Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-001 Date Collected: 11/11/2013 Date Received: 11/12/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg < 0.2 ng/L U 0.5 0.2 JAB 11/20/2013 EPA 1631E

Sample Number: 134582-002 Date Collected: 11/11/2013 Date Received: 11/12/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.87 ug/L 0.5 0.1 DPC 11/15/2013 13:36 EPA 200.8

Arsenic, As 105 ug/L 1 0.3 DPC 11/15/2013 13:36 EPA 200.8

Barium, Ba 67.4 ug/L 1 0.2 DPC 11/15/2013 13:36 EPA 200.8

Beryllium, Be < 5 ug/L U 20 5 DAM 11/15/2013 13:39 EPA 200.7

Cadmium, Cd 26.5 ug/L 0.5 0.1 DPC 11/15/2013 13:36 EPA 200.8

Chromium, Cr 29.5 ug/L 2 0.4 DPC 11/15/2013 13:36 EPA 200.8

Cobalt, Co 29.1 ug/L 0.2 0.04 DPC 11/15/2013 13:36 EPA 200.8

Copper, Cu 29.6 ug/L 0.5 0.1 DPC 11/15/2013 13:36 EPA 200.8

Lead, Pb 9.32 ug/L 0.1 0.02 DPC 11/15/2013 13:36 EPA 200.8

Mercury, Hg 202000 ng/L 5000 2000 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 64.2 ug/L 0.5 0.1 DPC 11/15/2013 13:36 EPA 200.8

Nickel, Ni 269 ug/L 2 0.5 DPC 11/15/2013 13:36 EPA 200.8

Selenium, Se 105 ug/L 5 2 DPC 11/15/2013 13:36 EPA 200.8

Silver, Ag 0.06 ug/L J 0.1 0.02 DPC 11/15/2013 13:36 EPA 200.8

Thallium, Tl 1.66 ug/L 0.5 0.02 DPC 11/15/2013 13:36 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 11/15/2013 13:39 EPA 200.7

Titanium, Ti 103 ug/L 100 20 DAM 11/15/2013 13:39 EPA 200.7

Zinc, Zn 309 ug/L 5 1 DPC 11/15/2013 13:36 EPA 200.8

Aluminum, Al 0.615 mg/L 0.01 0.003 DPC 11/15/2013 13:36 EPA 200.8

Boron, B 489 mg/L 1 0.2 DAM 11/15/2013 13:39 EPA 200.7

Calcium, Ca 3790 mg/L 1 0.2 DAM 11/15/2013 13:39 EPA 200.7

Iron, Fe 50.3 mg/L 2 0.5 DAM 11/15/2013 13:39 EPA 200.7

Magnesium, Mg 4300 mg/L 0.5 0.1 DAM 11/15/2013 13:39 EPA 200.7

Manganese, Mn 74.1 mg/L 0.02 0.005 DAM 11/15/2013 13:39 EPA 200.7

Potassium, K 82.0 mg/L 2 0.4 DAM 11/15/2013 13:38 EPA 200.7

Sodium, Na 447 mg/L 2 0.4 DAM 11/15/2013 13:37 EPA 200.7

Strontium, Sr 31.5 mg/L 0.05 0.02 DAM 11/15/2013 13:37 EPA 200.7

Ammonia, NH3, as N 0.72 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 12.3 mg/L 5 1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 44.7 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 1 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-002A Date Collected: 11/11/2013 Date Received: 11/12/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.64 ug/L 0.5 0.1 DPC 11/15/2013 13:41 EPA 200.8

Arsenic, As 7.96 ug/L 1 0.3 DPC 11/15/2013 13:41 EPA 200.8

Barium, Ba 7.30 ug/L 1 0.2 DPC 11/15/2013 13:41 EPA 200.8

Beryllium, Be < 5 ug/L U 20 5 DAM 11/15/2013 13:43 EPA 200.7

Cadmium, Cd 22.8 ug/L 0.5 0.1 DPC 11/15/2013 13:41 EPA 200.8

Chromium, Cr 1 ug/L J 2 0.4 DPC 11/15/2013 13:41 EPA 200.8

Cobalt, Co 23.0 ug/L 0.2 0.04 DPC 11/15/2013 13:41 EPA 200.8

Copper, Cu 1.43 ug/L 0.5 0.1 DPC 11/15/2013 13:41 EPA 200.8

Lead, Pb 0.04 ug/L J 0.1 0.02 DPC 11/15/2013 13:41 EPA 200.8

Mercury, Hg 21200 ng/L 500 200 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 53.7 ug/L 0.5 0.1 DPC 11/15/2013 13:41 EPA 200.8

Nickel, Ni 225 ug/L 2 0.5 DPC 11/15/2013 13:41 EPA 200.8

Selenium, Se 62.8 ug/L 5 2 DPC 11/15/2013 13:41 EPA 200.8

Selenite, Se+4 (Hydride) 348 ug/L 20 4 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag < 0.02 ug/L U 0.1 0.02 DPC 11/15/2013 13:41 EPA 200.8

