenol 

8270 C 24ethyl4,Winitrophenol (4,6-Dinitro-2-methylphenol) 

8270 C 24ethylnaphthalene 

8270 C 2-Methylphenol (o-cresol, 2-Hydroxytoluene) 

3-Nitroaniline 

4,CMethylenebis (N,N-dimethylaniline) 

4-Bromophenyl Phenyl Ether 

4-Chloro-3methylphenol 

4-Chloroaniline 

4-Chlorophenyl Phenyl Ether 

4-Nitrophenol 

Acenaphthene 

8270 C Acenaphthylene 

8270 C Aniline 

8270 c Anthrawne 

8270 C Benzo(k)fluoranthene 

8270 C Benroic Acid 

8270 C Benzyl alcohol 

8270 C bis(2-Ethylhexyl) phthalate (DEHP) - . - 

The expiration for the laboratory's certification is 10131/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 
BWXT Services - Lynchburg 

Resource Conservation and Recovery Act 

Page 6 of 6 

Orqanic Instrumentation 

8270 C Carbazole 

8270 C Dibenzo(a,h)anthracene 

8270 C Dibenzofuran 

8270 C Diphenylamine 

8270 C Fluoranthene 

8270 C Fluorene 

8270 C Hexachlorobenzene 

8270 C Hexachlorobutadiene 

8270 C Hexachlorocyclopentadiene 

8270 C Hexachloroethane 

8270 C lsophorone 

8270 C n-Nitrosdi-n-Propy lamine 

8270 C n-Nitrosodiphenylarnine 

8270 C N-Nitrosomethylethylamine 

8270 C Naphthalene 

8270 C Nitrobenzene 

8270 C Pentachlorophenol 

8270 C Semivolatile Organic Compounds 

The effective date of this certificate letter is: 11/1/2003. 

The analytes by method which a laboratory is authorized to perform at any given time will be those 

indicated in the most recent certificate letter. The most recent certification letter supersedes all 

previous certification or authorization letters. It is the certified laboratory's responsibility to review 

this letter for discrepancies. The certified laboratory must document any discrepancies in this letter 

and send notice to this bureau within 15 days of receipt. This certificate letter will be recalled in the 

event your laboratory's certification is revoked. 

Charles ~roko~p,-~r. P.H. 

Director 

-% -- -- 

The expiration for the laboratory's certification is 10/31/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 
of Health 

DIVISION OF EPIDEMIOLOGY 

AN11 1.AHORA'rORY SERVICES 

State of Utah 

Michael 0. Leavitt 

Gover~lor. 

Rod L. Betit 

Executive Diloctor 

Charles D. Brokopp, Dr. P.H. 

Director. 

ID# BWNU 

Account # 8045226000 

BWXT Services - Lynchburg 

David .S Kohl Director 

2016 Mt. Athos Road 

Lynchburg VA 24504-5447 

Director, 

On the basis of your most recent assessment, Proficiency Testing results and continuing 

compliance with the ELCP requirements, the laboratory listed is certified for environmental 

monitoring under the Safe Drinking Water Act and authorized to perform the following methods, for 

the analytes and matrix listed: 

Drlnkimr Water 

Radionuclides 

900.0 Gross Alpha 

900.0 Gross Beta 

901 .I Gamma Emitting Radionudiii in Drinking Water 

906.0 Tritium in Drinking Water Uquid Scintillation Technique 

The effective date of this certificate letter is: 11/1/2003. 

The analytes by method which a laboratory is authorized to perform at any given time will be those 

indicated in the most recent certificate letter. The most recent certification letter supersedes all 

previous certification or authorization letters. It is the certified laboratory's responsibility to review 

this letter for discrepancies. The certified laboratory must document any discrepancies in this letter 

and send notice to this bureau within 15 days of receipt. This certificate letter will be recalled in the 

event your laboratory's ceM1cation is revoked. 

Respectfully, 

Director 

The expiration for the laboratovs certification is 10/31/2004. The Utah Environmental Laboratory Certification 

Program (ELCP) encourages clients and data users to verify the most current certification letter for the 

authorized method. For further assistance please call Lorna Ward 801-584-8469. 

Bureau of Laboratory Improvement 46 North Medical I)l.ive Salt 1,;tkc City, Ut.ah H411:3-1105 

'li:lcphot~c~. (X01 1 5x4-486') Fax: (SO1 I 584-H501 hl.t~~:Nhlunix.hl.st:~t.c.ut .us/ols/l~l)irnl) 

Laboratory Scope of Accreditation Page I of 6 

THIS LlSTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WlTH A VALID CERTIFICATE 

State Laboratory ID: Efj7769 

E87769 

Eno Rivcr Labs, LLC 

2445 S. Alston Ave. 

Durham. NC 27713-441 1 

EPA Lab Code: NC01324 (9 19) 544-5729 

Matrix: Drinking Watcr 

Certification 

Analyte Methodmech Category TY Effective Date 

2,3,7,8-Tetrachlorodibenzo-paioxin EPA 1613 Dioxin NELAP 6/25/01 

"STATE" indicates certification fur the analyte by the method specified. "NELAP" furtl~er NON-TRANSFERABLE 05105/2004-E87769 

indicates certification compliant with the NELAC Standards. 
Laboratory Scope of Accreditation Page 3 of 6 

THIS LISTING OF' ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A vALm CERTIFICATE 

State Laboratory ID: E87769 EPA Lab Code: NC01324 (91 9) 544-5729 

E87769 

Eno Rivcr Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-441 1 

Matrix: Non-Potable Water 

Certification 

Analyte Methodmech Category Type Effective Date 

2,3,7,8-Tetrachlorodibe11~3-p40~1n EPA 8290 Extractable Organics NELAP 71 1 103 

"STATE" indicates certification for the analyte by the method specified. "NELAP" hrtl~er NON-TRANSFERABLE 05/05/2004-E87769 

indicates certification compliant with the NELAC Standards. 
Laboratory Scope ofAccreditation Page 5 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87769 EPA Lab Code: NC01324 (919) 544-5729 

E87769 

Eno River Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-441 1 

Matrix: Solid and Chemical Materials 

Certification 

Analyte MethodtTeeh Category Type Effective Date 

2,3,7,8-Tetrachlorodibenzo-p-dioxin EPA 8290 Extractable Organics NELAP 6/25/01 

"STATE" indicates certification for the analyte by the method specified. "NELAP" further NON-TRANSFERABLE 05/0512004-E87769 

indicates certification co~npliant wit11 fhe NELAC Standards. 
Eno River Labs Certifications 

deb Bush John 8. Agwunobl. M.D.,M.S.A. 

Gavmmor Secretary 

Luborutory Scope of Accredilation Page 1 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State 1.aboratory ID: E87769 EPA Lab Code: NC01324 (919) 544-5729 

E87769 

Eno River Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-4411 - -. Matrix: Drinking Water 

Certification 

Anaiyte Methodmech Category Type Effective Date 

2,3,7,8-Tet1achloro&knzo-p-d1oxin EPA 1613 DIOXIII NELAP 6/25/2001 

"STATE" indicates certification for the analyte by the method specified. "NEL,AP" further NON-'rKANSFEKAHLE M/0112004-EX7769 

indicates certification compliant with the NEI.AC Standards. 
Laboratory Scope of Accreditation Page 2 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Lahoratory ID: E87769 EPA Lab Code: NC01324 (919) 544-5729 

E87769 

Eno River Labs, LLC 

2445 S. Aiston Ave. 

Durham, NC 27713-441 1 

Matrix: Non-Potable Water 

Certification 

Analyte MethodlTech Category TY pe Effective Date 

1,2,3,4,6,7,8,9-Octachlorodibcnzo~uran (OCDF) EPA 161 3 Extraclable Organ~cs NELAP 6/25/2001 

1,2,3,4,6,7,8.9-Octachlorodibe~~mfuran (OCDF) EPA 8290 Extractable Organlcs NELAP 7/1/2003 

1,2,3,4,6,7,8,9-Oct,Ichlorodibenzo-pdioxin EPA 1613 Extractable Organics NELAP 6/25/2001 

(OCDD) 

EPA 8290 Extractable Organics NELAP 

EPA 1613 Ext~xctable Organics NELAP 

EPA 8290 Extractablc Orgartics NELAP 

EPA 1613 Extractable Organics NELAP 

EPA 8290 Extractab? Organics NELAP 

EPA 1613 Extractable Organics NELAP 

EPA 8290 Extractable Organics NELAP 

EPA 1613 

RPA 8290 

EPA 1613 

EPA 8290 

EPA 1613 

EPA 8290 

EPA 1617 

EPA 8290 

EI'A I613 

EPA 8290 

EPA 1613 

ht'A 8290 

HPA 16 1 7 

EPA 8290 

EPA 1613 

EPA 8290 

EPA 1617 

EPA 8290 

EPA 1617 

EPA 8290 

EPA I611 

HPA 8290 

EPA 1611 

Extraclable Organics 

F.xtractablc Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extraclablc Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extraclabk Organics 

Extrdclable Organics 

Exlraclablc Organics 

13xt1aclablc Organics 

Extratable Organics 

Extractablc Organics 

Extractable Organics 

Ext~xtable Organics 

Extractable Organics 

Extraclablc Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

NELAP 

N ELA P 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NkLAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

"STATIC" indicates certification for the analyte by the method specilied. "NELAP" further NON-TRANSFERABLE 06/01/2004-E87769 

indicates certification compliant with the NEI,AC Standards. 
Laboratory Scope of Accreditation Page 3 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87769 EPA Lab Code: NC01324 (919) 544-5729 

E87769 

Eno River Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-4411 

Matrix: Non-Potable Water 

Certification 

Analyte Methodmech Category TYW Effective Date 

2,3,7,8-Tetrachlorodibcn7~-p-ciioxin EPA 8290 Extractable 0rG-t~~ NELAP 711 12003 

"STATE" indicates certification for the analyte by the n~elhod specified. "NELAP" further NON-TRANSFERABLE 06/01/2004-E87769 

indicates certification compliant with the NEI,AC Standards. 
Jnhn 0. Agwunobf, M.D.,M,B.A. 

Secxetary 

Laboratory Scope of Accreditation Page 4 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VAI,ID CERTIFICATE 

State Laboratory ID: E87769 EPA 1,ah Code: NC01324 (919) 544-5729 

E87769 

Eno River Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-4411 

Matrix: Solid and Chemical Materials 

Certification 

Analyts MethnUl'ech Category TY ~e Effective Date -- 

1,2,3,4,6,7,8,9-OctachlorOdibenu,furan (OCDFI EPA 8280 Extractable Organics NELAP 6/25/20 1 

1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF) EPA 8290 Extractable Organics NELAP 6/25/200 1 

1,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin EPA 8280 Extractablc Organics NRLAP 6/25/200 1 

(OCDD) 

1,2,3,4,6,7,8,9-Octachlortdibenzo-pdioxin 

(OCDD) 

1,2,3,4,6,7,8-Hep(ach1orociibenzofuran 

(1,2,3,4,6,7,8-hpcdR 

I ,2,3,4,6,7,8-Hcptachlorodibenzofut.an 

(1 2,3,4,6,7,8-hpcdo 

1,2,3,4,6,7.8-Heptachlorcdibe~~zo-pdioxin 

(1,2,3,4,6,7,8-hpcdd) 

1,2,3,4,6,7,8-Heptachlordibcnzo-p-dioxi11 

(1,2,3,4,6,7,8-hlxdd) 

1,2.3,4,7,8,9-Heplachlorodiht:nzofuran 

(1,2,3,4,7,8,9-hpcdf) 

1,2,3 ,4.7,8,9-Heptachlorodibenzofunn 

(1,2,3,4,7,8,9-hpcdf) 

1,2,3,4,7,8-Hxcdd 

EPA 8290 Extractable Organics NELAI' 

EPA 8280 Extractable Organics NELAP 

Extractable Organics NELAP 

EPA 8280 Exlractahle Organics NELAP 

EPA 8290 Extractablc Organics NELAP 

EPA 8280 

EPA 8290 

Extractablc Organics NRLAP 

Extractable Organics NELAP 

EPA 8280 

RPA 8290 

EPA 8280 

HPA 8290 

EPA 8280 

EPA 8290 

EPA 8280 

EPA 8290 

EPA 8280 

EPA 8290 

Exuaclahle Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

Extractal>le Organics 

Extractable Organics 

Extractable Organics 

Extractable Organics 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

EPA 8280 

EPA 8290 

EPA 8280 

EPA 8290 

HPA 8280 

Hxtractablc Organics 

Extractablc Organics 

Extractable Organics 

Extractablc Organics 

Extractable Organics 

NELAP 6/25/200 1 

NELAP 6/25/2001 

NELAI' 6/25/2001 

NELAP 6125t200 1 

NELAP <d25/2oOl 

EPA 8290 

EPA 8280 

EPA 8290 

BPA 8280 

EPA 8290 

Extractable Organics NHLAP 6/25/200 1 

Extraclahlc Organics NELAP 6/25/2001 

Extractable Organics N HLAP 6/25/200 1 

Extraclable Organics NELAP 6/25/2001 

Extractable Organlcs NELAP 6/25/2001 

2,3,7,8-TCDF EPA 82x0 Extractable Organics NELAP 6/25/2001 

2,3,7,8-TCDF EPA 8290 Extractable Organics NELAP 6/25/200 1 

2,3,7,8-Tetrachlorodiben7.o-pdioxin EPA 8280 Extractable Organics NELAP (d2.51200 1 

"STATE" indicates certifiwtio~~ for thc analyte by the mell~od specified. "NEI,APW further NON-TRANSFERABLE 06/01/2004-I337769 

indicates certification compliant with the NELAC Standards. 
Laboratory Scope of Accreditation Page 5 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: ES7769 EPA Lab Code: NC01324 (919) 544-5729 

ES7769 

Eno River Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-4411 

Matrix: Solid and Chemical Materials 

Certification 

Analyte Methodmech Category Type Effective Date 

2,3,7,8-Tetrachlorodibem-pdioxin EPA 8290 Exlnctahle Organics NELAP 6/2SRM)1 

8, . . S1 ATIS" indicates certification for the analyte by the method specified. "NEI,APW further NON-TRANSFERABLE 06/01/2004-E87769 

indicates certification compliant with the NEI,AC Slandards. 
dab Bush John 0. Agwunobi, M.D.,M.S.A, 

Grrvarnor Se-tary 

Laboratory Scope of Accreditation Page 6 of 6 

THIS LISTING OF ACCREDITED ANALYTES SHOULD BE USED ONLY WHEN 

ASSOCIATED WITH A VALID CERTIFICATE 

State Laboratory ID: E87769 EPA Lab Code: NC01324 (919) 544-5729 

E87769 

Eno River Labs, LLC 

2445 S. Alston Ave. 

Durham, NC 27713-4411 

Matrix: Biological Tissue 

Certification 

Analyte Methog'ech Category TY pe Effective Date 

1,2,3,4,6,7,8,9-Octachlorodikn-mfum (OCDF) EPA 8290 Exlraclablc Organlcs NFLAP 7/1/2003 

1,2,3,4,6,7,8,9-0ctachlorodibt:nm-p-dloxin 

(OCDD) 

1,2,3,4,6,7,8-Heptachlorodiknzofuran 

(1,2,3,4,6,7,8-hpcdO 

1,2,3,4,6,7,8-Heptachlorodibenzo-pdioxln 

(12,3,4,6.7,8-hpcdd) 

1,2,3,4.7,8,9-Heptilchlorodibenzofuran 

(1,2,3,4,7,8,9-llpcdo 

1,2,7,4.7,8-Hxcdd 

EPA 8290 

EPA 8290 

EPA 8290 

EPA 8290 

FPA 8290 

EPA 8290 

EPA 8290 

EPA 8290 

EPA 8290 

EPA 8290 

EPA 8290 

Fxtractable Organics 

Extractablc Organics 

Extractable Organics 

Extnctablc Organics 

Extriictable Organics 

Extractable Organics 

Extractable Organics 

F~triactable Organics 

Extractablc Organics 

Extractable Organics 

Extractable Orga~iics 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NEI,AP 

1,2,3,7,8-Pccdf EPA 8290 Extractable Organics NELAP 7/1/2003 

2,3,4,6,7,8-Hxcdf EPA 8290 Extnctablc Orgailu NELAP 7/1/2003 

2,3,4,7,8-Pccdf EPA 8290 Extraclai~le Organtcs NELAP 7/1/2003 

2,3.7,8-TCDP EPA 8290 Extractable Organics NELAP 7/1/2003 

2,3,7,8-T&xhlomdibenzo-p-d~oxtn EPA 8290 Extractable Organlcs NELAP 71 112003 

"STATIC" indicates certitication for the analyte hy tile method specified. "NEI.AP" further NON-TRANSFERABLE 06/01/2004-E87769 

indicates certification compliant with the NK1,AC Standards. 
STL St. Louis Laboratory Certifications 

deb Bush 

Gwernnr 

Jahn 0. Agwunobi, M.D., M.B.A. 

