doi:10.25923/s8qq-ac19
2

I. OVERVIEW

A. Cruise Period

This document contains Project Instructions for EX-12-05 Leg I of NOAA Ship Okeanos Explorer’s

exploration of the Blake Ridge and Hatteras Transverse Canyon in the Western Atlantic Ocean. EX-12-

05 Leg 1 operations will commence on July 5, 2012 from Davisville, RI and conclude on July 24, 2012 

in Morehead City, NC. 

B. Operating Area

The operating area for EX-12-05 Leg 1 will be offshore of the US East Coast, from Rhode Island, south 

to the Blake Ridge off the coast of South Carolina (figure. 1). There will be two areas of focused 

exploration during this cruise. The first will be engineering dives conducted in 5,000m of water or 

deeper. The location of these dives is the Hatteras Transverse Canyon, about 200nm ESE of Morehead 

City, NC. Okeanos Explorer will spend approximately three days at Hatteras Transverse Canyon

conducting deepwater testing of the AUV Sentry, and mapping while Sentry is out of the water.

Figure 1: Google Earth map showing overall EX-12-05 Leg 1 operation areas. The white rectangle 

shows the primary project operating area at Blake Ridge. Three days of engineering dives will be 

conducted at Hatteras Transverse Canyon. The blue lines represent State EEZ’s.

Hatteras Transverse 

Canyon
3

Figure 2: Google Earth map showing 

EX-12-05 Leg 1 Hatteras Transverse

Canyon area. Multibeam bathymetry 

from previous Okeanos Explorer cruises 

and US Law of Sea project.

Location Latitude Longitude

NE 34.1790 N -72.4954 W

NW 34.3243 N -72.9165 W

CE 33.6842 N -73.3215 W

CW 33.5820 N -72.8635 W

SW 33.0552 N -73.4027 W

SE 33.0201 N -72.9204 W

Table 1: Bounding box coordinates of the 

Hatteras Transverse Canyon area.

Once engineering dives are completed Okeanos Explorer will transit to the project operating area on the 

Blake Ridge (figures 4-7), approximately 300km off the coast of North and South Carolina. The transit 

will take less than a day from the Hatteras Transverse Canyon area to the Blake Ridge. During transits 

the ship will conduct 24hr mapping operations. The primary operating area at the Blake Ridge will be 

the Blake Ridge Diapir, the Cape Fear Diapir complex and the 800-1000-m isobath (figures 4, 5). 

This area is located entirely within the U.S. Exclusive Economic Zone.

Figure 4. Location of the Blake Ridge Diapir (BRD), the Cape Fear Diapir Complex (CFDC), and the 

1000-m isobaths on the Blake Plateau/Blake Escarpment.

Hatteras Transverse 

Canyon
Multibeam bathymetry has been collected for this area as part of the Law of the Sea Extended 

Continental Shelf Project. Little is known about the seeps in the area of the diapirs and the biological 

communities associated with them. Okeanos Explorer will spend 10-11 days conducting operations 

around the diapirs, related structures, and nearby 1000m isobath, acquiring data with the Sentry AUV, 

EM302 multibeam sonar, EK60 singlebeam sonar, Knudsen sub-bottom profiler and the CTD rosette 

system with in situ sensors. 

Senior Scientist, Cindy Van Dover, will lead a team of students and scientists participating remotely via 

telepresence from the Inner Space Center at the University of Rhode Island during AUV operations in 

the Blake Ridge area. Senior Scientist and core AUV team member, Dana Yoerger, will also participate 

in the cruise from shore via telepresence. Chris German will lead the effort to integrate water column, 

mapping, and sensor data as tools for prospecting for seep environments. This cruise is experimental in 

nature and a component of this cruise includes integrating the Sentry AUV into telepresence-enabled 

exploration.

Figure 5: Google Earth view of study area. 

Box dimension: 50 km x 100 km. Dashed 

line is approximate location of the 1000 m 

isobath; red line is a 25 km target length 

for multibeam mapping.

Point ID Latitude (N) Longitude (W)

OpsSW 32 35' 21.294" N 76 30' 47.105" W

OpsSE 32 23' 54.82" N 76 4' 27.56" W

OpsNE 33 06' 44.28 N 75 43' 57.74" W

OpsNW 33 14' 47.43" N 76 8' 51.1" W

Table 1: Primary Project Operations Area. 

Includes BRD, CFD, unbreached diapirs, 

1000-m isobaths.

Tracking of the Sentry AUV and acquisition of precise navigation data will require Okeanos Explorer to 

remain in relatively close proximity to the vehicle while it is submerged. Simultaneous Sentry AUV and 

hull-mounted sonar mapping operations are not expected. However, if operations allow Okeanos 

Explorer may conduct CTD operations that will not interfere with Sentry’s operations. While Sentry is 

on deck for data download, battery charging and programming, the ship will conduct mapping 

operations, exploring for water column seeps, acquiring sub-bottom profiler data, and adding to 

bathymetry collected by the Extended Continental Shelf Project.

Project activities in the Blake Ridge area will be coordinated with R/V Endeavor, which will be in the 

same region from 16 July to the end of Okeanos Explorer operations. Sentry will be acquiring data in the 
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operating area of both vessels, and scientists onboard R/V Endeavor are interested in getting Sentry data 

from Okeanos Explorer to inform ongoing science operations. Sentry data products will be created by 

shore-side science participants, and e-mailed to R/V Endeavor scientists. No impact to at-sea operations 

are expected.

Upon completion of operations in the Blake Ridge operating area Okeanos Explorer will transit to 

Morehead City, North Carolina. During the transit mapping data will be collected. 

Figure 6: Blake Ridge targets: Blake Ridge 

Diapir (survey area for shipboard Chirp

survey outlined in yellow, small dot is ODP 

hole 996); two unbreached diapirs (small

dots), Cape Fear Diapir and the 1000 m 

contour. Small dots on the Cape Fear Diapir 

are ODP holes 991,992,993.The unbreached 

diapir to the south of the Cape Fear Diapir 

is diapir 1, and the unbreached diapir to the 

north is diapir 2.

Table 3: Key Targets, Blake Plateau

Feature Lat1 Long2 Lat Long

Water 

Depth

Borehole

Depth BSR

BSR

Dept

h

ODP site 996-BRD 

seep

32° 

29.633′

76° 

11.454′

32.4938833

3 76.1909 2170 63 No

BRD depression 1

BRD depression 2 TBD

BRD depression 3

ODP site 991-CFD

32° 

59.018′

75° 

55.801′

32.9836333

3

75.9300166

6 2567 56.6 No

ODP site 992-CFD

32° 

58.542′

75° 

54.961′ 32.9757

75.9160166

7 2587 50.3 No

ODP site 993-CFD

32° 

57.779′

75° 

53.685′ 32.9629833 75.89475 2642 51.9 No

sm subsurface diapir 1 32° 52.35′ 75° 56′ 32.8725 75.93333

lg subsurface diapir 2 33° 05′ 75° 55′

33.0833333

3 75.9166666
6

ODP site 994

31° 

47.141′

75° 

32.751′ 31.785735 75.54585 2808 704 No

ODP site 995

31° 

38.210′

75° 

31.343′ 31.6368333

75.5223833

3 2789 704 Yes 440

ODP site 997

31° 

50.588′

75° 

28.118′

31.8431333

3 75.4686333 2770 750 Yes 464

1000-m isobath 50-km extent, between BRD and CFD

C. Summary of Objectives

The EX-12-05 Leg 1 Sentry AUV cruise represents a partnership between NOAA Okeanos Explorer

Program, National Science Foundation (NSF) and Woods Hole Oceanographic Institution (WHOI) -

with each partner bringing different but complementary objectives to the table. NOAA's Office of 

Ocean Exploration and Research (OER) primary focus during EX-12-05 Leg 1 is to test the use of 

an AUV operated from Okeanos Explorer while the ship is outfitted for "full" exploration mode 

(with joint ROV operations), to explore what it will take to integrate an AUV into telepresenceenabled exploration. NSF and WHOI objectives for this cruise include a series of engineering trials 

and experiments of the Sentry AUV capabilities. NSF objectives for this cruise also include survey 

data collection using the Sentry AUV and Okeanos Explorer systems that will support a follow-on 

NSF-funded project at Blake Ridge in 2013 with Principle Investigator, Cindy Van Dover. 

Engineering Dives at Hatteras Transverse Canyon

Engineering & Operations Objectives:

• Calibrate the Sentry USBL prior to engineering trials (needs to be done early during the 

cruise in 1-3000m of water. Will probably take about 12 hours) 

• Test the ability to operate the Sentry AUV from aboard Okeanos Explorer as if the ship were

in full exploration mode (with joint ROV operations)

• Conduct three days (three dives) of engineering dives with WHOI equipment in deep water 

(5,000-6,000m). See Appendix D for specific engineering objectives

• Test operational and engineering procedures to prepare the Sentry AUV for deployment 

remotely from shore through telepresence

• Train and develop new engineers on use of Sentry

Telepresence Objectives

• Test operational and engineering procedures to prepare the Sentry AUV for deployment 

remotely through telepresence 

• Assess what a standard Sentry AUV product suite might look like for future Okeanos 

Explorer telepresence-enabled cruises

• Test Sentry data and product data sharing and pipeline

• Test use of collaboration tools to share and communicate about the latest cruise datasets

• Collaborate with shore-side scientists to communicate the latest data, discuss findings, and 

plan the next steps of the at-sea operation

• Provide context about ongoing AUV operations to shore-side participants by streaming, e.g. 

the AUV navigation stream to shore as a live video feed.
7

• Test the functional capacity of the URI Inner Space Center to host and support engineering 

objectives for an AUV cruise from Okeanos Explorer

Science Objectives 

• Add science value to engineering dives by engaging interested members of the science 

community, and sharing the data

• Explore Hatteras Transverse Canyon habitats

• Acquire data to look for evidence of mass wasting and sediment transport

Mapping Objectives

• Conduct training of new mapping interns and watchstanders.

• Collect multibeam, singlebeam and subbottom data during transit

• Collect single beam and sub-bottom profiler data of the Hatteras Transverse Canyon and 

surrounding area 

• Test the ability to conduct EM302 multibeam mapping operations while the Sentry AUV is 

on the seafloor

• Add to pre-existing Law of the Sea and Okeanos Explorer bathymetric data coverage in the 

region if possible

• Develop joint mapping products (TBD) with the Sentry AUV team

Data Management Objectives

• Incorporate the Sentry AUV data and products into Okeanos Explorer data workflow for 

sharing with the shore-side science team during the cruise

Operations at Blake Ridge

Telepresence Objectives

• Explore the use of telepresence during AUV operations by streaming AUV data, e.g. 

underwater vehicle data and/or navigation data to shore

• Test use of collaboration tools to share and communicate about the latest cruise datasets

o This may include piping the raw multibeam data to shore

• Collaborate with shore-side scientists to communicate the latest data, discuss findings, and 

plan the next steps of the at-sea operation

• Test the ability for a core AUV team member to successfully participate in an at-sea cruise 

from shore. This objective includes sending large amounts of raw data to shore for 

processing and product development.

• Assess what a standard Sentry AUV product suite might look like for future Okeanos 

Explorer telepresence-enabled cruises

• Test the functional capacity of the URI Inner Space Center to host and support mission 

objectives for an AUV cruise from Okeanos Explorer

• Collect topside video of AUV operations 

Science Objectives 

• Map and explore the diversity of seep habitats of the Blake Ridge Diapir system
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• Reoccupy the Blake Ridge Diapir and investigate temporal stability of subsurface conduits 

by remapping the 2003 grid

• Collect a 100% photomosaic cover of the known Blake Ridge Diapir seep site

• Use photomosaic strip method to test for seep communities at putative seep sites on the 

Blake Ridge Diapir

• Map two additional diapirs for evidence of seepage, with photo ground truth of map targets

• Test the hypothesis that there may be seepage and chemosynthetic communities along the 

800-1000 m isobaths at the boundary of the methane hydrate stability zone using mapping 

and photo ground- truthing of selected targets

• Test efficacy of multiple approaches to localizing seeps (mapping, sensors, images, water 

column plumes, etc)

• Create documentary film of program

Mapping Objectives

• Collect multibeam, singlebeam and subbottom data during transit

• Collect multibeam and subbottom data at the primary project sites, including water-column 

data where appropriate

• Develop joint mapping products (TBD) with the Sentry AUV team

• Assess the Reson 7125 multibeam system for potential integration on the Pheonix ROV or 

another future OER vehicle

• Add to pre-existing Law of the Sea and Okeanos Explorer bathymetric data coverage in the 

region

• Conduct training of new mapping interns and watchstanders

XBT Operations

• During mapping operations, XBT casts will be conducted

CTD Rosette Objectives

• Conduct vertical casts in the primary Blake Ridge operating area to acquire in situ sensor 

data

• Re-establish standard CTD operating procedures on Okeanos Explorer

• Assess what standard CTD and in situ sensor data products OER might consider for the 

future

• Train onboard personnel in CTD rosette operations

Data Management Objectives

• Test data pipeline for daily transfer of raw AUV data to shore for processing and product 

development 

• Incorporate the Sentry AUV data and products into Okeanos Explorer data workflow for 

sharing with the shore-side science team during the cruise

• Incorporate select Sentry data and products into Okeanos Explorer data workflow for postcruise archival

Education & Outreach Objectives

• Develop ship-to-shore education and outreach opportunities (TBD)
9

• Support shore-side artist’s efforts (Philip Brubaker, DUKE)

URI Inner Space Center Objectives

• Support shore-side participation of mission and engineering personnel 

• Explore the engagement and contribution of shore-side participants to at-sea AUV operations 

• Train scientists on how to use online collaboration tools and technologies to conduct remote 

science; develop/refine SOPs

• Ongoing system familiarization and training

• Collect video and still images of shore-side participation

• Host education and outreach efforts as required

D. Participating Institutions 

National Oceanic and Atmospheric Administration (NOAA) - Office of Ocean Exploration and 

Research (OER) - 1315 East-West Hwy, Silver Spring, MD 20910 USA

The National Science Foundation (NSF), 4201 Wilson Boulevard, Arlington, Virginia 22230, USA

phone: (703) 292-5111,

Woods Hole Oceanographic Institute (WHOI), Woods Hole Oceanographic Institution, Woods Hole, 

MA 02543-1541, fax: (508) 457-2163

Duke University Marine Lab, 135 Duke Marine Lab Road, Beaufort, NC 28516 phone: 252.504.7503 

University of Rhode Island (URI), 215 South Ferry Road, Narragansett, RI 02882-1197, USA

University Corporation for Atmospheric Research Joint Office for Science Support (JOSS), PO Box 

3000 Boulder, CO 80307

University of New Hampshire (UNH) - Center for Coastal and Ocean Mapping (CCOM) - Jere A. Chase 

Ocean Engineering Lab, 24 Colovos Road, Durham, NH 03824 USA

Louisiana State University (LSU), Baton Rouge, LA, 70803

E. Personnel (Science Party) 

The experimental nature of this cruise necessitates a compliment of experienced personnel from all the 

mission disciplines. Required mission personnel include an expedition coordinator, mapping leads, 

WHOI’s AUV team, telepresence team, and UCAR ROV support personnel as well as mapping watch 

standers.

Name Affiliation Position M/F Status

1 Kelley Elliott OER Expedition Coordinator F US Citizen

2 Webb Pinner OER Telepresence Lead M US Citizen
10

Table 4: Full list of mission personnel and their affiliation

Shore-side Participants (Location and duration of participation will vary):

3 Elizabeth “Meme”

Lobecker OER CO-Mapping Lead F US Citizen

4 Adam Skarke OER CO-Mapping Lead M US Citizen

5 Laura Brothers USGS Mapping Watchstander

/Scientist F US Citizen

6 Dominique Paxton UCAR Mapping Watchstander F US Citizen

7 Carl Keiser WHOI AUV Team Lead M US Citizen

8 Andrew Billings WHOI AUV Team M US Citizen

9 Justin Fujji WHOI AUV Team M US Citizen

10 Al Duester WHOI AUV Team M US Citizen

11 Brian Bingham UCAR AUV Support M US Citizen

12 Joshua Carlson UCAR AUV Support M US Citizen

13 Lora Van Uffelen UCAR AUV Support F US Citizen

14 Roland Brian UCAR Video Engineer M US Citizen

15 Tara Smithee UCAR Video Team F US Citizen

16 Jay Sheehan UCAR CTD/Survey Technician F US Citizen

17 Brendan Reser OER/NCDDC Data M US Citizen

18

19 LT Laura Gallant OMAO OPS in Training F US Citizen

NAME INSTITUTION ROLE PARTICIPATION DATES

Catalina Martinez OER Regional Manager ECC Coordinator

LTJG Brian 

Kennedy OER Expedition Operations Assistant ECC Coordinator

Kathy Catanach USGS Geologist

Science 

Participant

Location TBD

07/9-

07/11

Rhian Waller U. Maine Marine Biologist

Science 

Participant

Location TBD

07/9-

07/11

Cindy Van Dover Duke 

University

Science Lead/Principle 

Investigator Science Lead 07/11 –07/23

Dana Yoerger WHOI Senior Scientist/AUV Team AUV Team

James Kinsey WHOI AUV Team AUV Team

Chris German WHOI Senior Scientist Senior Scientist 07/11 –

07/23

Megumi Shimizu Duke Biologist (PhD Student, 3rd 

year)

Science 

Participant

07/11 –

07/23

Jamie Wagner Duke Biologist (PhD Student, 1st 

Year)

Science 

Participant

07/11 –

07/23
11

Table 5: List of expected shore-side science participants working out of the URI ISC, 

collaborating via intercom, ftp data sharing and teleconferences.