Thallium, Tl 1.39 ug/L 0.5 0.02 DPC 11/15/2013 13:41 EPA 200.8

Tin, Sn < 100 ug/L U 500 100 DAM 11/15/2013 13:44 EPA 200.7

Titanium, Ti < 20 ug/L U 100 20 DAM 11/15/2013 13:44 EPA 200.7

Zinc, Zn 113 ug/L 5 1 DPC 11/15/2013 13:41 EPA 200.8

Aluminum, Al 0.0110 mg/L 0.01 0.003 DPC 11/15/2013 13:41 EPA 200.8

Boron, B 514 mg/L 1 0.2 DAM 11/15/2013 13:43 EPA 200.7

Calcium, Ca 673 mg/L 1 0.2 DAM 11/15/2013 13:43 EPA 200.7

Iron, Fe < 0.5 mg/L U 2 0.5 DAM 11/15/2013 13:44 EPA 200.7

Magnesium, Mg 4510 mg/L 0.5 0.1 DAM 11/15/2013 13:43 EPA 200.7

Manganese, Mn 75.5 mg/L 0.02 0.005 DAM 11/15/2013 13:43 EPA 200.7

Potassium, K 83.9 mg/L 2 0.4 DAM 11/15/2013 13:42 EPA 200.7

Sodium, Na 475 mg/L 2 0.4 DAM 11/15/2013 13:42 EPA 200.7

Strontium, Sr 9.62 mg/L 0.05 0.02 DAM 11/15/2013 13:42 EPA 200.7

Mountaineer Plant, 134582 Page 2 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-003 Date Collected: 11/11/2013 Date Received: 11/12/2013

Primary Clarifier Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 4.88 ug/L 0.05 0.01 DPC 11/15/2013 14:32 EPA 200.8

Arsenic, As 5.48 ug/L 0.1 0.03 DPC 11/15/2013 14:32 EPA 200.8

Barium, Ba 60.3 ug/L 0.1 0.02 DPC 11/15/2013 14:32 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 13:48 EPA 200.7

Cadmium, Cd 95.2 ug/L 0.05 0.01 DPC 11/15/2013 14:32 EPA 200.8

Chromium, Cr 10.5 ug/L 0.2 0.04 DPC 11/15/2013 14:32 EPA 200.8

Cobalt, Co 153 ug/L 0.02 0.004 DPC 11/15/2013 14:32 EPA 200.8

Copper, Cu 8.57 ug/L 0.05 0.01 DPC 11/15/2013 14:32 EPA 200.8

Lead, Pb 1.65 ug/L 0.01 0.002 DPC 11/15/2013 14:32 EPA 200.8

Mercury, Hg 5090 ng/L 50 20 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 556 ug/L 0.05 0.01 DPC 11/15/2013 14:32 EPA 200.8

Nickel, Ni 1370 ug/L 0.2 0.05 DPC 11/15/2013 14:32 EPA 200.8

Selenium, Se 544 ug/L 0.5 0.2 DPC 11/15/2013 14:32 EPA 200.8

Silver, Ag 0.034 ug/L 0.01 0.002 DPC 11/15/2013 14:32 EPA 200.8

Thallium, Tl 9.28 ug/L 0.05 0.002 DPC 11/15/2013 14:32 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 13:48 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 13:48 EPA 200.7

Zinc, Zn 265 ug/L 0.5 0.1 DPC 11/15/2013 14:32 EPA 200.8

Aluminum, Al 0.350 mg/L 0.001 0.0003 DPC 11/15/2013 14:32 EPA 200.8

Boron, B 441 mg/L 0.2 0.04 DAM 11/15/2013 13:48 EPA 200.7

Calcium, Ca 630 mg/L 0.2 0.04 DAM 11/15/2013 13:48 EPA 200.7

Iron, Fe 1.17 mg/L 0.5 0.1 DAM 11/15/2013 13:48 EPA 200.7

Magnesium, Mg 3980 mg/L 0.1 0.02 DAM 11/15/2013 13:48 EPA 200.7

Manganese, Mn 63.4 mg/L 0.005 0.001 DAM 11/15/2013 13:48 EPA 200.7

Potassium, K 71.7 mg/L 0.5 0.07 DAM 11/15/2013 13:46 EPA 200.7

Sodium, Na 422 mg/L 0.3 0.08 DAM 11/15/2013 13:46 EPA 200.7

Strontium, Sr 7.88 mg/L 0.01 0.003 DAM 11/15/2013 13:46 EPA 200.7

Ammonia, NH3, as N 2.84 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 6.17 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 36.7 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 3 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-003A Date Collected: 11/11/2013 Date Received: 11/12/2013

Primary Clarifier Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 4.35 ug/L 0.05 0.01 DPC 11/15/2013 14:37 EPA 200.8

Arsenic, As 4.03 ug/L 0.1 0.03 DPC 11/15/2013 14:37 EPA 200.8

Barium, Ba 53.0 ug/L 0.1 0.02 DPC 11/15/2013 14:37 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 14:17 EPA 200.7

Cadmium, Cd 85.0 ug/L 0.05 0.01 DPC 11/15/2013 14:37 EPA 200.8

Chromium, Cr 3.0 ug/L 0.2 0.04 DPC 11/15/2013 14:37 EPA 200.8

Cobalt, Co 137 ug/L 0.02 0.004 DPC 11/15/2013 14:37 EPA 200.8

Copper, Cu 4.69 ug/L 0.05 0.01 DPC 11/15/2013 14:37 EPA 200.8

Lead, Pb 0.022 ug/L 0.01 0.002 DPC 11/15/2013 14:37 EPA 200.8

Mercury, Hg 2580 ng/L 50 20 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 496 ug/L 0.05 0.01 DPC 11/15/2013 14:37 EPA 200.8