Secfalary 

Page 1 of 27 

'TIIIS LAISTIKG 017 AC:C!KElWI'EU ANALYl'ES SHOUI,II RE USED ONLY WHEN 

ASSOCIATEI> W11'H A VALID CPRTlBICKITC 

State Laboratory ID: Kg7689 EPA Lab Cocle: MoOUU54 (314) 298-8566 

lilt7689 

Sir, St. Louis 

13715 Rider Truil North 

Ea~lh City, hIO 63045 -.--- ------.-- ----..-.-, 

Matrix: Dri~tliing Water 

Certification 

Annlyte Meti~udflech Category Type EfCceilve Date 

-.,...-. -,,.-. ---- .--..--,--,.-...--- 

I ,I ,I l-Tct~schlon)ctl~~mc El'h 5243 Cimup 11 tinreplatcul Contaltiinartts NElAP 7/17iZU03 

EI'A 524.2 Otticr Rcguliltcd Contaminiults NELAP 71 I7/2003 

EPA 524.2 Cintup 11 IJ~trqmfatcrl L'ontaai~mnk NELAI' 711 712003 

EPA 524.2 Otl~cr Rcgulwrvl C.'onMn~inants KELAP 71 17i2003 

E PA 5242 Group II IJnrcgulrtal C:onlamroantr NELhP 7/17/2003 

CPA 524.2 

13PA 524.2 

Ef'A 524.2 

EPA 524.2 

EPA 524.2 

Other Rcgulatcd Ct~nlumirulnls NELAP 7/171201)3 

(imup 11 Urucgul~ul Contuminsnis NELAP 71 1 71203 

Ci~rup 11 tlnrcgulatnd Conlaminiiits MEWI' 7/ 1 712003 

Qmup I1 Unrcgutntcd Coritiut;uninairls NEMl' 711 712003 

Group I1 LJt~cgulettxl Cuslitniu~ants NELhP 7i 1 7LM03 

1.2.4-Tnn~ethylbaizeitc . EPA 524.2 Group Ii Ulucgul~ccl C:trn~itririnants NELAP 1/17/2003 

1.2-Bil~roiolrw-3chlorii(ru~;lnc (DBCP) EPA 524.2 Gmup 11 U~u~~ulatcd Coslar~iinonts NEI.AIa ?I 1 i:2rfO! 

1 .Z-Dibran~c~c~harle (F,lX%, Elltylcnc dibro~rrirlc) EIaA 524.2 

1.2-~>ichlur(ibc~~zine EPh 524.2 

1.2-r)ichlord1ii1c EPA 524.2 

1,2-Dieltkm~priipitut. iiPA 524.2 

1.3.5-Ttitiic~l~ylbmi.cnc ' HPA 524.2 

.EPA 524.2 Group 11 linrcgulittcd Contalainar\ts NE.I.Al' 7'1 7Q003 

EPA 524.2 C;ioup I1 llnrcguliltrcl Contanii~lsnts NELAP ill 7,10(13 

f?PA 524.2 Other Kcgida~cd C'onlutninirnLs NELAP 7 i 1 7i2IM3 

EPA 524.2 Liro~ip I1 Urrcgulald C:tmliln~in:mls 'N Et.A E' 7ilW2003 

EI'A 524.2 Ciruup 11 Ut~rcgulatcd Conlan)i~lanlv NEiAP 7i17~003 

EPA 524.2 Gritup It Ilnrogulatal Co~~la~ninunlF NEIAI' 7/1712(Kl3 

CPA 5242 Croup 11 Ilrrn~lPtid Contarr~inrt~)ts NELAP 7/ 1 7i200.f 

EPA 524.2 Otller Rugulr~cd Cc~nlaminiinls NELAP 71 1712003 

I!PA 524.2 Ciroup 11 llnrcgulalcvt C:ont~nrinn~its NELAP ii17/.2003 

Ijl'A 524.2 Gmup 11 IJnrcguicud Coniarniiu?nls WELAP 71 17!2003 

EPA 524.2 

RI'A 524.2 

El'A 524.2 

Cin~up I1 Clrrcegu1;ltcd Co~i~nii~~rits NEI,AP 7/ 17003 

Gmtrp 11 Unrcgulntnd ~rrllillllil~lll~ NI-:I,AP 71 1 712003 

Other Kcgalaled Conhriiiiuuanls NELAI' 7/ 1 712003 

EI'A 524.2 Other Krgtrliitcd Coetanlirl;uils 'NEl.Af2 7/17/2003 

kPh 524.2 Grrrup fl Unrogulatcd Cootanrin&nls NE1.AP 7/1712003 

EI'A 524.2 

EPA 523.2 

F.PA 524.2 

Group 11 Unrqrli~tecl (:oeIaniieiuils NEI.AP 7/17i2003 

Ollier Regulated Coatan~inaols NELAP ?/l?RM)> 

Grttup 11 Unrcgulatcd Co1llilli,i11snls NE1.AP 711 7/2003 

Z~ibro~~lochinron~cthiwe EI'A 524.2 Group 11 ilrlrcyulaled L:orililn~inai~ls NEI,AIa 711 712003 

"STKI'E" indicates crrtificafino Cor thc anxlytc by thc n~ctltorl specifietl. "NELAP" furttrcr NON-TKANSf'ERABI,F, 1 III .WOOS-EX?iiRY 

indicatcs certiftcntio~i compliant with the NEI,AC Sla~uhrds. 
John 0. Agwunabi, M.D., M.B.A, 

Secretary 

Laborafoty Scope of Accreditatinti Page 2 of 27 

St~tc L~borato~ 1I3: E87689 EPA Lab Code: hiOOUO54 (314) 298-8S6 

E87689 

S'rL St. Idoub 

13715 Kidcr Trail North 

Earth Clty, iclO 63045 --,-,- --. -,...- --- .-.- Matrix: ~;&in~ water 

Ccr(ificatiun 

Analyte Mctl~odlt'ech CR tegory Effective 1)rite - '1LW -.,- 

Dibro~nomcthiure BiaA 52i.Y Gmup 11 umguGicd Con~-ln~iiutrits NELAP 7/ I 712003 

Dichktrwlifiuurunudii~ne EPA 524.2 Croup tl Unrcgulxtietl Contilttimunts Nl!L.AP 7/17/2003 

Dicbk~mmcLaac (DCM, Metbylole chloride) :)PA 524.2 

Wly lhar/errc PPA 524.2 

Ciam~rw Emiltcn EPA 901.1 

Gmss-alphn EPA WO 

Grctss-beta EPA 900 

Hcxschlorobuladicnc EI'A 524.2 

isqwopylbmzmc RPA 524.2 

McU~yl bn~micic (L\r01ruitnctl18nc) BPA 5242 

MeUlyl chlaride (Chloromctha~lc) CPA 524.2 

klcthyf tnz-ht~tyl rtilcr (MTBE) EPA 524.2 

Otller Rcguliited (:onta~oi~lants NELAP 711 7/2U03 

Cfll~w Kcgulnlcd Con(arnina111s NliLAP 71 3 712003 

itrdiuclrnriuy NICLAP 2/15/2002 

Rtwliochcn~Ltr)~ NEIAI' 21 1 30002 

Ruhchumistty NELAP 2/33/2002 

Group If Unregui:Ucd Corht~niinanls NBLAP 71 17J2W3 

Group 11 IJnr~%ulatcd Coalaminants NELAP 7/17/2001 

Group II llnrcgutatrct Contnnrinancs NELAP 7/17/2003 

Group 11 Unrcgukt~xi C:~~~t,lmioaets NEi.AP 7/ 1 7i70113 

Gnjup I1 Llnrtplied Cortlaminar~ts NELAf' 711 7i2003 

EI'A 524.2 Group 11 llnregulatcd Conri~minants NELAI' 711 7/2003 

ASTM U 5 174-91 I?adioclrwnistry NIJLAP ?!I 3.~2002 

PPA 514.2 

CPA 524.2 

fiPA 3 14.0 

EPA 903 

EPA 904 

EPA 5242 

ME St42 

1X)G Sr-02 

EPA 524.2 

EPA 524.2 

'fctmciy (Pmzhtomctiryicnc) EPA 524.2 

litlumc EPA 524.2 

tmns-1,2-Diclitorr~ctl1yi01~' EPA 524.2 

Lr~ns-l,3-DkhIomppylnic F3'A 524.2 

'f'rid~lotuclbe:~e (lrichloroc?hylcnc) IKI'A 524.2 

Trichluroflitoron~~~nc Lt'A 524.2 

Tritinm EPA 906 

Vinyl chtoridc EPA 524.2 

Group I1 U~ncguti~ted Contariiiier~% NIIiAP 7:l 7i2003 

Gn~up ll Un~ulalerl Cunii~mir~iu~ts NEI-AI' 711 7/21103 

Secontlary Inorguttic Conlanlinitnts NEIAI' 211 3i2002 

hdioche.~nistq+ NELAP 21 1 312(K)2 

Kadiocl~co~ht~y NELAP UI 3Q002 

Gmup I1 Unregulat~d Contanriisnls NEL.Ai' 71 1 712003 

Rudiochenrbtry K BIA P 2/13/2002 

Radinctrcntbtry NPLAP Yi3/202 

OUicr Rcguked Cbntarninuna NELAI' 7/17/2003 

Group I1 Unmgulatcd Cotktarriinants NELAP 711 712003 

Oihcr Rcguldeci Ck>ntanrirlants NBLAP 711 712003 

Other Hcpfiltcd Conliltniniu~ts NliLAI' 711 7/2W 

Other Kcgulntcvt Cijnutniinants NEI.AY 7/1'li2W3 

(imup If LJ~~rcgulatrd Coillaminants NEI.AIJ 7/ 1 7j2003 

Olha Regulated Co~ilitniintull?: NELAI1 7/17/M03 

Ciroup I1 Ihrcytated C~drrninenls NBLAP 71 1712003 

Radiocltemistry NELAP 2/13/2002 

Other Rcgul~ilal Conlninin;~i~ls NELAI' 711 7/2003 

"STA'I%:" indicntcs ccrtiftcltfiun for thcaortlytc hy ~bc mcthod sp'cifietl. "NELAP" further NON-TRANSI-EKABLE 1 1113/2003-887689 

indicates ccrtificatinn rurnpliatit with the NELAC Standards. 
John 0. Agwunobl, M.D., M.B.A. 

Sewetary 

Page 3 of 27 Laborurory Scope a f Accreditation 

'I'lilS LISTING OF ACCKEBI'I'ED AKAI,YrI'%S SilOULD BE IISEi) ONLY WREN 

ASSOCIATED WITH A VAIJlD Cft:RTSFICAI'E 

State t,ahorntory 112: Eg7689 EPA 1,nb Catic: MOO0054 (314) 298-8566 

E87689 

ST1, St. Louis 

13715 Hider Trl~il North 

Earth City, MU 63045 --- -- .-, ...-- Matrix: P&h-~otuble ~a;: 

Certification 

A~iaiyic Category Effective Date -. i\icthod/fecl~ .--- --- -----. 'fy pe 

1 .I ,I ,2~l'clracl1lometh~ne~~' EPA X260 Volalilo Orgoairs NELAP 7/1/2003 

1.1, t-l'richloroerhcnc EPA 624 Voli~lilc Organics NELAP 

NELAP 

NELAP 

NPLAP 

NEIAP 

KEtAP 

NELAP 

NELAP 

NELAP 

NEI.AP 

NRLAI' 

NELAI' 

NEL.AP 

NELAP 

NBLAP 

NEWP 

NELAP 

NELAP 

NEMP 

NCLAP 

NE1.AP 

NEiAP 

NELAP 

NELAP 

NElAP 

NELAP 

NEL.AP 

NEL.Al' 

NEIAP 

NELAI' 

NE1,AP 

NKIAf' 

NELAP 

NEI,AJ' 

IriELAl' 

EYA 8260 Volatilc Organics 

%PA 624 Volatile 0rg:toir; 

EPA 8260 

EI'A (34 

EPA 82W 

Volutilc Or@nics 

Volrtilc Or~~nics 

Volalilc Orgunis 

EPA 624 Vo)iirilc Organics 

EPA 8260 Voltttilc Orgmics 

EPA 624 

EPA 82M 

EPA 82U 

&PA 8260 

BPA 8269 

Volnlile Organics 

Volotile Organics 

Volatile Organics 

Volatile Ol.p:ilr~ii.: 

Volatile Or~~tnics 

FPA 8270 Exmloti~hle Orsanks 

FPA 625 Exlnclrhlc Orgiinks 

1,2,4-Trlblorohenzcnc EPA 8260 

1.2.4-'rrichlorobtrr~cnc EPA 8270 

1,2,4-'ltirncl~ylba1rcne 13PA 8260 

1,2-Dibron1o-.lcl~loro~p;me (IINCP) EPA 82M 

I ,2-Dibrona&me (EDB. EUtylcne dibronridc) E17A X2W 

VoL~tilc Orgmicu 

Extractable Organics 

Voliatilc Organics 

Volrrlilc Organics 

Vota~ilu Organiw 

EPA 624 Volntilc <)1~1iics 

EPA 625 Extrachblc Orpnics 

EPA 8260 Volatile Oganics 

1.iI'A 624 Volatile Oryiuaics 

Bf'A 8260 Volatilc Organiu: 

FJ'A 024 

EPA 8260 

EPA R2W 

Valnlile Organics 

Volatib Orgiulic~ 

Vohitilc Orgiaria 

EPh 8270 Extmclal~le Orgctnks 

BPA 8330 t.;xtnctable Orgainies 

EPA 624 Volntile Organics 

EPA (i25 Extnciubic Organics 

EPA 82Cfi Volatile 0rga11ia 

EPA 81(i0 Volalib <>rgitics 

EPA 8330 lix~dcfabk f)rga~lts 

"SrA'I'E" indicntcs ccrtificetiun for tbe anulytc by the method spccificd. "NE:L.AP" further NON-TRANSFERABLE 1111 3/2003-E87B89 

irldicatcr certificafian co~~~pfiant with tl~e N'EIAC Strndxrds. 
Jeb Bust* 

Govetrir~r 

John 0. Agwunobi. M.D., M.B.A. 

Secretary 

'FXIlS LIS'I'INC; Cli; ACCREDlTED ANAL,YTES SrIOUI,L) I%E tlSED ONLY WI.III:N 

ASSOC:ItII'EU W11'II A VALID CERTIFICA'1'P 

Shtc Laboratoty lD: E87689 PI'A 1,nb Code: MOO0054 (3 14) 298-8566 

E87689 

ST], St. Louis 

13715 Rider 'Frail North 

E~rth City, MO 63045 

- ,.-...---* ,--,...-.,.-.*--- ---. klntrix: Noa-Putablc {qiier 

Certification Analytc IilclhcdiTeeh Category - Effective Date --,- --A- Type -- 

I ,4-Uichlorohenxeoc EPA 624 Volatile Orgutlics NELAI' 2?13Q(302 

1 -4-Mclilorobcw,mr: EPA 625 ~~t(tblc Dr@i~kics NELAP 2'13/2002 

1,4-uicl1lor~~vrne II'A X2fd Volatile Orga~iics NELAP 7/li2M)3 

1 -4-l)ioxnnc (I -4- Diclhyicneoxidc) EPA 8260 

I$-Naphthoquincmc EPA 1270 

I-Nsphlhyla~tiiae EPA 8270 

2.2-DicLlor~y1ro~xu1~ EPA 82CXJ 

2,3,4,6-Tc1mchltmphcnol EPA 8270 

2.4,s-T EYA 8151 

2..l,b-'likhloroF)1cnol EI'A 625 

2.4.6~likl~lompttmn1~l El'h 80.41 

3.4 h-Triehloroptitnol BPA 82711 

?.A:.(,-Trinilrutolun,~ (2.4.5-TN1') BPA 8330 

':..l.D fiPA 8151 

: : .::-l)D Sil'A 8151 

Volatilc Orgnt~ics NELAP 7/1/2003 

Extractable Organics NEMP 711I2003 

Erlm~trhlc Organics N ELAP 7/ 112003 

Volutile Orpin is Nl!I.AP 7/1/2003 

Exl~ctubla Organics NElAl' 7/1/2003 

P~'cslicid~-fIerhic~t:~-i*CI3's NE1.AP 7/ I DUO3 

t'.xtnctabIcOt.g&~ics NELAP 2113/M02 

Extnslablc Orgu~ics N BLAP 71 112003 

Bx~mc~ibl~~. Orgitnics NE1.AP 71 l/UW3 

ExLri~clilhle Or@cnics NKLAP 7/1/2003 

1'cslicidc.s-llrrt,icidrs-f'CH's NELAP 7/1/20;)3 

Paticidcs-I.I~ulricidcs-PCR's NGSP 7/ 1/200! 

