ANALYTICAL REPORT

Job Number: 500-53034-1

Job Description: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, SC 29651

Attention: Mr. Robert Stevens

_____________________________________________

Approved for release.

Cindy R Pritchard

Project Mgmt. Assistant

12/26/2012 4:17 PM

Designee for

Donna L Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

12/26/2012

cc: Mr. David Kirby

Mr. Robert Malcomson

These test results meet all the requirements of NELAC for accredited parameters.

The Lab Certification ID# is 100201.

All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears

on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be

reproduced only in its entirety.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.

TestAmerica Laboratories, Inc.

TestAmerica Chicago 2417 Bond Street, University Park, IL 60484

Tel (708) 534-5200 Fax (708) 534-5211 www.testamericainc.com

Page 1 of 360 12/26/2012
Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56

Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86

Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 87

Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88

Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 113

Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117

Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 117

Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 147

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 168

Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 168

Page 2 of 360 12/26/2012
Table of Contents

Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 171

Method 8260B MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 174

Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 176

Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 182

Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 185

Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 185

Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 186

Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187

Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 190

Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 190

Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 201

Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 205

Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 221

Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 229

Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 235

Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 247

Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 251

Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 257

Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 269

General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 275

Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 276

Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 277

Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 280

Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 280

Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 284

Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 285

Page 3 of 360 12/26/2012
Table of Contents

Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 287

Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 290

Gen Chem Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 308

Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 310

Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 318

Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 333

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 355

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 359

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 360

Page 4 of 360 12/26/2012
Job Narrative

500-53034-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/7/2012 9:50 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 3.3o C.

GC/MS VOA 

Method(s) 8260B: Due to the high concentration of Acetone, the matrix spike / matrix spike duplicate (-2MS/-2MSD) for sample -2 could 

not be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.

No other analytical or quality issues were noted.

Metals 

No analytical or quality issues were noted.

General Chemistry 

No analytical or quality issues were noted.

Page 5 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53034-1

Instrument ID: CMS16 Analysis Batch Number: 170196

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD1 500-170196/6 IC

11/19/12 12:14 16I1119A.D GC Column: DB624 ID: 0.2(mm)

Acetone 1.91 Poor chromatography wernerb 11/19/12 13:19

8260B

Page 6 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53034-1

Instrument ID: CMS22 Analysis Batch Number: 172614

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD01 500-172614/2 IC

12/11/12 14:23 22I1211A.D GC Column: DB624 ID: 0.2(mm)

Trichloroethene 7.55 Baseline alikpalae 12/11/12 19:50

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD02 500-172614/3 IC

12/11/12 14:51 22I1211B.D GC Column: DB624 ID: 0.2(mm)

Bromomethane 2.01 Baseline alikpalae 12/11/12 19:54

Acetonitrile 3.59 Split Peak alikpalae 12/11/12 19:54

Tetrachloroethene 9.75 Split Peak alikpalae 12/11/12 19:54

8260B

Page 7 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53034-1

Instrument ID: CMS22 Analysis Batch Number: 172615

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD01 500-172615/2 IC

12/11/12 14:23 22I1211A.D GC Column: DB624 ID: 0.2(mm)

Trichloroethene 7.55 Baseline alikpalae 12/11/12 19:50

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD02 500-172615/3 IC

12/11/12 14:51 22I1211B.D GC Column: DB624 ID: 0.2(mm)

Bromomethane 2.01 Baseline alikpalae 12/11/12 19:54

Acetonitrile 3.59 Split Peak alikpalae 12/11/12 19:54

Tetrachloroethene 9.75 Split Peak alikpalae 12/11/12 19:54

8260B

Page 8 of 360 12/26/2012
SAMPLE SUMMARY

Client: Project Integration, Inc Job Number: 500-53034-1

Lab Sample ID Client Sample ID Client Matrix Sampled Received

Date/Time Date/Time

500-53034-1 FC Composite 2 Solid 12/06/2012 1430 12/07/2012 0950

500-53034-2 FC Discrete 2 Solid 12/06/2012 1425 12/07/2012 0950

500-53034-3 FC EB 2 Water 12/06/2012 1415 12/07/2012 0950

500-53034-4 Trip Blank Water 12/06/2012 0000 12/07/2012 0950

TestAmerica Chicago Page 9 of 360 12/26/2012
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53034-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53034-1 FC COMPOSITE 2

Barium 377 B 3.64 mg/Kg 6010B

Copper 959 3.64 mg/Kg 6010B

Chromium 9290 3.64 mg/Kg 6010B

Nickel 78.7 3.64 mg/Kg 6010B

Lead 261 B 1.82 mg/Kg 6010B

Vanadium 158 1.82 mg/Kg 6010B

Zinc 381 7.28 mg/Kg 6010B

Mercury 0.635 0.0600 mg/Kg 7471A

Flashpoint >176 40.0 Degrees F 1010

Chromium, hexavalent 4.31 3.60 mg/Kg 7196A

Sulfide 223 86.5 mg/Kg 9034

pH 9.02 0.200 SU 9045C

HEM (Oil & Grease) 21500 1780 mg/Kg 9071B

Percent Moisture 73 0.10 % Moisture

Percent Solids 27 0.10 % Moisture

% Moisture 73.0 0.100 % SM 2540G

Total Solids 27.0 0.100 % SM 2540G

TCLP

Copper 0.0355 0.0250 mg/L 6010B

Chromium 0.0524 0.0250 mg/L 6010B

Nickel 0.646 0.0250 mg/L 6010B

Zinc 0.0685 J 0.100 mg/L 6010B

Mercury 0.0000559 J B 0.000200 mg/L 7470A

500-53034-2 FC DISCRETE 2

Acetone 9130 870 ug/Kg 8260B

2-Butanone (MEK) 72.6 17.4 ug/Kg 8260B

Percent Moisture 71 0.10 % Moisture

Percent Solids 29 0.10 % Moisture

TestAmerica Chicago Page 10 of 360 12/26/2012
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53034-1

Description Lab Location Method Preparation Method

Matrix: Solid

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Metals TAL CHI SW846 3050B

Metals (ICP) TAL CHI SW846 6010B

TCLP Extraction TAL CHI SW846 1311

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

TCLP Extraction TAL CHI SW846 1311

Preparation, Mercury TAL CHI SW846 7470A

Mercury (CVAA) TAL CHI SW846 7471A

Preparation, Mercury TAL CHI SW846 7471A

Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010

Chromium, Hexavalent TAL CHI SW846 7196A

Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

pH TAL CHI SW846 9045C

HEM and SGT-HEM TAL CHI SW846 9071B

Preparation, HEM and SGT-HEM TAL CHI SW846 9071B

Percent Moisture TAL CHI EPA Moisture

Total, Fixed, and Volatile Solids TAL CHI SM SM 2540G

Matrix: Water

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

Preparation, Mercury TAL CHI SW846 7470A

HEM and SGT-HEM TAL CHI 1664A 1664A

HEM and SGT-HEM (SPE) TAL CHI 1664A 1664A

Chromium, Hexavalent TAL CHI SW846 7196A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

TestAmerica Chicago Page 11 of 360 12/26/2012
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53034-1

Description Lab Location Method Preparation Method

Lab References:

TAL CHI = TestAmerica Chicago

Method References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago Page 12 of 360 12/26/2012
METHOD / ANALYST SUMMARY

Client: Project Integration, Inc Job Number: 500-53034-1

Method Analyst Analyst ID

SW846 8260B Alikpala, Elaine EA

SW846 8260B Werner, Brian D BDW

SW846 6010B Jones, Paul PJ

SW846 6010B Smith, Todd D TDS

SW846 7470A Bills, Brandon J BJB

SW846 7471A Bills, Brandon J BJB

SW846 1010 Wasowicz, Andrew P APW

1664A 1664A Brogan, Mary T MTB

SW846 7196A Deb, Khona KD

SW846 7196A Wasowicz, Andrew P APW

SW846 9014 Treadwell, Eliane A EAT

SW846 9034 Boyd, Cheryl L CLB

SW846 9034 Moore, Colleen L CLM

SW846 9045C Moore, Colleen L CLM

SW846 9071B Brogan, Mary T MTB

EPA Moisture Veldhuizen, Chris M CMV

SM SM 2540G Veldhuizen, Chris M CMV

TestAmerica Chicago

Page 13 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

FC Discrete 2

Client Matrix: % Moisture: 71.3

500-53034-2

Solid

Date Sampled: 12/06/2012 1425

Date Received: 12/07/2012 0950

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/12/2012 0925

12/12/2012 0925

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53034-02.D

5 g

5 mL

5030B

CMS16

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-172698

N/A

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

2-Butanone (MEK) 72.6 6.30 17.4

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 117 70 - 134

Toluene-d8 (Surr) 104 75 - 122

4-Bromofluorobenzene (Surr) 97 70 - 122

Dibromofluoromethane 109 75 - 120

TestAmerica Chicago Page 14 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

FC Discrete 2

Client Matrix: % Moisture: 71.3

500-53034-2

Solid

Date Sampled: 12/06/2012 1425

Date Received: 12/07/2012 0950

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/11/2012 1127

12/13/2012 2204

50

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53034-02C.D

5 g

Run Type: DL 5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-172879

500-172604

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

Acetone 9130 226 870

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 97 75 - 125

Toluene-d8 (Surr) 98 75 - 120

4-Bromofluorobenzene (Surr) 92 75 - 120

Dibromofluoromethane 97 75 - 120

TestAmerica Chicago Page 15 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

FC EB 2

Client Matrix:

500-53034-3

Water

Date Sampled: 12/06/2012 1415

Date Received: 12/07/2012 0950

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/13/2012 1533

12/13/2012 1533

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53034-03.D

5 mL

5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-172880

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 95 75 - 125

Toluene-d8 (Surr) 98 75 - 120

4-Bromofluorobenzene (Surr) 95 75 - 120

Dibromofluoromethane 95 75 - 120

TestAmerica Chicago Page 16 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

Trip Blank

Client Matrix:

500-53034-4

Water

Date Sampled: 12/06/2012 0000

Date Received: 12/07/2012 0950

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/13/2012 1415

12/13/2012 1415

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53034-04.D

5 mL

5 mL

5030B

CMS22

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-172880

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 91 75 - 125

Toluene-d8 (Surr) 100 75 - 120

4-Bromofluorobenzene (Surr) 93 75 - 120

Dibromofluoromethane 94 75 - 120

TestAmerica Chicago Page 17 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

FC Composite 2

Client Matrix: % Moisture: 72.6

500-53034-1

Solid

Date Sampled: 12/06/2012 1430

Date Received: 12/07/2012 0950

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51210B

Dilution: 1.0 Initial Weight/Volume: 1.0011 g

12/10/2012 2054 Final Weight/Volume: 100 mL

12/07/2012 1600

3050B

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-172535

Prep Batch: 500-172306

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Barium 377 B 0.433 3.64

Copper 959 0.987 3.64

Chromium 9290 0.608 3.64

Nickel 78.7 0.797 3.64

Lead 261 B 0.626 1.82

Vanadium 158 0.276 1.82

Zinc 381 2.50 7.28

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: P51211B

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/11/2012 2021 Final Weight/Volume: 50 mL

12/11/2012 0913

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-172697

500-172581

500-172501

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/10/2012 1448

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Barium <0.500 0.0100 0.500

Copper 0.0355 0.0100 0.0250

Chromium 0.0524 0.0100 0.0250

Nickel 0.646 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc 0.0685 J 0.0200 0.100

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: 121212RA.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/12/2012 0941 Final Weight/Volume: 25 mL

12/11/2012 1500

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-172764

500-172640

500-172501

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/10/2012 1448

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Mercury 0.0000559 J B 0.0000200 0.000200

7471A Mercury (CVAA)

TestAmerica Chicago Page 18 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

FC Composite 2

Client Matrix: % Moisture: 72.6

500-53034-1

Solid

Date Sampled: 12/06/2012 1430

Date Received: 12/07/2012 0950

7471A Mercury (CVAA)

7471A Instrument ID:

Lab File ID: 1211112B.PRN

Dilution: 1.0 Initial Weight/Volume: 0.6083 g

12/11/2012 1259 Final Weight/Volume: 50 mL

12/10/2012 1500

7471A

HG5

Analysis Date:

Prep Date:

Analysis Batch: 500-172626

Prep Batch: 500-172460

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Mercury 0.635 0.0229 0.0600

TestAmerica Chicago Page 19 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

Client Sample ID:

Lab Sample ID:

FC EB 2

Client Matrix:

500-53034-3

Water

Date Sampled: 12/06/2012 1415

Date Received: 12/07/2012 0950

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P6121112B.asc

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/11/2012 2014 Final Weight/Volume: 50 mL

12/10/2012 1430

3010A

ICP6

Analysis Date:

Prep Date:

Analysis Batch: 500-172699

Prep Batch: 500-172512

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Barium <0.0100 0.000440 0.0100

Copper <0.0100 0.00106 0.0100

Chromium <0.0100 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead <0.00500 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc <0.0200 0.00472 0.0200

7470A Mercury (CVAA)

7470A Instrument ID:

Lab File ID: 121212RA.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/12/2012 1115 Final Weight/Volume: 25 mL

12/11/2012 1500

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-172764

Prep Batch: 500-172642

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000710 0.000200

TestAmerica Chicago Page 20 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC Composite 2

Client Matrix:

500-53034-1

Solid

Date Sampled: 12/06/2012 1430

Date Received: 12/07/2012 0950

Analyte Result Qual Units MDL RL Dil Method

Flashpoint >176 Degrees F 40.0 40.0 1.0 1010

Analysis Batch: 500-173558 Analysis Date (Start): 12/19/2012 1524 (End) 12/19/2012 1603 DryWt Corrected: N

Chromium, hexavalent 4.31 mg/Kg 1.40 3.60 1.0 7196A

Analysis Batch: 500-173341 Analysis Date (Start): 12/18/2012 1548 (End) 12/18/2012 1548 DryWt Corrected: Y

Prep Batch: 500-173258 Prep Date: 12/18/2012 1000

Cyanide, Total <1.81 mg/Kg 0.597 1.81 1.0 9014

Analysis Batch: 500-173074 Analysis Date (Start): 12/14/2012 1602 (End) 12/14/2012 1602 DryWt Corrected: Y

Prep Batch: 500-173012 Prep Date: 12/14/2012 1325

Sulfide 223 mg/Kg 13.8 86.5 1.0 9034

Analysis Batch: 500-173039 Analysis Date: 12/14/2012 1546 DryWt Corrected: Y

Prep Batch: 500-172997 Prep Date: 12/14/2012 1135

Sulfide, Reactive <48.6 mg/Kg 3.79 48.6 1.0 9034

Analysis Batch: 500-172643 Analysis Date: 12/11/2012 1239 DryWt Corrected: N

Prep Batch: 500-172578 Prep Date: 12/11/2012 1125

pH 9.02 SU 0.200 0.200 1.0 9045C

Analysis Batch: 500-173479 Analysis Date (Start): 12/20/2012 0620 (End) 12/20/2012 0719 DryWt Corrected: N

HEM (Oil & Grease) 21500 mg/Kg 788 1780 1.0 9071B

Analysis Batch: 500-173330 Analysis Date: 12/19/2012 1027 DryWt Corrected: Y

Prep Batch: 500-173324 Prep Date: 12/19/2012 0510

Percent Moisture 73 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-172275 Analysis Date: 12/07/2012 1259 DryWt Corrected: N

Percent Solids 27 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-172275 Analysis Date: 12/07/2012 1259 DryWt Corrected: N

% Moisture 73.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-172359 Analysis Date: 12/08/2012 1537 DryWt Corrected: N

Total Solids 27.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-172359 Analysis Date: 12/08/2012 1537 DryWt Corrected: N

TestAmerica Chicago Page 21 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC Discrete 2

Client Matrix:

500-53034-2

Solid

Date Sampled: 12/06/2012 1425

Date Received: 12/07/2012 0950

Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 71 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-172720 Analysis Date: 12/12/2012 1111 DryWt Corrected: N

Percent Solids 29 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-172720 Analysis Date: 12/12/2012 1111 DryWt Corrected: N

TestAmerica Chicago Page 22 of 360 12/26/2012
Analytical Data

Client: Project Integration, Inc Job Number: 500-53034-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC EB 2

Client Matrix:

500-53034-3

Water

Date Sampled: 12/06/2012 1415

Date Received: 12/07/2012 0950

Analyte Result Qual Units MDL RL Dil Method

HEM (Oil & Grease) <5.35 mg/L 1.55 5.35 1.0 1664A

Analysis Batch: 500-172888 Analysis Date: 12/14/2012 0821

Prep Batch: 500-172887 Prep Date: 12/14/2012 0605

Chromium, hexavalent <0.0100 mg/L 0.00325 0.0100 1.0 7196A

Analysis Batch: 500-172291 Analysis Date (Start): 12/07/2012 1152 (End) 12/07/2012 1152

Cyanide, Total <0.0100 mg/L 0.00331 0.0100 1.0 9014

Analysis Batch: 500-172923 Analysis Date (Start): 12/13/2012 1326 (End) 12/13/2012 1327

Prep Batch: 500-172878 Prep Date: 12/13/2012 1030

Sulfide <1.00 mg/L 0.230 1.00 1.0 9034

Analysis Batch: 500-172533 Analysis Date (Start): 12/10/2012 2344 (End) 12/10/2012 2349

Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034

Analysis Batch: 500-172532 Analysis Date: 12/10/2012 2332

Prep Batch: 500-172531 Prep Date: 12/10/2012 2012

TestAmerica Chicago Page 23 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53034-2 FC Discrete 2 109 117 104 97

MB 500-172698/4 109 106 114 107

LCS 500-172698/5 106 108 117 108

500-53034-2 MS FC Discrete 2 MS 107 110 108 103

500-53034-2 MSD FC Discrete 2 MSD 109 114 107 98

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

TestAmerica Chicago

Page 24 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53034-2 DL FC Discrete 2 DL 97 97 98 92

MB 500-172879/6 90 88 93 88

LCS 500-172879/4 97 96 99 100

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 25 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Water

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53034-3 FC EB 2 95 95 98 95

500-53034-4 Trip Blank 94 91 100 93

MB 500-172880/6 90 88 93 88

LCS 500-172880/4 97 96 99 100

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 26 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172698

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 16M1212.D5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

MB 500-172698/4 CMS16

Analysis Date: 12/12/2012 0826

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-172698

Prep Date:

Leach Date:

12/12/2012 0826

N/A

Analyte Result Qual MDL RL

Acetone <5.00 2.16 5.00

2-Butanone (MEK) <5.00 1.81 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 106 70 - 134

Toluene-d8 (Surr) 114 75 - 122

4-Bromofluorobenzene (Surr) 107 70 - 122

Dibromofluoromethane 109 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-172698

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 16S1212.D5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-172698/5 CMS16

Analysis Date: 12/12/2012 0849

Analysis Batch:

Prep Batch:

Leach Batch:

500-172698

N/A

N/A

Prep Date:

Leach Date:

12/12/2012 0849

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 47.36 95 50 - 138

2-Butanone (MEK) 50.0 47.66 95 58 - 133

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 108 70 - 134

Toluene-d8 (Surr) 117 75 - 122

4-Bromofluorobenzene (Surr) 108 70 - 122

Dibromofluoromethane 106 75 - 120

TestAmerica Chicago Page 27 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Dilution:

Dilution:

Solid

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

53034-02s.D

5 g

5 mL

53034-02t.D

5 g

5 mL

Method: 8260B

Preparation: 5030B

CMS16

CMS16

500-53034-2

500-53034-2

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-172698

12/12/2012 0949

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-172698

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/12/2012 1012

12/12/2012 1012

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-172698

N/A

N/A

12/12/2012 0949

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Acetone -745 -140 50 - 138 10 30 E 4 E 4

2-Butanone (MEK) 60 70 58 - 133 10 30

Surrogate MS % Rec MSD % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 110 114 70 - 134

Toluene-d8 (Surr) 108 107 75 - 122

4-Bromofluorobenzene (Surr) 103 98 70 - 122

Dibromofluoromethane 107 109 75 - 120

Solid

12/12/2012 0949 12/12/2012 1012

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Solid

Method: 8260B

Preparation: 5030B

MS Lab Sample ID: 500-53034-2 Units: ug/Kg MSD Lab Sample ID: 500-53034-2

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-172698

Analysis Date:

Prep Date:

Leach Date:

12/12/2012 0949

N/A

Analysis Date:

Prep Date:

Leach Date:

12/12/2012 1012

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Acetone 10800 174 174 9517 E 4 10570 E 4

2-Butanone (MEK) 72.6 174 174 176.3 194.9

TestAmerica Chicago Page 28 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172879

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22M1213.D5 mL

Units: ug/Kg 5 mL

Method: 8260B

Preparation: N/A

MB 500-172879/6 CMS22

Analysis Date: 12/13/2012 1324

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-172879

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.30 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 88 75 - 125

Toluene-d8 (Surr) 93 75 - 120

4-Bromofluorobenzene (Surr) 88 75 - 120

Dibromofluoromethane 90 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-172879

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22S1213.D5 mL

Units: ug/Kg 5 mL

Method: 8260B

Preparation: N/A

LCS 500-172879/4 CMS22

Analysis Date: 12/13/2012 1232

Analysis Batch:

Prep Batch:

Leach Batch:

500-172879

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 46.30 93 46 - 153

2-Butanone (MEK) 50.0 46.82 94 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 96 75 - 125

Toluene-d8 (Surr) 99 75 - 120

4-Bromofluorobenzene (Surr) 100 75 - 120

Dibromofluoromethane 97 75 - 120

TestAmerica Chicago Page 29 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172880

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22M1213.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

MB 500-172880/6 CMS22

Analysis Date: 12/13/2012 1324

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-172880

Prep Date:

Leach Date:

12/13/2012 1324

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 88 75 - 125

Toluene-d8 (Surr) 93 75 - 120

4-Bromofluorobenzene (Surr) 88 75 - 120

Dibromofluoromethane 90 75 - 120

Water

1.0

Lab Control Sample - Batch: 500-172880

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 22S1213.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-172880/4 CMS22

Analysis Date: 12/13/2012 1232

Analysis Batch:

Prep Batch:

Leach Batch:

500-172880

N/A

N/A

Prep Date:

Leach Date:

12/13/2012 1232

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 46.30 93 46 - 153

2-Butanone (MEK) 50.0 46.82 94 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 96 75 - 125

Toluene-d8 (Surr) 99 75 - 120

4-Bromofluorobenzene (Surr) 100 75 - 120

Dibromofluoromethane 97 75 - 120

TestAmerica Chicago Page 30 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172306

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51210B1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

MB 500-172306/1-A ICP5

Analysis Date: 12/10/2012 1821

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172535

500-172306

Prep Date:

Leach Date:

12/07/2012 1600

N/A

Analyte Result Qual MDL RL

Barium 0.1210 J 0.119 1.00

Copper <1.00 0.271 1.00

Chromium <1.00 0.167 1.00

Nickel <1.00 0.219 1.00

Lead 0.2260 J 0.172 0.500

Vanadium <0.500 0.0759 0.500

Zinc <2.00 0.686 2.00

Solid

1.0

Lab Control Sample - Batch: 500-172306

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51210B1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

LCS 500-172306/2-A ICP5

Analysis Date: 12/10/2012 1827

Analysis Batch:

Prep Batch:

Leach Batch:

500-172535

500-172306

N/A

Prep Date:

Leach Date:

12/07/2012 1600

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 200 200.1 100 80 - 120

Copper 25.0 25.45 102 80 - 120

Chromium 20.0 20.13 101 80 - 120

Nickel 50.0 49.47 99 80 - 120

Lead 10.0 10.11 101 80 - 120

Vanadium 50.0 50.49 101 80 - 120

Zinc 50.0 48.59 97 80 - 120

TestAmerica Chicago Page 31 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172512

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P6121112B.asc50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

MB 500-172512/1-A ICP6

Analysis Date: 12/11/2012 1804

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172699

500-172512

Prep Date:

Leach Date:

12/10/2012 1430

N/A

Analyte Result Qual MDL RL

Barium <0.0100 0.000440 0.0100

Copper <0.0100 0.00106 0.0100

Chromium <0.0100 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead <0.00500 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc <0.0200 0.00472 0.0200

Water

1.0

Lab Control Sample - Batch: 500-172512

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P6121112B.asc50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-172512/2-A ICP6

Analysis Date: 12/11/2012 1808

Analysis Batch:

Prep Batch:

Leach Batch:

500-172699

500-172512

N/A

Prep Date:

Leach Date:

12/10/2012 1430

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.974 99 80 - 120

Copper 0.250 0.2472 99 80 - 120

Chromium 0.200 0.1892 95 80 - 120

Nickel 0.500 0.4817 96 80 - 120

Lead 0.100 0.09773 98 80 - 120

Vanadium 0.500 0.4890 98 80 - 120

Zinc 0.500 0.4699 94 80 - 120

TestAmerica Chicago Page 32 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPW Leachate Blank - Batch: 500-172581

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51211B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

TCLP

LB2 500-172501/1-C ICP5

Analysis Date: 12/11/2012 1833

Analysis Batch:

Prep Batch:

Leach Batch: 500-172501

500-172697

500-172581

Prep Date:

Leach Date:

12/11/2012 0913

12/10/2012 1448

Analyte Result Qual MDL RL

Barium <0.500 0.0100 0.500

Copper <0.0250 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel <0.0250 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

Water

1.0

Lab Control Sample - Batch: 500-172581

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51211B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-172581/4-A ICP5

Analysis Date: 12/11/2012 1846

Analysis Batch:

Prep Batch:

Leach Batch:

500-172697

500-172581

N/A

Prep Date:

Leach Date:

12/11/2012 0913

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.936 97 80 - 120

Copper 0.250 0.2419 97 80 - 120

Chromium 0.200 0.1920 96 80 - 120

Nickel 0.500 0.4764 95 80 - 120

Lead 0.100 0.09745 97 80 - 120

Vanadium 0.500 0.4821 96 80 - 120

Zinc 0.500 0.4708 94 80 - 120

TestAmerica Chicago Page 33 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172640

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121212RA.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-172640/7-A HG6

Analysis Date: 12/12/2012 0857

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172764

500-172640

Prep Date:

Leach Date:

12/11/2012 1500

N/A

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000200 0.000200

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPW Leachate Blank - Batch: 500-172640

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121212RA.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

TCLP

LB2 500-172501/1-D HG6

Analysis Date: 12/12/2012 0912

Analysis Batch:

Prep Batch:

Leach Batch: 500-172501

500-172764

500-172640

Prep Date:

Leach Date:

12/11/2012 1500

12/10/2012 1448

Analyte Result Qual MDL RL

Mercury 0.00003710 J 0.0000200 0.000200

Water

1.0

Lab Control Sample - Batch: 500-172640

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121212RA.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-172640/8-A HG6

Analysis Date: 12/12/2012 0858

Analysis Batch:

Prep Batch:

Leach Batch:

500-172764

500-172640

N/A

Prep Date:

Leach Date:

12/11/2012 1500

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002027 101 80 - 120

TestAmerica Chicago Page 34 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172642

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121212RA.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-172642/7-A HG6

Analysis Date: 12/12/2012 1053

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172764

500-172642

Prep Date:

Leach Date:

12/11/2012 1500

N/A

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000710 0.000200

Water

1.0

Lab Control Sample - Batch: 500-172642

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121212RA.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-172642/8-A HG6

Analysis Date: 12/12/2012 1054

Analysis Batch:

Prep Batch:

Leach Batch:

500-172764

500-172642

N/A

Prep Date:

Leach Date:

12/11/2012 1500

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002054 103 80 - 120

TestAmerica Chicago Page 35 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172460

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1211112B.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

MB 500-172460/7-A HG5

Analysis Date: 12/11/2012 1107

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172626

500-172460

Prep Date:

Leach Date:

12/10/2012 1500

N/A

Analyte Result Qual MDL RL

Mercury <0.0167 0.00637 0.0167

Solid

1.0

Lab Control Sample - Batch: 500-172460

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1211112B.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

LCS 500-172460/8-A HG5

Analysis Date: 12/11/2012 1109

Analysis Batch:

Prep Batch:

Leach Batch:

500-172626

500-172460

N/A

Prep Date:

Leach Date:

12/10/2012 1500

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.167 0.1975 118 80 - 120

TestAmerica Chicago Page 36 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172887

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

MB 500-172887/1-A No Equipment 

Analysis Date: 12/14/2012 0800

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172888

500-172887

Prep Date:

Leach Date:

12/14/2012 0535

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <5.00 1.45 5.00

Dilution:

Dilution:

Lab Control Sample/

Lab Control Sample Duplicate Recovery Report - Batch: 500-172887

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

mg/L

1000 mL

1000 mL

1000 mL

mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

N/A

No Equipment 

No Equipment 

LCS 500-172887/2-A

LCSD 500-172887/3-A

Analysis Date:

Prep Date:

Leach Date:

12/14/2012 0803

12/14/2012 0540

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-172888

500-172887

N/A

Analysis Date:

Prep Date:

Leach Date:

12/14/2012 0807

12/14/2012 0545

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-172888

500-172887

N/A

Analyte LCS LCSD Limit RPD RPD Limit LCS Qual LCSD Qual

% Rec.

HEM (Oil & Grease) 102 96 78 - 114 7 18

Water

12/14/2012 0803

Dilution: 1.0 Dilution: 1.0

Client Matrix:

LCSD Lab Sample ID:

Client Matrix: Water

Laboratory Control/

Laboratory Duplicate Data Report - Batch: 500-172887

Method: 1664A

Preparation: 1664A

LCS Lab Sample ID: LCS 500-172887/2-A Units: mg/L LCSD 500-172887/3-A

Analysis Date:

Prep Date:

Leach Date:

12/14/2012 0540

Analysis Date:

Prep Date:

Leach Date:

12/14/2012 0807

12/14/2012 0545

N/A N/A

LCSD 

Result/Qual

LCS 

Result/Qual

LCSD Spike 

Amount

LCS Spike 

Amount Analyte

HEM (Oil & Grease) 40.0 40.0 40.90 38.30

TestAmerica Chicago Page 37 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172291

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 100 mL

Units: mg/L 100 mL

Method: 7196A

Preparation: N/A

N/A

MB 500-172291/3 SPEC5

Analysis Date: 12/07/2012 1151

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-172291

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <0.0100 0.00325 0.0100

Water

1.0

Lab Control Sample - Batch: 500-172291

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 100 mL

Units: mg/L 100 mL

Method: 7196A

Preparation: N/A

N/A

LCS 500-172291/4 SPEC5

Analysis Date: 12/07/2012 1151

Analysis Batch:

Prep Batch:

Leach Batch:

500-172291

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 0.250 0.2487 99 85 - 115

TestAmerica Chicago Page 38 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173258

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

MB 500-173258/1-A SPEC5

Analysis Date: 12/18/2012 1546

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173341

500-173258

Prep Date:

Leach Date:

12/18/2012 1000

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <1.00 0.389 1.00

Solid

1.0

Lab Control Sample - Batch: 500-173258

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173258/2-A SPEC5

Analysis Date: 12/18/2012 1546

Analysis Batch:

Prep Batch:

Leach Batch:

500-173341

500-173258

N/A

Prep Date:

Leach Date:

12/18/2012 1000

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 10.0 8.252 83 80 - 120

Solid

50

Lab Control Sample - Batch: 500-173258

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173258/3-A SPEC5

Analysis Date: 12/18/2012 1547

Analysis Batch:

Prep Batch:

Leach Batch:

500-173341

500-173258

N/A

Prep Date:

Leach Date:

12/18/2012 1000

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 1550 1601 104 80 - 120

TestAmerica Chicago Page 39 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172878

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-172878/1-A SPEC5

Analysis Date: 12/13/2012 1320

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172923

500-172878

Prep Date:

Leach Date:

12/13/2012 1030

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.0100 0.00331 0.0100

Water

1.0

Lab Control Sample - Batch: 500-172878

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-172878/2-A SPEC5

Analysis Date: 12/13/2012 1320

Analysis Batch:

Prep Batch:

Leach Batch:

500-172923

500-172878

N/A

Prep Date:

Leach Date:

12/13/2012 1030

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 0.100 0.1026 103 80 - 120

TestAmerica Chicago Page 40 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173012

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-173012/1-A SPEC5

Analysis Date: 12/14/2012 1558

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173074

500-173012

Prep Date:

Leach Date:

12/14/2012 1325

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.500 0.165 0.500

Solid

1.0

Lab Control Sample - Batch: 500-173012

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-173012/2-A SPEC5

Analysis Date: 12/14/2012 1558

Analysis Batch:

Prep Batch:

Leach Batch:

500-173074

500-173012

N/A

Prep Date:

Leach Date:

12/14/2012 1325

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 5.00 5.620 112 80 - 120

TestAmerica Chicago Page 41 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172531

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-172531/1-A No Equipment 

Analysis Date: 12/10/2012 2315

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172532

500-172531

Prep Date:

Leach Date:

12/10/2012 2000

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <1.00 1.00 1.00

Water

1.0

Lab Control Sample - Batch: 500-172531

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-172531/2-A No Equipment 

Analysis Date: 12/10/2012 2323

Analysis Batch:

Prep Batch:

Leach Batch:

500-172532

500-172531

N/A

Prep Date:

Leach Date:

12/10/2012 2006

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 3.60 3.907 109 80 - 120

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

250 mL

250 mL

250 mL

250 mL

Method: 9034

Preparation: 7.3.4

N/A

N/A

No Equipment 

No Equipment 

500-53034-3

500-53034-3

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-172531

12/10/2012 2341

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-172532

500-172531

N/A

Analysis Date:

Prep Date:

Leach Date:

12/10/2012 2350

12/10/2012 2024

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-172532

500-172531

N/A

12/10/2012 2018

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Sulfide, Reactive 95 101 75 - 125 5 20

TestAmerica Chicago Page 42 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Water

12/10/2012 2341 12/10/2012 2350

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Water

Method: 9034

Preparation: 7.3.4

MS Lab Sample ID: 500-53034-3 Units: mg/L MSD Lab Sample ID: 500-53034-3

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-172531

Analysis Date:

Prep Date:

Leach Date:

12/10/2012 2018

N/A

Analysis Date:

Prep Date:

Leach Date:

12/10/2012 2024

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Sulfide, Reactive <1.00 3.60 3.60 3.434 3.623

TestAmerica Chicago Page 43 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172533

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: N/A

N/A

MB 500-172533/1 No Equipment 

Analysis Date: 12/10/2012 2315

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-172533

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Sulfide <1.00 0.230 1.00

Water

1.0

Lab Control Sample - Batch: 500-172533

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: N/A

N/A

LCS 500-172533/2 No Equipment 

Analysis Date: 12/10/2012 2319

Analysis Batch:

Prep Batch:

Leach Batch:

500-172533

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 3.60 3.900 108 80 - 120

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

250 mL

250 mL

250 mL

250 mL

Method: 9034

Preparation: N/A

N/A

N/A

No Equipment 

No Equipment 

500-53034-3

500-53034-3

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-172533

12/10/2012 2349

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-172533

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/10/2012 2354

N/A

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-172533

N/A

N/A

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Sulfide 95 100 75 - 125 5 20

TestAmerica Chicago Page 44 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Water

12/10/2012 2349 12/10/2012 2354

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Water

Method: 9034

Preparation: N/A

MS Lab Sample ID: 500-53034-3 Units: mg/L MSD Lab Sample ID: 500-53034-3

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-172533

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Sulfide <1.00 3.60 3.60 3.428 3.617

TestAmerica Chicago Page 45 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172578

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-172578/1-A No Equipment 

Analysis Date: 12/11/2012 1230

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-172643

500-172578

Prep Date:

Leach Date:

12/11/2012 1015

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <50.0 3.90 50.0

Solid

1.0

Lab Control Sample - Batch: 500-172578

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-172578/2-A No Equipment 

Analysis Date: 12/11/2012 1230

Analysis Batch:

Prep Batch:

Leach Batch:

500-172643

500-172578

N/A

Prep Date:

Leach Date:

12/11/2012 1019

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 180 172.9 96 80 - 120

TestAmerica Chicago Page 46 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-172997

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.00000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

MB 500-172997/1-A No Equipment 

Analysis Date: 12/14/2012 1540

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173039

500-172997

Prep Date:

Leach Date:

12/14/2012 1135

N/A

Analyte Result Qual MDL RL

Sulfide <25.0 4.00 25.0

Solid

1.0

Lab Control Sample - Batch: 500-172997

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.00000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

LCS 500-172997/2-A No Equipment 

Analysis Date: 12/14/2012 1540

Analysis Batch:

Prep Batch:

Leach Batch:

500-173039

500-172997

N/A

Prep Date:

Leach Date:

12/14/2012 1135

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 180 179.7 100 80 - 120

TestAmerica Chicago Page 47 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173324

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

MB 500-173324/1-A No Equipment 

Analysis Date: 12/19/2012 0920

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173330

500-173324

Prep Date:

Leach Date:

12/19/2012 0510

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <500 222 500

Solid

1.0

Lab Control Sample - Batch: 500-173324

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

LCS 500-173324/2-A No Equipment 

Analysis Date: 12/19/2012 0931

Analysis Batch:

Prep Batch:

Leach Batch:

500-173330

500-173324

N/A

Prep Date:

Leach Date:

12/19/2012 0510

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 4000 4090 102 80 - 120

TestAmerica Chicago Page 48 of 360 12/26/2012
DATA REPORTING QUALIFIERS

Client: Project Integration, Inc Job Number: 500-53034-1

Lab Section Qualifier Description

GC/MS VOA

MS, MSD: The analyte present in the original sample is 4 times greater 

than the matrix spike concentration; therefore, control limits are not 

applicable.

4

E Result exceeded calibration range.

Metals

B Compound was found in the blank and sample.

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

TestAmerica Chicago Page 49 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS VOA

Prep Batch: 500-172604

500-53034-2DL FC Discrete 2 T Solid 5030B

Analysis Batch:500-172698

LCS 500-172698/5 Lab Control Sample T Solid 8260B

MB 500-172698/4 Method Blank T Solid 8260B

500-53034-2 FC Discrete 2 T Solid 8260B

500-53034-2MS Matrix Spike T Solid 8260B

500-53034-2MSD Matrix Spike Duplicate T Solid 8260B

Analysis Batch:500-172879

LCS 500-172879/4 Lab Control Sample T Solid 8260B

MB 500-172879/6 Method Blank T Solid 8260B

500-53034-2DL FC Discrete 2 T Solid 8260B 500-172604

Analysis Batch:500-172880

LCS 500-172880/4 Lab Control Sample T Water 8260B

MB 500-172880/6 Method Blank T Water 8260B

500-53034-3 FC EB 2 T Water 8260B

500-53034-4 Trip Blank T Water 8260B

Report Basis

T = Total

TestAmerica Chicago

Page 50 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Prep Batch: 500-172306

LCS 500-172306/2-A Lab Control Sample T Solid 3050B

MB 500-172306/1-A Method Blank T Solid 3050B

500-53034-1 FC Composite 2 T Solid 3050B

Prep Batch: 500-172460

LCS 500-172460/8-A Lab Control Sample T Solid 7471A

MB 500-172460/7-A Method Blank T Solid 7471A

500-53034-1 FC Composite 2 T Solid 7471A

Prep Batch: 500-172501

LB2 500-172501/1-C TCLP SPLPW Leachate Blank P Solid 1311

LB2 500-172501/1-D TCLP SPLPW Leachate Blank P Solid 1311

500-53034-1 FC Composite 2 P Solid 1311

Prep Batch: 500-172512

LCS 500-172512/2-A Lab Control Sample T Water 3010A

MB 500-172512/1-A Method Blank T Water 3010A

500-53034-3 FC EB 2 T Water 3010A

Analysis Batch:500-172535

LCS 500-172306/2-A Lab Control Sample T Solid 6010B 500-172306

MB 500-172306/1-A Method Blank T Solid 6010B 500-172306

500-53034-1 FC Composite 2 T Solid 6010B 500-172306

Prep Batch: 500-172581

LCS 500-172581/4-A Lab Control Sample T Water 3010A

LB2 500-172501/1-C TCLP SPLPW Leachate Blank P Solid 3010A 500-172501

500-53034-1 FC Composite 2 P Solid 3010A 500-172501

Analysis Batch:500-172626

LCS 500-172460/8-A Lab Control Sample T Solid 7471A 500-172460

MB 500-172460/7-A Method Blank T Solid 7471A 500-172460

500-53034-1 FC Composite 2 T Solid 7471A 500-172460

Prep Batch: 500-172640

LCS 500-172640/8-A Lab Control Sample T Water 7470A

MB 500-172640/7-A Method Blank T Water 7470A

LB2 500-172501/1-D TCLP SPLPW Leachate Blank P Solid 7470A 500-172501

500-53034-1 FC Composite 2 P Solid 7470A 500-172501

Prep Batch: 500-172642

LCS 500-172642/8-A Lab Control Sample T Water 7470A

MB 500-172642/7-A Method Blank T Water 7470A

500-53034-3 FC EB 2 T Water 7470A

TestAmerica Chicago

Page 51 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Analysis Batch:500-172697

LB2 500-172501/1-C TCLP SPLPW Leachate Blank P Solid 6010B 500-172581

LCS 500-172581/4-A Lab Control Sample T Water 6010B 500-172581

500-53034-1 FC Composite 2 P Solid 6010B 500-172581

Analysis Batch:500-172699

LCS 500-172512/2-A Lab Control Sample T Water 6010B 500-172512

MB 500-172512/1-A Method Blank T Water 6010B 500-172512

500-53034-3 FC EB 2 T Water 6010B 500-172512

Analysis Batch:500-172764

LB2 500-172501/1-D TCLP SPLPW Leachate Blank P Solid 7470A 500-172640

LCS 500-172640/8-A Lab Control Sample T Water 7470A 500-172640

MB 500-172640/7-A Method Blank T Water 7470A 500-172640

LCS 500-172642/8-A Lab Control Sample T Water 7470A 500-172642

MB 500-172642/7-A Method Blank T Water 7470A 500-172642

500-53034-1 FC Composite 2 P Solid 7470A 500-172640

500-53034-3 FC EB 2 T Water 7470A 500-172642

Report Basis

P = TCLP

T = Total

TestAmerica Chicago

Page 52 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-172275

500-53034-1 FC Composite 2 T Solid Moisture

Analysis Batch:500-172291

LCS 500-172291/4 Lab Control Sample T Water 7196A

MB 500-172291/3 Method Blank T Water 7196A

500-53034-3 FC EB 2 T Water 7196A

Analysis Batch:500-172359

500-53034-1 FC Composite 2 T Solid SM 2540G

Prep Batch: 500-172531

LCS 500-172531/2-A Lab Control Sample T Water 7.3.4

MB 500-172531/1-A Method Blank T Water 7.3.4

500-53034-3 FC EB 2 T Water 7.3.4

500-53034-3MS Matrix Spike T Water 7.3.4

500-53034-3MSD Matrix Spike Duplicate T Water 7.3.4

Analysis Batch:500-172532

LCS 500-172531/2-A Lab Control Sample T Water 9034 500-172531

MB 500-172531/1-A Method Blank T Water 9034 500-172531

500-53034-3 FC EB 2 T Water 9034 500-172531

500-53034-3MS Matrix Spike T Water 9034 500-172531

500-53034-3MSD Matrix Spike Duplicate T Water 9034 500-172531

Analysis Batch:500-172533

LCS 500-172533/2 Lab Control Sample T Water 9034

MB 500-172533/1 Method Blank T Water 9034

500-53034-3 FC EB 2 T Water 9034

500-53034-3MS Matrix Spike T Water 9034

500-53034-3MSD Matrix Spike Duplicate T Water 9034

Prep Batch: 500-172578

LCS 500-172578/2-A Lab Control Sample T Solid 7.3.4

MB 500-172578/1-A Method Blank T Solid 7.3.4

500-53034-1 FC Composite 2 T Solid 7.3.4

Analysis Batch:500-172643

LCS 500-172578/2-A Lab Control Sample T Solid 9034 500-172578

MB 500-172578/1-A Method Blank T Solid 9034 500-172578

500-53034-1 FC Composite 2 T Solid 9034 500-172578

Analysis Batch:500-172720

500-53034-2 FC Discrete 2 T Solid Moisture

TestAmerica Chicago

Page 53 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Prep Batch: 500-172878