Nickel, Ni 1240 ug/L 0.2 0.05 DPC 11/15/2013 14:37 EPA 200.8

Selenium, Se 496 ug/L 0.5 0.2 DPC 11/15/2013 14:37 EPA 200.8

Selenite, Se+4 (Hydride) 393 ug/L 20 4 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag 0.015 ug/L 0.01 0.002 DPC 11/15/2013 14:37 EPA 200.8

Thallium, Tl 8.41 ug/L 0.05 0.002 DPC 11/15/2013 14:37 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 14:17 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 14:17 EPA 200.7

Zinc, Zn 222 ug/L 0.5 0.1 DPC 11/15/2013 14:37 EPA 200.8

Aluminum, Al 0.0294 mg/L 0.001 0.0003 DPC 11/15/2013 14:37 EPA 200.8

Boron, B 456 mg/L 0.2 0.04 DAM 11/15/2013 14:17 EPA 200.7

Calcium, Ca 649 mg/L 0.2 0.04 DAM 11/15/2013 14:17 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 11/15/2013 14:17 EPA 200.7

Magnesium, Mg 4070 mg/L 0.1 0.02 DAM 11/15/2013 14:17 EPA 200.7

Manganese, Mn 65.3 mg/L 0.005 0.001 DAM 11/15/2013 14:17 EPA 200.7

Potassium, K 72.3 mg/L 0.5 0.07 DAM 11/15/2013 14:15 EPA 200.7

Sodium, Na 428 mg/L 0.3 0.08 DAM 11/15/2013 14:15 EPA 200.7

Strontium, Sr 8.01 mg/L 0.01 0.003 DAM 11/15/2013 14:15 EPA 200.7

Mountaineer Plant, 134582 Page 4 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-004 Date Collected: 11/11/2013 Date Received: 11/12/2013

CPS Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 3.77 ug/L 0.05 0.01 DPC 11/15/2013 14:42 EPA 200.8

Arsenic, As 3.92 ug/L 0.1 0.03 DPC 11/15/2013 14:42 EPA 200.8

Barium, Ba 58.9 ug/L 0.1 0.02 DPC 11/15/2013 14:42 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 14:26 EPA 200.7

Cadmium, Cd 4.62 ug/L 0.05 0.01 DPC 11/15/2013 14:42 EPA 200.8

Chromium, Cr 1.9 ug/L 0.2 0.04 DPC 11/15/2013 14:42 EPA 200.8

Cobalt, Co 95.2 ug/L 0.02 0.004 DPC 11/15/2013 14:42 EPA 200.8

Copper, Cu 1.14 ug/L 0.05 0.01 DPC 11/15/2013 14:42 EPA 200.8

Lead, Pb 0.140 ug/L 0.01 0.002 DPC 11/15/2013 14:42 EPA 200.8

Mercury, Hg 254 ng/L 20 8 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 414 ug/L 0.05 0.01 DPC 11/15/2013 14:42 EPA 200.8

Nickel, Ni 967 ug/L 0.2 0.05 DPC 11/15/2013 14:42 EPA 200.8

Selenium, Se 458 ug/L 0.5 0.2 DPC 11/15/2013 14:42 EPA 200.8

Silver, Ag 0.005 ug/L J 0.01 0.002 DPC 11/15/2013 14:42 EPA 200.8

Thallium, Tl 3.06 ug/L 0.05 0.002 DPC 11/15/2013 14:42 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 14:27 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 14:27 EPA 200.7

Zinc, Zn 165 ug/L 0.5 0.1 DPC 11/15/2013 14:42 EPA 200.8

Aluminum, Al 0.0728 mg/L 0.001 0.0003 DPC 11/15/2013 14:42 EPA 200.8

Boron, B 388 mg/L 0.2 0.04 DAM 11/15/2013 14:26 EPA 200.7

Calcium, Ca 536 mg/L 0.2 0.04 DAM 11/15/2013 14:26 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 11/15/2013 14:27 EPA 200.7

Magnesium, Mg 3490 mg/L 0.1 0.02 DAM 11/15/2013 14:26 EPA 200.7

Manganese, Mn 58.2 mg/L 0.005 0.001 DAM 11/15/2013 14:26 EPA 200.7

Potassium, K 61.6 mg/L 0.5 0.07 DAM 11/15/2013 14:25 EPA 200.7

Sodium, Na 356 mg/L 0.3 0.08 DAM 11/15/2013 14:25 EPA 200.7

Strontium, Sr 6.73 mg/L 0.01 0.003 DAM 11/15/2013 14:25 EPA 200.7

Ammonia, NH3, as N 3.22 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 5.52 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 34.7 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 5 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-004A Date Collected: 11/11/2013 Date Received: 11/12/2013

CPS Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 3.64 ug/L 0.05 0.01 DPC 11/15/2013 14:47 EPA 200.8

Arsenic, As 3.71 ug/L 0.1 0.03 DPC 11/15/2013 14:47 EPA 200.8

Barium, Ba 55.7 ug/L 0.1 0.02 DPC 11/15/2013 14:47 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 14:36 EPA 200.7