 

F. Administrative 

Key Points of Contact:

Ship Operations

Marine Operations Center, Atlantic (MOA)

439 West York Street

Norfolk, VA 23510-1145

Telephone: (757) 441-6776

Fax: (757) 441-6495

Chief, Operations Division, Atlantic (MOA)

LCDR Jason Appler

Telephone: (757) 441-6716

E-mail: ChiefOps.MOA@noaa.gov

Mission Operations

Kelley Elliott, Expedition Coordinator

NOAA Ocean Exploration and Research

Phone: (301) 734-1024/ (703) 927-5449

Email: Kelley.Elliott@noaa.gov

John McDonough, Deputy Director

NOAA Ocean Exploration & Research

Phone: 301-734-1023 / 240-676-5206

E-mail: John.McDonough@noaa.gov

CDR Robert Kamphaus, Commanding Officer

NOAA Ship Okeanos Explorer

Phone: (401) 378-8284

Email: CO.Explorer@noaa.gov

LT Megan Nadeau, Operations Officer

NOAA Ship Okeanos Explorer

Phone: (401) 932-4114 (o)/ (207) 240-0957 (c)

E-mail: Ops.Explorer@noaa.gov

Other Mission Contacts

Zachary 

McKelvey Duke Undergraduate Duke Bookout Scholar

Science 

Participant

07/11 –

07/23

Molly Mc Entee Duke Undergraduate Duke 

Bookout Scholar

Science 

Participant

07/11 –

07/23

Stephanie 

Sharuga LSU Guest Masters Student Science Participant

07/11 –

07/23

Philip Brubaker Duke Graduate Student, MFA Artist (Doc Film) 07/11 –

07/23

David Mindell WHOI Scientist/Engineer Science/Engineer

ing Participant

(David’s student) WHOI Student/Engineer Science/Engineer

ing Participant

Catalina Martinez, Regional Manager

NOAA Office of Ocean Exploration & Research

Phone: (401) 874-6250 (o) / (401) 330-9662 (c)

LCDR Nicola VerPlanck, Deputy EX Program 

Manager

NOAA Ocean Exploration & Research
12

G. Diplomatic Clearances

NOT APPLICABLE TO THIS CRUISE

H. Shipments

The AUV transducer pole will be delivered by WHOI personnel the week before the cruise (week of 25 

June 2012) for assembly and installation. Two (2) twenty foot containers from WHOI will be delivered 

to North Kingstown, RI for loading; a work van with reported weight of 14,000 lbs and a secondary van 

with a weight of 12,000 lbs. Container weights must be verified by certified scales or calibrated 

dynamometer at/prior to time of loading. 

Both containers will be offloaded in Morehead City, NC and shipped to Senty’s next project.

I. Licenses and Permits

See appendix C for categorical exclusion documentation

II. OPERATIONS

A. Cruise Plan Itinerary (All times and dates are subject to prevailing conditions and the 

discretion of the Commanding Officer). See figures 5 and 6 for reference.

Date Operations Remarks

July 2, 2012 Staging /loading Sentry 

containers at Davisville, RI

Crane barge arranged

July 5, 2012 Depart Davisville, RI 1300 departure time.

12 hr Steam to USBL 

calibration site

39° 33.654'N, 71° 

2.779'W approx.

July 5, 2012 ~0100 arrive USBL cal. Site Deck dept. not required.

July 5/6, 2012 Conduct Sentry USBL 

calibration in ~2-3000m

About 12 hours. Beacon 

pick-up needs to occur 

during daylight hours.

Email: Catalina.Martinez@noaa.gov

Elizabeth “Meme” Lobecker CO-Lead

NOAA Office of Ocean Exploration

and Research (ERT, Inc.)

Phone: (401) 662-9297/ (603)377-6319

E-mail: elizabeth.lobecker@noaa.gov

Dave Lovalvo, ROV Program Manager

Eastern Oceanics

Phone: 203-246-5531

Email: David.Lovalvo@noaa.gov

Phone: 206-526-4801

E-mail: Nicola.Verplanck@noaa.gov

Webb Pinner, Telepresence Lead

NOAA Office of Ocean Exploration & Research

Phone: (401) 874-6250 (o) / (401) 330-9662 (c)

Email: Webb.Pinner@noaa.gov

Adam Skarke, Mapping CO-Lead

NOAA Ocean Exploration & Research 

Phone: 603-862-0369/ 302-981-9908

E-mail: Adam.Skarke@noaa.gov
13

July 6, 2012 Recover USBL cal. equip. Anytime from 0600-1000, 

depending on calibration 

success.

July 6, 2012 Depart for Hatteras Transverse 

Canyon by ~1500

There will be a NOC 

network outage in Silver 

Spring from 9pm to 9am 

Eastern.

July 9, 2012 Arrive Hatteras Transverse 

Canyon ~0900

Commence engineering 

dives

July 9-11, 2012 Hatteras Transverse Canyon –

Engineering Dives

Three AUV dives; 

Okeanos mapping 

operations while AUV is 

on surface/charging

July 11, 2012 Depart from Hatteras 

Transverse Canyon by ~1800

Begin transit to Blake 

Ridge

July 12, 2012 Arrive Blake Ridge Op Area by 

~1200

Commence AUV 

Operations

July 13, 2012 Blake Ridge Diapir AUV: Multibeam/SSS 

data

Blake Ridge Diapir – Diapir 2 Ship: Multibeam, 

Singlebeam & SBP data. 

July 14, 2012 Blake Ridge Diapir, Seep 

Location

AUV: Photo data

Ship: CTD Cast

Blake Ridge, Diapir 2 Ship: Multibeam, 

Singlebeam & SBPdata 

transect

July 15, 2012 Blake Ridge, Pockmarks AUV: Photo data

Ship: CTD Cast

Blake Ridge, Diapir 2 Ship: Multibeam, 

Singlebeam & SBP data 

transect

July 16, 2012 Blake Ridge, Pockmarks AUV: Photo data

Ship: CTD Cast

Blake Ridge, Diapir 2 Ship: Multibeam, 

Singlebeam & SBP data 

transect

July 17, 2012 Blake Ridge, Pockmarks AUV: Photo data

Ship: CTD Cast

Blake Ridge, Diapir 1 Ship: Multibeam, 

Singlebeam & SBP data 

transect

July 18, 2012 Transect across 3 diapirs AUV: Multibeam/SSS

Ship: Multibeam/SBP 

Cape Fear Diapir Ship: Multibeam, 

Singlebeam & SBP data 
14

transect

July 19, 2012 Diapir 1 AUV: Multibeam

Ship: Multibeam, 

Singlebeam & SBP

AUV: Photo

Ship: CTD casts

Diapir 2 Ship: Multibeam, 

Singlebeam & SBP

July 20, 2012 Diapir 1 AUV: Photo

Ship: CTD casts

Cape Fear Slide Ship: Multibeam, 

Singlebeam & SBP

July 21, 2012 Diapir 2 Ship: Multibeam, 

Singlebeam & SBP

AUV: Multibeam

Ship: Multibeam, 

Singlebeam & SBP 

AUV: Photo

Ship: CTD casts

Cape Fear Slide Ship: Multibeam, 

Singlebeam & SBP

July 22, 2012 Cape Fear Diapir AUV: Multibeam

Ship: Multibeam, 

Singlebeam &SBP

AUV: Photo

Ship: CTD casts

Criss-cross 800m isobath Ship: Multibeam, 

Singlebeam & SBP

AUV: Charging

July 23, 2012 Criss-cross 800m isobath AUV: Multibeam/SSS

Ship: Multibeam, 

Singlebeam &SBP

(if time allows) Ship: Multibeam, 

Singlebeam & SBP

AUV: Charging

Depart Blake Ridge Op Area 12 hour return transit

July 24, 2012 Arrive Morehead City, NC (The ship usually pulls 

into port in the morning)

July 25, 2012 Sentry AUV de-staging; 

departure of Mission Personnel

Table 6: Details about operations from 05 July – 24 July, 2012 

B. Telepresence Events
15

A joint telepresence event with E/V Nautilus, the University of Rhode Island and Inner Space Center 

may take place the week of July 16, 2012.

C. In-Port Events

No port events are anticipated at this time. EX-12-05 Leg 1 Duke Marine Lab scientists will likely visit 

the ship on July 25, 2012.

D. Staging and Destaging

Bringing the Sentry AUV and related equipment onboard the ship brings with it a number of staging 

requirements, including loading two 20' vans.

MOBILIZATION

Date Operations Remarks

June 13th Block/winch wire to be 

taken down.

The A-Frame block with the winch wire will be taken down

by ship crew and Webb Pinner

June 21st or 22nd Transducer pole 

welding

Welding operations to make some changes to the ship in 

preparation for the transducer pole installation are desired in 

advance of the installation.

June 25 Transducer pole 

installation

Andy Bowen and one other person to arrive from WHOI to 

put the pole in place establish protocol for lowering and 

raising it. 

- The transducer will NOT actually be installed.

- No hot work is necessary if welding conducted prior

July 2nd Offloading and loading

of ROV and AUV 

containers

- Sentry team arrives in Davisville, RI

- ROV container to be offloaded

- AUV containers to arrive in the morning on a truck and be 

loaded onto the O-2 deck of the ship

- Crane arrangements are being arranged by WHOI

- One of these vans will need 450 VAC 3 phase, to be 

connected via an un-terminated cable.

July 3rd Mission personnel 

conduct cruise 

preparations

- Ensure CET, Webb Pinner and someone from the deck 

department is available. The Sentry team will want help with 

networking.

July 4th Sentry team conduct

cruise preparations

Ship crew rest day

Sentry team may use this day to build out network 

infrastructure and conduct testing. Need access to the ship, 

not support.

July 5th Ship departs From Davisville, RI

DE-MOBILIZATION

Date Operations Remarks

July 24th Ship arrives To Morehead City, NC
16

July 25th AUV containers taken off the 

ship

- Sentry AUV team to make crane arrangements for this

- Need to arrange parking the containers at the port for a 

week or so, or seeing if the NOAA facility in Seattle, WA 

will allow storage prior to follow-on Sentry cruise.

- Mission personnel depart ship

E. Sonar Operations 

Mapping Operations

EM 302, EK 60, and Knudsen sub-bottom data acquisition are planned for this cruise. The mapping 

team will ensure that all the standard protocols are accomplished as laid out by the Commanding 

Officer. Mapping lead directives will be followed for efficient and safe mapping operations. The

Knudsen sub-bottom profiler is anticipated to be operated during the day time (1000-1600) at minimum 

power level settings (Power level at 1) and lowest possible pulse length setting (1-4 ms). XBTs will be 

conducted every 2-4 hours, or less/more often as necessary to maintain multibeam data quality. Okeanos 

Explorer hull mounted multibeam sonar may cause interference with Sentry’s multibeam therefore the 

two systems cannot be in operation simultaneously. 

Mapping data from Sentry’s Reson 7125 multibeam sonar will also be collected. The AUV data will be 

processed and cleaned by WHOI personnel during the cruise. 

F. SCUBA Dive Plan 

NOT APPLICABLE TO THIS CRUISE

G. Applicable Restrictions 

NOT APPLICABLE TO THIS CRUISE

III. EQUIPMENT

A. Equipment and capabilities provided by the ship 

• Kongsberg Simrad EM 302 Multibeam Echosounder (MBES)

• Kongsberg Simrad EK 60 Singlebeam Echosounder

• Knudsen Chirp 3260 Sub-bottom profiler (SBP)

• LHM Sippican XBT (various probes)

• Seabird SBE 911Plus CTD

• Seabird SBE 32 Carousel and 24 2.5 L Niskin Bottles 

• CNAV GPS

• POS/MV

• Seabird SBE-45 (Micro TSG)

• Reson SVP-70

• Kongsberg Dynamic Positioning-1 System
17

• NetApps mapping storage system

• CARIS HIPS Software

• IVS Fledermaus Software

• SIS Software

• Hypack Software

• Scientific Computing System (SCS)

• ECDIS

• Met/Wx Sensor Package

• Cruise Information Management System (CIMS)

• High Speed VSAT (10 mbps ship-to-shore; T1 shore-to-ship)

B. Equipment and capabilities provided by the scientists 

• Sentry AUV

• Sonardyne USBL System

IV. HAZARDOUS MATERIALS

A. Policy and Compliance

All HAZMAT brought aboard by visiting scientists for EX1205 operations will comply with DMS, 

Fleet Environmental Compliance #07, Hazardous Material and Hazardous Waste Management 

Requirements for Visiting Scientists, released July 2002.

Hazardous Materials (HAZMAT) Anticipated to be brought aboard by mission personnel

• Ultralife Lithium Power Cell

• Epoxy Resin

• Super Glue

• G5 Adhesive

• Silicone Sealant

• Braycote Micronic hydrolic oil

• Silikroil lubricant (aerosol)

• Scotchkote brand electrical coating 

Neutralizing agents, buffers and/or absorbents required for HAZMAT

See appendix D for HAZMAT material safety data sheets (MSDS).

Guest scientists and the Expedition Coordinator are responsible for ensuring the HAZMAT are 

listed, packaged, labeled and transported in compliance with DOT regulations

A. Radioactive Isotopes 

NOT APPLICABLE TO THIS CRUISE

B. Inventory 
18

NOT APPLICABLE TO THIS CRUISE

V. ADDITIONAL PROJECTS

A. Supplementary Projects

NOT APPLICABLE TO THIS CRUISE

B. NOAA Fleet Ancillary Projects

NOT APPLICABLE TO THIS CRUISE

VI. DISPOSITION OF DATA AND REPORTS

A. Data Responsibilities 

All data acquired on Okeanos Explorer will be provided to the public archives without proprietary 

rights. All data management activities shall be executed in accordance with NAO 212-15, Management 

of Environmental and Geospatial Data and Information

[http://www.corporateservices.noaa.gov/ames/NAOs/Chap_212/naos_212_15.html].

Ship Responsibilities

The Commanding Officer is responsible for all data collected for missions until those data have been 

transferred to mission party designees. Data transfers will be documented on NOAA Form 61-29. 

Reporting and sending copies of project data to NESDIS (ROSCOP form) is the responsibility of 

OER.

NOAA OER Responsibilities

The Expedition Coordinator will work with Okeanos Explorer Operations Officer to ensure data 

pipeline protocols are followed for final archive of all data acquired on the EX without proprietary 

rights. 

Deliverables

a. At sea

• Daily plans of the Day (POD)

• Daily situation reports (SITREPS)

• Daily summary bathymetry data files

b. Post cruise

• Refined SOPs for all pertinent operational activities

• Assessments of all activities

c. Science

• Multibeam and XBT raw and processed data (see appendix B for the formal cruise data 

management plan)

• Mapping data report

• AUV collected sonar raw and processed data
19

• AUV still images

Archive

• The Program and ship will work together to ensure documentation and

 stewardship of acquired data sets in accordance with NAO 212-15. The Cruise Information 

Management System is the primary tool used to accomplish this activity.

B. Pre and Post Cruise Meeting 

Pre-Cruise Meeting

Prior to departure, the Operation’s Officer will conduct a meeting of the scientific party to inform them 

of cruise objectives and vessel protocols, e.g., meals, watches, etiquette, etc.

Post-Cruise Meeting

Upon completion of the cruise, a meeting will be held by the Operation’s Officer and attended by the 

ship’s Survey Technicians, the Expedition Coordinator and members of the scientific party to review the 

cruise. Concerns regarding safety, efficiency, and suggestions for improvements for future cruises 

should be discussed. 

Shipboard Meetings

Daily Operations Briefing meetings will be held at 1500 in the forward lounge to review the current day, 

and define operations, associated requirements and staffing needs for the following day. A Plan of the 

Day (POD) will be posted each evening for the next day in specified locations throughout the ship. A 

safety brief and overview of POD will occur on the Bridge each morning at 0800. Daily Situation 

Reports (SITREPS) will be posted as well and shared daily through e-mail and/or the EX PLONE site (

http://tethys.gso.uri.edu/OkeanosExplorerPortal ) and/or Okeanos Explorer FTP site.

C. Ship Operation Evaluation Report 

Within seven days of the completion of the cruise, a Ship Operation Evaluation form is to be completed 

by the Expedition Coordinator and lead scientist. The preferred method of transmittal of this form is via 

email to OMAO.Customer.Satisfaction@noaa.gov. If email is not an option, a hard copy may be 

forwarded to:

Director, NOAA Marine and Aviation Operations

NOAA Office of Marine and Aviation Operations

8403 Colesville Road, Suite 500

Silver Spring, MD 20910

VII. MISCELLANEOUS

A. Meals and Berthing 
20

Meals and berthing are required for up to 19 scientists. Meals will be served 3 times daily beginning one 

hour before scheduled departure, extending throughout the cruise, and ending two hours after the 

termination of the cruise. Since the watch schedule is split between day and night, the night watch may 

often miss daytime meals and will require adequate food and beverages (for example a variety of 

sandwich items, cheeses, fruit, milk, juices) during what are not typically meal hours. Special dietary 

requirements for scientific participants will be made available to the ship’s command at least twenty-one

days prior to the survey (e.g., Expedition Coordinator is allergic to fin fish). Berthing requirements, 

including number and gender of the scientific party, will be provided to the ship by the Expedition 

Coordinator. The Expedition Coordinator and Operations Officer will work together on a detailed 

berthing plan to accommodate the gender mix of the scientific party taking into consideration the current 

make-up of the ship’s complement. The Expedition Coordinator is responsible for ensuring the scientific 

berthing spaces are left in the condition in which they were received; for stripping bedding and linen 

return; and for the return of any room keys which were issued. The Expedition Coordinator is also 

responsible for the cleanliness of the laboratory spaces and the storage areas utilized by the scientific 

party, both during the cruise and at its conclusion prior to departing the ship.

All NOAA scientists will have proper travel orders when assigned to any NOAA ship. The Expedition 

Coordinator will ensure that all non NOAA or non Federal scientists aboard also have proper orders. It is 

the responsibility of the Expedition Coordinator to ensure that the entire scientific party has a 

mechanism in place to provide lodging and food and to be reimbursed for these costs in the event that 

the ship becomes uninhabitable and/or the galley is closed during any part of the scheduled project. 

All persons boarding NOAA vessels give implied consent to comply with all safety and security policies 

and regulations which are administered by the Commanding Officer. All spaces and equipment on the 

vessel are subject to inspection or search at any time. All personnel must comply with OMAO's Drug 

and Alcohol Policy dated May 7, 1999 which forbids the possession and/or use of illegal drugs and 

alcohol aboard NOAA Vessels.