LCS 500-172878/2-A Lab Control Sample T Water 9010B

MB 500-172878/1-A Method Blank T Water 9010B

500-53034-3 FC EB 2 T Water 9010B

Prep Batch: 500-172887

LCS 500-172887/2-A Lab Control Sample T Water 1664A

LCSD 500-172887/3-A Lab Control Sample Duplicate T Water 1664A

MB 500-172887/1-A Method Blank T Water 1664A

500-53034-3 FC EB 2 T Water 1664A

Analysis Batch:500-172888

LCS 500-172887/2-A Lab Control Sample T Water 1664A 500-172887

LCSD 500-172887/3-A Lab Control Sample Duplicate T Water 1664A 500-172887

MB 500-172887/1-A Method Blank T Water 1664A 500-172887

500-53034-3 FC EB 2 T Water 1664A 500-172887

Analysis Batch:500-172923

LCS 500-172878/2-A Lab Control Sample T Water 9014 500-172878

MB 500-172878/1-A Method Blank T Water 9014 500-172878

500-53034-3 FC EB 2 T Water 9014 500-172878

Prep Batch: 500-172997

LCS 500-172997/2-A Lab Control Sample T Solid 9030B

MB 500-172997/1-A Method Blank T Solid 9030B

500-53034-1 FC Composite 2 T Solid 9030B

Prep Batch: 500-173012

LCS 500-173012/2-A Lab Control Sample T Solid 9010B

MB 500-173012/1-A Method Blank T Solid 9010B

500-53034-1 FC Composite 2 T Solid 9010B

Analysis Batch:500-173039

LCS 500-172997/2-A Lab Control Sample T Solid 9034 500-172997

MB 500-172997/1-A Method Blank T Solid 9034 500-172997

500-53034-1 FC Composite 2 T Solid 9034 500-172997

Analysis Batch:500-173074

LCS 500-173012/2-A Lab Control Sample T Solid 9014 500-173012

MB 500-173012/1-A Method Blank T Solid 9014 500-173012

500-53034-1 FC Composite 2 T Solid 9014 500-173012

TestAmerica Chicago

Page 54 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Prep Batch: 500-173258

LCS 500-173258/2-A Lab Control Sample T Solid 3060A

LCS 500-173258/3-A Lab Control Sample T Solid 3060A

MB 500-173258/1-A Method Blank T Solid 3060A

500-53034-1 FC Composite 2 T Solid 3060A

Prep Batch: 500-173324

LCS 500-173324/2-A Lab Control Sample T Solid 9071B

MB 500-173324/1-A Method Blank T Solid 9071B

500-53034-1 FC Composite 2 T Solid 9071B

Analysis Batch:500-173330

LCS 500-173324/2-A Lab Control Sample T Solid 9071B 500-173324

MB 500-173324/1-A Method Blank T Solid 9071B 500-173324

500-53034-1 FC Composite 2 T Solid 9071B 500-173324

Analysis Batch:500-173341

LCS 500-173258/2-A Lab Control Sample T Solid 7196A 500-173258

LCS 500-173258/3-A Lab Control Sample T Solid 7196A 500-173258

MB 500-173258/1-A Method Blank T Solid 7196A 500-173258

500-53034-1 FC Composite 2 T Solid 7196A 500-173258

Analysis Batch:500-173479

500-53034-1 FC Composite 2 T Solid 9045C

Analysis Batch:500-173558

500-53034-1 FC Composite 2 T Solid 1010

Report Basis

T = Total

TestAmerica Chicago

Page 55 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Laboratory Chronicle

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:30 Received Date/Time: 500-53034-1 FC Composite 2

P:3050B 500-53034-A-1-A 500-172535 500-172306 12/07/2012 16:00 1 TAL CHI RL

A:6010B 500-53034-A-1-A 500-172535 500-172306 12/10/2012 20:54 1 TAL CHI TDS

P:3010A 500-53034-A-1-E 500-172697 500-172581 12/11/2012 09:13 1 TAL CHI LAH

A:6010B 500-53034-A-1-E 500-172697 500-172581 12/11/2012 20:21 1 TAL CHI TDS

P:7470A 500-53034-A-1-G 500-172764 500-172640 12/11/2012 15:00 1 TAL CHI BJB

A:7470A 500-53034-A-1-G 500-172764 500-172640 12/12/2012 09:41 1 TAL CHI BJB

P:7471A 500-53034-A-1-B 500-172626 500-172460 12/10/2012 15:00 1 TAL CHI BJB

A:7471A 500-53034-A-1-B 500-172626 500-172460 12/11/2012 12:59 1 TAL CHI BJB

A:1010 500-53034-A-1 500-173558 12/19/2012 15:24 1 TAL CHI APW

P:3060A 500-53034-A-1-J 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A 500-53034-A-1-J 500-173341 500-173258 12/18/2012 15:48 1 TAL CHI APW

P:9010B 500-53034-A-1-I 500-173074 500-173012 12/14/2012 13:25 1 TAL CHI EAT

A:9014 500-53034-A-1-I 500-173074 500-173012 12/14/2012 16:02 1 TAL CHI EAT

P:7.3.4 500-53034-A-1-F 500-172643 500-172578 12/11/2012 11:25 1 TAL CHI CLM

A:9034 500-53034-A-1-F 500-172643 500-172578 12/11/2012 12:39 1 TAL CHI CLM

P:9030B 500-53034-A-1-H 500-173039 500-172997 12/14/2012 11:35 1 TAL CHI CLM

A:9034 500-53034-A-1-H 500-173039 500-172997 12/14/2012 15:46 1 TAL CHI CLM

A:9045C 500-53034-A-1 500-173479 12/20/2012 06:20 1 TAL CHI CLM

P:9071B 500-53034-A-1-K 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B 500-53034-A-1-K 500-173330 500-173324 12/19/2012 10:27 1 TAL CHI MTB

A:Moisture 500-53034-A-1 500-172275 12/07/2012 12:59 1 TAL CHI CMV

A:SM 2540G 500-53034-A-1 500-172359 12/08/2012 15:37 1 TAL CHI CMV

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:25 Received Date/Time: 500-53034-2 FC Discrete 2

P:5030B 500-53034-A-2 500-172698 12/12/2012 09:25 1 TAL CHI BDW

A:8260B 500-53034-A-2 500-172698 12/12/2012 09:25 1 TAL CHI BDW

P:5030B 500-53034-A-2-A DL 500-172879 500-172604 12/11/2012 11:27 50 TAL CHI BDW

A:8260B 500-53034-A-2-A DL 500-172879 500-172604 12/13/2012 22:04 50 TAL CHI EA

A:Moisture 500-53034-A-2 500-172720 12/12/2012 11:11 1 TAL CHI CMV

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:25 Received Date/Time: 500-53034-2 MS FC Discrete 2

P:5030B 500-53034-A-2 MS 500-172698 12/12/2012 09:49 1 TAL CHI BDW

A:8260B 500-53034-A-2 MS 500-172698 12/12/2012 09:49 1 TAL CHI BDW

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 56 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Laboratory Chronicle

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:25 Received Date/Time: 500-53034-2 MSD FC Discrete 2

P:5030B 500-53034-A-2 MSD 500-172698 12/12/2012 10:12 1 TAL CHI BDW

A:8260B 500-53034-A-2 MSD 500-172698 12/12/2012 10:12 1 TAL CHI BDW

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:15 Received Date/Time: 500-53034-3 FC EB 2

P:5030B 500-53034-A-3 500-172880 12/13/2012 15:33 1 TAL CHI EA

A:8260B 500-53034-A-3 500-172880 12/13/2012 15:33 1 TAL CHI EA

P:3010A 500-53034-E-3-A 500-172699 500-172512 12/10/2012 14:30 1 TAL CHI RL

A:6010B 500-53034-E-3-A 500-172699 500-172512 12/11/2012 20:14 1 TAL CHI PJ

P:7470A 500-53034-E-3-B 500-172764 500-172642 12/11/2012 15:00 1 TAL CHI BJB

A:7470A 500-53034-E-3-B 500-172764 500-172642 12/12/2012 11:15 1 TAL CHI BJB

P:1664A 500-53034-H-3-A 500-172888 500-172887 12/14/2012 06:05 1 TAL CHI MTB

A:1664A 500-53034-H-3-A 500-172888 500-172887 12/14/2012 08:21 1 TAL CHI MTB

A:7196A 500-53034-G-3 500-172291 12/07/2012 11:52 1 TAL CHI KD

P:9010B 500-53034-D-3-A 500-172923 500-172878 12/13/2012 10:30 1 TAL CHI EAT

A:9014 500-53034-D-3-A 500-172923 500-172878 12/13/2012 13:26 1 TAL CHI EAT

P:7.3.4 500-53034-F-3-A 500-172532 500-172531 12/10/2012 20:12 1 TAL CHI CLB

A:9034 500-53034-F-3-A 500-172532 500-172531 12/10/2012 23:32 1 TAL CHI CLB

A:9034 500-53034-F-3 500-172533 12/10/2012 23:44 1 TAL CHI CLB

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:15 Received Date/Time: 500-53034-3 MS FC EB 2

P:7.3.4 500-53034-F-3-B MS 500-172532 500-172531 12/10/2012 20:18 1 TAL CHI CLB

A:9034 500-53034-F-3-B MS 500-172532 500-172531 12/10/2012 23:41 1 TAL CHI CLB

A:9034 500-53034-F-3 MS 500-172533 12/10/2012 23:49 1 TAL CHI CLB

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 14:15 Received Date/Time: 500-53034-3 MSD FC EB 2

P:7.3.4 500-53034-F-3-C 

MSD

500-172532 500-172531 12/10/2012 20:24 1 TAL CHI CLB

A:9034 500-53034-F-3-C 

MSD

500-172532 500-172531 12/10/2012 23:50 1 TAL CHI CLB

A:9034 500-53034-F-3 MSD 500-172533 12/10/2012 23:54 1 TAL CHI CLB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 57 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Laboratory Chronicle

12/07/2012 09:50

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/06/2012 00:00 Received Date/Time: 500-53034-4 Trip Blank

P:5030B 500-53034-A-4 500-172880 12/13/2012 14:15 1 TAL CHI EA

A:8260B 500-53034-A-4 500-172880 12/13/2012 14:15 1 TAL CHI EA

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

MB N/A

P:5030B MB 500-172698/4 500-172698 12/12/2012 08:26 1 TAL CHI BDW

A:8260B MB 500-172698/4 500-172698 12/12/2012 08:26 1 TAL CHI BDW

P:5030B MB 500-172880/6 500-172880 12/13/2012 13:24 1 TAL CHI EA

A:8260B MB 500-172879/6 500-172879 12/13/2012 13:24 1 TAL CHI EA

A:8260B MB 500-172880/6 500-172880 12/13/2012 13:24 1 TAL CHI EA

P:3050B MB 500-172306/1-A 500-172535 500-172306 12/07/2012 16:00 1 TAL CHI RL

A:6010B MB 500-172306/1-A 500-172535 500-172306 12/10/2012 18:21 1 TAL CHI TDS

P:3010A MB 500-172512/1-A 500-172699 500-172512 12/10/2012 14:30 1 TAL CHI RL

A:6010B MB 500-172512/1-A 500-172699 500-172512 12/11/2012 18:04 1 TAL CHI PJ

P:7470A MB 500-172640/7-A 500-172764 500-172640 12/11/2012 15:00 1 TAL CHI BJB

A:7470A MB 500-172640/7-A 500-172764 500-172640 12/12/2012 08:57 1 TAL CHI BJB

P:7470A MB 500-172642/7-A 500-172764 500-172642 12/11/2012 15:00 1 TAL CHI BJB

A:7470A MB 500-172642/7-A 500-172764 500-172642 12/12/2012 10:53 1 TAL CHI BJB

P:7471A MB 500-172460/7-A 500-172626 500-172460 12/10/2012 15:00 1 TAL CHI BJB

A:7471A MB 500-172460/7-A 500-172626 500-172460 12/11/2012 11:07 1 TAL CHI BJB

P:1664A MB 500-172887/1-A 500-172888 500-172887 12/14/2012 05:35 1 TAL CHI MTB

A:1664A MB 500-172887/1-A 500-172888 500-172887 12/14/2012 08:00 1 TAL CHI MTB

A:7196A MB 500-172291/3 500-172291 12/07/2012 11:51 1 TAL CHI KD

P:3060A MB 500-173258/1-A 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A MB 500-173258/1-A 500-173341 500-173258 12/18/2012 15:46 1 TAL CHI APW

P:9010B MB 500-172878/1-A 500-172923 500-172878 12/13/2012 10:30 1 TAL CHI EAT

A:9014 MB 500-172878/1-A 500-172923 500-172878 12/13/2012 13:20 1 TAL CHI EAT

P:9010B MB 500-173012/1-A 500-173074 500-173012 12/14/2012 13:25 1 TAL CHI EAT

A:9014 MB 500-173012/1-A 500-173074 500-173012 12/14/2012 15:58 1 TAL CHI EAT

P:7.3.4 MB 500-172531/1-A 500-172532 500-172531 12/10/2012 20:00 1 TAL CHI CLB

A:9034 MB 500-172531/1-A 500-172532 500-172531 12/10/2012 23:15 1 TAL CHI CLB

A:9034 MB 500-172533/1 500-172533 12/10/2012 23:15 1 TAL CHI CLB

P:7.3.4 MB 500-172578/1-A 500-172643 500-172578 12/11/2012 10:15 1 TAL CHI CLM

A:9034 MB 500-172578/1-A 500-172643 500-172578 12/11/2012 12:30 1 TAL CHI CLM

P:9030B MB 500-172997/1-A 500-173039 500-172997 12/14/2012 11:35 1 TAL CHI CLM

A:9034 MB 500-172997/1-A 500-173039 500-172997 12/14/2012 15:40 1 TAL CHI CLM

P:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 09:20 1 TAL CHI MTB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 58 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LB2 N/A

P:3010A LB2 500-172501/1-C 500-172697 500-172581 12/11/2012 09:13 1 TAL CHI LAH

A:6010B LB2 500-172501/1-C 500-172697 500-172581 12/11/2012 18:33 1 TAL CHI TDS

P:7470A LB2 500-172501/1-D 500-172764 500-172640 12/11/2012 15:00 1 TAL CHI BJB

A:7470A LB2 500-172501/1-D 500-172764 500-172640 12/12/2012 09:12 1 TAL CHI BJB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 59 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LCS N/A

P:5030B LCS 500-172698/5 500-172698 12/12/2012 08:49 1 TAL CHI BDW

A:8260B LCS 500-172698/5 500-172698 12/12/2012 08:49 1 TAL CHI BDW

P:5030B LCS 500-172880/4 500-172880 12/13/2012 12:32 1 TAL CHI EA

A:8260B LCS 500-172879/4 500-172879 12/13/2012 12:32 1 TAL CHI EA

A:8260B LCS 500-172880/4 500-172880 12/13/2012 12:32 1 TAL CHI EA

P:3050B LCS 500-172306/2-A 500-172535 500-172306 12/07/2012 16:00 1 TAL CHI RL

A:6010B LCS 500-172306/2-A 500-172535 500-172306 12/10/2012 18:27 1 TAL CHI TDS

P:3010A LCS 500-172512/2-A 500-172699 500-172512 12/10/2012 14:30 1 TAL CHI RL

A:6010B LCS 500-172512/2-A 500-172699 500-172512 12/11/2012 18:08 1 TAL CHI PJ

P:3010A LCS 500-172581/4-A 500-172697 500-172581 12/11/2012 09:13 1 TAL CHI LAH

A:6010B LCS 500-172581/4-A 500-172697 500-172581 12/11/2012 18:46 1 TAL CHI TDS

P:7470A LCS 500-172640/8-A 500-172764 500-172640 12/11/2012 15:00 1 TAL CHI BJB

A:7470A LCS 500-172640/8-A 500-172764 500-172640 12/12/2012 08:58 1 TAL CHI BJB

P:7470A LCS 500-172642/8-A 500-172764 500-172642 12/11/2012 15:00 1 TAL CHI BJB

A:7470A LCS 500-172642/8-A 500-172764 500-172642 12/12/2012 10:54 1 TAL CHI BJB

P:7471A LCS 500-172460/8-A 500-172626 500-172460 12/10/2012 15:00 1 TAL CHI BJB

A:7471A LCS 500-172460/8-A 500-172626 500-172460 12/11/2012 11:09 1 TAL CHI BJB

P:1664A LCS 500-172887/2-A 500-172888 500-172887 12/14/2012 05:40 1 TAL CHI MTB

A:1664A LCS 500-172887/2-A 500-172888 500-172887 12/14/2012 08:03 1 TAL CHI MTB

A:7196A LCS 500-172291/4 500-172291 12/07/2012 11:51 1 TAL CHI KD

P:3060A LCS 500-173258/2-A 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A LCS 500-173258/2-A 500-173341 500-173258 12/18/2012 15:46 1 TAL CHI APW

P:3060A LCS 500-173258/3-A 500-173341 500-173258 12/18/2012 10:00 50 TAL CHI APW

A:7196A LCS 500-173258/3-A 500-173341 500-173258 12/18/2012 15:47 50 TAL CHI APW

P:9010B LCS 500-172878/2-A 500-172923 500-172878 12/13/2012 10:30 1 TAL CHI EAT

A:9014 LCS 500-172878/2-A 500-172923 500-172878 12/13/2012 13:20 1 TAL CHI EAT

P:9010B LCS 500-173012/2-A 500-173074 500-173012 12/14/2012 13:25 1 TAL CHI EAT

A:9014 LCS 500-173012/2-A 500-173074 500-173012 12/14/2012 15:58 1 TAL CHI EAT

A:9034 LCS 500-172533/2 500-172533 12/10/2012 23:19 1 TAL CHI CLB

P:7.3.4 LCS 500-172531/2-A 500-172532 500-172531 12/10/2012 20:06 1 TAL CHI CLB

A:9034 LCS 500-172531/2-A 500-172532 500-172531 12/10/2012 23:23 1 TAL CHI CLB

P:7.3.4 LCS 500-172578/2-A 500-172643 500-172578 12/11/2012 10:19 1 TAL CHI CLM

A:9034 LCS 500-172578/2-A 500-172643 500-172578 12/11/2012 12:30 1 TAL CHI CLM

P:9030B LCS 500-172997/2-A 500-173039 500-172997 12/14/2012 11:35 1 TAL CHI CLM

A:9034 LCS 500-172997/2-A 500-173039 500-172997 12/14/2012 15:40 1 TAL CHI CLM

P:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 09:31 1 TAL CHI MTB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 60 of 360 12/26/2012
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53034-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LCSD N/A

P:1664A LCSD 

500-172887/3-A

500-172888 500-172887 12/14/2012 05:45 1 TAL CHI MTB

A:1664A LCSD 

500-172887/3-A

500-172888 500-172887 12/14/2012 08:07 1 TAL CHI MTB

Lab References:

TAL CHI = TestAmerica Chicago

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 61 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1664 HEM_00060 04/26/13 Mallin / JTBaker, Lot E50600 / K19H00 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L

SGT-HEM 4000 mg/L

8260 IS WK_00381 12/03/12 11/19/12 1, Lot NA 5 mL 8260 IS SK_00026 5 mL 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

.8260 IS SK_00026 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW IS_00104 12/14/12 11/30/12 MEOH, Lot DA946 20 mL 8260 IS SK_00027 4000 uL 1,4-Dichlorobenzene-d4 50 ug/mL

1,4-Difluorobenzene 50 ug/mL

Chlorobenzene-d5 50 ug/mL

Pentafluorobenzene 50 ug/mL

.8260 IS SK_00027 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW SS_00106 12/14/12 11/30/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 SS WK_00378 12/03/12 11/19/12 1, Lot NA 5 mL 8260 SS SK_00031 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

.8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

Page 62 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

Page 63 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Page 64 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

8260 STD WK_00216 12/25/12 12/11/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Page 65 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Page 66 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

ACR/NITRSTDWK_00212 12/18/12 12/11/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00034 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00034 02/28/13 Restek, Lot A091858 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

GAS STD WK RE_00244 11/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Page 67 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

GAS STD WK RE_00254 12/18/12 12/11/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

5 mL 8260 SS WK_00384 0.8656 1,2-Dichloroethane-d4 (Surr) 43.28 ug/L

uL

INST16 IS/SS_00222 12/26/12 12/12/12 1, Lot NA

4-Bromofluorobenzene (Surr) 43.28 ug/L

Dibromofluoromethane 43.28 ug/L

Toluene-d8 (Surr) 43.28 ug/L

.8260 SS WK_00384 12/26/12 12/12/12 1, Lot NA 5 mL 8260 SS SK_00032 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00183 12/18/12 12/04/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

Page 68 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acetone 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

Acetone 100 ug/mL

KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

level 1_00011 12/31/16 03/20/12 1, Lot CY647 1 mL level1std5ppm_00006 100 uL Benzene 0.5 ug/mL

Ethylbenzene 0.5 ug/mL

m-Xylene & p-Xylene 1 ug/mL

o-Xylene 0.5 ug/mL

Toluene 0.5 ug/mL

Trichloroethene 0.5 ug/mL

Vinyl chloride 0.5 ug/mL

.level1std5ppm_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level18260wk_00006 100 uL Benzene 5 ug/mL

Ethylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

o-Xylene 5 ug/mL

Toluene 5 ug/mL

Trichloroethene 5 ug/mL

level1gaswk_00006 100 uL Vinyl chloride 5 ug/mL

..level18260wk_00006 06/30/12 03/22/11 1, Lot NA 1 mL level18260sk_00001 1 mL Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

...level18260sk_00001 06/30/12 Restek, Lot AO67921 (Purchased Reagent) Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

..level1gaswk_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level1gaspt_00005 100 uL Vinyl chloride 100 ug/mL

...level1gaspt_00005 02/28/12 03/22/11 MEOH, Lot NA 1 mL level1gassk_00001 1 mL Vinyl chloride 2000 ug/mL

....level1gassk_00001 02/28/12 SUPELCO, Lot LB65254 (Purchased Reagent) Vinyl chloride 2000 ug/mL

LOW8260SS WK_00042 12/03/12 11/19/12 1, Lot DA057 1 mL 8260 SS WK_00378 200 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS WK_00378 12/03/12 11/19/12 1, Lot NA 5 mL 8260 SS SK_00031 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

Page 69 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

LOW8260STD WK_00209 11/26/12 11/19/12 1, Lot DG596 1 mL 8260 STD WK_00212 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Page 70 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00244 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00180 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00175 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

Page 71 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

Page 72 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

Page 73 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00244 11/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOW8260STD WK_00215 12/18/12 12/11/12 1, Lot DG860 1 mL 8260 STD WK_00216 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

Page 74 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00254 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Dichlorofluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00184 50 uL 2-Butanone (MEK) 5 ug/mL

Page 75 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00179 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00216 12/25/12 12/11/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

Page 76 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Page 77 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00254 12/18/12 12/11/12 METHANOL, Lot NA 2 mL GAS STD SK_00028 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00028 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Page 78 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00179 12/25/12 12/11/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOWACRSTD WK_00189 11/26/12 11/19/12 MEOH, Lot DG596 1 mL ACR/NITRSTDWK_00205 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

LOWACRSTD WK_00193 12/18/12 12/11/12 MEOH, Lot DG860 1 mL ACR/NITRSTDWK_00212 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00212 12/18/12 12/11/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00034 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00034 02/28/13 Restek, Lot A091858 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

M11FSTKHG_00001 05/31/17 ULTRA, Lot L00365 (Purchased Reagent) Mercury 1000 ug/mL

M12ASTKHG_00001 01/01/13 Inorganic Ventures, Lot E2-HG02091 (Purchased Reagent) Mercury 1000 ug/mL

M12JSPKIC_00002 05/23/13 10/04/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Page 79 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Page 80 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12KCCVIC_00002 07/10/13 11/20/12 1, Lot N/A 1000 mL M12GSTKIC_00002 10 mL Barium 0.5 ug/mL

Chromium 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.5 ug/mL

Nickel 0.5 ug/mL

Vanadium 5 ug/mL

Zinc 0.5 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12KSPKIC_00001 05/23/13 11/20/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Page 81 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12LCRIIC_00001 06/01/13 12/03/12 1, Lot NA 1000 mL M12ESTKIC_00002 2 mL Barium 20 ug/L

Chromium 20 ug/L

Copper 20 ug/L

Lead 10 ug/L

Page 82 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Nickel 20 ug/L

Vanadium 10 ug/L

Zinc 40 ug/L

.M12ESTKIC_00002 06/01/13 IV, Lot F2-MEB423074 (Purchased Reagent) Barium 10 ug/mL

Chromium 10 ug/mL

Copper 10 ug/mL

Lead 5 ug/mL

Nickel 10 ug/mL

Vanadium 5 ug/mL

Zinc 20 ug/mL

M12LICVIC_00001 07/10/13 12/06/12 1, Lot N/A 1000 mL M12GSTKIC_00002 8 mL Barium 0.4 ug/mL

Chromium 0.4 ug/mL

Copper 0.4 ug/mL

Lead 0.4 ug/mL

Nickel 0.4 ug/mL

Vanadium 4 ug/mL

Zinc 0.4 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12LISAIC_00001 12/01/13 12/03/12 1, Lot na 1000 mL M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

M12LISBIC_00001 09/01/13 12/03/12 1, Lot B51037 1000 mL M12ISTKIC_00003 10 mL Ag 0.2 ug/mL

As 0.1 ug/mL

Barium 0.5 ug/mL

Be 0.5 ug/mL

Cd 1 ug/mL

Chromium 0.5 ug/mL

Co 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.05 ug/mL

Mn 0.5 ug/mL

Nickel 1 ug/mL

Sb 0.6 ug/mL

Se 0.05 ug/mL

Tl 0.1 ug/mL

Vanadium 0.5 ug/mL

Page 83 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Zinc 1 ug/mL

M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12ISTKIC_00003 09/01/13 IV, Lot E2-MEB399019 (Purchased Reagent) Ag 20 ug/mL

As 10 ug/mL

Barium 50 ug/mL

Be 50 ug/mL

Cd 100 ug/mL

Chromium 50 ug/mL

Co 50 ug/mL

Copper 50 ug/mL

Lead 5 ug/mL

Mn 50 ug/mL

Nickel 100 ug/mL

Sb 60 ug/mL

Se 5 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 100 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VA/2CEVESTDWK_00179 12/25/12 12/11/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00024 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00025 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00024 02/21/13 11/21/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00025 02/21/13 11/21/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VOC/THF SPK_00124 12/03/12 11/19/12 1, Lot DG596 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00126 12/18/12 12/04/12 1, Lot DG596 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Page 84 of 360 12/26/2012
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00127 12/25/12 12/11/12 1, Lot DG860 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

WSTCR1_00008 04/30/15 ERA, Lot 160412 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTCR13_00623 12/25/12 STL, Lot Lead(II)Chrom_00001 (Purchased Reagent) Chromium, hexavalent 38.64 mg/L

WSTCR2_00008 05/31/17 Ultra Scientific, Lot L00439 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTINCN1_00564 12/13/12 12/13/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN1_00565 12/14/12 12/14/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN2_00556 12/13/12 12/13/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTINCN2_00557 12/14/12 12/14/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTSF1_00036 11/15/13 NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL (Purchased Reagent) Sulfide 180 mg/L

Sulfide as H2S 209.1 mg/L

Sulfide, Reactive 180 mg/L

Page 85 of 360 12/26/2012
Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory Authority Program EPA Region Certification ID

TestAmerica Chicago Alabama State Program 4 40461

TestAmerica Chicago California NELAP 9 01132CA

TestAmerica Chicago Georgia State Program 4 939

TestAmerica Chicago Georgia State Program 4 N/A

TestAmerica Chicago Hawaii State Program 9 N/A

TestAmerica Chicago Illinois NELAP 5 100201

TestAmerica Chicago Indiana State Program 5 C-IL-02

TestAmerica Chicago Iowa State Program 7 82

TestAmerica Chicago Kansas NELAP 7 E-10161

TestAmerica Chicago Kentucky State Program 4 90023

TestAmerica Chicago Kentucky (UST) State Program 4 66

TestAmerica Chicago L-A-B DoD ELAP L2304

TestAmerica Chicago L-A-B ISO/IEC 17025 L2304

TestAmerica Chicago Louisiana NELAP 6 30720

TestAmerica Chicago Massachusetts State Program 1 M-IL035

TestAmerica Chicago Mississippi State Program 4 N/A

TestAmerica Chicago North Carolina DENR State Program 4 291

TestAmerica Chicago North Dakota State Program 8 R-194

TestAmerica Chicago Oklahoma State Program 6 8908

TestAmerica Chicago South Carolina State Program 4 77001

TestAmerica Chicago Texas NELAP 6 T104704252-09-TX

TestAmerica Chicago USDA Federal P330-12-00038

TestAmerica Chicago Virginia NELAP 3 460142

TestAmerica Chicago Wisconsin State Program 5 999580010

TestAmerica Chicago Wyoming State Program 8 8TMS-Q

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s 

current list of certified methods and analytes.

Page 86 of 360 TestAmerica Chicago 12/26/2012
Method 8260B

Volatile Organic Compounds (GC/MS) 

by Method 8260B

Page 87 of 360 12/26/2012
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53034-1

SDG No.:

Matrix: Solid Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC Discrete 2 500-53034-2 109 117 104 97

MB 500-172698/4 109 106 114 107

LCS 500-172698/5 106 108 117 108

FC Discrete 2 MS 500-53034-2 MS 107 110 108 103

FC Discrete 2 MSD 500-53034-2 MSD 109 114 107 98

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B

# Column to be used to flag recovery values

Page 88 of 360 12/26/2012
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53034-1

SDG No.:

Matrix: Solid Level: Medium

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC Discrete 2 DL 500-53034-2 DL 97 97 98 92

MB 500-172879/6 90 88 93 88

LCS 500-172879/4 97 96 99 100

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 89 of 360 12/26/2012
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53034-1

SDG No.:

Matrix: Water Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC EB 2 500-53034-3 95 95 98 95

Trip Blank 500-53034-4 94 91 100 93

MB 500-172880/6 90 88 93 88

LCS 500-172880/4 97 96 99 100

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 90 of 360 12/26/2012
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53034-1

Solid Lab File ID: 16S1212.D

Lab ID: LCS 500-172698/5 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 47.36 95 50-138

2-Butanone (MEK) 50.0 47.66 95 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 91 of 360 12/26/2012
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Medium

500-53034-1

Solid Lab File ID: 22S1213.D

Lab ID: LCS 500-172879/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 46.30 93 46-153

2-Butanone (MEK) 50.0 46.82 94 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 92 of 360 12/26/2012
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53034-1

Water Lab File ID: 22S1213.D

Lab ID: LCS 500-172880/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/L)

SPIKE

ADDED

(ug/L)

#

LCS LCS

COMPOUND

Acetone 50.0 46.30 93 46-153

2-Butanone (MEK) 50.0 46.82 94 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 93 of 360 12/26/2012
GC/MS VOA MATRIX SPIKE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53034-1

Solid Lab File ID: 53034-02s.D

Lab ID: 500-53034-2 MS Client ID: FC Discrete 2 MS

TestAmerica Chicago

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED

(ug/Kg) (ug/Kg) (ug/Kg)

#

MS MS

Acetone 174 10800 9517 -745 50-138 E 4

2-Butanone (MEK) 174 72.6 176.3 60 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 94 of 360 12/26/2012
GC/MS VOA MATRIX SPIKE DUPLICATE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53034-1

Solid Lab File ID: 53034-02t.D

Lab ID: 500-53034-2 MSD Client ID: FC Discrete 2 MSD

TestAmerica Chicago

COMPOUND

SPIKE

ADDED CONCENTRATION %

REC

%

RPD

QC LIMITS

(ug/Kg) (ug/Kg) RPD REC 

#

MSD MSD

Acetone 174 10570 -140 10 30 50-138 E 4

2-Butanone (MEK) 174 194.9 70 10 30 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 95 of 360 12/26/2012
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/13/2012 13:24

DB624

Heated Purge:(Y/N) N

CMS22

Lab File ID: 22M1213.D Lab Sample ID: MB 500-172879/6

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-172879/4 22S1213.D 12/13/2012 12:32

FC Discrete 2 DL 500-53034-2 DL 53034-02C.D 12/13/2012 22:04

FORM IV 8260B

Page 96 of 360 12/26/2012
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/12/2012 08:26

DB624

Heated Purge:(Y/N) Y

CMS16

Lab File ID: 16M1212.D Lab Sample ID: MB 500-172698/4

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-172698/5 16S1212.D 12/12/2012 08:49

FC Discrete 2 500-53034-2 53034-02.D 12/12/2012 09:25

FC Discrete 2 MS 500-53034-2 MS 53034-02s.D 12/12/2012 09:49

FC Discrete 2 MSD 500-53034-2 MSD 53034-02t.D 12/12/2012 10:12

FORM IV 8260B

Page 97 of 360 12/26/2012
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53034-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/13/2012 13:24

DB624

Heated Purge:(Y/N) N

CMS22

Lab File ID: 22M1213.D Lab Sample ID: MB 500-172880/6

Matrix: Water

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-172880/4 22S1213.D 12/13/2012 12:32

Trip Blank 500-53034-4 53034-04.D 12/13/2012 14:15

FC EB 2 500-53034-3 53034-03.D 12/13/2012 15:33

FORM IV 8260B

Page 98 of 360 12/26/2012
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53034-1

Lab File ID:

Instrument ID:

16B1119c.D

CMS16

11/19/2012

11:14

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 170196

50 15.0 - 40.0 % of mass 95 19.7 

75 30.0 - 60.0 % of mass 95 53.5 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.7 (1.0)1

174 50.0 - 120.00 % of mass 95 75.9 

175 5.0 - 9.0 % of mass 174 5.3 (6.9)1

176 95.0 - 101.0 % of mass 174 74.4 (98.0)1

177 5.0 - 9.0 % of mass 176 5.8 (7.8)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-170196/6 16I1119A.D 11/19/2012 12:14

STD2 500-170196/7 16I1119B.D 11/19/2012 12:37

STD3 500-170196/8 16I1119C.D 11/19/2012 13:00

STD4 500-170196/9 16I1119D.D 11/19/2012 13:23

STD5 500-170196/10 16I1119E.D 11/19/2012 13:46

STD6 500-170196/11 16I1119F.D 11/19/2012 14:09

ICV 500-170196/19 16S1119.D 11/19/2012 17:14

FORM V 8260B Page 99 of 360 12/26/2012
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53034-1

Lab File ID:

Instrument ID:

16B1212.D

CMS16

12/12/2012

07:05

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172698

50 15.0 - 40.0 % of mass 95 25.2 

75 30.0 - 60.0 % of mass 95 55.3 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 8.2 

173 Less than 2.0 % of mass 174 0.5 (0.6)1

174 50.0 - 120.00 % of mass 95 82.1 

175 5.0 - 9.0 % of mass 174 5.8 (7.0)1

176 95.0 - 101.0 % of mass 174 79.6 (96.9)1

177 5.0 - 9.0 % of mass 176 5.5 (6.9)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCVIS 500-172698/2 16C1212.D 12/12/2012 07:39

CCV 500-172698/3 16D1212.D 12/12/2012 08:03

MB 500-172698/4 16M1212.D 12/12/2012 08:26

LCS 500-172698/5 16S1212.D 12/12/2012 08:49

FC Discrete 2 500-53034-2 53034-02.D 12/12/2012 09:25

FC Discrete 2 MS 53034-02s.

D

500-53034-2 MS 12/12/2012 09:49

FC Discrete 2 MSD 53034-02t.

D

500-53034-2 MSD 12/12/2012 10:12

FORM V 8260B Page 100 of 360 12/26/2012
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53034-1

Lab File ID:

Instrument ID:

22B1211.D

CMS22

12/11/2012

13:45

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172614

50 15.0 - 40.0 % of mass 95 22.6 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 86.2 

175 5.0 - 9.0 % of mass 174 5.9 (6.8)1

176 95.0 - 101.0 % of mass 174 86.4 (100.2)1

177 5.0 - 9.0 % of mass 176 4.9 (5.7)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD01 500-172614/2 22I1211A.D 12/11/2012 14:23

STD02 500-172614/3 22I1211B.D 12/11/2012 14:51

STD03 500-172614/4 22I1211C.D 12/11/2012 15:20

STD04 500-172614/5 22I1211D.D 12/11/2012 15:48

STD05 500-172614/6 22I1211E.D 12/11/2012 16:16

STD06 500-172614/7 22I1211F.D 12/11/2012 16:44

STD07 500-172614/8 22I1211G.D 12/11/2012 17:13

STD08 500-172614/9 22I1211H.D 12/11/2012 17:41

STD09 500-172614/10 22I1211I.D 12/11/2012 18:09

ICV 500-172614/23 22S1211.D 12/12/2012 00:17

FORM V 8260B Page 101 of 360 12/26/2012
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53034-1

Lab File ID:

Instrument ID:

22B1211.D

CMS22

12/11/2012

13:45

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172615

50 15.0 - 40.0 % of mass 95 22.6 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 86.2 

175 5.0 - 9.0 % of mass 174 5.9 (6.8)1

176 95.0 - 101.0 % of mass 174 86.4 (100.2)1

177 5.0 - 9.0 % of mass 176 4.9 (5.7)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD01 500-172615/2 22I1211A.D 12/11/2012 14:23

STD02 500-172615/3 22I1211B.D 12/11/2012 14:51

STD03 500-172615/4 22I1211C.D 12/11/2012 15:20

STD04 500-172615/5 22I1211D.D 12/11/2012 15:48

STD05 500-172615/6 22I1211E.D 12/11/2012 16:16

STD06 500-172615/7 22I1211F.D 12/11/2012 16:44

STD07 500-172615/8 22I1211G.D 12/11/2012 17:13

STD08 500-172615/9 22I1211H.D 12/11/2012 17:41

STD09 500-172615/10 22I1211I.D 12/11/2012 18:09

ICV 500-172615/23 22S1211.D 12/12/2012 00:17

FORM V 8260B Page 102 of 360 12/26/2012
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53034-1

Lab File ID:

Instrument ID:

22B1213.D

CMS22

12/13/2012

11:02

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172879

50 15.0 - 40.0 % of mass 95 25.1 

75 30.0 - 60.0 % of mass 95 49.6 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.6 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 90.1 

175 5.0 - 9.0 % of mass 174 8.0 (8.8)1

176 95.0 - 101.0 % of mass 174 89.0 (98.9)1

177 5.0 - 9.0 % of mass 176 7.1 (8.0)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-172879/2 22C1213.D 12/13/2012 11:40

CCV 500-172879/3 22D1213.D 12/13/2012 12:06

LCS 500-172879/4 22S1213.D 12/13/2012 12:32

MB 500-172879/6 22M1213.D 12/13/2012 13:24

FC Discrete 2 DL 53034-02C.

D

500-53034-2 DL 12/13/2012 22:04

FORM V 8260B Page 103 of 360 12/26/2012
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53034-1

Lab File ID:

Instrument ID:

22B1213.D

CMS22

12/13/2012

11:02

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 172880

50 15.0 - 40.0 % of mass 95 25.1 

75 30.0 - 60.0 % of mass 95 49.6 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.6 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 90.1 

175 5.0 - 9.0 % of mass 174 8.0 (8.8)1

176 95.0 - 101.0 % of mass 174 89.0 (98.9)1

177 5.0 - 9.0 % of mass 176 7.1 (8.0)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-172880/2 22C1213.D 12/13/2012 11:40

CCV 500-172880/3 22D1213.D 12/13/2012 12:06

LCS 500-172880/4 22S1213.D 12/13/2012 12:32

MB 500-172880/6 22M1213.D 12/13/2012 13:24

Trip Blank 500-53034-4 53034-04.D 12/13/2012 14:15

FC EB 2 500-53034-3 53034-03.D 12/13/2012 15:33

FORM V 8260B Page 104 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: STD3 500-170196/8 Date Analyzed: 11/19/2012 13:00

Lab File ID (Standard): 16I1119C.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10620

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

464716

116179 170040

680160

134826

539304

INITIAL CALIBRATION MID-POINT 3.42 3.99 6.38

3.92

2.92

4.49

3.49

6.88

5.88

232358 340080 269652

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170196/19 258949 3.42 378895 3.99 285510 6.38

CCVIS 500-172698/2 273608 3.42 395398 3.99 306910 6.38

CCV 500-172698/3 270384 3.42 394659 3.99 300811 6.38

MB 500-172698/4 256948 3.42 372988 3.99 292825 6.38

LCS 500-172698/5 263198 3.42 380732 3.99 302033 6.38

500-53034-2 FC Discrete 2 237666 3.42 347632 3.99 237541 6.38

500-53034-2 MS FC Discrete 2 MS 249779 3.41 360391 3.99 263190 6.38

500-53034-2 MSD FC Discrete 2 MSD 240312 3.42 356544 3.99 252786 6.38

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 105 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: STD3 500-170196/8 Date Analyzed: 11/19/2012 13:00

Lab File ID (Standard): 16I1119C.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10620

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

283260

70815

INITIAL CALIBRATION MID-POINT 8.21

8.71

7.71

141630

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170196/19 139276 8.21

CCVIS 500-172698/2 147074 8.21

CCV 500-172698/3 148102 8.21

MB 500-172698/4 138797 8.21

LCS 500-172698/5 150233 8.21

500-53034-2 FC Discrete 2 81347 8.21

500-53034-2 MS FC Discrete 2 MS 108628 8.21

500-53034-2 MSD FC Discrete 2 MSD 96028 8.21

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 106 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: CCVIS 500-172698/2 Date Analyzed: 12/12/2012 07:39

Lab File ID (Standard): 16C1212.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10621

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

547216

136804 197699

790796

153455

613820

12/24 HOUR STD 3.42 3.99 6.38

3.92

2.92

4.49

3.49

6.88

5.88

273608 395398 306910

LAB SAMPLE ID CLIENT SAMPLE ID

CCV 500-172698/3 270384 3.42 394659 3.99 300811 6.38

MB 500-172698/4 256948 3.42 372988 3.99 292825 6.38

LCS 500-172698/5 263198 3.42 380732 3.99 302033 6.38

500-53034-2 FC Discrete 2 237666 3.42 347632 3.99 237541 6.38

500-53034-2 MS FC Discrete 2 MS 249779 3.41 360391 3.99 263190 6.38

500-53034-2 MSD FC Discrete 2 MSD 240312 3.42 356544 3.99 252786 6.38

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 107 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: CCVIS 500-172698/2 Date Analyzed: 12/12/2012 07:39

Lab File ID (Standard): 16C1212.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10621

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

294148

73537

12/24 HOUR STD 8.21

8.71

7.71

147074

LAB SAMPLE ID CLIENT SAMPLE ID

CCV 500-172698/3 148102 8.21

MB 500-172698/4 138797 8.21

LCS 500-172698/5 150233 8.21

500-53034-2 FC Discrete 2 81347 8.21

500-53034-2 MS FC Discrete 2 MS 108628 8.21

500-53034-2 MSD FC Discrete 2 MSD 96028 8.21

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 108 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: STD06 500-172614/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10829

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

1409738

352435 493044

1972176

417716

1670864

INITIAL CALIBRATION MID-POINT 6.27 7.24 10.64

6.77

5.77

7.74

6.74

11.14

10.14

704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172614/23 772269 6.26 1099840 7.24 931671 10.64

CCV 500-172879/2 803413 6.26 1119844 7.24 962009 10.64

CCV 500-172879/3 711972 6.26 994059 7.24 834331 10.64

LCS 500-172879/4 823916 6.26 1136899 7.24 955127 10.64

MB 500-172879/6 753178 6.27 1047011 7.24 904207 10.64

500-53034-2 DL FC Discrete 2 DL 743297 6.26 1060731 7.24 898918 10.64

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 109 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: STD06 500-172614/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10829

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

1003186

250797

INITIAL CALIBRATION MID-POINT 13.08

13.58

12.58

501593

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172614/23 542063 13.08

CCV 500-172879/2 576322 13.08

CCV 500-172879/3 464399 13.08

LCS 500-172879/4 570738 13.08

MB 500-172879/6 489274 13.07

500-53034-2 DL FC Discrete 2 DL 483522 13.08

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 110 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: STD06 500-172615/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10830

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

1409738

352435 493044

1972176

417716

1670864

INITIAL CALIBRATION MID-POINT 6.27 7.24 10.64

6.77

5.77

7.74

6.74

11.14

10.14

704869 986088 835432

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172615/23 772269 6.26 1099840 7.24 931671 10.64

CCV 500-172880/2 803413 6.26 1119844 7.24 962009 10.64

CCV 500-172880/3 711972 6.26 994059 7.24 834331 10.64

LCS 500-172880/4 823916 6.26 1136899 7.24 955127 10.64

MB 500-172880/6 753178 6.27 1047011 7.24 904207 10.64

500-53034-4 Trip Blank 778296 6.27 1070689 7.24 930273 10.64

500-53034-3 FC EB 2 809730 6.26 1121152 7.24 945352 10.64

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 111 of 360 12/26/2012
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53034-1

Sample No.: STD06 500-172615/7 Date Analyzed: 12/11/2012 16:44

Lab File ID (Standard): 22I1211F.D

Instrument ID: CMS22 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) N

Calibration ID: 10830

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

1003186

250797

INITIAL CALIBRATION MID-POINT 13.08

13.58

12.58

501593

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-172615/23 542063 13.08

CCV 500-172880/2 576322 13.08

CCV 500-172880/3 464399 13.08

LCS 500-172880/4 570738 13.08

MB 500-172880/6 489274 13.07

500-53034-4 Trip Blank 509611 13.08

500-53034-3 FC EB 2 525515 13.08

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 112 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC Discrete 2

SDG No.:

500-53034-1

Lab Sample ID: 500-53034-2

Matrix: Lab File ID: 53034-02.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/06/2012 14:25

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.3

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/12/2012 09:25

DB624 ID:

Analysis Batch No.: 172698 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

78-93-3 2-Butanone (MEK) 72.6 17.4 6.30

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 117 70-134

2037-26-5 Toluene-d8 (Surr) 104 75-122

460-00-4 4-Bromofluorobenzene (Surr) 97 70-122

1868-53-7 Dibromofluoromethane 109 75-120

FORM I 8260B

Page 113 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC Discrete 2 DL

SDG No.:

500-53034-1

Lab Sample ID: 500-53034-2 DL

Matrix: Lab File ID: 53034-02C.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/06/2012 14:25

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.3

50

Level: (low/med) Medium

5(g)

5 (mL)

5(mL) 0.2(mm)

Date Analyzed: 12/13/2012 22:04

DB624 ID:

Analysis Batch No.: 172879 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 9130 870 226

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-125

2037-26-5 Toluene-d8 (Surr) 98 75-120

460-00-4 4-Bromofluorobenzene (Surr) 92 75-120

1868-53-7 Dibromofluoromethane 97 75-120

FORM I 8260B

Page 114 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC EB 2

SDG No.:

500-53034-1

Lab Sample ID: 500-53034-3

Matrix: Lab File ID: 53034-03.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/06/2012 14:15

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/13/2012 15:33

DB624 ID:

Analysis Batch No.: 172880 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 75-125

2037-26-5 Toluene-d8 (Surr) 98 75-120

460-00-4 4-Bromofluorobenzene (Surr) 95 75-120

1868-53-7 Dibromofluoromethane 95 75-120

FORM I 8260B

Page 115 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

Trip Blank

SDG No.:

500-53034-1

Lab Sample ID: 500-53034-4

Matrix: Lab File ID: 53034-04.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/06/2012 00:00

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/13/2012 14:15

DB624 ID:

Analysis Batch No.: 172880 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 91 75-125

2037-26-5 Toluene-d8 (Surr) 100 75-120

460-00-4 4-Bromofluorobenzene (Surr) 93 75-120

1868-53-7 Dibromofluoromethane 94 75-120

FORM I 8260B

Page 116 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170196/6 16I1119A.D

Level 2 STD2 500-170196/7 16I1119B.D

Level 3 STD3 500-170196/8 16I1119C.D

Level 4 STD4 500-170196/9 16I1119D.D

Level 5 STD5 500-170196/10 16I1119E.D

Level 6 STD6 500-170196/11 16I1119F.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Dichlorodifluoromethane 0.5101 0.4328 0.4745 0.4472 0.4791 Ave 5.9

0.4553

0.4665 0.0100 15.0

Chloromethane 0.6409 0.5486 0.6042 0.5514 0.5726 Ave 6.2

0.5611

0.5798 0.1000 15.0

Vinyl chloride 0.5489 0.4879 0.5232 0.4889 0.5055 Ave 4.9

0.4889

0.5072 0.0100 15.0

Bromomethane 0.2173 0.1622 0.1619 0.1577 0.1599 Lin2 0.9990

0.1594

0.3023 0.1550 0.0100 0.9900

Chloroethane 0.2848 0.2512 0.2658 0.2550 0.2653 Ave 4.4

0.2627

0.2641 0.0100 15.0

Trichlorofluoromethane 0.6410 0.5479 0.5898 0.5813 0.5855 Ave 5.1

0.5792

0.5875 0.0100 15.0

Acrolein 0.0833 0.0649 0.0739 0.0632 0.0635 Lin2 0.9920

0.0576

4.1129 0.0627 0.0010 0.9900

1,1-Dichloroethene 0.3883 0.3810 0.3940 0.3681 0.3657 Ave 4.2

0.3520

0.3748 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.4271 0.3940 0.4076 0.3784 0.3788 Ave 6.6

0.3531

0.3898 0.0100 15.0

Acetone 0.2177 0.1065 0.1169 0.1078 0.1047 Lin1 0.9950

0.0952

0.5599 0.0976 0.0100 0.9900

Carbon disulfide 1.2281 1.2015 1.3462 1.3937 1.2778 Ave 5.7

1.2592

1.2844 0.0100 15.0

Acetonitrile 0.0349 0.0327 0.0349 0.0328 0.0329 Ave 6.1

0.0294

0.0330 0.0010 15.0

Methylene Chloride 0.4402 0.4262 0.4539 0.4254 0.4228 Ave 4.4

0.3973

0.4276 0.0100 15.0

Acrylonitrile 0.1608 0.1223 0.1370 0.1213 0.1263 Lin2 0.9950

0.1142

1.5562 0.1209 0.0010 0.9900

trans-1,2-Dichloroethene 0.4687 0.4410 0.4603 0.4325 0.4314 Ave 4.6

0.4139

0.4413 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 117 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Methyl tert-butyl ether 1.2409 1.0967 1.2053 1.0887 1.1030 Ave 7.6

1.0084

1.1238 0.0100 15.0

1,1-Dichloroethane 0.9158 0.8754 0.8985 0.8573 0.8580 Ave 4.0

0.8171

0.8704 0.1000 15.0

Vinyl acetate 0.7794 0.7899 0.8439 0.8848 0.9027 Ave 6.1

0.8075

0.8347 0.0100 15.0

2,2-Dichloropropane 0.5123 0.4762 0.4910 0.4760 0.4692 Ave 5.5

0.4333

0.4764 0.0100 15.0

cis-1,2-Dichloroethene 0.5178 0.4752 0.4900 0.4699 0.4727 Ave 4.9

0.4468

0.4787 0.0100 15.0

2-Butanone (MEK) 0.1907 0.1661 0.1744 0.1666 0.1738 Ave 7.0

0.1547

0.1710 0.0100 15.0

Propionitrile 0.0377 0.0303 0.0325 0.0300 0.0310 Ave 10.0

0.0283

0.0316 0.0010 15.0

Bromochloromethane 0.2134 0.1810 0.1955 0.1835 0.1826 Ave 7.7

0.1724

0.1881 0.0100 15.0

Tetrahydrofuran 0.1362 0.1110 0.1157 0.1060 0.1101 Lin2 0.9970

0.0981

0.1550 0.1053 0.0100 0.9900

Chloroform 0.8071 0.7676 0.7909 0.7569 0.7592 Ave 3.9

0.7200

0.7669 0.0100 15.0

1,1,1-Trichloroethane 0.6379 0.6227 0.6514 0.6248 0.6266 Ave 3.7

0.5828

0.6244 0.0100 15.0

Carbon tetrachloride 0.3601 0.3514 0.3626 0.3590 0.3620 Ave 1.9

0.3457

0.3568 0.0100 15.0

1,1-Dichloropropene 0.6628 0.6440 0.6397 0.6320 0.6326 Ave 3.2

0.6014

0.6354 0.0100 15.0

Benzene 1.2960 1.2332 1.2212 1.1893 1.1679 Ave 5.2

1.1124

1.2033 0.0100 15.0

1,2-Dichloroethane 0.4036 0.3828 0.3925 0.3773 0.3822 Ave 3.7

0.3615

0.3833 0.0100 15.0

Trichloroethene 0.3071 0.2871 0.2880 0.2787 0.2819 Ave 4.3

0.2706

0.2856 0.0100 15.0

1,2-Dichloropropane 0.2945 0.3110 0.2983 0.3002 0.3013 Ave 2.3

0.2903

0.2993 0.0100 15.0

Dibromomethane 0.1499 0.1401 0.1448 0.1410 0.1445 Ave 3.6

0.1346

0.1425 0.0100 15.0

Bromodichloromethane 0.3131 0.3276 0.3492 0.3570 0.3677 Ave 5.9

0.3548

0.3449 0.0100 15.0

2-Chloroethyl vinyl ether 0.1275 0.1289 0.1333 0.1400 0.1446 Ave 5.1

0.1302

0.1341 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 118 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

cis-1,3-Dichloropropene 0.3823 0.3878 0.3955 0.4081 0.4277 Ave 4.1

0.4075

0.4015 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.2134 0.2212 0.2438 0.2360 0.2310 Ave 5.2

0.2176

0.2272 0.0100 15.0

Toluene 0.7563 0.7457 0.7103 0.7065 0.7016 Ave 4.3

0.6724

0.7155 0.0100 15.0

trans-1,3-Dichloropropene 0.3019 0.3263 0.3366 0.3455 0.3644 Ave 6.4

0.3505

0.3375 0.0100 15.0

1,1,2-Trichloroethane 0.2720 0.2647 0.2830 0.2757 0.2832 Ave 2.6

0.2710

0.2749 0.0100 15.0

Tetrachloroethene 0.3877 0.3857 0.3641 0.3770 0.3714 Ave 3.1

0.3585

0.3741 0.0100 15.0

1,3-Dichloropropane 0.4386 0.4678 0.4537 0.4585 0.4651 Ave 2.7

0.4404

0.4540 0.0100 15.0

2-Hexanone 0.1953 0.1931 0.1955 0.2045 0.1961 Ave 2.7

0.1880

0.1954 0.0100 15.0

Dibromochloromethane 0.2040 0.2329 0.2507 0.2602 0.2677 Ave 9.7

0.2616

0.2462 0.0100 15.0

1,2-Dibromoethane 0.1811 0.1775 0.1848 0.1786 0.1848 Ave 2.7

0.1720

0.1798 0.0100 15.0

1-Chlorohexane 0.6093 0.5831 0.5505 0.5582 0.5737 Ave 4.3

0.5435

0.5697 0.0100 15.0

Chlorobenzene 0.9184 0.9225 0.9033 0.9116 0.9054 Ave 2.2

0.8681

0.9049 0.3000 15.0

1,1,1,2-Tetrachloroethane 0.2930 0.2979 0.3101 0.3188 0.3208 Ave 3.6

0.3132

0.3090 0.0100 15.0

Ethylbenzene 0.5544 0.5503 0.5126 0.5352 0.5171 Ave 4.1

0.5009

0.5284 0.0100 15.0

m&p-Xylene 1.3686 1.3827 1.3012 1.2861 1.2289 Ave 6.9

1.1453

1.2855 0.0100 15.0

o-Xylene 1.3495 1.4372 1.3698 1.3557 1.3252 Ave 4.5

1.2528

1.3484 0.0100 15.0

Styrene 0.9608 1.0612 1.0145 1.0388 1.0303 Ave 3.6

0.9843

1.0150 0.0100 15.0

Bromoform 0.1125 0.1362 0.1408 0.1514 0.1643 Ave 13.0

0.1539

0.1432 0.1000 15.0

Isopropylbenzene 3.1539 3.6540 3.1572 3.3315 3.1688 Ave 6.7

3.0455

3.2518 0.0100 15.0

Bromobenzene 0.6695 0.7563 0.7093 0.7420 0.7361 Ave 4.2

0.7199

0.7222 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 119 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

1,1,2,2-Tetrachloroethane 0.5452 0.5696 0.5597 0.5706 0.5758 Ave 3.0

0.5328

0.5589 0.3000 15.0

1,2,3-Trichloropropane 0.1912 0.1794 0.1660 0.1701 0.1701 Ave 6.1

0.1622

0.1732 0.0100 15.0

N-Propylbenzene 3.9287 4.2993 3.7879 3.9367 3.7362 Ave 6.3

3.5832

3.8787 0.0100 15.0

2-Chlorotoluene 2.3554 2.5038 2.2305 2.3361 2.2656 Ave 4.9

2.1830

2.3124 0.0100 15.0

1,3,5-Trimethylbenzene 2.6219 2.9360 2.6333 2.7109 2.6361 Ave 5.3

2.5201

2.6764 0.0100 15.0

4-Chlorotoluene 2.6491 2.9401 2.6216 2.7188 2.6440 Ave 5.1

2.5353

2.6848 0.0100 15.0

tert-Butylbenzene 2.2801 2.5455 2.2199 2.2982 2.2247 Ave 6.1

2.1418

2.2850 0.0100 15.0

1,2,4-Trimethylbenzene 2.7631 3.0061 2.6438 2.7255 2.6458 Ave 5.8

2.5511

2.7226 0.0100 15.0

sec-Butylbenzene 3.5331 3.8935 3.3623 3.4462 3.3180 Ave 7.1

3.1870

3.4567 0.0100 15.0

1,3-Dichlorobenzene 1.4471 1.5053 1.3813 1.4255 1.3778 Ave 4.0

1.3501

1.4145 0.0100 15.0

p-Isopropyltoluene 2.9586 3.2474 2.8310 2.8845 2.8017 Ave 6.6

2.6869

2.9017 0.0100 15.0

1,4-Dichlorobenzene 1.3977 1.4878 1.3669 1.4117 1.3954 Ave 3.8

1.3295

1.3982 0.0100 15.0

n-Butylbenzene 2.8602 3.1543 2.7994 2.7899 2.7599 Ave 6.2

2.6239

2.8313 0.0100 15.0

1,2-Dichlorobenzene 1.2797 1.3306 1.2155 1.2573 1.2376 Ave 3.9

1.1916

1.2521 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0873 0.0832 0.0794 0.0812 0.0900 Ave 4.7

0.0826

0.0839 0.0100 15.0

1,2,4-Trichlorobenzene 0.9789 0.9823 0.8678 0.7520 0.7794 Ave 13.0

0.7396

0.8500 0.0100 15.0

Hexachlorobutadiene 0.6292 0.6291 0.5100 0.4198 0.4138 Qua1 0.9940

+++++

0.7417 0.5403 -0.001 0.0100 0.9900

Naphthalene 1.6968 1.5945 1.4268 1.3407 1.4423 Lin2 0.9970

1.3291

1.6628 1.3908 0.0100 0.9900

1,2,3-Trichlorobenzene 0.7531 0.7667 0.6080 0.5315 0.5708 Qua2 0.9900

0.5407

0.4654 0.6784 -0.001 0.0100 0.9900

Dibromofluoromethane 0.4012 0.4120 0.3878 0.4079 Ave 4.3

0.3703

0.3958 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 120 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

1,2-Dichloroethane-d4 (Surr) 0.3252 0.3396 0.3092 0.3325 Ave 6.0

0.2918

0.3196 0.0100 15.0

Toluene-d8 (Surr) 1.0538 1.0512 0.9999 1.0425 Ave 4.8

0.9393

1.0174 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5024 0.5042 0.4741 0.5018 Ave 5.3

0.4456

0.4856 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 121 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170196/6 16I1119A.D

Level 2 STD2 500-170196/7 16I1119B.D

Level 3 STD3 500-170196/8 16I1119C.D

Level 4 STD4 500-170196/9 16I1119D.D

Level 5 STD5 500-170196/10 16I1119E.D

Level 6 STD6 500-170196/11 16I1119F.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Dichlorodifluoromethane PFB Ave 12902 50070 127370 264568 422626

553924

5.00 20.0 50.0 100 150

200

Chloromethane PFB Ave 16213 63463 162200 326211 505093

682571

5.00 20.0 50.0 100 150

200

Vinyl chloride PFB Ave 13885 56436 140448 289222 445896

594740

5.00 20.0 50.0 100 150

200

Bromomethane PFB Lin2 5496 18758 43458 93314 141095

193922

5.00 20.0 50.0 100 150

200

Chloroethane PFB Ave 7205 29060 71345 150837 234006

319655

5.00 20.0 50.0 100 150

200

Trichlorofluoromethane PFB Ave 16215 63387 158331 343881 516513

704692

5.00 20.0 50.0 100 150

200

Acrolein PFB Lin2 84258 300252 793200 1494545 2240120

2801943

200 800 2000 4000 6000

8000

1,1-Dichloroethene PFB Ave 9821 44072 105755 217759 322621

428198

5.00 20.0 50.0 100 150

200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 10804 45578 109401 223828 334178

429549

5.00 20.0 50.0 100 150

200

Acetone PFB Lin1 5507 12315 31383 63749 92368

115814

5.00 20.0 50.0 100 150

200

Carbon disulfide PFB Ave 31066 138989 361364 824494 1127201

1531938

5.00 20.0 50.0 100 150

200

Acetonitrile PFB Ave 7059 30299 75012 155141 232468

286410

40.0 160 400 800 1200

1600

Methylene Chloride PFB Ave 11136 49301 121856 251650 373003

483310

5.00 20.0 50.0 100 150

200

Acrylonitrile PFB Lin2 32531 113188 294241 574185 891617

1111839

40.0 160 400 800 1200

1600

trans-1,2-Dichloroethene PFB Ave 11855 51013 123566 255847 380526

503496

5.00 20.0 50.0 100 150

200

Methyl tert-butyl ether PFB Ave 31388 126868 323557 644017 972967

1226790

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 122 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

1,1-Dichloroethane PFB Ave 23166 101272 241193 507139 756847

994036

5.00 20.0 50.0 100 150

200

Vinyl acetate PFB Ave 19714 91380 226543 523396 796266

982422

5.00 20.0 50.0 100 150

200

2,2-Dichloropropane PFB Ave 12960 55088 131791 281610 413914

527180

5.00 20.0 50.0 100 150

200

cis-1,2-Dichloroethene PFB Ave 13099 54969 131526 277962 416945

543539

5.00 20.0 50.0 100 150

200

2-Butanone (MEK) PFB Ave 4823 19213 46819 98580 153328

188153

5.00 20.0 50.0 100 150

200

Propionitrile DFB Ave 11092 40835 102296 208849 323908

406897

40.0 160 400 800 1200

1600

Bromochloromethane PFB Ave 5399 20944 52481 108571 161097

209785

5.00 20.0 50.0 100 150

200

Tetrahydrofuran PFB Lin2 3446 12837 31053 62700 97150

119315

5.00 20.0 50.0 100 150

200

Chloroform PFB Ave 20416 88794 212306 447767 669705

875928

5.00 20.0 50.0 100 150

200

1,1,1-Trichloroethane PFB Ave 16137 72040 174862 369627 552754

709015

5.00 20.0 50.0 100 150

200

Carbon tetrachloride DFB Ave 13245 59272 142459 312633 472055

620557

5.00 20.0 50.0 100 150

200

1,1-Dichloropropene PFB Ave 16767 74498 171713 373900 558058

731603

5.00 20.0 50.0 100 150

200

Benzene DFB Ave 47671 208006 479794 1035802 1523052

1996925

5.00 20.0 50.0 100 150

200

1,2-Dichloroethane DFB Ave 14847 64572 154226 328584 498369

649012

5.00 20.0 50.0 100 150

200

Trichloroethene DFB Ave 11297 48428 113149 242684 367651

485784

5.00 20.0 50.0 100 150

200

1,2-Dichloropropane DFB Ave 10834 52448 117184 261424 392941

521104

5.00 20.0 50.0 100 150

200

Dibromomethane DFB Ave 5515 23635 56895 122814 188390

241667

5.00 20.0 50.0 100 150

200

Bromodichloromethane DFB Ave 11517 55249 137199 310916 479512

636972

5.00 20.0 50.0 100 150

200

2-Chloroethyl vinyl ether DFB Ave 4691 21736 52381 121903 188565

233764

5.00 20.0 50.0 100 150

200

cis-1,3-Dichloropropene DFB Ave 14063 65411 155392 355410 557705

731626

5.00 20.0 50.0 100 150

200

4-Methyl-2-pentanone (MIBK) DFB Ave 7850 37307 95785 205560 301187

390574

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 123 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Toluene DFB Ave 27820 125770 279057 615277 914875

1207131

5.00 20.0 50.0 100 150

200

trans-1,3-Dichloropropene DFB Ave 11105 55044 132225 300866 475199

629293

5.00 20.0 50.0 100 150

200

1,1,2-Trichloroethane PFB Ave 6881 30616 75972 163072 249804

329645

5.00 20.0 50.0 100 150

200

Tetrachloroethene CBZ Ave 11739 49681 113412 247302 371178

488872

5.00 20.0 50.0 100 150

200

1,3-Dichloropropane CBZ Ave 13281 60253 141339 300730 464793

600568

5.00 20.0 50.0 100 150

200

2-Hexanone CBZ Ave 5913 24867 60900 134127 195945

256358

5.00 20.0 50.0 100 150

200

Dibromochloromethane CBZ Ave 6176 29991 78104 170673 267577

356811

5.00 20.0 50.0 100 150

200

1,2-Dibromoethane DFB Ave 6662 29944 72598 155572 240952

308703

5.00 20.0 50.0 100 150

200

1-Chlorohexane PFB Ave 15413 67451 147771 330227 506094

661180

5.00 20.0 50.0 100 150

200

Chlorobenzene CBZ Ave 27808 118815 281396 597934 904889

1183858

5.00 20.0 50.0 100 150

200

1,1,1,2-Tetrachloroethane CBZ Ave 8870 38367 96602 209122 320615

427140

5.00 20.0 50.0 100 150

200

Ethylbenzene CBZ Ave 16785 70876 159684 351002 516773

683074

5.00 20.0 50.0 100 150

200

m&p-Xylene CBZ Ave 82877 356156 810673 1687130 2456378

3123829

10.0 40.0 100 200 300

400

o-Xylene CBZ Ave 40858 185102 426723 889192 1324449

1708514

5.00 20.0 50.0 100 150

200

Styrene CBZ Ave 29090 136679 316041 681314 1029721

1342275

5.00 20.0 50.0 100 150

200

Bromoform CBZ Ave 3407 17540 43862 99282 164184

209852

5.00 20.0 50.0 100 150

200

Isopropylbenzene DCB Ave 51019 228406 516591 1065124 1575324

2017775

5.00 20.0 50.0 100 150

200

Bromobenzene DCB Ave 10830 47272 116055 237235 365963

476962

5.00 20.0 50.0 100 150

200

1,1,2,2-Tetrachloroethane DCB Ave 8819 35605 91578 182439 286268

352978

5.00 20.0 50.0 100 150

200

1,2,3-Trichloropropane DCB Ave 3093 11214 27159 54392 84576

107459

5.00 20.0 50.0 100 150

200

N-Propylbenzene DCB Ave 63553 268743 619776 1258627 1857403

2373990

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 124 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

2-Chlorotoluene DCB Ave 38102 156509 364951 746878 1126306

1446295

5.00 20.0 50.0 100 150

200

1,3,5-Trimethylbenzene DCB Ave 42413 183522 430864 866728 1310538

1669636

5.00 20.0 50.0 100 150

200

4-Chlorotoluene DCB Ave 42853 183778 428943 869237 1314457

1679760

5.00 20.0 50.0 100 150

200

tert-Butylbenzene DCB Ave 36885 159113 363220 734777 1106000

1419051

5.00 20.0 50.0 100 150

200

1,2,4-Trimethylbenzene DCB Ave 44697 187908 432579 871394 1315353

1690213

5.00 20.0 50.0 100 150

200

sec-Butylbenzene DCB Ave 57153 243374 550146 1101803 1649521

2111505

5.00 20.0 50.0 100 150

200

1,3-Dichlorobenzene DCB Ave 23410 94092 226011 455769 684977

894523

5.00 20.0 50.0 100 150

200

p-Isopropyltoluene DCB Ave 47861 202992 463212 922211 1392838

1780196

5.00 20.0 50.0 100 150

200

1,4-Dichlorobenzene DCB Ave 22610 92998 223660 451341 693731

880833

5.00 20.0 50.0 100 150

200

n-Butylbenzene DCB Ave 46268 197168 458033 891981 1372078

1738419

5.00 20.0 50.0 100 150

200

1,2-Dichlorobenzene DCB Ave 20701 83175 198883 401981 615248

789503

5.00 20.0 50.0 100 150

200

1,2-Dibromo-3-Chloropropane DCB Ave 1412 5199 12985 25946 44755

54754

5.00 20.0 50.0 100 150

200

1,2,4-Trichlorobenzene DCB Ave 15835 61405 141991 240412 387497

490028

5.00 20.0 50.0 100 150

200

Hexachlorobutadiene DCB Qua1 10179 39324 83450 134222 205730

+++++

5.00 20.0 50.0 100 150

+++++

Naphthalene DCB Lin2 27448 99668 233455 428628 717029

880550

5.00 20.0 50.0 100 150

200

1,2,3-Trichlorobenzene DCB Qua2 12182 47927 99479 169921 283755

358235

5.00 20.0 50.0 100 150

200

Dibromofluoromethane PFB Ave 46408 110602 229403 359839

450525

20.0 50.0 100 150

200

1,2-Dichloroethane-d4 (Surr) DFB Ave 54848 133405 269262 433613

523883

20.0 50.0 100 150

200

Toluene-d8 (Surr) DFB Ave 177743 413010 870860 1359449

1686334

20.0 50.0 100 150

200

4-Bromofluorobenzene (Surr) CBZ Ave 64705 157084 310979 501486

607718

20.0 50.0 100 150

200

FORM VI 8260B Page 125 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend:

Ave = Average ISTD

Lin1 = Linear 1/conc ISTD

Lin2 = Linear 1/conc^2 ISTD

Qua1 = Quadratic 1/conc ISTD

Qua2 = Quadratic 1/conc^2 ISTD

FORM VI 8260B Page 126 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172614/2 22I1211A.D

Level 2 STD02 500-172614/3 22I1211B.D

Level 3 STD03 500-172614/4 22I1211C.D

Level 4 STD04 500-172614/5 22I1211D.D

Level 5 STD05 500-172614/6 22I1211E.D

Level 6 STD06 500-172614/7 22I1211F.D

Level 7 STD07 500-172614/8 22I1211G.D

Level 8 STD08 500-172614/9 22I1211H.D

Level 9 STD09 500-172614/10 22I1211I.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883 Ave 9.9

0.5798 0.5632 0.5150 0.5364

0.5420 0.0100 15.0

Chloromethane 0.8256 0.7243 0.6267 0.6890 Ave 7.9

0.7182 0.7230 0.6810 0.7012

0.7111 0.1000 15.0

Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130 Ave 8.0

0.6517 0.6618 0.6041 0.6323

0.6381 0.0100 15.0

Bromomethane 0.1659 0.2203 0.1716 0.1726 Ave 13.0

0.2077 0.2258 0.2110 0.2234

0.1998 0.0100 15.0

Chloroethane 0.4113 0.3289 0.3175 0.3315 Ave 10.0

0.3369 0.3333 0.3044 0.3069

0.3338 0.0100 15.0

Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079 Ave 6.3

0.9817 1.0066 0.9437 0.9571

0.9993 0.0100 15.0

Acetone +++++ +++++ 0.0554 0.0635 Ave 7.8

0.0614 0.0672 0.0690 0.0671

0.0639 0.0100 15.0

Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319 Ave 7.9

0.8320 0.8249 0.7635 0.7796

0.8265 0.0100 15.0

Acrolein 0.0331 0.0421 0.0314 0.0388 Ave 13.0

0.0392 0.0429 0.0450 0.0450

0.0397 0.0010 15.0

1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008 Ave 4.7

0.3938 0.3925 0.3935 0.4040

0.4001 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785 Ave 6.7

0.4739 0.4784 0.4696 0.4829

0.4862 0.0100 15.0

Methylene Chloride +++++ 0.4011 0.3629 0.4004 Ave 4.0

0.3719 0.3777 0.3682 0.3859

0.3812 0.0100 15.0

Carbon disulfide 1.5962 1.3713 1.3219 1.4559 Ave 6.5

1.5313 1.5882 1.4767 1.4979

1.4799 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 127 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Acetonitrile 0.0371 0.0333 0.0243 0.0295 Ave 13.0

0.0262 0.0281 0.0299 0.0295

0.0297 0.0010 15.0

Acrylonitrile 0.0750 0.0912 0.0677 0.0823 Ave 9.0

0.0764 0.0821 0.0846 0.0849

0.0805 0.0010 15.0

trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560 Ave 4.4

0.4456 0.4511 0.4430 0.4552

0.4499 0.0100 15.0

2-Butanone (MEK) +++++ +++++ 0.0823 0.0919 Ave 6.1

0.0908 0.0953 0.0973 0.0970

0.0924 0.0100 15.0

Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577 Ave 5.4

0.7230 0.7592 0.7369 0.7564

0.7369 0.0100 15.0

Vinyl acetate +++++ 0.6129 0.5650 0.6423 Ave 5.2

0.6107 0.6494 0.6338 0.6642

0.6255 0.0100 15.0

Tetrahydrofuran +++++ +++++ 0.0538 0.0611 Ave 4.2

0.0583 0.0572 0.0571 0.0595

0.0578 0.0100 15.0

1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189 Ave 6.2

0.8749 0.8925 0.8704 0.9084

0.8857 0.1000 15.0

2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515 Ave 5.5

0.7243 0.7285 0.7200 0.7474

0.7341 0.0100 15.0

cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663 Ave 6.4

0.4508 0.4630 0.4488 0.4652

0.4554 0.0100 15.0

Propionitrile 0.0230 0.0200 0.0163 0.0205 Ave 10.0

0.0191 0.0201 0.0217 0.0219

0.0203 0.0010 15.0

Bromochloromethane 0.2191 0.1652 0.1606 0.1825 Ave 10.0

0.1747 0.1747 0.1737 0.1772

0.1785 0.0100 15.0

Chloroform 0.7988 0.7465 0.6742 0.7604 Ave 4.9

0.7195 0.7370 0.7200 0.7434

0.7375 0.0100 15.0

1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390 Ave 4.7

0.7317 0.7368 0.7320 0.7583

0.7394 0.0100 15.0

Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871 Ave 3.4

0.4883 0.4750 0.4767 0.4948

0.4834 0.0100 15.0

1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649 Ave 6.9

0.6479 0.6478 0.6435 0.6685

0.6488 0.0100 15.0

Benzene 1.2306 1.3508 1.2179 1.1306 1.2550 Ave 4.7

1.2277 1.2183 1.1975 1.2355

1.2293 0.0100 15.0

1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618 Ave 5.6

0.3558 0.3552 0.3521 0.3644

0.3536 0.0100 15.0

4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561 Ave 5.1

0.1535 0.1552 0.1604 0.1580

0.1536 0.0100 15.0

2-Hexanone +++++ +++++ 0.1035 0.1187 Ave 7.3

0.1220 0.1257 0.1256 0.1271

0.1204 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 128 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516 Ave 4.9

0.3434 0.3325 0.3291 0.3406

0.3450 0.0100 15.0

1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264 Ave 6.4

0.3130 0.3110 0.3089 0.3197

0.3152 0.0100 15.0

Dibromomethane 0.1457 0.1306 0.1153 0.1288 Ave 6.9

0.1238 0.1238 0.1224 0.1261

0.1271 0.0100 15.0

Bromodichloromethane 0.3875 0.3507 0.3319 0.3726 Ave 4.6

0.3533 0.3599 0.3552 0.3686

0.3600 0.0100 15.0

2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096 Ave 3.2

0.1015 0.1078 0.1021 0.1054

0.1054 0.0100 15.0

cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222 Ave 4.1

0.4033 0.4109 0.4067 0.4210

0.4091 0.0100 15.0

Toluene 0.9341 0.8388 0.7909 0.7458 0.8161 Ave 6.2

0.8023 0.8060 0.7995 0.8258

0.8177 0.0100 15.0

trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412 Ave 8.6

0.3304 0.3383 0.3448 0.3521

0.3392 0.0100 15.0

1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681 Ave 7.7

0.1638 0.1667 0.1692 0.1728

0.1723 0.0100 15.0

Tetrachloroethene 0.5511 0.4482 0.4255 0.4568 Ave 9.0

0.4446 0.4384 0.4251 0.4400

0.4537 0.0100 15.0

1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542 Ave 4.9

0.3407 0.3413 0.3399 0.3540

0.3491 0.0100 15.0

Dibromochloromethane 0.2702 0.2371 0.2274 0.2693 Ave 6.9

0.2630 0.2690 0.2675 0.2786

0.2603 0.0100 15.0

1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607 Ave 10.0

0.1572 0.1634 0.1626 0.1665

0.1651 0.0100 15.0

Chlorobenzene 1.1305 1.0221 0.9605 1.0363 Ave 5.3

0.9949 0.9884 0.9670 0.9960

1.0120 0.3000 15.0

1-Chlorohexane 0.7176 0.7070 0.6491 0.6984 Ave 3.1

0.6765 0.6760 0.6835 0.6837

0.6865 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448 Ave 5.0

0.3425 0.3461 0.3458 0.3585

0.3400 0.0100 15.0

Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796 Ave 3.4

0.5801 0.5769 0.5619 0.5822

0.5753 0.0100 15.0

m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876 Ave 4.5

1.4534 1.4554 1.3960 1.3942

1.4275 0.0100 15.0

o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780 Ave 5.5

1.4493 1.4706 1.4590 1.5151

1.4564 0.0100 15.0

Styrene 1.1505 1.0719 0.9871 1.1405 Ave 5.6

1.1318 1.1478 1.1460 1.1845

1.1200 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 129 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1602 0.1366 0.1243 0.1553 Ave 10.0

0.1546 0.1600 0.1660 0.1720

0.1536 0.1000 15.0

Isopropylbenzene 3.8233 3.3535 3.0653 3.4816 Ave 7.4

3.1927 3.1639 3.1360 3.2790

3.3119 0.0100 15.0

Bromobenzene 0.8632 0.7552 0.6812 0.7730 Ave 8.2

0.6922 0.7028 0.6972 0.7345

0.7374 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089 Ave 6.0

0.3542 0.3640 0.3676 0.3874

0.3844 0.3000 15.0

1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046 Ave 6.1

0.2704 0.2691 0.2728 0.2923

0.2827 0.0100 15.0

N-Propylbenzene 4.4856 4.0360 3.6439 4.1493 Ave 6.5

3.8858 3.8875 3.7881 3.8936

3.9712 0.0100 15.0

4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065 Ave 7.0

2.1662 2.2029 2.1653 2.2760

2.2416 0.0100 15.0

1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026 Ave 5.8

2.6929 2.7638 2.7107 2.8237

2.7652 0.0100 15.0

2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174 Ave 6.4

2.5627 2.6413 2.6089 2.7193

2.6625 0.0100 15.0

tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552 Ave 7.3

2.4553 2.4418 2.4420 2.5773

2.5582 0.0100 15.0

1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710 Ave 6.3

2.6381 2.7234 2.6840 2.8189

2.7134 0.0100 15.0

sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075 Ave 5.8

3.6796 3.6591 3.6577 3.7738

3.7828 0.0100 15.0

1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907 Ave 8.4

1.4814 1.5187 1.5128 1.5667

1.5748 0.0100 15.0

p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705 Ave 6.4

3.1719 3.2121 3.1807 3.2836

3.2868 0.0100 15.0

1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651 Ave 6.9

1.4798 1.5043 1.4758 1.5340

1.5559 0.0100 15.0

1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033 Ave 6.4

1.2786 1.2876 1.2674 1.3183

1.3233 0.0100 15.0

n-Butylbenzene 3.1126 2.8700 2.6461 2.9480 Ave 4.7

2.8772 2.9149 2.9548 3.0267

2.9188 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678 Ave 12.0

0.0613 0.0622 0.0635 0.0659

0.0661 0.0100 15.0

1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999 Ave 5.3

0.8675 0.9149 0.9059 0.9063

0.8970 0.0100 15.0

Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351 Ave 9.3

0.7318 0.6946 0.7407 0.7100

0.7568 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 130 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.0319 0.9651 0.8910 1.0003 Ave 5.7

0.9350 0.9776 1.0179 1.0659

0.9856 0.0100 15.0

1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392 Ave 5.4

0.6972 0.7092 0.7197 0.7238

0.7171 0.0100 15.0

Dibromofluoromethane 0.4088 Ave 3.6

0.3747 0.4105 0.3974 0.4034

0.3990 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2898 Ave 2.8

0.2681 0.2786 0.2783 0.2818

0.2793 0.0100 15.0

Toluene-d8 (Surr) 1.2317 Ave 3.0

1.1353 1.2008 1.1689 1.1817

1.1837 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5022 Ave 2.5

0.4792 0.5117 0.5010 0.5085

0.5005 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 131 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172614/2 22I1211A.D

Level 2 STD02 500-172614/3 22I1211B.D

Level 3 STD03 500-172614/4 22I1211C.D

Level 4 STD04 500-172614/5 22I1211D.D

Level 5 STD05 500-172614/6 22I1211E.D

Level 6 STD06 500-172614/7 22I1211F.D

Level 7 STD07 500-172614/8 22I1211G.D

Level 8 STD08 500-172614/9 22I1211H.D

Level 9 STD09 500-172614/10 22I1211I.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 8283 14019 34084 128973

408706 762307 1110898 1572519

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 10611 19121 44725 181982

506217 978702 1468998 2055922

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 2072 9537 16111 40052 161885

459341 895799 1302949 1853836

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Ave 2132 5817 12250 45578

146376 305638 455210 654905

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 5286 8684 22657 87550

237436 451232 656528 899737

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 14493 27342 66676 266205

691989 1362610 2035639 2806119

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Ave +++++ +++++ 3957 16764

43292 90934 148822 196769

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 12483 22039 55227 219705

586466 1116585 1646914 2285626

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 16997 44508 89671 410157

1104663 2325112 3885554 5276134

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 5414 11300 26186 105858

277562 531364 848798 1184587

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 7210 13042 32193 126370

334028 647515 1013020 1415755

1.00 2.00 5.00 20.0

50.0 100 150 200

Methylene Chloride PFB Ave +++++ 10588 25901 105736

262156 511318 794285 1131397

+++++ 2.00 5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 20516 36202 94343 384523

1079379 2149891 3185269 4391617

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3815 7023 13902 62328

147511 304606 515971 692080

8.00 16.0 40.0 160

400 800 1200 1600

FORM VI 8260B Page 132 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Acrylonitrile PFB Ave 7715 19252 38635 173831

430688 889127 1460725 1990459

8.00 16.0 40.0 160

400 800 1200 1600

trans-1,2-Dichloroethene PFB Ave 6143 12190 29175 120435

314119 610637 955652 1334459

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave +++++ +++++ 5877 24272

64002 128968 209900 284336

+++++ +++++ 5.00 20.0

50.0 100 150 200

Methyl tert-butyl ether PFB Ave 10253 18092 48485 200118

509651 1027632 1589481 2217547

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave +++++ 16181 40320 169641

430488 879019 1367143 1947324

+++++ 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave +++++ +++++ 3843 16127

41123 77379 123251 174315

+++++ +++++ 5.00 20.0

50.0 100 150 200

1,1-Dichloroethane PFB Ave 12660 21793 57801 242674

616675 1208102 1877461 2663163

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 10444 18966 47829 198464

510518 986077 1552961 2191135

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 6562 11093 29875 123154

317732 626799 968176 1363967

1.00 2.00 5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 3274 5826 13049 61580

150541 311165 533857 726579

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 2816 4362 11462 48207

123109 236461 374570 519660

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 10267 19708 48119 200834

507134 997634 1553050 2179601

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 10394 19135 48811 195166

515733 997347 1578989 2223267

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 8845 18161 44839 182447

481514 918644 1463204 2051034

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 9406 15734 42090 175593

456667 876844 1388026 1960009

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 5292 24000 44324 113004 470128

1210657 2356179 3675431 5120985

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 6813 12420 31493 135519

350802 686980 1080708 1510261

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave +++++ +++++ 13833 58466

151375 300182 492445 654734

+++++ +++++ 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave +++++ +++++ 8872 37503

101953 206593 337483 453433

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1541 6794 12213 33134 131705

338598 643029 1009984 1411923

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 6308 11028 28481 122258

308626 601403 948132 1325238

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 133 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane DFB Ave 2589 4753 11529 48251

122106 239384 375807 522887

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 6884 12765 33178 139566

348406 696059 1090230 1527793

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chloroethyl vinyl ether DFB Ave 1869 3984 10192 41067

100134 208398 313500 436785

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 7564 14930 37294 158135

397656 794708 1248175 1745247

1.00 2.00 5.00 20.0

50.0 100 150 200

Toluene DFB Ave 4017 14904 28786 74548 305710

791155 1558816 2453857 3422834

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 7005 11724 29021 127802

325796 654311 1058276 1459268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane DFB Ave 3579 6500 15804 62968

161526 322360 519398 716065

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 8289 14024 36478 144290

371408 720453 1142505 1570157

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 5569 11637 27497 111881

284612 560890 913572 1263367

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 4064 7418 19500 85045

219735 442108 718959 994298

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 3616 5912 14445 60214

154974 316106 499079 690159

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 17003 31983 82345 327328

831189 1624419 2599260 3554021

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 9223 18665 46324 184447

476816 915102 1474279 2004578

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 5151 10625 25733 108914

286131 568808 929412 1279270

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 2120 9059 17971 45661 183060

484613 948132 1510230 2077566

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 10400 45804 87017 223793 939704

2428374 4783893 7504852 9950024

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 5285 23810 43602 110873 466833

1210753 2416819 3921614 5406441

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 17304 33541 84628 360216

945512 1886331 3080454 4226631

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 2410 4275 10660 49043

129169 263003 446109 613724

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 31324 57244 148746 610310

1601454 3109566 5106365 6881199

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 7072 12892 33053 135512

347188 690763 1135272 1541345

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 134 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 3258 7169 18231 71670

177658 357760 598529 812983

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 2270 5288 12868 53399

135614 264488 444171 613409

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 36750 68894 176823 727359

1949080 3820722 6168362 8171167

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 21017 38120 97903 404326

1086544 2165096 3525867 4776401

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 24843 46048 121204 508814

1350744 2716376 4413867 5925708

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 24693 44629 117536 476349

1285442 2595965 4248167 5706737

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 24197 44012 114646 465442

1231564 2399839 3976419 5408653

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 24293 46692 115053 485753

1323232 2676625 4370483 5915680

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 34897 64452 172232 684971

1845685 3596271 5955880 7919600

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 15196 28192 68974 278836

743079 1492625 2463360 3287950

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 30451 57429 145300 590843

1590983 3156888 5179163 6891004

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 14514 28274 70862 274358

742273 1478508 2403110 3219268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 12130 22897 58683 245994

641352 1265519 2063725 2766492

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 25501 48990 128404 516775

1443162 2864857 4811328 6351852

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 517 1453 2909 11888

30736 61117 103368 138335

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 8084 14950 39749 157753

435120 899145 1475044 1901927

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 7491 13587 35512 128859

367053 682660 1206171 1489923

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 8454 16474 43237 175344

469003 960821 1657420 2236810

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 6507 11786 32167 129572

349729 697002 1171916 1518870

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 107966

264099 555702 857139 1182785

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 108560

264333 538799 854290 1167924

20.0

50.0 100 150 200

FORM VI 8260B Page 135 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172614

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10829

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 461399

1119518 2322467 3587473 4898132

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 158632

400320 840950 1346757 1814509

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

FORM VI 8260B Page 136 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172615/2 22I1211A.D

Level 2 STD02 500-172615/3 22I1211B.D

Level 3 STD03 500-172615/4 22I1211C.D

Level 4 STD04 500-172615/5 22I1211D.D

Level 5 STD05 500-172615/6 22I1211E.D

Level 6 STD06 500-172615/7 22I1211F.D

Level 7 STD07 500-172615/8 22I1211G.D

Level 8 STD08 500-172615/9 22I1211H.D

Level 9 STD09 500-172615/10 22I1211I.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6445 0.5310 0.4776 0.4883 Ave 9.9

0.5798 0.5632 0.5150 0.5364

0.5420 0.0100 15.0

Chloromethane 0.8256 0.7243 0.6267 0.6890 Ave 7.9

0.7182 0.7230 0.6810 0.7012

0.7111 0.1000 15.0

Vinyl chloride 0.6665 0.7420 0.6103 0.5612 0.6130 Ave 8.0

0.6517 0.6618 0.6041 0.6323

0.6381 0.0100 15.0

Bromomethane 0.1659 0.2203 0.1716 0.1726 Ave 13.0

0.2077 0.2258 0.2110 0.2234

0.1998 0.0100 15.0

Chloroethane 0.4113 0.3289 0.3175 0.3315 Ave 10.0

0.3369 0.3333 0.3044 0.3069

0.3338 0.0100 15.0

Dichlorofluoromethane 1.1276 1.0357 0.9343 1.0079 Ave 6.3

0.9817 1.0066 0.9437 0.9571

0.9993 0.0100 15.0

Acetone +++++ +++++ 0.0554 0.0635 Ave 7.8

0.0614 0.0672 0.0690 0.0671

0.0639 0.0100 15.0

Trichlorofluoromethane 0.9712 0.8348 0.7738 0.8319 Ave 7.9

0.8320 0.8249 0.7635 0.7796

0.8265 0.0100 15.0

Acrolein 0.0331 0.0421 0.0314 0.0388 Ave 13.0

0.0392 0.0429 0.0450 0.0450

0.0397 0.0010 15.0

1,1-Dichloroethene 0.4212 0.4280 0.3669 0.4008 Ave 4.7

0.3938 0.3925 0.3935 0.4040

0.4001 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5610 0.4940 0.4511 0.4785 Ave 6.7

0.4739 0.4784 0.4696 0.4829

0.4862 0.0100 15.0

Methylene Chloride +++++ 0.4011 0.3629 0.4004 Ave 4.0

0.3719 0.3777 0.3682 0.3859

0.3812 0.0100 15.0

Carbon disulfide 1.5962 1.3713 1.3219 1.4559 Ave 6.5

1.5313 1.5882 1.4767 1.4979

1.4799 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 137 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Acetonitrile 0.0371 0.0333 0.0243 0.0295 Ave 13.0