Cadmium, Cd 2.88 ug/L 0.05 0.01 DPC 11/15/2013 14:47 EPA 200.8

Chromium, Cr 1.4 ug/L 0.2 0.04 DPC 11/15/2013 14:47 EPA 200.8

Cobalt, Co 89.1 ug/L 0.02 0.004 DPC 11/15/2013 14:47 EPA 200.8

Copper, Cu 0.72 ug/L 0.05 0.01 DPC 11/15/2013 14:47 EPA 200.8

Lead, Pb 0.560 ug/L 0.01 0.002 DPC 11/15/2013 14:47 EPA 200.8

Mercury, Hg 9.0 ng/L 2 0.8 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 395 ug/L 0.05 0.01 DPC 11/15/2013 14:47 EPA 200.8

Nickel, Ni 918 ug/L 0.2 0.05 DPC 11/15/2013 14:47 EPA 200.8

Selenium, Se 431 ug/L 0.5 0.2 DPC 11/15/2013 14:47 EPA 200.8

Selenite, Se+4 (Hydride) 375 ug/L 20 4 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag 0.003 ug/L J 0.01 0.002 DPC 11/15/2013 14:47 EPA 200.8

Thallium, Tl 2.69 ug/L 0.05 0.002 DPC 11/15/2013 14:47 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 14:36 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 14:36 EPA 200.7

Zinc, Zn 155 ug/L 0.5 0.1 DPC 11/15/2013 14:47 EPA 200.8

Aluminum, Al 0.0242 mg/L 0.001 0.0003 DPC 11/15/2013 14:47 EPA 200.8

Boron, B 392 mg/L 0.2 0.04 DAM 11/15/2013 14:36 EPA 200.7

Calcium, Ca 545 mg/L 0.2 0.04 DAM 11/15/2013 14:36 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 11/15/2013 14:36 EPA 200.7

Magnesium, Mg 3540 mg/L 0.1 0.02 DAM 11/15/2013 14:36 EPA 200.7

Manganese, Mn 58.9 mg/L 0.005 0.001 DAM 11/15/2013 14:36 EPA 200.7

Potassium, K 63.5 mg/L 0.5 0.07 DAM 11/15/2013 14:34 EPA 200.7

Sodium, Na 362 mg/L 0.3 0.08 DAM 11/15/2013 14:34 EPA 200.7

Strontium, Sr 6.86 mg/L 0.01 0.003 DAM 11/15/2013 14:34 EPA 200.7

Mountaineer Plant, 134582 Page 6 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-005 Date Collected: 11/11/2013 Date Received: 11/12/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 10.5 ug/L 0.05 0.01 DPC 11/15/2013 14:52 EPA 200.8

Arsenic, As 29.4 ug/L 0.1 0.03 DPC 11/15/2013 14:52 EPA 200.8

Barium, Ba 37.8 ug/L 0.1 0.02 DPC 11/15/2013 14:52 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 14:45 EPA 200.7

Cadmium, Cd 51.2 ug/L 0.05 0.01 DPC 11/15/2013 14:52 EPA 200.8

Chromium, Cr 1.4 ug/L 0.2 0.04 DPC 11/15/2013 14:52 EPA 200.8

Cobalt, Co 63.3 ug/L 0.02 0.004 DPC 11/15/2013 14:52 EPA 200.8

Copper, Cu 2.42 ug/L 0.05 0.01 DPC 11/15/2013 14:52 EPA 200.8

Lead, Pb 0.241 ug/L 0.01 0.002 DPC 11/15/2013 14:52 EPA 200.8

Mercury, Hg 276 ng/L 10 4 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 5710 ug/L 0.05 0.01 DPC 11/15/2013 14:52 EPA 200.8

Nickel, Ni 522 ug/L 0.2 0.05 DPC 11/15/2013 14:52 EPA 200.8

Selenium, Se 399 ug/L 0.5 0.2 DPC 11/15/2013 14:52 EPA 200.8

Silver, Ag 0.006 ug/L J 0.01 0.002 DPC 11/15/2013 14:52 EPA 200.8

Thallium, Tl 5.70 ug/L 0.05 0.002 DPC 11/15/2013 14:52 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 14:46 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 14:45 EPA 200.7

Zinc, Zn 146 ug/L 0.5 0.1 DPC 11/15/2013 14:52 EPA 200.8

Aluminum, Al 0.154 mg/L 0.001 0.0003 DPC 11/15/2013 14:52 EPA 200.8

Boron, B 206 mg/L 0.2 0.04 DAM 11/15/2013 14:45 EPA 200.7

Calcium, Ca 485 mg/L 0.2 0.04 DAM 11/15/2013 14:45 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 11/15/2013 14:46 EPA 200.7

Magnesium, Mg 1660 mg/L 0.1 0.02 DAM 11/15/2013 14:45 EPA 200.7

Manganese, Mn 23.3 mg/L 0.005 0.001 DAM 11/15/2013 14:45 EPA 200.7

Potassium, K 116 mg/L 0.5 0.07 DAM 11/15/2013 14:44 EPA 200.7

Sodium, Na 1650 mg/L 0.3 0.08 DAM 11/15/2013 14:44 EPA 200.7

Strontium, Sr 6.90 mg/L 0.01 0.003 DAM 11/15/2013 14:44 EPA 200.7

Ammonia, NH3, as N 1.88 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.52 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 18.5 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 7 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-005A Date Collected: 11/11/2013 Date Received: 11/12/2013