B. Medical Forms and Emergency Contacts 

The NOAA Health Services Questionnaire (NHSQ, Revised: 02 JAN 2012) must be completed in 

advance by each participating scientist. The NHSQ can be obtained from the Expedition Coordinator or 

the NOAA website at NOAA Health Services Questionnaire. The completed form should be sent to the 

Regional Director of Health Services at Marine Operations Center. The participant can mail, fax, or scan 

the form into an email using the contact information below. The NHSQ should reach the Health Services 

Office no later than 4 weeks prior to the cruise to allow time for the participant to obtain and submit 

additional information that health services might require before clearance to sail can be granted. Please 

contact MOC Health Services with any questions regarding eligibility or completion of the NHSQ. Be 

sure to include proof of tuberculosis (TB) testing, sign and date the form, and indicate the ship or ships 

the participant will be sailing on. Clearances are valid for 2 years for personnel under age 50 and 1 year 

for age 50 and over. All PPD’s expire after one year from the date of administration. The participant will 

receive an email notice when medically cleared to sail if a legible email address is provided on the 

NHSQ. 

Contact information:
21

Regional Director of Health Services

Marine Operations Center – Atlantic

439 W. York Street

Norfolk, VA 23510

Telephone 757.441.6320

Fax 757.441.3760

E-mail: MOA.Health.Services@noaa.gov

Please make sure the medical.explorer@noaa.gov email address is cc’d on all medical correspondence.

Prior to departure, the Expedition Coordinator must provide a listing of emergency contacts to the 

Operations Officer for all members of the scientific party, with the following information: name, 

address, relationship to member, and telephone number.

Emergency contact form is included as Appendix A.

C. Shipboard Safety 

Wearing open-toed footwear or shoes that do not completely enclose the foot (such as sandals or clogs) 

outside of private berthing areas is not permitted. Steel-toed shoes are required to participate in any 

work dealing with suspended loads, including CTD deployments and recovery. The ship does not 

provide steel-toed boots. Hard hats are also required when working with suspended loads. Work vests 

are required when working near open railings and during small boat launch and recovery operations. 

Hard hats and work vests will be provided by the ship when required.

Operational Risk Management: For every operation to be conducted aboard the ship (NOAA-wide 

initiative), risk management procedures will be followed. For each operation, risks will be identified and 

assessed for probability and severity. Risk mitigation strategies / measures will be investigated and 

implemented where possible. After mitigation, the residual risk will have to be assessed to make Go-No 

Go decisions for the operations. Particularly with new operations, risk assessment will be ongoing and 

updated as necessary. This applies to over-the-side operations andto everyday tasks aboard the vessel 

that pose risk to personnel and property. 

• CTD, ROV (and other pertinent) ORM documents will be followed by all personnel 

working on board the EX.

• All personnel on board are in the position of calling a halt to operations/activities in the 

event of a safety concern.

D. Communications 

A daily situation report (SITREP) on operations prepared by the Expedition Coordinator will be relayed 

to the program office. Sometimes it is necessary for the Expedition Coordinator to communicate with 

another vessel, aircraft, or shore facility. Through various modes of communication, the ship is able to 

maintain contact with the Marine Operations Center on an as needed basis. These methods will be made 

available to the Expedition Coordinator upon request, in order to conduct official business. The ship’s 

primary means of communication with the Marine Operations Center is via e-mail and the Very Small 
22

Aperture Terminal (VSAT) link. Standard VSAT bandwidth at 128kbs is shared by all vessels staff and 

the science team at no charge. Increased bandwidth in 30 day increments is available on the VSAT 

systems at increased cost to the scientific party. If increased bandwidth is being considered, program 

accounting is required it must be arranged at least 30 days in advance.

Specific information on how to contact NOAA Ship Okeanos Explorer and all other fleet vessels can be 

found at: http://www.moc.noaa.gov/phone.htm

Important Telephone and Facsimile Numbers and E-mail Addresses

Ocean Exploration and Research (OER):

OER Program Administration:

Phone: (301) 734-1010

Fax: (301) 713-4252 

E-mail: Firstname.Lastname@noaa.gov

University of New Hampshire, Center for Coastal and Ocean Mapping

Phone: (603) 862-3438

Fax: (603) 862-0839

University of Rhode Island, Innerspace Center

Phone: (401) 874-6158

Email: innerspacecenter@gmail.com

NOAA Ship Okeanos Explorer - Telephone methods listed in order of increasing expense:

EX Cellular: (401) 378-7947

EX Iridium: (808) 659-9179

OER Mission Iridium (dry lab): (808) 851-3827

EX INMARSAT B

Line 1: 011-872-764-852-328

Line 2: 011-872-764-852-329

 Voice Over IP (VoIP) Phone: 

301-713-7772 (expect a delay once picked up by directory)

E-Mail: Ops.Explorer@noaa.gov - (mention the person’s name in SUBJECT field)

expeditioncoordinator.explorer@noaa.gov - For dissemination of all hands emails by Expedition 

Coordinator while on board. See ET for password.

E. IT Security

Any computer that will be hooked into the ship's network must comply with the NMAO Fleet IT 
23

Security Policy prior to establishing a direct connection to the NOAA WAN. Requirements include, but 

are not limited to:

1. Installation of the latest virus definition (.DAT) file on all systems and performance of a virus 

scan on each system. 

2. Installation of the latest critical operating system security patches. 

3. No external public Internet Service Provider (ISP) connections. 

Completion of these requirements prior to boarding the ship is required.

Non-NOAA personnel using the ship's computers or connecting their own computers to the ship's 

network must complete NOAA’s IT Security Awareness Course within 3 days of embarking.

F. Foreign National Guests Access to OMAO Facilities and Platforms 

NOT APPLICABLE TO THIS CRUISE

No Foreign National Guests are expected for this Cruise.

All foreign national access to the vessel shall be in accordance with NAO 207-12 and RADM De Bow’s 

March 16, 2006 memo. 

The following are basic requirements. Full compliance with NAO 207-12 is required.

Responsibilities of the Expedition Coordinator: 

1. Provide the Commanding Officer with the e-mail generated by the FRNS granting approval for 

the foreign national guest’s visit. This e-mail will identify the guest’s DSN and will serve as 

evidence that the requirements of NAO 207-12 have been complied with. 

2. Escorts – The Expedition Coordinator is responsible to provide escorts to comply with NAO 

207-12 Section 5.10, or as required by the vessel’s DOC/OSY Regional Security Officer. Ensure 

all non-foreign national members of the scientific party receive the briefing on Espionage 

Indicators (NAO 207-12) at least annually or as required by the servicing Regional Security 

Officer. 

3. Export Control - The NEFSC currently neither possesses nor utilizes technologies that are 

subject to Export Administration Regulations (EAR). 

The Commanding Officer and the Expedition Coordinator will work together to implement any 

access controls necessary to ensure no unlicensed export occurs of any controlled technology 

onboard regardless of ownership.

Responsibilities of the Commanding Officer:

1. Ensure only those foreign nationals with DOC/OSY clearance are granted access. 

2. Deny access to OMAO platforms and facilities by foreign nationals from countries controlled for 

anti-terrorism (AT) reasons and individuals from Cuba or Iran without written NMAO approval 

and compliance with export and sanction regulations. 
24

3. Ensure foreign national access is permitted only if unlicensed deemed export is not likely to 

occur. 

4. Ensure receipt from the Expedition Coordinator or the DSN of the FRNS e-mail granting 

approval for the foreign national guest’s visit. 

5. Ensure Foreign Port Officials, e.g., Pilots, immigration officials, receive escorted access in 

accordance with maritime custom to facilitate the vessel’s visit to foreign ports. 

6. Export Control - 8 weeks in advance of the cruise, provide the Expedition Coordinator with a 

current inventory of OMAO controlled technology onboard the vessel and a copy of the vessel 

Technology Access Control Plan (TACP). Also notify the Expedition Coordinator of any 

OMAO-sponsored foreign nationals that will be onboard while program equipment is aboard so 

that the Expedition Coordinator can take steps to prevent unlicensed export of Program 

controlled technology. The Commanding Officer and the Expedition Coordinator will work 

together to implement any access controls necessary to ensure no unlicensed export occurs of 

any controlled technology onboard regardless of ownership. 

7. Ensure all OMAO personnel onboard receive the briefing on Espionage Indicators (NAO 207-

12) at least annually or as required by the servicing Regional Security Officer. 

Responsibilities of the Foreign National Sponsor:

1. Export Control - The foreign national’s sponsor is responsible for obtaining any required export 

licenses and complying with any conditions of those licenses prior to the foreign national being 

provided access to the controlled technology onboard regardless of the technology’s ownership. 

2. The DSN of the foreign national shall assign an on-board Program individual, who will be 

responsible for the foreign national while on board. The identified individual must be a U.S. 

citizen, NOAA (or DOC) employee. According to DOC/OSY, this requirement cannot be 

altered. 

3. Ensure completion and submission of the Certification of Conditions and Responsibilities for a 

Foreign National Guest as required by NAO 207-12 Section 5.03.h. 
25

Appendix A

EMERGENCY DATA SHEET

NOAA OKEANOS EXPLORER

PRINT CLEARLY 

NAME: __________________________________________________________

(Last, First, Middle)

Mailing Address ____________________________________________________

 _____________________________________________________

 _____________________________________________________

(Other than the ship address)

Phone (Home) _________________________________________________________

 (Cell) ___________________________________________________________

Date of Birth ___________________________________________________________

Email Address:__________________________________________________________

Emergency Contact: _____________________________________________________

(Name and Relationship)

Address: ______________________________________________________________

 ______________________________________________________________

 _______________________________________________________________

Phone (Home) ____________________________________________________

(Work) ____________________________________________________

(Cell) _____________________________________________________

E.C. Email: ________________________________________________________________

Signature __________________________________ Date _______________________
26

Appendix B: EX-12-05 Leg I Data Management Plan

All data collected during this expedition will be archived at the National Geophysical Data Center 

(NGDC) in accordance with the NOAA / OER data management protocols. Detailed data management 

plans are being developed currently and will be provided to the ship by end of the expedition. 
27

Appendix C: 
28

Appendix D: 

EX-12-05 Leg 1 Cruise Engineering Test Plans

Sentry AUV

1. Dive 1: - Misc Testing (5000 – 6000m of water)

1.1. Thruster and Servo test in deep water – drive in a straight line with close bottom following and make a 

couple of large altitude changes

1.2. Speed verification – benchmark the speed of the vehicle in deep water and with drag improvements. 

Make reciprocal lines at [0.5:0.1:1.0] m/s. Use current spy channels to collect data regarding power 

consumed 

1.3. Benchmark USBL performance – collect cross correlations and SNR’s from the avtrack regularly on the 

vehicle

1.4. Sidescan/SBP cold start test – leave the SSS and SBP off on the launch and descent, use mission 

controller directives to turn it on and run a short sidescan survey first at 30m then at 5m. Turn the 

SSS/SBP back off – can make this a science targeted block Science opportunity for 1-2 sq km of sidescan 

coverage

1.5. Reson Cold start test – leave the Reson off at launch. Use a mission controller directive to turn the 

reson on, the reson configurator to set it up, and run a short survey. – can make this a science targeted 

block – Science opportunity for ~ 1sq km of multibeam coverage

1.6. Strobe test – test new strobe and see what light distribution looks like in deep water – Science 

opportunity for ~100m square of photo coverage

1.7. SVP probe test – Run the SVP and log the data, do not do anything with it yet.

1.8. WHOI Acomms – run the WHOI acomms and attempt to communicate two ways with the vehicle. Log 

performance statistics to find out how solid communication is

1.9. NAVEST test – run an additional version of navest on the vehicle in neutered mode.

1.10. EH sensor checkout – check the correct polarity of the EH probe

2. Dive 2 – Remote Ops – See “Remote Operations and Visualization Plan for the VanDover Okeanos Explorer 

Cruise” in separate document Water depth TBD

2.1. Retest Strobe if necessary

2.2. Secondary Avtrack test – add an additional avtrack to the vehicle on isolated RS-232 only. Collect cross 

correlation and SNR data and compare it to fully integrated Avtrack logs for the same dive.

2.3. Most of the dive is available for science, but there are some tight parameters. I would like to discuss 

this over the phone.

3. Dive 3 – Additional Testing (5000 – 6000m of water)

3.1. Imaging Cold start test – use mission directives to start the camera, imaging stack, and strobe from cold 

and take pictures in a science selected block Science opportunity for approximately 100m square of 

photo coverage

3.2. SVP full integration – plumb the SVP fully into the data pipeline and use it to make a multibeam map of 

a science selected target. – Science opportunity for 1 – 2 square km of multibeam map but it must be 

on a slope that gives at least 300 – 400m of vertical relief and more if possible.

3.3. Test “Hover” flight mode – put the vehicle into “ROV” mode and make small square transects about a 

fixed point. Start with 0.3m/x and gradually decrease speed and leg length to see how tightly we can 

hold station before we go unstable. 

3.4. Test out Steve Martin “Vane Mode” – see if we can get the vehicle to hold in a fixed spot

3.5. LBL and XR tests to be determined.

3.6. Likely to be some science flex time at the end of this one
29

Appendix D: 

MSDS Sheets
MATERIAL SAFETY 3M

DATA SHEET 3M Center

 St. Paul, Minnesota

 55144-1000

 1-800-364-3577 or (651) 737-6501 (24 hours)

 Copyright, 2001, Minnesota Mining and Manufacturing Company.

 All rights reserved. Copying and/or downloading of this

 information for the purpose of properly utilizing 3M products

 is allowed provided that:

 1) the information is copied in full with no changes unless

 prior agreement is obtained from 3M, and

 2) neither the copy nor the original is resold or otherwise

 distributed with the intention of earning a profit thereon.

DIVISION: ELECTRICAL PRODUCTS DIVISION

TRADE NAME:

 SCOTCHKOTE BRAND ELECTRICAL COATING

ID NUMBER/U.P.C.:

 80-6107-3307-5 00-54007-14853-1 80-6112-0519-8 00-54007-43906-6

 CS-0406-0592-8 - - -

ISSUED: November 27, 2001

SUPERSEDES: October 24, 2000

DOCUMENT: 10-2644-2

-----------------------------------------------------------------------------

 1. INGREDIENT C.A.S. NO. PERCENT

-----------------------------------------------------------------------------

ACETONE................................. 67-64-1 40.0 - 45.0

METHYL ETHYL KETONE..................... 78-93-3 12.0 - 15.0

TOLUENE................................. 108-88-3 12.0 - 15.0

ACRYLONITRILE-BUTADIENE POLYMER......... 9003-18-3 10.0 - 15.0

PHENOL-FORMALDEHYDE RESIN............... 25085-50-1 3.0 - 7.0

GLYCEROL ESTERS OF ROSIN ACIDS.......... 8050-31-5 3.0 - 7.0

SALICYLIC ACID.......................... 69-72-7 1.0 - 2.0

ZINC OXIDE.............................. 1314-13-2 1.0 - 2.0

ANTIOXIDANT............................. 68411-46-1 0.1 - 1.0

 IN CASE OF EMERGENCY: THE NUMBERS AT THE TOP OF THIS PAGE PROVIDE 24

 HOUR RESPONSE FROM ANY PHONE FOR ALL EMERGENCIES WITH THIS PRODUCT.

 The components of this product are in compliance with the chemical

 notification requirements of TSCA.

 All ingredients on TSCA; EINECS; CDSL

This product contains the following toxic chemical or chemicals subject to

the reporting requirements of Section 313 of Title III of the Emergency

Planning and Community Right-To-Know Act of 1986 and 40 CFR Part 372:

 METHYL ETHYL KETONE

 TOLUENE

 ZINC OXIDE

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 2

-----------------------------------------------------------------------------

 2. PHYSICAL DATA

-----------------------------------------------------------------------------

BOILING POINT:................. 56.5C

VAPOR PRESSURE:................ 229 mm Hg @25C

VAPOR DENSITY:................. 2.00

EVAPORATION RATE:.............. N/D

SOLUBILITY IN WATER:........... Nil

SPECIFIC GRAVITY:.............. 0.88

PERCENT VOLATILE:.............. 75

pH:............................ N/A

VISCOSITY:..................... 325cps

MELTING POINT:................. N/D

APPEARANCE AND ODOR:

 Liquid, Brown, solvent odor

-----------------------------------------------------------------------------

 3. FIRE AND EXPLOSION HAZARD DATA

-----------------------------------------------------------------------------

FLASH POINT:................... 0F Closed Cup

FLAMMABLE LIMITS - LEL:........ 2.15%

FLAMMABLE LIMITS - UEL:........ 13.0%

AUTOIGNITION TEMPERATURE:...... N/D

EXTINGUISHING MEDIA:

 Carbon dioxide, Dry chemical, Foam

SPECIAL FIRE FIGHTING PROCEDURES:

 Wear full protective clothing, including helmet, self-contained,

 positive pressure or pressure demand breathing apparatus, bunker coat

 and pants, bands around arms, waist and legs, face mask, and

 protective covering for exposed areas of the head.

UNUSUAL FIRE AND EXPLOSION HAZARDS:

 Vapors may travel long distances along the ground or floor to an

 ignition source and flash back.

NFPA HAZARD CODES: HEALTH: 2 FIRE: 3 REACTIVITY: 0

 UNUSUAL REACTION HAZARD: none

OSHA FIRE HAZARD CLASS: Class IB Flammable Liquid

-----------------------------------------------------------------------------

 4. REACTIVITY DATA

-----------------------------------------------------------------------------

STABILITY: Stable

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 3

-----------------------------------------------------------------------------

 4. REACTIVITY DATA (continued)

-----------------------------------------------------------------------------

INCOMPATIBILITY - MATERIALS/CONDITIONS TO AVOID:

 None known.

HAZARDOUS POLYMERIZATION: Hazardous polymerization will not occur.

HAZARDOUS DECOMPOSITION PRODUCTS:

 Carbon Monoxide and Carbon Dioxide, Oxides of Nitrogen, Hydrocarbons,

 Amine Compounds.

-----------------------------------------------------------------------------

 5. ENVIRONMENTAL INFORMATION

-----------------------------------------------------------------------------

SPILL RESPONSE:

 Observe precautions from other sections. Ventilate area. Extinguish

 all ignition sources. Contain spill. Cover with inorganic absorbent

 material. Collect spilled material. Clean up residue. Place in an

 approved metal container.

RECOMMENDED DISPOSAL:

 Incinerate in a permitted hazardous waste incinerator.