0.0262 0.0281 0.0299 0.0295

0.0297 0.0010 15.0

Acrylonitrile 0.0750 0.0912 0.0677 0.0823 Ave 9.0

0.0764 0.0821 0.0846 0.0849

0.0805 0.0010 15.0

trans-1,2-Dichloroethene 0.4780 0.4617 0.4088 0.4560 Ave 4.4

0.4456 0.4511 0.4430 0.4552

0.4499 0.0100 15.0

2-Butanone (MEK) +++++ +++++ 0.0823 0.0919 Ave 6.1

0.0908 0.0953 0.0973 0.0970

0.0924 0.0100 15.0

Methyl tert-butyl ether 0.7977 0.6853 0.6794 0.7577 Ave 5.4

0.7230 0.7592 0.7369 0.7564

0.7369 0.0100 15.0

Vinyl acetate +++++ 0.6129 0.5650 0.6423 Ave 5.2

0.6107 0.6494 0.6338 0.6642

0.6255 0.0100 15.0

Tetrahydrofuran +++++ +++++ 0.0538 0.0611 Ave 4.2

0.0583 0.0572 0.0571 0.0595

0.0578 0.0100 15.0

1,1-Dichloroethane 0.9850 0.8255 0.8099 0.9189 Ave 6.2

0.8749 0.8925 0.8704 0.9084

0.8857 0.1000 15.0

2,2-Dichloropropane 0.8126 0.7184 0.6702 0.7515 Ave 5.5

0.7243 0.7285 0.7200 0.7474

0.7341 0.0100 15.0

cis-1,2-Dichloroethene 0.5106 0.4202 0.4186 0.4663 Ave 6.4

0.4508 0.4630 0.4488 0.4652

0.4554 0.0100 15.0

Propionitrile 0.0230 0.0200 0.0163 0.0205 Ave 10.0

0.0191 0.0201 0.0217 0.0219

0.0203 0.0010 15.0

Bromochloromethane 0.2191 0.1652 0.1606 0.1825 Ave 10.0

0.1747 0.1747 0.1737 0.1772

0.1785 0.0100 15.0

Chloroform 0.7988 0.7465 0.6742 0.7604 Ave 4.9

0.7195 0.7370 0.7200 0.7434

0.7375 0.0100 15.0

1,1,1-Trichloroethane 0.8087 0.7248 0.6839 0.7390 Ave 4.7

0.7317 0.7368 0.7320 0.7583

0.7394 0.0100 15.0

Carbon tetrachloride 0.4978 0.4990 0.4486 0.4871 Ave 3.4

0.4883 0.4750 0.4767 0.4948

0.4834 0.0100 15.0

1,1-Dichloropropene 0.7318 0.5960 0.5898 0.6649 Ave 6.9

0.6479 0.6478 0.6435 0.6685

0.6488 0.0100 15.0

Benzene 1.2306 1.3508 1.2179 1.1306 1.2550 Ave 4.7

1.2277 1.2183 1.1975 1.2355

1.2293 0.0100 15.0

1,2-Dichloroethane 0.3835 0.3413 0.3151 0.3618 Ave 5.6

0.3558 0.3552 0.3521 0.3644

0.3536 0.0100 15.0

4-Methyl-2-pentanone (MIBK) +++++ +++++ 0.1384 0.1561 Ave 5.1

0.1535 0.1552 0.1604 0.1580

0.1536 0.0100 15.0

2-Hexanone +++++ +++++ 0.1035 0.1187 Ave 7.3

0.1220 0.1257 0.1256 0.1271

0.1204 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 138 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Trichloroethene 0.3583 0.3824 0.3356 0.3315 0.3516 Ave 4.9

0.3434 0.3325 0.3291 0.3406

0.3450 0.0100 15.0

1,2-Dichloropropane 0.3550 0.3030 0.2849 0.3264 Ave 6.4

0.3130 0.3110 0.3089 0.3197

0.3152 0.0100 15.0

Dibromomethane 0.1457 0.1306 0.1153 0.1288 Ave 6.9

0.1238 0.1238 0.1224 0.1261

0.1271 0.0100 15.0

Bromodichloromethane 0.3875 0.3507 0.3319 0.3726 Ave 4.6

0.3533 0.3599 0.3552 0.3686

0.3600 0.0100 15.0

2-Chloroethyl vinyl ether 0.1052 0.1095 0.1020 0.1096 Ave 3.2

0.1015 0.1078 0.1021 0.1054

0.1054 0.0100 15.0

cis-1,3-Dichloropropene 0.4257 0.4102 0.3731 0.4222 Ave 4.1

0.4033 0.4109 0.4067 0.4210

0.4091 0.0100 15.0

Toluene 0.9341 0.8388 0.7909 0.7458 0.8161 Ave 6.2

0.8023 0.8060 0.7995 0.8258

0.8177 0.0100 15.0

trans-1,3-Dichloropropene 0.3943 0.3221 0.2903 0.3412 Ave 8.6

0.3304 0.3383 0.3448 0.3521

0.3392 0.0100 15.0

1,1,2-Trichloroethane 0.2014 0.1786 0.1581 0.1681 Ave 7.7

0.1638 0.1667 0.1692 0.1728

0.1723 0.0100 15.0

Tetrachloroethene 0.5511 0.4482 0.4255 0.4568 Ave 9.0

0.4446 0.4384 0.4251 0.4400

0.4537 0.0100 15.0

1,3-Dichloropropane 0.3703 0.3719 0.3207 0.3542 Ave 4.9

0.3407 0.3413 0.3399 0.3540

0.3491 0.0100 15.0

Dibromochloromethane 0.2702 0.2371 0.2274 0.2693 Ave 6.9

0.2630 0.2690 0.2675 0.2786

0.2603 0.0100 15.0

1,2-Dibromoethane 0.2035 0.1624 0.1445 0.1607 Ave 10.0

0.1572 0.1634 0.1626 0.1665

0.1651 0.0100 15.0

Chlorobenzene 1.1305 1.0221 0.9605 1.0363 Ave 5.3

0.9949 0.9884 0.9670 0.9960

1.0120 0.3000 15.0

1-Chlorohexane 0.7176 0.7070 0.6491 0.6984 Ave 3.1

0.6765 0.6760 0.6835 0.6837

0.6865 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3425 0.3396 0.3001 0.3448 Ave 5.0

0.3425 0.3461 0.3458 0.3585

0.3400 0.0100 15.0

Ethylbenzene 0.5881 0.6023 0.5743 0.5326 0.5796 Ave 3.4

0.5801 0.5769 0.5619 0.5822

0.5753 0.0100 15.0

m&p-Xylene 1.4425 1.5227 1.3904 1.3052 1.4876 Ave 4.5

1.4534 1.4554 1.3960 1.3942

1.4275 0.0100 15.0

o-Xylene 1.4661 1.5830 1.3934 1.2932 1.4780 Ave 5.5

1.4493 1.4706 1.4590 1.5151

1.4564 0.0100 15.0

Styrene 1.1505 1.0719 0.9871 1.1405 Ave 5.6

1.1318 1.1478 1.1460 1.1845

1.1200 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 139 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1602 0.1366 0.1243 0.1553 Ave 10.0

0.1546 0.1600 0.1660 0.1720

0.1536 0.1000 15.0

Isopropylbenzene 3.8233 3.3535 3.0653 3.4816 Ave 7.4

3.1927 3.1639 3.1360 3.2790

3.3119 0.0100 15.0

Bromobenzene 0.8632 0.7552 0.6812 0.7730 Ave 8.2

0.6922 0.7028 0.6972 0.7345

0.7374 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.3977 0.4200 0.3757 0.4089 Ave 6.0

0.3542 0.3640 0.3676 0.3874

0.3844 0.3000 15.0

1,2,3-Trichloropropane 0.2771 0.3098 0.2652 0.3046 Ave 6.1

0.2704 0.2691 0.2728 0.2923

0.2827 0.0100 15.0

N-Propylbenzene 4.4856 4.0360 3.6439 4.1493 Ave 6.5

3.8858 3.8875 3.7881 3.8936

3.9712 0.0100 15.0

4-Chlorotoluene 2.5653 2.2332 2.0176 2.3065 Ave 7.0

2.1662 2.2029 2.1653 2.2760

2.2416 0.0100 15.0

1,3,5-Trimethylbenzene 3.0323 2.6976 2.4978 2.9026 Ave 5.8

2.6929 2.7638 2.7107 2.8237

2.7652 0.0100 15.0

2-Chlorotoluene 3.0140 2.6145 2.4222 2.7174 Ave 6.4

2.5627 2.6413 2.6089 2.7193

2.6625 0.0100 15.0

tert-Butylbenzene 2.9534 2.5783 2.3626 2.6552 Ave 7.3

2.4553 2.4418 2.4420 2.5773

2.5582 0.0100 15.0

1,2,4-Trimethylbenzene 2.9651 2.7353 2.3710 2.7710 Ave 6.3

2.6381 2.7234 2.6840 2.8189

2.7134 0.0100 15.0

sec-Butylbenzene 4.2594 3.7758 3.5493 3.9075 Ave 5.8

3.6796 3.6591 3.6577 3.7738

3.7828 0.0100 15.0

1,3-Dichlorobenzene 1.8548 1.6516 1.4214 1.5907 Ave 8.4

1.4814 1.5187 1.5128 1.5667

1.5748 0.0100 15.0

p-Isopropyltoluene 3.7168 3.3643 2.9943 3.3705 Ave 6.4

3.1719 3.2121 3.1807 3.2836

3.2868 0.0100 15.0

1,4-Dichlorobenzene 1.7715 1.6564 1.4603 1.5651 Ave 6.9

1.4798 1.5043 1.4758 1.5340

1.5559 0.0100 15.0

1,2-Dichlorobenzene 1.4806 1.3414 1.2093 1.4033 Ave 6.4

1.2786 1.2876 1.2674 1.3183

1.3233 0.0100 15.0

n-Butylbenzene 3.1126 2.8700 2.6461 2.9480 Ave 4.7

2.8772 2.9149 2.9548 3.0267

2.9188 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0631 0.0851 0.0599 0.0678 Ave 12.0

0.0613 0.0622 0.0635 0.0659

0.0661 0.0100 15.0

1,2,4-Trichlorobenzene 0.9867 0.8758 0.8191 0.8999 Ave 5.3

0.8675 0.9149 0.9059 0.9063

0.8970 0.0100 15.0

Hexachlorobutadiene 0.9143 0.7960 0.7318 0.7351 Ave 9.3

0.7318 0.6946 0.7407 0.7100

0.7568 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 140 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.0319 0.9651 0.8910 1.0003 Ave 5.7

0.9350 0.9776 1.0179 1.0659

0.9856 0.0100 15.0

1,2,3-Trichlorobenzene 0.7942 0.6905 0.6629 0.7392 Ave 5.4

0.6972 0.7092 0.7197 0.7238

0.7171 0.0100 15.0

Dibromofluoromethane 0.4088 Ave 3.6

0.3747 0.4105 0.3974 0.4034

0.3990 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2898 Ave 2.8

0.2681 0.2786 0.2783 0.2818

0.2793 0.0100 15.0

Toluene-d8 (Surr) 1.2317 Ave 3.0

1.1353 1.2008 1.1689 1.1817

1.1837 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5022 Ave 2.5

0.4792 0.5117 0.5010 0.5085

0.5005 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 141 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD01 500-172615/2 22I1211A.D

Level 2 STD02 500-172615/3 22I1211B.D

Level 3 STD03 500-172615/4 22I1211C.D

Level 4 STD04 500-172615/5 22I1211D.D

Level 5 STD05 500-172615/6 22I1211E.D

Level 6 STD06 500-172615/7 22I1211F.D

Level 7 STD07 500-172615/8 22I1211G.D

Level 8 STD08 500-172615/9 22I1211H.D

Level 9 STD09 500-172615/10 22I1211I.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 8283 14019 34084 128973

408706 762307 1110898 1572519

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 10611 19121 44725 181982

506217 978702 1468998 2055922

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 2072 9537 16111 40052 161885

459341 895799 1302949 1853836

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Ave 2132 5817 12250 45578

146376 305638 455210 654905

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 5286 8684 22657 87550

237436 451232 656528 899737

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 14493 27342 66676 266205

691989 1362610 2035639 2806119

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Ave +++++ +++++ 3957 16764

43292 90934 148822 196769

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 12483 22039 55227 219705

586466 1116585 1646914 2285626

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 16997 44508 89671 410157

1104663 2325112 3885554 5276134

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 5414 11300 26186 105858

277562 531364 848798 1184587

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 7210 13042 32193 126370

334028 647515 1013020 1415755

1.00 2.00 5.00 20.0

50.0 100 150 200

Methylene Chloride PFB Ave +++++ 10588 25901 105736

262156 511318 794285 1131397

+++++ 2.00 5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 20516 36202 94343 384523

1079379 2149891 3185269 4391617

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3815 7023 13902 62328

147511 304606 515971 692080

8.00 16.0 40.0 160

400 800 1200 1600

FORM VI 8260B Page 142 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Acrylonitrile PFB Ave 7715 19252 38635 173831

430688 889127 1460725 1990459

8.00 16.0 40.0 160

400 800 1200 1600

trans-1,2-Dichloroethene PFB Ave 6143 12190 29175 120435

314119 610637 955652 1334459

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave +++++ +++++ 5877 24272

64002 128968 209900 284336

+++++ +++++ 5.00 20.0

50.0 100 150 200

Methyl tert-butyl ether PFB Ave 10253 18092 48485 200118

509651 1027632 1589481 2217547

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave +++++ 16181 40320 169641

430488 879019 1367143 1947324

+++++ 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave +++++ +++++ 3843 16127

41123 77379 123251 174315

+++++ +++++ 5.00 20.0

50.0 100 150 200

1,1-Dichloroethane PFB Ave 12660 21793 57801 242674

616675 1208102 1877461 2663163

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 10444 18966 47829 198464

510518 986077 1552961 2191135

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 6562 11093 29875 123154

317732 626799 968176 1363967

1.00 2.00 5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 3274 5826 13049 61580

150541 311165 533857 726579

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 2816 4362 11462 48207

123109 236461 374570 519660

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 10267 19708 48119 200834

507134 997634 1553050 2179601

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 10394 19135 48811 195166

515733 997347 1578989 2223267

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 8845 18161 44839 182447

481514 918644 1463204 2051034

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 9406 15734 42090 175593

456667 876844 1388026 1960009

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 5292 24000 44324 113004 470128

1210657 2356179 3675431 5120985

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 6813 12420 31493 135519

350802 686980 1080708 1510261

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave +++++ +++++ 13833 58466

151375 300182 492445 654734

+++++ +++++ 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave +++++ +++++ 8872 37503

101953 206593 337483 453433

+++++ +++++ 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1541 6794 12213 33134 131705

338598 643029 1009984 1411923

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 6308 11028 28481 122258

308626 601403 948132 1325238

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 143 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane DFB Ave 2589 4753 11529 48251

122106 239384 375807 522887

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 6884 12765 33178 139566

348406 696059 1090230 1527793

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chloroethyl vinyl ether DFB Ave 1869 3984 10192 41067

100134 208398 313500 436785

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 7564 14930 37294 158135

397656 794708 1248175 1745247

1.00 2.00 5.00 20.0

50.0 100 150 200

Toluene DFB Ave 4017 14904 28786 74548 305710

791155 1558816 2453857 3422834

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 7005 11724 29021 127802

325796 654311 1058276 1459268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane DFB Ave 3579 6500 15804 62968

161526 322360 519398 716065

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 8289 14024 36478 144290

371408 720453 1142505 1570157

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 5569 11637 27497 111881

284612 560890 913572 1263367

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 4064 7418 19500 85045

219735 442108 718959 994298

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 3616 5912 14445 60214

154974 316106 499079 690159

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 17003 31983 82345 327328

831189 1624419 2599260 3554021

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 9223 18665 46324 184447

476816 915102 1474279 2004578

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 5151 10625 25733 108914

286131 568808 929412 1279270

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 2120 9059 17971 45661 183060

484613 948132 1510230 2077566

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 10400 45804 87017 223793 939704

2428374 4783893 7504852 9950024

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 5285 23810 43602 110873 466833

1210753 2416819 3921614 5406441

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 17304 33541 84628 360216

945512 1886331 3080454 4226631

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 2410 4275 10660 49043

129169 263003 446109 613724

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 31324 57244 148746 610310

1601454 3109566 5106365 6881199

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 7072 12892 33053 135512

347188 690763 1135272 1541345

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 144 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 3258 7169 18231 71670

177658 357760 598529 812983

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 2270 5288 12868 53399

135614 264488 444171 613409

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 36750 68894 176823 727359

1949080 3820722 6168362 8171167

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 21017 38120 97903 404326

1086544 2165096 3525867 4776401

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 24843 46048 121204 508814

1350744 2716376 4413867 5925708

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 24693 44629 117536 476349

1285442 2595965 4248167 5706737

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 24197 44012 114646 465442

1231564 2399839 3976419 5408653

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 24293 46692 115053 485753

1323232 2676625 4370483 5915680

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 34897 64452 172232 684971

1845685 3596271 5955880 7919600

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 15196 28192 68974 278836

743079 1492625 2463360 3287950

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 30451 57429 145300 590843

1590983 3156888 5179163 6891004

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 14514 28274 70862 274358

742273 1478508 2403110 3219268

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 12130 22897 58683 245994

641352 1265519 2063725 2766492

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 25501 48990 128404 516775

1443162 2864857 4811328 6351852

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 517 1453 2909 11888

30736 61117 103368 138335

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 8084 14950 39749 157753

435120 899145 1475044 1901927

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 7491 13587 35512 128859

367053 682660 1206171 1489923

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 8454 16474 43237 175344

469003 960821 1657420 2236810

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 6507 11786 32167 129572

349729 697002 1171916 1518870

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 107966

264099 555702 857139 1182785

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 108560

264333 538799 854290 1167924

20.0

50.0 100 150 200

FORM VI 8260B Page 145 of 360 12/26/2012
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53034-1

CMS22

Analy Batch No.: 172615

Calibration Start Date: 12/11/2012 14:23 Calibration End Date: 10830

N

12/11/2012 18:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 461399

1119518 2322467 3587473 4898132

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 158632

400320 840950 1346757 1814509

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

FORM VI 8260B Page 146 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

11/19/2012 17:14

11/19/2012 12:14

11/19/2012 14:09

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.4665 0.4279 0.0100 45.9 50.0 -8.3 25.0

Chloromethane Ave 0.5798 0.5246 0.1000 45.2 50.0 -9.5 25.0

Vinyl chloride Ave 0.5072 0.5248 0.0100 51.7 50.0 3.5 25.0

Bromomethane Lin2 0.1523 0.0100 47.2 50.0 -5.7 25.0

Chloroethane Ave 0.2641 0.2426 0.0100 45.9 50.0 -8.2 25.0

Trichlorofluoromethane Ave 0.5875 0.5702 0.0100 48.5 50.0 -2.9 25.0

Acrolein Lin2 0.0673 0.0010 2080 2000 4.0 25.0

1,1-Dichloroethene Ave 0.3748 0.3758 0.0100 50.1 50.0 0.2 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.3898 0.3311 0.0100 42.5 50.0 -15.1 25.0

Acetone Lin1 0.1027 0.0100 46.9 50.0 -6.2 25.0

Carbon disulfide Ave 1.284 1.296 0.0100 50.4 50.0 0.9 25.0

Acetonitrile Ave 0.0330 0.0367 0.0010 446 400 11.4 25.0

Methylene Chloride Ave 0.4276 0.4290 0.0100 50.2 50.0 0.3 25.0

Acrylonitrile Lin2 0.1268 0.0010 407 400 1.7 25.0

trans-1,2-Dichloroethene Ave 0.4413 0.4669 0.0100 52.9 50.0 5.8 25.0

Methyl tert-butyl ether Ave 1.124 1.023 0.0100 45.5 50.0 -9.0 25.0

1,1-Dichloroethane Ave 0.8704 0.8721 0.1000 50.1 50.0 0.2 25.0

Vinyl acetate Ave 0.8347 0.8804 0.0100 52.7 50.0 5.5 25.0

2,2-Dichloropropane Ave 0.4764 0.4986 0.0100 52.3 50.0 4.7 25.0

cis-1,2-Dichloroethene Ave 0.4787 0.4840 0.0100 50.6 50.0 1.1 25.0

2-Butanone (MEK) Ave 0.1710 0.1524 0.0100 44.6 50.0 -10.9 25.0

Propionitrile Ave 0.0316 0.0316 0.0010 399 400 -0.2 25.0

Bromochloromethane Ave 0.1881 0.1702 0.0100 45.2 50.0 -9.5 25.0

Tetrahydrofuran Lin2 0.1042 0.0100 48.0 50.0 -4.0 25.0

Chloroform Ave 0.7669 0.7748 0.0100 50.5 50.0 1.0 25.0

1,1,1-Trichloroethane Ave 0.6244 0.6555 0.0100 52.5 50.0 5.0 25.0

Carbon tetrachloride Ave 0.3568 0.3724 0.0100 52.2 50.0 4.4 25.0

1,1-Dichloropropene Ave 0.6354 0.6306 0.0100 49.6 50.0 -0.8 25.0

Benzene Ave 1.203 1.216 0.0100 50.5 50.0 1.1 25.0

1,2-Dichloroethane Ave 0.3833 0.3697 0.0100 48.2 50.0 -3.5 25.0

Trichloroethene Ave 0.2856 0.2917 0.0100 51.1 50.0 2.1 25.0

1,2-Dichloropropane Ave 0.2993 0.2959 0.0100 49.4 50.0 -1.1 25.0

Dibromomethane Ave 0.1425 0.1397 0.0100 49.0 50.0 -2.0 25.0

Bromodichloromethane Ave 0.3449 0.3379 0.0100 49.0 50.0 -2.0 25.0

2-Chloroethyl vinyl ether Ave 0.1341 0.1258 0.0100 46.9 50.0 -6.2 25.0

cis-1,3-Dichloropropene Ave 0.4015 0.4011 0.0100 53.7 53.8 -0.1 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.2272 0.2120 0.0100 46.7 50.0 -6.7 25.0

Toluene Ave 0.7155 0.7132 0.0100 49.8 50.0 -0.3 25.0

trans-1,3-Dichloropropene Ave 0.3375 0.3348 0.0100 48.2 48.6 -0.8 25.0

1,1,2-Trichloroethane Ave 0.2749 0.2675 0.0100 48.6 50.0 -2.7 25.0

FORM VII 8260B

Page 147 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

11/19/2012 17:14

11/19/2012 12:14

11/19/2012 14:09

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Tetrachloroethene Ave 0.3741 0.3914 0.0100 52.3 50.0 4.6 25.0

1,3-Dichloropropane Ave 0.4540 0.4541 0.0100 50.0 50.0 0.0 25.0

2-Hexanone Ave 0.1954 0.1831 0.0100 46.9 50.0 -6.3 25.0

Dibromochloromethane Ave 0.2462 0.2483 0.0100 50.4 50.0 0.9 25.0

1,2-Dibromoethane Ave 0.1798 0.1719 0.0100 47.8 50.0 -4.4 25.0

1-Chlorohexane Ave 0.5697 0.5208 0.0100 45.7 50.0 -8.6 25.0

Chlorobenzene Ave 0.9049 0.8647 0.3000 47.8 50.0 -4.4 25.0

1,1,1,2-Tetrachloroethane Ave 0.3090 0.3084 0.0100 49.9 50.0 -0.2 25.0

Ethylbenzene Ave 0.5284 0.5301 0.0100 50.2 50.0 0.3 25.0

m&p-Xylene Ave 1.285 1.283 0.0100 99.8 100 -0.2 25.0

o-Xylene Ave 1.348 1.295 0.0100 48.0 50.0 -4.0 25.0

Styrene Ave 1.015 1.029 0.0100 50.7 50.0 1.4 25.0

Bromoform Ave 0.1432 0.1401 0.1000 48.9 50.0 -2.2 25.0

Isopropylbenzene Ave 3.252 3.211 0.0100 49.4 50.0 -1.3 25.0

Bromobenzene Ave 0.7222 0.7556 0.0100 52.3 50.0 4.6 25.0

1,1,2,2-Tetrachloroethane Ave 0.5589 0.5584 0.3000 50.0 50.0 -0.1 25.0

1,2,3-Trichloropropane Ave 0.1732 0.1680 0.0100 48.5 50.0 -3.0 25.0

N-Propylbenzene Ave 3.879 3.806 0.0100 49.1 50.0 -1.9 25.0

2-Chlorotoluene Ave 2.312 2.300 0.0100 49.7 50.0 -0.6 25.0

1,3,5-Trimethylbenzene Ave 2.676 2.896 0.0100 54.1 50.0 8.2 25.0

4-Chlorotoluene Ave 2.685 2.597 0.0100 48.4 50.0 -3.3 25.0

tert-Butylbenzene Ave 2.285 2.273 0.0100 49.7 50.0 -0.5 25.0

1,2,4-Trimethylbenzene Ave 2.723 2.842 0.0100 52.2 50.0 4.4 25.0

sec-Butylbenzene Ave 3.457 3.410 0.0100 49.3 50.0 -1.4 25.0

1,3-Dichlorobenzene Ave 1.415 1.361 0.0100 48.1 50.0 -3.8 25.0

p-Isopropyltoluene Ave 2.902 2.828 0.0100 48.7 50.0 -2.5 25.0

1,4-Dichlorobenzene Ave 1.398 1.440 0.0100 51.5 50.0 3.0 25.0

n-Butylbenzene Ave 2.831 2.940 0.0100 51.9 50.0 3.8 25.0

1,2-Dichlorobenzene Ave 1.252 1.205 0.0100 48.1 50.0 -3.8 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0839 0.0784 0.0100 46.7 50.0 -6.6 25.0

1,2,4-Trichlorobenzene Ave 0.8500 0.8024 0.0100 47.2 50.0 -5.6 25.0

Hexachlorobutadiene Qua1 0.5223 0.0100 51.7 50.0 3.4 25.0

Naphthalene Lin2 1.356 0.0100 47.5 50.0 -4.9 25.0

1,2,3-Trichlorobenzene Qua2 0.5963 0.0100 45.8 50.0 -8.3 25.0

Dibromofluoromethane Ave 0.3958 0.3997 0.0100 43.7 43.3 1.0 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3112 0.0100 42.1 43.3 -2.6 25.0

Toluene-d8 (Surr) Ave 1.017 1.099 0.0100 46.8 43.3 8.1 25.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.5002 0.0100 44.6 43.3 3.0 25.0

FORM VII 8260B

Page 148 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

11/19/2012 17:14

11/19/2012 14:32

11/19/2012 16:28

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.4262 0.3493 0.0100 41.0 50.0 -18.0 25.0

Iodomethane Ave 0.5737 0.6405 0.0100 55.8 50.0 11.6 25.0

Methyl acetate Ave 0.3675 0.2295 0.0100 31.2 50.0 -37.6* 25.0

Hexane Ave 0.7834 0.6708 0.0100 42.8 50.0 -14.4 25.0

Cyclohexane Lin2 0.8544 0.0100 46.7 50.0 -6.6 25.0

Heptane Ave 0.5932 0.5269 0.0100 44.4 50.0 -11.2 25.0

Methylcyclohexane Ave 0.5531 0.5154 0.0100 46.6 50.0 -6.8 25.0

1,3,5-Trichlorobenzene Ave 1.012 1.063 0.0100 52.5 50.0 5.0 25.0

FORM VII 8260B

Page 149 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

12/12/2012 07:39

11/19/2012 12:14

11/19/2012 14:09

CCVIS 500-172698/2

DB624

TestAmerica Chicago

Lab File ID: 16C1212.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.4665 0.5240 0.0100 56.2 50.0 12.3 50.0

Chloromethane Ave 0.5798 0.5912 0.1000 51.0 50.0 2.0 50.0

Vinyl chloride Ave 0.5072 0.5504 0.0100 54.3 50.0 8.5 20.0

Bromomethane Lin2 0.1557 0.0100 48.3 50.0 -3.5 50.0

Chloroethane Ave 0.2641 0.2656 0.0100 50.3 50.0 0.6 50.0

Trichlorofluoromethane Ave 0.5875 0.6401 0.0100 54.5 50.0 9.0 50.0

Acrolein Lin2 0.0595 0.0010 1830 2000 -8.5 50.0

1,1-Dichloroethene Ave 0.3748 0.3552 0.0100 47.4 50.0 -5.2 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.3898 0.3641 0.0100 46.7 50.0 -6.6 50.0

Acetone Lin1 0.0960 0.0100 43.5 50.0 -13.1 50.0

Carbon disulfide Ave 1.284 1.036 0.0100 40.3 50.0 -19.3 50.0

Acetonitrile Ave 0.0330 0.0337 0.0010 409 400 2.2 50.0

Methylene Chloride Ave 0.4276 0.4061 0.0100 47.5 50.0 -5.0 50.0

Acrylonitrile Lin2 0.1231 0.0010 394 400 -1.4 50.0

trans-1,2-Dichloroethene Ave 0.4413 0.4250 0.0100 48.2 50.0 -3.7 50.0

Methyl tert-butyl ether Ave 1.124 1.041 0.0100 46.3 50.0 -7.3 50.0

1,1-Dichloroethane Ave 0.8704 0.8295 0.1000 47.7 50.0 -4.7 50.0

Vinyl acetate Ave 0.8347 0.8161 0.0100 48.9 50.0 -2.2 50.0

2,2-Dichloropropane Ave 0.4764 0.4681 0.0100 49.1 50.0 -1.7 50.0

cis-1,2-Dichloroethene Ave 0.4787 0.4729 0.0100 49.4 50.0 -1.2 50.0

2-Butanone (MEK) Ave 0.1710 0.1470 0.0100 43.0 50.0 -14.1 50.0

Propionitrile Ave 0.0316 0.0321 0.0010 405 400 1.3 50.0

Bromochloromethane Ave 0.1881 0.1768 0.0100 47.0 50.0 -6.0 50.0

Tetrahydrofuran Lin2 0.1068 0.0100 49.2 50.0 -1.5 50.0

Chloroform Ave 0.7669 0.7555 0.0100 49.3 50.0 -1.5 20.0

1,1,1-Trichloroethane Ave 0.6244 0.6250 0.0100 50.1 50.0 0.0 50.0

Carbon tetrachloride Ave 0.3568 0.3676 0.0100 51.5 50.0 3.0 50.0

1,1-Dichloropropene Ave 0.6354 0.6157 0.0100 48.4 50.0 -3.1 50.0

Benzene Ave 1.203 1.197 0.0100 49.7 50.0 -0.6 50.0

1,2-Dichloroethane Ave 0.3833 0.3875 0.0100 50.6 50.0 1.1 50.0

Trichloroethene Ave 0.2856 0.2925 0.0100 51.2 50.0 2.4 50.0

1,2-Dichloropropane Ave 0.2993 0.2952 0.0100 49.3 50.0 -1.3 20.0

Dibromomethane Ave 0.1425 0.1446 0.0100 50.7 50.0 1.5 50.0

Bromodichloromethane Ave 0.3449 0.3563 0.0100 51.7 50.0 3.3 50.0

2-Chloroethyl vinyl ether Ave 0.1341 0.1322 0.0100 49.3 50.0 -1.4 50.0

cis-1,3-Dichloropropene Ave 0.4015 0.4068 0.0100 50.7 50.0 1.3 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.2272 0.2147 0.0100 47.3 50.0 -5.5 50.0

Toluene Ave 0.7155 0.7231 0.0100 50.5 50.0 1.1 20.0

trans-1,3-Dichloropropene Ave 0.3375 0.3521 0.0100 52.2 50.0 4.3 50.0

1,1,2-Trichloroethane Ave 0.2749 0.2808 0.0100 51.1 50.0 2.1 50.0

FORM VII 8260B

Page 150 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

12/12/2012 07:39

11/19/2012 12:14

11/19/2012 14:09

CCVIS 500-172698/2

DB624

TestAmerica Chicago

Lab File ID: 16C1212.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Tetrachloroethene Ave 0.3741 0.3751 0.0100 50.1 50.0 0.3 50.0

1,3-Dichloropropane Ave 0.4540 0.4624 0.0100 50.9 50.0 1.8 50.0

2-Hexanone Ave 0.1954 0.1781 0.0100 45.6 50.0 -8.9 50.0

Dibromochloromethane Ave 0.2462 0.2443 0.0100 49.6 50.0 -0.8 50.0

1,2-Dibromoethane Ave 0.1798 0.1856 0.0100 51.6 50.0 3.2 50.0

1-Chlorohexane Ave 0.5697 0.5742 0.0100 50.4 50.0 0.8 50.0

Chlorobenzene Ave 0.9049 0.9218 0.3000 50.9 50.0 1.9 50.0

1,1,1,2-Tetrachloroethane Ave 0.3090 0.3095 0.0100 50.1 50.0 0.2 50.0

Ethylbenzene Ave 0.5284 0.5391 0.0100 51.0 50.0 2.0 20.0

m&p-Xylene Ave 1.285 1.332 0.0100 104 100 3.6 50.0

o-Xylene Ave 1.348 1.374 0.0100 51.0 50.0 1.9 50.0

Styrene Ave 1.015 1.045 0.0100 51.5 50.0 3.0 50.0

Bromoform Ave 0.1432 0.1451 0.1000 50.7 50.0 1.3 50.0

Isopropylbenzene Ave 3.252 3.481 0.0100 53.5 50.0 7.0 50.0

Bromobenzene Ave 0.7222 0.7638 0.0100 52.9 50.0 5.8 50.0

1,1,2,2-Tetrachloroethane Ave 0.5589 0.5606 0.3000 50.2 50.0 0.3 50.0

1,2,3-Trichloropropane Ave 0.1732 0.1785 0.0100 51.5 50.0 3.1 50.0

N-Propylbenzene Ave 3.879 4.153 0.0100 53.5 50.0 7.1 50.0

2-Chlorotoluene Ave 2.312 2.417 0.0100 52.3 50.0 4.5 50.0

1,3,5-Trimethylbenzene Ave 2.676 2.826 0.0100 52.8 50.0 5.6 50.0

4-Chlorotoluene Ave 2.685 2.850 0.0100 53.1 50.0 6.1 50.0

tert-Butylbenzene Ave 2.285 2.344 0.0100 51.3 50.0 2.6 50.0

1,2,4-Trimethylbenzene Ave 2.723 2.801 0.0100 51.4 50.0 2.9 50.0

sec-Butylbenzene Ave 3.457 3.555 0.0100 51.4 50.0 2.8 50.0

1,3-Dichlorobenzene Ave 1.415 1.466 0.0100 51.8 50.0 3.7 50.0

p-Isopropyltoluene Ave 2.902 2.988 0.0100 51.5 50.0 3.0 50.0

1,4-Dichlorobenzene Ave 1.398 1.470 0.0100 52.6 50.0 5.2 50.0

n-Butylbenzene Ave 2.831 2.902 0.0100 51.2 50.0 2.5 50.0

1,2-Dichlorobenzene Ave 1.252 1.254 0.0100 50.1 50.0 0.1 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0839 0.0754 0.0100 44.9 50.0 -10.2 50.0

1,2,4-Trichlorobenzene Ave 0.8500 0.7623 0.0100 44.8 50.0 -10.3 50.0

Hexachlorobutadiene Qua1 0.4816 0.0100 47.2 50.0 -5.7 50.0

Naphthalene Lin2 1.221 0.0100 42.7 50.0 -14.6 50.0

1,2,3-Trichlorobenzene Qua2 0.5334 0.0100 40.7 50.0 -18.7 50.0

Dibromofluoromethane Ave 0.3958 0.4128 0.0100 45.1 43.3 4.3 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3282 0.0100 44.4 43.3 2.7 50.0

Toluene-d8 (Surr) Ave 1.017 1.130 0.0100 48.1 43.3 11.1 50.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.5126 0.0100 45.7 43.3 5.6 50.0

FORM VII 8260B

Page 151 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

12/12/2012 08:03

11/19/2012 12:14

11/19/2012 14:09

CCV 500-172698/3

DB624

TestAmerica Chicago

Lab File ID: 16D1212.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3958 0.4162 0.0100 45.5 43.3 5.1 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3326 0.0100 45.0 43.3 4.1 50.0

Toluene-d8 (Surr) Ave 1.017 1.142 0.0100 48.6 43.3 12.2 50.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.5278 0.0100 47.0 43.3 8.7 50.0

FORM VII 8260B

Page 152 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS16

12/12/2012 08:03

11/19/2012 14:32

11/19/2012 16:28

CCV 500-172698/3

DB624

TestAmerica Chicago

Lab File ID: 16D1212.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 0.5997 0.4891 0.0100 40.8 50.0 -18.5 50.0

Ethyl ether Ave 0.4262 0.4021 0.0100 47.2 50.0 -5.7 50.0

Iodomethane Ave 0.5737 0.5300 0.0100 92.4 100 -7.6 50.0

3-Chloropropene Ave 0.2319 0.2215 0.0100 95.5 100 -4.5 50.0

Methyl acetate Ave 0.3675 0.3796 0.0100 51.6 50.0 3.3 50.0

Hexane Ave 0.7834 0.7513 0.0100 48.0 50.0 -4.1 50.0

Isopropyl ether Ave 1.776 1.768 0.0100 49.8 50.0 -0.4 50.0

2-Chloro-1,3-butadiene Ave 0.8947 0.8887 0.0100 49.7 50.0 -0.7 50.0

Ethyl acetate Ave 0.3031 0.3050 0.0100 503 500 0.6 50.0

Methacrylonitrile Ave 0.2264 0.2225 0.0100 98.2 100 -1.8 50.0

Cyclohexane Lin2 0.9026 0.0100 49.4 50.0 -1.2 50.0

Isobutyl alcohol Ave 0.0107 0.0105 0.0010 3935 4000 -1.6 50.0

2,2,4-Trimethylpentane Ave 1.405 1.422 0.0100 50.6 50.0 1.2 50.0

Heptane Ave 0.5932 0.6180 0.0100 52.1 50.0 4.2 50.0

n-Butyl alcohol Ave 0.0063 0.0062 0.0010 3954 4000 -1.1 50.0

Methylcyclohexane Ave 0.5531 0.5583 0.0100 50.5 50.0 0.9 50.0

Methyl methacrylate Ave 0.2123 0.2181 0.0100 103 100 2.7 50.0

2-Nitropropane Ave 0.0771 0.0829 0.0100 4304 4000 7.6 50.0

Ethyl methacrylate Ave 0.3579 0.3758 0.0100 105 100 5.0 50.0

Cyclohexanone Lin1 0.0572 0.0100 4683 4000 17.1 50.0

trans-1,4-Dichloro-2-butene Ave 0.0868 0.0843 0.0100 97.1 100 -2.9 50.0

Pentachloroethane Ave 0.2111 0.2140 0.0100 101 100 1.4 50.0

1,3,5-Trichlorobenzene Ave 1.012 1.074 0.0100 53.0 50.0 6.1 50.0

2-Methylnaphthalene Qua2 0.4677 0.0100 34.9 50.0 -30.1 50.0

FORM VII 8260B

Page 153 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172614/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.4239 0.0100 39.1 50.0 -21.8 25.0

Chloromethane Ave 0.7111 0.5561 0.1000 39.1 50.0 -21.8 25.0

Vinyl chloride Ave 0.6381 0.5920 0.0100 46.4 50.0 -7.2 25.0

Bromomethane Ave 0.1998 0.1541 0.0100 38.6 50.0 -22.9 25.0

Chloroethane Ave 0.3338 0.2911 0.0100 43.6 50.0 -12.8 25.0

Dichlorofluoromethane Ave 0.999 0.8378 0.0100 41.9 50.0 -16.2 25.0

Trichlorofluoromethane Ave 0.8265 0.7409 0.0100 44.8 50.0 -10.4 25.0

Acrolein Ave 0.0397 0.0406 0.0010 2044 2000 2.2 25.0

1,1-Dichloroethene Ave 0.4001 0.3815 0.0100 47.7 50.0 -4.7 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4598 0.0100 47.3 50.0 -5.4 25.0

Acetone Ave 0.0639 0.0621 0.0100 48.5 50.0 -2.9 25.0

Carbon disulfide Ave 1.480 1.369 0.0100 46.3 50.0 -7.5 25.0

Acetonitrile Ave 0.0297 0.0292 0.0010 393 400 -1.7 25.0

Methylene Chloride Ave 0.3812 0.3602 0.0100 47.2 50.0 -5.5 25.0

Acrylonitrile Ave 0.0805 0.0797 0.0010 396 400 -1.0 25.0

trans-1,2-Dichloroethene Ave 0.4499 0.4398 0.0100 48.9 50.0 -2.3 25.0

Methyl tert-butyl ether Ave 0.7369 0.6905 0.0100 46.9 50.0 -6.3 25.0

1,1-Dichloroethane Ave 0.8857 0.8456 0.1000 47.7 50.0 -4.5 25.0

Vinyl acetate Ave 0.6255 0.6214 0.0100 49.7 50.0 -0.6 25.0

2,2-Dichloropropane Ave 0.7341 0.6853 0.0100 46.7 50.0 -6.6 25.0

cis-1,2-Dichloroethene Ave 0.4554 0.4436 0.0100 48.7 50.0 -2.6 25.0

2-Butanone (MEK) Ave 0.0924 0.0837 0.0100 45.3 50.0 -9.4 25.0

Propionitrile Ave 0.0203 0.0211 0.0010 414 400 3.5 25.0

Bromochloromethane Ave 0.1785 0.1638 0.0100 45.9 50.0 -8.2 25.0

Tetrahydrofuran Ave 0.0578 0.0548 0.0100 47.3 50.0 -5.3 25.0

Chloroform Ave 0.7375 0.7135 0.0100 48.4 50.0 -3.3 25.0

1,1,1-Trichloroethane Ave 0.7394 0.7299 0.0100 49.4 50.0 -1.3 25.0

Carbon tetrachloride Ave 0.4834 0.4652 0.0100 48.1 50.0 -3.8 25.0

1,1-Dichloropropene Ave 0.6488 0.6138 0.0100 47.3 50.0 -5.4 25.0

Benzene Ave 1.229 1.148 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichloroethane Ave 0.3536 0.3244 0.0100 45.9 50.0 -8.3 25.0

Trichloroethene Ave 0.3450 0.3212 0.0100 46.6 50.0 -6.9 25.0

1,2-Dichloropropane Ave 0.3152 0.2970 0.0100 47.1 50.0 -5.8 25.0

Dibromomethane Ave 0.1271 0.1149 0.0100 45.2 50.0 -9.6 25.0

Bromodichloromethane Ave 0.3600 0.3216 0.0100 44.7 50.0 -10.7 25.0

2-Chloroethyl vinyl ether Ave 0.1054 0.0957 0.0100 45.4 50.0 -9.2 25.0

cis-1,3-Dichloropropene Ave 0.4091 0.3814 0.0100 50.1 53.8 -6.8 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1404 0.0100 45.7 50.0 -8.6 25.0

Toluene Ave 0.8177 0.7569 0.0100 46.3 50.0 -7.4 25.0

trans-1,3-Dichloropropene Ave 0.3392 0.3107 0.0100 44.5 48.6 -8.4 25.0

FORM VII 8260B

Page 154 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172614/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1573 0.0100 45.6 50.0 -8.7 25.0

Tetrachloroethene Ave 0.4537 0.4260 0.0100 47.0 50.0 -6.1 25.0

1,3-Dichloropropane Ave 0.3491 0.3223 0.0100 46.2 50.0 -7.7 25.0

2-Hexanone Ave 0.1204 0.1135 0.0100 47.1 50.0 -5.7 25.0

Dibromochloromethane Ave 0.2603 0.2454 0.0100 47.1 50.0 -5.7 25.0

1,2-Dibromoethane Ave 0.1651 0.1486 0.0100 45.0 50.0 -10.0 25.0

Chlorobenzene Ave 1.012 0.9004 0.3000 44.5 50.0 -11.0 25.0

1-Chlorohexane Ave 0.6865 0.6546 0.0100 47.7 50.0 -4.6 25.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3297 0.0100 48.5 50.0 -3.0 25.0

Ethylbenzene Ave 0.5753 0.5498 0.0100 47.8 50.0 -4.4 25.0

m&p-Xylene Ave 1.427 1.339 0.0100 93.8 100 -6.2 25.0

o-Xylene Ave 1.456 1.295 0.0100 44.5 50.0 -11.1 25.0

Styrene Ave 1.120 1.076 0.0100 48.0 50.0 -3.9 25.0

Bromoform Ave 0.1536 0.1521 0.1000 49.5 50.0 -1.0 25.0

Isopropylbenzene Ave 3.312 2.951 0.0100 44.6 50.0 -10.9 25.0

Bromobenzene Ave 0.7374 0.6901 0.0100 46.8 50.0 -6.4 25.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3650 0.3000 47.5 50.0 -5.1 25.0