Landfill Leachate Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 9.77 ug/L 0.05 0.01 DPC 11/15/2013 14:57 EPA 200.8

Arsenic, As 26.2 ug/L 0.1 0.03 DPC 11/15/2013 14:57 EPA 200.8

Barium, Ba 33.9 ug/L 0.1 0.02 DPC 11/15/2013 14:57 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 14:55 EPA 200.7

Cadmium, Cd 48.8 ug/L 0.05 0.01 DPC 11/15/2013 14:57 EPA 200.8

Chromium, Cr 0.9 ug/L 0.2 0.04 DPC 11/15/2013 14:57 EPA 200.8

Cobalt, Co 59.4 ug/L 0.02 0.004 DPC 11/15/2013 14:57 EPA 200.8

Copper, Cu 1.81 ug/L 0.05 0.01 DPC 11/15/2013 14:57 EPA 200.8

Lead, Pb 0.010 ug/L 0.01 0.002 DPC 11/15/2013 14:57 EPA 200.8

Mercury, Hg 53.2 ng/L 2 0.8 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 5460 ug/L 0.05 0.01 DPC 11/15/2013 14:57 EPA 200.8

Nickel, Ni 495 ug/L 0.2 0.05 DPC 11/15/2013 14:57 EPA 200.8

Selenium, Se 377 ug/L 0.5 0.2 DPC 11/15/2013 14:57 EPA 200.8

Selenite, Se+4 (Hydride) 317 ug/L 20 4 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag 0.003 ug/L J 0.01 0.002 DPC 11/15/2013 14:57 EPA 200.8

Thallium, Tl 5.55 ug/L 0.05 0.002 DPC 11/15/2013 14:57 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 14:55 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 14:55 EPA 200.7

Zinc, Zn 131 ug/L 0.5 0.1 DPC 11/15/2013 14:57 EPA 200.8

Aluminum, Al 0.0506 mg/L 0.001 0.0003 DPC 11/15/2013 14:57 EPA 200.8

Boron, B 205 mg/L 0.2 0.04 DAM 11/15/2013 14:55 EPA 200.7

Calcium, Ca 485 mg/L 0.2 0.04 DAM 11/15/2013 14:55 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 11/15/2013 14:55 EPA 200.7

Magnesium, Mg 1660 mg/L 0.1 0.02 DAM 11/15/2013 14:55 EPA 200.7

Manganese, Mn 23.1 mg/L 0.005 0.001 DAM 11/15/2013 14:55 EPA 200.7

Potassium, K 115 mg/L 0.5 0.07 DAM 11/15/2013 14:54 EPA 200.7

Sodium, Na 1640 mg/L 0.3 0.08 DAM 11/15/2013 14:54 EPA 200.7

Strontium, Sr 6.84 mg/L 0.01 0.003 DAM 11/15/2013 14:54 EPA 200.7

Mountaineer Plant, 134582 Page 8 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-006 Date Collected: 11/11/2013 Date Received: 11/12/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 7.03 ug/L 0.05 0.01 DPC 11/15/2013 15:02 EPA 200.8

Arsenic, As 15.8 ug/L 0.1 0.03 DPC 11/15/2013 15:02 EPA 200.8

Barium, Ba 51.1 ug/L 0.1 0.02 DPC 11/15/2013 15:02 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 15:04 EPA 200.7

Cadmium, Cd 27.1 ug/L 0.05 0.01 DPC 11/15/2013 15:02 EPA 200.8

Chromium, Cr 1.9 ug/L 0.2 0.04 DPC 11/15/2013 15:02 EPA 200.8

Cobalt, Co 82.5 ug/L 0.02 0.004 DPC 11/15/2013 15:02 EPA 200.8

Copper, Cu 1.87 ug/L 0.05 0.01 DPC 11/15/2013 15:02 EPA 200.8

Lead, Pb 0.142 ug/L 0.01 0.002 DPC 11/15/2013 15:02 EPA 200.8

Mercury, Hg 275 ng/L 10 4 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 2950 ug/L 0.05 0.01 DPC 11/15/2013 15:02 EPA 200.8

Nickel, Ni 790 ug/L 0.2 0.05 DPC 11/15/2013 15:02 EPA 200.8

Selenium, Se 445 ug/L 0.5 0.2 DPC 11/15/2013 15:02 EPA 200.8

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 11/15/2013 15:02 EPA 200.8

Thallium, Tl 4.26 ug/L 0.05 0.002 DPC 11/15/2013 15:02 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 15:05 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 15:05 EPA 200.7

Zinc, Zn 164 ug/L 0.5 0.1 DPC 11/15/2013 15:02 EPA 200.8

Aluminum, Al 0.135 mg/L 0.001 0.0003 DPC 11/15/2013 15:02 EPA 200.8

Boron, B 309 mg/L 0.2 0.04 DAM 11/15/2013 15:04 EPA 200.7

Calcium, Ca 515 mg/L 0.2 0.04 DAM 11/15/2013 15:04 EPA 200.7

Iron, Fe 0.2 mg/L J 0.5 0.1 DAM 11/15/2013 15:05 EPA 200.7

Magnesium, Mg 2690 mg/L 0.1 0.02 DAM 11/15/2013 15:04 EPA 200.7

Manganese, Mn 43.4 mg/L 0.005 0.001 DAM 11/15/2013 15:04 EPA 200.7

Potassium, K 84.8 mg/L 0.5 0.07 DAM 11/15/2013 15:03 EPA 200.7

Sodium, Na 911 mg/L 0.3 0.08 DAM 11/15/2013 15:03 EPA 200.7

Strontium, Sr 6.79 mg/L 0.01 0.003 DAM 11/15/2013 15:03 EPA 200.7

Ammonia, NH3, as N 2.36 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 5.01 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 32.1 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 9 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-006A Date Collected: 11/11/2013 Date Received: 11/12/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 6.44 ug/L 0.05 0.01 DPC 11/15/2013 15:08 EPA 200.8