ENVIRONMENTAL DATA:

 Not determined.

REGULATORY INFORMATION:

 Volatile Organic Compounds: ca. 2.1 lb/gal.

 VOC Less H2O & Exempt Solvents: ca. 251 gms/liter.

 Since regulations vary, consult applicable regulations or authorities

 before disposal. In the event of an uncontrolled release of this

 material, the user should determine if the release qualifies as a

 reportable quantity. U.S. EPA Hazardous Waste Number = D001

 (Ignitable)

EPCRA HAZARD CLASS:

 FIRE HAZARD: Yes PRESSURE: No REACTIVITY: No ACUTE: Yes CHRONIC: Yes

-----------------------------------------------------------------------------

 6. SUGGESTED FIRST AID

-----------------------------------------------------------------------------

EYE CONTACT:

 Immediately flush eyes with large amounts of water for at least 15

 minutes. Get immediate medical attention.

SKIN CONTACT:

 Immediately flush skin with large amounts of water. Remove

 contaminated clothing. If irritation persists, call a physician. Wash

 contaminated clothing before reuse.

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 4

-----------------------------------------------------------------------------

 6. SUGGESTED FIRST AID (continued)

-----------------------------------------------------------------------------

INHALATION:

 Remove person to fresh air. If not breathing, give artificial

 respiration. If breathing is difficult, get immediate medical

 attention.

IF SWALLOWED:

 Do not induce vomiting. Drink two glasses of water. Call a physician.

-----------------------------------------------------------------------------

 7. PRECAUTIONARY INFORMATION

-----------------------------------------------------------------------------

EYE PROTECTION:

 Avoid eye contact. Wear unvented goggles during operations in which

 exposure is likely.

SKIN PROTECTION:

 Avoid skin contact. Wear appropriate gloves when handling this

 material. A pair of gloves made from the following material(s) are

 recommended: butyl rubber. Use one or more of the following

 personal protection items as necessary to prevent skin contact:

 apron, coveralls.

RECOMMENDED VENTILATION:

 Use with appropriate local exhaust ventilation. Provide appropriate

 local exhaust ventilation at transfer points. Provide appropriate

 local exhaust ventilation on open containers. Provide sufficient

 ventilation to maintain emissions below recommended exposure limits.

 If exhaust ventilation is not adequate, use appropriate respiratory

 protection.

RESPIRATORY PROTECTION:

 Avoid breathing of vapors, mists or spray. Select one of the

 following NIOSH approved respirators based on airborne concentration

 of contaminants and in accordance with OSHA regulations: half-mask

 organic vapor respirator, full-face organic vapor respirator.

PREVENTION OF ACCIDENTAL INGESTION:

 Do not eat, drink or smoke when using this product. Wash exposed

 areas thoroughly with soap and water.

RECOMMENDED STORAGE:

 Store in a cool place. Store away from acids. Store out of direct

 sunlight. Keep container in well-ventilated area. Contents may be

 under pressure, open carefully. Keep out of the reach of children.

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 5

-----------------------------------------------------------------------------

 7. PRECAUTIONARY INFORMATION (continued)

-----------------------------------------------------------------------------

FIRE AND EXPLOSION AVOIDANCE:

 Keep container tightly closed. Flammable liquid and vapor. Keep

 away from heat, sparks, open flame, and other sources of ignition.

 Ground containers securely when transferring contents. Wear low

 static or properly grounded shoes. No smoking while handling this

 material. Vapors may ignite explosively.

 EXPOSURE LIMITS

INGREDIENT VALUE UNIT TYPE AUTH SKIN*

-----------------------------------------------------------------------------

ACETONE.............................. 500 PPM TWA ACGIH

ACETONE.............................. 750 PPM STEL ACGIH

ACETONE.............................. 750 PPM TWA OSHAV

 OSHA VACATED PEL

ACETONE.............................. 1000 PPM STEL OSHAV

 OSHA VACATED PEL

ACETONE.............................. 1000 PPM TWA OSHA

METHYL ETHYL KETONE.................. 200 PPM TWA OSHA

METHYL ETHYL KETONE.................. 300 PPM STEL OSHA

METHYL ETHYL KETONE.................. 200 PPM TWA ACGIH

METHYL ETHYL KETONE.................. 300 PPM STEL ACGIH

TOLUENE.............................. 50 PPM TWA ACGIH Y

TOLUENE.............................. 100 PPM TWA OSHAV

 OSHA VACATED PEL

TOLUENE.............................. 150 PPM STEL OSHAV

 OSHA VACATED PEL

TOLUENE.............................. 200 PPM TWA OSHA

TOLUENE.............................. 300 PPM CEIL OSHA

TOLUENE.............................. 75 PPM STEL CMRG Y

ACRYLONITRILE-BUTADIENE POLYMER...... NONE NONE NONE NONE

PHENOL-FORMALDEHYDE RESIN............ NONE NONE NONE NONE

GLYCEROL ESTERS OF ROSIN ACIDS....... NONE NONE NONE NONE

SALICYLIC ACID....................... NONE NONE NONE NONE

ZINC OXIDE........................... 10 MG/M3 TWA ACGIH

 AS DUST

ZINC OXIDE........................... 10 MG/M3 TWA OSHAV

 AS DUST

 OSHA VACATED PEL

ZINC OXIDE........................... 5 MG/M3 TWA ACGIH

 as fume

ZINC OXIDE........................... 10 MG/M3 STEL ACGIH

 as fume

ZINC OXIDE........................... 5 MG/M3 TWA OSHA

 as fume

ZINC OXIDE........................... 10 MG/M3 STEL OSHAV

 as fume

 OSHA VACATED PEL

ZINC OXIDE........................... 15 MG/M3 TWA OSHA

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 6

 EXPOSURE LIMITS (continued)

INGREDIENT VALUE UNIT TYPE AUTH SKIN*

-----------------------------------------------------------------------------

 AS TOTAL DUST

ZINC OXIDE........................... 5 MG/M3 TWA OSHA

 RESPIRABLE

ANTIOXIDANT.......................... NONE NONE NONE NONE

* SKIN NOTATION: Listed substances indicated with 'Y' under SKIN refer to

the potential contribution to the overall exposure by the cutaneous route

including mucous membrane and eye, either by airborne or, more particularly,

by direct contact with the substance. Vehicles can alter skin absorption.

SOURCE OF EXPOSURE LIMIT DATA:

- ACGIH: American Conference of Governmental Industrial Hygienists

- CMRG: Chemical Manufacturer Recommended Exposure Guidelines

- OSHA: Occupational Safety and Health Administration

- OSHAV: Occupational Safety and Health Administration Vacated PEL.

 Vacated Permissible Exposure Limits (PEL) are enforced as

 the OSHA PEL in some states. Check with your local

 regulatory authority.

- NONE: None Established

-----------------------------------------------------------------------------

 8. HEALTH HAZARD DATA

-----------------------------------------------------------------------------

EYE CONTACT:

 Moderate Eye Irritation: signs/symptoms can include redness, swelling,

 pain, tearing, and hazy vision.

SKIN CONTACT:

 Moderate Skin Irritation (after prolonged or repeated contact):

 signs/symptoms can include redness, swelling, itching, and dryness.

 May be absorbed through the skin and produce effects similiar to

 those caused by inhalation and/or ingestion.

INHALATION:

 Central Nervous System Depression: signs/symptoms can include

 headache, dizziness, drowsiness, incoordination, slowed reaction time,

 slurred speech, giddiness and unconsciousness.

 Irritation (upper respiratory): signs/symptoms can include soreness

 of the nose and throat, coughing and sneezing.

 Vapors of the uncured product may cause irritation of the respiratory

 system.

 Prolonged or repeated exposure may cause:

 Blood disorders: signs/symptoms can include prolonged weakness

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 7

-----------------------------------------------------------------------------

 8. HEALTH HAZARD DATA (continued)

-----------------------------------------------------------------------------

 and fatigue.

 Liver Effects: signs/symptoms can include yellow skin(jaundice)

 and tenderness of upper abdomen.

 Prolonged or repeated overexposure, above recommended guidelines, may

 cause:

 Cardiac Sensitization: sudden heart stoppage due to a reflex

 effect on the nerves which control the heart. This effect

 usually occurs only after inhalation of concentrated vapors such

 as in intentional abusive sniffing of certain solvents and

 propellants.

IF SWALLOWED:

 Ingestion is not a likely route of exposure to this product.

 Irritation of Gastrointestinal Tissues: signs/symptoms can include

 pain, vomiting, abdominal tenderness, nausea, blood in vomitus, and

 blood in feces.

 Central Nervous System Depression: signs/symptoms can include

 headache, dizziness, drowsiness, muscular weakness, incoordination,

 slowed reaction time, fatigue, blurred vision, slurred speech,

 giddiness, tremors and convulsions.

 Aspiration Pneumonitis: signs/symptoms can include coughing,

 difficulty breathing, wheezing, coughing up blood and pneumonia,

 which can be fatal.

 Repeated ingestion may cause:

 Kidney Effects: signs/symptoms can include reduced urine volume,

 blood in urine and back pain.

 Liver Effects: signs/symptoms can include yellow skin(jaundice)

 and tenderness of upper abdomen.

REPRODUCTIVE/DEVELOPMENTAL TOXINS:

 WARNING: Contains a chemical which can cause birth defects. (108-88-

 3)

 SALICYLIC ACID (69-72-7) has been associated with lower birth weights,

 increased perinatal mortality, ante- and postpartum hemorrhage,

 prolonged gestation and complicated deliveries.

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately
MSDS: SCOTCHKOTE BRAND ELECTRICAL COATING

November 27, 2001 PAGE 8

-----------------------------------------------------------------------------

SECTION CHANGE DATES

-----------------------------------------------------------------------------

PRECAUTIONARY INFO. SECTION CHANGED SINCE October 24, 2000 ISSUE

-----------------------------------------------------------------------------

Abbreviations: N/D - Not Determined N/A - Not Applicable CA - Approximately

-----------------------------------------------------------------------------

The information in this Material Safety Data Sheet (MSDS) is believed to

be correct as of the date issued. 3M MAKES NO WARRANTIES, EXPRESSED OR

IMPLIED, INCLUDING, BUT NOT LIMITED TO, ANY IMPLIED WARRANTY OF

MERCHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE OR COURSE OF

PERFORMANCE OR USAGE OF TRADE. User is responsible for determining

whether the 3M product is fit for a particular purpose and suitable for

user's method of use or application. Given the variety of factors that

can affect the use and application of a 3M product, some of which are

uniquely within the user's knowledge and control, it is essential that

the user evaluate the 3M product to determine whether it is fit for a

particular purpose and suitable for user's method of use or application.

3M provides information in electronic form as a service to its customers.

Due to the remote possibility that electronic transfer may have resulted

in errors, omissions or alterations in this information, 3M makes no

representations as to its completeness or accuracy. In addition,

information obtained from a database may not be as current as the

information in the MSDS available directly from 3M.
ULTRALIFE BATTERIES MSDS001 

Page 1 of 6 Rev.: K 

 Date: JUN 13 2008

MATERIAL SAFETY DATA SHEET

MSDS001 

Section 1. Chemical Product And Company Identification 

Ultralife Part Number: U9VL; U9VL-FP; U9VL-J; U9VLBUG; 

U9VLBUG-FP (Lectro)

Description: Ultralife Lithium Power Cell

Size: 9.6 Volts

Customer Part Number: N/A

Customer Description: N/A

National Stock Code: U9VL: 6135-01-369-9792

Manufactured by Ultralife Batteries, Inc. 

2000 Technology Pkwy 

Newark, NY 14513-2175 

CAGE Code 0UU59 

Emergency Telephone Number: Chemtrec for Spills, Leaks, Fires 

USA 1-800-424-9300 

International 703-527-3887 

Technical Contact Telephone Number: 1-800-332-5000 

Section 2. Composition/Information on Ingredients 

Chemical Name CAS # Exposure Limits

Percent of 

Content 

Manganese Dioxide, MnO2 1313-13-9 None Listed 35 – 40 

Lithium Metal, Li 7439-93-2 None Listed 1 – 4 

Propylene Carbonate, C4H6O3 108-32-7 None Listed 8 – 10 

1,3-Dioxolane, C3H6O2 646-06-0 None Listed 5 – 9 

Lithium Hexafluoroarsenate, LiAsF6 29935-35-1 As: .01 mg/m3 1 – 4 

Important Note: The materials in this section may only represent a hazard if the integrity of 

the battery is compromised or if the battery is physically or electrically abused. 
ULTRALIFE BATTERIES MSDS001 

Page 2 of 6 Rev.: K 

 Date: JUN 13 2008

Section 3. Hazards Identification 

3.1 Emergency overview: May leak and /or flame if opened, recharged, 

 connected improperly, or disposed of in fire. 

3.2 Potential health effects: Skin contact may cause irritation and absorption. 

Contact with raw lithium may cause burns. 

Routes of entry: Inhalation or ingestion of electrolyte may have toxic effects. 

Acute exposure: Electrolyte may irritate skin and eyes. 

Effects of chronic exposure: Dry Skin 

Section 4. First Aid Measures 

Electrolyte Contact 

Skin- Immediately flush with plenty of water for at least 15 minutes. If symptoms 

are present after flushing, get medical attention. 

Eyes- Immediately flush with plenty of water for at least 15 minutes and get 

medical attention. 

Lithium Metal Contact 

Skin- Remove particles of lithium from skin as rapidly as possible. Immediately 

flush with plenty of water for at least 15 minutes and get medical attention. 

Eyes- Immediately flush with plenty of water for at least 15 minutes and get 

immediate medical attention. 

Section 5. Fire Fighting Measures 

Extinguishing Media: 

Copious amounts of cold water are an effective extinguishing medium for lithium 

batteries. Do not use warm or hot water. 

Do not use Halon type extinguishing material. 

Fire Fighting Procedures 

Use a positive pressure self-contained breathing apparatus if batteries are 

involved in a fire. 

Full protective clothing is necessary. 

During water application, caution is advised as burning pieces of lithium may be 

ejected from the fire. 

Unusual Fire and Explosion Hazards 

Batteries may flame or leak potentially hazardous organic vapors if exposed to 

excessive heat or fire. 

Hazardous combustion products 

Fire or excessive heat may produce hazardous decomposition products. 

Damaged or opened batteries can result in rapid heating and the release of 

flammable vapors. Vapors are heavier than air and may travel along the 

ground or be moved by ventilation to an ignition source and flash back. 
ULTRALIFE BATTERIES MSDS001 

Page 3 of 6 Rev.: K 

 Date: JUN 13 2008

Section 6. Accidental Release Measures 

Damaged batteries that are not hot or burning should be placed in a sealed plastic 

bag or container. 

Section 7. Handling And Storage 

Do not store batteries in a manner that allows terminals to short circuit. 

Batteries should be separated from other materials and stored in a non-combustible, 

well ventilated, sprinkler-protected structure with sufficient clearance between walls 

and battery stacks. Do not place batteries near heating equipment, nor expose to 

direct sunlight for long periods 

Batteries should be stored in a cool (below 70°F), dry area. Air conditioning or 

cooling is not required unless excessively high temperatures will be encountered. 

Elevated storage temperatures can result in reduced battery shelf life and service 

life, and should be avoided. Batteries should be kept as cool as possible in order to 

maximize shelf life and service life. 

Batteries are not designed to be recharged. Charging a battery may result in 

electrolyte leakage and/ or cause the battery to flame. 

Never disassemble a battery. 

Should a battery unintentionally be crushed, thus releasing its contents, rubber 

gloves must be used to handle all battery components. Avoid inhalation of any 

vapors that may be emitted. 

In the event of skin or eye exposure to the electrolyte, refer to Section 4, First Aid 

Measures. 

More than a momentary short circuit will generally reduce the battery service life. 

Batteries with fuses will no longer be functional after being shorted. 

Extended short circuiting creates high temperatures in the cell. High temperatures 

can cause burns in skin or cause the cell to flame.

Avoid reversing battery polarity within the battery assembly. To do so may cause 

cell to flame or to leak. 

The use of old and new batteries or batteries of varying sizes and types in the same 

battery assembly should be avoided. The batteries’ electrical characteristics and 

capabilities vary and damage may result to batteries or electrical equipment. 

Section 8. Exposure Controls/Personal Protection 

No engineering controls are required for handling batteries that have not been 

damaged. Personal protective equipment for damaged batteries should include 

chemical resistant gloves and safety glasses. In the event of a fire, SCBA should be 

worn along with thermally protective outer garments. 
ULTRALIFE BATTERIES MSDS001 

Page 4 of 6 Rev.: K 

 Date: JUN 13 2008

Section 9. Physical And Chemical Properties 

Not Applicable 

Section 10. Stability And Reactivity 

(1) This product is stable under ordinary conditions of use and storage. 

(2) It is not recommended that this product be stored above 85°C (194°F). 

(3) Damaged batteries will react with water. Non-discharged batteries contain 

elemental Lithium. This is water reactive. This reaction gives off heat and hydrogen 

gas. A thermal reaction may occur. 

(4) Hazardous decomposition products: Carbon Monoxide (CO), and 

 Hydrogen Flouride (HF) 

Section 11. Toxicological Information 

(1) Irritancy: The electrolytes contained in this battery can irritate eyes with any 

contact. Prolonged contact with the skin or mucous membranes may cause 

irritation. 

(2) Sensitization: No information is available at this time. 

(3) Carcinogenicity: No information is available at this time. 

(4) Reproductive toxicity: No information is available at this time. 

(5) Teratogenicity: No information is available at this time. 

(6) Mutagenicity: No information is available at this time. 

Section 12. Ecological Information 

Not applicable to this material/product. 