1,2,3-Trichloropropane Ave 0.2827 0.2697 0.0100 47.7 50.0 -4.6 25.0

N-Propylbenzene Ave 3.971 3.489 0.0100 43.9 50.0 -12.2 25.0

4-Chlorotoluene Ave 2.242 2.042 0.0100 45.5 50.0 -8.9 25.0

1,3,5-Trimethylbenzene Ave 2.765 2.737 0.0100 49.5 50.0 -1.0 25.0

2-Chlorotoluene Ave 2.663 2.355 0.0100 44.2 50.0 -11.6 25.0

tert-Butylbenzene Ave 2.558 2.302 0.0100 45.0 50.0 -10.0 25.0

1,2,4-Trimethylbenzene Ave 2.713 2.637 0.0100 48.6 50.0 -2.8 25.0

sec-Butylbenzene Ave 3.783 3.418 0.0100 45.2 50.0 -9.6 25.0

1,3-Dichlorobenzene Ave 1.575 1.369 0.0100 43.5 50.0 -13.1 25.0

p-Isopropyltoluene Ave 3.287 2.935 0.0100 44.7 50.0 -10.7 25.0

1,4-Dichlorobenzene Ave 1.556 1.454 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichlorobenzene Ave 1.323 1.190 0.0100 45.0 50.0 -10.1 25.0

n-Butylbenzene Ave 2.919 2.736 0.0100 46.9 50.0 -6.3 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0567 0.0100 42.9 50.0 -14.2 25.0

1,2,4-Trichlorobenzene Ave 0.8970 0.7803 0.0100 43.5 50.0 -13.0 25.0

Hexachlorobutadiene Ave 0.7568 0.6904 0.0100 45.6 50.0 -8.8 25.0

Naphthalene Ave 0.9856 0.8667 0.0100 44.0 50.0 -12.1 25.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6586 0.0100 45.9 50.0 -8.2 25.0

Dibromofluoromethane Ave 0.3990 0.3761 0.0100 47.1 50.0 -5.7 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2556 0.0100 45.8 50.0 -8.5 25.0

Toluene-d8 (Surr) Ave 1.184 1.117 0.0100 47.2 50.0 -5.6 25.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4730 0.0100 47.3 50.0 -5.5 25.0

FORM VII 8260B

Page 155 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.4239 0.0100 39.1 50.0 -21.8 25.0

Chloromethane Ave 0.7111 0.5561 0.1000 39.1 50.0 -21.8 25.0

Vinyl chloride Ave 0.6381 0.5920 0.0100 46.4 50.0 -7.2 25.0

Bromomethane Ave 0.1998 0.1541 0.0100 38.6 50.0 -22.9 25.0

Chloroethane Ave 0.3338 0.2911 0.0100 43.6 50.0 -12.8 25.0

Dichlorofluoromethane Ave 0.999 0.8378 0.0100 41.9 50.0 -16.2 25.0

Trichlorofluoromethane Ave 0.8265 0.7409 0.0100 44.8 50.0 -10.4 25.0

Acrolein Ave 0.0397 0.0406 0.0010 2044 2000 2.2 25.0

1,1-Dichloroethene Ave 0.4001 0.3815 0.0100 47.7 50.0 -4.7 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.4598 0.0100 47.3 50.0 -5.4 25.0

Acetone Ave 0.0639 0.0621 0.0100 48.5 50.0 -2.9 25.0

Carbon disulfide Ave 1.480 1.369 0.0100 46.3 50.0 -7.5 25.0

Acetonitrile Ave 0.0297 0.0292 0.0010 393 400 -1.7 25.0

Methylene Chloride Ave 0.3812 0.3602 0.0100 47.2 50.0 -5.5 25.0

Acrylonitrile Ave 0.0805 0.0797 0.0010 396 400 -1.0 25.0

trans-1,2-Dichloroethene Ave 0.4499 0.4398 0.0100 48.9 50.0 -2.3 25.0

Methyl tert-butyl ether Ave 0.7369 0.6905 0.0100 46.9 50.0 -6.3 25.0

1,1-Dichloroethane Ave 0.8857 0.8456 0.1000 47.7 50.0 -4.5 25.0

Vinyl acetate Ave 0.6255 0.6214 0.0100 49.7 50.0 -0.6 25.0

2,2-Dichloropropane Ave 0.7341 0.6853 0.0100 46.7 50.0 -6.6 25.0

cis-1,2-Dichloroethene Ave 0.4554 0.4436 0.0100 48.7 50.0 -2.6 25.0

2-Butanone (MEK) Ave 0.0924 0.0837 0.0100 45.3 50.0 -9.4 25.0

Propionitrile Ave 0.0203 0.0211 0.0010 414 400 3.5 25.0

Bromochloromethane Ave 0.1785 0.1638 0.0100 45.9 50.0 -8.2 25.0

Tetrahydrofuran Ave 0.0578 0.0548 0.0100 47.3 50.0 -5.3 25.0

Chloroform Ave 0.7375 0.7135 0.0100 48.4 50.0 -3.3 25.0

1,1,1-Trichloroethane Ave 0.7394 0.7299 0.0100 49.4 50.0 -1.3 25.0

Carbon tetrachloride Ave 0.4834 0.4652 0.0100 48.1 50.0 -3.8 25.0

1,1-Dichloropropene Ave 0.6488 0.6138 0.0100 47.3 50.0 -5.4 25.0

Benzene Ave 1.229 1.148 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichloroethane Ave 0.3536 0.3244 0.0100 45.9 50.0 -8.3 25.0

Trichloroethene Ave 0.3450 0.3212 0.0100 46.6 50.0 -6.9 25.0

1,2-Dichloropropane Ave 0.3152 0.2970 0.0100 47.1 50.0 -5.8 25.0

Dibromomethane Ave 0.1271 0.1149 0.0100 45.2 50.0 -9.6 25.0

Bromodichloromethane Ave 0.3600 0.3216 0.0100 44.7 50.0 -10.7 25.0

2-Chloroethyl vinyl ether Ave 0.1054 0.0957 0.0100 45.4 50.0 -9.2 25.0

cis-1,3-Dichloropropene Ave 0.4091 0.3814 0.0100 50.1 53.8 -6.8 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1404 0.0100 45.7 50.0 -8.6 25.0

Toluene Ave 0.8177 0.7569 0.0100 46.3 50.0 -7.4 25.0

trans-1,3-Dichloropropene Ave 0.3392 0.3107 0.0100 44.5 48.6 -8.4 25.0

FORM VII 8260B

Page 156 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/12/2012 00:17

12/11/2012 14:23

12/11/2012 18:09

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1573 0.0100 45.6 50.0 -8.7 25.0

Tetrachloroethene Ave 0.4537 0.4260 0.0100 47.0 50.0 -6.1 25.0

1,3-Dichloropropane Ave 0.3491 0.3223 0.0100 46.2 50.0 -7.7 25.0

2-Hexanone Ave 0.1204 0.1135 0.0100 47.1 50.0 -5.7 25.0

Dibromochloromethane Ave 0.2603 0.2454 0.0100 47.1 50.0 -5.7 25.0

1,2-Dibromoethane Ave 0.1651 0.1486 0.0100 45.0 50.0 -10.0 25.0

Chlorobenzene Ave 1.012 0.9004 0.3000 44.5 50.0 -11.0 25.0

1-Chlorohexane Ave 0.6865 0.6546 0.0100 47.7 50.0 -4.6 25.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3297 0.0100 48.5 50.0 -3.0 25.0

Ethylbenzene Ave 0.5753 0.5498 0.0100 47.8 50.0 -4.4 25.0

m&p-Xylene Ave 1.427 1.339 0.0100 93.8 100 -6.2 25.0

o-Xylene Ave 1.456 1.295 0.0100 44.5 50.0 -11.1 25.0

Styrene Ave 1.120 1.076 0.0100 48.0 50.0 -3.9 25.0

Bromoform Ave 0.1536 0.1521 0.1000 49.5 50.0 -1.0 25.0

Isopropylbenzene Ave 3.312 2.951 0.0100 44.6 50.0 -10.9 25.0

Bromobenzene Ave 0.7374 0.6901 0.0100 46.8 50.0 -6.4 25.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3650 0.3000 47.5 50.0 -5.1 25.0

1,2,3-Trichloropropane Ave 0.2827 0.2697 0.0100 47.7 50.0 -4.6 25.0

N-Propylbenzene Ave 3.971 3.489 0.0100 43.9 50.0 -12.2 25.0

4-Chlorotoluene Ave 2.242 2.042 0.0100 45.5 50.0 -8.9 25.0

1,3,5-Trimethylbenzene Ave 2.765 2.737 0.0100 49.5 50.0 -1.0 25.0

2-Chlorotoluene Ave 2.663 2.355 0.0100 44.2 50.0 -11.6 25.0

tert-Butylbenzene Ave 2.558 2.302 0.0100 45.0 50.0 -10.0 25.0

1,2,4-Trimethylbenzene Ave 2.713 2.637 0.0100 48.6 50.0 -2.8 25.0

sec-Butylbenzene Ave 3.783 3.418 0.0100 45.2 50.0 -9.6 25.0

1,3-Dichlorobenzene Ave 1.575 1.369 0.0100 43.5 50.0 -13.1 25.0

p-Isopropyltoluene Ave 3.287 2.935 0.0100 44.7 50.0 -10.7 25.0

1,4-Dichlorobenzene Ave 1.556 1.454 0.0100 46.7 50.0 -6.6 25.0

1,2-Dichlorobenzene Ave 1.323 1.190 0.0100 45.0 50.0 -10.1 25.0

n-Butylbenzene Ave 2.919 2.736 0.0100 46.9 50.0 -6.3 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0567 0.0100 42.9 50.0 -14.2 25.0

1,2,4-Trichlorobenzene Ave 0.8970 0.7803 0.0100 43.5 50.0 -13.0 25.0

Hexachlorobutadiene Ave 0.7568 0.6904 0.0100 45.6 50.0 -8.8 25.0

Naphthalene Ave 0.9856 0.8667 0.0100 44.0 50.0 -12.1 25.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6586 0.0100 45.9 50.0 -8.2 25.0

Dibromofluoromethane Ave 0.3990 0.3761 0.0100 47.1 50.0 -5.7 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2556 0.0100 45.8 50.0 -8.5 25.0

Toluene-d8 (Surr) Ave 1.184 1.117 0.0100 47.2 50.0 -5.6 25.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4730 0.0100 47.3 50.0 -5.5 25.0

FORM VII 8260B

Page 157 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/12/2012 00:17

12/11/2012 19:06

12/11/2012 23:48

ICV 500-172614/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.2603 0.2517 0.0100 48.3 50.0 -3.3 25.0

Iodomethane Lin1 0.6879 0.0100 52.8 50.0 5.6 25.0

Methyl acetate Ave 0.2127 0.1450 0.0100 34.1 50.0 -31.8* 25.0

Hexane Ave 0.8764 0.9019 0.0100 51.5 50.0 2.9 25.0

Cyclohexane Lin1 1.057 0.0100 49.4 50.0 -1.2 25.0

Heptane Ave 0.7351 0.6922 0.0100 47.1 50.0 -5.8 25.0

Methylcyclohexane Ave 0.5969 0.6069 0.0100 50.8 50.0 1.7 25.0

1,3,5-Trichlorobenzene Ave 1.226 1.140 0.0100 46.5 50.0 -7.0 25.0

FORM VII 8260B

Page 158 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/12/2012 00:17

12/11/2012 19:06

12/11/2012 23:48

ICV 500-172615/23

DB624

TestAmerica Chicago

Lab File ID: 22S1211.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.2603 0.2517 0.0100 48.3 50.0 -3.3 25.0

Iodomethane Lin1 0.6879 0.0100 52.8 50.0 5.6 25.0

Methyl acetate Ave 0.2127 0.1450 0.0100 34.1 50.0 -31.8* 25.0

Hexane Ave 0.8764 0.9019 0.0100 51.5 50.0 2.9 25.0

Cyclohexane Lin1 1.057 0.0100 49.4 50.0 -1.2 25.0

Heptane Ave 0.7351 0.6922 0.0100 47.1 50.0 -5.8 25.0

Methylcyclohexane Ave 0.5969 0.6069 0.0100 50.8 50.0 1.7 25.0

1,3,5-Trichlorobenzene Ave 1.226 1.140 0.0100 46.5 50.0 -7.0 25.0

FORM VII 8260B

Page 159 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 11:40

12/11/2012 14:23

12/11/2012 18:09

CCV 500-172879/2

DB624

TestAmerica Chicago

Lab File ID: 22C1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.5338 0.0100 49.2 50.0 -1.5 50.0

Chloromethane Ave 0.7111 0.6697 0.1000 47.1 50.0 -5.8 50.0

Vinyl chloride Ave 0.6381 0.6245 0.0100 48.9 50.0 -2.1 20.0

Bromomethane Ave 0.1998 0.2221 0.0100 55.6 50.0 11.1 50.0

Chloroethane Ave 0.3338 0.3231 0.0100 48.4 50.0 -3.2 50.0

Dichlorofluoromethane Ave 0.999 0.9535 0.0100 47.7 50.0 -4.6 50.0

Trichlorofluoromethane Ave 0.8265 0.8111 0.0100 49.1 50.0 -1.9 50.0

Acrolein Ave 0.0397 0.0382 0.0010 1922 2000 -3.9 50.0

1,1-Dichloroethene Ave 0.4001 0.4128 0.0100 51.6 50.0 3.2 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.5026 0.0100 51.7 50.0 3.4 50.0

Acetone Ave 0.0639 0.0558 0.0100 43.6 50.0 -12.8 50.0

Carbon disulfide Ave 1.480 1.336 0.0100 45.1 50.0 -9.7 50.0

Acetonitrile Ave 0.0297 0.0258 0.0010 347 400 -13.3 50.0

Methylene Chloride Ave 0.3812 0.3828 0.0100 50.2 50.0 0.4 50.0

Acrylonitrile Ave 0.0805 0.0728 0.0010 362 400 -9.5 50.0

trans-1,2-Dichloroethene Ave 0.4499 0.4608 0.0100 51.2 50.0 2.4 50.0

Methyl tert-butyl ether Ave 0.7369 0.7227 0.0100 49.0 50.0 -1.9 50.0

1,1-Dichloroethane Ave 0.8857 0.8841 0.1000 49.9 50.0 -0.2 50.0

Vinyl acetate Ave 0.6255 0.5422 0.0100 43.4 50.0 -13.3 50.0

2,2-Dichloropropane Ave 0.7341 0.7463 0.0100 50.8 50.0 1.7 50.0

cis-1,2-Dichloroethene Ave 0.4554 0.4710 0.0100 51.7 50.0 3.4 50.0

2-Butanone (MEK) Ave 0.0924 0.0799 0.0100 43.2 50.0 -13.5 50.0

Propionitrile Ave 0.0203 0.0181 0.0010 356 400 -10.9 50.0

Bromochloromethane Ave 0.1785 0.1803 0.0100 50.5 50.0 1.0 50.0

Tetrahydrofuran Ave 0.0578 0.0574 0.0100 49.7 50.0 -0.7 50.0

Chloroform Ave 0.7375 0.7437 0.0100 50.4 50.0 0.8 20.0

1,1,1-Trichloroethane Ave 0.7394 0.7493 0.0100 50.7 50.0 1.3 50.0

Carbon tetrachloride Ave 0.4834 0.4939 0.0100 51.1 50.0 2.2 50.0

1,1-Dichloropropene Ave 0.6488 0.6749 0.0100 52.0 50.0 4.0 50.0

Benzene Ave 1.229 1.261 0.0100 51.3 50.0 2.5 50.0

1,2-Dichloroethane Ave 0.3536 0.3610 0.0100 51.1 50.0 2.1 50.0

Trichloroethene Ave 0.3450 0.3570 0.0100 51.8 50.0 3.5 50.0

1,2-Dichloropropane Ave 0.3152 0.3182 0.0100 50.5 50.0 0.9 20.0

Dibromomethane Ave 0.1271 0.1288 0.0100 50.7 50.0 1.3 50.0

Bromodichloromethane Ave 0.3600 0.3677 0.0100 51.1 50.0 2.2 50.0

2-Chloroethyl vinyl ether Ave 0.1054 0.1132 0.0100 53.7 50.0 7.4 50.0

cis-1,3-Dichloropropene Ave 0.4091 0.4233 0.0100 51.7 50.0 3.5 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1405 0.0100 45.7 50.0 -8.6 50.0

Toluene Ave 0.8177 0.8458 0.0100 51.7 50.0 3.4 20.0

trans-1,3-Dichloropropene Ave 0.3392 0.3421 0.0100 50.4 50.0 0.9 50.0

FORM VII 8260B

Page 160 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 11:40

12/11/2012 14:23

12/11/2012 18:09

CCV 500-172879/2

DB624

TestAmerica Chicago

Lab File ID: 22C1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1765 0.0100 51.2 50.0 2.4 50.0

Tetrachloroethene Ave 0.4537 0.4632 0.0100 51.1 50.0 2.1 50.0

1,3-Dichloropropane Ave 0.3491 0.3626 0.0100 51.9 50.0 3.9 50.0

2-Hexanone Ave 0.1204 0.1131 0.0100 47.0 50.0 -6.1 50.0

Dibromochloromethane Ave 0.2603 0.2757 0.0100 53.0 50.0 5.9 50.0

1,2-Dibromoethane Ave 0.1651 0.1701 0.0100 51.5 50.0 3.0 50.0

Chlorobenzene Ave 1.012 1.041 0.3000 51.4 50.0 2.9 50.0

1-Chlorohexane Ave 0.6865 0.7024 0.0100 51.2 50.0 2.3 50.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3544 0.0100 52.1 50.0 4.2 50.0

Ethylbenzene Ave 0.5753 0.6003 0.0100 52.2 50.0 4.3 20.0

m&p-Xylene Ave 1.427 1.512 0.0100 106 100 5.9 50.0

o-Xylene Ave 1.456 1.500 0.0100 51.5 50.0 3.0 50.0

Styrene Ave 1.120 1.177 0.0100 52.5 50.0 5.1 50.0

Bromoform Ave 0.1536 0.1668 0.1000 54.3 50.0 8.6 50.0

Isopropylbenzene Ave 3.312 3.294 0.0100 49.7 50.0 -0.5 50.0

Bromobenzene Ave 0.7374 0.7428 0.0100 50.4 50.0 0.7 50.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3896 0.3000 50.7 50.0 1.4 50.0

1,2,3-Trichloropropane Ave 0.2827 0.2926 0.0100 51.8 50.0 3.5 50.0

N-Propylbenzene Ave 3.971 4.021 0.0100 50.6 50.0 1.3 50.0

4-Chlorotoluene Ave 2.242 2.261 0.0100 50.4 50.0 0.9 50.0

1,3,5-Trimethylbenzene Ave 2.765 2.824 0.0100 51.1 50.0 2.1 50.0

2-Chlorotoluene Ave 2.663 2.687 0.0100 50.5 50.0 0.9 50.0

tert-Butylbenzene Ave 2.558 2.553 0.0100 49.9 50.0 -0.2 50.0

1,2,4-Trimethylbenzene Ave 2.713 2.748 0.0100 50.6 50.0 1.3 50.0

sec-Butylbenzene Ave 3.783 3.833 0.0100 50.7 50.0 1.3 50.0

1,3-Dichlorobenzene Ave 1.575 1.609 0.0100 51.1 50.0 2.2 50.0

p-Isopropyltoluene Ave 3.287 3.338 0.0100 50.8 50.0 1.6 50.0

1,4-Dichlorobenzene Ave 1.556 1.593 0.0100 51.2 50.0 2.4 50.0

1,2-Dichlorobenzene Ave 1.323 1.354 0.0100 51.2 50.0 2.3 50.0

n-Butylbenzene Ave 2.919 3.043 0.0100 52.1 50.0 4.2 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0612 0.0100 46.3 50.0 -7.4 50.0

1,2,4-Trichlorobenzene Ave 0.8970 0.9077 0.0100 50.6 50.0 1.2 50.0

Hexachlorobutadiene Ave 0.7568 0.7747 0.0100 51.2 50.0 2.4 50.0

Naphthalene Ave 0.9856 0.9469 0.0100 48.0 50.0 -3.9 50.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6971 0.0100 48.6 50.0 -2.8 50.0

Dibromofluoromethane Ave 0.3990 0.3878 0.0100 48.6 50.0 -2.8 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2633 0.0100 47.1 50.0 -5.7 50.0

Toluene-d8 (Surr) Ave 1.184 1.185 0.0100 50.1 50.0 0.0 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4903 0.0100 49.0 50.0 -2.1 50.0

FORM VII 8260B

Page 161 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 11:40

12/11/2012 14:23

12/11/2012 18:09

CCV 500-172880/2

DB624

TestAmerica Chicago

Lab File ID: 22C1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.5420 0.5338 0.0100 49.2 50.0 -1.5 50.0

Chloromethane Ave 0.7111 0.6697 0.1000 47.1 50.0 -5.8 50.0

Vinyl chloride Ave 0.6381 0.6245 0.0100 48.9 50.0 -2.1 20.0

Bromomethane Ave 0.1998 0.2221 0.0100 55.6 50.0 11.1 50.0

Chloroethane Ave 0.3338 0.3231 0.0100 48.4 50.0 -3.2 50.0

Dichlorofluoromethane Ave 0.999 0.9535 0.0100 47.7 50.0 -4.6 50.0

Trichlorofluoromethane Ave 0.8265 0.8111 0.0100 49.1 50.0 -1.9 50.0

Acrolein Ave 0.0397 0.0382 0.0010 1922 2000 -3.9 50.0

1,1-Dichloroethene Ave 0.4001 0.4128 0.0100 51.6 50.0 3.2 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.4862 0.5026 0.0100 51.7 50.0 3.4 50.0

Acetone Ave 0.0639 0.0558 0.0100 43.6 50.0 -12.8 50.0

Carbon disulfide Ave 1.480 1.336 0.0100 45.1 50.0 -9.7 50.0

Acetonitrile Ave 0.0297 0.0258 0.0010 347 400 -13.3 50.0

Methylene Chloride Ave 0.3812 0.3828 0.0100 50.2 50.0 0.4 50.0

Acrylonitrile Ave 0.0805 0.0728 0.0010 362 400 -9.5 50.0

trans-1,2-Dichloroethene Ave 0.4499 0.4608 0.0100 51.2 50.0 2.4 50.0

Methyl tert-butyl ether Ave 0.7369 0.7227 0.0100 49.0 50.0 -1.9 50.0

1,1-Dichloroethane Ave 0.8857 0.8841 0.1000 49.9 50.0 -0.2 50.0

Vinyl acetate Ave 0.6255 0.5422 0.0100 43.4 50.0 -13.3 50.0

2,2-Dichloropropane Ave 0.7341 0.7463 0.0100 50.8 50.0 1.7 50.0

cis-1,2-Dichloroethene Ave 0.4554 0.4710 0.0100 51.7 50.0 3.4 50.0

2-Butanone (MEK) Ave 0.0924 0.0799 0.0100 43.2 50.0 -13.5 50.0

Propionitrile Ave 0.0203 0.0181 0.0010 356 400 -10.9 50.0

Bromochloromethane Ave 0.1785 0.1803 0.0100 50.5 50.0 1.0 50.0

Tetrahydrofuran Ave 0.0578 0.0574 0.0100 49.7 50.0 -0.7 50.0

Chloroform Ave 0.7375 0.7437 0.0100 50.4 50.0 0.8 20.0

1,1,1-Trichloroethane Ave 0.7394 0.7493 0.0100 50.7 50.0 1.3 50.0

Carbon tetrachloride Ave 0.4834 0.4939 0.0100 51.1 50.0 2.2 50.0

1,1-Dichloropropene Ave 0.6488 0.6749 0.0100 52.0 50.0 4.0 50.0

Benzene Ave 1.229 1.261 0.0100 51.3 50.0 2.5 50.0

1,2-Dichloroethane Ave 0.3536 0.3610 0.0100 51.1 50.0 2.1 50.0

Trichloroethene Ave 0.3450 0.3570 0.0100 51.8 50.0 3.5 50.0

1,2-Dichloropropane Ave 0.3152 0.3182 0.0100 50.5 50.0 0.9 20.0

Dibromomethane Ave 0.1271 0.1288 0.0100 50.7 50.0 1.3 50.0

Bromodichloromethane Ave 0.3600 0.3677 0.0100 51.1 50.0 2.2 50.0

2-Chloroethyl vinyl ether Ave 0.1054 0.1132 0.0100 53.7 50.0 7.4 50.0

cis-1,3-Dichloropropene Ave 0.4091 0.4233 0.0100 51.7 50.0 3.5 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1536 0.1405 0.0100 45.7 50.0 -8.6 50.0

Toluene Ave 0.8177 0.8458 0.0100 51.7 50.0 3.4 20.0

trans-1,3-Dichloropropene Ave 0.3392 0.3421 0.0100 50.4 50.0 0.9 50.0

FORM VII 8260B

Page 162 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 11:40

12/11/2012 14:23

12/11/2012 18:09

CCV 500-172880/2

DB624

TestAmerica Chicago

Lab File ID: 22C1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.1723 0.1765 0.0100 51.2 50.0 2.4 50.0

Tetrachloroethene Ave 0.4537 0.4632 0.0100 51.1 50.0 2.1 50.0

1,3-Dichloropropane Ave 0.3491 0.3626 0.0100 51.9 50.0 3.9 50.0

2-Hexanone Ave 0.1204 0.1131 0.0100 47.0 50.0 -6.1 50.0

Dibromochloromethane Ave 0.2603 0.2757 0.0100 53.0 50.0 5.9 50.0

1,2-Dibromoethane Ave 0.1651 0.1701 0.0100 51.5 50.0 3.0 50.0

Chlorobenzene Ave 1.012 1.041 0.3000 51.4 50.0 2.9 50.0

1-Chlorohexane Ave 0.6865 0.7024 0.0100 51.2 50.0 2.3 50.0

1,1,1,2-Tetrachloroethane Ave 0.3400 0.3544 0.0100 52.1 50.0 4.2 50.0

Ethylbenzene Ave 0.5753 0.6003 0.0100 52.2 50.0 4.3 20.0

m&p-Xylene Ave 1.427 1.512 0.0100 106 100 5.9 50.0

o-Xylene Ave 1.456 1.500 0.0100 51.5 50.0 3.0 50.0

Styrene Ave 1.120 1.177 0.0100 52.5 50.0 5.1 50.0

Bromoform Ave 0.1536 0.1668 0.1000 54.3 50.0 8.6 50.0

Isopropylbenzene Ave 3.312 3.294 0.0100 49.7 50.0 -0.5 50.0

Bromobenzene Ave 0.7374 0.7428 0.0100 50.4 50.0 0.7 50.0

1,1,2,2-Tetrachloroethane Ave 0.3844 0.3896 0.3000 50.7 50.0 1.4 50.0

1,2,3-Trichloropropane Ave 0.2827 0.2926 0.0100 51.8 50.0 3.5 50.0

N-Propylbenzene Ave 3.971 4.021 0.0100 50.6 50.0 1.3 50.0

4-Chlorotoluene Ave 2.242 2.261 0.0100 50.4 50.0 0.9 50.0

1,3,5-Trimethylbenzene Ave 2.765 2.824 0.0100 51.1 50.0 2.1 50.0

2-Chlorotoluene Ave 2.663 2.687 0.0100 50.5 50.0 0.9 50.0

tert-Butylbenzene Ave 2.558 2.553 0.0100 49.9 50.0 -0.2 50.0

1,2,4-Trimethylbenzene Ave 2.713 2.748 0.0100 50.6 50.0 1.3 50.0

sec-Butylbenzene Ave 3.783 3.833 0.0100 50.7 50.0 1.3 50.0

1,3-Dichlorobenzene Ave 1.575 1.609 0.0100 51.1 50.0 2.2 50.0

p-Isopropyltoluene Ave 3.287 3.338 0.0100 50.8 50.0 1.6 50.0

1,4-Dichlorobenzene Ave 1.556 1.593 0.0100 51.2 50.0 2.4 50.0

1,2-Dichlorobenzene Ave 1.323 1.354 0.0100 51.2 50.0 2.3 50.0

n-Butylbenzene Ave 2.919 3.043 0.0100 52.1 50.0 4.2 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0661 0.0612 0.0100 46.3 50.0 -7.4 50.0

1,2,4-Trichlorobenzene Ave 0.8970 0.9077 0.0100 50.6 50.0 1.2 50.0

Hexachlorobutadiene Ave 0.7568 0.7747 0.0100 51.2 50.0 2.4 50.0

Naphthalene Ave 0.9856 0.9469 0.0100 48.0 50.0 -3.9 50.0

1,2,3-Trichlorobenzene Ave 0.7171 0.6971 0.0100 48.6 50.0 -2.8 50.0

Dibromofluoromethane Ave 0.3990 0.3878 0.0100 48.6 50.0 -2.8 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2633 0.0100 47.1 50.0 -5.7 50.0

Toluene-d8 (Surr) Ave 1.184 1.185 0.0100 50.1 50.0 0.0 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.4903 0.0100 49.0 50.0 -2.1 50.0

FORM VII 8260B

Page 163 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 12:06

12/11/2012 14:23

12/11/2012 18:09

CCV 500-172879/3

DB624

TestAmerica Chicago

Lab File ID: 22D1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3990 0.3864 0.0100 48.4 50.0 -3.1 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2652 0.0100 47.5 50.0 -5.0 50.0

Toluene-d8 (Surr) Ave 1.184 1.187 0.0100 50.1 50.0 0.3 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.5077 0.0100 50.7 50.0 1.4 50.0

FORM VII 8260B

Page 164 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 12:06

12/11/2012 14:23

12/11/2012 18:09

CCV 500-172880/3

DB624

TestAmerica Chicago

Lab File ID: 22D1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3990 0.3864 0.0100 48.4 50.0 -3.1 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2793 0.2652 0.0100 47.5 50.0 -5.0 50.0

Toluene-d8 (Surr) Ave 1.184 1.187 0.0100 50.1 50.0 0.3 50.0

4-Bromofluorobenzene (Surr) Ave 0.5005 0.5077 0.0100 50.7 50.0 1.4 50.0

FORM VII 8260B

Page 165 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 12:06

12/11/2012 19:06

12/11/2012 23:48

CCV 500-172879/3

DB624

TestAmerica Chicago

Lab File ID: 22D1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Lin1 0.8634 0.0100 53.1 50.0 6.2 50.0

Ethyl ether Ave 0.2603 0.2932 0.0100 56.3 50.0 12.6 50.0

Iodomethane Lin1 0.7397 0.0100 111 100 11.4 50.0

3-Chloropropene Ave 0.2462 0.2847 0.0100 116 100 15.6 50.0

Methyl acetate Ave 0.2127 0.2410 0.0100 56.7 50.0 13.3 50.0

Hexane Ave 0.8764 1.027 0.0100 58.6 50.0 17.2 50.0

2-Chloro-1,3-butadiene Ave 0.9423 1.089 0.0100 57.8 50.0 15.6 50.0

Isopropyl ether Ave 1.545 1.729 0.0100 56.0 50.0 11.9 50.0

Ethyl acetate Ave 0.1956 0.2138 0.0100 546 500 9.3 50.0

Methacrylonitrile Ave 0.1427 0.1600 0.0100 112 100 12.2 50.0

Cyclohexane Lin1 1.187 0.0100 55.5 50.0 11.1 50.0

Isobutyl alcohol Ave 0.0073 0.0083 0.0010 4562 4000 14.0 50.0

2,2,4-Trimethylpentane Ave 1.673 1.989 0.0100 59.5 50.0 18.9 50.0

Heptane Ave 0.7351 0.8581 0.0100 58.4 50.0 16.7 50.0

n-Butyl alcohol Ave 0.0045 0.0051 0.0010 4567 4000 14.2 50.0

Methylcyclohexane Ave 0.5969 0.7086 0.0100 59.4 50.0 18.7 50.0

Methyl methacrylate Ave 0.1655 0.1871 0.0100 113 100 13.1 50.0

2-Nitropropane Ave 0.0618 0.0790 0.0100 5117 4000 27.9 50.0

Ethyl methacrylate Ave 0.2528 0.2978 0.0100 118 100 17.8 50.0

Cyclohexanone Ave 0.0256 0.0564 0.0100 8825 4000 120.6* 50.0

trans-1,4-Dichloro-2-butene Ave 0.0710 0.0791 0.0100 111 100 11.4 50.0

Pentachloroethane Ave 0.2758 0.3355 0.0100 122 100 21.6 50.0

1,3,5-Trichlorobenzene Ave 1.226 1.477 0.0100 60.2 50.0 20.4 50.0

2-Methylnaphthalene Ave 0.6831 0.6873 0.0100 50.3 50.0 0.6 50.0

FORM VII 8260B

Page 166 of 360 12/26/2012
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53034-1

CMS22

12/13/2012 12:06

12/11/2012 19:06

12/11/2012 23:48

CCV 500-172880/3

DB624

TestAmerica Chicago

Lab File ID: 22D1213.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Lin1 0.8634 0.0100 53.1 50.0 6.2 50.0

Ethyl ether Ave 0.2603 0.2932 0.0100 56.3 50.0 12.6 50.0

Iodomethane Lin1 0.7397 0.0100 111 100 11.4 50.0

3-Chloropropene Ave 0.2462 0.2847 0.0100 116 100 15.6 50.0

Methyl acetate Ave 0.2127 0.2410 0.0100 56.7 50.0 13.3 50.0

Hexane Ave 0.8764 1.027 0.0100 58.6 50.0 17.2 50.0

2-Chloro-1,3-butadiene Ave 0.9423 1.089 0.0100 57.8 50.0 15.6 50.0

Isopropyl ether Ave 1.545 1.729 0.0100 56.0 50.0 11.9 50.0

Ethyl acetate Ave 0.1956 0.2138 0.0100 546 500 9.3 50.0

Methacrylonitrile Ave 0.1427 0.1600 0.0100 112 100 12.2 50.0

Cyclohexane Lin1 1.187 0.0100 55.5 50.0 11.1 50.0

Isobutyl alcohol Ave 0.0073 0.0083 0.0010 4562 4000 14.0 50.0

2,2,4-Trimethylpentane Ave 1.673 1.989 0.0100 59.5 50.0 18.9 50.0

Heptane Ave 0.7351 0.8581 0.0100 58.4 50.0 16.7 50.0

n-Butyl alcohol Ave 0.0045 0.0051 0.0010 4567 4000 14.2 50.0

Methylcyclohexane Ave 0.5969 0.7086 0.0100 59.4 50.0 18.7 50.0

Methyl methacrylate Ave 0.1655 0.1871 0.0100 113 100 13.1 50.0

2-Nitropropane Ave 0.0618 0.0790 0.0100 5117 4000 27.9 50.0

Ethyl methacrylate Ave 0.2528 0.2978 0.0100 118 100 17.8 50.0

Cyclohexanone Ave 0.0256 0.0564 0.0100 8825 4000 120.6* 50.0

trans-1,4-Dichloro-2-butene Ave 0.0710 0.0791 0.0100 111 100 11.4 50.0

Pentachloroethane Ave 0.2758 0.3355 0.0100 122 100 21.6 50.0

1,3,5-Trichlorobenzene Ave 1.226 1.477 0.0100 60.2 50.0 20.4 50.0

2-Methylnaphthalene Ave 0.6831 0.6873 0.0100 50.3 50.0 0.6 50.0

FORM VII 8260B

Page 167 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53034-1

Lab Sample ID: MB 500-172698/4

Matrix: Lab File ID: 16M1212.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/12/2012 08:26

DB624 ID:

Analysis Batch No.: 172698 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 2.16

78-93-3 2-Butanone (MEK) <5.00 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 106 70-134

2037-26-5 Toluene-d8 (Surr) 114 75-122

460-00-4 4-Bromofluorobenzene (Surr) 107 70-122

1868-53-7 Dibromofluoromethane 109 75-120

FORM I 8260B

Page 168 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53034-1

Lab Sample ID: MB 500-172879/6

Matrix: Lab File ID: 22M1213.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5(mL)

5 (mL)

5(mL) 0.2(mm)

Date Analyzed: 12/13/2012 13:24

DB624 ID:

Analysis Batch No.: 172879 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.30

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 88 75-125

2037-26-5 Toluene-d8 (Surr) 93 75-120

460-00-4 4-Bromofluorobenzene (Surr) 88 75-120

1868-53-7 Dibromofluoromethane 90 75-120

FORM I 8260B

Page 169 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53034-1

Lab Sample ID: MB 500-172880/6

Matrix: Lab File ID: 22M1213.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/13/2012 13:24

DB624 ID:

Analysis Batch No.: 172880 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 88 75-125

2037-26-5 Toluene-d8 (Surr) 93 75-120

460-00-4 4-Bromofluorobenzene (Surr) 88 75-120

1868-53-7 Dibromofluoromethane 90 75-120

FORM I 8260B

Page 170 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53034-1

Lab Sample ID: LCS 500-172698/5

Matrix: Lab File ID: 16S1212.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/12/2012 08:49

DB624 ID:

Analysis Batch No.: 172698 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 47.36 5.00 2.16

78-93-3 2-Butanone (MEK) 47.66 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 108 70-134

2037-26-5 Toluene-d8 (Surr) 117 75-122

460-00-4 4-Bromofluorobenzene (Surr) 108 70-122

1868-53-7 Dibromofluoromethane 106 75-120

FORM I 8260B

Page 171 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53034-1

Lab Sample ID: LCS 500-172879/4

Matrix: Lab File ID: 22S1213.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5(mL)

5 (mL)

5(mL) 0.2(mm)

Date Analyzed: 12/13/2012 12:32

DB624 ID:

Analysis Batch No.: 172879 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 46.30 5.00 1.30

78-93-3 2-Butanone (MEK) 46.82 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-125

2037-26-5 Toluene-d8 (Surr) 99 75-120

460-00-4 4-Bromofluorobenzene (Surr) 100 75-120

1868-53-7 Dibromofluoromethane 97 75-120

FORM I 8260B

Page 172 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53034-1

Lab Sample ID: LCS 500-172880/4

Matrix: Lab File ID: 22S1213.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL)

0.2(mm)

Date Analyzed: 12/13/2012 12:32

DB624 ID:

Analysis Batch No.: 172880 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 46.30 5.00 1.29

78-93-3 2-Butanone (MEK) 46.82 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-125

2037-26-5 Toluene-d8 (Surr) 99 75-120

460-00-4 4-Bromofluorobenzene (Surr) 100 75-120

1868-53-7 Dibromofluoromethane 97 75-120

FORM I 8260B

Page 173 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC Discrete 2 MS

SDG No.:

500-53034-1

Lab Sample ID: 500-53034-2 MS

Matrix: Lab File ID: 53034-02s.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/06/2012 14:25

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.3

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/12/2012 09:49

DB624 ID:

Analysis Batch No.: 172698 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 9517 17.4 7.52

78-93-3 2-Butanone (MEK) 176.3 17.4 6.30

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 110 70-134

2037-26-5 Toluene-d8 (Surr) 108 75-122

460-00-4 4-Bromofluorobenzene (Surr) 103 70-122

1868-53-7 Dibromofluoromethane 107 75-120

FORM I 8260B

Page 174 of 360 12/26/2012
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC Discrete 2 MSD

SDG No.:

500-53034-1

Lab Sample ID: 500-53034-2 MSD

Matrix: Lab File ID: 53034-02t.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/06/2012 14:25

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.3

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/12/2012 10:12

DB624 ID:

Analysis Batch No.: 172698 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 10570 17.4 7.52

78-93-3 2-Butanone (MEK) 194.9 17.4 6.30

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 114 70-134

2037-26-5 Toluene-d8 (Surr) 107 75-122

460-00-4 4-Bromofluorobenzene (Surr) 98 70-122

1868-53-7 Dibromofluoromethane 109 75-120

FORM I 8260B

Page 175 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53034-1

CMS16

170196

Start Date:

End Date: 11/19/2012 17:14

11/19/2012 11:14

BFB 500-170196/5 11/19/2012 11:14 1 16B1119c.D DB624 0.2(mm)

STD1 500-170196/6 IC 11/19/2012 12:14 1 16I1119A.D DB624 0.2(mm)

STD2 500-170196/7 IC 11/19/2012 12:37 1 16I1119B.D DB624 0.2(mm)

STD3 500-170196/8 

ICIS

11/19/2012 13:00 1 16I1119C.D DB624 0.2(mm)

STD4 500-170196/9 IC 11/19/2012 13:23 1 16I1119D.D DB624 0.2(mm)

STD5 500-170196/10 

IC

11/19/2012 13:46 1 16I1119E.D DB624 0.2(mm)

STD6 500-170196/11 

IC

11/19/2012 14:09 1 16I1119F.D DB624 0.2(mm)

STD1AP 500-170196/12 

IC

11/19/2012 14:32 1 DB624 0.2(mm)

STD2AP 500-170196/13 

IC

11/19/2012 14:55 1 DB624 0.2(mm)

STD3AP 500-170196/14 

IC

11/19/2012 15:18 1 DB624 0.2(mm)

STD4AP 500-170196/15 

IC

11/19/2012 15:42 1 DB624 0.2(mm)

STD5AP 500-170196/16 

IC

11/19/2012 16:05 1 DB624 0.2(mm)

STD6AP 500-170196/17 

IC

11/19/2012 16:28 1 DB624 0.2(mm)

ICV 500-170196/19 11/19/2012 17:14 1 16S1119.D DB624 0.2(mm)

8260B

Page 176 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53034-1

CMS16

172698

Start Date:

End Date: 12/12/2012 14:06

12/12/2012 07:05

BFB 500-172698/1 12/12/2012 07:05 1 16B1212.D DB624 0.2(mm)

CCVIS 500-172698/2 12/12/2012 07:39 1 16C1212.D DB624 0.2(mm)

CCV 500-172698/3 12/12/2012 08:03 1 16D1212.D DB624 0.2(mm)

MB 500-172698/4 12/12/2012 08:26 1 16M1212.D DB624 0.2(mm)

LCS 500-172698/5 12/12/2012 08:49 1 16S1212.D DB624 0.2(mm)

500-53034-2 FC Discrete 2 12/12/2012 09:25 1 53034-02.D DB624 0.2(mm)

500-53034-2 MS FC Discrete 2 MS 12/12/2012 09:49 1 53034-02s.D DB624 0.2(mm)

500-53034-2 MSD FC Discrete 2 MSD 12/12/2012 10:12 1 53034-02t.D DB624 0.2(mm)

ZZZZZ 12/12/2012 10:36 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 10:59 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 11:22 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 11:46 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 12:09 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 12:32 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 12:55 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 13:18 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 13:42 1 DB624 0.2(mm)

ZZZZZ 12/12/2012 14:06 1 DB624 0.2(mm)

8260B

Page 177 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53034-1

CMS22

172614

Start Date:

End Date: 12/12/2012 00:17

12/11/2012 13:45

BFB 500-172614/1 12/11/2012 13:45 1 22B1211.D DB624 0.2(mm)

STD01 500-172614/2 

IC

12/11/2012 14:23 1 22I1211A.D DB624 0.2(mm)

STD02 500-172614/3 

IC

12/11/2012 14:51 1 22I1211B.D DB624 0.2(mm)

STD03 500-172614/4 

IC

12/11/2012 15:20 1 22I1211C.D DB624 0.2(mm)

STD04 500-172614/5 

IC

12/11/2012 15:48 1 22I1211D.D DB624 0.2(mm)

STD05 500-172614/6 

IC

12/11/2012 16:16 1 22I1211E.D DB624 0.2(mm)

STD06 500-172614/7 

ICIS

12/11/2012 16:44 1 22I1211F.D DB624 0.2(mm)

STD07 500-172614/8 

IC

12/11/2012 17:13 1 22I1211G.D DB624 0.2(mm)

STD08 500-172614/9 

IC

12/11/2012 17:41 1 22I1211H.D DB624 0.2(mm)

STD09 500-172614/10 

IC

12/11/2012 18:09 1 22I1211I.D DB624 0.2(mm)

STD02AP 

500-172614/12 IC

12/11/2012 19:06 1 DB624 0.2(mm)

STD05AP 

500-172614/15 IC

12/11/2012 20:30 1 DB624 0.2(mm)

STD06AP 

500-172614/16 IC

12/11/2012 20:59 1 DB624 0.2(mm)

STD07AP 

500-172614/17 IC

12/11/2012 21:27 1 DB624 0.2(mm)

STD08AP 

500-172614/18 IC

12/11/2012 21:55 1 DB624 0.2(mm)

STD09AP 

500-172614/19 IC

12/11/2012 22:24 1 DB624 0.2(mm)

STD03AP 

500-172614/21 IC

12/11/2012 23:20 1 DB624 0.2(mm)

STD04AP 

500-172614/22 IC

12/11/2012 23:48 1 DB624 0.2(mm)

ICV 500-172614/23 12/12/2012 00:17 1 22S1211.D DB624 0.2(mm)

8260B

Page 178 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53034-1

CMS22

172615

Start Date:

End Date: 12/12/2012 00:17

12/11/2012 13:45

BFB 500-172615/1 12/11/2012 13:45 1 22B1211.D DB624 0.2(mm)