EPA fit5 Exlnatablc Orgafiics NUAP 211 3i2002 

BPA 8270 Extrucci~hle Organics NHLAt' 7/1L?OU3 

EPA 625 Estnctak)lc Orgilnics NE1.AP 2/ 13!2002 

BYA 804 1 tJxtmctJ1)lc Orgmlics NELAl' 7/1 J2003 

El'A 8270 Uxhclabtc Orgai~ics NBLAP 7/ 1j2003 

EPA 625 Extnffit;thtc Orga~~ics NELAP U13/2002 

EPA 8041 ktritablc Organics NEIAP 7/1/2003 

BPA 8270 hlrac~ahlc Orpmks 

).:PA 625 Fxtsxtablc Orgntricr 

EPA 8270 Extnctablc Oi-g:ut~?s 

NEIAP 7/1/2W)I 

NBLAP 2/ 13/2002 

NCLAP 1/ 112003 

EPA S330 ~r~~tiihlc Organics NELAP 71 112003 

EI'A 8270 Exlrd~lahle Orp~lics NELAP 71112tW3 

BPI\ 625 Exk~~cinhlc Organics NELAP 2! 13/W02 

EPA 8270 Exlr&c~ablc Orgi~~iics NILAP 7/ li2003 

EPA 8330 Exiractohlc Orgimitx NGI-AP 71 117,003 

2-An~iturf,6~lmilrotnlucne(2-~1n~~tnt) EPA 8330 

2-A~i~intunU~raquinone EPA K2 70 

Z-Bu(ant)nc (Methyl cUiyl kulorw, MEK) EPA 8260 

2-CJ~londhyl vinyl dli~r 

2-Clilortu~hyi vinyl dllcr 

2-Cirlorunapt1tl1aknt: 

EPA 624 

EPA X2(* 

BPA 625 

Exirucliible Organrs NEI..Af' 7/1/2003 

Bxtmcfahle Organics NELAY 7/1/2003 

Volalilc Oryitnics N14:I,AP 711i2W3 

"STATE" indicntcs ccrtilicrtiun fur the analytc by thc n~cthod spccificd. "NELAP" further NON-TKANSFERAHLE f l/lW003-E8768~l 

inrlicalt% ccrlificxtino co~iil)liant with the NE1,AC StandariL!. 
Jeb Bosh 

Governor 

John 0. Agwunobi, M.O., M.B.A. 

Secreiery 

Laboratory Scope of Accreditation Page 5 of 27 

State Laboratory 11): ~8768') EPA lab Code: MOO0054 (314) 298-8566 

E87689 

Sl't St. Louis 

13715 Rider Trail Norflt 

Eurtll City, &I0 63045 

----- ------A - - -- - .-. - ---- hlatrix: Non-Pobhlc Watcr 

Cerf Zfication 

Analyte Methodmcch Category Ty PC tilkctivc Dale 

--+-. --*--- - 2-Chlnronopti~knc El'A 8270 Pxtr-tablc Org~IItcs NEL.AP 7/ IR003 

2Chloropl1enol EPA b25 Exf~ilcIabl~ Orgmirs NEIAP 21 13/2002 

2.Chlornpl1n101 EPA 804 1 Extmclnhlc Orpirs NE1.AI' 7/1/2003 

EPA 8270 

EPA 8260 

ISPA 1260 

Et'A 625 

EPA 8270 

EI'A A270 

EPA 625 

EPA 804 1 

Et'A 8270 

EPA 83.30 

EPA 8270 

EPA 625 

PA 8270 

EI'A 8270 

EPA 8270 

CPA 8270 

BPA 8270 

EPA 8270 

Et'A 83.70 

EPA 148 

EPA 8081 

EPA 608 

Extnctd~lc Orgnnics NELAP 7/ 112003 

Voli41e Orgai~ics NELAP 7/1/2003 

Vcrlt~lilc Organics NBLAP 7/1TU)03 

Extn~tabic Chganks NBLAP 211 3/2M)2 

Extmublc ihganic% 'NELAP 7/ 1 1203 

Extwbbic Organics 

Fhmtahlc <)rpiiics 

ExtritebleOrgar~ics 

Fxtruc~nbic Organics 

Extmli~hlc &giu>ics 

NELAP 

NEWP 

NEt,hP 

NELAP 

NELAP 

NELAI' 

NBLAP 

NELAP 

N ELAP 

NBI..AP 7/1:2003 

NEI-AI' 71112003 

NBLAP 7/11200.7 

N6LAP 711R003 

NELAP 711 12003 

4,4'-~0e EPA 808 I I'eslicides-Hcrbicidcs-PC:Es NELAP 7/1/2003 

4.4'-DDT EPA 608 Pcslici(ies-lIcrbicidcs.PC[?t's NBLAP 2/ 1312002 

4,4'-DD'i' EI'A 8081 Pcslicirtes-l Icrhicitlc~-PCB's NELAP 7/ 112003 

4-Aminu-2,kIi11itmtoiucr1c(4-i1n1-drit) EPA 8330 Ex~n~clahle Orgi~nics NCLAP 7/1/2003 

4-Aininohiph~?1yl EPA 8270 Pxlr~ckthlc Organics NELAP 7/1/2003 

4-Bmnwphcnyl phcngl CUIN 

4-Chluro-3-mcthyiphcnul 

4-Ctilori~-3-nr[hylpJ~r1lol 

4-Ch lore-3 -IIICI~IY I~IIcI-K>! 

4-Cttlonutniline 

4Cl1lorr1phcnyl phcnylcthcr 

BPA 625 Exlraclable Organics NElhP 211 312002 

EPA 625 Exlnclabic: Orgii~ics NEI,A!' PI 312002 

EPh 8041 Ex(mcfitblc Orgi~llks NCLAP 71 1 U0(M 

BPA 8270 Cxlrnciahlc Orgiknbs NELAP 7/ it2003 

EPA 8270 Ex~ctahlt! O~&.~~II~CS NBLAP 7/1/2U03 

EPA 625 Exlr&lublc Orgntaics NELAP 2J13R02 

"STATE" iodicates certification for the analytc hy the nrctl~od spccificd "NELi\l'" furtlicr NIIN-1'MNSF~RA13L.t;: 1 1/13/2003-E87680 

indicates cerl'tficalion centpliant with the IVELAC Standartis. 
Jub Hntct~ 

Govorrtor 

John 0. Agwunobi, M.0:. M.B.A. 

Secretary 

Page 6 of 27 

'I'HIS LISTING OF ACCREI)ITFL) ANALY'I'ES STIOUI,FI BE USED ONLY WHEN 

ASSOCIA'f'ED \IVITR A VALID CERTIFICATE 

Statc L~borntury If): E$7689 EPA Lab Code: b1000054 (314) 298-8566 

E87689 

STL St. Luuis 

t3715 Rider Trail North 

Earth City, MO 63045 

Anulyte Met hodn'cch Category ---------- 

4-Chlorophcnyf plunylclher EPA 8270 kxrmlahlc Orgimicl: 

4Xitlorc~toLolucr~e EPA 8260 Votatile Orgnnics 

4-DiitsLyl ~rnincw.i1bu,7.~wc EPA 870 E~tmclilhlc Org;lnie< 

EPA 8260 

EPA 870 

EPA 8270 

Volatilc Orgcrnia 

Elctwbblc Organics 

Extmclablc Organics 

Cerlificalio~~ , , 

ype.-- NGLAP 

NELAI' 

NELAY 

NEIAP 

NEI-AP 

NELAP 

NELAP 

NELAP 

Effective Dale 

7/1/2003 

7i11203 

7/l/2003 

711 12003 

7/1L?003 

7/11UX)3 

UIX'2002 

7/ll2003 

4-Nitrotoluene EPA 8330 Fi~lrd~ti~hl~ Orgtai>ks NELAP 7/1/2003 

7.12-Dimctlry lhctv.(n) anthri~ctmc BPA 8270 Exuru;tnhlc Orga~rics NEIAP 7/1/2003 

Aciylositrile 

Acryluiiitritc 

Aldrin 

Aldrin 

Alk~lii~ity PS CaC03 

UPA 8270 

BPA 625 

El'A 8270 

EPA S310 

EPA 425 

ExmCoble Orgilriics 

Extractable Orgitnics 

Extwlnble Organics 

Exwirnhlc: Orgdnics 

ExtriK'tvhic Organics 

N6IAl' 7/ 112603 

NBLAP Z!l3l2ciD2 

NELAP ;/I12003 

NElhl' 7/1/2003 

NELAP 21 1112w2 

t3PA 8270 Extnchbie Organics NEIAP 711/2003 

El'A $3 10 Eximctllble 0rgariic.s NELAP 711 /ZOO3 

EPA 8260 Volalilr Orgitnics 

EPA b2hO Volntilu Orgitfiic?; 

EVA 8270 Extnrctlbic 01 pnics 

EPA 624 Volnulc Organics 

EPA 8260 Volatile Orgiinir~ 

NELAP 711 12003 

NfiLAP 7/1/2003 

NEl.I\P 71 l /XI03 

NEKAP 2/13/2002 

NELAP 7/112003 

EPA 624 

CPA 11260 

EPA 608 

Volatile Organics N ELAP 2/13/2002 

Volatilc Organics NfiLAP 71IiUHf3 

I'cslicides-Hwbicidczi-Pt?D's NBLAP 2113:2W2 

EPA 8081 Pccticidcs-Liabicidrts-PCD's N El-AI' 711i2003 

EPA 310.1 Gcnual C:hrn~isiiy NELAI' 2/13/2002 

Atlyl cl~loride (3~Chloropropctic) EPll 82-54 

nlpha-DH(: (f pha-~iexacI~brwy~loh~xane) EPA 608 

alpln-HiiC (alpha-Hcxnckbr~cyck)t1c~anc) EPA 1108 I 

Volatilc Organics N ElhP 71 112003 

P~slieidcs-flerbicide8-PCI1's NELAP 2?1312002 

Pcslicidrs-i lerhicidcs-PC:H1$ NELAP I/ 112003 

Alu~aittut~~ 

Alunimunl 

Alun~u~ut~r 

Alun~hum 

Anlitwnia RS N 

Aniline 

EPA 200.7 General C'hemisiry,lrlvlalt. NELAP 21 1312002 

EPh 200.8 Metals NELAP 2t1312002 

EPA 60 10 Metals NELAP 71li2W3 

€PA 6020 hlc?nls NELAP 7/ 1 /2003 

BPA 350.1 tienml Cllcrt~istry NELAP 211312002 

EPA 8270 Exxtractsbb Organrs NELAP 7i1ncwj 

"SrA'1'1.:" indicates certification fur the ana1y-t~ t~y the method specified 'tNEI.AP" further NON-TRANSFERABLE 1 111 3L?00D-t!768L) 

indicates certification coruplinnt witti ttrc F;&:I,AC Standards, 
Jeb Bush 

Oovemor 

John 0. Agwunobl. M.O., M.B.A. 

Sewetary 

Lahoraicjty Scope of Accrcdilnfiort Page 7 of 27 

THIS LkSTlNG OF ACCREDITEII ANALYTES SI.IUUI..I) HE USED ONI,Y WHEN 

ASSOC'IKL'EI) WITH A VAI.,ID CER'I'IPICATE 

State Laborntory ID: E87689 EPA Lab Cude: MOO0054 (314) 29&8566 

W689 

STL St Louis 

13715 Rider Trait North 

Earth City, MO 63045 .----- --.-. -- 

Matfir: Non-Potable Water 

CcrtificatIon 

Analyte MethodfI'ech Cittqury 'Typc Effective Date -....---- ---.,--- -- --- 

hthicme EPA 625 'x vacluhle Orgsc~ics NELAP 2/134002 

Mhracarc EPA 8270 Extmc1al)lc Organics NELAf' 7lli2003 

AnUwacmc EPA 8310 F~rmlnhle Organic% NELAP ~IILWO~ 

Arockrr-1248 (PCB-1 248) 

Aroclor-1254 (PCB- 1254) 

Aroclw-1254 (PCB-1 2.54) 

hbi-1260 (PCB-120) 

Amlor- 1260 (PCB-I 260) 

Arwnic 

Arsenic 

Anark 

Anmic 

Rarium 

Barium 

Barium 

Barium 

BPA 200.7 hl&ls NRLAP 2t1312002 

EPA 200.8 M&ls NEL.AP 2 1 312002 

EItA 6010 hldiiis NRLAP 71 11200.3 

&PA 60,020 M~*als NELAP 71 1 /ZOO3 

EPA 8270 htractishlc Organics NGMP 7/ 1 I203 

!.PA fiO8 

EPA 8082 

Pps~ieides-Hcrbicid~5-PCB's NELAP 211 312002 

Pcslieidcs-tlerhicitIw-13CB's h( f3i.At' 7/ 1 /2003 

Bt'A 608 Pcslicides-fJerbicidm-PCWs NEI-AP 211 3120112 

EI'A 8082 Fwticidrs-il&iCidcs-WfIs NEihP 711 12003 

EPA 6OX Prsticids-l+cr\licidcs-PLPLfYs NELAP 21 1312(!02 

EPA 8082 Pcsticdw-fierbi~ici~-rCB's NEl.AP 7/1!2OO? 

EPA 608 Psticidcs-Iicrbicides-IiiiH'd NClAP 21 312002 

EI'A $082 Pcjticitlc~-1ierhicid~-PC13's lu'E.LAP 7; l l200.1 

EPA 608 I'esticklcs-ficrhicid~s.PCBs NELhP 211 312002 

EPA 8082 Pwticidc?;-Hcrl)iCidcs-IY:B~ NELAP 7/1/2003 

EM GO8 Pcsticidcs-1Icrbiciclcs-PCB's NEL.AP 2/13/2002 

El'A 8082 Peslicides-llerhicidcs-PCB's NEI.AP 7/ 1/2003 

EPA GOR Y~~ici~s-I.lcrbicid~-PCB's NELAP 21 13rZO02 

EPA 8082 P~ticides-Hcrl~icidcs-I'C~t3~~ NELAP 7/11U)03 

EPA 200.7 

EPA 200.8 

EPA 60 10 

FPA 6020 

EPA 200.7 

Cicw~mt Cl~anistry,Mdals NELAP U 1 3120(12 

hicbk NEIhf' U1312002 

hlclais NEtnP 7i1/2003 

Metals NBIAY 1/1/2003 

Meiufs NEl.AP 2/1312002 

EPA 200.8 Mals 

EPA 6010 Metals 

BPA 6020 McUIS 

NELAP 2/13iZO(12 

NELAP 7/ 11201 

NELAP 7/112003 

EPA 624 Volulilc Organics NELAP 21 1312002 

EPA 802 1 Vnlaiilc: Orgatiics NELAP 7/1/2003 

EPA 8264 Volti~jia Orj&~nics NELAP 7/ 1 t2W3 

BPA 625 ExIT,x!IBI~Ic 0rga11ics NELAY 2/ 13t2W2 

BPA f 270 Sx~raclithle Orgaiiics NELAP 7/iRUO3 

EPA 625 Gxiraclrhio (frgulics NELAP 21 3 312002 

"STATE" indicates certifintion fur the anolytc by the method specified. "NEI,AY" furthcr NON-TRANSFERAl3i.E I I/l3/203-E87689 

indicates certification comjdiant with thc NELAC Standnrds. 
John 0. Agwvnobl, M.Q., IW.8.A. 