Section 13. Disposal Considerations 

Batteries must be completely discharged prior to disposal and/ or the terminals must 

be taped or capped to prevent short circuit. This product does not contain any 

materials listed by the United Stated EPA as requiring specific waste disposal 

requirements. When completely discharged it is not considered hazardous. Disposal 

of large quantities of lithium power cells may be subject to Federal, State, or Local 

regulations. Consult your local, state and provincial regulations regarding disposal 

of these batteries. 
ULTRALIFE BATTERIES MSDS001 

Page 5 of 6 Rev.: K 

 Date: JUN 13 2008

Section 14. Transport Information 

Ultralife’s lithium metal primary cells and batteries and lithium ion cells and batteries are classified and 

regulated as Class 9 dangerous goods (also known as “hazardous materials” in the United States) by the

International Civil Aviation Organization (ICAO), International Air Transport Association (IATA), International 

Maritime Organization (IMO) and many government agencies such as the U.S. Department of Transportation

(DOT). These organizations and agencies publish regulations that contain detailed packaging, marking, 

labeling, documentation, and training requirements that must be followed when offering (shipping) Ultralife’s 

cells and batteries for transportation. However, small cells and batteries are not subject to certain 

provisions of the regulations (e.g., Class 9 labeling and UN specification packaging) if they meet 

specific requirements. The regulations are based on the UN Recommendations on the Transport of 

Dangerous Goods Model Regulations and the UN Manual of Tests and Criteria. These regulations also 

apply to shipments of cells and batteries that are packed with or contained in equipment. Failure to 

comply with these regulations can result in substantial civil or criminal penalties. 

Cell and Battery Testing Requirements

The dangerous goods regulations require that each cell and battery design be subject to tests contained in 

Section 38.3 of the UN Manual of Tests and Criteria prior to being offered for transport. Ultralife’s cells and 

batteries have been tested and comply with all of the UN testing requirements. Batteries or battery packs 

constructed from Ultralife’s cells must be subjected to tests contained in the UN Manual of Tests and 

Criteria.

Additional Information

UN Recommendations on the Transport of Dangerous Goods Model Regulations 

IATA Dangerous Goods Regulations 

International Maritime Dangerous Goods Code 

European Road Regulations (ADR) 

U.S. Hazardous Materials Regulations 

For more information, please refer to the Transportation Regulations Page on 

Ultralife’s Web Site: 

http://www.ultralifebatteries.com/subcategory.php?ID=12

Product is shipped as: 

Ground (DOT/ADR) Air (IATA/ICAO) Water(IMDG Code) 

May be shipped without 

being declared as Class 

9 dangerous goods.

May be shipped without 

being declared as Class 9 

dangerous goods.

May be shipped without 

being declared as Class 9 

dangerous goods.

UN specification packaging 

is not required. No Class 9 

label or UN number is 

required on outer package. 

In addition, no shipper’s 

declaration for dangerous 

goods is required.

UN specification packaging is 

not required. No Class 9 label 

or UN number is required on 

outer package. In addition, no 

shipper’s declaration for 

dangerous goods is required. 

These batteries cannot be 

shipped on passenger aircraft 

from, to or within the USA. 

UN specification packaging 

is not required. No Class 9 

label or UN number is 

required on outer package. 

In addition, no shipper’s 

declaration for dangerous 

goods is required.
ULTRALIFE BATTERIES MSDS001 

Page 6 of 6 Rev.: K 

 Date: JUN 13 2008

Special shipping information: This battery has been tested to Section 38.3 of ‘UN 

Manual of Tests and Criteria’. The amount of Lithium contained in these batteries is 

below the limits set by the DOT in Section 49CFR173.185 and IATA A45. There is an 

exception to ship these with the following shipping label: 

LITHIUM BATTERIES 

Do not damage or mishandle this package 

If package is damaged, batteries must be 

quarantined, inspected and repacked. 

For emergency information, call CHEMTREC 

1-800-424-9300 North America 

 1-703-527-3887 International 

These batteries cannot be shipped by passenger aircraft. 

Section 15. Regulatory Information 

USA: This MSDS meets/exceeds OSHA requirements. 

Canada: This product has been classified in accordance with the hazard criteria of 

the Controlled Products Regulations and the MSDS contains all of the information 

required by those regulations. 

International: This MSDS conforms to European Union (EU), the International 

Standards Organization (ISO) and the International Labour Organization (ILO) and as 

documented in ANSI (American National Standards Institute) Standard Z400.1-1993. 

Section 16. Other Information 

The information contained herein is furnished without warranty of any kind. Users 

should consider this data only as a supplement to other information gathered by 

them and must make independent determinations of the suitability and 

completeness of information from all sources to assure proper use and disposal of 

these materials and the safety and health of employees and customers. 
MATERIAL SAFETY DATA SHEET 

Gougeon Brothers, Inc. 

1. CHEMICAL PRODUCT AND COMPANY IDENTIFICATION

PRODUCT NAME:............................. G5 Adhesive - Part B. 

PRODUCT CODE: ............................. 865 

CHEMICAL FAMILY:...................... Mercaptan. 

CHEMICAL NAME:.......................... Mercaptan polymer. 

FORMULA:......................................... Not applicable. 

MANUFACTURER: EMERGENCY TELEPHONE NUMBERS:

West System Inc. Transportation 

102 Patterson Ave. CHEMTREC: ............800-424-9300 (U.S.) 

Bay City, MI 48706, U.S.A. 703-527-3887 (International)

Phone: 866-937-8797 or 989-684-7286 Non-transportation 

www.westsystem.com Poison Hotline:..........800-222-1222 

2. COMPOSITION/INFORMATION ON HAZARDOUS INGREDIENTS

INGREDIENT NAME CAS# CONCENTRATION

Tris (dimethylaminomethyl) phenol 90-72-2 < 20% 

Mercaptan terminated polymer Trade Secret 

3. HAZARDS IDENTIFICATION

EMERGENCY OVERVIEW

HMIS Hazard Rating: Health - 2 Flammability - 1 Reactivity - 1

WARNING. Moderate skin and respiratory irritant. Can be corrosive to eye tissue. Harmful if swallowed. Amber 

colored liquid with mercaptan odor and high viscosity. 

PRIMARY ROUTE(S) OF ENTRY:..............................Inhalation, skin contact, eye contact. 

POTENTIAL HEALTH EFFECTS:

ACUTE INHALATION:..................................................Can cause irritation to the respiratory tract when exposed to 

high concentrations of vapor. 

CHRONIC INHALATION: ............................................Overexposure to fumes and vapors may cause delayed lung 

damage and chemical pneumonia. 

ACUTE SKIN CONTACT:.............................................Slightly irritating. May be more severe with prolonged 

contact. 

CHRONIC SKIN CONTACT:........................................Prolonged irritation or rash. Possible corrosion skin tissue. 

EYE CONTACT:..............................................................Can be corrosive to eye tissue leading to permanent damage. 

INGESTION:....................................................................Slightly toxic. May cause gastrointestinal irritation. 

MSDS# 865B-05a Last Revised: 02JAN07
Gougeon Brothers, Inc. Page 2 of 4 G5 Adhesive - Part B 

SYMPTOMS OF OVEREXPOSURE:...........................Respiratory tract irritation. Skin irritation. Severe eye 

irritation.

MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE:

Existing skin, eye and lung conditions such as that resulting from allergies. 

4. FIRST AID MEASURES:

FIRST AID FOR EYES:..................................................Immediately flush with water for at least 15 minutes. Get 

prompt medical attention. 

FIRST AID FOR SKIN: ..................................................Remove contaminated clothing. Wipe excess off skin. Wash 

affected area with soap and water. Get medical attention should irritation develop. 

FIRST AID FOR INHALATION:..................................Move to fresh air if effects occur. 

FIRST AID FOR INGESTION:......................................Give conscious person at least 2 glasses of water. Do not 

induce vomiting. If vomiting should occur spontaneously, keep airway clear. Get medical attention. 

5. FIRE FIGHTING MEASURES:

FLASH POINT:................................................................495°F (COC) 

EXTINGUISHING MEDIA:...........................................Water spray, dry chemical, alcohol foam and carbond dioxide 

(CO2). 

SPECIAL FIRE FIGHTING PROCEDURES:.............Burning material will generate toxic fumes. Use full-body 

protective gear and a self-contained breathing apparatus. If spill has ignited, use water spray to disperse vapors and

protect personnel attempting to stop leak. Use water to cool fire-exposed containers. 

6. ACCIDENTAL RELEASE MEASURES:

SPILL OR LEAK PROCEDURES: Stop leak without additional risk. Wear proper personal protective equipment. 

Dike and contain spill. Ventilate area. Absorb with inert absorbent material and remove to disposal container. Wash

spill residue with warm, soapy water if necessary. 

7. HANDLING AND STORAGE:

STORAGE TEMPERATURE (MIN./MAX):................40°F (4°C) / 90°F (32°C) 

STORAGE: .......................................................................Store in cool, dry place. Keep containers tightly closed. 

HANDLING PRECAUTIONS:.......................................Use only with adequate ventilation. Do not breath vapors or 

mists from heated product. Avoid contact with skin and eyes. Wash thoroughly after handling. 

8. EXPOSURE CONTROLS/PERSONAL PROTECTION:

EYE PROTECTION GUIDELINES:.............................Chemical splash goggles or full-face shield. 

SKIN PROTECTION GUIDELINES:...........................Wear liquid-proof, chemical resistant gloves (nitrile-butyl 

rubber, neoprene, butyl rubber or natural rubber) and full body-covering clothing. 

RESPIRATORY/VENTILATION GUIDELINES:

General mechanical or local exhaust ventilation. In the absence of adequate ventilation controls, use a NIOSH/MSHA

approved air purifying respirator with an organic vapor cartridge. 

MSDS# 865B-07a Last Revised: 02JAN07
Gougeon Brothers, Inc. Page 3 of 4 G5 Adhesive - Part B 

ADDITIONAL PROTECTIVE MEASURES: ..............Use where there is immediate access to safety shower and 

emergency eye wash. Provide proper wash/cleanup facilities for proper hygiene. 

OCCUPATIONAL EXPOSURE LIMITS:....................Not established for product as whole. Refer to OSHA’s 

Permissible Exposure Level (PEL) or the ACGIH Guidelines for information on specific ingredients. 

9. PHYSICAL AND CHEMICAL PROPERTIES:

PHYSICAL FORM ..........................................................Viscous liquid. 

COLOR .............................................................................Light yellow to amber. 

ODOR................................................................................Mercaptan odor. 

BOILING POINT.............................................................No data. 

MELTING POINT/FREEZE POINT.............................No data. 

pH.......................................................................................3-5 

SOLUBILITY IN WATER..............................................Slight. 

SPECIFIC GRAVITY......................................................1.14 

BULK DENSITY..............................................................9.5 pounds/gallon. 

VAPOR PRESSURE........................................................No data. 

VAPOR DENSITY ...........................................................No data. 

% VOLATILE BY WEIGHT..........................................1.52% 

10. REACTIVITY:

STABILITY:.....................................................................Stable. 

HAZARDOUS POLYMERIZATION:...........................Will not occur. 

INCOMPATIBILITIES:..................................................Avoid contact with strong oxidants. Contact with large 

masses of epoxy resin generates large quantities of heat due to exothermic reaction. 

DECOMPOSITION PRODUCTS:.................................Carbon dioxide, carbon monoxide, hydrogen sulfide, oxides 

of nitrogen, and oxides of sulfur. 

11. TOXICOLOGICAL INFORMATION:

No specific oral, inhalation or dermal toxicology data is known for this product.

Oral:....................................................... Slightly toxic. 

Inhalation:.............................................. No data. 

Dermal:.................................................. Slightly toxic. 

CARCINOGENICITY:

NTP .............................................................................No. 

IARC ...........................................................................No. 

OSHA..........................................................................No. 

This product contains no known carcinogens in concentrations greater than 0.1%. 

12. ECOLOGICAL INFORMATION:

No specific data. Wastes from this product may present long term environmental hazards. Do not allow into sewers, on 

the ground or in any body of water. 

13. DISPOSAL CONSIDERATIONS:

MSDS# 865B-07a Last Revised: 02JAN07
Gougeon Brothers, Inc. Page 4 of 4 G5 Adhesive - Part B 

WASTE DISPOSAL METHOD: ....................................Evaluation of this product using RCRA criteria shows that it is 

not a hazardous waste, either by listing or characteristics, in its purchased form. It is the responsibility of the user to 

determine proper disposal methods. 

Incinerate, recycle (fuel blending) or reclaim may be preferred methods when conducted in accordance with federal, 

state and local regulations. 

14. TRANSPORTATION INFORMATION:

D.O.T. SHIPPING NAME:..............................................Not regulated by DOT. 

TECHNICAL SHIPPING NAME: .................................Not applicable. 

D.O.T. HAZARD CLASS:...............................................Not applicable. 

U.N./N.A. NUMBER: .......................................................Not applicable. 

PACKING GROUP: ........................................................Not applicable. 

15. REGULATORY INFORMATION:

OSHA STATUS:...............................................................Irritant. 

TSCA STATUS:................................................................All components are listed on TSCA inventory. 

SARA TITLE III:

SECTION 313 TOXIC CHEMICALS ....................None. 

STATE REGULATORY INFORMATION:

The following chemicals are specifically listed or otherwise regulated by individual states. For details on your 

regulatory requirements you should contact the appropriate agency in your state. 

COMPONENT NAME 

/CAS NUMBER CONCENTRATION STATE CODE

None known. 

16. OTHER INFORMATION:

REASON FOR ISSUE:....................................................Update in Section 2. 

PREPARED BY: ..............................................................T. J. Atkinson 

APPROVED BY:..............................................................G. M. House 

TITLE: ..............................................................................Health, Safety & Environmental Manager 

APPROVAL DATE: ........................................................January 2, 2007 

SUPERSEDES DATE:.....................................................January 3, 2005 

MSDS NUMBER:.............................................................865B-07a 

Note: The Hazardous Material Indexing System (HMIS), cited in the Emergency Overview of Section 3, uses the following 

index to assess hazard rating: 0 = Minimal; 1 = Slight: 2 = Moderate; 3 = Serious; and 4 = Severe. 

This information is furnished without warranty, expressed or implied, except that it is accurate to the best knowledge of 

Gougeon Brothers, Inc. The data on this sheet is related only to the specific material designated herein. Gougeon Brothers, 

Inc. assumes no legal responsibility for use or reliance upon these data. 

MSDS# 865B-07a Last Revised: 02JAN07
MATERIAL SAFETY DATA SHEET

West System Inc.

MSDS# 865A-05a Last Revised: 03JAN05

1. CHEMICAL PRODUCT AND COMPANY IDENTIFICATION

PRODUCT NAME: ....................... G5 Adhesive - Part A.

PRODUCT CODE:........................ 865

CHEMICAL FAMILY:................. Epoxy resin.

CHEMICAL NAME:..................... Bisphenol-A based epoxy resin.

FORMULA:.................................... Not applicable.

MANUFACTURER: EMERGENCY TELEPHONE NUMBERS:

West System Inc. Transportation

102 Patterson Ave. CHEMTREC: .........800-424-9300 (U.S.)

Bay City, MI 48706, U.S.A. 703-527-3887 (International)

Phone: 866-937-8797 or 989-684-7286 Non-transportation

www.westsystem.com Poison Hotline: .......800-222-1222

2. COMPOSITION/INFORMATION ON HAZARDOUS INGREDIENTS

INGREDIENT NAME CAS # CONCENTRATION

Bisphenol-A type epoxy resin 25085-99-8 > 50%

Bisphenol-F type epoxy resin 28064-14-4 < 50%

3. HAZARDS IDENTIFICATION

EMERGENCY OVERVIEW

HMIS Hazard Rating: Health - 2 Flammability - 1 Reactivity - 0

CAUTION. Moderate eye irritant. Moderate skin irritant. Possible skin sensitizer. Light-yellow liquid with

mild odor and high viscosity.

PRIMARY ROUTE(S) OF ENTRY: ..................... Skin contact.

POTENTIAL HEALTH EFFECTS:

ACUTE INHALATION:......................................... Not likely to cause acute effects unless heated to high

temperatures. If product is heated, vapors generated can cause headache, nausea, dizziness and possible

respiratory irritation if inhaled in high concentrations.

CHRONIC INHALATION:.................................... Not likely to cause chronic effects. Repeated exposure to

high vapor concentrations may cause irritation of pre-existing lung allergies and increase the chance of

developing allergy symptoms to this product.

ACUTE SKIN CONTACT:..................................... May cause allergic skin response in certain individuals.

May cause moderate irritation to the skin such as redness and itching.
West System Inc. Page 2 of 6 G5 Adhesive - Part A

MSDS# 865A-05a Last Revised: 03JAN05

CHRONIC SKIN CONTACT: ............................... May cause sensitization in susceptible individuals. May

cause moderate irritation to the skin.

EYE CONTACT:..................................................... May cause irritation.

INGESTION:............................................................ Low acute oral toxicity.

SYMPTOMS OF OVEREXPOSURE: .................. Possible sensitization and subsequent allergic reactions

usually seen as redness and rashes. Repeated exposure is not likely to cause other adverse health effects.

MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE:

Pre-existing skin and respiratory disorders may be aggravated by exposure to this product. Pre-existing lung

and skin allergies may increase the chance of developing allergic symptoms to this product.

4. FIRST AID MEASURES:

FIRST AID FOR EYES: ......................................... Flush with plenty of water for at least 15 minutes and

seek medical advice.

FIRST AID FOR SKIN:.......................................... Remove contaminated clothing. Wash contact area with

soap and water.

FIRST AID FOR INHALATION:.......................... Remove to fresh air. If effects occur and persist get

medical attention.

FIRST AID FOR INGESTION:............................. Do not induce vomiting. In general, no treatment is

necessary unless large quantities are ingested. Get medical advice.

5. FIRE FIGHTING MEASURES:

FLASH POINT: ....................................................... > 200°F (TCC)

EXTINGUISHING MEDIA: .................................. Water fog, alcohol foam, carbon dioxide (CO2) or dry

chemical.

SPECIAL FIRE FIGHTING PROCEDURES:..... Burning material will generate toxic fumes. Wear

complete fire protection gear and a self-contained breathing apparatus. Cool fire-exposed containers with

water spray. Material will not burn unless preheated.

6. ACCIDENTAL RELEASE MEASURES:

SPILL OR LEAK PROCEDURES:....................... Stop leak without additional risk. Dike and contain spill.

Wear appropriate personal protective equipment. Soak up in absorbent material or scrape up in bulk.

Residual can be removed with safe, non-flammable solvent or warm soap and water.