STD01 500-172615/2 

IC

12/11/2012 14:23 1 22I1211A.D DB624 0.2(mm)

STD02 500-172615/3 

IC

12/11/2012 14:51 1 22I1211B.D DB624 0.2(mm)

STD03 500-172615/4 

IC

12/11/2012 15:20 1 22I1211C.D DB624 0.2(mm)

STD04 500-172615/5 

IC

12/11/2012 15:48 1 22I1211D.D DB624 0.2(mm)

STD05 500-172615/6 

IC

12/11/2012 16:16 1 22I1211E.D DB624 0.2(mm)

STD06 500-172615/7 

ICIS

12/11/2012 16:44 1 22I1211F.D DB624 0.2(mm)

STD07 500-172615/8 

IC

12/11/2012 17:13 1 22I1211G.D DB624 0.2(mm)

STD08 500-172615/9 

IC

12/11/2012 17:41 1 22I1211H.D DB624 0.2(mm)

STD09 500-172615/10 

IC

12/11/2012 18:09 1 22I1211I.D DB624 0.2(mm)

STD02AP 

500-172615/12 IC

12/11/2012 19:06 1 DB624 0.2(mm)

STD05AP 

500-172615/15 IC

12/11/2012 20:30 1 DB624 0.2(mm)

STD06AP 

500-172615/16 IC

12/11/2012 20:59 1 DB624 0.2(mm)

STD07AP 

500-172615/17 IC

12/11/2012 21:27 1 DB624 0.2(mm)

STD08AP 

500-172615/18 IC

12/11/2012 21:55 1 DB624 0.2(mm)

STD09AP 

500-172615/19 IC

12/11/2012 22:24 1 DB624 0.2(mm)

STD03AP 

500-172615/21 IC

12/11/2012 23:20 1 DB624 0.2(mm)

STD04AP 

500-172615/22 IC

12/11/2012 23:48 1 DB624 0.2(mm)

ICV 500-172615/23 12/12/2012 00:17 1 22S1211.D DB624 0.2(mm)

8260B

Page 179 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53034-1

CMS22

172879

Start Date:

End Date: 12/13/2012 22:04

12/13/2012 11:02

BFB 500-172879/1 12/13/2012 11:02 1 22B1213.D DB624 0.2(mm)

CCV 500-172879/2 12/13/2012 11:40 1 22C1213.D DB624 0.2(mm)

CCV 500-172879/3 12/13/2012 12:06 1 22D1213.D DB624 0.2(mm)

LCS 500-172879/4 12/13/2012 12:32 1 22S1213.D DB624 0.2(mm)

MB 500-172879/6 12/13/2012 13:24 1 22M1213.D DB624 0.2(mm)

500-53034-2 DL FC Discrete 2 DL 12/13/2012 22:04 50 53034-02C.D DB624 0.2(mm)

8260B

Page 180 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53034-1

CMS22

172880

Start Date:

End Date: 12/13/2012 21:38

12/13/2012 11:02

BFB 500-172880/1 12/13/2012 11:02 1 22B1213.D DB624 0.2(mm)

CCV 500-172880/2 12/13/2012 11:40 1 22C1213.D DB624 0.2(mm)

CCV 500-172880/3 12/13/2012 12:06 1 22D1213.D DB624 0.2(mm)

LCS 500-172880/4 12/13/2012 12:32 1 22S1213.D DB624 0.2(mm)

MB 500-172880/6 12/13/2012 13:24 1 22M1213.D DB624 0.2(mm)

ZZZZZ 12/13/2012 13:50 1 DB624 0.2(mm)

500-53034-4 Trip Blank 12/13/2012 14:15 1 53034-04.D DB624 0.2(mm)

ZZZZZ 12/13/2012 14:41 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 15:06 1 DB624 0.2(mm)

500-53034-3 FC EB 2 12/13/2012 15:33 1 53034-03.D DB624 0.2(mm)

ZZZZZ 12/13/2012 15:59 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 16:25 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 16:51 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 17:17 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 17:43 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 18:09 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 18:35 10 DB624 0.2(mm)

ZZZZZ 12/13/2012 19:02 100 DB624 0.2(mm)

ZZZZZ 12/13/2012 19:28 20 DB624 0.2(mm)

ZZZZZ 12/13/2012 19:54 200 DB624 0.2(mm)

ZZZZZ 12/13/2012 20:20 2 DB624 0.2(mm)

ZZZZZ 12/13/2012 20:46 20 DB624 0.2(mm)

ZZZZZ 12/13/2012 21:12 1 DB624 0.2(mm)

ZZZZZ 12/13/2012 21:38 1 DB624 0.2(mm)

8260B

Page 181 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GC/MS VOA BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

172604 12/11/12 11:27 Werner, Brian D

Batch Method:

TestAmerica Chicago

5030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount AnalysisComment

500-53034-A-2 FC Discrete 2 5030B, 8260B T 5 g 5 mL meoh

Batch Notes

Balance ID C-0133

Methanol Lot Number DEH187

Pipette ID C-2207

Basis Basis Description

T Total/NA

8260B Page 1 of 1

Page 182 of 360 12/26/2012


METALS

Page 185 of 360 12/26/2012
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

METALS

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53034-1

FC Composite 2 500-53034-1 

FC EB 2 500-53034-3 

Comments:

Page 186 of 360 12/26/2012
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53034-1

Date Received: 12/07/2012 09:50

500-53034-1

FC Composite 2

Solid Date Sampled: 12/06/2012 14:30

Reporting Basis: DRY

METALS

TestAmerica Chicago

% Solids: 27.4

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 377 3.64 0.433 mg/Kg B 1 6010B

7440-50-8 Copper 959 3.64 0.987 mg/Kg 1 6010B

7440-47-3 Chromium 9290 3.64 0.608 mg/Kg 1 6010B

7440-02-0 Nickel 78.7 3.64 0.797 mg/Kg 1 6010B

7439-92-1 Lead 261 1.82 0.626 mg/Kg B 1 6010B

7440-62-2 Vanadium 158 1.82 0.276 mg/Kg 1 6010B

7440-66-6 Zinc 381 7.28 2.50 mg/Kg 1 6010B

7439-97-6 Mercury 0.635 0.0600 0.0229 mg/Kg 1 7471A

FORM IA-IN Page 187 of 360 12/26/2012
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53034-1

Date Received: 12/07/2012 09:50

500-53034-1

FC Composite 2

Solid Date Sampled: 12/06/2012 14:30

Reporting Basis: WET

METALS - TCLP

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.500 0.500 0.0100 mg/L 1 6010B

7440-50-8 Copper 0.0355 0.0250 0.0100 mg/L 1 6010B

7440-47-3 Chromium 0.0524 0.0250 0.0100 mg/L 1 6010B

7440-02-0 Nickel 0.646 0.0250 0.0100 mg/L 1 6010B

7439-92-1 Lead <0.0500 0.0500 0.00500 mg/L 1 6010B

7440-62-2 Vanadium <0.0250 0.0250 0.00500 mg/L 1 6010B

7440-66-6 Zinc 0.0685 0.100 0.0200 mg/L J 1 6010B

7439-97-6 Mercury 0.0000559 0.000200 0.000020 mg/L J B

0

1 7470A

FORM IA-IN Page 188 of 360 12/26/2012
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53034-3

Date Received: 12/07/2012 09:50

500-53034-1

FC EB 2

Water Date Sampled: 12/06/2012 14:15

Reporting Basis: WET

METALS

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.0100 0.0100 0.000440 mg/L 1 6010B

7440-50-8 Copper <0.0100 0.0100 0.00106 mg/L 1 6010B

7440-47-3 Chromium <0.0100 0.0100 0.000960 mg/L 1 6010B

7440-02-0 Nickel <0.0100 0.0100 0.00190 mg/L 1 6010B

7439-92-1 Lead <0.00500 0.00500 0.00158 mg/L 1 6010B

7440-62-2 Vanadium <0.00500 0.00500 0.000620 mg/L 1 6010B

7440-66-6 Zinc <0.0200 0.0200 0.00472 mg/L 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000071 mg/L

0

1 7470A

FORM IA-IN Page 189 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M12LICVIC_00001 mg/L

M12KCCVIC_00002

Analyte

ICV 500-172535/10

12/10/2012 15:39

Found C True %R

CCV 500-172535/27

12/10/2012 17:31

CCV 500-172535/39

12/10/2012 18:54

Found C True %R Found C True %R

Barium 0.4082 0.400 102 0.5045 0.500 101 0.4964 0.500 99

Chromium 0.4104 0.400 103 0.5067 0.500 101 0.5095 0.500 102

Copper 0.4115 0.400 103 0.5113 0.500 102 0.5085 0.500 102

Lead 0.4113 0.400 103 0.4998 0.500 100 0.5060 0.500 101

Nickel 0.4038 0.400 101 0.4970 0.500 99 0.4993 0.500 100

Vanadium 4.057 4.00 101 5.005 5.00 100 5.011 5.00 100

Zinc 0.4013 0.400 100 0.4948 0.500 99 0.5018 0.500 100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 190 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M12LICVIC_00001 mg/L

M12KCCVIC_00002

Analyte

CCV 500-172535/51

12/10/2012 20:11

Found C True %R

CCV 500-172535/63

12/10/2012 21:34

Found C True %R Found C True %R

Barium 0.5110 0.500 102 0.5119 0.500 102

Chromium 0.5217 0.500 104 0.5199 0.500 104

Copper 0.5231 0.500 105 0.5253 0.500 105

Lead 0.5179 0.500 104 0.5141 0.500 103

Nickel 0.5116 0.500 102 0.5096 0.500 102

Vanadium 5.138 5.00 103 5.132 5.00 103

Zinc 0.5137 0.500 103 0.5104 0.500 102

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 191 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M12LICVIC_00001 mg/L

M12KCCVIC_00002

Analyte

ICV 500-172697/10

12/11/2012 17:42

Found C True %R

CCV 500-172697/15

12/11/2012 18:15

CCV 500-172697/27

12/11/2012 19:32

Found C True %R Found C True %R

Barium 0.4068 0.400 102 0.5193 0.500 104 0.5143 0.500 103

Chromium 0.4118 0.400 103 0.5162 0.500 103 0.5185 0.500 104

Copper 0.4112 0.400 103 0.5258 0.500 105 0.5215 0.500 104

Lead 0.4159 0.400 104 0.5180 0.500 104 0.5191 0.500 104

Nickel 0.4085 0.400 102 0.5103 0.500 102 0.5122 0.500 102

Vanadium 4.075 4.00 102 5.127 5.00 103 5.127 5.00 103

Zinc 0.4078 0.400 102 0.5035 0.500 101 0.5094 0.500 102

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 192 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M12LICVIC_00001 mg/L

M12KCCVIC_00002

Analyte

CCV 500-172697/39

12/11/2012 20:49

Found C True %R Found C True %R Found C True %R

Barium 0.5113 0.500 102

Chromium 0.5114 0.500 102

Copper 0.5158 0.500 103

Lead 0.5126 0.500 103

Nickel 0.5072 0.500 101

Vanadium 5.075 5.00 101

Zinc 0.5025 0.500 101

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 193 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M12LICVIC_00001 mg/L

M12KCCVIC_00002

Analyte

ICV 500-172699/6

12/11/2012 15:27

Found C True %R

CCV 500-172699/38

12/11/2012 17:37

CCV 500-172699/51

12/11/2012 18:32

Found C True %R Found C True %R

Barium 0.3952 0.400 99 0.4956 0.500 99 0.4964 0.500 99

Chromium 0.3936 0.400 98 0.4796 0.500 96 0.4984 0.500 100

Copper 0.4015 0.400 100 0.4931 0.500 99 0.5070 0.500 101

Lead 0.4059 0.400 101 0.5098 0.500 102 0.5053 0.500 101

Nickel 0.4025 0.400 101 0.5100 0.500 102 0.5088 0.500 102

Vanadium 3.973 4.00 99 4.877 5.00 98 5.029 5.00 101

Zinc 0.4100 0.400 102 0.5197 0.500 104 0.5157 0.500 103

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 194 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M12LICVIC_00001 mg/L

M12KCCVIC_00002

Analyte

CCV 500-172699/64

12/11/2012 19:27

Found C True %R

CCV 500-172699/75

12/11/2012 20:18

Found C True %R Found C True %R

Barium 0.5028 0.500 101 0.5067 0.500 101

Chromium 0.4908 0.500 98 0.4727 0.500 95

Copper 0.5147 0.500 103 0.4989 0.500 100

Lead 0.5104 0.500 102 0.5008 0.500 100

Nickel 0.5139 0.500 103 0.5114 0.500 102

Vanadium 5.028 5.00 101 4.906 5.00 98

Zinc 0.5178 0.500 104 0.5039 0.500 101

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 195 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-172626/7

12/11/2012 09:37

Found C True %R

CCV 500-172626/45

12/11/2012 10:52

CCV 500-172626/57

12/11/2012 11:15

Found C True %R Found C True %R

Mercury 2.000 2.00 100 0.9860 1.00 99 1.120 1.00 112

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 196 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-172626/100

12/11/2012 12:54

Found C True %R

CCV 500-172626/106

12/11/2012 13:06

Found C True %R Found C True %R

Mercury 1.070 1.00 107 1.100 1.00 110

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 197 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-172764/7

12/12/2012 08:49

Found C True %R

CCV 500-172764/19

12/12/2012 09:14

CCV 500-172764/31

12/12/2012 09:37

Found C True %R Found C True %R

Mercury 2.001 2.00 100 1.099 J 1.00 110 1.074 J 1.00 107

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 198 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-172764/43

12/12/2012 10:00

Found C True %R

CCV 500-172764/67

12/12/2012 10:47

CCV 500-172764/79

12/12/2012 11:11

Found C True %R Found C True %R

Mercury <2.00 1.00 97 1.091 1.00 109 1.014 1.00 101

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 199 of 360 12/26/2012
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53034-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-172764/83

12/12/2012 11:19

Found C True %R Found C True %R Found C True %R

Mercury 0.9528 1.00 95

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 200 of 360 12/26/2012
2B-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-172535/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02018 101 50-150

Copper 0.0200 0.02005 100 50-150

Chromium 0.0200 0.02066 103 50-150

Nickel 0.0200 0.02052 103 50-150

Lead 0.0100 0.01125 113 50-150

Vanadium 0.0100 0.01058 106 50-150

Zinc 0.0400 0.04112 103 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-172535/70

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02003 100 50-150

Copper 0.0200 0.02000 100 50-150

Chromium 0.0200 0.02101 105 50-150

Nickel 0.0200 0.02125 106 50-150

Lead 0.0100 0.01032 103 50-150

Vanadium 0.0100 0.009850 99 50-150

Zinc 0.0400 0.04183 105 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-172697/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02027 101 50-150

Copper 0.0200 0.01973 99 50-150

Chromium 0.0200 0.02048 102 50-150

Nickel 0.0200 0.02067 103 50-150

Lead 0.0100 0.01172 117 50-150

Vanadium 0.0100 0.01024 102 50-150

Zinc 0.0400 0.04086 102 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 201 of 360 12/26/2012
2B-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP6

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-172699/9

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.01943 97 50-150

Copper 0.0200 0.01988 99 50-150

Chromium 0.0200 0.01883 94 50-150

Nickel 0.0200 0.01943 97 50-150

Lead 0.0100 0.01089 109 50-150

Vanadium 0.0100 0.009676 97 50-150

Zinc 0.0400 0.03932 98 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 202 of 360 12/26/2012
2B-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

CRQL CHECK STANDARD

METALS

Method: 7470A Instrument ID: HG6

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-172764/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 <2.00 103 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 203 of 360 12/26/2012
2B-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

CRQL CHECK STANDARD

METALS

Method: 7471A Instrument ID: HG5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-172626/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 0.1160 J 58 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 204 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-172535/11 CCB 500-172535/28 CCB 500-172535/40 CCB 500-172535/52

12/10/2012 15:47 12/10/2012 17:37 12/10/2012 19:00 12/10/2012 20:17

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 205 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

mg/L

Analyte RL Found C Found C Found C Found C

CCB 500-172535/64

12/10/2012 21:41

3-IN

Barium 0.0100 <0.0100

Chromium 0.0100 <0.0100

Copper 0.0100 <0.0100

Lead 0.00500 <0.00500

Nickel 0.0100 <0.0100

Vanadium 0.00500 <0.00500

Zinc 0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 206 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-172697/11 CCB 500-172697/16 CCB 500-172697/28 CCB 500-172697/40

12/11/2012 17:48 12/11/2012 18:21 12/11/2012 19:38 12/11/2012 20:55

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 207 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-172699/7 CCB 500-172699/39 CCB 500-172699/52 CCB 500-172699/65

12/11/2012 15:31 12/11/2012 17:41 12/11/2012 18:36 12/11/2012 19:31

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 208 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

mg/L

Analyte RL Found C Found C Found C Found C

CCB 500-172699/76

12/11/2012 20:22

3-IN

Barium 0.0100 <0.0100

Chromium 0.0100 <0.0100

Copper 0.0100 <0.0100

Lead 0.00500 <0.00500

Nickel 0.0100 <0.0100

Vanadium 0.00500 <0.00500

Zinc 0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 209 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-172626/8 CCB 500-172626/46 CCB 500-172626/58 CCB 500-172626/101

12/11/2012 09:39 12/11/2012 10:54 12/11/2012 11:17 12/11/2012 12:57

3-IN

Mercury 0.200 <0.200 <0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 210 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

ug/L

Analyte RL Found C Found C Found C Found C

CCB 500-172626/107

12/11/2012 13:09

3-IN

Mercury 0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 211 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-172764/8 CCB 500-172764/20 CCB 500-172764/32 CCB 500-172764/44

12/12/2012 08:52 12/12/2012 09:16 12/12/2012 09:39 12/12/2012 10:02

3-IN

Mercury 2.00 <2.00 <2.00 <2.00 <2.00

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 212 of 360 12/26/2012
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53034-1

ug/L

Analyte RL Found C Found C Found C Found C

CCB 500-172764/68 CCB 500-172764/80 CCB 500-172764/84

12/12/2012 10:48 12/12/2012 11:13 12/12/2012 11:21

3-IN

Mercury 2.00 <0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 213 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-172306/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: ICP5

METHOD BLANK

METALS

 172535

TestAmerica Chicago

7440-39-3 Barium 0.1210 J 6010B

7440-50-8 Copper <1.00 6010B

7440-47-3 Chromium <1.00 6010B

7440-02-0 Nickel <1.00 6010B

7439-92-1 Lead 0.2260 J 6010B

7440-62-2 Vanadium <0.500 6010B

7440-66-6 Zinc <2.00 6010B

FORM III-IN

Page 214 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB2 500-172501/1-C

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: ICP5

METHOD BLANK

METALS - TCLP

 172697

TestAmerica Chicago

7440-39-3 Barium <0.500 6010B

7440-50-8 Copper <0.0250 6010B

7440-47-3 Chromium <0.0250 6010B

7440-02-0 Nickel <0.0250 6010B

7439-92-1 Lead <0.0500 6010B

7440-62-2 Vanadium <0.0250 6010B

7440-66-6 Zinc <0.100 6010B

FORM III-IN

Page 215 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-172512/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: ICP6

METHOD BLANK

METALS

 172699

TestAmerica Chicago

7440-39-3 Barium <0.0100 6010B

7440-50-8 Copper <0.0100 6010B

7440-47-3 Chromium <0.0100 6010B

7440-02-0 Nickel <0.0100 6010B

7439-92-1 Lead <0.00500 6010B

7440-62-2 Vanadium <0.00500 6010B

7440-66-6 Zinc <0.0200 6010B

FORM III-IN

Page 216 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-172640/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: HG6

METHOD BLANK

METALS

 172764

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 217 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-172642/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: HG6

METHOD BLANK

METALS

 172764

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 218 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB2 500-172501/1-D

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: HG6

METHOD BLANK

METALS - TCLP

 172764

TestAmerica Chicago

7439-97-6 Mercury 0.00003710 J 7470A

FORM III-IN

Page 219 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-172460/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53034-1

Instrument Code: HG5

METHOD BLANK

METALS

 172626

TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN

Page 220 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSA 500-172535/13

P51210B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0018

Copper -0.0021

Lead 0.0028

Nickel 0.0009

Vanadium 0.0040

Zinc 0.0079

Aluminum 500 515 103

Antimony -0.0005

Arsenic 0.0007

Beryllium -0.0001

Boron 0.0004

Cadmium 0.0021

Calcium 500 487 97

Cobalt 0.0001

Iron 200 190 95

Magnesium 500 523 105

Manganese 0.0041

Molybdenum 0.0121

Potassium -0.0139

Selenium -0.0011

Silicon 0.0156

Silver -0.0001

Sodium 0.0093

Strontium 0.0023

Thallium 0.0027

Tin 0.0009

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 221 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSAB 500-172535/14

P51210B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.522 104

Chromium 0.500 0.487 97

Copper 0.500 0.562 112

Lead 0.0500 0.0512 102

Nickel 1.00 0.941 94

Vanadium 0.500 0.510 102

Zinc 1.00 0.907 91

Aluminum 500 516 103

Antimony 0.600 0.617 103

Arsenic 0.100 0.103 103

Beryllium 0.500 0.482 96

Boron 0.0005

Cadmium 1.00 0.930 93

Calcium 500 490 98

Cobalt 0.500 0.472 94

Iron 200 192 96

Magnesium 500 525 105

Manganese 0.500 0.503 101

Molybdenum 0.0117

Potassium -0.0089

Selenium 0.0500 0.0492 98

Silicon 0.0157

Silver 0.200 0.224 112

Sodium -0.0049

Strontium 0.0023

Thallium 0.100 0.105 105

Tin 0.0016

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 222 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSA 500-172535/71

P51210B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0023

Copper -0.0023

Lead 0.0012

Nickel 0.0015

Vanadium 0.0046

Zinc 0.0082

Aluminum 500 516 103

Antimony -0.0022

Arsenic -0.0008

Beryllium -0.0001

Boron 0.0004

Cadmium 0.0023

Calcium 500 494 99

Cobalt -0.0002

Iron 200 193 96

Magnesium 500 527 105

Manganese 0.0041

Molybdenum 0.0143

Potassium -0.0051

Selenium 0.0002

Silicon 0.0229

Silver 0.0000

Sodium 0.0264

Strontium 0.0023

Thallium -0.0010

Tin 0.0020

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 223 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSAB 500-172535/72

P51210B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.521 104

Chromium 0.500 0.492 98

Copper 0.500 0.564 113

Lead 0.0500 0.0504 101

Nickel 1.00 0.951 95

Vanadium 0.500 0.513 103

Zinc 1.00 0.925 92

Aluminum 500 517 103

Antimony 0.600 0.621 103

Arsenic 0.100 0.102 102

Beryllium 0.500 0.488 98

Boron 0.0006

Cadmium 1.00 0.946 95

Calcium 500 497 99

Cobalt 0.500 0.478 96

Iron 200 195 97

Magnesium 500 530 106

Manganese 0.500 0.507 101

Molybdenum 0.0144

Potassium -0.0063

Selenium 0.0500 0.0504 101

Silicon 0.0233

Silver 0.200 0.225 112

Sodium 0.0056

Strontium 0.0023

Thallium 0.100 0.105 105

Tin 0.0018

Titanium 0.0009

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 224 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSA 500-172697/13

P51211B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium -0.0001

Chromium 0.0022

Copper -0.0027

Lead 0.0000

Nickel 0.0010

Vanadium 0.0047

Zinc 0.0082

Aluminum 500 512 102

Antimony -0.0025

Arsenic -0.0016

Beryllium -0.0001

Boron 0.0005

Cadmium 0.0018

Calcium 500 486 97

Cobalt 0.0000

Iron 200 192 96

Magnesium 500 535 107

Manganese 0.0032

Molybdenum 0.0122

Potassium -0.0069

Selenium 0.0010

Silicon -0.0348

Silver 0.0000

Sodium 0.0261

Strontium 0.0023

Thallium 0.0034

Tin 0.0016

Titanium 0.0000

Total Heavy Metals 0.0000

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 225 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSAB 500-172697/14

P51211B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.523 105

Chromium 0.500 0.491 98

Copper 0.500 0.565 113

Lead 0.0500 0.0491 98

Nickel 1.00 0.973 97

Vanadium 0.500 0.516 103

Zinc 1.00 0.930 93

Aluminum 500 516 103

Antimony 0.600 0.617 103

Arsenic 0.100 0.102 102

Beryllium 0.500 0.490 98

Boron 0.0003

Cadmium 1.00 0.963 96

Calcium 500 485 97

Cobalt 0.500 0.483 97

Iron 200 193 97

Magnesium 500 536 107

Manganese 0.500 0.508 102

Molybdenum 0.0066

Potassium -0.0138

Selenium 0.0500 0.0529 106

Silicon -0.0375

Silver 0.200 0.224 112

Sodium 0.0182

Strontium 0.0023

Thallium 0.100 0.108 108

Tin -0.0001

Titanium 0.0000

Total Heavy Metals 4.05 3.97 98

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 226 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSA 500-172699/10

P6121112B.asc

mg/L

M12LISAIC_00001

ICP6

INTERFERENCE CHECK STANDARD

METALS

Barium -0.0005

Chromium 0.0025

Copper 0.0040

Lead 0.0041

Nickel 0.0010

Vanadium 0.0012

Zinc -0.0011

Aluminum 500 510 102

Antimony -0.0004

Arsenic 0.0034

Beryllium 0.0004

Bismuth -0.0052

Boron 0.0094

Cadmium 0.0003

Calcium 500 472 94

Cobalt -0.0020

Iron 200 190 95

Magnesium 500 510 102

Manganese 0.0003

Molybdenum 0.0007

Potassium -0.0069

Selenium 0.0058

Silicon -0.0019

Silver 0.0013

Sodium 0.0717

Strontium 0.0023

Thallium -0.0093

Tin 0.0067

Titanium 0.0028

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 227 of 360 12/26/2012
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53034-1

ICSAB 500-172699/11

P6121112B.asc

mg/L

M12LISBIC_00001

ICP6

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.495 99

Chromium 0.500 0.466 93

Copper 0.500 0.550 110

Lead 0.0500 0.0565 113

Nickel 1.00 1.00 100

Vanadium 0.500 0.491 98

Zinc 1.00 1.01 101

Aluminum 500 515 103

Antimony 0.600 0.602 100

Arsenic 0.100 0.103 103

Beryllium 0.500 0.507 101

Bismuth -0.0054

Boron 0.0087

Cadmium 1.00 1.01 101

Calcium 500 477 95

Cobalt 0.500 0.512 102

Iron 200 191 96

Magnesium 500 515 103

Manganese 0.500 0.462 92

Molybdenum 0.0011

Potassium -0.0442

Selenium 0.0500 0.0491 98

Silicon 0.0017

Silver 0.200 0.220 110

Sodium 0.0674

Strontium 0.0023

Thallium 0.100 0.0922 92

Tin 0.0042

Titanium 0.0047

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 228 of 360 12/26/2012
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-172306/2-A 

Lab Name: Job No.: 500-53034-1

Sample Matrix: Solid LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Barium 200 200.1 100 80 120 6010B

Copper 25.0 25.45 102 80 120 6010B

Chromium 20.0 20.13 101 80 120 6010B

Nickel 50.0 49.47 99 80 120 6010B

Lead 10.0 10.11 101 80 120 6010B

Vanadium 50.0 50.49 101 80 120 6010B

Zinc 50.0 48.59 97 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 229 of 360 12/26/2012
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-172581/4-A 

Lab Name: Job No.: 500-53034-1

Sample Matrix: Water LCS Source: M12KSPKIC_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.936 97 80 120 6010B

Copper 0.250 0.2419 97 80 120 6010B

Chromium 0.200 0.1920 96 80 120 6010B

Nickel 0.500 0.4764 95 80 120 6010B

Lead 0.100 0.09745 97 80 120 6010B

Vanadium 0.500 0.4821 96 80 120 6010B

Zinc 0.500 0.4708 94 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 230 of 360 12/26/2012
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-172512/2-A 

Lab Name: Job No.: 500-53034-1

Sample Matrix: Water LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.974 99 80 120 6010B

Copper 0.250 0.2472 99 80 120 6010B

Chromium 0.200 0.1892 95 80 120 6010B

Nickel 0.500 0.4817 96 80 120 6010B

Lead 0.100 0.09773 98 80 120 6010B

Vanadium 0.500 0.4890 98 80 120 6010B

Zinc 0.500 0.4699 94 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 231 of 360 12/26/2012
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-172640/8-A 

Lab Name: Job No.: 500-53034-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002027 101 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 232 of 360 12/26/2012
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-172642/8-A 

Lab Name: Job No.: 500-53034-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002054 103 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 233 of 360 12/26/2012
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-172460/8-A 

Lab Name: Job No.: 500-53034-1

Sample Matrix: Solid LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Mercury 0.167 0.1975 118 80 120 7471A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 234 of 360 12/26/2012
9-IN

Instrument ID: ICP5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:20

Prep Method: 3050B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Barium 1 0.119

Chromium 1 0.167

Copper 1 0.271

Lead 0.5 0.172

Nickel 1 0.219

Vanadium 0.5 0.0759

Zinc 2 0.686

FORM IX - IN

Page 235 of 360 12/26/2012
9-IN

Instrument ID: ICP5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:03

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 236 of 360 12/26/2012
9-IN

Instrument ID: ICP6

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:03

Prep Method: 3010A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.01 0.00044

Chromium 0.01 0.00096

Copper 0.01 0.00106

Lead 0.005 0.00158

Nickel 0.01 0.0019

Vanadium 0.005 0.00062

Zinc 0.02 0.00472

FORM IX - IN

Page 237 of 360 12/26/2012
9-IN

Instrument ID: ICP6

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:07

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 238 of 360 12/26/2012
9-IN

Instrument ID: ICP5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 11/01/2005 15:36

Prep Method: 3010A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.5 0.01

Chromium 0.025 0.01

Copper 0.025 0.01

Lead 0.05 0.005

Nickel 0.025 0.01

Vanadium 0.025 0.005

Zinc 0.1 0.02

FORM IX - IN

Page 239 of 360 12/26/2012
9-IN

Instrument ID: ICP5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 01/28/2008 10:37

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.01

Chromium 0.01 0.01

Copper 0.01 0.01

Lead 0.005 0.005

Nickel 0.01 0.01

Vanadium 0.005 0.005

Zinc 0.02 0.02

FORM IX - IN

Page 240 of 360 12/26/2012
9-IN

Instrument ID: HG6

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 08/31/2012 10:08

Prep Method: 7470A

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 241 of 360 12/26/2012
9-IN

Instrument ID: HG6

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 08/31/2012 10:08

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 242 of 360 12/26/2012
9-IN

Instrument ID: HG6

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 11/01/2005 11:39

Prep Method: 7470A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 2 0.2

FORM IX - IN

Page 243 of 360 12/26/2012
9-IN

Instrument ID: HG6

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 09/16/2006 08:48

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 2 1

FORM IX - IN

Page 244 of 360 12/26/2012
9-IN

Instrument ID: HG5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7471A MDL Date: 08/31/2012 10:15

Prep Method: 7471A

Analyte Wavelength/

Mass

RL MDL

(ug/Kg) (ug/Kg)

Mercury 16.7 6.37

FORM IX - IN

Page 245 of 360 12/26/2012
9-IN

Instrument ID: HG5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7471A XMDL Date: 08/31/2012 10:16

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 246 of 360 12/26/2012
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53034-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

ICP5

SDG No.:

(mg/L)

11/19/2012 14:31

METALS

Barium 20 6010B

Copper 20 6010B

Chromium 50 6010B

Nickel 50 6010B

Lead 50 6010B

Vanadium 100 6010B

Zinc 20 6010B

FORM XI - IN

Page 247 of 360 12/26/2012
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53034-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

ICP6

SDG No.:

(mg/L)

11/19/2012 14:24

METALS

Barium 20 6010B

Copper 20 6010B

Chromium 20 6010B

Nickel 20 6010B

Lead 100 6010B

Vanadium 20 6010B

Zinc 20 6010B

FORM XI - IN

Page 248 of 360 12/26/2012
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53034-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG5

SDG No.:

(ug/L)

03/01/2008 11:18

METALS

Mercury 5.0 7471A

FORM XI - IN

Page 249 of 360 12/26/2012
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53034-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG6

SDG No.:

(ug/L)

11/01/2010 11:39

METALS

Mercury 5.0 7470A

FORM XI - IN

Page 250 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

METALS

TestAmerica Chicago

Prep Method: 3050B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-172306/1-A 12/07/2012 16:00 172306 1 100

LCS 500-172306/2-A 12/07/2012 16:00 172306 1 100

500-53034-1 12/07/2012 16:00 172306 1.0011 100

FORM XII-IN

Page 251 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-172512/1-A 12/10/2012 14:30 172512 50 50

LCS 500-172512/2-A 12/10/2012 14:30 172512 50 50

500-53034-3 12/10/2012 14:30 172512 50 50

FORM XII-IN

Page 252 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

LB2 500-172501/1-C 12/11/2012 09:13 172581 50 50

LCS 500-172581/4-A 12/11/2012 09:13 172581 50 50

500-53034-1 12/11/2012 09:13 172581 50 50

FORM XII-IN

Page 253 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

METALS

TestAmerica Chicago

Prep Method: 7471A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-172460/7-A 12/10/2012 15:00 172460 0.6 50

LCS 500-172460/8-A 12/10/2012 15:00 172460 0.6 50

500-53034-1 12/10/2012 15:00 172460 0.6083 50

FORM XII-IN

Page 254 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-172640/7-A 12/11/2012 15:00 172640 25 25

LCS 500-172640/8-A 12/11/2012 15:00 172640 25 25

LB2 500-172501/1-D 12/11/2012 15:00 172640 25 25

500-53034-1 12/11/2012 15:00 172640 25 25

FORM XII-IN

Page 255 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-172642/7-A 12/11/2012 15:00 172642 25 25

LCS 500-172642/8-A 12/11/2012 15:00 172642 25 25

500-53034-3 12/11/2012 15:00 172642 25 25

FORM XII-IN

Page 256 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

ICP5

12/10/2012 14:39 12/10/2012 22:49

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 14:39

ZZZZZZ 14:45

ZZZZZZ 14:52

ZZZZZZ 14:58

ZZZZZZ 15:04

ZZZZZZ 15:09

ZZZZZZ 15:14

ZZZZZZ 15:22

ZZZZZZ 15:30

ICV 500-172535/10 1 15:39 X X X X X X X

ICB 500-172535/11 1 15:47 X X X X X X X

CRI 500-172535/12 1 15:53 X X X X X X X

ICSA 500-172535/13 1 16:00 X X X X X X X

ICSAB 500-172535/14 1 16:06 X X X X X X X

CCV 500-172535/15 16:14

CCB 500-172535/16 16:20

ZZZZZZ 16:27

ZZZZZZ 16:33

ZZZZZZ 16:39

ZZZZZZ 16:45

ZZZZZZ 16:51

ZZZZZZ 16:58

ZZZZZZ 17:04

ZZZZZZ 17:10

ZZZZZZ 17:16

ZZZZZZ 17:22

CCV 500-172535/27 1 17:31 X X X X X X X

CCB 500-172535/28 1 17:37 X X X X X X X

ZZZZZZ 17:43

ZZZZZZ 17:49

ZZZZZZ 17:56

ZZZZZZ 18:02

ZZZZZZ 18:08

MB 500-172306/1-A 1 T 18:21 X X X X X X X

LCS 500-172306/2-A 1 T 18:27 X X X X X X X

ZZZZZZ 18:33

ZZZZZZ 18:40

ZZZZZZ 18:46

CCV 500-172535/39 1 18:54 X X X X X X X

CCB 500-172535/40 1 19:00 X X X X X X X

ZZZZZZ 19:07

ZZZZZZ 19:13

FORM XIII-IN Page 257 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

ICP5

12/10/2012 14:39 12/10/2012 22:49

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 19:19

ZZZZZZ 19:25

ZZZZZZ 19:31

ZZZZZZ 19:38

ZZZZZZ 19:44

ZZZZZZ 19:50

ZZZZZZ 19:56

ZZZZZZ 20:02

CCV 500-172535/51 1 20:11 X X X X X X X

CCB 500-172535/52 1 20:17 X X X X X X X

ZZZZZZ 20:23

ZZZZZZ 20:29

ZZZZZZ 20:36

ZZZZZZ 20:42

ZZZZZZ 20:48

500-53034-1 1 T 20:54 X X X X X X X

ZZZZZZ 21:00

ZZZZZZ 21:13

ZZZZZZ 21:20

ZZZZZZ 21:26

CCV 500-172535/63 1 21:34 X X X X X X X

CCB 500-172535/64 1 21:41 X X X X X X X

ZZZZZZ 21:47

ZZZZZZ 21:53

ZZZZZZ 21:59

ZZZZZZ 22:05

ZZZZZZ 22:12

CRI 500-172535/70 1 22:22 X X X X X X X

ICSA 500-172535/71 1 22:28 X X X X X X X

ICSAB 500-172535/72 1 22:35 X X X X X X X

CCV 500-172535/73 22:43

CCB 500-172535/74 22:49

Prep Types

T = Total/NA

FORM XIII-IN Page 258 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

ICP5

12/11/2012 16:42 12/11/2012 23:22

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 16:42

ZZZZZZ 16:48

ZZZZZZ 16:54

ZZZZZZ 17:01

ZZZZZZ 17:07

ZZZZZZ 17:12

ZZZZZZ 17:17

ZZZZZZ 17:25

ZZZZZZ 17:33

ICV 500-172697/10 1 17:42 X X X X X X X

ICB 500-172697/11 1 17:48 X X X X X X X

CRI 500-172697/12 1 17:54 X X X X X X X

ICSA 500-172697/13 1 18:00 X X X X X X X

ICSAB 500-172697/14 1 18:06 X X X X X X X

CCV 500-172697/15 1 18:15 X X X X X X X

CCB 500-172697/16 1 18:21 X X X X X X X

ZZZZZZ 18:27

LB2 500-172501/1-C 1 P 18:33 X X X X X X X

ZZZZZZ 18:40

LCS 500-172581/4-A 1 T 18:46 X X X X X X X

ZZZZZZ 18:52

ZZZZZZ 18:58

ZZZZZZ 19:04

ZZZZZZ 19:11

ZZZZZZ 19:17

ZZZZZZ 19:23

CCV 500-172697/27 1 19:32 X X X X X X X

CCB 500-172697/28 1 19:38 X X X X X X X

ZZZZZZ 19:44

ZZZZZZ 19:50

ZZZZZZ 19:57

ZZZZZZ 20:03

ZZZZZZ 20:09

ZZZZZZ 20:15

500-53034-1 1 P 20:21 X X X X X X X

ZZZZZZ 20:28

ZZZZZZ 20:34

ZZZZZZ 20:40

CCV 500-172697/39 1 20:49 X X X X X X X

CCB 500-172697/40 1 20:55 X X X X X X X

ZZZZZZ 21:01

ZZZZZZ 21:07

FORM XIII-IN Page 259 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

ICP5

12/11/2012 16:42 12/11/2012 23:22

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 21:13

ZZZZZZ 21:20

ZZZZZZ 21:26

ZZZZZZ 21:32

ZZZZZZ 21:38

ZZZZZZ 21:45

ZZZZZZ 21:51

ZZZZZZ 21:57

CCV 500-172697/51 22:05

CCB 500-172697/52 22:12

ZZZZZZ 22:18

ZZZZZZ 22:24

ZZZZZZ 22:30

ZZZZZZ 22:37

ZZZZZZ 22:43

ZZZZZZ 22:49

ZZZZZZ 22:55

ZZZZZZ 23:01

ZZZZZZ 23:08

CCV 500-172697/62 23:16

CCB 500-172697/63 23:22

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 260 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

ICP6

12/11/2012 15:06 12/11/2012 20:22

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 15:06

ZZZZZZ 15:10

ZZZZZZ 15:14

ZZZZZZ 15:18

ZZZZZZ 15:22

ICV 500-172699/6 1 15:27 X X X X X X X

ICB 500-172699/7 1 15:31 X X X X X X X

ICVL 500-172699/8 15:34

CRI 500-172699/9 1 15:38 X X X X X X X

ICSA 500-172699/10 1 15:42 X X X X X X X

ICSAB 500-172699/11 1 15:47 X X X X X X X

CCV 500-172699/12 15:52

CCB 500-172699/13 15:56

CCVL 500-172699/14 15:59

ZZZZZZ 16:03

ZZZZZZ 16:06

ZZZZZZ 16:10

ZZZZZZ 16:15

ZZZZZZ 16:19

ZZZZZZ 16:23

ZZZZZZ 16:28

ZZZZZZ 16:32

ZZZZZZ 16:36

ZZZZZZ 16:40

CCV 500-172699/25 16:44

CCB 500-172699/26 16:48

CCVL 500-172699/27 16:52

ZZZZZZ 16:56

ZZZZZZ 17:00

ZZZZZZ 17:04

ZZZZZZ 17:08

ZZZZZZ 17:12

ZZZZZZ 17:16

ZZZZZZ 17:20

ZZZZZZ 17:24

ZZZZZZ 17:28

ZZZZZZ 17:32

CCV 500-172699/38 1 17:37 X X X X X X X

CCB 500-172699/39 1 17:41 X X X X X X X

CCVL 500-172699/40 17:45

ZZZZZZ 17:49

ZZZZZZ 17:55

FORM XIII-IN Page 261 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

ICP6

12/11/2012 15:06 12/11/2012 20:22

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 18:00

MB 500-172512/1-A 1 T 18:04 X X X X X X X

LCS 500-172512/2-A 1 T 18:08 X X X X X X X

ZZZZZZ 18:12

ZZZZZZ 18:16

ZZZZZZ 18:20

ZZZZZZ 18:24

ZZZZZZ 18:28

CCV 500-172699/51 1 18:32 X X X X X X X

CCB 500-172699/52 1 18:36 X X X X X X X

CCVL 500-172699/53 18:40

ZZZZZZ 18:44

ZZZZZZ 18:48

ZZZZZZ 18:52

ZZZZZZ 18:56

ZZZZZZ 19:00

ZZZZZZ 19:04

ZZZZZZ 19:08

ZZZZZZ 19:13

ZZZZZZ 19:18

ZZZZZZ 19:22

CCV 500-172699/64 1 19:27 X X X X X X X

CCB 500-172699/65 1 19:31 X X X X X X X

ZZZZZZ 19:35

ZZZZZZ 19:40

ZZZZZZ 19:45

ZZZZZZ 19:49

ZZZZZZ 19:54

ZZZZZZ 19:59

ZZZZZZ 20:05

ZZZZZZ 20:10

500-53034-3 1 T 20:14 X X X X X X X

CCV 500-172699/75 1 20:18 X X X X X X X

CCB 500-172699/76 1 20:22 X X X X X X X

Prep Types

T = Total/NA

FORM XIII-IN Page 262 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

HG6

12/12/2012 08:37 12/12/2012 11:21

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

ZZZZZZ 08:37

ZZZZZZ 08:38

ZZZZZZ 08:40

ZZZZZZ 08:42

ZZZZZZ 08:44

ZZZZZZ 08:47

ICV 500-172764/7 1 08:49 X

ICB 500-172764/8 1 08:52 X

CRA 500-172764/9 1 08:55 X

MB 500-172640/7-A 1 T 08:57 X

LCS 500-172640/8-A 1 T 08:58 X

ZZZZZZ 09:00

ZZZZZZ 09:03

ZZZZZZ 09:05

ZZZZZZ 09:07

ZZZZZZ 09:08

ZZZZZZ 09:10

LB2 500-172501/1-D 1 P 09:12 X

CCV 500-172764/19 1 09:14 X

CCB 500-172764/20 1 09:16 X

ZZZZZZ 09:18

ZZZZZZ 09:20

ZZZZZZ 09:22

ZZZZZZ 09:24

ZZZZZZ 09:26

ZZZZZZ 09:28

ZZZZZZ 09:30

ZZZZZZ 09:32

ZZZZZZ 09:33

ZZZZZZ 09:35

CCV 500-172764/31 1 09:37 X

CCB 500-172764/32 1 09:39 X

500-53034-1 1 P 09:41 X

ZZZZZZ 09:43

ZZZZZZ 09:45

ZZZZZZ 09:47

ZZZZZZ 09:49

ZZZZZZ 09:51

ZZZZZZ 09:52

ZZZZZZ 09:54

ZZZZZZ 09:56

ZZZZZZ 09:58

FORM XIII-IN Page 263 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

HG6

12/12/2012 08:37 12/12/2012 11:21

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

CCV 500-172764/43 1 10:00 X

CCB 500-172764/44 1 10:02 X

ZZZZZZ 10:05

ZZZZZZ 10:07

ZZZZZZ 10:08

ZZZZZZ 10:10

ZZZZZZ 10:12

ZZZZZZ 10:15

ZZZZZZ 10:16

ZZZZZZ 10:18

ZZZZZZ 10:20

ZZZZZZ 10:22

CCV 500-172764/55 10:24

CCB 500-172764/56 10:26

ZZZZZZ 10:28

ZZZZZZ 10:30

ZZZZZZ 10:32

ZZZZZZ 10:34

ZZZZZZ 10:35

ZZZZZZ 10:37

ZZZZZZ 10:39

ZZZZZZ 10:41

ZZZZZZ 10:43

ZZZZZZ 10:45

CCV 500-172764/67 1 10:47 X

CCB 500-172764/68 1 10:48 X

ZZZZZZ 10:51

MB 500-172642/7-A 1 T 10:53 X

LCS 500-172642/8-A 1 T 10:54 X

ZZZZZZ 10:56

ZZZZZZ 10:59

ZZZZZZ 11:01

ZZZZZZ 11:03

ZZZZZZ 11:04

ZZZZZZ 11:06

ZZZZZZ 11:09

CCV 500-172764/79 1 11:11 X

CCB 500-172764/80 1 11:13 X

500-53034-3 1 T 11:15 X

ZZZZZZ 11:17

CCV 500-172764/83 1 11:19 X

CCB 500-172764/84 1 11:21 X FORM XIII-IN Page 264 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