Secretary 

Laboratory Sccrye of Accretlitntiort Page 8 of 27 

'I'lIlS LISTING OF ACCREDITED ANAI,Y'l'tc:S SHOULD BE USED ONLY WHE;h' 

ASSOCIATED Wl'X7I A VAI,IL) CERTIFICATE 

State Laboratory ID: E87689 El'A Lnb Code: MC)[jOOS4 (314) 298-8566 

687689 

STL St. Louis 

13715 Hider Trail North 

Earth CiB, MO 63045 ----4-.--.-- ---...,.,..---- --,- 

Afatrix: Non-YotabL Water 

Ccrtificnf ion 

-- 

Analgte RiIcH~odTTech Cntqory Effcctivc Unte ---, - -.-..,, --- - ,-- --..---- Type -"--.- - Uenro(a)anthracale Et'A 8270 Exinctable Organics NELAP 7/ I ROO3 

13enim(a)Hntl~r;tcu1e 

Uenz@a)py~e~lc 

Hen;ro(a)pyrme 

Raiw(a)pyrenc: 

I3mxdb)Buc~r3ntho1c 

Hc~/a(b)flucinnLa~c 

Bmza(b)fIuomllrme 

Un~ro(g,h.i)pcxyIc~~c 

B~nzo(y b,i)lrrylcnc 

I+a~iofy ,ir.i)pcryle~ic 

. I?rnzc~k)fluc~rn~hcl~u 

Hutz~~k)fluorun~Ii~~c 

'tionzo(k)lluo~anll~uie 

tknzoic acid 

Bcnzyl alcohol 

13crylliuni 

I)M).lliuln 

Lkryllium 

brylliucn 

~IP-BIiC: (h~,~ir-f.lesi~~hl~~ycIol~rn~mc) 

hr!-BHC (hctn-H~xochio~n~cIoIi~~a~ic) 

bcl;l-Niph%~ykcait~e 

Dmcllnirical oxygen dennl~d 

bis(2-Clrlomc~~oxy)11idI1il~it: 

bis(2Chloroeihoxy)mctl1~nc 

bis(2-Chloroerhyl) elhw 

his(2-Chlon~uhyl) c&n 

his(2-Chl~r~bi~>pt<~pyl) dhcr 

bis(2C1rlon~hopropyl) L%~IL? 

his(2-Bthylh~x~l) ptilhnlstc (DEHP) 

his(2-Erbylhcxyl) phUlulrttc (DEI.LP) 

Boron 

&>run 

Bromide 

FJroniuicir 

EPA 8310 

EPA 625 

EPA 8270 

EPA 8310 

EPA 625 

EPA 8270 

EPA 8310 

E1"A 625 

EPA X270 

EPA 8310 

EPA 625 

EI'A 8270 

FI'A 8310 

EPA 8270 

EPA 8270 

EPA 200.7 

EPA 30.8 

EllA 6010 

&PA 6020 

EPA 608 

BPA 11081 

CI'A 8270 

EI'A 405.1 

EPA 625 

EPA 8271) 

PFA 625 

EPA 1270 

EPA 625 

CPA 8270 

EPA 625 

EBA 8270 

EYA 200.7 

EQA 6010 

EPA 30lj.1) 

EPA 9056 

GxWict;ihlc Organics 

f:,xtractublc Org~bics 

Extrdctithlc Org&t1ics 

F.ztr&tahle Orgnics 

Ext~cLablc Or~arrics 

Ext~ctoblc Orgaoics 

Extrnctablc Oryarrics 

Exitactable Organic% 

Extmctublr Organics 

I;,xtmcwhlr; 0rgaitic.s 

Extractable Oga~rics 

Extmctablc Organics 

htmctsble Orgnnics 

Exirirclithle 0rg;inics 

F-xlrac~ol>lc. C)rganics 

Gm~ml Cl~r~lislq~,Metrrls 

MEI~IS 

Met~ls 

Meals 

PcsiGdes-Hc&icida-PC13's 

Pcslicidcs.HchicicIw-I'<:H'b: 

Gttmctahlc Organics 

Oenrnl Chrt~dstry 

Ex~m~sbla O-anics 

ExtriiLuhlc Orsariics 

Ex~n~~uhlc Orpnics 

Extne1ill)lc Urga~ies 

Extmlnhlc Organics 

Extmctitblc Orwnics 

Extreclablc Orgmics 

Extmieblc Organics 

hlf%?b 

Mats 

Cicnml I:licn~islry 

Gcoaal Clicmislry 

"STATE" incticates cerfificaiion for the anaiptc by tlte methud spcelfied. "HEI,AY" firrtllcr 

indicntcs ccrtificalinn compliant with thc NELAC Stanciards. 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

NELAP 

Nt:,I..AP 

NEIAIx 

NBthY 

NELAP 

NELAP 

NI;l.AP 

NELAP 

NELAP 

NELAP 

NIiIAP 

NL!L.AP 

NELAP 

NELAP 

NPLAP 

NELAY 

NliLAt' 

NELAI' 

NELAP 

NELAP 

NEL.AP 

NEIAP 

NE1.AP 

NELAP 

NELAP 

NEl AP 

NElAP 
Jeb Bush 

Governor 

John 0. Agwunobi. M.D., M.B,A. 

Secretary 

Labornto y Scope of'Accredit~cfio~~ Page 9 of 27 

THIS 'I,.tS'I'ING OF ACCREDITED ANALYT.KS SIIOULD RE USEU ONLY WtlEN 

ASSOCIATED WIT11 A VALID CEWIFICATE 

State Luboratoq 10: E87689 EPA Lalt Code: h1000054 (3 14) 298-8566 

E87689 

STL St. Lollis 

13715 Rider Trail Nortl~ 

Earth C:ity, MO 63045 -,*---- ---- - ---- - ,..----. 

Matrix: Nan-Potable Water 

Certliicatittn 

Analpte 

-.-. filethod~eeli Cntcgory Type Effective Datc --.*.-, --,-.---- Bronmlm~mrc BPA 8260 Volalilc Organics NELAP 7/1/2003 

Hromochlomntcthanc EPA 8260 Volatile Orgalu~ NELAP 11 112003 

Cadmium 

Cadmium 

Chcisintl oxygeo dailarid 

Chlonl;cne (tech.) 

Chlordune (~wh.) 

Chloridc 

Chloridc 

EPA 624 Volatilc Orgat~ics 

EPA 8260 Volofile Organics' 

EPA 624 \'ohiilr? Organics 

NEIAP UI 3!2002 

NELAP 711 C2003 

NELAP 21 312002 

EPA 821U 

EPA 625 

Et'A 8270 

Vokilc Orpnia NELAP 71 112003 

Ektracloblc Organis NBLAP 2/ 130002 

Bxtmtablc Orgr~tMs NEl.AP 7JIi2UC3 

EQA 200.7 Gci~crel Ckrcn~islry.Metuls NSLAt' 2/13/2002 

EPA 200.8 h,leUl~ NELAP U 1 312W2 

'EPA 60 10 Metals 

EPA 6020 Mt.t;lls 

NELAP 7/ 1 12003 

HALAP 7jl :?O(i:r 

EI'A .200.7 

'EPA 60 10 

EPA 6020 

EPA 8270 

EPA 8260 

Generill Chcmistry,Mdals NEl,l\l' 2 '1 ?,';3i12 

Metals NEL.t\P 711 !2011:\ 

Metals Nf LAI' 1 t: :#'21?i).: 

E~hc~ahlr. Orgmics NElAP iili200; 

Volelilc: Ogunici NEI.AP 'li ! i20t)3 

EPA 624 Volatitc Orp~~ics 

EPA 8260 Volatile Orgatrics 

NELAP i+ l3.!2lX,2 

NElAP 7/ l i2003 

Et'A 4 10.4 

EI'A 608 

El'A 8081 

EPA 300.0 

EPA 90% 

G~neril Chcmistty NCL4P 2i 1 312002 

Padcidcs-Herhicitfzs-IYyH's NELAP ?/ 1312002 

Pmlicidcs-H~hicidw-PCB\ NEI.AP 7/ 1 /BUS 

Uencnl Cl~nnislry NELAP 24 38002 

Cjenmf C)~ni~islly NEMP 711 it003 

CPA 621 Vulalilc Organics: 

EPA 8260 Voluiile Orgimics 

EPA 624 Volo~ilc Organics 

Bt'A 8260 Yolatilo Orgi~nics 

EPA 624 Volatile Drganib 

EPA 8241 \lolntiIc Otg~llia 

El'A 8260 Volnlilc Organics 

CPA 2W.7 Mchls 

El'A 200.8 

EPA MI0 

EPA GO20 

NELI~P 2113R002 

NELAP 7/ 1 12003 

NCLAP 211 312002 

Nl'.f..AP 711 i2003 

NELAP 211 332002 

NEIAP 7/1/2003 

NK1,AP 7/1/2003 

NElAI' 2~1312002 

"STATE" indicates ccrtificafion for the anrlgtc by tlic mcthod specifietl. "NELAP" fi~rthcr NON-'I'RANSFEIbiBLE i ill 32003-fiS76X9 

indicates certification curnplirnt with the NELAC Standards. 
John 0. Afiwunobt, M.D., M.~.A. 

Secretary 

deb Hutst? 

Governor 

Laboratory Scope of Accrcditafinn Page 10 of 27 

I'ILIS LTSTfNC; OF ACCREDITED ANALYTES SIIOULD RE USED ONI,Y WHEN 

ASSOCIATED WITH A VALJII CKKTIFECA'I'E 

State In: E87689 EPA Lab Code: MOO0054 (314) 29&8566 

E87689 

STL St. Louis 

13715 Rider Trail North 

Earth City, MO 63045 --.-- ---.- - ---- ----- - - - -- ----- -- -- -. --- 

hlatrix: Non-Potable Water 

Certification 

Ancllyte hlethodfi'ech Category 'I'ypc Effective Date ---.,,--- 

Chrysmt? EI'A 625 ExLrucl;thlc Orpanics NELAP 211 312002 

cis- i ,2-L)ichlo1od1ylolo 

cis- 1,3-Dic11loropropc11c 

cis- l,3-i~icl1lompropc11c 

cis- t ,l-Did1Ioro.2-hutcnc 

C~lhiil t 

Cfibult 

Cohlr 

Coball 

Contluclivily 

Condudibity 

O*rk7 

Cupper 

I>ichlorodifli~omt~irl~iane 

Dic~~It~rnpml, (lkchlorprop) 

Wddrin 

-' I>ieldriii 

Dictliyl tti~cr 

I>icthyI pli~haki~c 

EPA X270 Exiraclal~lc Orga~lics NELAP 71 1 /ZOO3 

El'A 83 10 Exlrxtnhlc Organics NEL.AP 7/1/2003 

EPA 8260 

EPA 624 

EPA 8260 

EYA 82W 

EPA 200.7 

11l'A 200.8 

EPA 60 10 

EPA 6020 

'EI'A 120.1 

EI'A 4050 

EPA 200.7 

EPA 200.8 

Volatilc Organics 

Volatile Orgailici 

Volatile Orydnics 

Voixtilc Organics 

hielill$ 

Mcwls 

hlelals 

Mctals 

Genrmt Chcniislry 

Oenrril Ch~w~islr). 

Gcclual Chn~lislry,l\ldals 

Mcbls 

NLLAI' 

NELAP 

NEIAP 

NEIAP 

NELAP 

NELAP 

NELAP 

l46LAP 

NELAP 

MELAP 

NEL.AI' 

Nl3.Al' 

EPA 60 10 ~IC~~IS NELAI' 7~112003 

EM GOB Mt9ls NELM' 7/1/2003 

EPn 9040 Gaa~mi Chcn~isey NCLAP 7/1/2003 

EPA 8151 P~ticid~s~Hcrbicides-PCWs NELAY 7llf2003 

EPA 608 ~'esticida-lierbici~i~~-1'(:t~s NE1.AP Z/13/ZW2 

EPA 808 1 Prsticicl~.s-tlerbir:ii1cs-I'~'H's NELAI' 7/3/2003 

EI'A 8270 E~tmlUhll: Orfiit~lics NELAP 7/1/2003 

MA 625 

EPA 8270 

EI'A 8310 

EPA 624 Volalilc Orgianics 

EPA 82M) Volalilc 0rgmiics 

NCLAP 211 3R002 

Nl!LAP 7/ 112003 

NEI.AP 7/1/2003 

Volatile 0rg:mics NELAP 7/112003 

Volitiilt. Organics NE1-AP 7/112003 

Pcs~icirlc+Hchiciites-PC B's NELhP 7/1/2003 

EI'A 8264 Voltltilc Orpaics NELAP 7/1/2003 

Bl'A 8151 Ywticidrs-Hcrhici[tcs-PCD's NDLAP 7/1/2003 

tl'A GO8 Pesiicidcs-Hchicidm-PCB's NELAP 21 512002 

EF'A 8081 P~~li~id~s-Hcrbicid~s-I'CD(~ NELAP 71 1 /2MM 

EPA 82fiO Vc~lniilc Orguni~x NELAP 7/1/2003 

EPA 625 bmrc~blc Orgailks KELAP 211 3.0002 

"STATE" indicntcs eerlification for the analyte hy thc nicthod spccificd. "NE;I,AP1' h~rthcr NON-TRANSFERABLE 1 111 3/2003-E87089 

indicates ccrtificatiun compliant with thc NELAC Standl~rds. 
John 0. Agwunobi, M.D., M.8.A. 

Secretary 

Jsb FJIJSII 

Goverrrczr 

Laboratory Scope Ilf~ccreditafio~z Page 11 of 27 

TZIIS LIS'I'INC OF ACZKEDITED ANALWES SHOtJfJD BE USED ONLY WHEN 

ASSOCEATED WITH A VALID CERTIFICATE 

State Laboralory ID: EST689 EI'A tab Code: MOO0054 (314) 298-8566 

E87681) 

SW, St. 1,uuis 

13715 Rider Trail North 

Earth Cify, hIO 63045 

Matrix: NosPotable Water 

Certifieatio~t 

Aualyfe hlcthod/'Fcch Category I'ype Effective Datc LSd.",,. -..-.,- --- - 

Didhyl phlhakrte EIIA 8270 Extractable Organics NCLAI' 7/ll2(M3 

Din~cf ryl pt~tlmbtc 

Diinahyl phll&k 

Ui-11-bulyl phlhalnlc 

Di-81-lwtyl phthalntc 

Di-n.octyt phtlishte 

EI'A 625 Exhctablc Organics 

EPA 8270 Eshactable Organics 

EPA 625 Exi~~~h~c Organics 

EPA 8270 Extmctahlc OT~~ES 

EPA 625 Extraolabic Organics 

NI:'iAP UL3n002 

NELAP 7/112003 

NfStAP 2/13t20(12 

NHAP 7llRO03 

NELAP 2/13/2002 

Di-n-cctyl phlhabto BPA 8270 

Dinuseb (2~~-hutyl-4,6-clini~pt1~.10I~ DNUP) EPA 8151 

iUsulFotoct BPA 8270 

Exiracroblo Organics NELAP 7/112003 

Pcsticidcs-l.Ictbicides-f'C:H's NELAP 7lIR003 

Bxmctablc Orgsnics NELAP 7Il/aUO.1 

EI'A 608 Pcsticitlrs-Hcrbicid--PCB's NEI.AP 21 1312002 

EPA 809 I Pwticitks-licmicidm-PCB's NEl AP 7lli2003 

EPA 608 

EPA 8081 

EI'A 608 

ETJh "hHOSl 

EPh fiOX 

EPA (1081 

EPA 608 

P~ticid~~-t~ahicid~~-i'CI3'~ NELAP 211 3RW2 

Pcsticidccl4~d)icides- PCX's MCLAP 71 112003 

Pesticides-1fcri:icidoj-PCB's NE1,AI' 2t13i2002 

Pcstici~les-l.#c&icida-PCD's Wf?Laf' 5/112003 

I'e~ticides-Hcrbicidm-PCBs NELAP 2 1312002 

I'csticidm-Hdicidcs-PCIYs NELAP 7/1/2003 

Pcs~icidn-ltehidda-I'CISs NCLAf' 21 13/2002 

F,PA 80x1 P-iicidcs-IIcrl~iciclitles-1'CDh' NfilAl' 7/1/2003 

EPA 8260 Voiitti le Organics NE1.AP 711 12003 

EPA 82.60 Vniasill: Drjyt~ics 

EPA 624 Voliltilc Org.mics 

Ef'A 8021 Volntilc Organics 

NElAP 711 1200.3 

NBLAP 2t131~002 

NELAP 71 1/2003 

Et'A 8260 

6PA 8270 

EPA 625 

EPA 8270 

EPA 83 10 

Vojatile Orgrnics NELA1' 71 1t2W5 

Extrdctabtc Orgarnics NELAP 7/1/2003 

Extractable Orgu~k~ NELAP 2!1312002 

Fxtructnbtc Organics NEUP 71 112003 

Eslrachbic Organics NELAP 7/1/2003 

EPA 625 

EPA 8270 

EPA X3i0 

SPA 300.0 

Et'A 905G 

!:PA 608 

Ex~mciabkc Orgttlics 

Exmtnblc Organics 

Exmmmbic Organics 

(>cuml Ctiai~islv 

Gcnm>l Cliatiistry 

Pcsticidcs-tiehicidcs-PCYH's 

NELAP 

NEIAP 

NELAP 

NELAP 

NBLAP 

NELAP 

I'luoridc 

Fluoride 

gasurn-01 IC: (Li~ld;ioe, 

ganim~l~lmact~lc~rwyc~I~~hexane) 

gsmrm-BHC (Lindanc, 

g;inu~u-Hexaclilnr~~ycInl~cxanc) 

Grt>ssidplta 

EPA $081 

NELAP 

"SI'ATE" indicate ccrlificafion for the analytc by thc mcthod specified. "NEl>AY" further NON-TRANSFBRARLfr 1 111 3/2M)3-EX7689 

intlicrtes ccrtificntion ccnwpliant with tht NELAC Standards. 
Jcrb Bush 

Oovemor 

John 0. Agwunobi, M.D., M.B.A. 