Arsenic, As 12.6 ug/L 0.1 0.03 DPC 11/15/2013 15:08 EPA 200.8

Barium, Ba 44.4 ug/L 0.1 0.02 DPC 11/15/2013 15:08 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 15:14 EPA 200.7

Cadmium, Cd 23.7 ug/L 0.05 0.01 DPC 11/15/2013 15:08 EPA 200.8

Chromium, Cr 1.2 ug/L 0.2 0.04 DPC 11/15/2013 15:08 EPA 200.8

Cobalt, Co 73.7 ug/L 0.02 0.004 DPC 11/15/2013 15:08 EPA 200.8

Copper, Cu 1.19 ug/L 0.05 0.01 DPC 11/15/2013 15:08 EPA 200.8

Lead, Pb 0.038 ug/L 0.01 0.002 DPC 11/15/2013 15:08 EPA 200.8

Mercury, Hg 22.7 ng/L 2 0.8 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 2660 ug/L 0.05 0.01 DPC 11/15/2013 15:08 EPA 200.8

Nickel, Ni 717 ug/L 0.2 0.05 DPC 11/15/2013 15:08 EPA 200.8

Selenium, Se 395 ug/L 0.5 0.2 DPC 11/15/2013 15:08 EPA 200.8

Selenite, Se+4 (Hydride) 361 ug/L 20 4 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 11/15/2013 15:08 EPA 200.8

Thallium, Tl 3.82 ug/L 0.05 0.002 DPC 11/15/2013 15:08 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 15:14 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 15:14 EPA 200.7

Zinc, Zn 142 ug/L 0.5 0.1 DPC 11/15/2013 15:08 EPA 200.8

Aluminum, Al 0.0359 mg/L 0.001 0.0003 DPC 11/15/2013 15:08 EPA 200.8

Boron, B 305 mg/L 0.2 0.04 DAM 11/15/2013 15:14 EPA 200.7

Calcium, Ca 509 mg/L 0.2 0.04 DAM 11/15/2013 15:14 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 11/15/2013 15:14 EPA 200.7

Magnesium, Mg 2660 mg/L 0.1 0.02 DAM 11/15/2013 15:14 EPA 200.7

Manganese, Mn 42.7 mg/L 0.005 0.001 DAM 11/15/2013 15:14 EPA 200.7

Potassium, K 83.7 mg/L 0.5 0.07 DAM 11/15/2013 15:13 EPA 200.7

Sodium, Na 896 mg/L 0.3 0.08 DAM 11/15/2013 15:13 EPA 200.7

Strontium, Sr 6.69 mg/L 0.01 0.003 DAM 11/15/2013 15:13 EPA 200.7

Mountaineer Plant, 134582 Page 10 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-007 Date Collected: 11/11/2013 Date Received: 11/12/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.40 ug/L 0.05 0.01 DPC 11/15/2013 15:13 EPA 200.8

Arsenic, As 15.4 ug/L 0.1 0.03 DPC 11/15/2013 15:13 EPA 200.8

Barium, Ba 36.2 ug/L 0.1 0.02 DPC 11/15/2013 15:13 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 15:37 EPA 200.7

Cadmium, Cd 1.17 ug/L 0.05 0.01 DPC 11/15/2013 15:13 EPA 200.8

Chromium, Cr 1.0 ug/L 0.2 0.04 DPC 11/15/2013 15:13 EPA 200.8

Cobalt, Co 41.4 ug/L 0.02 0.004 DPC 11/15/2013 15:13 EPA 200.8

Copper, Cu 0.34 ug/L 0.05 0.01 DPC 11/15/2013 15:13 EPA 200.8

Lead, Pb 0.029 ug/L 0.01 0.002 DPC 11/15/2013 15:13 EPA 200.8

Mercury, Hg 79.3 ng/L 2 0.8 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 4190 ug/L 0.05 0.01 DPC 11/15/2013 15:13 EPA 200.8

Nickel, Ni 200 ug/L 0.2 0.05 DPC 11/15/2013 15:13 EPA 200.8

Selenium, Se 11.7 ug/L 0.5 0.2 DPC 11/15/2013 15:13 EPA 200.8

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 11/15/2013 15:13 EPA 200.8

Thallium, Tl 0.43 ug/L 0.05 0.002 DPC 11/15/2013 15:13 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 15:38 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 15:38 EPA 200.7