HG6

12/12/2012 08:37 12/12/2012 11:21

7470A

METALS

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 265 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

HG5

12/11/2012 09:16 12/11/2012 13:09

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

STD01REP1 09:16 X

500-172626/1 IC 

STD02REP1 09:18 X

500-172626/2 IC 

STD03REP1 09:20 X

500-172626/3 IC 

STD04REP1 09:22 X

500-172626/4 IC 

STD05REP1 09:23 X

500-172626/5 IC 

STD06REP1 09:25 X

500-172626/6 IC 

ICV 500-172626/7 1 09:37 X

ICB 500-172626/8 1 09:39 X

CRA 500-172626/9 1 09:41 X

ZZZZZZ 09:43

ZZZZZZ 09:44

ZZZZZZ 09:46

ZZZZZZ 09:48

ZZZZZZ 09:50

ZZZZZZ 09:52

ZZZZZZ 09:54

ZZZZZZ 09:56

ZZZZZZ 09:57

CCV 500-172626/19 09:59

CCB 500-172626/20 10:01

ZZZZZZ 10:03

ZZZZZZ 10:05

ZZZZZZ 10:07

ZZZZZZ 10:08

ZZZZZZ 10:10

ZZZZZZ 10:12

ZZZZZZ 10:14

ZZZZZZ 10:16

ZZZZZZ 10:17

ZZZZZZ 10:19

CCV 500-172626/31 10:21

CCV 500-172626/32 10:27

CCV 500-172626/33 10:30

CCB 500-172626/34 10:32

ZZZZZZ 10:34

ZZZZZZ 10:35

ZZZZZZ 10:37

ZZZZZZ 10:39

ZZZZZZ 10:41

FORM XIII-IN Page 266 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

HG5

12/11/2012 09:16 12/11/2012 13:09

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

ZZZZZZ 10:43

ZZZZZZ 10:45

ZZZZZZ 10:47

ZZZZZZ 10:48

ZZZZZZ 10:50

CCV 500-172626/45 1 10:52 X

CCB 500-172626/46 1 10:54 X

ZZZZZZ 10:56

ZZZZZZ 10:58

ZZZZZZ 11:00

ZZZZZZ 11:02

ZZZZZZ 11:04

ZZZZZZ 11:05

MB 500-172460/7-A 1 T 11:07 X

LCS 500-172460/8-A 1 T 11:09 X

ZZZZZZ 11:11

ZZZZZZ 11:13

CCV 500-172626/57 1 11:15 X

CCB 500-172626/58 1 11:17 X

ZZZZZZ 11:19

ZZZZZZ 11:21

ZZZZZZ 11:22

ZZZZZZ 11:24

ZZZZZZ 11:26

ZZZZZZ 11:28

ZZZZZZ 11:30

ZZZZZZ 11:32

ZZZZZZ 11:33

ZZZZZZ 11:35

CCV 500-172626/69 11:37

CCB 500-172626/70 11:39

ZZZZZZ 11:41

ZZZZZZ 11:43

ZZZZZZ 11:45

ZZZZZZ 11:47

ZZZZZZ 11:49

ZZZZZZ 11:51

ZZZZZZ 11:53

ZZZZZZ 11:55

ZZZZZZ 11:57

ZZZZZZ 11:59

CCV 500-172626/81 12:01

FORM XIII-IN Page 267 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

HG5

12/11/2012 09:16 12/11/2012 13:09

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

CCB 500-172626/82 12:03

ZZZZZZ 12:05

ZZZZZZ 12:07

ZZZZZZ 12:08

CCV 500-172626/86 12:10

CCB 500-172626/87 12:12

CCV 500-172626/88 12:31

CCB 500-172626/89 12:33

ZZZZZZ 12:35

ZZZZZZ 12:37

ZZZZZZ 12:39

ZZZZZZ 12:41

ZZZZZZ 12:42

ZZZZZZ 12:44

ZZZZZZ 12:46

ZZZZZZ 12:48

ZZZZZZ 12:50

ZZZZZZ 12:52

CCV 500-172626/100 1 12:54 X

CCB 500-172626/101 1 12:57 X

500-53034-1 1 T 12:59 X

ZZZZZZ 13:01

ZZZZZZ 13:03

ZZZZZZ 13:04

CCV 500-172626/106 1 13:06 X

CCB 500-172626/107 1 13:09 X

Prep Types

T = Total/NA

FORM XIII-IN Page 268 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/07/12 16:22

172306 12/07/12 16:00

Batch Method:

TestAmerica Chicago

3050B

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg InitialAmount FinalAmount M12JSPKIC 00002

CALC NOT SET TO 

RUN

MB 500-172306/1 3050B, 6010B 1 g 100 mL

CALC NOT SET TO 

RUN

LCS 1 g 100 mL 1 mL

500-172306/2

3050B, 6010B

FC Composite 2 CALC NOT SET TO 

RUN

500-53034-A-1 3050B, 6010B T 1.0011 g 100 mL

Batch Notes

Analyst BL

Balance ID C-1966

First End time 1622

Hydrogen peroxide lot number L08A06

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hood ID or number 3

Hot Block ID number 8

Oven, Bath or Block Temperature 1 90 Degrees C

Oven, Bath or Block Temperature 2 90 Degrees C

Pipette ID 1628

First Start time 1600

ID number of the thermometer J59717

Digestion Tube/Cup Lot # MF06LKK01

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 269 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/10/12 15:00

172512 12/10/12 14:30

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12JSPKIC 00002

MB 500-172512/1 3010A, 6010B 50 mL 50 mL

LCS 50 mL 50 mL 0.5 mL

500-172512/2

3010A, 6010B

500-53034-E-3 FC EB 2 3010A, 6010B T 50 mL 50 mL

Batch Notes

First End time 1500

Filter Paper Lot Number 400022

Hot Block ID number 3

Pipette ID 1627

First Start time 1430

ID number of the thermometer C24127

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Degrees C

Uncorrected Temperature 2 90 Degrees C

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 270 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Hudson, Lawrence A

12/11/12 09:43

172581 12/11/12 09:13

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment

LB2 50 mL 50 mL T-724

500-172501/1-A

3010A, 6010B

LCS 50 mL 50 mL 0.5 mL

500-172581/4

3010A, 6010B

500-53034-A-1-C FC Composite 2 3010A, 6010B P 50 mL 50 mL LB2

Batch Notes

Batch Comment T-724/T-728

First End time 0943

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hot Block ID number 4

Pipette ID 1627

First Start time 0913

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

P TCLP

6010B Page 1 of 1

Page 271 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/11/12 17:00

172640 12/11/12 15:00

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-172640/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-172640/8

7470A, 7470A

LB2 25 mL 25 mL

500-172501/1-A

7470A, 7470A

500-53034-A-1-C FC Composite 2 7470A, 7470A P 25 mL 25 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK

Basis Basis Description

P TCLP 7470A Page 1 of 1

Page 272 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/11/12 17:00

172642 12/11/12 15:00

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-172642/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-172642/8

7470A, 7470A

500-53034-E-3 FC EB 2 7470A, 7470A T 25 mL 25 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK

Basis Basis Description

T Total/NA

7470A Page 1 of 1

Page 273 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/10/12 15:30

172460 12/10/12 15:00

Batch Method:

TestAmerica Chicago

7471A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-172460/7 7471A, 7471A 0.6 g 50 mL

LCS 0.6 g 50 mL 0.0001 mL

500-172460/8

7471A, 7471A

500-53034-A-1 FC Composite 2 7471A, 7471A T 0.6083 g 50 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Balance ID c0975

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Blank Soil Lot Number teflon strip_00001

Filter Lot # 21782182

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 2

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 90

Oven, Bath or Block Temperature 2 90

Pipette ID 1631

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Syringe Lot # 1292669

ID number of the thermometer j60025

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

T Total/NA

7471A Page 1 of 1

Page 274 of 360 12/26/2012
GENERAL CHEMISTRY

Page 275 of 360 12/26/2012
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

GENERAL CHEMISTRY

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53034-1

FC Composite 2 500-53034-1 

FC Discrete 2 500-53034-2 

FC EB 2 500-53034-3 

Comments:

Page 276 of 360 12/26/2012
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53034-1

Date Received: 12/07/2012 09:50

500-53034-1

FC Composite 2

Solid Date Sampled: 12/06/2012 14:30

Reporting Basis: DRY

GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 27.4

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent 4.31 3.60 1.40 mg/Kg 1 7196A

57-12-5 Cyanide, Total <1.81 1.81 0.597 mg/Kg 1 9014

18496-25-8 Sulfide 223 86.5 13.8 mg/Kg 1 9034

HEM (Oil & Grease) 21500 1780 788 mg/Kg 1 9071B

FORM IB-IN Page 277 of 360 12/26/2012
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53034-1

Date Received: 12/07/2012 09:50

500-53034-1

FC Composite 2

Solid Date Sampled: 12/06/2012 14:30

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

Sulfide, Reactive <48.6 48.6 3.79 mg/Kg 1 9034

Flashpoint >176 Degrees 

F

40.0 40.0 1 1010

pH 9.02 0.200 0.200 SU 1 9045C

% Moisture 73.0 0.100 0.100 % 1 SM 2540G

Total Solids 27.0 0.100 0.100 % 1 SM 2540G

FORM IB-IN Page 278 of 360 12/26/2012
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53034-3

Date Received: 12/07/2012 09:50

500-53034-1

FC EB 2

Water Date Sampled: 12/06/2012 14:15

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 1 7196A

57-12-5 Cyanide, Total <0.0100 0.0100 0.00331 mg/L 1 9014

Sulfide, Reactive <1.00 1.00 1.00 mg/L 1 9034

HEM (Oil & Grease) <5.35 5.35 1.55 mg/L 1 1664A

18496-25-8 Sulfide <1.00 1.00 0.230 mg/L 1 9034

FORM IB-IN Page 279 of 360 12/26/2012
2-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

Analyst: KD Batch Start Date: 12/07/2012

Reporting Units: mg/L Analytical Batch No.: 172291

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 11:50 Chromium, hexavalent 0.2502 0.250 100 90-110 WSTCR2_00008

 2 ICB 11:50 Chromium, hexavalent <0.0100

 12 CCV 11:56 Chromium, hexavalent 0.4889 0.500 98 90-110 WSTCR1_00008

 13 CCB 11:56 Chromium, hexavalent <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 280 of 360 12/26/2012
2-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

Analyst: APW Batch Start Date: 12/18/2012

Reporting Units: mg/L Analytical Batch No.: 173341

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 15:45 Chromium, hexavalent 0.2699 0.250 108 90-110 WSTCR2_00008

 2 ICB 15:45 Chromium, hexavalent <0.0200

 10 CCV 15:50 Chromium, hexavalent 0.5250 0.500 105 90-110 WSTCR1_00008

 11 CCB 15:51 Chromium, hexavalent <0.0200

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 281 of 360 12/26/2012
2-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

Analyst: EAT Batch Start Date: 12/13/2012

Reporting Units: mg/L Analytical Batch No.: 172923

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 13:20 Cyanide, Total 0.09940 0.100 99 90-110 WSTINCN2_00556

 2 ICB 13:20 Cyanide, Total <0.0100

 13 CCV 13:23 Cyanide, Total 0.1803 0.200 90 90-110 WSTINCN1_00564

 14 CCB 13:24 Cyanide, Total <0.0100

 26 CCV 13:27 Cyanide, Total 0.2052 0.200 103 90-110 WSTINCN1_00564

 27 CCB 13:28 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 282 of 360 12/26/2012
2-IN

Lab Name: Job No.:

SDG No.:

500-53034-1

Analyst: EAT Batch Start Date: 12/14/2012

Reporting Units: mg/L Analytical Batch No.: 173074

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 15:58 Cyanide, Total 0.1097 0.100 110 90-110 WSTINCN2_00557

 2 ICB 15:58 Cyanide, Total <0.0100

 15 CCV 16:01 Cyanide, Total 0.2182 0.200 109 90-110 WSTINCN1_00565

 16 CCB 16:01 Cyanide, Total <0.0100

 26 CCV 16:03 Cyanide, Total 0.2184 0.200 109 90-110 WSTINCN1_00565

 27 CCB 16:03 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 283 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Method Analyte Result Qual Dil

3-IN

500-53034-1

Lab Sample ID Units

TestAmerica Chicago

METHOD BLANK

GENERAL CHEMISTRY

RL

Batch ID: 172888 Date: 12/14/2012 08:00 Prep Batch: 172887 Date: 12/14/2012 05:35

1664A MB 500-172887/1-A HEM (Oil & Grease) <5.00 mg/L 5.00 1

Batch ID: 172291 Date: 12/07/2012 11:51

7196A MB 500-172291/3 Chromium, hexavalent <0.0100 mg/L 0.0100 1

Batch ID: 173341 Date: 12/18/2012 15:46 Prep Batch: 173258 Date: 12/18/2012 10:00

7196A MB 500-173258/1-A Chromium, hexavalent <1.00 mg/Kg 1.00 1

Batch ID: 172923 Date: 12/13/2012 13:20 Prep Batch: 172878 Date: 12/13/2012 10:30

9014 MB 500-172878/1-A Cyanide, Total <0.0100 mg/L 0.0100 1

Batch ID: 173074 Date: 12/14/2012 15:58 Prep Batch: 173012 Date: 12/14/2012 13:25

9014 MB 500-173012/1-A Cyanide, Total <0.500 mg/Kg 0.500 1

Batch ID: 172532 Date: 12/10/2012 23:15 Prep Batch: 172531 Date: 12/10/2012 20:00

9034 MB 500-172531/1-A Sulfide, Reactive <1.00 mg/L 1.00 1

Batch ID: 172533 Date: 12/10/2012 23:15

9034 MB 500-172533/1 Sulfide <1.00 mg/L 1.00 1

Batch ID: 172643 Date: 12/11/2012 12:30 Prep Batch: 172578 Date: 12/11/2012 10:15

9034 MB 500-172578/1-A Sulfide, Reactive <50.0 mg/Kg 50.0 1

Batch ID: 173039 Date: 12/14/2012 15:40 Prep Batch: 172997 Date: 12/14/2012 11:35

9034 MB 500-172997/1-A Sulfide <25.0 mg/Kg 25.0 1

Batch ID: 173330 Date: 12/19/2012 09:20 Prep Batch: 173324 Date: 12/19/2012 05:10

9071B MB 500-173324/1-A HEM (Oil & Grease) <500 mg/Kg 500 1

FORM III-IN

Page 284 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53034-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 172532 Date: 12/10/2012 23:41 Prep Batch: 172531 Date: 12/10/2012 20:18

9034 500-53034-3 Sulfide, Reactive <1.00 mg/L

9034 500-53034-3 

MS 

Sulfide, Reactive 3.434 mg/L 3.60 95 75-125

Batch ID: 172533 Date: 12/10/2012 23:49

9034 500-53034-3 Sulfide <1.00 mg/L

9034 500-53034-3 

MS 

Sulfide 3.428 mg/L 3.60 95 75-125

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 285 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53034-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 172532 Date: 12/10/2012 23:50 Prep Batch: 172531 Date: 12/10/2012 20:24

9034 500-53034-3 

MSD 

Sulfide, Reactive 3.623 mg/L 3.60 101 75-125 5 20

Batch ID: 172533 Date: 12/10/2012 23:54

9034 500-53034-3 

MSD 

Sulfide 3.617 mg/L 3.60 100 75-125 5 20

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 286 of 360 12/26/2012
7A-IN

Job No.: 500-53034-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Solid

TestAmerica Chicago

Batch ID: 173341 Date: 12/18/2012 15:46 Prep Batch: 173258 Date: 12/18/2012 10:00

LCS Source: WSTCR2_00008

7196A LCS 10.0 83

500-173258/2-

A

Chromium, hexavalent 8.252 mg/Kg 80-120

Batch ID: 173341 Date: 12/18/2012 15:47 Prep Batch: 173258 Date: 12/18/2012 10:00

LCS Source: WSTCR13_00623

7196A LCS 1550 104

500-173258/3-

A

Chromium, hexavalent 1601 mg/Kg 80-120

Batch ID: 173074 Date: 12/14/2012 15:58 Prep Batch: 173012 Date: 12/14/2012 13:25

LCS Source: WSTINCN2_00557

9014 LCS 5.00 112

500-173012/2-

A

Cyanide, Total 5.620 mg/Kg 80-120

Batch ID: 172643 Date: 12/11/2012 12:30 Prep Batch: 172578 Date: 12/11/2012 10:19

LCS Source: WSTSF1_00036

9034 LCS 180 96

500-172578/2-

A

Sulfide, Reactive 172.9 mg/Kg 80-120

Batch ID: 173039 Date: 12/14/2012 15:40 Prep Batch: 172997 Date: 12/14/2012 11:35

LCS Source: WSTSF1_00036

9034 LCS 180 100

500-172997/2-

A

Sulfide 179.7 mg/Kg 80-120

Batch ID: 173330 Date: 12/19/2012 09:31 Prep Batch: 173324 Date: 12/19/2012 05:10

LCS Source: 1664 HEM_00060

9071B LCS 4000 102

500-173324/2-

A

HEM (Oil & Grease) 4090 mg/Kg 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 287 of 360 12/26/2012
7A-IN

Job No.: 500-53034-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Water

TestAmerica Chicago

Batch ID: 172888 Date: 12/14/2012 08:03 Prep Batch: 172887 Date: 12/14/2012 05:40

LCS Source: 1664 HEM_00060

1664A LCS 40.0 102 18

500-172887/2-

A

HEM (Oil & Grease) 40.90 mg/L 78-114 7

Batch ID: 172291 Date: 12/07/2012 11:51

LCS Source: WSTCR2_00008

7196A LCS 0.250 99

500-172291/4

Chromium, hexavalent 0.2487 mg/L 85-115

Batch ID: 172923 Date: 12/13/2012 13:20 Prep Batch: 172878 Date: 12/13/2012 10:30

LCS Source: WSTINCN2_00556

9014 LCS 0.100 103

500-172878/2-

A

Cyanide, Total 0.1026 mg/L 80-120

Batch ID: 172533 Date: 12/10/2012 23:19

LCS Source: WSTSF1_00036

9034 LCS 3.60 108

500-172533/2

Sulfide 3.900 mg/L 80-120

Batch ID: 172532 Date: 12/10/2012 23:23 Prep Batch: 172531 Date: 12/10/2012 20:06

LCS Source: WSTSF1_00036

9034 LCS 3.60 109

500-172531/2-

A

Sulfide, Reactive 3.907 mg/L 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 288 of 360 12/26/2012
7A-IN

Job No.: 500-53034-1

LAB CONTROL SAMPLE DUPLICATE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Water

TestAmerica Chicago

Batch ID: 172888 Date: 12/14/2012 08:07 Prep Batch: 172887 Date: 12/14/2012 05:45

LCSD Source: 1664 HEM_00060

1664A LCSD 40.0 96 18

500-172887/3-

A

HEM (Oil & Grease) 38.30 mg/L 78-114 7

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 289 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 10:43

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 290 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:44

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 291 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 14:44

Prep Method: 3060A

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Chromium, hexavalent 1 0.389

FORM IX - IN

Page 292 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:45

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.02 0.00325

FORM IX - IN

Page 293 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:18

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Cyanide, Total 0.5 0.165

FORM IX - IN

Page 294 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:19

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 295 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:22

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 296 of 360 12/26/2012
9-IN

Instrument ID: SPEC5

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:22

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 297 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 16:25

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide, Reactive 50 3.9

FORM IX - IN

Page 298 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 01/02/2006 09:18

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide, Reactive 1 1

FORM IX - IN

Page 299 of 360 12/26/2012
9-IN

Instrument ID: FP4

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1010 MDL Date: 11/11/2005 10:25

Analyte Wavelength/

Mass

RL MDL

(Degrees (Degrees F)

Flashpoint 40 40

FORM IX - IN

Page 300 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1664A MDL Date: 05/29/2012 15:22

Prep Method: 1664A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

HEM (Oil & Grease) 5 1.45

FORM IX - IN

Page 301 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:57

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide 1 0.23

FORM IX - IN

Page 302 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:59

Prep Method: 9030B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide 25 4

FORM IX - IN

Page 303 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9045C MDL Date: 11/01/2005 06:06

Analyte Wavelength/

Mass

RL MDL

(SU) (SU)

pH 0.2 0.2

FORM IX - IN

Page 304 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9071B MDL Date: 05/29/2012 15:24

Prep Method: 9071B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

HEM (Oil & Grease) 500 222

FORM IX - IN

Page 305 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: Moisture MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

Percent Moisture 0.1 0.1

Percent Solids 0.1 0.1

FORM IX - IN

Page 306 of 360 12/26/2012
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53034-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: SM 2540G MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

% Moisture 0.1 0.1

Total Solids 0.1 0.1

FORM IX - IN

Page 307 of 360 12/26/2012
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53034-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

SPEC5

SDG No.:

(mg/L)

05/03/2010 07:21

GENERAL CHEMISTRY

Chromium, hexavalent 0.5 7196A

Cyanide, Total 0.400 9014

FORM XI - IN

Page 308 of 360 12/26/2012
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53034-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

SPEC5

SDG No.:

(mg/L)

05/03/2010 07:27

GENERAL CHEMISTRY

Chromium, hexavalent 1.0 7196A

FORM XI - IN

Page 309 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-172531/1-A 12/10/2012 20:00 172531 250 250

LCS 500-172531/2-A 12/10/2012 20:06 172531 250 250

500-53034-3 12/10/2012 20:12 172531 250 250

500-53034-3 MS 12/10/2012 20:18 172531 250 250

500-53034-3 MSD 12/10/2012 20:24 172531 250 250

FORM XII-IN

Page 310 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-172578/1-A 12/11/2012 10:15 172578 10.0000 10

LCS 500-172578/2-A 12/11/2012 10:19 172578 10.0000 10

500-53034-1 12/11/2012 11:25 172578 10.2965 10

FORM XII-IN

Page 311 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-172878/1-A 12/13/2012 10:30 172878 50 50

LCS 500-172878/2-A 12/13/2012 10:30 172878 50 50

500-53034-3 12/13/2012 10:30 172878 50 50

FORM XII-IN

Page 312 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173012/1-A 12/14/2012 13:25 173012 1.0000 50

LCS 500-173012/2-A 12/14/2012 13:25 173012 1.0000 50

500-53034-1 12/14/2012 13:25 173012 1.0080 50

FORM XII-IN

Page 313 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 3060A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173258/1-A 12/18/2012 10:00 173258 2.5 100

LCS 500-173258/2-A 12/18/2012 10:00 173258 2.5 100

LCS 500-173258/3-A 12/18/2012 10:00 173258 2.5 100

500-53034-1 12/18/2012 10:00 173258 2.5280 100

FORM XII-IN

Page 314 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 1664A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-172887/1-A 12/14/2012 05:35 172887 1000 1000

LCS 500-172887/2-A 12/14/2012 05:40 172887 1000 1000

LCSD 500-172887/3-A 12/14/2012 05:45 172887 1000 1000

500-53034-3 12/14/2012 06:05 172887 934 1000

FORM XII-IN

Page 315 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9030B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-172997/1-A 12/14/2012 11:35 172997 10.00000 10

LCS 500-172997/2-A 12/14/2012 11:35 172997 10.00000 10

500-53034-1 12/14/2012 11:35 172997 10.5360 10

FORM XII-IN

Page 316 of 360 12/26/2012
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53034-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9071B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173324/1-A 12/19/2012 05:10 173324 10 10

LCS 500-173324/2-A 12/19/2012 05:10 173324 10 10

500-53034-1 12/19/2012 05:10 173324 10.2635 10

FORM XII-IN

Page 317 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

SPEC5

12/07/2012 11:50 12/07/2012 11:59

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-172291/1 1 11:50 X

ICB 500-172291/2 1 11:50 X

MB 500-172291/3 1 T 11:51 X

LCS 500-172291/4 1 T 11:51 X

500-53034-3 1 T 11:52 X

ZZZZZZ 11:52

ZZZZZZ 11:53

ZZZZZZ 11:53

ZZZZZZ 11:54

ZZZZZZ 11:54

ZZZZZZ 11:55

CCV 500-172291/12 1 11:56 X

CCB 500-172291/13 1 11:56 X

ZZZZZZ 11:57

ZZZZZZ 11:57

ZZZZZZ 11:58

CCV 500-172291/17 11:58

CCB 500-172291/18 11:59

Prep Types

T = Total/NA

FORM XIII-IN Page 318 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

SPEC5

12/18/2012 15:45 12/18/2012 15:59

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-173341/1 1 15:45 X

ICB 500-173341/2 1 15:45 X

MB 500-173258/1-A 1 T 15:46 X

LCS 500-173258/2-A 1 T 15:46 X

LCS 500-173258/3-A 50 T 15:47 X

500-53034-1 1 T 15:48 X

ZZZZZZ 15:48

ZZZZZZ 15:49

ZZZZZZ 15:50

CCV 500-173341/10 1 15:50 X

CCB 500-173341/11 1 15:51 X

ZZZZZZ 15:52

ZZZZZZ 15:52

ZZZZZZ 15:53

ZZZZZZ 15:54

ZZZZZZ 15:54

ZZZZZZ 15:55

ZZZZZZ 15:56

CCV 500-173341/19 15:56

CCB 500-173341/20 15:57

ZZZZZZ 15:58

CCV 500-173341/22 15:58

CCB 500-173341/23 15:59

Prep Types

T = Total/NA

FORM XIII-IN Page 319 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

SPEC5

12/13/2012 13:20 12/13/2012 13:29

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-172923/1 1 13:20 X

ICB 500-172923/2 1 13:20 X

MB 500-172878/1-A 1 T 13:20 X

LCS 500-172878/2-A 1 T 13:20 X

ZZZZZZ 13:21

ZZZZZZ 13:21

ZZZZZZ 13:21

ZZZZZZ 13:22

ZZZZZZ 13:22

ZZZZZZ 13:22

ZZZZZZ 13:23

ZZZZZZ 13:23

CCV 500-172923/13 1 13:23 X

CCB 500-172923/14 1 13:24 X

ZZZZZZ 13:24

ZZZZZZ 13:24

ZZZZZZ 13:25

ZZZZZZ 13:25

ZZZZZZ 13:25

ZZZZZZ 13:25

ZZZZZZ 13:26

ZZZZZZ 13:26

500-53034-3 1 T 13:26 X

ZZZZZZ 13:27

CCV 500-172923/25 13:27

CCV 500-172923/26 1 13:27 X

CCB 500-172923/27 1 13:28 X

ZZZZZZ 13:28

ZZZZZZ 13:28

ZZZZZZ 13:29

CCV 500-172923/31 13:29

CCB 500-172923/32 13:29

Prep Types

T = Total/NA

FORM XIII-IN Page 320 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

SPEC5

12/14/2012 15:58 12/14/2012 16:03

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-173074/1 1 15:58 X

ICB 500-173074/2 1 15:58 X

MB 500-173012/1-A 1 T 15:58 X

LCS 500-173012/2-A 1 T 15:58 X

ZZZZZZ 15:58

ZZZZZZ 15:59

ZZZZZZ 15:59

ZZZZZZ 15:59

ZZZZZZ 15:59

ZZZZZZ 15:59

ZZZZZZ 16:00

ZZZZZZ 16:00

CCV 500-173074/13 16:00

CCB 500-173074/14 16:00

CCV 500-173074/15 1 16:01 X

CCB 500-173074/16 1 16:01 X

ZZZZZZ 16:01

ZZZZZZ 16:01

ZZZZZZ 16:01

500-53034-1 1 T 16:02 X

ZZZZZZ 16:02

ZZZZZZ 16:02

ZZZZZZ 16:02

ZZZZZZ 16:03

ZZZZZZ 16:03

CCV 500-173074/26 1 16:03 X

CCB 500-173074/27 1 16:03 X

Prep Types

T = Total/NA

FORM XIII-IN Page 321 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/10/2012 23:15 12/10/2012 23:50

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-172531/1-A 1 T 23:15 X

LCS 500-172531/2-A 1 T 23:23 X

500-53034-3 1 T 23:32 X

500-53034-3 MS 1 T 23:41 X

500-53034-3 MSD 1 T 23:50 X

Prep Types

T = Total/NA

FORM XIII-IN Page 322 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/11/2012 12:30 12/11/2012 12:39

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-172578/1-A 1 T 12:30 X

LCS 500-172578/2-A 1 T 12:30 X

ZZZZZZ 12:31

ZZZZZZ 12:31

ZZZZZZ 12:32

ZZZZZZ 12:32

ZZZZZZ 12:33

ZZZZZZ 12:34

ZZZZZZ 12:34

ZZZZZZ 12:35

ZZZZZZ 12:35

ZZZZZZ 12:36

ZZZZZZ 12:37

ZZZZZZ 12:37

ZZZZZZ 12:38

ZZZZZZ 12:38

500-53034-1 1 T 12:39 X

Prep Types

T = Total/NA

FORM XIII-IN Page 323 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

FP4

12/19/2012 14:45 12/19/2012 18:00

1010

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

F

P

T

y

p

e

ZZZZZZ 14:45

500-53034-1 1 T 15:24 X

ZZZZZZ 16:03

ZZZZZZ 16:42

ZZZZZZ 17:21

ZZZZZZ 18:00

Prep Types

T = Total/NA

FORM XIII-IN Page 324 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/14/2012 08:00 12/14/2012 09:16

1664A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-172887/1-A 1 T 08:00 X

LCS 500-172887/2-A 1 T 08:03 X

LCSD 500-172887/3-A 1 T 08:07 X

ZZZZZZ 08:10

ZZZZZZ 08:14

ZZZZZZ 08:18

500-53034-3 1 T 08:21 X

ZZZZZZ 08:25

ZZZZZZ 08:29

ZZZZZZ 08:32

ZZZZZZ 08:36

ZZZZZZ 08:39

ZZZZZZ 08:43

ZZZZZZ 08:47

ZZZZZZ 08:50

ZZZZZZ 08:54

ZZZZZZ 08:58

ZZZZZZ 09:01

ZZZZZZ 09:05

ZZZZZZ 09:09

ZZZZZZ 09:12

ZZZZZZ 09:16

Prep Types

T = Total/NA

FORM XIII-IN Page 325 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/10/2012 23:15 12/10/2012 23:54

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-172533/1 1 T 23:15 X

LCS 500-172533/2 1 T 23:19 X

ZZZZZZ 23:24

ZZZZZZ 23:29

ZZZZZZ 23:34

ZZZZZZ 23:39

500-53034-3 1 T 23:44 X

500-53034-3 MS 1 T 23:49 X

500-53034-3 MSD 1 T 23:54 X

Prep Types

T = Total/NA

FORM XIII-IN Page 326 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/14/2012 15:40 12/14/2012 15:49

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-172997/1-A 1 T 15:40 X

LCS 500-172997/2-A 1 T 15:40 X

ZZZZZZ 15:41

ZZZZZZ 15:42

ZZZZZZ 15:42

ZZZZZZ 15:43

ZZZZZZ 15:44

ZZZZZZ 15:44

ZZZZZZ 15:45

ZZZZZZ 15:46

500-53034-1 1 T 15:46 X

ZZZZZZ 15:47

ZZZZZZ 15:48

ZZZZZZ 15:48

ZZZZZZ 15:49

Prep Types

T = Total/NA

FORM XIII-IN Page 327 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/19/2012 13:35 12/20/2012 17:10

9045C

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

p

H

T

y

p

e

ZZZZZZ 13:35

ZZZZZZ 13:41

ZZZZZZ 13:47

ZZZZZZ 13:53

ZZZZZZ 13:59

ZZZZZZ 18:30

ZZZZZZ 19:29

ZZZZZZ 20:28

ZZZZZZ 21:28

ZZZZZZ 22:27

ZZZZZZ 23:26

ZZZZZZ 00:25

ZZZZZZ 01:24

ZZZZZZ 02:23

ZZZZZZ 03:22

ZZZZZZ 04:22

ZZZZZZ 05:21

500-53034-1 1 T 06:20 X

ZZZZZZ 07:19

ZZZZZZ 08:18

ZZZZZZ 09:17

ZZZZZZ 10:16

ZZZZZZ 11:16

ZZZZZZ 12:15

ZZZZZZ 13:14

ZZZZZZ 14:13

ZZZZZZ 15:12

ZZZZZZ 16:11

ZZZZZZ 17:10

Prep Types

T = Total/NA

FORM XIII-IN Page 328 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/19/2012 09:20 12/19/2012 11:23

9071B

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-173324/1-A 1 T 09:20 X

LCS 500-173324/2-A 1 T 09:31 X

ZZZZZZ 09:42

ZZZZZZ 09:53

ZZZZZZ 10:05

ZZZZZZ 10:16

500-53034-1 1 T 10:27 X

ZZZZZZ 10:38

ZZZZZZ 10:50

ZZZZZZ 11:01

ZZZZZZ 11:12

ZZZZZZ 11:23

Prep Types

T = Total/NA

FORM XIII-IN Page 329 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/07/2012 12:59 12/07/2012 12:59

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

ZZZZZZ 12:59

500-53034-1 1 T 12:59 X X

Prep Types

T = Total/NA

FORM XIII-IN Page 330 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/12/2012 08:37 12/12/2012 13:47

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 08:37

ZZZZZZ 08:37

ZZZZZZ 08:37

ZZZZZZ 08:37

ZZZZZZ 08:37

ZZZZZZ 08:37

ZZZZZZ 08:37

ZZZZZZ 08:56

ZZZZZZ 08:56

ZZZZZZ 08:56

ZZZZZZ 08:56

ZZZZZZ 08:56

ZZZZZZ 08:56

ZZZZZZ 10:10

500-53034-2 1 T 11:11 X X

ZZZZZZ 11:11

ZZZZZZ 13:01

ZZZZZZ 13:01

ZZZZZZ 13:01

ZZZZZZ 13:01

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:27

ZZZZZZ 13:47

Prep Types

T = Total/NA

FORM XIII-IN Page 331 of 360 12/26/2012
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53034-1

NOEQUIP

12/08/2012 15:37 12/08/2012 15:37

SM 2540G

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

M

o

i

s

t

T

S

T

y

p

e

ZZZZZZ 15:37

ZZZZZZ 15:37

ZZZZZZ 15:37

ZZZZZZ 15:37

ZZZZZZ 15:37

500-53034-1 1 T 15:37 X X

Prep Types

T = Total/NA

FORM XIII-IN Page 332 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Deb, Khona

12/07/12 12:00

172291 12/07/12 11:50

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL 100 mL Color Resp. is 

Blank

ICV 25 uL

500-172291/1

7196A

100 mL 100 mL Color Resp. is 

Blank

ICB 

500-172291/2

7196A

100 mL 100 mL Color Resp. is 

Blank

MB 500-172291/3 7196A

100 mL 100 mL Color Resp. is 

Blank

LCS 25 uL

500-172291/4

7196A

FC EB 2 100 mL 100 mL Color Resp. is 

Blank

500-53034-G-3 7196A T

100 mL 100 mL Color Resp. is 

Blank

CCV 50 uL

500-172291/12

7196A

100 mL 100 mL Color Resp. is 

Blank

CCB 

500-172291/13

7196A

Batch Notes

Batch Comment filter paper lot# 100232

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number Hexa Chrome Color Reagent-00007

First End time See Start Date/Time

First Start time See Start Date/Time

Sulfuric Acid Reagent ID Number H2SO4 00007

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 333 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/18/12 11:00

173258 12/18/12 10:00

Batch Method:

TestAmerica Chicago

3060A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount Initial pH Final pH WSTCR13 00623 WSTCR2 00008

MB 500-173258/1 3060A, 7196A 2.5 g 100 mL 13 SU 7.5 SU

LCS 2.5 g 100 mL 13 SU 7.5 SU 25 uL

500-173258/2

3060A, 7196A

LCS 2.5 g 100 mL 13 SU 7.5 SU 100 mL

500-173258/3

3060A, 7196A

500-53034-A-1 FC Composite 2 3060A, 7196A T 2.5280 g 100 mL 13 SU 7.5 SU

Lab Sample ID Client Sample ID Method Chain Basis AnalysisComment

MB 500-173258/1 3060A, 7196A

LCS soluble

500-173258/2

3060A, 7196A

insoluble 

0.0240

LCS 

500-173258/3

3060A, 7196A

500-53034-A-1 FC Composite 2 3060A, 7196A T

Batch Notes

Alkaline Digestion Solution Reagent ID CR6digestion_00028

Batch Comment Filter Paper Lot # 100727

First End time see above

Potassium Chromate Lot # K00741

Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002

Lead Chromate Lot # 15813PE

Lead Chromate Vendor ID Lead(II)Chrom_00001

Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002)

Magnesium Chloride Vendor JT Baker

First Start time see above

Ending Temperature 90 Celsius

Starting Temperature 90 Celsius

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 334 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/18/12 16:00

173341 12/18/12 15:45

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL Color Resp. is 

Blank

ICV 25 uL

500-173341/1

7196A

Color Resp. is 

Blank

ICB 

500-173341/2

7196A

Color Resp. is 

Blank

MB 

500-173258/1-A

7196A

Color Resp. is 

Blank

LCS 

500-173258/2-A

7196A

Color Resp. is 

Blank

LCS 

500-173258/3-A

7196A

FC Composite 2 Color Resp. is 

Blank

500-53034-A-1-J 7196A T

100 mL Color Resp. is 

Blank

CCV 50 uL

500-173341/10

7196A

Color Resp. is 

Blank

CCB 

500-173341/11

7196A

Batch Notes

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number CR+6 ColorRGT_00007

Sulfuric Acid Reagent ID Number H2SO4_00007

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 335 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/13/12 12:00

172878 12/13/12 10:30

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00556

MB 500-172878/1 9010B, 9014 50 mL 50 mL y

LCS 50 mL 50 mL y 500 uL

500-172878/2

9010B, 9014

500-53034-D-3 FC EB 2 9010B, 9014 T 50 mL 50 mL y

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00017

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

9014 Page 1 of 1

Page 336 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/13/12 13:30

172923 12/13/12 13:20

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00564 WSTINCN2 00556

ICV 25 mL 25 mL 250 uL

500-172923/1

9014

CCV 25 mL 25 mL 500 uL

500-172923/13

9014

CCV 25 mL 25 mL 500 uL

500-172923/26

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

9014 Page 1 of 1

Page 337 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/14/12 14:55

173012 12/14/12 13:25

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00557

MB 500-173012/1 9010B, 9014 1.0000 g 50 mL y

LCS 1.0000 g 50 mL y 500 uL

500-173012/2

9010B, 9014

500-53034-A-1 FC Composite 2 9010B, 9014 T 1.0080 g 50 mL y

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00017

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

9014 Page 1 of 1

Page 338 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/14/12 16:04

173074 12/14/12 15:58

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00565 WSTINCN2 00557

ICV 25 mL 25 mL 250 uL

500-173074/1

9014

CCV 25 mL 25 mL 500 uL

500-173074/15

9014

CCV 25 mL 25 mL 500 uL

500-173074/26

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

9014 Page 1 of 1

Page 339 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/10/12 20:30

172531 12/10/12 20:00

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount

MB 500-172531/1 7.3.4, 9034 250 mL 250 mL

LCS 250 mL 250 mL

500-172531/2

7.3.4, 9034

500-53034-F-3 FC EB 2 7.3.4, 9034 T 250 mL 250 mL

500-53034-F-3 FC EB 2 250 mL 250 mL

MS

7.3.4, 9034 T

500-53034-F-3 FC EB 2 250 mL 250 mL

MSD

7.3.4, 9034 T

Batch Notes

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 340 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/10/12 23:59

172532 12/10/12 23:15

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036

MB 250 mL 5 mL 4.90 mL OK 250 mL

500-172531/1-A

9034

LCS 250 mL 5 mL 2.34 mL OK 250 mL 5 mL

500-172531/2-A

9034

500-53034-F-3-A FC EB 2 9034 T 250 mL 5 mL 4.84 mL OK 250 mL

500-53034-F-3-B FC EB 2 250 mL 5 mL 2.64 mL OK 250 mL 5 mL

MS

9034 T

500-53034-F-3-C FC EB 2 250 mL 5 mL 2.52 mL OK 250 mL 5 mL

MSD

9034 T

Batch Notes

Normality of Iodine Solution 0.0237 N

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 341 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/11/12 11:30

172578 12/11/12 10:15

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-172578/1 7.3.4, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-172578/2

7.3.4, 9034

500-53034-A-1 FC Composite 2 7.3.4, 9034 T 10.2965 g 10 mL

Batch Notes

Batch Comment Balance ID # 2489

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 342 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/11/12 12:40

172643 12/11/12 12:30

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount

MB 10 mL 5 mL 4.79 mL OK 10 mL

500-172578/1-A

9034

LCS 10 mL 5 mL 0.33 mL OK 10 mL

500-172578/2-A

9034

500-53034-A-1-F FC Composite 2 9034 T 10 mL 5 mL 4.92 mL OK 10 mL

Batch Notes

Normality of Iodine Solution 0.0232 N

Nominal Amount Used 10 g

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 343 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/19/12 18:40

173558 12/19/12 14:45

Batch Method:

TestAmerica Chicago

1010

Lab Sample ID Client Sample ID Method Chain Basis AnalysisComment

500-53034-A-1 FC Composite 2 1010 T gray-brown clay

Batch Notes

Equipment ID HFP 339

Basis Basis Description

T Total/NA

1010 Page 1 of 1

Page 344 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/14/12 07:25

172887 12/14/12 05:35

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis GrossWeight TareWeight InitialAmount FinalAmount

MB 500-172887/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL

LCS 1390 g 390 g 1000 mL 1000 mL

500-172887/2

1664A, 1664A

LCSD 1390 g 390 g 1000 mL 1000 mL

500-172887/3

1664A, 1664A

500-53034-H-3 FC EB 2 1664A, 1664A T 1321 g 387 g 934 mL 1000 mL

Batch Notes

Batch Comment phase separating filter lot # 6711653

Concentration End Time See end date/time

Concentration Start Time See start date/time

Person's name who did the concentration See analyst name

Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, 

pf-70610210

Evaporator Temperature 50 DEG. Degrees C

Extraction Analyst see analyst name

Sulfuric Acid Lot Number MALG35029

Hexane Lot# HEXANES_00012

Manifold ID 1851

Methanol Lot Number Methanol_00007

Na2SO4 Lot Number Na2SO4_00006

Nominal Amount Used 1000 mL

Sufficient volume for MS/MSD? NO

Basis Basis Description

T Total/NA

1664A Page 1 of 1

Page 345 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/14/12 09:20

172888 12/14/12 08:00

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 1000 mL 1000 mL 14 2.3398 g 2.3409 g 2.3405 g

500-172887/1-A

1664A

LCS 1000 mL 1000 mL 15 6.2984 g 6.3392 g 6.3393 g

500-172887/2-A

1664A

LCSD 1000 mL 1000 mL 16 6.2644 g 6.3031 g 6.3027 g

500-172887/3-A

1664A

500-53034-H-3-A FC EB 2 1664A T 1000 mL 1000 mL 20 2.3874 g 2.3884 g 2.3883 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2 1664 HEM 00060

Pass_0.0005g 0.0011000000000

001 g

0.0007000000000

00145 g

MB 

500-172887/1-A

1664A

Pass_0.0005g 0.0407999999999

999 g

0.0408999999999

997 g

LCS 5 mL

500-172887/2-A

1664A

Pass_0.0005g 0.0386999999999

995 g

0.0382999999999

996 g

LCSD 5 mL

500-172887/3-A

1664A

FC EB 2 Pass_0.0005g 0.0009999999999

9989 g

0.0009000000000

00123 g

500-53034-H-3-A 1664A T

Batch Notes

Balance ID 1634 No Unit

Calibration Check After 2nd Weighing 0.0020 / 0.9999 g

Calibration Check Before 1st Weighing 0.0021 / 1.0000 g

Batch Comment phase separating filter lot # 6711653

Person's name who did the concentration See analst name

Evaporator Temperature 50 Degrees C

Hexane Lot# Hexanes_00012

Methanol Lot Number Methanol_00006

Na2SO4 Lot Number Na2SO4_00006

Silica Gel Lot Number Silica gel_00003 (checked in batch 157954 - 

7/31/12)

Speedvap ID# 1563

Weight Set ID 2495 / 1144

Basis Basis Description

T Total/NA

1664A Page 1 of 1

Page 346 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/10/12 23:59

172533 12/10/12 23:15

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036

MB 500-172533/1 9034 4.90 mL 5 mL 250 mL 250 mL OK

LCS 2.34 mL 5 mL 250 mL 250 mL OK 5 mL

500-172533/2

9034

500-53034-F-3 FC EB 2 9034 T 4.84 mL 5 mL 250 mL 250 mL OK

500-53034-F-3 FC EB 2 2.64 mL 5 mL 250 mL 250 mL OK 5 mL

MS

9034 T

500-53034-F-3 FC EB 2 2.52 mL 5 mL 250 mL 250 mL OK 5 mL

MSD

9034 T

Batch Notes

First End time 23:59

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0237 N

Sodium Thiosulfate Lot Number NO2S2O300008

Sodium Thiosulfate Vendor INHOUSE

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

First Start time 23:15

Sulfuric Acid Reagent ID Number 6NHCL00006

Normality of first Titrant 0.0246 N

Titrant Standardization Date 11/21/12

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 347 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/14/12 14:55

172997 12/14/12 11:35

Batch Method:

TestAmerica Chicago

9030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-172997/1 9030B, 9034 10.00000 g 10 mL

LCS 10.00000 g 10 mL 10 mL

500-172997/2

9030B, 9034

500-53034-A-1 FC Composite 2 9030B, 9034 T 10.5360 g 10 mL

Batch Notes

Batch Comment BAlance ID #2489

Distillation Temperature 70 Degrees C

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014

Sulfuric Acid Reagent ID Number 20% H2SO4_00003

Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 348 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/14/12 15:50

173039 12/14/12 15:40

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount IodineAmount TitrantVolume1 CalcMsg

MB 10 mL 5 mL 4.84 mL OK

500-172997/1-A

9034

LCS 10 mL 5 mL 0.21 mL OK

500-172997/2-A

9034

500-53034-A-1-H FC Composite 2 9034 T 10 mL 5 mL 3.14 mL OK

Batch Notes

HCl Concentration 6N

Lot # of hydrochloric acid 6NHCL00006

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0235 N

Sodium Thiosulfate Reagent ID Number NO2S2O300008

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

Normality of first Titrant 0.0246 N

Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 349 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/19/12 07:35

173324 12/19/12 05:10

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount 1664 HEM 00060

MB 500-173324/1 9071B, 9071B 10 g 10 mL

LCS 10 g 10 mL 5 mL

500-173324/2

9071B, 9071B

500-53034-A-1 FC Composite 2 9071B, 9071B T 10.2635 g 10 mL

Batch Notes

Acid used for pH adjust Lot # J23A13

Balance ID 1634

Concentration End Time See end date / time

Concentration Start Time See start date / time

Evaporator Temperature 50 DEG. C

Filter Paper Lot Number 6711653

Hexane Lot# HEXANES_00012

Na2SO4 Lot Number Na2SO4_00006

Basis Basis Description

T Total/NA

9071B Page 1 of 1

Page 350 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/19/12 11:35

173330 12/19/12 09:20

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 10 mL 10 mL 24 2.3781 g 2.3790 g 2.3791 g

500-173324/1-A

9071B

LCS 10 mL 10 mL 25 2.3332 g 2.3745 g 2.3741 g

500-173324/2-A

9071B

500-53034-A-1-K FC Composite 2 9071B T 10 mL 10 mL 30 2.2995 g 2.3600 g 2.3600 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2

Pass_0.0005g 0.0009000000000

00123 g

0.0010000000000

0033 g

MB 

500-173324/1-A

9071B

Pass_0.0005g 0.0412999999999

997 g

0.0408999999999

997 g

LCS 

500-173324/2-A

9071B

FC Composite 2 Pass_0.0005g 0.0604999999999

998 g

0.0604999999999

998 g

500-53034-A-1-K 9071B T

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0019 / 0.9999

Calibration Check Before 1st Weighing 0.0019 / 0.9999

Evaporator Temperature 50 Celsius

Filter Paper Lot # 6711653

Basis Basis Description

T Total/NA

9071B Page 1 of 1

Page 351 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

172275 12/07/12 12:59 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53034-A-1 FC Composite 2 Moisture T 13 33.89 g 44.24 g 36.73 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/07/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 1315

Date samples were removed from oven 12/08/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 0800

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

Moisture Page 1 of 1

Page 352 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

172720 12/12/12 08:37 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53034-A-2 FC Discrete 2 Moisture T 38 1.26 g 11.39 g 4.17 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/12/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 0900

Date samples were removed from oven 12/13/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 0700

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

Moisture Page 1 of 1

Page 353 of 360 12/26/2012
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53034-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

172359 12/08/12 15:37 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

SM 2540G

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg

FC Composite 2 Not Calculated. 