Secrelery 

Laboratory Scope ~j~ccreditorina Paw12 of 27 

TIUS L,ISTING OF ACCREDITED ANAI,Y1'ES SI3OULD BE tISEL1 ONLY WlIEN 

ASSOCIATED W1.'Ml A VALID CERTIl:1CAI'E 

Slate Laboratory 11): E87689 EPA lab Code: MOO0054 (314) 298-8566 

E87689 

STL St Louis 

13715 Rider Trail North 

Earth City, MO 63045 

---- . ----.-..-,. --.- .- 

Matrix: Non-Potable Water 

Certificatirbn 

AnaIytc Methodn'ech C~teg01-y Trpc Effective Date -------- --dm-- .-" 

GroP-bch RPA 900 Kadioche~i~htq NELAP 211 312002 

EPA 130.2 

EPA 608 

EPA SO81 

Gwcnil Chemistry NELAP 2/13iXW)2 

Pesticid~?i-Hcrbicidcs-PCB's NELAP 211 3/2002 

Pesticides-Hcrbicids-PCU's NELAP 711i2003 

EPA 608 Pcslicida-Hehicid~uc-PCIA N ELAP 211 312002 

EPA 808 1 Pcsticidm-lidicides-PCB'\ NCLAY 71 112003 

EPA 625 Exinctrble Orgilnct. NELAl' 2/13/2002 

KIsA R270 Extnrt~blc Orgmlrcs Nt?IAP 7/1!2003 

EPA 625 Extractable Q~gu~ies NlilAI' 21138002 

EPA 82M Voletilc Organics NELAP 7/1/2003 

EPA 8270 Exlrwtahlc 01g.znics NELAP 7f 112003 

EPA 625 ExtractuMe C)rgitnios NELAP 31312002 

Et'A 8270 Extraciiib,bie Oyarric:,. NELA P 7/1/2003 

EPA 625 Exlr~ctablc Orpc~ics NEt.AP 2/13/2002 

EPA 82W Volagle Orgaxri~x NE1,AP 7/ 112003 

BPA 8210 Extactablo Orgiinics NGLAP 78'1 /2003 

EVA 8270 E.~lmcBbIc C)qanics NEL.AP 7/ 1!2003 

EPA $270 l~nln~bble Orranies NEUP 7/ 1 R00.3 

EVA 1010 Cmcnhl Ctrmei~lry 

EPA 625 Exlnctoblc Orgarhics 

EPA 8270 Extnctablc Organics 

EVA 8310 Exbiitahlu Orpnics 

EPA 200.7 Metals 

h EPA 6010 

Imn EPA 6020 

lsobutyi alcohol (2-Methyl-l -pruparu)l) BPA 8260 

NELAP 7/1/2003 

N ELAP 1 l #ROD3 

NPLAP 7/1/2W3 

EPA 8270 Extrnctablc Organics NPLAP 7/lfZ(H)3 

EPA 625 Extractable Orgnnica NELAP 2/13/2(H12 

EPA 8260 Volatilc Orp~aicj 

EPA 8270 Bxtmcfahlc Orgdnmicb 

EPA 8270 Extmctable Orpnks 

NBLAP 7/1/2003 

NELAP 7/1/2003 

NEI.AP 71'1i2003 

EPA 200.7 

BI'A 200.8 

E1'A 60 10 

Nlr'LAP 7/1m~03 

NCLAP 7lli200.1 

"STATE" indicntcs certilication for thc snslytc by the rncthod specified. "NELAP" furthcr NON-TfUNSFFKAl3l.E I l/lU2fH)3-iX7GB 

indicates ccrfificatisn campliant with tbc NEI,A<: Standards. 
John 0. Agwunobi, M.D., M.B.A. 

Secretary 

Laboratory Scope of Accrcditafio~r Page 13 of 27 

THIS LISTING OF ACCRE:I)ITED ANAI,Y'I'ES SIlOULD BE IISEI) ONi,Y WHKN 

ASSOCIATED iYITll A VALID UER'I'LVJCA'l'E 

Stetc Laboratory 11): Kg7689 EPA Lab Codc: MOO0054 (334) 298-8566 

ES7689 

Sl't St. Louis 

13715 Rider TraiI Norfh 

Earth City, MO 63045 -.-- . - .,.- .- ---,,--, -.. -.-- 

hfatrix: Nun-Potrablc Water 

Certification 

Anaiyte McthodlTcch Cntcgor). Typ~ Kffeclivc Date ---- - - .- ,--- ..- .-.---.- -- 

hlapcsium EPA 200.7 C;cnml Cho11irslry,h4~1s NELAP 2/13/2002 

hiagncsiu~a EI'A 200.8 hleli~is NELAI' 24 13/2002 

Magncsiu~lr EPA 6010 Mct;~ls NELAP 7/132003 

EI'A 6020 htc~11~ NE1,AP 1 1/7/2005 

EPA 200.7 Citn~mI Chetnistr).,Metais NELAP 21 1312002 

EPh 200.8 Mculls NELAP 2/ t 3i2002 

EPA 6010 hlchls NEtAP 71 f i2W3 

EPA 6028 Mctuls NELAP 71 112003 

EPA 8151 Pesticide-Herhicicles-PCD's NELAP 71 112003 

EPA 8151 Cmticidti-Hmhicidcs-I'C:H'S NEX.AP 7/1/2003 

El'A 245.1 h4elitlc NElAP 211 3/2002 

EPA 7470 hicL1LIs NFJAP 7/1/2003 

EPA 82W Volatilc Organics NDLAP 7/1/2003 

EPA 8270 

EPA 624 

EM 8261) 

IIPA 624 

EPA 8260 

hlctl~ytndl,acryla(e EPA 8260 

Mclllyi pwdthic~n (ParaUtio~r, nlethyl) LPA 8270 

McUlyl lcrf-hulyl cthm (hl7'DE) EPA $260 

bfclhy lcne cllloride El'A 624 

Melttylalc cl~bridc ]'!PA 8260 

n-Bulyl ulcolial 

r~-Burylbcnzenc 

Nickel 

Extrxlablc Or$ankk NEIhP 7/ Li2003 

Vnlatilc Organics NBlAP 2/I J12W2 

Vok~lilc Orgiulics NB1,AI' 71f 12003 

Volutilc Orgunirri NEI..AP 2/ i3/2002 

Volatile Orgattics NEIhP 71 112003 

EFA 200.7 Mclak 

EPA 200.8 hlslnls 

CPA 6010 hlcbls 

EPA 8260 VoL~iik Organin: 

EPA 625 Ertractnblc Organics 

NElhP 711120Q3 

NELAP 71 I RW3 

NELAP 71lI2W3 

NEl.AB 2/13,0002 

NELAI' 711i2003 

NELnP 211 312002 

NEI,AP 2/13/2002 

NELAP 71112003 

NELAY 71 ~noo 

NCLAP 21 1312002 

EPA 11260 Volalilc Or&ini~?i NELAP 7/ti2003 

EPA 8270 Extraarhle Orguttics NELAP 71 1/20(33 

&PA 8310 Est~ctabte Organics NELAP 7/ 1 DO03 

EPA 8260 Volatifc Organics NELAP 7/ It2003 

PPA 8260 Volali)c NELAP 711 12003 

EPA 200.7 Cie~~cni Chemietry,Mclals NGUP 211 3!2002 

"STATE" bdicotes certifiertion for the aaalyte by the nlcthoti specified. "NEI,AP" f~rrfhrr NON-TRANSFE.RAI3I.E 1111312003-887689 

indieatcs certification contplia~tt witb thc NEf,AC Standards. 
Jet2 Bush 

Governor 

John 0. Agwunobi, M.D., M.B.A. 

Secretary 

Luborafory Scope of Accre~litatio~t Page 14 of 27 

THIS I,ISTINCI OF ACCREIII'I'ED ANALY'I'ES SHOULD DF: tlSElf ONI,Y WHEN 

ASSOCIA'l'I!!D WITH A VALID CERTIFICATE 

Slate I~boratory 11): E87689 EPA Lab Cude: It1000054 (314) 298-8566 

F27689 

STL St. Louis 

13715 Itider Trail Nortli 

Earth City, MU 63045 .---,----- .-<-- 

Alatrix: Nun-l'otablc Water 

Certification 

Anslytc Mcthodn'ccfi Category Type Effecfivc Date -,-,.--------.------ ---- 

Nickel EPA 200.8 Wdats NELAP 2/13RO(f2 

Nickel EPA 6OiO hlmls NELAP 71 112003 

Nickcl EPA 6020 Metals NELAP 7/1/2003 

Nimte CPA 90SG Gencnl Cliemislry NBLAP I/ 11203 

hlitnte as N WA 300.0 Gcnea~l C:ticmirctry NELAP 21 1332002 

Nirmu as N H=A 353.1 Gtslcml Cl~cnustry NEL,AP 2/ 1312002 

EI'A 300.9 Gmcnl Cl~crnistty KELAP 2113f2002 

WA 9056 Cicnernl Cl~cnristry NElhP I/ If2003 

EPA 300.0 (icrrcml Chcti~istty NELAP U13/202 

EPA 354.1 Ciencml Chuii~istry NELAP 211 3Ra02 

BI'A 625 Er~rdc~ctahlc Orx.mics NELAP 21 13/2002 

EPA 8270 Cxlractabb Orgiulics NBLAP 71 1 /2003 

EPA 83-30 Exlnctabtc Orpanics N ELAI1 71 1/2003 

EPA 8270 

EPA 625 

Et'A 8270 

EPA 8270 

EPA 625 

Iixtmcrablc Organics NELAP 7/1!ZO03 

Extn~tablc Organics NCLAP 211 312002 

ExmctrbfcOrgmics NELAY 71' 11 2003 

BxwL.lbb Organics KEI.AP 71 ll'2.003 

Ifx~n~ctabtc Orgi~nics NP.lAP 21 3/2U02 

BPA 625 ExtnriabIc Organics NELAP 2/13/20(12 

fiI'A 8270 Ex~racttbke Organics NELAP 711003 

f!I'A 8270 

EPA 8270 

EPA 8270 

r-Nitiasopyrmiidinc EPA 8270 

~il~~upyhawtc EPA 8260 

OctahyOrn-1,3,S,7-tdnmitm-L,3,S,7-tc~rzoci1~~ BPA 8330 

(HMX) 

Oil gL Cirm..~ EPA 16M 

Oil gL Cicca..~ 

Oil & Cirase 

EPA 413.1 

EPA 9070 

EPA 300.0 Cctlcrdl C:h~iaisiry 

EM '3056 Gcnc'rdl Cl~crnistry 

EPA 8260 Volittilc Orprmes 

NELAP 71 112003 

NEI-AP 711 I2003 

NEIAI' 7/1/2003 

NE1.AP 711 12003 

NE1,AP 7/1/2003 

NELAP 7/1/2003 

NELAP 711 12003 

NELhP Z1312002 

NELAP U1312002 

NPLAP 71 1 I203 

NCLAP 2~13R002 

NELAP 71 1 I2003 

NELAP 71112003 

Ef'A 8270 Exrr.cccahie Organics NELAP 71112003 

EPA 82M Vvtatilc 0rg:inia NCLAP 7/1/2003 

EPA 8270 F:x(rirliihlc Orgi~niou NPLAP ~~IIZOO~ 

"STATE" inrlicatcs ccrfification fur thc analyte by tt~c motbad sltccified. "NEI,AP" furtl~cr NON-eI'KANSPEKAUtE t llI3/2003-E8761(9 

indicates ccrtificstiun cun~pIinat with the NE1,AC: Shntlards. 
John 0; Agwunabi, M.D., M.B.A. 

Secretary 

Jeb Bush 

Owemor 

Labora to1 y Scope qf Acc~vditatior~ Page 15 of 27 

THIS LISTING OF ACCREDITED ANALYTES Sl.IOUIdD BE USED ONLY WHEN 

ASSOCIATED WIT11 A VALlf) ClFR1'IFICA'I'E 

State Laboratory ID: E87689 EPA I.eb Codc: h100UU54 (314) 298-8566 

IT87689 

STL St Louis 

13715 Rider l'raii North 

hrth City, MO 63045 ,.-"--- --,----. 

Mmtrh Non-Potable Water 

C.'crtificntioe 

hl* MethocllTech Category 511~ Effective i)ate ---.---,---,- 

Partrrblmba~zcne EI'A 8270 Exlr,tclnblc Organics NEi,AP 7/ 1 f2003 

kntachluroecham EPA X260 Volalile Organics NBLAI' 7/lf.?UO3 

..Pheml 

Phcnd 

Phmltc 

Phoqhm, total 

15ckmrn 

phpmpyttoIu~mc 

hlassiwn 

Potassium 

Potas!si~~~l 

-(Kert?> 

Rupionilrilc @thy1 cyanide) 

P-Xylm 

'9- 

Pyrmc 

PytaKI 

Pyridine 

~iumZ26 

RDX (hcxabydro-1~~-irinitro-l3,S-&i11c) 

Rcsiduc-fiftaabk (TDS) 

Residue-nmfilimbtc (TSS) 

ElbA 8270 Exmloblc Organics NELAI' 711;21)03 

EPA 625 Extnctablc Organics NELAP UlUWO2 

EPA 804 1 

CPA 8151 

EPA 8270 

BI'A 150.1 

EIBA W0 

EPA 8270 

EPA 625 

EPA 8270 

&PA 83 10 

: F.Ph 625 

Hxtmcl&lc Or&;mic~ NEf .AP 71 l i203 

Pesticides-I lcrbici~1~~-1~CIf's NELAP 7/1/2003 

Ex~mck~blc Organics NELAP 71 1 12003 

Gcnncn~l Che~nislq NELAY 24 3.LM2 

(im~cn~l Chm~istry NELAP 711 t200.3 

Extmtablc Orgmics r\ZEiAP 7:li2W3 

E~it~~t~hlc O~~~II~CS NELAP 2~13i2002 

F~lmctidhlc Organics NELAP 7/1 i2IIO3 

F.x~ruct&le Organics NCLAP 7:1/2C03 

Exlrxtablc Orgaricr NE1,AP ?.!I :Diik\2 

EPA. 804 1 Ertncta1)lc Organics NEUB 711/2W)3 

EPA 8270 Extmttablc Orgitnis NISLAP 7!1 /?LXii 

EPA 8270 Extsi~table Organics NELAP 7! I tZC'03 

EPA 365.1 GCTIWI C~IC~~S~N NL3.AP 2/ i 3!202 

EM Rt51 Pcsticidcs-Habicidm-I'CtYs NELAP 7/ 1/2(M3 

CPA 8260 Voiatite Organics NELAP 71 1 /ZOO3 

EPA 200.7 ~cfa~s KELAP unno(12 

EPA GO10 Metills NEIAP 71 1 12003 

EPA 6020 Mruls NELAP 1 li-112003 

EPA 8270 Bxlnctsblc Clrganics NBIAI' 7/112003 

EPA R2M) Volalilc Oqa~rics NELAP 7/ 1 /ZOO3 

EPA 8260 Volatilc Organi~ NEMP 7/ll20W 

BPA 625 

EPA 8270 

EVA 8310 

fiPA 8270 

Bt'A 903 

EPA 8330 

EI'A 160. I 

EPA 160.2 

EPA 160.5 Genw~l Cl~emisiry 

EPA 160.3 Cm~cnd C:hemistry 

NELAP 

NELAP 

NELAP 

NPLAP 

NELAP 

NELAP 

NELAP 

N CLAP 

NELAP 2/13/2002 

NCLAP 2/132002 

"STATE" indicates ccrtifk~cation for the anaiyte by the method sprcificd. "NELAP" fr~rther NON-TRANSFERABLE I 1113/2003-EX7689 

indicates cerlificatioa romplbnt with the NELAC Stand;~rds. 
John 0. Agwurmbi, M.D., M.B.A. 