7. HANDLING AND STORAGE:

STORAGE TEMPERATURE (MIN./MAX):....... 40°F (4°C) / 120°F (49°C)

STORAGE:............................................................... Store in cool, dry place with tightly closed container to

prevent loss of volatiles.
West System Inc. Page 3 of 6 G5 Adhesive - Part A

MSDS# 865A-05a Last Revised: 03JAN05

HANDLING PRECAUTIONS: .............................. Ventilate work area. Avoid skin contact. Wash

thoroughly after using.

8. EXPOSURE CONTROLS/PERSONAL PROTECTION:

EYE PROTECTION GUIDELINES:.................... Safety glasses with side shield protection. Additional

face shield or chemical goggles when exposure is more likely.

SKIN PROTECTION GUIDELINES:................... Wear liquid-proof, chemical resistant gloves (nitrilebutyl rubber, neoprene, butyl rubber or natural rubber) and full body-covering clothing.

RESPIRATORY/VENTILATION GUIDELINES:

General mechanical and local exhaust ventilation is sufficient for most operations. A NIOSH/MSHA

approved respirator with an organic vapor cartridge may be used when adequate ventilation is not possible or

when using heated product.

ADDITIONAL PROTECTIVE MEASURES:

Practice good caution and personal cleanliness to avoid skin and eye contact. Avoid skin contact when

removing gloves and other protective equipment. Wash thoroughly after handling..

OCCUPATIONAL EXPOSURE LIMITS: ........... Not established for product as whole. Refer to OSHA’s

Permissible Exposure Level (PEL) or the ACGIH Guidelines for information on specific ingredients.

9. PHYSICAL AND CHEMICAL PROPERTIES:

PHYSICAL FORM.................................................. Viscous liquid.

COLOR..................................................................... Pale yellow.

ODOR ....................................................................... Mild.

BOILING POINT .................................................... > 400°F.

MELTING POINT/FREEZE POINT.................... No data.

pH.............................................................................. No data.

SOLUBILITY IN WATER ..................................... Slight.

SPECIFIC GRAVITY............................................. 1.15

BULK DENSITY ..................................................... 9.6 pounds/gallon.

VAPOR PRESSURE ............................................... < 1 mmHg @ 20°C.

VAPOR DENSITY................................................... Heavier than air.

% VOLATILE BY WEIGHT................................. < 1%

10. REACTIVITY:

STABILITY: ............................................................ Stable.

HAZARDOUS POLYMERIZATION:.................. Will not occur.

INCOMPATIBILITIES:......................................... Strong acids, bases, amines and mercaptans can cause

polymerization.

DECOMPOSITION PRODUCTS: ........................ Carbon monoxide and carbon dioxide fumes may be

produced when heated to decomposition.
West System Inc. Page 4 of 6 G5 Adhesive - Part A

MSDS# 865A-05a Last Revised: 03JAN05

11. TOXICOLOGICAL INFORMATION:

No specific oral, inhalation or dermal toxicology data is known for this product. Specific toxicology

information for a bisphenol-A based epoxy resin present in this product is indicated below:

Oral: ................................................. LD50 > 5000 mg/kg (rats)

Inhalation: ........................................ No Data.

Dermal: ............................................ LD50 = 20,000 mg/kg (skin absorption in rabbits)

TERATOLOGY:........................................................ Diglycidyl ether bisphenol-A (DGEBPA) did not cause

birth defects or other adverse effects on the fetus when pregnant rabbits were exposed by skin contact, the

most likely route of exposure, or when pregnant rats or rabbits were exposed orally.

REPRODUCTIVE EFFECTS: .................................. DGEBPA, in animal studies, has been shown not to

interfere with reproduction.

MUTAGENICITY:.................................................... DGEBPA in animal mutagenicity studies were negative.

In vitro mutagenicity were negative in some cases and positive in others.

CARCINOGENICITY:

NTP ..................................................................... Product not listed.

IARC ................................................................... Product not listed.

OSHA .................................................................. Product not listed.

Many studies have been conducted to assess the potential carcinogenicity of diglycidyl ether of bisphenolA. Although some weak evidence of carcinogenicity has been reported in animals, when all of the data

are considered, the weight of evidence does not show that DGEBPA is carcinogenic. Indeed, the most

recent review of the available data by the International Agency for Research on Cancer (IARC) has

concluded that DGEBPA is not classified as a carcinogen.

Epichlorohydrin, an impurity in this product (<25 ppm) has been reported to produce cancer in laboratory

animals and to produce mutagenic changes in bacteria and cultured human cells. It has been established

by the International Agency for Research on Cancer (IARC) as a probable human carcinogen (Group 2A)

based on the following conclusions: human evidence – inadequate; animal evidence – sufficient. It has

been classified as an anticipated human carcinogen by the National Toxicology Program (NTP).

12. ECOLOGICAL INFORMATION:

Prevent entry into sewers and natural waters. May cause localized fish kill. 

Movement and Partitioning:

Bioconcentration potential is moderate (BCF between 100 - 3000 or Log Kow between 3 - 5).

Degradation and Transformation:

Theoretical oxygen demand is calculated to be 2.35 p/p. 20-day biochemical oxygen demand is

< 2.5%.

Ecotoxicology:

Material is moderately toxic to aquatic organisms on an acute basis. LC50/EC50 between 1 - 10

mg/L in most sensitive species.
West System Inc. Page 5 of 6 G5 Adhesive - Part A

MSDS# 865A-05a Last Revised: 03JAN05

13. DISPOSAL CONSIDERATIONS:

WASTE DISPOSAL METHOD:............................ Evaluation of this product using RCRA criteria shows

that it is not a hazardous waste, either by listing or characteristics, in its purchased form. It is the

responsibility of the user to determine proper disposal methods.

Incinerate, recycle (fuel blending) or reclaim may be preferred methods when conducted in accordance with

federal, state and local regulations.

14. TRANSPORTATION INFORMATION:

D.O.T. SHIPPING NAME:..................................... Not regulated by DOT.

TECHNICAL SHIPPING NAME:......................... Not applicable.

D.O.T. HAZARD CLASS: ...................................... Not applicable.

U.N./N.A. NUMBER:............................................... Not applicable.

PACKING GROUP:................................................ Not applicable.

15. REGULATORY INFORMATION:

OSHA STATUS: ...................................................... Slight irritant; possible sensitizer.

TSCA STATUS:....................................................... All components are listed on TSCA inventory.

SARA TITLE III:

SECTION 313 TOXIC CHEMICALS ............ None.

STATE REGULATORY INFORMATION:

The following chemicals are specifically listed or otherwise regulated by individual states. For details on

your regulatory requirements you should contact the appropriate agency in your state.

COMPONENT NAME

/CAS NUMBER CONCENTRATION STATE CODE

Epichlorohydrin

106-89-8 < 5ppm 1CA, MA, PA, RI

Phenyl glycidyl ether

122-60-1 <5ppm 1CA

1. These substances are known to the State of California to cause cancer or reproductive harm, or both.

16. OTHER INFORMATION:

REASON FOR ISSUE:............................................ Update in Section 1.

PREPARED BY:...................................................... T. J. Atkinson

APPROVED BY: ..................................................... G. M. House

TITLE:...................................................................... Health, Safety & Environmental Manager

APPROVAL DATE:................................................ January 3, 2005

SUPERSEDES DATE: ............................................ January 5, 2004

MSDS NUMBER: .................................................... 865A-05a
West System Inc. Page 6 of 6 G5 Adhesive - Part A

MSDS# 865A-05a Last Revised: 03JAN05

Note: The Hazardous Material Indexing System (HMIS), cited in the Emergency Overview of Section 3, uses the

following index to assess hazard rating: 0 = Minimal; 1 = Slight: 2 = Moderate; 3 = Serious; and 4 = Severe.

This information is furnished without warranty, expressed or implied, except that it is accurate to the best

knowledge of West System Inc. The data on this sheet is related only to the specific material designated herein.

West System Inc. assumes no legal responsibility for use or reliance upon these data.
Page 1 of 5 

KANO LABORATORIES, INC. 

SAFETY DATA SHEET

SECTION 1: PRODUCT AND COMPANY IDENTIFICATION 

Manufacturer: Kano Laboratories, Inc. 

 1000 E. Thompson Lane 

Nashville, TN 37211 

Information Phone Number: (615) 833-4101 

Fax: (615) 833-5790 Emergency: 800-424-9300 (Chemtrec) 

Website: www.kanolaboratories.com 

HMIS Hazard Rating 

 HEALTH 1 

 FLAMMABILITY 2 

 REACTIVITY 0 

 PERSONAL PROTECTION X 

Product Name: SILIKROIL (aerosol) 

MSDS Date of Preparation: 6/7/09 

Product Use: Penetrant/Lubricant for Industrial Use 

SECTION 2: HAZARDS IDENTIFICATION 

Slightly reddish liquid with a refreshing odor packaged as an aerosol. 

EMERGENCY OVERVIEW

WARNING! Contents under pressure. Heated can may rupture. Combustible Liquid and Vapor. May cause eye and 

skin irritation. May be harmful if absorbed through the skin. Inhalation of vapors or mist may cause respiratory 

irritation and central nervous system effects such as headache, dizziness, nausea and vomiting. Harmful or fatal if 

swallowed. Aspiration into the lungs during ingestion or vomiting may cause lung damage. May cause chronic 

effects.

Potential Health Effects:

Eye: May cause eye irritation with redness, tearing and stinging. Corneal injury is possible if not promptly removed. 

Skin: May cause mild irritation with redness, rash, swelling. Prolonged or repeated contact may result in defatting 

and dermatitis. May be absorbed through the skin with effects similar to inhalation and ingestion. 

Inhalation: Inhalation of vapors or mists may cause mucous membrane and upper respiratory tract irritation and 

central nervous system depression. Symptoms may include burning sensation, coughing, wheezing, sore throat, 

shortness of breath, headache, dizziness, drowsiness, nausea, vomiting, depressed respiration and heart rate, heart 

rhythm irregularities and unconsciousness. 

Ingestion: Ingestion is an unlikely route of exposure for aerosol products. Swallowing may cause gastrointestinal 

irritation with abdominal pain, nausea, vomiting and diarrhea and central nervous system depression with symptoms 

including headache, dizziness, intoxication, weakness, respiratory failure, convulsions, cardiovascular collapse and 

pulmonary edema. Aspiration into the lungs during ingestion or vomiting may cause lung damage. 

Chronic Hazards: Prolonged or repeated exposure may cause damage to the central nervous system, blood, kidney 

and liver. This product contains chemicals that in animal studies caused harm to the developing fetus, but only at 

exposure levels that harm the pregnant animal. There is no evidence of adverse fetal or reproductive effects in 

humans. 

Carcinogen Status: None of the components of this product at greater than 0.1% are listed as carcinogens by 

OSHA, IARC or NTP. 

Medical Conditions Aggravated by Exposure: Pre-existing eye, skin, respiratory, heart, central nervous system, 

liver and kidney disorders. 
SILIKROIL (aerosol) 

6/7/05 

Page 2 of 5 

SECTION 3: COMPOSITION/INFORMATION ON INGREDIENTS 

Chemical Name CAS# % 

Severely Hydrotreated Petroleum Distillates 64742-52-5 30-50 

Light Petroleum Distillates 64742-95-6/64742-88-7/ 

64742-47-8

30-50

Aliphatic Alcohols 78-92-2/123-42-2 1-5 

Glycol Ether 111-76-2 1-5 

Silicone 63148-62-9 1-10 

Proprietary Ingredients Proprietary 5-15 

Carbon Dioxide Propellant 124-38-9 1-15 

SECTION 4: FIRST AID MEASURES

Eye: Rinse thoroughly with water for at least 15 minutes, holding the eye lids open to be sure the material is 

washed out. Get immediate medical attention. 

Skin: Remove contaminated clothing. Wash contact area thoroughly with soap and water. Get medical attention if 

irritation or symptoms of exposure develop. Launder clothing before re-use. 

Inhalation: Remove victim to fresh air. Give artificial respiration if needed. If breathing is difficult, oxygen 

should be administered by qualified personnel. Get immediate medical attention. 

Ingestion: Ingestion is an unlikely route of exposure for aerosol products. DO NOT induce vomiting. Keep the 

victim calm and warm. Never give anything by mouth to an unconscious or drowsy person. Get immediate medical 

attention. 

SECTION 5: FIRE FIGHTING MEASURES

Flash Point: 124°F (51oC) COC Flammable Limits: LEL: 0.9% 

 UEL: 10.6% 

Autoignition Temperature: Not Determined 

Aerosol Flame Extension: None 

Aerosol Flashback: None 

Aerosol Protection Level (NPPA 30B): Level 3 

Extinguishing Media: Use carbon dioxide, dry chemical or foam. Water may be ineffective but can be used to 

cool containers and structures. 

Special Fire Fighting Procedures: Wear NIOSH approved, positive pressure, self-contained breathing apparatus 

and full protective clothing. Cool fire exposed containers with water. 

Unusual Fire Hazards: Contents under pressure. Keep away from heat and open flames. Container may rupture or 

explode in the heat of a fire. Prolonged exposure to temperatures above 120o

F may cause cans to burst. Vapors are 

heavier than air and may travel along surfaces to remote ignition sources and flash back. Never use welding or cutting 

torch on or near containers (even empty) because product can ignite explosively. Combustion products may be 

hazardous.

Hazardous Decomposition Products: Oxides of carbon, organic compounds, smoke and fumes. 

SECTION 6: ACCIDENTAL RELEASE MEASURES

Spill: Remove all ignition sources such as open flames, spark producing equipment, pilot lights, etc. Wear 

appropriate protective clothing to prevent eye and skin contact including impervious gloves, safety goggles and 

respirator if needed (refer to Section 8 for specific recommendations). Ventilate area. Cover with an inert absorbent 
SILIKROIL (aerosol) 

6/7/05 

Page 3 of 5 

material and collect into an appropriate container for disposal. Report spills and releases as required to appropriate 

authorities. 

SECTION 7: HANDLING AND STORAGE

Handling: Avoid breathing vapors, aerosols and mists. Use with adequate ventilation. Avoid contact with the eyes, 

skin and clothing. Wash exposed skin thoroughly with soap and water after use. Keep product away from heat, 

sparks, flames and all other sources of ignition. No smoking in storage or use areas. Do not cut, braze, solder, grind 

or weld on or near containers. Contents under pressure. Do not puncture or incinerate container. 

Storage Store in a cool, well ventilated area at temperatures below 120o

F. Do not store in direct sunlight. Store as a 

Level 3 aerosol. 

SECTION 8: EXPOSURE CONTROLS/PERSONAL PROTECTION 

Chemical Name Exposure Limits 

Severely Hydrotreated Petroleum Distillates 5 mg/m3 OSHA PEL-TWA 

5 mg/m3 ACGIH TLV-TWA 

10 mg/m3 ACGIH TLV-STEL 

Light Petroleum Distillates 100 ppm OSHA PEL-TWA 

100 ppm ACGIH TLV-TWA 

Aliphatic Alcohol 150 ppm OSHA PEL-TWA 

100 ppm ACGIH TLV-TWA 

Aliphatic Alcohol 50 ppm OSHA PEL-TWA 

50 ppm ACGIH TLV-TWA 

Glycol Ether 50 ppm OSHA PEL-TWA 

20 ppm ACGIH TLV-TWA 

Silicone None Established 

Proprietary Ingredients None Established 

Carbon Dioxide Propellant 5000 ppm OSHA PEL-TWA 

5000 ppm ACGIH TLV-TWA 

30000 ppm ACGIH TLV-STEL 

Ventilation: Use with adequate general or local exhaust ventilation to maintain concentrations below the 

occupational exposure limits. Use explosion proof electrical equipment and wiring where required. 

Respiratory Protection: If needed, a NIOSH approved respirator with organic vapor cartridges may be used. For 

higher exposures, a supplied air respirator may be required. Respirator selection and use should be based on 

contaminant type, form and concentration. Follow OSHA 1910.134, ANSI Z88.2 and good Industrial Hygiene practice. 

Skin Protection Impervious gloves are recommended when needed to avoid skin contact. Based on available test data, 

4H or Silver Shield gloves are suggested. 

Eye Protection: Chemical safety goggles recommended. 

Other Protective Equipment: Impervious clothing as required to prevent skin contact and contamination of 

personal clothing. Suitable eye wash and washing facilities should be available in the work area. 

SECTION 9: PHYSICAL AND CHEMICAL PROPERTIES

Appearance and Odor: Slightly reddish liquid with a refreshing odor packaged as an aerosol. 

pH: 6-7 Specific Gravity: 0.87 

Boiling Point: 258F Melting Point: Not applicable 

Vapor Pressure: 12 mm Hg @ 20C (aliphatic alcohol) Water Solubility: Negligible 

Vapor Density (air =1): Greater than 1 Evaporation Rate (ether=1): Less than 1 
SILIKROIL (aerosol) 

6/7/05 

Page 4 of 5 

SECTION 10: STABILITY AND REACTIVITY 

Stability: Stable under normal conditions of storage or use. 

Incompatibility/Conditions to Avoid: Avoid strong oxidizing agents, reducing agents, acids, bases, amines, 

alkanolamines, ammonia, chlorinated compounds. Avoid heat, sparks, flames and all other sources of ignition. 

Hazardous Decomposition Products: Combustion will produce oxides of carbon, organic compounds, smoke and 

fumes. 

Hazardous Polymerization: Will not occur. 

SECTION 11: TOXICOLOGICAL INFORMATION

Toxicological testing has not been performed on this product as a mixture. 

The calculated acute toxicity values, as determined by the DOT and other agency standard formula are: Oral LD50 

= 2270; Dermal LD50 = 1500 mg/kg. Silikroil is not classified as toxic under workplace or transportation criteria. 

SECTION 12: ECOLOGICAL INFORMATION

No data available. 

SECTION 13: DISPOSAL INFORMATION

Dispose in accordance with all local, state and federal regulations. Do not puncture or incinerate containers. When 

contents are depleted, continue to depress button until all gas is expelled. 

SECTION 14: TRANSPORT INFORMATION 

DOT Proper Shipping Name: Consumer Commodity 

DOT Technical Name: None

DOT Hazard Class: ORM-D 

UN Number: None 

DOT Labels Required (49CFR172.101): None

Hazardous Substance (49CFR172.101): None 

Reportable Quantity: None 

DOT Marine Pollutants: This product does not contain marine pollutants as defined in 49CFR 171.8. 