RunCalculation 

is NULL

500-53034-A-1 SM 2540G T

Batch Notes

Basis Basis Description

T Total/NA

SM 2540G Page 1 of 1

Page 354 of 360 12/26/2012





Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53034-1

Login Number: 53034

Question Answer Comment

Creator: Scott, Sherri L

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 3.3

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

TestAmerica Chicago Page 360 of 360 12/26/2012
ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Chicago

2417 Bond Street

University Park, IL 60484

Tel: (708)534-5200

TestAmerica Job ID: 500-53034-1

Client Project/Site: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, South Carolina 29651

Attn: Mr. Robert Stevens

Authorized for release by:

12/26/2012 4:16:40 PM

Cindy Pritchard

Project Mgmt. Assistant

cindy.pritchard@testamericainc.com

Designee for

Donna Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited

parameters, exceptions are noted in this report. This report may not be reproduced except in full,

and with written approval from the laboratory. For questions please contact the Project Manager

at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is

intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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Table of Contents

Client: Project Integration, Inc

Project/Site: John Deere Des Moines Works (JDDMW)

TestAmerica Job ID: 500-53034-1

Page 2 of 31

TestAmerica Chicago

12/26/2012

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

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Case Narrative

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Job ID: 500-53034-1

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-53034-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/7/2012 9:50 AM; the samples arrived in good condition, properly preserved and, where required, on ice. 

The temperature of the cooler at receipt was 3.3o C.

GC/MS VOA 

Method(s) 8260B: Due to the high concentration of Acetone, the matrix spike / matrix spike duplicate (-2MS/-2MSD) for sample -2 could not 

be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.

No other analytical or quality issues were noted.

Metals 

No analytical or quality issues were noted.

General Chemistry 

No analytical or quality issues were noted.

TestAmerica Chicago Page 3 of 31 12/26/2012

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Detection Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 2 Lab Sample ID: 500-53034-1

Barium ☼

RL

3.64 mg/Kg

MDL

0.433

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

377 B 1 6010B Total/NA

Copper 959 3.64 0.987 mg/Kg 1 ☼ 6010B Total/NA

Chromium 9290 3.64 0.608 mg/Kg 1 ☼ 6010B Total/NA

Nickel 78.7 3.64 0.797 mg/Kg 1 ☼ 6010B Total/NA

Lead 261 B 1.82 0.626 mg/Kg 1 ☼ 6010B Total/NA

Vanadium 158 1.82 0.276 mg/Kg 1 ☼ 6010B Total/NA

Zinc 381 7.28 2.50 mg/Kg 1 ☼ 6010B Total/NA

Copper 0.0355 0.0250 0.0100 mg/L 1 6010B TCLP

Chromium 0.0524 0.0250 0.0100 mg/L 1 6010B TCLP

Nickel 0.646 0.0250 0.0100 mg/L 1 6010B TCLP

Zinc 0.0685 J 0.100 0.0200 mg/L 1 6010B TCLP

Mercury 0.0000559 J B 0.000200 0.0000200 mg/L 1 7470A TCLP

Mercury 0.635 0.0600 0.0229 mg/Kg 1 ☼ 7471A Total/NA

Flashpoint >176 40.0 40.0 Degrees F 1 1010 Total/NA

Chromium, hexavalent 4.31 3.60 1.40 mg/Kg 1 ☼ 7196A Total/NA

Sulfide 223 86.5 13.8 mg/Kg 1 ☼ 9034 Total/NA

pH 9.02 0.200 0.200 SU 1 9045C Total/NA

HEM (Oil & Grease) 21500 1780 788 mg/Kg 1 ☼ 9071B Total/NA

Total Solids 27.0 0.100 0.100 % 1 SM 2540G Total/NA

Client Sample ID: FC Discrete 2 Lab Sample ID: 500-53034-2

2-Butanone (MEK) ☼

RL

17.4 ug/Kg

MDL

6.30

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

72.6 1 8260B Total/NA

Acetone - DL 9130 870 226 ug/Kg 50 ☼ 8260B Total/NA

Client Sample ID: FC EB 2 Lab Sample ID: 500-53034-3

 No Detections

Client Sample ID: Trip Blank Lab Sample ID: 500-53034-4

 No Detections

TestAmerica Chicago

Page 4 of 31 12/26/2012

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Method Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method Method Description Protocol Laboratory

8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI

6010B Metals (ICP) SW846 TAL CHI

7470A Mercury (CVAA) SW846 TAL CHI

7471A Mercury (CVAA) SW846 TAL CHI

1010 Ignitability, Pensky-Martens Closed-Cup Method SW846 TAL CHI

1664A HEM and SGT-HEM 1664A TAL CHI

7196A Chromium, Hexavalent SW846 TAL CHI

9014 Cyanide SW846 TAL CHI

9034 Sulfide, Reactive SW846 TAL CHI

9034 Sulfide, Acid soluble and Insoluble (Titrimetric) SW846 TAL CHI

9045C pH SW846 TAL CHI

9071B HEM and SGT-HEM SW846 TAL CHI

Moisture Percent Moisture EPA TAL CHI

SM 2540G Total, Fixed, and Volatile Solids SM TAL CHI

Protocol References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

TestAmerica Chicago

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Sample Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Lab Sample ID Client Sample ID Matrix Collected Received

500-53034-1 FC Composite 2 Solid 12/06/12 14:30 12/07/12 09:50

500-53034-2 FC Discrete 2 Solid 12/06/12 14:25 12/07/12 09:50

500-53034-3 FC EB 2 Water 12/06/12 14:15 12/07/12 09:50

500-53034-4 Trip Blank Water 12/06/12 00:00 12/07/12 09:50

TestAmerica Chicago

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 2 Lab Sample ID: 500-53034-1

Date Collected: 12/06/12 14:30 Matrix: Solid

Date Received: 12/07/12 09:50 Percent Solids: 27.4

Method: 6010B - Metals (ICP)

RL MDL

Barium 377 B 3.64 0.433 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 959 3.64 0.987 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Chromium 9290 3.64 0.608 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Nickel 78.7 3.64 0.797 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Lead 261 B 1.82 0.626 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Vanadium 158 1.82 0.276 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Zinc 381 7.28 2.50 mg/Kg ☼ 12/07/12 16:00 12/10/12 20:54 1

Method: 6010B - Metals (ICP) - TCLP

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/11/12 09:13 12/11/12 20:21 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.0355 0.0250 0.0100 mg/L 12/11/12 09:13 12/11/12 20:21 1

Chromium 0.0524 0.0250 0.0100 mg/L 12/11/12 09:13 12/11/12 20:21 1

Nickel 0.646 0.0250 0.0100 mg/L 12/11/12 09:13 12/11/12 20:21 1

Lead <0.0500 0.0500 0.00500 mg/L 12/11/12 09:13 12/11/12 20:21 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/11/12 09:13 12/11/12 20:21 1

Zinc 0.0685 J 0.100 0.0200 mg/L 12/11/12 09:13 12/11/12 20:21 1

Method: 7470A - Mercury (CVAA) - TCLP

RL MDL

Mercury 0.0000559 J B 0.000200 0.0000200 mg/L 12/11/12 15:00 12/12/12 09:41 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.635 0.0600 0.0229 mg/Kg ☼ 12/10/12 15:00 12/11/12 12:59 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

Flashpoint >176 40.0 40.0 Degrees F 12/19/12 15:24 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent 4.31 3.60 1.40 mg/Kg ☼ 12/18/12 10:00 12/18/12 15:48 1

Cyanide, Total <1.81 1.81 0.597 mg/Kg ☼ 12/14/12 13:25 12/14/12 16:02 1

Sulfide 223 86.5 13.8 mg/Kg ☼ 12/14/12 11:35 12/14/12 15:46 1

Sulfide, Reactive <48.6 48.6 3.79 mg/Kg 12/11/12 11:25 12/11/12 12:39 1

pH 9.02 0.200 0.200 SU 12/20/12 06:20 1

HEM (Oil & Grease) 21500 1780 788 mg/Kg ☼ 12/19/12 05:10 12/19/12 10:27 1

Total Solids 27.0 0.100 0.100 % 12/08/12 15:37 1

TestAmerica Chicago

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Discrete 2 Lab Sample ID: 500-53034-2

Date Collected: 12/06/12 14:25 Matrix: Solid

Date Received: 12/07/12 09:50 Percent Solids: 28.7

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

2-Butanone (MEK) 72.6 17.4 6.30 ug/Kg ☼ 12/12/12 09:25 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 117 70 - 134 12/12/12 09:25 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 104 75 - 122 12/12/12 09:25 1

4-Bromofluorobenzene (Surr) 97 70 - 122 12/12/12 09:25 1

Dibromofluoromethane 109 75 - 120 12/12/12 09:25 1

Method: 8260B - Volatile Organic Compounds (GC/MS) - DL

RL MDL

Acetone 9130 870 226 ug/Kg ☼ 12/11/12 11:27 12/13/12 22:04 50

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 97 75 - 125 12/11/12 11:27 12/13/12 22:04 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 98 75 - 120 12/11/12 11:27 12/13/12 22:04 50

4-Bromofluorobenzene (Surr) 92 75 - 120 12/11/12 11:27 12/13/12 22:04 50

Dibromofluoromethane 97 75 - 120 12/11/12 11:27 12/13/12 22:04 50

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC EB 2 Lab Sample ID: 500-53034-3

Date Collected: 12/06/12 14:15 Matrix: Water

Date Received: 12/07/12 09:50

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/13/12 15:33 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/13/12 15:33 1

1,2-Dichloroethane-d4 (Surr) 95 75 - 125 12/13/12 15:33 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 98 75 - 120 12/13/12 15:33 1

4-Bromofluorobenzene (Surr) 95 75 - 120 12/13/12 15:33 1

Dibromofluoromethane 95 75 - 120 12/13/12 15:33 1

Method: 6010B - Metals (ICP)

RL MDL

Barium <0.0100 0.0100 0.000440 mg/L 12/10/12 14:30 12/11/12 20:14 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0100 0.0100 0.00106 mg/L 12/10/12 14:30 12/11/12 20:14 1

Chromium <0.0100 0.0100 0.000960 mg/L 12/10/12 14:30 12/11/12 20:14 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/10/12 14:30 12/11/12 20:14 1

Lead <0.00500 0.00500 0.00158 mg/L 12/10/12 14:30 12/11/12 20:14 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/10/12 14:30 12/11/12 20:14 1

Zinc <0.0200 0.0200 0.00472 mg/L 12/10/12 14:30 12/11/12 20:14 1

Method: 7470A - Mercury (CVAA)

RL MDL

Mercury <0.000200 0.000200 0.0000710 mg/L 12/11/12 15:00 12/12/12 11:15 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

HEM (Oil & Grease) <5.35 5.35 1.55 mg/L 12/14/12 06:05 12/14/12 08:21 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/07/12 11:52 1

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/13/12 10:30 12/13/12 13:26 1

Sulfide <1.00 1.00 0.230 mg/L 12/10/12 23:44 1

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/10/12 20:12 12/10/12 23:32 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: Trip Blank Lab Sample ID: 500-53034-4

Date Collected: 12/06/12 00:00 Matrix: Water

Date Received: 12/07/12 09:50

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/13/12 14:15 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/13/12 14:15 1

1,2-Dichloroethane-d4 (Surr) 91 75 - 125 12/13/12 14:15 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 100 75 - 120 12/13/12 14:15 1

4-Bromofluorobenzene (Surr) 93 75 - 120 12/13/12 14:15 1

Dibromofluoromethane 94 75 - 120 12/13/12 14:15 1

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Definitions/Glossary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Qualifiers

GC/MS VOA

Qualifier Description

4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not 

applicable.

Qualifier

E Result exceeded calibration range.

Metals

Qualifier Description

B Compound was found in the blank and sample.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

EDL Estimated Detection Limit

EPA United States Environmental Protection Agency

MDA Minimum detectable activity

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

GC/MS VOA

Prep Batch: 172604

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-2 - DL FC Discrete 2 Total/NA Solid 5030B

Analysis Batch: 172698

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-2 FC Discrete 2 Total/NA Solid 8260B

500-53034-2 MS FC Discrete 2 Total/NA Solid 8260B

500-53034-2 MSD FC Discrete 2 Total/NA Solid 8260B

LCS 500-172698/5 Lab Control Sample Total/NA Solid 8260B

MB 500-172698/4 Method Blank Total/NA Solid 8260B

Analysis Batch: 172879

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-2 - DL FC Discrete 2 Total/NA Solid 8260B 172604

LCS 500-172879/4 Lab Control Sample Total/NA Solid 8260B

MB 500-172879/6 Method Blank Total/NA Solid 8260B

Analysis Batch: 172880

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 8260B

500-53034-4 Trip Blank Total/NA Water 8260B

LCS 500-172880/4 Lab Control Sample Total/NA Water 8260B

MB 500-172880/6 Method Blank Total/NA Water 8260B

Metals

Prep Batch: 172306

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 3050B

LCS 500-172306/2-A Lab Control Sample Total/NA Solid 3050B

MB 500-172306/1-A Method Blank Total/NA Solid 3050B

Prep Batch: 172460

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 7471A

LCS 500-172460/8-A Lab Control Sample Total/NA Solid 7471A

MB 500-172460/7-A Method Blank Total/NA Solid 7471A

Leach Batch: 172501

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 TCLP Solid 1311

LB2 500-172501/1-C LB2 Method Blank TCLP Solid 1311

LB2 500-172501/1-D LB2 Method Blank TCLP Solid 1311

Prep Batch: 172512

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 3010A

LCS 500-172512/2-A Lab Control Sample Total/NA Water 3010A

MB 500-172512/1-A Method Blank Total/NA Water 3010A

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Metals (Continued)

Analysis Batch: 172535

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 6010B 172306

LCS 500-172306/2-A Lab Control Sample Total/NA Solid 6010B 172306

MB 500-172306/1-A Method Blank Total/NA Solid 6010B 172306

Prep Batch: 172581

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 TCLP Solid 3010A 172501

LB2 500-172501/1-C LB2 Method Blank TCLP Solid 3010A 172501

LCS 500-172581/4-A Lab Control Sample Total/NA Solid 3010A

Analysis Batch: 172626

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 7471A 172460

LCS 500-172460/8-A Lab Control Sample Total/NA Solid 7471A 172460

MB 500-172460/7-A Method Blank Total/NA Solid 7471A 172460

Prep Batch: 172640

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 TCLP Solid 7470A 172501

LB2 500-172501/1-D LB2 Method Blank TCLP Solid 7470A 172501

LCS 500-172640/8-A Lab Control Sample Total/NA Solid 7470A

MB 500-172640/7-A Method Blank Total/NA Solid 7470A

Prep Batch: 172642

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 7470A

LCS 500-172642/8-A Lab Control Sample Total/NA Water 7470A

MB 500-172642/7-A Method Blank Total/NA Water 7470A

Analysis Batch: 172697

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 TCLP Solid 6010B 172581

LB2 500-172501/1-C LB2 Method Blank TCLP Solid 6010B 172581

LCS 500-172581/4-A Lab Control Sample Total/NA Solid 6010B 172581

Analysis Batch: 172699

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 6010B 172512

LCS 500-172512/2-A Lab Control Sample Total/NA Water 6010B 172512

MB 500-172512/1-A Method Blank Total/NA Water 6010B 172512

Analysis Batch: 172764

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 TCLP Solid 7470A 172640

500-53034-3 FC EB 2 Total/NA Water 7470A 172642

LB2 500-172501/1-D LB2 Method Blank TCLP Solid 7470A 172640

LCS 500-172640/8-A Lab Control Sample Total/NA Solid 7470A 172640

LCS 500-172642/8-A Lab Control Sample Total/NA Water 7470A 172642

MB 500-172640/7-A Method Blank Total/NA Solid 7470A 172640

MB 500-172642/7-A Method Blank Total/NA Water 7470A 172642

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry

Analysis Batch: 172275

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid Moisture

Analysis Batch: 172291

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 7196A

LCS 500-172291/4 Lab Control Sample Total/NA Water 7196A

MB 500-172291/3 Method Blank Total/NA Water 7196A

Analysis Batch: 172359

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid SM 2540G

Prep Batch: 172531

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 7.3.4

500-53034-3 MS FC EB 2 Total/NA Water 7.3.4

500-53034-3 MSD FC EB 2 Total/NA Water 7.3.4

LCS 500-172531/2-A Lab Control Sample Total/NA Water 7.3.4

MB 500-172531/1-A Method Blank Total/NA Water 7.3.4

Analysis Batch: 172532

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 9034 172531

500-53034-3 MS FC EB 2 Total/NA Water 9034 172531

500-53034-3 MSD FC EB 2 Total/NA Water 9034 172531

LCS 500-172531/2-A Lab Control Sample Total/NA Water 9034 172531

MB 500-172531/1-A Method Blank Total/NA Water 9034 172531

Analysis Batch: 172533

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 9034

500-53034-3 MS FC EB 2 Total/NA Water 9034

500-53034-3 MSD FC EB 2 Total/NA Water 9034

LCS 500-172533/2 Lab Control Sample Total/NA Water 9034

MB 500-172533/1 Method Blank Total/NA Water 9034

Prep Batch: 172578

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 7.3.4

LCS 500-172578/2-A Lab Control Sample Total/NA Solid 7.3.4

MB 500-172578/1-A Method Blank Total/NA Solid 7.3.4

Analysis Batch: 172643

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9034 172578

LCS 500-172578/2-A Lab Control Sample Total/NA Solid 9034 172578

MB 500-172578/1-A Method Blank Total/NA Solid 9034 172578

Analysis Batch: 172720

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-2 FC Discrete 2 Total/NA Solid Moisture

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 172878

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 9010B

LCS 500-172878/2-A Lab Control Sample Total/NA Water 9010B

MB 500-172878/1-A Method Blank Total/NA Water 9010B

Prep Batch: 172887

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 1664A

LCS 500-172887/2-A Lab Control Sample Total/NA Water 1664A

LCSD 500-172887/3-A Lab Control Sample Dup Total/NA Water 1664A

MB 500-172887/1-A Method Blank Total/NA Water 1664A

Analysis Batch: 172888

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 1664A 172887

LCS 500-172887/2-A Lab Control Sample Total/NA Water 1664A 172887

LCSD 500-172887/3-A Lab Control Sample Dup Total/NA Water 1664A 172887

MB 500-172887/1-A Method Blank Total/NA Water 1664A 172887

Analysis Batch: 172923

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-3 FC EB 2 Total/NA Water 9014 172878

LCS 500-172878/2-A Lab Control Sample Total/NA Water 9014 172878

MB 500-172878/1-A Method Blank Total/NA Water 9014 172878

Prep Batch: 172997

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9030B

LCS 500-172997/2-A Lab Control Sample Total/NA Solid 9030B

MB 500-172997/1-A Method Blank Total/NA Solid 9030B

Prep Batch: 173012

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9010B

LCS 500-173012/2-A Lab Control Sample Total/NA Solid 9010B

MB 500-173012/1-A Method Blank Total/NA Solid 9010B

Analysis Batch: 173039

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9034 172997

LCS 500-172997/2-A Lab Control Sample Total/NA Solid 9034 172997

MB 500-172997/1-A Method Blank Total/NA Solid 9034 172997

Analysis Batch: 173074

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9014 173012

LCS 500-173012/2-A Lab Control Sample Total/NA Solid 9014 173012

MB 500-173012/1-A Method Blank Total/NA Solid 9014 173012

Prep Batch: 173258

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 3060A

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 173258 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LCS 500-173258/2-A Lab Control Sample Total/NA Solid 3060A

LCS 500-173258/3-A Lab Control Sample Total/NA Solid 3060A

MB 500-173258/1-A Method Blank Total/NA Solid 3060A

Prep Batch: 173324

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9071B

LCS 500-173324/2-A Lab Control Sample Total/NA Solid 9071B

MB 500-173324/1-A Method Blank Total/NA Solid 9071B

Analysis Batch: 173330

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9071B 173324

LCS 500-173324/2-A Lab Control Sample Total/NA Solid 9071B 173324

MB 500-173324/1-A Method Blank Total/NA Solid 9071B 173324

Analysis Batch: 173341

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 7196A 173258

LCS 500-173258/2-A Lab Control Sample Total/NA Solid 7196A 173258

LCS 500-173258/3-A Lab Control Sample Total/NA Solid 7196A 173258

MB 500-173258/1-A Method Blank Total/NA Solid 7196A 173258

Analysis Batch: 173479

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 9045C

Analysis Batch: 173558

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53034-1 FC Composite 2 Total/NA Solid 1010

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Surrogate Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (70-134) (75-122) (70-122) (75-120)

12DCE TOL BFB DBFM

500-53034-2 117 104 97 109

Percent Surrogate Recovery (Acceptance Limits)

FC Discrete 2

500-53034-2 MS FC Discrete 2 110 108 103 107

500-53034-2 MSD FC Discrete 2 114 107 98 109

LCS 500-172698/5 Lab Control Sample 108 117 108 106

MB 500-172698/4 Method Blank 106 114 107 109

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE DBFM TOL BFB

500-53034-2 - DL 97 97 98 92

Percent Surrogate Recovery (Acceptance Limits)

FC Discrete 2

LCS 500-172879/4 Lab Control Sample 96 97 99 100

MB 500-172879/6 Method Blank 88 90 93 88

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Water Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE TOL BFB DBFM

500-53034-3 95 98 95 95

Percent Surrogate Recovery (Acceptance Limits)

FC EB 2

500-53034-4 Trip Blank 91 100 93 94

LCS 500-172880/4 Lab Control Sample 96 99 100 97

MB 500-172880/6 Method Blank 88 93 88 90

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: MB 500-172698/4 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172698

RL MDL

Acetone <5.00 5.00 2.16 ug/Kg 12/12/12 08:26 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.81 ug/Kg 12/12/12 08:26 1

1,2-Dichloroethane-d4 (Surr) 106 70 - 134 12/12/12 08:26 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 114 75 - 122 12/12/12 08:26 1

4-Bromofluorobenzene (Surr) 107 70 - 122 12/12/12 08:26 1

Dibromofluoromethane 109 75 - 120 12/12/12 08:26 1

Lab Sample ID: LCS 500-172698/5 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172698

Acetone 50.0 47.36 ug/Kg 95 50 - 138

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 47.66 ug/Kg 95 58 - 133

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

108

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 117 75 - 122

4-Bromofluorobenzene (Surr) 108 70 - 122

Dibromofluoromethane 106 75 - 120

Lab Sample ID: 500-53034-2 MS Client Sample ID: FC Discrete 2

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172698

Acetone 10800 174 9517 E 4 ug/Kg ☼ -745 50 - 138

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

2-Butanone (MEK) 72.6 174 176.3 ug/Kg ☼ 60 58 - 133

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

110

MS MS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 108 75 - 122

4-Bromofluorobenzene (Surr) 103 70 - 122

Dibromofluoromethane 107 75 - 120

Lab Sample ID: 500-53034-2 MSD Client Sample ID: FC Discrete 2

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172698

Acetone 10800 174 10570 E 4 ug/Kg ☼ -140 50 - 138 10 30

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

2-Butanone (MEK) 72.6 174 194.9 ug/Kg ☼ 70 58 - 133 10 30

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

114

MSD MSD

%Recovery Qualifier Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: 500-53034-2 MSD Client Sample ID: FC Discrete 2

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172698

Toluene-d8 (Surr) 75 - 122

Surrogate

107

MSD MSD

%Recovery Qualifier Limits

4-Bromofluorobenzene (Surr) 98 70 - 122

Dibromofluoromethane 109 75 - 120

Lab Sample ID: MB 500-172879/6 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172879

RL MDL

Acetone <5.00 5.00 1.30 ug/Kg 12/13/12 13:24 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/Kg 12/13/12 13:24 1

1,2-Dichloroethane-d4 (Surr) 88 75 - 125 12/13/12 13:24 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 93 75 - 120 12/13/12 13:24 1

4-Bromofluorobenzene (Surr) 88 75 - 120 12/13/12 13:24 1

Dibromofluoromethane 90 75 - 120 12/13/12 13:24 1

Lab Sample ID: LCS 500-172879/4 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172879

Acetone 50.0 46.30 ug/Kg 93 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 46.82 ug/Kg 94 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

96

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 99 75 - 120

4-Bromofluorobenzene (Surr) 100 75 - 120

Dibromofluoromethane 97 75 - 120

Lab Sample ID: MB 500-172880/6 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172880

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/13/12 13:24 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/13/12 13:24 1

1,2-Dichloroethane-d4 (Surr) 88 75 - 125 12/13/12 13:24 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 93 75 - 120 12/13/12 13:24 1

4-Bromofluorobenzene (Surr) 88 75 - 120 12/13/12 13:24 1

Dibromofluoromethane 90 75 - 120 12/13/12 13:24 1

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: LCS 500-172880/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172880

Acetone 50.0 46.30 ug/L 93 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 46.82 ug/L 94 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

96

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 99 75 - 120

4-Bromofluorobenzene (Surr) 100 75 - 120

Dibromofluoromethane 97 75 - 120

Method: 6010B - Metals (ICP)

Lab Sample ID: MB 500-172306/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172535 Prep Batch: 172306

RL MDL

Barium 0.1210 J 1.00 0.119 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <1.00 1.00 0.271 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

Chromium <1.00 1.00 0.167 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

Nickel <1.00 1.00 0.219 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

Lead 0.2260 J 0.500 0.172 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

Vanadium <0.500 0.500 0.0759 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

Zinc <2.00 2.00 0.686 mg/Kg 12/07/12 16:00 12/10/12 18:21 1

Lab Sample ID: LCS 500-172306/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172535 Prep Batch: 172306

Barium 200 200.1 mg/Kg 100 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 25.0 25.45 mg/Kg 102 80 - 120

Chromium 20.0 20.13 mg/Kg 101 80 - 120

Nickel 50.0 49.47 mg/Kg 99 80 - 120

Lead 10.0 10.11 mg/Kg 101 80 - 120

Vanadium 50.0 50.49 mg/Kg 101 80 - 120

Zinc 50.0 48.59 mg/Kg 97 80 - 120

Lab Sample ID: MB 500-172512/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172699 Prep Batch: 172512

RL MDL

Barium <0.0100 0.0100 0.000440 mg/L 12/10/12 14:30 12/11/12 18:04 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0100 0.0100 0.00106 mg/L 12/10/12 14:30 12/11/12 18:04 1

Chromium <0.0100 0.0100 0.000960 mg/L 12/10/12 14:30 12/11/12 18:04 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/10/12 14:30 12/11/12 18:04 1

Lead <0.00500 0.00500 0.00158 mg/L 12/10/12 14:30 12/11/12 18:04 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/10/12 14:30 12/11/12 18:04 1

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP) (Continued)

Lab Sample ID: MB 500-172512/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172699 Prep Batch: 172512

RL MDL

Zinc <0.0200 0.0200 0.00472 mg/L 12/10/12 14:30 12/11/12 18:04 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172512/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172699 Prep Batch: 172512

Barium 2.00 1.974 mg/L 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2472 mg/L 99 80 - 120

Chromium 0.200 0.1892 mg/L 95 80 - 120

Nickel 0.500 0.4817 mg/L 96 80 - 120

Lead 0.100 0.09773 mg/L 98 80 - 120

Vanadium 0.500 0.4890 mg/L 98 80 - 120

Zinc 0.500 0.4699 mg/L 94 80 - 120

Lab Sample ID: LCS 500-172581/4-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172697 Prep Batch: 172581

Barium 2.00 1.936 mg/L 97 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2419 mg/L 97 80 - 120

Chromium 0.200 0.1920 mg/L 96 80 - 120

Nickel 0.500 0.4764 mg/L 95 80 - 120

Lead 0.100 0.09745 mg/L 97 80 - 120

Vanadium 0.500 0.4821 mg/L 96 80 - 120

Zinc 0.500 0.4708 mg/L 94 80 - 120

Lab Sample ID: LB2 500-172501/1-C LB2 Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 172697 Prep Batch: 172581

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/11/12 09:13 12/11/12 18:33 1

LB2 LB2

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0250 0.0250 0.0100 mg/L 12/11/12 09:13 12/11/12 18:33 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/11/12 09:13 12/11/12 18:33 1

Nickel <0.0250 0.0250 0.0100 mg/L 12/11/12 09:13 12/11/12 18:33 1

Lead <0.0500 0.0500 0.00500 mg/L 12/11/12 09:13 12/11/12 18:33 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/11/12 09:13 12/11/12 18:33 1

Zinc <0.100 0.100 0.0200 mg/L 12/11/12 09:13 12/11/12 18:33 1

Method: 7470A - Mercury (CVAA)

Lab Sample ID: MB 500-172640/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172764 Prep Batch: 172640

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/11/12 15:00 12/12/12 08:57 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7470A - Mercury (CVAA) (Continued)

Lab Sample ID: LCS 500-172640/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172764 Prep Batch: 172640

Mercury 0.00200 0.002027 mg/L 101 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-172642/7-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172764 Prep Batch: 172642

RL MDL

Mercury <0.000200 0.000200 0.0000710 mg/L 12/11/12 15:00 12/12/12 10:53 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172642/8-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172764 Prep Batch: 172642

Mercury 0.00200 0.002054 mg/L 103 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LB2 500-172501/1-D LB2 Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 172764 Prep Batch: 172640

RL MDL

Mercury 0.00003710 J 0.000200 0.0000200 mg/L 12/11/12 15:00 12/12/12 09:12 1

LB2 LB2

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

Lab Sample ID: MB 500-172460/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172626 Prep Batch: 172460

RL MDL

Mercury <0.0167 0.0167 0.00637 mg/Kg 12/10/12 15:00 12/11/12 11:07 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172460/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172626 Prep Batch: 172460

Mercury 0.167 0.1975 mg/Kg 118 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 1664A - HEM and SGT-HEM

Lab Sample ID: MB 500-172887/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172888 Prep Batch: 172887

RL MDL

HEM (Oil & Grease) <5.00 5.00 1.45 mg/L 12/14/12 05:35 12/14/12 08:00 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 1664A - HEM and SGT-HEM (Continued)

Lab Sample ID: LCS 500-172887/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172888 Prep Batch: 172887

HEM (Oil & Grease) 40.0 40.90 mg/L 102 78 - 114

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LCSD 500-172887/3-A Client Sample ID: Lab Control Sample Dup

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172888 Prep Batch: 172887

HEM (Oil & Grease) 40.0 38.30 mg/L 96 78 - 114 7 18

Analyte

LCSD LCSD

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits RPD Limit

RPD

Method: 7196A - Chromium, Hexavalent

Lab Sample ID: MB 500-172291/3 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172291

RL MDL

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/07/12 11:51 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172291/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172291

Chromium, hexavalent 0.250 0.2487 mg/L 99 85 - 115

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173258/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173341 Prep Batch: 173258

RL MDL

Chromium, hexavalent <1.00 1.00 0.389 mg/Kg 12/18/12 10:00 12/18/12 15:46 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173258/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173341 Prep Batch: 173258

Chromium, hexavalent 10.0 8.252 mg/Kg 83 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LCS 500-173258/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173341 Prep Batch: 173258

Chromium, hexavalent 1550 1601 mg/Kg 104 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9014 - Cyanide

Lab Sample ID: MB 500-172878/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172923 Prep Batch: 172878

RL MDL

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/13/12 10:30 12/13/12 13:20 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172878/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172923 Prep Batch: 172878

Cyanide, Total 0.100 0.1026 mg/L 103 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173012/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173074 Prep Batch: 173012

RL MDL

Cyanide, Total <0.500 0.500 0.165 mg/Kg 12/14/12 13:25 12/14/12 15:58 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173012/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173074 Prep Batch: 173012

Cyanide, Total 5.00 5.620 mg/Kg 112 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9034 - Sulfide, Reactive

Lab Sample ID: MB 500-172531/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172532 Prep Batch: 172531

RL MDL

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/10/12 20:00 12/10/12 23:15 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172531/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172532 Prep Batch: 172531

Sulfide, Reactive 3.60 3.907 mg/L 109 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: 500-53034-3 MS Client Sample ID: FC EB 2

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172532 Prep Batch: 172531

Sulfide, Reactive <1.00 3.60 3.434 mg/L 95 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9034 - Sulfide, Reactive (Continued)

Lab Sample ID: 500-53034-3 MSD Client Sample ID: FC EB 2

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172532 Prep Batch: 172531

Sulfide, Reactive <1.00 3.60 3.623 mg/L 101 75 - 125 5 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Lab Sample ID: MB 500-172578/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172643 Prep Batch: 172578

RL MDL

Sulfide, Reactive <50.0 50.0 3.90 mg/Kg 12/11/12 10:15 12/11/12 12:30 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172578/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 172643 Prep Batch: 172578

Sulfide, Reactive 180 172.9 mg/Kg 96 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)

Lab Sample ID: MB 500-172533/1 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172533

RL MDL

Sulfide <1.00 1.00 0.230 mg/L 12/10/12 23:15 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172533/2 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172533

Sulfide 3.60 3.900 mg/L 108 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: 500-53034-3 MS Client Sample ID: FC EB 2

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172533

Sulfide <1.00 3.60 3.428 mg/L 95 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53034-3 MSD Client Sample ID: FC EB 2

Matrix: Water Prep Type: Total/NA

Analysis Batch: 172533

Sulfide <1.00 3.60 3.617 mg/L 100 75 - 125 5 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)

Lab Sample ID: MB 500-172997/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173039 Prep Batch: 172997

RL MDL

Sulfide <25.0 25.0 4.00 mg/Kg 12/14/12 11:35 12/14/12 15:40 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-172997/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173039 Prep Batch: 172997

Sulfide 180 179.7 mg/Kg 100 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9071B - HEM and SGT-HEM

Lab Sample ID: MB 500-173324/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173330 Prep Batch: 173324

RL MDL

HEM (Oil & Grease) <500 500 222 mg/Kg 12/19/12 05:10 12/19/12 09:20 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173324/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173330 Prep Batch: 173324

HEM (Oil & Grease) 4000 4090 mg/Kg 102 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC Composite 2 Lab Sample ID: 500-53034-1

Date Collected: 12/06/12 14:30 Matrix: Solid

Date Received: 12/07/12 09:50 Percent Solids: 27.4

Prep 3050B 172306 12/07/12 16:00 RL TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Analysis 6010B 1 172535 12/10/12 20:54 TDS TAL CHI

Total/NA Prep 7471A 172460 12/10/12 15:00 BJB TAL CHI

Total/NA Analysis 7471A 1 172626 12/11/12 12:59 BJB TAL CHI

TCLP Leach 1311 172501 12/10/12 14:48 DB TAL CHI

TCLP Prep 3010A 172581 12/11/12 09:13 LAH TAL CHI

TCLP Analysis 6010B 1 172697 12/11/12 20:21 TDS TAL CHI

TCLP Prep 7470A 172640 12/11/12 15:00 BJB TAL CHI

TCLP Analysis 7470A 1 172764 12/12/12 09:41 BJB TAL CHI

Total/NA Analysis Moisture 1 172275 12/07/12 12:59 CMV TAL CHI

Total/NA Analysis SM 2540G 1 172359 12/08/12 15:37 CMV TAL CHI

Total/NA Prep 7.3.4 172578 12/11/12 11:25 CLM TAL CHI

Total/NA Analysis 9034 1 172643 12/11/12 12:39 CLM TAL CHI

Total/NA Prep 9030B 172997 12/14/12 11:35 CLM TAL CHI

Total/NA Analysis 9034 1 173039 12/14/12 15:46 CLM TAL CHI

Total/NA Prep 9010B 173012 12/14/12 13:25 EAT TAL CHI

Total/NA Analysis 9014 1 173074 EAT TAL CHI

12/14/12 16:02

12/14/12 16:02

(Start)

(End)

Total/NA Prep 9071B 173324 12/19/12 05:10 MTB TAL CHI

Total/NA Analysis 9071B 1 173330 12/19/12 10:27 MTB TAL CHI

Total/NA Prep 3060A 173258 12/18/12 10:00 APW TAL CHI

Total/NA Analysis 7196A 1 173341 APW TAL CHI

12/18/12 15:48

12/18/12 15:48

(Start)

(End)

Total/NA Analysis 9045C 1 173479 CLM TAL CHI

12/20/12 06:20

12/20/12 07:19

(Start)

(End)

Total/NA Analysis 1010 1 173558 APW TAL CHI

12/19/12 15:24

12/19/12 16:03

(Start)

(End)

Client Sample ID: FC Discrete 2 Lab Sample ID: 500-53034-2

Date Collected: 12/06/12 14:25 Matrix: Solid

Date Received: 12/07/12 09:50 Percent Solids: 28.7

Analysis 8260B 1 172698 12/12/12 09:25 BDW TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 5030B DL 172604 12/11/12 11:27 BDW TAL CHI

Total/NA Analysis 8260B DL 50 172879 12/13/12 22:04 EA TAL CHI

Total/NA Analysis Moisture 1 172720 12/12/12 11:11 CMV TAL CHI

TestAmerica Chicago

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC EB 2 Lab Sample ID: 500-53034-3

Date Collected: 12/06/12 14:15 Matrix: Water

Date Received: 12/07/12 09:50

Analysis 8260B 1 172880 12/13/12 15:33 EA TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 3010A 172512 12/10/12 14:30 RL TAL CHI

Total/NA Analysis 6010B 1 172699 12/11/12 20:14 PJ TAL CHI

Total/NA Prep 7470A 172642 12/11/12 15:00 BJB TAL CHI

Total/NA Analysis 7470A 1 172764 12/12/12 11:15 BJB TAL CHI

Total/NA Analysis 7196A 1 172291 KD TAL CHI

12/07/12 11:52

12/07/12 11:52

(Start)

(End)

Total/NA Prep 7.3.4 172531 12/10/12 20:12 CLB TAL CHI

Total/NA Analysis 9034 1 172532 12/10/12 23:32 CLB TAL CHI

Total/NA Analysis 9034 1 172533 CLB TAL CHI

12/10/12 23:44

12/10/12 23:49

(Start)

(End)

Total/NA Prep 1664A 172887 12/14/12 06:05 MTB TAL CHI

Total/NA Analysis 1664A 1 172888 12/14/12 08:21 MTB TAL CHI

Total/NA Prep 9010B 172878 12/13/12 10:30 EAT TAL CHI

Total/NA Analysis 9014 1 172923 EAT TAL CHI

12/13/12 13:26

12/13/12 13:27

(Start)

(End)

Client Sample ID: Trip Blank Lab Sample ID: 500-53034-4

Date Collected: 12/06/12 00:00 Matrix: Water

Date Received: 12/07/12 09:50

Analysis 8260B 1 172880 12/13/12 14:15 EA TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

TestAmerica Chicago

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Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53034-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory: TestAmerica Chicago

All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Alabama State Program 4 40461 04-30-13

California NELAP 9 01132CA 04-30-13

Georgia State Program 4 N/A 04-30-13

Georgia State Program 4 939 04-30-13

Hawaii State Program 9 N/A 04-30-13

Illinois NELAP 5 100201 04-30-13

Indiana State Program 5 C-IL-02 04-30-13

Iowa State Program 7 82 05-01-14

Kansas NELAP 7 E-10161 10-31-13

Kentucky State Program 4 90023 12-31-12

Kentucky (UST) State Program 4 66 04-11-13

L-A-B DoD ELAP L2304 01-06-13

L-A-B ISO/IEC 17025 L2304 01-06-13

Louisiana NELAP 6 30720 06-30-13

Massachusetts State Program 1 M-IL035 06-30-13

Mississippi State Program 4 N/A 04-30-13

North Carolina DENR State Program 4 291 12-31-13

North Dakota State Program 8 R-194 04-30-13

Oklahoma State Program 6 8908 08-31-13

South Carolina State Program 4 77001 04-30-13

Texas NELAP 6 T104704252-09-TX 02-28-13

USDA Federal P330-12-00038 02-06-15

Virginia NELAP 3 460142 06-14-13

Wisconsin State Program 5 999580010 08-31-13

Wyoming State Program 8 8TMS-Q 04-30-13

TestAmerica Chicago

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Page 30 of 31 12/26/2012

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Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53034-1

Login Number: 53034

Question Answer Comment

Creator: Scott, Sherri L

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 3.3

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

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