Secrelary 

THIS I.,l'S?'ING OF ACCREDITED ANN,YTES SkIOULI) BE IISED ONLY WHEN 

ASSOCIATED WIrI.'H A VAI,II) CERl'IPICA?'E 

State I.aborntrrry ID: E87689 EPA Lab Code: hmOoO.% (314) 298-8566 

E87689 

STL St. 1.auis 

13715 Hider Trail Nurth 

Earth Ciiy, MO 63045 ----,....,.,---- "-,- 

I\.Iatrix: NU~-Potahf~ Water 

C:crtificatinn 

A~~nlpte Clctegory Effective Date -. ----.-----.-.----.--..-.-- Mctt~odn'ech -a ..,. Type 

Safmb EVA 8270 Exlrnctnl~lc Urgniiics NElhP 7z2.003 

se-ButyIbenxnc EPA 8260 Volndie Organics NELAP 7/1/2003 

Scicoium EllA 200.7 kfeuls .NELAP 2113/2002 

Scle~~iutn EPA 200 8 Mctals NBLAP 211 RRM12 

Seienium EPA 60 LO hlelals NELAP 7/I/MD3 

.%lcniu~a 

Silicon 

Silic011 

Silvcr 

Silv~~ 

Silvcr 

Silvur 

,Silvex (2A.S-TP) 

Sutlium 

Cidium 

SoJiut~~ 

Sko~itiurn 

WA 6020 

EPA 200.7 

EM <@I0 

iS1'A 200.7 

EPA 200.8 

NCLAF l lt7i2003 

NELAP 211 32002 

NBLAI' 7/l/2W3 

NElAP 2/13RU02 

NELAP 211 3QlM2 

Ef'A GO I0 Metals NBI,AP 71' ;2rM3 

EPA 6020 Mcwls NClhP 711 121303 

EPA 8151 P~~doido;-HL71~iCidc~-P~~B's Nlil AP 7/1/2003 

ElaA 200.7 Metals NELAP 2il3 2092 

EPA 6010 hlctils NBLAP 7/1tf00.! 

EPA 6020 Melals NEUP I Lt7M)03 

BPA 6010 hlcllrls NELAI' 7) l iUK)j 

EPA 82(# Vabtilc Orga~ics NEL-AI' 7/1/2003 

BPA 300.0 Cicne~al Cl~emistry N EUP 2/13/2002 

EPA 9056 Geneml C:hcn~istry NELAP 71 11200; 

BPA 376.1 Gcneml C:hcnristv NELhY 21 13/2(302 

EPA 8270 I'mticid~s-H~rtricides-PCDDs NELAP 7/1/Ui03 

tcrt-Butylba~~,rrw EPA 82W 

'l'rtmchturoehylecle (l'achlomclhylcne) EPA 624 

't'~ncl~loroelhylc~t (I'~ch1orocrhylwic) EPA 82W 

l'aryl (n1nhyl-2$,6-trini1mpl~ny Inilnm~ine) EPA 8330 

Tliulliu~s EPA 200.7 

EPA 200.1 

EPA 60 LO 

EPA 6020 

Et'A 8270 

EPA 6010 

Vrdatilc Orgiuiic-s 

Volntilc Organics 

Vofatilc Orgiioics 

f?xtracl,?hit: Organics 

Mc~als 

NELAP 7i112W3 

NELAP ?/I 3,Q1)132 

NEUP 711~m3 

NELM 71 112003 

NELAP 31 312002 

h?c.c3ls NEI-AP 24 3!2(N2 

Mculs NELAP 711i2w 

hlcbls NCLAIJ 7/1i2003 

I'es~i~ii~l;li-H~~hi~id~~~P~IB's NELAP 1/1/2003 

hlehls NEIAY 71lf2UOS 

EPA 624 Volatilc Organics 

EPA 8021 Vcrlnulc Orgmics 

EPA 8260 Volalilc Orgimics 

NCLAP 31 3R002 

NEiAP 7/ 112003 

NCLAP 7/1/2003 

Total cyanide EPA 335.2 Gencn~l Chctriislty NCL.AP 21 13/2002 

"Ij'l'Kf'E:" indicate cerfiOeation for the analyte by thr mctbod spccificd. "h'E1,AP" further NON-'i'KANSFERAI3L1E 1 1/13/2OU3-E87689 

intlicatcs ccrtllicrrtion cotuplbnt wlth the NELAC Standards. 
deb Bush 

Governor 

John 0, Agwunobi, M.D., M.B.A. 

Secretary 

Page 17 of 27 

TIiIS LISTING OF ACCREDI'rED ANALY'I'PS SI.IOULD BE USED ONLY WIIEN 

ASSOClATED WITII A VliLID CERTIFICATE 

State Lnhmtory ID: B?iiS9 El'A Lab Code: h-fCH10054 (314) 298-8561 

E87689 

STL St. Louis 

13715 Rider Trail North 

Earth City, MO 63045 --..------,----. ------------ ---,--.--,-.---. Matrix: Noli-Potable Water 

Certification 

Analytc Riethodn'ech Caiegov Type Efkctivc Date -.. - Tntai cpnidc EPA W10 Gcnml Chclnislry NELAP 711 12003 

7fotal cyanide EPA IM 12 Gwml Chal~islry NELAP 7/10W3 

Told ziiUatc~tiitritc EPA 300.0 Gct)crul Clwmhlr). NElAP 2/13120(32 

'Fotal nitratc-nilritc 

?'otal organic mtwn 

Totel organic carkn~ 

Toti11 organic t~~liiles (T0X) 

Tolal phenolics 

9056 

EPA 415.1 

OVA 9060 

[:'PA YO20 Gcnml Ct~crsustry 

EPA 420.2 Gcnml Chtn~istry 

'Tomi pl~cnoitics EI'A W&6 

'rototn~ sulfid~ EPA 9034 

'I'oxaphFnc (Chlorisat~xl mtxipbcnc) CPA 608 

NELAP 1/1/2003 

NELAP 5/14/2003 

'NELAI' 7/112003 

NELAP 7/1/2003 

NELAP 2!13m2 

Cieneml C:limnislry NRLAP 1/1/2003 

Cicneral Chumistry NCLAP 7/111.003 

Palicidcs-Hc+ricidca-PCB's NDLAP 2! 1 3Q002 

Toxopt.me (Chlorinalctl ca~.anlph(mc) EI'A 8081 Pesticides-tlabicidw-I'Ces NEI-At' 7!1120R? 

tt'sl&-i.Z-Dicl~lor~~~hyIwe EPA 624 Volatile 01.ganim NElAB 2/ 1313002 

Irm- l3-Diclilor0clhpl~i~ EPA 8260 

tmns-l.3-l~ichloro~nu~~y1~11c EPA 624 

~s-l,3-Dichloropropylaic EPA 8260 

Irans-l,4-F~icliIo~-2-br~t~ne EVA 826U 

T~idilomt~hcnc (liichk,mclhyten@ EPA 624 

Trichlamctticnc (Trichlorocliiylcmc) EPA 8260 

l'ncltlomfiuorol~ifllianc EPA 624 

V~nudium 

Vinyl uceta(c 

Vinyl dll~xidc 

Vinyl chkrridc 

Xylc11c (lcllul) 

Xylcnt. (told) 

Xylmtc (lulnl) 

Zinc 

Zinc 

Zinc 

Zinc 

Volutilc Oqpnics 

Voiatilc Orgartics 

Vohti lc Orgattiw 

Volatile Organic-$ 

Voli~tile Org;miu 

\'o!i~rilo Organics 

Votalilc Orgnrtic~ 

NPLAP 71112003 

NELAP 211 ~Q~WZ 

NBI,A F 731i2003 

KELAI' 7! IR003 

NELAP 211 3RW2 

KELAP 7/1/2003 

KELAI' 12f16r202 

EPA 826U Vohiilc Organics NI?l-A P 7/lL!(M3 

EJaA 200.8 M&ls NF.LAP 211 312002 

EPA 200.7 Cieneril Chc~nia.rry,Mdnls NE1.AP 1/1312002 

EPA 200.8 Mclals NBLAP 211 3/20(32 

EM 6010 ~eca~s NELAP 71 1nw3 

EPA 6020 

EPA 82260 

il'A 624 

EPA 8260 

EI'A 624 

EPA 8021 

Ef'A 8260 

EPA 200.7 

Mclals 

Volatile Organits 

Volatilc Orga~iics 

Volatilc Organics 

Volalile Org;i~~im 

NfiLAY I llfi2003 

NEI-AP 71 i 0003 

NELAI' u 1~m2 

NE1.At' 71 IRW3 

NELAI' 2t132Qil2 

Volatile O~ganics NElAP 7/1/2003 

Volatilc Organics NELAP 711n03 

Cic~irnl Che~nistry,.Mclals NELAP 2/13/2002 

"STATE" indiratcs certification for the nnalytc by the n~cthcd specified. "NEl,APW furtlacr NON-'I'KhNSFERABLB 1 llt3/2003-E87689 

indicntas ccrtification complimt with thc NELAC Stsndarlts. 
John 0. Agwunabi, M.D., M.B.A. 

Secretary 

Laboratory Scope of Accreditatiori Page 18 of 27 

TI11S I.ISVI'ING OF ACC:REDI'I'ED ANALY'TES SIlOULD BE USED ONLY WIIEN 

ASSOCIATED WITII A VALID CERTIFICATE 

Statc L.uhertitory ID: E87689 EQA I~ll Code: MOO0054 (314) 298-8566 

E87689 

STL St i..ouis 

13715 Hidcr Trttif North 

Earth City, MO 63045 -,------.--..--,.---- Matrix: Solid aud Ci~ernical Matcrirls 

Certification 

Analyte Mef hocVI'ech Cotegory Effective I'lrte .-- ?.-".---.---. - -.-- 'I'Ypc --- 

1,1,1,2-'~etmchIor0~~l1a1i~' EPA 8260 Voliktilc Orgilnirs NELAP 2/1 Y2002 

1.1 ,l -'frichloroethnc EPA 82GO Voln&lc Organics NPLAF 2/13/2002 

1,1,2,2~18tn~chlod1a11c t3PA 8260 Vohtilc Orgmics NELAP 21 I .3mO2 

1, I ,2-Trichlmcthme 6PA 8260 \'olalilc Ofgalin NELAP U 13M2 

1 ,I-nicbkbtoe(hicne EPA 82CQ Vnlatilc Orgtutics NELAP Zi1312002 

EPA 8260 

EPh 8260 

EPA 8260 

EPA 8200 

El'h 8270 

Ef'A 8269 

EPA 8270 

EPA $200 

I.lJ'A 8260 

FPA 82Cd 

VolatilcOrgai~ics 

Volatilc Organics 

Volatile Organics 

Vukl~ileO~i~i~ 

Exmiable Organics 

Volntilc Organics 

Ilxiractablc Organics 

\'oIatile Orp~nia 

Volntila Otgunia 

Volatile Orguii~r 

El'A 8260 Voktilc Orgmicx 

EPA 8260 Volatiic Orgiu~ics 

EPA 8260 

fiPA $260 

E13A 8270 

ElaA 8330 

PPA K2Cd) 

EPA 8260 

EPA 8330 

EPA 8260 

EQA R2Ca 

El'A 8270 

EPh 8270 

EPA 8260 

E.PA 8270 

Volulile Or#,anits 

Volirlilc Orgmics 

Exincioblc Orgru~ics 

Extrnctablc Organics 

Volatilc Organi~ 

Vohtilc Orl~ania 

Exuuclnhlc Organics 

Voliltilc Orxilics 

Vohtilc Organics 

Extractnl,lc Orgiuiics 

Extnlctable OFyallics 

Volatilc Organis 

Extr~tahlc Organics 

NELAP 

NEtnP 

NELAP 

NELAP 

NELAY 

NEI.AY 

NEIAP 

NEI-AP 

NELi,P 

NBL.AP 

NCLAF' 31 332002 

NCLAP 313i2002 

NELAP 5'1 30002 

NELAl' 21 1 32w2 

NELhP U 13!202 

NELAP 

NELAP 

NEUP 

NELAf' 

NRLAP 

NEL.AP 

NELAP 

NWAP 

2.4,s-T EPA B151 Peslicidw-kiabicicles-1'CB's NEL.AP 21 13/2002 

2.4,6=Trkl1lorcrpbonnl EPA 8041 Extr;&tiblc Organics NELAP 2/13/2002 

2.4,6-Trichlorophcnol EPA 8270 Cxtractablc Organics NBL.AP 2'1 332002 

2.4.6-Tri~cikolalua~c (2.4.6-TWJ EPA 8330 Exlrdctablc Organics hfELAP 21 1 3/2002 

2,4.0 CPA 8151 Pmticidcs-l.lc~icides-I'CH's NEMP 21 13R002 

2,4-DB EPA 8tSl Pesticiclcs-Iierhicidw-I'CH's NELAP 31 3QM2 

"Sl'ATK" indicates ccrtifieation for thc anrlylc by the ntelbod spccifiod. "NELAP" further NON-TRANSFBKAI3I.E I 111 3/2003-Fi?(i80 

indicater ccrtific~tion com~dinnt with the NELAC Standards. 
Jet) Rt~rrh 

Guvernor 

John 0. Agwunobi, M.D., M.B.A. 

secretary 

Lubnmfory Scope of~ccredifa fioa Page 19 of 27 

THIS I,IS?'INC OF ACCRII:UI?:ED ANA1,YI'ES SflOULD BE USED ONLY WIZKN 

ASSC)CIA'I'ED WITH A VALID CERTIFICATE 

Shte Laburntory If): E876g9 EPA 1,ab (:ode: hIOQO054 (314) 298-8566 

E87689 

STL St. 1,auis 

13715 Ridcr Trail Nortll 

Earth City, iVO 63045 --... -...-.-,---- hlatrix: Sotid and Cbcnticlrl Msterials 

Ccrlification 

Analyte 

---.- I\.idhod/l'ecli Cntcgory Effective Date 

.-...--------,------.-.---- Type .-..*.-.--- 

2,4-Dichloraplicnd EPA 8270 i:.strdctnhlc Ogtrnks NELAP 211 3i2W2 

EFA 804 1 

EL'A 8270 

EPA 8041 

EM 8210 

EPA 8270 

2.4-Diai1romtuene(2,4-I)NT) EPA K330 

2,b-Uichlnropltmd EPA 8270 

2,6-Dinit1otolucnc(2,6-DNT) EPA 8271) 

2P-DinitWolunie (2,6-I>KT) EM 8330 

2-Aniini)4,6dini1rotoluaic(2-a1ii-tb11) EPA 8330 

2-Aniiiicumtlinquinonc EPA 8270 

3-Dutiumiic (McUiyl c8yl ketc?lic, MEK) EPA 8260 

?-Clloructl~pl vinyl dhcr EPA 8260 

ZtChlontnaphlhabic EPA 8270 

2Clilc1rptimc4 BPA 8041 

FI~mrctahlc Orgirnics 

Extwti~hle Organics 

Exlrzeiublc Orp~ics 

Eslnvlublc Orpnklrrlcs 

Ex~toblc Organics 

Exlmctablc Organics 

fixtractable Organics 

Extniclable Orgiinics 

Extmctahlc Organics 

Fxlntelablc Orgnnks 

ktnclablc Organics 

Volatile Organics 

Volit(ik Organic% 

Exlrtlelablc Orgmiic1; 

hlnclablc Orgsliics 

EPA 8270 l3.inctablc Organics 

EPA 8260 Volatik: Organics 

EI'A 8260 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8041 

EI'A 8210 

FPA 8338 

EPA 8270 

Volatiie Organics 

Exlmtablc Orgnnics 

Dxlnctabl~ Orgaiks 

Cxtruciabia Orp,;~n;inics 

Extriiable Organics 

Exlrilablr: Organics 

Exln1cish2e Chgmics 

Ex1rucW)tc Org.wics 

EPA 8270 Ex1w1Rhlc Orgmics 

WA 8270 Extncrabic 00rp;mics 

EPA 8270 Ertracbblc Organics 

FPA 8270 E.xirrtctablc: Orgi~iiics 

E.PA 8270 Extmctablc Organics 

EPA 8270 Extmctablc Or,qunics 

EPA 8330 Cxttactablc Organics 

EYA 8081 Prsticides-s-liwhici~1c~-PCR's 

EPA XU81 I'cslicidcs-kb.bicides-1.~CH's 

EPA 808 I l'cslicidcs-llerhicides-PCH's 

"S'LVrC:'' indicates certification for the snalyte by the ~r~cthod spcctfred. "NELAYt' furthcr 

indicates certification compliant with tile NELAC Standards. 

NELAP 

NELAP 

NELAP 

NEI1,AP 

NELAP 

NE1.Afl 

NE1,AP 

NEl.AP 

KEUP 

Nk?LAI' 

NEIAI' 

NE1.b.P 

KBi.AP 

WCLAP 

NhiA12 

NEIAI' 

NEWP 

NCLAP 

NELAI' 

'NEIAI' 

NELAP 

NELAP 

NELAP 

NBLAP 

NElhP 

NEI-AP 

NElAP 

NEI,AP 

NELAP 

NF.LAJ1 

NELAP 

NEI-AP 

NEtAP 

NELAP 

NEf,At' 
John 0. Agwunabi, M.D., M.B.A. 