Zinc, Zn 6.1 ug/L 0.5 0.1 DPC 11/15/2013 15:13 EPA 200.8

Aluminum, Al 0.507 mg/L 0.001 0.0003 DPC 11/15/2013 15:13 EPA 200.8

Boron, B 211 mg/L 0.2 0.04 DAM 11/15/2013 15:37 EPA 200.7

Calcium, Ca 492 mg/L 0.2 0.04 DAM 11/15/2013 15:37 EPA 200.7

Iron, Fe 1.05 mg/L 0.5 0.1 DAM 11/15/2013 15:38 EPA 200.7

Magnesium, Mg 1700 mg/L 0.1 0.02 DAM 11/15/2013 15:37 EPA 200.7

Manganese, Mn 25.5 mg/L 0.005 0.001 DAM 11/15/2013 15:37 EPA 200.7

Potassium, K 120 mg/L 0.5 0.07 DAM 11/15/2013 15:36 EPA 200.7

Sodium, Na 1620 mg/L 0.3 0.08 DAM 11/15/2013 15:36 EPA 200.7

Strontium, Sr 6.84 mg/L 0.01 0.003 DAM 11/15/2013 15:36 EPA 200.7

Ammonia, NH3, as N 0.62 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 5.51 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 1.22 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 11 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-007A Date Collected: 11/11/2013 Date Received: 11/12/2013

2nd Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 1.38 ug/L 0.05 0.01 DPC 11/15/2013 15:48 EPA 200.8

Arsenic, As 13.5 ug/L 0.1 0.03 DPC 11/15/2013 15:48 EPA 200.8

Barium, Ba 32.8 ug/L 0.1 0.02 DPC 11/15/2013 15:48 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 15:47 EPA 200.7

Cadmium, Cd 0.57 ug/L 0.05 0.01 DPC 11/15/2013 15:48 EPA 200.8

Chromium, Cr 0.9 ug/L 0.2 0.04 DPC 11/15/2013 15:48 EPA 200.8

Cobalt, Co 39.0 ug/L 0.02 0.004 DPC 11/15/2013 15:48 EPA 200.8

Copper, Cu 0.20 ug/L 0.05 0.01 DPC 11/15/2013 15:48 EPA 200.8

Lead, Pb 0.017 ug/L 0.01 0.002 DPC 11/15/2013 15:48 EPA 200.8

Mercury, Hg 14.2 ng/L 1 0.4 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 3940 ug/L 0.05 0.01 DPC 11/15/2013 15:48 EPA 200.8

Nickel, Ni 188 ug/L 0.2 0.05 DPC 11/15/2013 15:48 EPA 200.8

Selenium, Se 5.9 ug/L 0.5 0.2 DPC 11/15/2013 15:48 EPA 200.8

Selenite, Se+4 (Hydride) < 0.4 ug/L U 2 0.4 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag < 0.002 ug/L U 0.01 0.002 DPC 11/15/2013 15:48 EPA 200.8

Thallium, Tl 0.38 ug/L 0.05 0.002 DPC 11/15/2013 15:48 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 15:47 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 15:47 EPA 200.7

Zinc, Zn 9.4 ug/L 0.5 0.1 DPC 11/15/2013 15:48 EPA 200.8

Aluminum, Al 0.455 mg/L 0.001 0.0003 DPC 11/15/2013 15:48 EPA 200.8

Boron, B 202 mg/L 0.2 0.04 DAM 11/15/2013 15:47 EPA 200.7

Calcium, Ca 469 mg/L 0.2 0.04 DAM 11/15/2013 15:47 EPA 200.7

Iron, Fe 0.979 mg/L 0.5 0.1 DAM 11/15/2013 15:47 EPA 200.7

Magnesium, Mg 1620 mg/L 0.1 0.02 DAM 11/15/2013 15:47 EPA 200.7

Manganese, Mn 24.2 mg/L 0.005 0.001 DAM 11/15/2013 15:47 EPA 200.7

Potassium, K 114 mg/L 0.5 0.07 DAM 11/15/2013 15:46 EPA 200.7

Sodium, Na 1540 mg/L 0.3 0.08 DAM 11/15/2013 15:46 EPA 200.7

Strontium, Sr 6.53 mg/L 0.01 0.003 DAM 11/15/2013 15:46 EPA 200.7

Mountaineer Plant, 134582 Page 12 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-008 Date Collected: 11/11/2013 Date Received: 11/12/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.17 ug/L 0.05 0.01 DPC 11/15/2013 15:53 EPA 200.8

Arsenic, As 0.70 ug/L 0.1 0.03 DPC 11/15/2013 15:53 EPA 200.8

Barium, Ba 35.2 ug/L 0.1 0.02 DPC 11/15/2013 15:53 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 15:57 EPA 200.7

Cadmium, Cd 0.23 ug/L 0.05 0.01 DPC 11/15/2013 15:53 EPA 200.8

Chromium, Cr 0.8 ug/L 0.2 0.04 DPC 11/15/2013 15:53 EPA 200.8

Cobalt, Co 0.096 ug/L 0.02 0.004 DPC 11/15/2013 15:53 EPA 200.8

Copper, Cu 0.14 ug/L 0.05 0.01 DPC 11/15/2013 15:53 EPA 200.8

Lead, Pb 0.015 ug/L 0.01 0.002 DPC 11/15/2013 15:53 EPA 200.8

Mercury, Hg 15.2 ng/L 1 0.4 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 563 ug/L 0.05 0.01 DPC 11/15/2013 15:53 EPA 200.8