IMDG Shipping Description: Aerosols, 2, UN1950, FP 51 C, Limited Quantity 

ID Number: UN1950 

Hazard Class: 2 

Packing Group: None 

Labels Required: None 

Marking Required: Aerosol Marking On Carton 

Placards Required: Limited Quantities On Transport Containers 

SECTION 15: REGULATORY INFORMATION

U.S. FEDERAL REGULATIONS:

CERCLA 103 Reportable Quantity: This product is not subject to CERCLA reporting requirements, however, oil 

spills are reportable to the National Response Center under the Clean Water Act and many states have more 

stringent release reporting requirements. Report spills required under federal, state and local regulations. 
SILIKROIL (aerosol) 

6/7/05 

Page 5 of 5 

SARA TITLE III:

Hazard Category for Section 311/312: Acute Health, Chronic Health, Fire Hazard, Sudden Release of Pressure 

Section 313 Toxic Chemicals: This product contains the following chemicals subject to SARA Title III Section 

313 Reporting requirements: 

Aliphatic Alcohol 78-92-2 1-5% 

Glycol Ether 111-76-2 1-5% 

1,2,4-Trimethylbenzene 95-63-6 .5 - < 5% 

Section 302 Extremely Hazardous Substances (TPQ): None 

EPA Toxic Substances Control Act (TSCA) Status: All of the components of this product are listed on the TSCA 

inventory. 

SECTION 16: OTHER INFORMATION

HMIS Ratings: Health - 1 Flammability - 2 Reactivity - 0 

NFPA Ratings: Health - 1 Flammability - 2 Reactivity - 0 

==================================================================================

The information contained herein has been developed based upon current available scientific data. New information 

may be developed from time to time which may render the conclusions of this report obsolete. Therefore, no 

warranty is extended as to the applicability of this information to the user’s intended purpose or the consequences of 

its use or misuse. 
BURMAH-CASTROL INC-BRAY PRODUCTS DIV. -- BRAYCOTE MICRONIC 756 E --

9150-00-082-7524

===================== Product Identification =====================

Product ID:BRAYCOTE MICRONIC 756 E

MSDS Date:01/01/1987

FSC:9150

NIIN:00-082-7524

MSDS Number: BCYCP

=== Responsible Party ===

Company Name:BURMAH-CASTROL INC-BRAY PRODUCTS DIV.

Emergency Phone Num:714-660-9414

CAGE:DO827

=== Contractor Identification ===

Company Name:BURMAH-CASTROL INC.

Address:30 EXECUTIVE AVE

City:EDISON

State:NJ

ZIP:08817

Country:US

Phone:201 287-3120

CAGE:DO827

Company Name:CASTROL INDUSTRIAL NORTH AMERICA INC SPECIALTY PRODUCTS

 DIV

Address:1001 WEST 31ST STREET

Box:City:DOWNERS GROVE

State:IL

ZIP:60515-1280

Country:US

Phone:800-621-2661/ FAX: 630-241-4140

CAGE:2R128

============= Composition/Information on Ingredients =============

Ingred Name:PETROLEUM SOLVENT,CAS#64742-46-7 (60-70%) TAKE TLV AS

 OILMIST

CAS:64742-46-7

RTECS #:JN9379645

Fraction by Wt: 65.0%

ACGIH TLV:5MG/CUM(OILMIST

Ingred Name:ADDITIVES (PROPRIETARY COMPOSITION)

Fraction by Wt: <35%

ACGIH TLV:NOT SPECIFIED

===================== Hazards Identification =====================

Effects of Overexposure:MAY AFFECT VERY SENSITIVE PERSON.MAY CAUSE EYE

 IRRITATION.PROLONGED CONTACT MAY DEFAT SKIN/DERMATITI

======================= First Aid Measures =======================

First Aid:EYE CONTACT:FLUSH THOROUGHLY WITH WATER;SKIN CONTACT;WIPE,

 THEN WASH WITH SOAP AND WATER.INGESTION:DO NOT INDUCE VOMITING,CALL

 PHYSICIAN

===================== Fire Fighting Measures =====================

Flash Point:215F/102C (COC)

Extinguishing Media:CARBON DIOXIDE, DRY CHEMICAL, FOAM, WATER FOG

Fire Fighting Procedures:USE WATER AS WATER FOG ONLY TO COOL CONTAINERS

 TO AVOID TEM

Unusual Fire/Explosion Hazard:NONE

http://www.hazard.com/msds/f2/bcy/bcycp.html

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================== Accidental Release Measures ==================

Spill Release Procedures:STOP FLOW.WIPE, MOP, OR ABSORB WITH

 CLAY,DIATOMACEOUS EARTH,OR OTHER INERT MATERIAL AND STORE IN CLOSED

 METAL CONTAINERS.

====================== Handling and Storage ======================

Handling and Storage Precautions:NO SPECIAL PRECAUTIONS,EXCEPT DO NOT

 STORE NEAR HEAT, OPEN FLAME, OR OTHER SOURCES OF IGNITION

Other Precautions:AVOID CONT WITH SKIN AND EYES.DO NOT USE CONTAMINATED

 CLOTHES.WASH AFTER EACH USE.

============= Exposure Controls/Personal Protection =============

Respiratory Protection:USE NIOSH APPROVED RESPIRATOR FOR ORGANIC

 VAPORS/OIL MIST

Ventilation:LOCAL EXHAUST RECOMMENDED ONLY FOR MIST

Protective Gloves:IMPERVIOUS

Eye Protection:SAFETY GLASSES RECOMMENDE

Other Protective Equipment:FULL WORK CLOTHING TO PREVENT REPEATED OR

 PROLONGED CONTACT.

Supplemental Safety and Health

MSDS DATED:10/17/85.

================== Physical/Chemical Properties ==================

HCC:V6

Boiling Pt:B.P. Text:>400/204C

Spec Gravity:0.875

Solubility in Water:INSOL.

Appearance and Odor:LOW VISCOSITY FLUID,DYED RED,PETROLEUM ODOR

================= Stability and Reactivity Data =================

Stability Indicator/Materials to Avoid:YES

AVOID STRONG OXIDIZING AGENTS

Hazardous Decomposition Products:COMBUSTION MAY PRODUCE CO AND

 ASPHYXIANTS.

==================== Disposal Considerations ====================

Waste Disposal Methods:CONTROLLED INCINERATION OR OTHER METHOD IAW

 LOCAL,STATE, AND FEDERAL REGULATIONS REGARDING HEALTH,AIR, AND

 WATER POLLUTION

 Disclaimer (provided with this information by the compiling agencies):

 This information is formulated for use by elements of the Department

 of Defense. The United States of America in no manner whatsoever,

 expressly or implied, warrants this information to be accurate and

 disclaims all liability for its use. Any person utilizing this

 document should seek competent professional advice to verify and

 assume responsibility for the suitability of this information to their

 particular situation.

http://www.hazard.com/msds/f2/bcy/bcycp.html

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Material Safety Data Sheet

Version: 1.1

11/01/2005

RTV112 12T-Tube (0.770LBS-0.350KG) 

SILICONE SEALANT 

Page 1/8 

1. CHEMICAL PRODUCT AND COMPANY IDENTIFICATION 

Manufactured By: GES Waterford Plant 

260 Hudson River Rd 

Waterford NY 12188 

Revised: 11/01/2005 

Preparer: PRODUCT STEWARDSHIP COMPLIANCE AND STANDARDS

CHEMTREC 1-800-424-9300

Chemical Family/Use: Sealant

Formula: Mixture 

HMIS 

Flammability: 2 Reactivity: 0 Health: 0 Prot. Equipm.: 

NFPA 

Flammability: 2 Reactivity: 0 Health: 1 Special Haz.: 

2. COMPOSITION/INFORMATION ON INGREDIENTS 

PRODUCT COMPOSITION CAS REG NO. WGT. %

A. HAZARDOUS

Methyltriacetoxysilane 4253-34-3 1 - 5 % 

Octamethylcyclotetrasiloxane 556-67-2 1 - 5 % 

Diacetoxydi-tert-butoxysilane 13170-23-5 1 - 5 % 

B. NON-HAZARDOUS

Siloxanes & Silicones, 

Dimethylpolymers 

w/Methylsilsesquioxanes

68554-67-6 5 - 10 %

Silica 7631-86-9 10 - 30 %

Dimethylpolysiloxane 70131-67-8 60 - 90 %

3. HAZARDS IDENTIFICATION 

EMERGENCY OVERVIEW 

WARNING! May be harmful if swallowed. Irritating to eyes, respiratory system and skin. Adverse liver and 

reproductive effects reported in animals. 

Form: solid Color: white Odor: Acetic acid 
Material Safety Data Sheet

Version: 1.1

11/01/2005

RTV112 12T-Tube (0.770LBS-0.350KG) 

SILICONE SEALANT 

Page 2/8 

POTENTIAL HEALTH EFFECTS

INGESTION 

May be harmful if swallowed. 

SKIN 

Uncured product contact will irritate lips, gums and tongue. Skin irritation is possible after contact with 

the uncured product.

INHALATION 

Inhalation of vapors may cause irritation of the respiratory tract. Applies in uncured state. 

EYES 

Eye irritation is possible after contact with the uncured product. 

MEDICAL CONDITIONS AGGRAVATED

None known. 

SUBCHRONIC (TARGET ORGAN )

Liver; Reproductive hazard.

CHRONIC EFFECTS / CARCINOGENICITY

This product or one of its ingredients present at 0.1% or more is NOT listed as a carcinogen or 

suspected carcinogen by NTP, IARC, or OSHA.

ROUTES OF EXPOSURE

dermal

OTHER

Acetic acid released during curing. This product contains methylpolysiloxanes which can 

generate formaldehyde at approximately 300 F (150 C) and above in atmospheres which contain 

oxygen. Formaldehyde is a skin and respiratory sensitizer, eye and throat irritant, acute toxicant, 

and potential cancer hazard. An MSDS for formaldehyde is available from GE Advanced 

Materials - Silicones.

4. FIRST AID MEASURES 

INGESTION 

Do not induce vomiting. If victim is conscious, give 1-3 glasses of water to drink. Never give 

anything by mouth to an unconscious person. Get medical attention if irritation persists.

SKIN 

To clean from skin, remove completely with a dry cloth or paper towel, before washing with 

detergent and water. Get medical attention if irritation persists.

INHALATION 

If inhaled, remove to fresh air. If not breathing give artificial respiration using a barrier device. If 

breathing is difficult give oxygen. Get medical attention.
Material Safety Data Sheet

Version: 1.1

11/01/2005

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EYES 

In case of contact, immediately flush eyes with plenty of water for at least 15 minutes and get 

medical attention if irritation persists.

NOTE TO PHYSICIAN 

Treatment is symptomatic and supportive.

5. FIRE-FIGHTING MEASURES 

FLASH POINT: ca. 72 °C; 161.60 °F

METHOD: 

IGNITION TEMPERATURE: 

FLAMMABLE LIMITS IN AIR - LOWER (%): not applicable

FLAMMABLE LIMITS IN AIR - UPPER (%): not applicable

SENSITIVITY TO MECHANICAL IMPACT: No 

SENSITIVITY TO STATIC DISCHARGE 

Sensitivity to static discharge is not expected.

EXTINGUISHING MEDIA 

All standard extinguishing agents are suitable.

SPECIAL FIRE FIGHTING PROCEDURES 

Combustible, Firefighters must wear NIOSH/MSHA approved positive pressure self-contained 

breathing apparatus with full face mask and full protective clothing.

6. ACCIDENTAL RELEASE MEASURES 

ACTION TO BE TAKEN IF MATERIAL IS RELEASED OR SPILLED 

Wipe, scrape or soak up in an inert material and put in a container for disposal. Wash walking 

surfaces with detergent and water to reduce slipping hazard. Wear proper protective equipment as 

specified in the protective equipment section. 

7. HANDLING AND STORAGE 

STORAGE 

Store away from heat, sources of ignition, and incompatibles. Keep out of the reach of children. Keep 

container tightly closed. 

PRECAUTIONS TO BE TAKEN IN HANDLING AND STORAGE 

Product releases acetic acid during application and curing. Use only in well-ventilated areas. Avoid 

contact with skin and eyes. Remove contact lenses before using sealant. Do not handle lenses until all 

sealant has been cleaned from the fingertips, nails and cuticles. Residual sealant may remain on 

fingers for several days and transfer to lenses and cause severe eye irritation. 
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8. EXPOSURE CONTROLS / PERSONAL PROTECTION 

ENGINEERING CONTROLS 

Eyewash stations; Showers; Exhaust ventilation

RESPIRATORY PROTECTION 

If exposure limits are exceeded or respiratory irritation is experienced, NIOSH/MSHA approved 

respiratory protection should be worn. Supplied air respirators may be required for non-routine or 

emergency situations. Respiratory protection must be provided in accordance with OSHA regulations 

(see 29 CFR 1910.134). 

PROTECTIVE GLOVES 

Impermeable or chemical resistant gloves. 

EYE AND FACE PROTECTION 

Safety glasses

OTHER PROTECTIVE EQUIPMENT 

Wear suitable protective clothing and eye/face protection.

Exposure Guidelines

Component CAS RN Source Value

Absence of values indicates none found 

PEL - OSHA Permissible Exposure Limit; TLV - ACGIH Threshold Limit Value; TWA - Time Weighted Average 

OSHA revoked the Final Rule Limits of January 19, 1989 in response to the 11th Circuit Court of Appeals decision (AFL-CIO v. OSHA) 

effective June 30, 1993. See 29 CFR 1910.1000 (58 FR 35338). 

9. PHYSICAL AND CHEMICAL PROPERTIES 

BOILING POINT - C & F: no data available

VAPOR PRESSURE (20 C) (MM HG): no data available

VAPOR DENSITY (AIR=1): no data available

FREEZING POINT: no data available

MELTING POINT: no data available

PHYSICAL STATE: solid

ODOR: Acetic acid 

COLOR: white

EVAPORATION RATE (BUTYL ACETATE=1): < 1 

SPECIFIC GRAVITY (WATER=1): 1.05 

DENSITY (KG/M3): ca. 1.05 KG/M3 

ACID / ALKALINITY (MEQ/G): Unknown

pH: Unknown

VOLATILE ORGANIC CONTENT (VOL): 5 %(m) 
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SOLUBILITY IN WATER (20 C): insoluble

SOLUBILITY IN ORGANIC SOLVENT (STATE 

SOLVENT): 

Soluble in toluene

VOC EXCL. H2O & EXEMPTS (G/L): < 52 

10. STABILITY AND REACTIVITY 

STABILITY 

Stable 

HAZARDOUS POLYMERIZATION 

Will not occur 

HAZARDOUS THERMAL DECOMPOSITION / COMBUSTION PRODUCTS 

carbon dioxide (CO2); Carbon monoxide; Acetic acid; Silicon dioxide.; formaldehyde

INCOMPATIBILITY (MATERIALS TO AVOID) 

None known. 

CONDITIONS TO AVOID 

None known. 

11. TOXICOLOGICAL INFORMATION 

ACUTE ORAL 

Unknown

ACUTE DERMAL 

Unknown

ACUTE INHALATION 

NONE FOUND

OTHER 

Octamethylcyclotetrasiloxane Ingestion: Rodents given large doses via oral gavage of 

octamethylcyclotetrasiloxane (1600 mg/kg day, 14 days) developed increased liver weights relative to 

unexposed control animals due to hepatocellular hyperplasia (increased number of liver cells which 

appear normal) as well as hypertrophy (increased cell size). Inhalation: In inhalation studies, 

laboratory rodents exposed to octamethylcyclotetrasiloxane (300 ppm five days week, 90 days) 

developed increased liver weights in female animals relative to unexposed control animals. When the 

exposure was stopped, liver weights returned to normal. Microscopic examination of the liver cells did 

not show any evidence of pathology. Inhalation studies utililizing laboratory rabbits and guinea pigs 

showed no effects on liver weights. Inhalation exposures typical of industrial usage (5-10 ppm) 

showed no toxic effects in rodents. Range finding reproductive studies were conducted (whole body 

inhalation, 70 days prior to mating, through mating, gestation and lactation) with 

octamethylcyclotetrasiloxane (D4). Rats were exposed to 70 and 700 ppm. In the 700 ppm group, 

there was a statistically significant reduction in mean litter size and in implantation sites. No D4 
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related clinical signs were observed in the pups and no exposure related pathological findings were 

found. Interim results from a two generation reproductive study in rats exposed to 500 and 700 ppm 

D4 (whole body inhalation, 70 days prior to mating, through mating, gestation and lactation) resulted in 

a statistically significant decrease in live mean litter size as well as extended periods of off-spring 

delivery (dystocia). These results were not observed at the 70 and 300 ppm dosing levels. Preliminary 

results from an ongoing 24-month combined chronic/oncogenicity study in rats exposed to 10, 30, 150, 

or 700 ppm D4 showed test-article related effects in the kidney (male and female) and uterus of rats 

exposed for 12 to 24 months. These effects include increased kidney weight and severity of chronic 

nephropathy, increased uterine weight, increased incidence of endometrial cell hyperplasia, and an 

increased incidence of endometrial adenomas. All of these effects are limited to the 700 ppm 

exposure group. The relevance of these data to humans is unclear. Further studies are ongoing. In 

developmental toxicity studies, rats and rabbits were exposed to octamethylcyclotetrasiloxane at 

concentrations up to 700 ppm and 500 ppm respectively. No teratogenic effects (birth defects) were 

observed in either study.

SENSITIZATION 

no data available

SKIN IRRITATION 

no data available

EYE IRRITATION 

no data available

MUTAGENICITY 

Unknown

12. ECOLOGICAL INFORMATION 

ECOTOXICOLOGY 

no data available

CHEMICAL FATE 

no data available

DISTRIBUTION 

no data available

13. DISPOSAL CONSIDERATIONS 

DISPOSAL METHOD 

Disposal should be made in accordance with federal, state and local regulations.

14. TRANSPORT INFORMATION 

Not Regulated if Section is Blank
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DOT SHIPPING NAME: Combustible liquid, n.o.s. 