Secretary 

Lubrmxtory Scuye of Aucrt'dit~ctiu~z Page 20 of 27 

TILIS LISTING; OF ACCRKIII'I'ED ANALYTES SHOIfI.rL) 13K l~SH> ONLY WHEN 

ASSOCIA'I'EI) \VITIf A VA1,II) CXKl'l l2lCA'l'E 

State Laboratory ID: ER7h89 &PA Lab Code: M0000S4 (314) 298-8566 

E876R9 

STI, St. Louis 

13715 Hider Trail North 

Earth City, MO 63045 

- 

Mtltrix: Solid atui Clrerniral hlateriwls 

Crrtifrc~tion 

Analytc 

---.----.- MethodTTcch Category Type Effective Date 

4-A1~iino-2.Mi1riwtc,lurnc(4-em-dnt) BPA 8330 ---- ---- ---. ISxtrdctable 

--.---.----.-.-.+---.- Organanics ------,--..--.---------- NELAP ..,... -- 

51 14!2003 

4-Amu~obiphmyl EPA 8270 Sx~ncfable Organics Ntii.Ala 2/ 1312002 

4-Cl1loro-3-n1ctIiy1~tu1~1 EPA 804 1 RruacUrblc Organios NELAP 2/ 1312002 

4-Ch brib3-nict bylpliaiol 

4-Chloroanilinc 

4Chiony1h~nyl phcnyfcthcr 

4Chkrrcflolurmt: 

4-DialcIltyl osiintwoh~nn~.r(:e 

4-hlcthyl-2-pcntmric (MIHK) 

4-Mdliylphca~ol (pCrso1) 

4-Nitroaniline 

d-Nitroplten~t 

4-Nitrot~lucnc 

EPA 8270 

EPA 8270 

EPA 8270 

EPA 8260 

EPA 8270 

El'A 820 

El*A 8270 

EI'A 8270 

EPA $270 

EM 83W 

APA 8270 

EI'A 8270 

CPA L270 

EPA 8310 

F.PA 8270 

EX~rd~tabk Organics 

Extzrtuhlu Organics 

Exmtnhlc Organics 

Volatilc Organics 

Entmctable Organics 

Volatile Orga~~is 

Extractable Orpnicu 

Exlmtahlc Otgttnies 

Pxt~aztable t)rgatties 

Ewtmcti\t)lc Organics 

Extractiihlr Clrganics 

Extmeli~hlc Orgmics 

Extwclublc Organics 

Exlnctal~lc Oigiudcs 

Hslmtahfe Organics 

NELAP 

MEIAI' 

NBLAP 

NELAP 

NELAP 

NCLAP 

NE1-AI' 

NF,L.AP 

NELAP 

NELAP 

NEI.AP 

NHI.Al' 

NE1,AI1 

NELAP 

NDLAP 

EPA 8310 Ext~tctiibk Organics NELAI' 21 1 3Tr002 

EPA 8260 VolrlilcOrgani~s NRLAI' 2/13/2002 

EPA X2Mt 

EPA 8270 

EVA 8210 

Volu~ile Orgu~iits 

bimct;rble Organics 

Volatile Org~lics 

NEt.AP 2!13Q002 

NELAP 2/13f2002 

NELAP 2/13/2002 

Acrylonitrik EPA R2MI Volnli.le Organics NELAP 211 312002 

Aidrin EI'A 808 1 P&~icides-JlcrbiciOes-PC:H's NEL..AF 2/ 13/2002 

Ally1 chloride (3-Ctilorapropc11c) EPA S2M) Volatile Orgitnia NELAI' 2 1 3i2W2 

alpha-HI1C: (rtlplta-I~exacI~k~rffiycbf~cxa~ic) !.!PA 8081 Pcslicidas-Hc&:rbicidc;-J'CH's NELAP 33 3RW2 

nlun~inuti~ EPA 6010 Metals NELAP 2/13G!002 

EPA 6020 

EPA 8270 

BPA 8270 

Me(;ils NELAP 24 31202 

Dxtnclal~lc Clr&ac~ics NELAP 2t 131202 

Ex~ti111lc Orgatiics NELAP U1W2 

EPA 8310 Extmlilblc Org~l~cs NELAP 2:13i20~2 

EPA M) LO Mckls NELAP 2113it002 

EPA 6020 MCUIS NGLAP 211 3i2M2 

EPA 8270 Extraublc Orgulics NEL,AP 211 3i2002 

EPA 8082 Pmticidc~.It!rl~icid~-PCI3's NELAP 211 3/2002 

"S'l'ATE" indicates certification for (hc nnalytc I)y the method specified. "NELAP" h~rthcr NON-TRANSFERABLE 11/1312W3-W7h89 

indicates certificatio~l corn)bliant with tllc NEL.,AE: Sta~rdarBs, 
John 0. Agwunobi, M.D., M.B.A. 

Secretary 

Laboratory Scope if ~cereditation Page 21 of 27 

THIS I,ISIYNG OF ACCW,DITED ANALYTES SR0UL.D BE IJ'SED ON1,Y WHEfi 

ASSOCIATEII WJTIi A VALID CERTIFICATE 

State L~bornlary 1D: X876t)g EPA Lnb Codc: &20000% (314) 298-8566 

I387689 

STL St. Louis 

13715 Rider Trail North 

Earth City, MO 63065 ----. --".--- ----. Matrh: Solid and Chcmic~i Materiafs 

Certificatiou 

Anr ly te Mctbodn'cch Cutegory Type Effective Date 

Amclor- 1221 (PCB-1221) --" ,----.,- -,.-- PPA 11082 Pes~icides-He~ici~Ic~-I'C:l~'s 

-- 

NELAQ 211 3nU02 

- 

Arcclor-1232 (PCB-I 232) 

Ar~cIor-1242 (PCH-1242) 

A~o~lor-1248 (PCB- 1248) 

EM 8012 Pzsticidcs-Hcmicidw-JIC'R's 

EPA 8082 Pestsriciilcs-lichicidcs.l'CH's 

t!IIA 8082 Pcsticidcs-Herl>icirles-PCWs 

NE1-A!' 

KEI.A1' 

MElhP 

NELAP 

NELAP 

NEMP 

NELAf' 

NlsLAP 

NEUIJ 

NElAP 

NCLAP 

NI!I,AP 

NBLAI' 

NEL.AP 

NELAP 

NEWP 

NJ3.AI1 

NElAP 

NEl-AP 

NELAP 

NELAP 

KELAP 

NELAP 

NEI-AP 

NELAP 

NELAP 

NEUP 

NCLAP 

NELAJ' 

NELAP 

NELAI' 

FEIAP 

NE1,AI' 

NELAP 

NELAY 

Aroclor-1254 (PCB- 1254) 

Anxior-1 2b0 (PCB. 1260) 

Amic 

6PA 8082 

Ei'A 8082 

EPA 6010 

P~+cidwHerhiddcs-PCB's 

Psticidw-licrt~icidei-PCB's 

Mctals 

EPA 6020 Mctils 

EPA MI10 Mettti~ 

EVA 6020 

El'A 8021 

BPA 5260 

EPA 8270 

EPA 8270 

Molrcis 

Volntill: Organics 

Vutcltik: Organics 

EntractabtcOrganics 

Exmc~blc Organics 

EPA 8310 

EPA 8270 

Et'h 8310 

EPA 'A270 

BYA 8310 

Exlr~clablc Orgo~rks 

Exti-xlablc Organics 

Extractable 01-ganks 

fixtnctuhlc Orgnnks 

Extncublc Organics 

EPA 8270 Extnc~at~lc 0rwnic.s 

EPA 8310 htractablc Organics 

PPA 11270 F-wiictiible Organics 

CPA 8310 t.:xtwh~hlc Organics 

EPA 8270 Exlmclablc Organics 

EPA 8270 Cxlwcluhle Organics 

EtyA 6010 Mctals 

&ryl liuns 6Pn 6020 

hclr-BflC (heb-licxncI~~or~~yc~~~f~cx'~ne) EPA UORI 

bis(2CI1lorocti1oxy)1~sc(t11111~ EPA 8270 

Mctals 

Pnticides-tlc~bicidcs~f CWs 

Llxtwt;lblcOr~irics 

his(2-Chbnretbyl) cthcr EPA H270 

his(2Chlomiwproppl) dlrcr EPA a70 

his(2-E1ilylhcxyl) phtllalatc (DCliP) EPA 8270 

Extr&ti~blc Organics 

Extmt;ible Orgaoics 

Ewtri~ctithlc C)rp~nics 

EPA hOlO hlt?als 

EPA 90% Ga~cml C:~IC~IIS~I~ 

EPA 8260 Volatile Orgaaics 

EPA 8260 Volatile Orgimics 

"STATE" Indicates ccrtificnlion for the analytc by the methud specified. "NKLAP" furtbcr 

indicates certification comftliant with the NELAC Standards. 
John 0, Agwunubl, M.D., M.B.A. 

Secretary 

Laboratory Scope c$Accredifctfion Page 22 of 27 

'rHNS IAIS'flNC OF ACCREDITED ANAI.,YTES SIlOUIaD HE USED ONLY WHEN 

ASSOC:IA'FEJ) WK'TII A VA1..11) Ufi;R'J'IFICX'i'fi: 

Stm Laboratory ID: &8761)3 EPA Lab Code: MOO0054 (314) 298-8566 

E87689 

STL St. Louis 

13715 Rider 'f'rdl North 

Earth City, MO 63045 --. "*.. ------.--.------ Afntrix: Solid and Cl~en~ical Materials 

Certification 

Antliyte MethodTCech Category I'Y pe Effective Date -----.--+ -- --.-.. BromxticI~ioron~d~u~? EPA 82U Voletilc Organics NELAP 2/13/2002 

mlapm 

drlla-RILC 

Did liltc 

EPA 8270 ExtrachBlc Orga~lics 

EPA 6010 Metals 

tiPA 6020 

EDA 6010 

EI'A GO20 

BPA 8270 Hwimctahlc Orgmrics 

EPA 8260 Volatilc Organics 

EPA S2U Volatilr: Orgnics 

EPA 808 1 l'r~licittcs-l~lcrhici~I~'~-PC:t3's 

EPA W56 Genecrl Cirun~klry 

EPA 8260 Vola(ilc Orpt~ics 

1FA 820 Volittilc Orgaeirs 

EPA $269 

EPA R?Ci 

EPA 6010 

EPA 6020 

KI'A 7 t (9G 

Volatitc Organics 

Vtrk~tilc Organics 

h4~Anis 

hlclals 

Cenml Climbistry 

EI'A 8270 Exlrwlohlc Orgunics 

Ei3A 8310 Extnactshle Organics 

EPA 8260 Volb~ilc Orgoniw 

EPA 8260 Volatile Orgiinics 

CPA 8260 Volatile Organics 

EI'A 6010 

EPA (420 

EPA 3050 

EPh 60 10 h4wls 

EPA 6020 Mmls 

EPARISI 

EPA XOR l 

PPA 8270 

EPA 8270 ExlrdcUhlc Orpnics 

EPA 8310 klnsctnhic. Organics 

I)~~~OIIKIC~I~TUIII~INIC EPA 8264 Volslile Organics 

S)ihn~nu~fi~~omn~ctl~anc EPA 8260 Voletilc Ogintics 

NELAP 

NELAP 

NEtAP 

NCLAP 

NRtAP 

NELAP 

NEMP 

NELAP 

NELAP 

NE1.AP 

NEl AP 

NElAP 

NELAP 

NEL.AP 

NEtnt' 

NfXAlb 

NELAP 

NEUP 

NELAI1 

NELA1' 

NELAP 

NEthP 

NDI.AP 

NLLAP 

NELAP 

NEI-AP 

NE1.AI' 

NEI.AP 

NElAP 

NEIAI' 

NELAP 

NEI.A13 

NELAP 

NEIA t' 

NE1,AP 

"STATE" indicalcs ccrlification for the anafytc by Ihc ntethod specifird. "NGLAP" furlhcr 

ii~dicatcs certtlication compliant with lbc NEL.AC Stantlards. 
John 0. Agwnobi, M.D,, M.B.A. 

Secrelary 

Page 23 of 27 

THIS LISTING OF ACCREDI'FED ANALYYES S~fOtll,,I) BE USED Oh'1,Y WHEN 

ASSOCIATED WITI.1 A VA'I.ID C~EI<'I'~FlCA'l'E 

Stite Laboratory ID: ]E87689 OPA lab Code: iM00(1054 (31 4) 298-8566 

E87689 

Sl'f, St. Loois 

13725 Rider Trail North 

Parth City, MO 63045 

..-.-,...-- --.-...-,,-.--.---+-.- 

Matrix: Sofid ttrld CI~et~iical Rlateri~ls 

Ccrtification 

A~ritlytc h3etitodlTech Cntcgory 'I'ype Effective Date 

.-,- ,.,.,--.- -..-..---.---------...-----. l>hromomctha~~c EPA 8260 Volatilc Orgaliics NELAP 2j13/2002 

Di~mnbi~ HPA XI51 i'aticitlrs-l.liubicidcs-PCD's NELAP 2/13/UH)2 

Dichl~irdifluomn~~~mic EPA 82trO V<~lulile Oqat~ics NELAP 24 3/2(Mt 

Dichloroprop (Uicltlaq~mp) EPA 8151 Pi%ficidc$-,-i.i&icides-I'CU's NEUP 2/13/2002 

Dicldn-n EPA 8081 Pe~icidcs-tlirbicirics-)PCB's NELAP 2/13/2002 

Didhyl ethcr EPA 8260 Volnlllu Organics NEIAP 2/ 1 3/2002 

Oidtyl pltlhahlL. EI'A 8270 Exincbblc Or~ni~s NELAP 2 1 312002 

I)ilndhyl pl~thohtc EPA 8270 Ex~ractablc Organics NBLAP 21 3 3/2002 

Ili-11-butyl pittlwlott EPA 8270 lixtractabic 0rga;tics NELAP 2/13/2002 

Di-n-cxtyl phtbbte: PPA 8270 Extractable Orpnics NElAP 2/13/2002 

Uirusseh (2~~-b11lyI4,6-diftihu}~f1~11d, DNBP) BPA 8151 P&licidcs-1lerhicide~-M:H's Nt:.I.AP 211 3!2002 

1)isuiIiit~ EPA 8270 P~sticidc~-Herbicidc~-PCt3's NELAP 2/13/2002 

151dosull'ai I EPA 8081 Pczticidcs-Hcrhicidcs-PCWs NELAP 1! 131202 

!iitdosulfan 11 EPA 80x1 Pcsticidcs-f 3rrbicidcs-PCB's NELAP 2!l3.Q002 

Endisulfan wlfate EPA XOXI Paticida-i.terbici(tc.s-PCtf's NEI..AfB 2/1312002 

iindrin EM 8081 P-ticids-Hrrhici~lw-PC:H's NEUP 2/13f2002 

E~~drir akld~ydc l?PA 808) Pcsticidcs-H~rhicides-M3tYs NGLAP 21 13,rt(X)2 

F~hyl jccute 

Ethyl rncth;rcrylnte 

Ethylhenzerrc 

EUwlhcmmmr 

Lxlnctnblc nrganics hnlid~s (EOX) 

EPA 82ii 

EPA 8260 

EPA 8021 

IlI'A 8260 

EI'A 9023 

EI'A 8270 

EPA 8270 

EPA 8310 

EPA 8270 

EM 8310 

Slt'A 9056 

EI'A 808 1 

CPA 9310 

Vctlatilc Organis 

Volitlile Orglnics 

Volalile Organics 

Volalile Organics 

Gcttml Chaaistfy 

t'cslicidcs-flc~bicidcs-PC:Es 

Extnlcvahlc Organics 

Extnct,lhle Owitnics 

Extmtlahlc Orgunics 

Ex1n~L;thlc Orgiutics 

Gcnnnl Cbcmislry 

Pcsticidcs-f ItvBici<les-PCB's 

N ELAP 21 13iL002 

NEI-AP 21 13!2W2 

N EL4 I' 2/1 ,VL002 

NEIhP 211312002 

NDLAP 2f1312002 

EPA 93 111 Kadiochcrntilry KEI.AP 2/ 13~2002 

EI'A XU81 Pcsticida-H~rhi~id~"j-PCB's NELAf' S/21Lrt003 

EPA 808 1 i'c?iticid~-1~letbi~i~l~~-I'~IH's NELAP 21 3:2002 

LPA 8270 Ex(mciahle Or~anics NE1.AP 2/ 1 3.Q002 

EPA X2MI Vohlile Organics NEI.AP 2'132002 

EPA 8270 Extnrclahle Organics Nl?i,AtF 2113m02 

"STATE:" indicates ccrtificxIion for thc aaalytc by thc ~t~ofhnd specified. "NELAP" fitrthcr NON-TRANSI'EKAULE 11/13/2/2003-E87689 

iailic~tcs certification compliant with thc NELAC Stnitdardi. 
Job Buah 

Governor 

John 0. Agwunubi, M.D., M.B.A. 