Nickel, Ni 4.81 ug/L 0.2 0.05 DPC 11/15/2013 15:53 EPA 200.8

Selenium, Se 2.2 ug/L 0.5 0.2 DPC 11/15/2013 15:53 EPA 200.8

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 11/15/2013 15:53 EPA 200.8

Thallium, Tl 0.02 ug/L J 0.05 0.002 DPC 11/15/2013 15:53 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 15:57 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 15:57 EPA 200.7

Zinc, Zn 1.3 ug/L 0.5 0.1 DPC 11/15/2013 15:53 EPA 200.8

Aluminum, Al 1.33 mg/L 0.001 0.0003 DPC 11/15/2013 15:53 EPA 200.8

Boron, B 203 mg/L 0.2 0.04 DAM 11/15/2013 15:57 EPA 200.7

Calcium, Ca 491 mg/L 0.2 0.04 DAM 11/15/2013 15:57 EPA 200.7

Iron, Fe 1.23 mg/L 0.5 0.1 DAM 11/15/2013 15:57 EPA 200.7

Magnesium, Mg 1680 mg/L 0.1 0.02 DAM 11/15/2013 15:57 EPA 200.7

Manganese, Mn 24.0 mg/L 0.005 0.001 DAM 11/15/2013 15:57 EPA 200.7

Potassium, K 125 mg/L 0.5 0.07 DAM 11/15/2013 15:55 EPA 200.7

Sodium, Na 1570 mg/L 0.3 0.08 DAM 11/15/2013 15:55 EPA 200.7

Strontium, Sr 6.81 mg/L 0.01 0.003 DAM 11/15/2013 15:55 EPA 200.7

Ammonia, NH3, as N 0.48 mg/L 0.05 0.02 DMM 11/15/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 7.28 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 2.21 mg/L 0.1 0.02 DMM 11/19/2013 SM20 4500NO3 H

Mountaineer Plant, 134582 Page 13 of 14
Location: Mountaineer Plant Report Date: 12/18/2013

Sample Number: 134582-008A Date Collected: 11/11/2013 Date Received: 11/12/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.14 ug/L 0.05 0.01 DPC 11/15/2013 15:58 EPA 200.8

Arsenic, As 0.65 ug/L 0.1 0.03 DPC 11/15/2013 15:58 EPA 200.8

Barium, Ba 32.2 ug/L 0.1 0.02 DPC 11/15/2013 15:58 EPA 200.8

Beryllium, Be < 1 ug/L U 5 1 DAM 11/15/2013 16:06 EPA 200.7

Cadmium, Cd 0.16 ug/L 0.05 0.01 DPC 11/15/2013 15:58 EPA 200.8

Chromium, Cr 0.8 ug/L 0.2 0.04 DPC 11/15/2013 15:58 EPA 200.8

Cobalt, Co 0.104 ug/L 0.02 0.004 DPC 11/15/2013 15:58 EPA 200.8

Copper, Cu 0.06 ug/L 0.05 0.01 DPC 11/15/2013 15:58 EPA 200.8

Lead, Pb 0.022 ug/L 0.01 0.002 DPC 11/15/2013 15:58 EPA 200.8

Mercury, Hg 5.5 ng/L 0.5 0.2 JAB 11/20/2013 EPA 1631E

Molybdenum, Mo 500 ug/L 0.05 0.01 DPC 11/15/2013 15:58 EPA 200.8

Nickel, Ni 4.67 ug/L 0.2 0.05 DPC 11/15/2013 15:58 EPA 200.8

Selenium, Se 1.8 ug/L 0.5 0.2 DPC 11/15/2013 15:58 EPA 200.8

Selenite, Se+4 (Hydride) < 0.08 ug/L U 0.4 0.08 TLT 12/04/2013 AEP Method

AEP Method for Se speciation is not accredited through any agency. Results are for internal use only.

Silver, Ag < 0.002 ug/L U 0.01 0.002 DPC 11/15/2013 15:58 EPA 200.8

Thallium, Tl 0.02 ug/L J 0.05 0.002 DPC 11/15/2013 15:58 EPA 200.8

Tin, Sn < 20 ug/L U 100 20 DAM 11/15/2013 16:06 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 11/15/2013 16:06 EPA 200.7

Zinc, Zn 3.3 ug/L 0.5 0.1 DPC 11/15/2013 15:58 EPA 200.8

Aluminum, Al 1.22 mg/L 0.001 0.0003 DPC 11/15/2013 15:58 EPA 200.8

Boron, B 206 mg/L 0.2 0.04 DAM 11/15/2013 16:06 EPA 200.7

Calcium, Ca 498 mg/L 0.2 0.04 DAM 11/15/2013 16:06 EPA 200.7

Iron, Fe 1.15 mg/L 0.5 0.1 DAM 11/15/2013 16:06 EPA 200.7

Magnesium, Mg 1710 mg/L 0.1 0.02 DAM 11/15/2013 16:06 EPA 200.7

Manganese, Mn 24.3 mg/L 0.005 0.001 DAM 11/15/2013 16:06 EPA 200.7

Potassium, K 126 mg/L 0.5 0.07 DAM 11/15/2013 16:05 EPA 200.7

Sodium, Na 1580 mg/L 0.3 0.08 DAM 11/15/2013 16:05 EPA 200.7

Strontium, Sr 6.83 mg/L 0.01 0.003 DAM 11/15/2013 16:05 EPA 200.7

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 134582 Page 14 of 14