(METHYLTRIACETOXYSILANE,,)

DOT HAZARD CLASS: CBL

DOT LABEL (S): 

UN/NA NUMBER: NA 1993 

PACKING GROUP: III

Remarks

IMDG: DOT Regulated Only - Not IMDG Regulated 

15. REGULATORY INFORMATION 

Inventories 

Canada DSL Inventory y (positive listing) 

Japan Inventory of Existing & 

New Chemical Substances 

(ENCS) 

y (positive listing) 

Korea Existing Chemicals 

Inventory (KECI) 

y (positive listing) 

China Inventory of Existing 

Chemical Substances 

y (positive listing) 

Australia Inventory of Chemical 

Substances (AICS) 

y (positive listing) 

Philippines Inventory of 

Chemicals and Chemical 

Substances (PICCS) 

y (positive listing) 

TSCA list y (positive listing) 

EU list of existing chemical 

substances 

y (positive listing) 

Canada NDSL Inventory n (Negative listing) 

For inventories that are marked as quantity restricted or special cases, please contact GE.

US Regulatory Information 

CERCLA 

PRODUCT COMPOSITION Chemical CERCLA Reportable Quantity 

CLEAN AIR ACT 

CLEAN WATER ACT 

SARA SECTION 302 
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SARA (311,312) HAZARD CLASS 

Acute Health Hazard; Chronic Health Hazard; Fire Hazard

SARA (313) CHEMICALS 

Canadian Regulatory Information 

WHMIS HAZARD CLASS 

Combustible Liquid, D2A VERY TOXIC MATERIALS, D2B TOXIC MATERIALS

Other 

SCHDLE B/HTSUS: 3214.10 Mastic Based on Rubber 

ECCN: EAR99 

CALIFORNIA PROPOSITION 65 

This product does not contain any chemicals known to State of California to cause cancer, birth 

defects or any other harm. 

16. OTHER INFORMATION 

OTHER 

C = ceiling limit NEGL = negligible EST = estimated NF = none found NA = not 

applicable UNKN = unknown NE = none established REC = recommended ND = none 

determined V = recommended by vendor SKN = skin TS = trade secret R = 

recommended MST = mist NT = not tested STEL = short term exposure limit ppm = 

parts per million ppb = parts per billion By-product= reaction by-product, TSCA inventory status 

not required under 40 CFR part 720.30(h-2)., These data are offered in good faith as typical values 

and not as product specifications. No warranty, either expressed or implied, is made. The 

recommended industrial hygiene and safe handling procedures are believed to be generally 

applicable. However, each user should review these recommendations in the specific context of the 

intended use and determine whether they are appropriate. 
MANUFACTURER

Devcon Consumer Products

2107 West Blue Heron BLVD.

Riviera Beach, FL 33404

Emergency telephone number 

(CHEMTREC): (800) 424-9300

Other Calls: (561) 845-2425

EMERGENCY INFORMATION

SUPER GLUE

Printed: 1/22/2003

2. COMPOSITION/INFORMATION ON INGREDIENTS

"TLV" means the Threshold Limit Value exposure (eight-hour, time-weighted average, unless otherwise noted) established by the American 

Conference of Governmental Industrial Hygienists. "STEL" indicates a short-term exposure limit. "PEL" indicates the OSHA Permissible Exposure 

Limit."n/e" indicates that no exposure limit has been established. An asterisk (*) indicates a substance whose identity is a trade secret of our supplier 

and unknown to us.

Last revised: 08/13/02

HAZARDOUS CONSTITUENTS

 Emergency Overview

WARNING! Contains Cyanoacrylate Esters. Can cause severe eye injury. Bonds body tissue in seconds. 

3. HAZARDS IDENTIFICATION

Appearance, form, odor: colorless viscous liquid with slightly pungent odor.

S-290 S-2900 S-2940 S-298

This product appears in the following stock number(s):

Constituent ACGIH 

TLV

CAS No. Weight

 percent

OSHA

PEL

Other 

Limits

Abbr.

Ethyl-2-cyanoacrylate 7085850 >80 0.2 ppm n/e n/e

Polymethyl methacrylate 9011874 <20 n/e n/e n/e

Eyes: May bond eyelid. A large drop may cause a burn upon solidification. Lachrymator, double vision.

Inhalation:

Avoid prolonged inhalation. Vapors may cause irritation of nose and bronchial passages.

Potential health effects

Skin: Bonds skin rapidly and strongly. Large quantities may cause burns.

Symptoms of acute overexposure:

Primary routes of exposure: Skin contact Skin absorption Eye contact Inhalation Ingestion

Exposure limits

1. CHEMICAL PRODUCT AND COMPANY IDENTIFICATION

Tradename: SUPER GLUE

General use: Bonds skin and eyes immediately. In case of skin or eye contact, do not force bonded surfaces

apart; follow first aid instructions below.

Chemical family: Cyanoacrylates

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Unusual fire and explosion hazards: 

Water may spread fire due to product floating on surface. Cloths used to wipe spills may polymerize and auto-ignite.

Hazardous products of combustion:

Oxides of carbon, oxides of nitrogen, trace amounts of hydrogen cyanide and unidentified organic combustion

products.

Containment: 

N/A

Spill control: 

Flood area with water to cure and to control product vapors. Wear protective clothing and a NIOSH approved

respirator for organic vapors or a self-contained breathing apparatus if needed.

6. ACCIDENTAL RELEASE MEASURES

Water Carbon dioxide Dry chemical Foam Alcohol foam

Extinguishing media:

Flash Point (°F): > 170 Method: SCC

Explosive limits in air (percent) -- Lower: nd Upper: nd

Special firefighting procedures: 

Wear full protective equipment including self-contained breathing apparatus.

5. FIRE FIGHTING MEASURES

First aid for skin: 

Immerse in warm soapy water. Do not force apart.

First aid for ingestion: 

Apply warm water to lips. Use maximum wetting with saliva. Position victim to prevent ingestion of solid. Call a

physician.

First aid for inhalation: 

Move to fresh air. If symptoms persist, call a physician.

4. FIRST AID MEASURES

First aid for eyes: 

Flush with lukewarm water for 15 minutes. Call a physician immediately. Do not attempt to peal bonded eyelid from

eye!

Medical conditions which may be aggravated by exposure: 

Eye, skin, respiratory disorders.

 Effects of chronic overexposure: 

Possible respiratory sensitization, asthmatic effects.

Other effects:

None known.

OSHA regulated: No ACGIH: No National Toxicology Program: No

International Agency for Research on Cancer: No

Cancer-suspect constituent(s) : none

Carcinogenicity --

Ingestion:

The adhesive solidifies and adheres in the mouth, almost impossible to swallow. Lips may bond.

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9. PHYSICAL AND CHEMICAL PROPERTIES

Melting point (°F): n/d

Boiling point (°F): >300

Vapor density (air = 1): >1

Specific gravity: 1.08

Solubility in water: <0.1%

pH (5% solution or slurry in water): n/d

Percent volatile by volume: 0

VOC (grams/liter): n/d

Percent solids by weight: 100

Vapor pressure (mmHg): 0.17 mm Hg at 68 °F

Cleanup: 

Scrape up cured product and dispose of in accordance with all applicable disposal regulations.

Special procedures: 

Contact with cotton or wool may result in a strong exothermic reaction which can result in a fire. 

Storage: 

Store away from heat and direct sunlight. Store in a dry location. Keep container tightly closed when not in use.

Other engineering controls : 

Have emergency shower and eye wash available.

Skin protection: 

Polyethylene gloves and apron. Do not wear rubber or cloth gloves.

Respiratory protection: 

Use NIOSH approved respirator for organic vapors or self-contained breathing apparatus if appropriate ventillation is

not available.

Personal protective equipment

Eye and face protection: 

Safety glasses with side shields or safety goggles.

8. EXPOSURE CONTROLS/PERSONAL PROTECTION 

Engineering controls

Ventilation : 

General ventillation is adequate for occasional use. Where the adhesive is in continual use or is heated, or heating

cured adhesive over 400 F, provide local exhaust to keep vapors below the TLV.

7. HANDLING AND STORAGE

Handling precautions: 

Cyanoacrylates bond skin rapidly and strongly. May also bond eyelid to eyelid and/or skin. Wear appropriate

personal protective equipment (see Section 8). Provide appropriate ventilation/respiratory protection against

decomposition products (see Section 10) during welding/flame cutting operations and to protect against nuisance dust

during sanding/grinding of cured product. 

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Acute dermal effects: 

Instantly bonds skin. Large drops may cause burns upon solidification.

LD50 (rabbit): not determined

Acute inhalation effects: 

Causes irritation of nose and bronchial passages.

LC50 (rat): not determined Exposure: hours. 

Hazardous products of decomposition:

Oxides of carbon, oxides of nitrogen, trace amounts of hydrogen cyanide and unidentified organic decomposition

products.

Conditions under which hazardous polymerization may occur: 

Contamination with water,alkaline materials or peroxides may build-up pressure in a closed container.

Incompatible materials: 

Base cotton, wool, water, alkaline materials

Eye irritation:

Instantly bonds eyelid to eyelid and/or eye.

Subchronic effects: 

None known.

Other chronic effects: 

None known.

Carcinogenicity, teratogenicity, and mutagenicity: 

None known.

Mobility and persistence: 

Acute oral effects: LD50 (rat): not determined

11. TOXICOLOGICAL INFORMATION

10. STABILITY AND REACTIVITY

This material is chemically Unstable. 

Conditions to avoid : 

High temperatures and humidity

Hazardous polymerization may occur.

12 ECOLOGICAL INFORMATION

Ecotoxicity: 

No data available.

Constituent Oral LD50

(rat) 

Dermal LD50

(rabbit)

Inhalation LC50

4hr, (rat)

Ethyl-2-cyanoacrylate n/d n/d n/d

Polymethyl methacrylate n/d n/d n/d

Toxicological information on hazardous chemical constituents of this product:

'n/d' = 'not determined'

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No data available

Environmental fate: 

No data available.

For purposes of SARA Section 312 hazardous materials inventory reporting, the following hazard

14. TRANSPORT INFORMATION

Proper shipping name: Non-regulated

Technical name : N/A

Hazard class : N/A

UN number: N/A

Packing group: N/A

Emergency Response Guide no.: N/A

IMDG page number: N/A

Other: N/A

LtdQty : N/A

ORM-D : N/A

13. DISPOSAL CONSIDERATIONS

Waste management recommendations: 

As shipped this product is not a hazardous waste as specified in 40 CFR 261. Dispose of according to local, state,

and federal regulations.

Please see also Section 15, Regulatory Information.

Constituent Extremely 

Hazardous* 

Toxic

Chemical**

CERCLA 

RQ (lbs)

TSCA 12B Export

Notification

Ethyl-2-cyanoacrylate No No 0.0 Not required

Polymethyl methacrylate No No 0.0 Not required

Regulatory status of hazardous chemical constituents of this product:

*Consult the appropriate regulations for emergency planning and release reporting requirements for substances on the SARA Section 301

Extremely Hazardous Substance list. 

**Substances for which the "Toxic Chemical" column is marked "Yes" are on the SARA Section 313 list of

Toxic Chemicals, for which release reporting may be required. For specific requirements, consult the appropriate regulations.

15. REGULATORY INFORMATION

U.S. Federal Regulations

The following RCRA code(s) applies to this material if it becomes waste:

None

All ingredients of this product are listed, or are exempt from listing, on the TSCA inventory.

TSCA

:

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classes apply to this material:

- Immediate health hazard -- Fire hazard -

The information and recommendations in this document are based on the best information available to us at the time of preparation, but we make no 

other warranty, express or implied, as to its correctness or completeness, or as to the results of reliance on this document. 

Hazardous Materials 

Identification System (HMIS) 

ratings:

Health

2*

Flammability 

2

Reactivity 

2

16. OTHER INFORMATION

WHMIS hazard class(es) : D2B; B3

Canadian regulations

All components of this product are on the Domestic Substances List.

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PAGE: 1 of 3

PRINT DATE: 21/09/2000

SAFETY DATA SHEET REF: X0039

1. IDENTIFICATION OF THE SUBSTANCE/PREPARATION AND THE COMPANY/UNDERTAKING

Product name: 5-MINUTE EPOXY RESIN

Supplier: ITW Devcon

Shannon Industrial Estate Brunel Close, Park Farm Ind.

Est.,

Co. Clare, Ireland. Wellingborough, Northants

NN8 6QX

Emergency telephone number: 353(61)471299 01933 675299

Fax No: 353(61)471285 01933 675765

2. COMPOSITION/INFORMATION ON INGREDIENTS

Identification of the preparation

Chemical Name CAS-No EEC-No Class Weight %

BISPHENOL A-(EPICHLORHYDRIN)

{REACTION PRODUCT}

25068-38-6 603-074-00-

8

Xi; R36/38 R43 >60

3. HAZARDS IDENTIFICATION

Most important hazards: Moderate skin irritation

Specific hazards Irritating to eyes and skin. May cause sensitization by skin contact.

4. FIRST AID MEASURES

General advice: Show this safety data sheet to the doctor in attendance.Avoid contact with skin and

eyes.

Inhalation: Move to fresh air. Consult a physician after significant exposure.

Skin contact: Remove immediately adhering matter, Wash off immediately with soap and plenty of

water.If skin irritation persists, call a physician.

Eye contact: In case of contact with eyes, rinse immediately with plenty of water and seek medical

advice.

Ingestion: Rinse mouth, Do not induce vomiting, Call a physician immediately. If a person vomits

when lying on his back, turn over on his side.

5. FIRE-FIGHTING MEASURES

Suitable extinguishing media: dry powder, foam, Carbon Dioxide (CO 2

)

Extinguishing media which must not be used for safety reasons:

high volume water jet.

Specific hazards: Burning produces irritant fumes.

Special protective equipment for firefighters: In case of fire, wear a self contained breathing

apparatus, protective suit

Specific methods: Standard procedure for chemical fires

6. ACCIDENTAL RELEASE MEASURES

Personal precautions: Avoid contact with the skin and the eyes.Use personal protective

equipment.Ensure adequate ventilation.

Environmental precautions: Do not contaminate water. Avoid subsoil penetration.

Methods for cleaning up: Dam up, Scrape up, Soak up with inert absorbent material, Transfer to

covered steel drums.

7. HANDLING AND STORAGE

Handling: Use only in well-ventilated areas. Keep away from heat and sources of ignition. General

industrial hygiene practice.

Storage: Keep containers tightly closed in a cool, well-ventilated place.

8. EXPOSURE CONTROLS / PERSONAL PROTECTION

Chemical Name: National occupational exposure limits (Ref: British COSHH - EH40):
PAGE: 2 of 3

PRINT DATE: 21/09/2000 Product name: 5-MINUTE EPOXY RESIN

REF: X0039

BISPHENOL A-(EPICHLORHYDRIN) {REACTION PRODUCT} no data available

Engineering measures to

reduce exposure

- Respiratory protection: No personal respiratory protective equipment normally required. In case

of insufficient ventilation, wear suitable respiratory equipment.

- Hand protection: solvent-resistant gloves (butylrubber).

- Eye protection: safety glasses with side-shields, goggles.

- Skin and body protection: Wear as appropriate :.

Hygiene measures: Wash hands before breaks and immediately after handling the product,

Keep away from food, drink and animal feeding stuffs. Do not smoke.

General industrial hygiene practice.

9. PHYSICAL AND CHEMICAL PROPERTIES

Colour: light yellow. Odour: slight. Form: liquid.

pH: ( 50 g/l H2O) 7 ( 20 °C)

Boiling point/range: > 200 °C

Flash point: > 150 °C

Melting point/range: n/d °C

Autoignition temperature: >290 °C

Flammability (solid, gas): Not applicable

Oxidizing properties: Not applicable.

0.01 mm Hg ( 20 °C) Vapour pressure:

Relative density: - lower 1.147 ( 25 °C)

VOC: 1160 g/l

Water solubility negligible.

Partition coefficient (n-octanol/water) > 2.5

10. STABILITY AND REACTIVITY

Stability: Stable.

Conditions to avoid: Prolonged heating at temperatures above 50°C.

Materials to avoid: strong acids and oxidizing agents, amines.

Hazardous decomposition products: No decomposition if stored normally.

11. TOXICOLOGICAL INFORMATION

Acute toxicity: Epoxy constituents: LD50/oral/rat = 30g/Kg

 LD50/dermal/rabbit = > 20 ml/Kg

 LC50/inhalation/4h/rat = fatality = 0

Local effects: Moderate skin irritation

Sensitization: May cause sensitization by skin contact.

Long term toxicity: Components of the product may be absorbed into the body by inhalation and

ingestion.. Repeated or prolonged skin contact may cause allergic reactions with

susceptible persons.

12. ECOLOGICAL INFORMATION

Mobility: Do not contaminate water. Do not let product enter drains.

Other information: formulated product - not applicable.

13. DISPOSAL CONSIDERATIONS

Waste from residues / unused products: Solidify unexposed surplus and dispose of together with

processed material as cured plastic waste - In accordance

with local and national regulations

Contaminated packaging: In accordance with local and national regulations

European waste Catalogue No: 08 04 99
PAGE: 3 of 3

Product name: 5-MINUTE EPOXY RESIN PRINT DATE: 21/09/2000

REF: X0039

14. TRANSPORT INFORMATION

Proper shipping name: Not classified as dangerous in the meaning of transport regulations: UN,

ADR/RID, IMO & IATA/ICAO.

15. REGULATORY INFORMATION

Classification according to European directive on classification of hazardous preparations 93/21/EEC

- Contains: BISPHENOL A-(EPICHLORHYDRIN) {REACTION PRODUCT}

- Symbol(s):

Xi

R -phrase(s): R43 - May cause sensitization by skin contact. R36 - Irritating to eyes.. R38 - Irritating to

skin.

S -phrase(s): S2 - Keep out of reach of children.. S28 - After contact with skin, wash immediately with

plenty of .. water. S37/39 - Wear suitable gloves and eye/face protection.

16. OTHER INFORMATION

Recommended use: Adhesives.

Recommended restrictions:

When used in a mixture, read the labels and safety data sheets of all components.

Revision date: 01/10/2000.

The information provided in this Safety Data Sheet is correct to the best of our knowledge, information and belief at the date of its publication