Secretary 

Laboratory Scope ofA ccreditafian Page 24 of 27 

TfIlS IISTiNG OF ACCREDITED ANALYTES SIIOULD LIE USED ONLY WFiPN 

ASSOCIATED WiTIll A VALII) CERTIFICATE 

State Laboratory ID: Eg76g9 EPA Lab Cnde: k1000054 (314) 298-8566 

E87689 

STL St. IAOuis 

f 3715 Rider Trail North 

Earth City, MO 63045 --.- -----..---.-.- --,.--.- ..,., --. - -.---------.--, Mark: Sdid and Chemical Materials 

Certification 

Aaaiyte MethetilTech Category Type Effective Date 

fiacachblucyckqmfadime EPA 8270 Exlnshhtc NELAP 21 1 312002 

Orgnnbs,Pc.slicid~-HErhicic'ia-I'CB' 

$ 

Hcxacbtomethanc EFA 82ii Volatib Organics NELAP 2/ 13iKK)Z 

Bl'A 8270 Exlwk~ble Orgimifs 

EPA 8270 Exlruclablc Organics 

BPA to10 Ccncrsl Cherlbistry 

EPA 8270 Exmmctablo Orgmios 

EPA 8310 Bxtnclal)lc Clrgajtaics 

EPA 6610 Metals 

EPA a120 Mcuts 

isobutyl alcohol (2-Mclhyl-1 aop~mf) EPA 8260 

'~wtnn EPA 8270 

.~rysr,pylbcwma EPA 8260 

-rsasafrok Et'h 8270 

.irpmc EPA 8270 

Iwd 

icud 

Lithium 

klakMsjum 

Ma&nesirun 

Maw-= 

M~~ 

MCPA 

MCPP 

M-ry 

Melhrrylonilrils 

Mdhnpyrilenc 

Mahoxychlvr 

MeZhoxychlor 

Mdhyl h&e (Bwmon~cthznc) 

MrUlyl chloride (Chloromdbawc) 

Methyl ~Ihaqlatr: 

Methyl partllbion(Pa~aratbion. methyl) 

NELAfl 21 1 3/2002 

NEI.AP 211 3R002 

NEUP 2/ t 3/2W2 

NELAP 2J 1312002 

NELAP 2r13/2002 

Vohtilo Org~nics NELAY 2i13f2002 

Pcs~icidrs-tlcrhicidcs.PCB'r NELAP 21 3i2W2 

Voiatilc Organics NELhP 211 312002 

kIxtiactahlc Organics NO1,Ai' 2/ 13/?002 

I'csticicl~-Jierhici1te;5-l'CIYs NEUP 2/ 1 312002 

EPA 60 10 

BPA 6020 

EI'A 8151 

EI'A 8151 

EPA 7471 

NELAP 2JI312002 

NE1,AP 1 1/7/2003 

EPA 6010 hfctsls 

EPA 6020 Mclals 

BI'A 6010 kletals 

EPA 6010 ME~~~Is 

BPA 60% Mculs 

EPA R2(fi 

EPA R270 

BPA 8081 

EPA 8270 

EPA 82bO 

EPA 8260 

EPA 8260 

EPA 8270 

NRLAP 2/ 1 30002 

NELAP 2/ 13/20132 

NCLAP 21 t3/2002 

NELAP 21 1312002 

NEK.AP I I 17n0ir3 

Metals NELAP ' Z13.2002 

Mchis NELAP 2!13i2U02 

fbsticidcs-1lerhicidcs-PCB's NELAP 2113/7.(302 

Palicidrs-Ilerbicidcs-PCB's NELAP 24 31'2002 

Meuls NBLAP 2/13,Q002 

Mdhyl t&-butyl ethw (hl'rBB) EPA X2M) VolalilcOrgat~im 

Mdttytmc chloride EPA 8260 Volstilc Orp~iia 

NRUP 

NEI.Af1 

NEi.AP 

h'Ef.AP 

NElhP 

NELAP 

NELAP 

NElAP 

"STATE" indicata certification for the anulyte by the method spceified. "NE1,AP" furtl~cr NON-'I'UNSFERABLE I 1/13/20n3-fIR76R9 

indicates ccr4ification compliant with thc NELAC Standards. 
John Q. Agwunobi, M.D., M.B.A. 

Secretary 

Page 25 of 27 

THIS LIS'TING OF ACCRE1)ITIi:D ANALYTES SIIOULD RE IJSED ONL,Y WHEN 

ASSOCIATED \VI'I'fI A VAI..ID CERTIFICA'l'li: 

State tabomtory ID: Kg7689 ISPA I,rl~ Code: MOO0054 (314) 298-8566 

JB7689 

STL St. 1,oeis 

13715 Rider TraU North 

Earth City, MO 63045 -----. --.,. -.,-.- Matrix: ~olidarrd Chenlicol Materials 

Certification 

--7- 

Type Effective Date 

NELAP 12i9/2002 

III-Xylmc EPA 8260 Volalilc Otguii~s NELAP 

NELAP 

N EL..AP 

NEI..AY 

NEIAP 

NELAP 

NPMP 

NELAP 

I'ifi1,AP 

NKlAf' 

NELAP 

NELAP 

NBLAI' 

NEI,AIJ 

MELAI' 

NELAP 

NE.LAP 

NEIAP 

NELAP 

NEtAP 

HEUP 

NELAP 

NELAP 

Nnphlhnlem: 

Nopt~lltnkne 

Nnpltlhnknc 

n-Butyl almhtl 

n-U~~tylbcnzene 

Rich1 

Nickel 

Nitma 

Nitrile 

Nitnhxlrnis 

EPA 8260 

EPA 827b 

EPA 8310 

EPA 82MI 

EPA 8260 

EPA 6010 

EPA (a20 

CPA YO56 

EPA 9056 

El'A R270 

Voliitilc Orgartits 

Extractable Orgnrtics 

Extractable Orgnitics 

Valalitc Orgnnics 

Volalilc Ownivj 

Mctul6 

MciaIs 

Gcnerai Cltcz~tistry 

I.in~cnl Clicrnislr)' 

Extmctable Organics 

EPA R330 Bxlnrctnhlc Oty,wics 

EPA 8270 Eximc~oldo Orgunics 

EPA 8270 I:.xlractabb Qrgmics 

EI'A 8270 I:.xl~tclablr: Orgaoics 

n-Nitrosodifl~aiylilmine EPA 8270 Extnictable Organics 

EPA 8270 Ex!mcfnbIc Organics 

EPA 8270 Extr;tct:thlc Organics 

n-f'ropylbmzcnc BPA 8260 Volittilc Organics 

0,tr.o-Trielhyf t>l~~~pho#U~ioirt~ EPA 8270 Pcuticides-Hdicidcs-IWs 

Oil 8r Gmsc 

thihttphttsphatc as P 

EPA 9071 Gcrlml Chcnlistry 

CPA 9056 CiCrtcxnl Chcmislry 

NELAP 

NCUP 

NELAP 

N El hi' 

NE1,AY 

NEI.AP 

NELAP 

NEIAP 

NEIAP 

NEIAP 

NHIAI' 

NE[..AI' 

EPA X260 Voktilc Organics 

Ef'A 82.70 Extri~table Orgal~ics 

EPA 8260 Volatiic Orgwtim 

f3I1A 3095 Gei~cril Cltcmisby 

EIJA 8270 Pcsticidcs-1Crl)icides-PCB's 

Pailachlorohcn~me EPA 8270 Extractable Organics 

EI'A 82W Voli~lile Organia 

EI'A 8270 F-xtraclablu Orga~tics 

Pcn~icchlontphc~~ol EI'A 8041 Extractable Organics 

"STATE" indicfitcs rcrfiiication for itre analptc by fhc wetbod specified. "NE1,AP" f~trtlur 

indicates certification compliant crfth fhr NELAC Sfnntlards. 
John 0. Agwunobi, M.D., M.B.A. 

Sewetary 

Paw 26 of 27 

THIS LIS'I'INC OF ACCREl>l'i'E:D ANALYTES GTIOUL,D UE IISED ONLY WHEN 

ASSOCIATED WIT11 A VAUI) CERTIFICA'I'E 

Stntc Laboratory ID: EST689 $PA 1,sl) Coctc: MOO0054 (314) 298-8566 

E87689 

STL St. Louis 

13715 Rider 'L'rail North 

Eartlr City, MO 63045 --- -----.-.- ---.- ---- 

hfetrix: Solid and Cf~enlical Materials 

Certification 

An~fyth MethudRecl~ Category TYP~ Effective Oate 

- ,.---- --..-- --.- - ----- 

PenWhlomptlcnui BPA 8270 Extroclahlc Ogilnlcs NELAP 211 3/2W2 

PI~ 

PI( 

t'hcnacdie 

Phenantl~rme 

Phcrutnlhre~~c 

Phenol 

Phmiol 

Pllomtz 

Piclonm 

glsopropyllolucnr 

Pulnuriunj 

Potassiu~n 

Yro~~airiide (Kcrh) 

f'~vpio~\iuilc (Ethyl cyariidc) 

p-Xylmc 

Pymc 

Pyrcnc 

Pyridirtc 

Ra<tium-22# 

K13X (l1cx&ydrrr-1,3,5-trinitro.1,3,S-tri;) 

Rwctive cya~idc 

Rcaelive sulfidc 

SoCtvlc 

stc-Butylk.nxnc 

Scknium 

Sclcniulr~ 

Silicon 

Silver 

Silvw 

Silvcr (2,4,5-1'P) 

Sodium 

Siaiurn 

Sln!nliun~ 

Slyrene 

SulLte 

EPA 9040 

EPA 9045 

EPA 8270 

EPA 8270 

LiPA 83 10 

EI'A 804 1 

EPA 8270 

EPA 8270 

PPA %is1 

EPA 8260 

EPA 6010 

EI'A 6020 

EPA $270 

EPA K2($1 

i'.l'A 8260 

EPA 8270 

EPh 83 10 

LPA 8270 

KI'A 9320 

EPA 8330 

EPA 7.3.3.2 

EPA 7.5.4.2 

EPA 8270 

EPA 8260 

EPA 6010 

El'A 6020 

EI'A 60 1 0 

EPA 60 l O 

EPA 6020 

EI'A 8151 

EPA (i010 

EI'A GO20 

EPA 6010 

6PA 8260 

EPA 9056 

General Chieclli~lry 

Gen~mI Chtmisliy 

~act:tblc Organics 

E.slractoblo Orgnics 

Extractable Organics 

Ex~rictaL~lc Orga~iics 

Extroclrtblc Oqf~nics 

Pekdcida-tlerbicidw-PCB's 

Pluticidcs-fiwliic&$-I'CIR's 

Volalilc Organics 

Metnls 

Mrblls 

Enbwtable Organics 

Volatile Organis 

Voliltilc Orga~lics 

Extnlctr~bie Orgtnics 

Exw.Lroble Orgnn~cs 

Extmctnhle Organics 

Ki~diochci~~btr): 

F~im~~~bl c Orga~illlDs 

Gcn~ml Chrniislry 

CI~L~I C:helnistry 

Extmctablc Organics 

Volntilc Orgullid 

Melds 

h4ehls 

hieiitls 

Metills 

Mehls 

P*;~i~ides-lltrbicides-P~~B's 

Mcbls 

Mculs 

Metnls 

Vofiitilc Orgu~~b 

Gcxn~l Cheniistry 

NELAP 

NEI.AI' 

NELAP 

NELAP 

NEtAP 

NBLAP 

NBIAP 

NBlAP 

NELAP 

NELAP 

NELAP 

NEI.AP 

NELAI' 

NEL.AP 

N13LAP 

NCLAP 

NELhP 

NEIAP 

NELAP 

NCLAP 

NfjLAP 

N HLA P 

NEtAt' 

NELhP 

NELAP 

NELAP 

NEI.AP 

NELAP 

NELAP 

Ni.;l,AP 

NEt.AP 

)riF,I.AP 

NE1.At' 

N EL.AP 

NEl.AP 

"STA'TE" indicalrr certification for the analytc by the ~~wtl~otl spccificd. "NELAP" further NON-7'KANSWRABL.E I1/13/2M)3-E876W9 

indicrtc% ccrtificstiola complinnt with tlte NKLAC Stantlrrds. 
John 0. Agwunobi, M.D., M.8.A. 

Secreli~ry 

Page 27 of 27 

TfIIS LISTING OF ACCREDITED ANALYTES SIIOULI) RE tfSEI) ONLY WHEN 

ASSOCIATED Wt'l'H A VALII) CERTIFICATE 

Stiite 1,eboratory ID: E87689 EPA Lab Code: MOO0054 (3f 4) 298-8566 

EX7689 

STI. St. K.ouis 

13715 itider Trail North 

Ei~rtIt City, MO 63045 

,----..-- ----.- -..--. Mrtrir: Solid and Cl~en~ical iMaterials 

Certification 

Analyto Mettiod/'Kccl~ C'ategoq Typ Effwtivc Uatc 

- -.-A- ---- .--.-. -.---.-- - 

Sulfotepp E1'A 11270 P~ticiJcs-Hcrbici11~~-f'CB's NE1,AI' 211 U202 

Sy111twtic I'raipitatiotr Lraciruig h~ceilurr: Et'A 1312 Gerrerul Clranisty NBIAP 211 312W2 

tat-Butylbenzcac Kt1A 8260 Vniotile Orgunis NEitAP 21 13i2W2 

?biul organic carboll 

Trcwl organic helul~r ('I'OX) 

-toliIl pll~llolics 

El'A 8260 

EPA 83.30 

BPAhOlO 

EPA 6020 

EPA 8270 

CPA 6010 

EPA 8021 

EI'A 82M 

DPA 9010 

EPA 9012 

EPA 9056 

BPA 91MO 

BPA 9020 

EPA 9066 

't'ulnt dionr CPA 93iS 

Tot& sulfidcs EVA W4 

Toxaplir?ic (Chkrrinatnl camphctle) BPA 808 I 

Ibxicity Charactcriatic Ixacl~iay Proctdurc EPA 13 11 

t~ns-l,2-Dict~laroetlryltne El'h 8260 

lms-1.3-Dicl1lor~1~~pyla& EPA 82# 

Inmr-I ,4-Dichloro-2-hutme EVA 82filt 

Trichiorocthc?~e (I'riclrio~Mtlhylnle)) EPA 8260 

Viinadiunr 

Vinyl wetale 

Vinyl d~loridc 

Xplrnc (lotul) 

Xylctrc (totnl) 

Zinc 

Xinc 

Vohtilc Organics 

Lxtraclablc Organics 

Metals 

Mctals 

Paticides-llerbicide-I'CU's 

Metals 

Volatilc Organic; 

Volatile Chg~tnics 

Ciencmi Chcnustc)' 

Ci~mrrat Chmristry 

Gnlaul Chnnistv 

Cia~cral Chcwjiatry 

(ici~cral Chanislry 

Cicnenl C:hanislry 

WEI.AP 

NEL.41' 

NELAP 

NEUP 

NELAP 

NELAP 

NEiAP 

NELAP 

NEMP 

NELAP 

NL-:i,AI' 

NEL.AI' 

NELAP 

KELAP 

Rodic~honistry NELAf 21 13/2w2 

Oarnill a~emislry N Bl AP 711 3!2002 

I'csticidcs-ffabicidw-PCB's NEI-AP 2/13/2002 

General O~IL'III~SI[)' NELAP 2/13/2002 

Vol~lile Orgtrn~w NEUP 211 2'2002 

Volalilc Organics 

Volatile Orgatric; 

Volntilc Orgariia 

EPA 82W Volatilc ofg~lli~~ 

EPA 60 10 Metals 

tiPA 6020 

EPA K2M) 

EPA 82GO 

EPA 8021 

HA 8260 

EPA &)lo 

EPA 6020 

KELAP 31 3,2002 

NELAP 2/13/2002 

NELAP 2/ 13t2W2 

NELAP 211 3/2@2 

NELnP 21 lfi2002 

NELAP l117i2001 

NELAP 2/13/2002 

KELAP 211 31202 

KELAP Ul3R002 

NPLAY 21 i3i2002 

NCLAP U13Q002 

NBLAP 211MOD2 

"S'l'A'fE" indicates certification fnrtbe asaiyte by the n~elltod specified. "KELAP" further NON-TRANSFEKAB1.E 1 1112r2003-EX7689 

indicutcs ccrtificatiin cnnipliant with the NE1.AC Standards.