840 S. Main Street  Akron, Ohio 44311-1516

Phone (330) 535-1300  Fax (330) 535-7246

e-mail: aal@aal-inc.com  www.aal-inc.com

AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Aleris Recycling, Inc. - Coldwater, MI

RE: Subpart RRR 114 Request

Coldwater, MI 49036

267 N Fillmore Rd

Gary C. Barnett

American Analytical Laboratories, Inc received a sample(s) on 19-Aug-10 12:00 for the analyses 

presented in the following report.

Please promptly take the time to carefully review this report and call us if you have any questions or 

additional needs. Delays may make it more difficult for us to answer your questions.

We thank you for using our services.

Sincerely, 

Richard E. Moore

American Analytical Laboratories, Inc.

Work Order: 1008107

03-Sep-10 10:59
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Sample ID Laboratory ID Matrix Date Sampled

ANALYTICAL REPORT FOR SAMPLES

Date Received

Particulate FgimrotFurn 1/2 1008107-01 Solid 16-Aug-10 00:00 19-Aug-10 12:00

Clean Lime 1008107-02 Solid 16-Aug-10 00:00 19-Aug-10 12:00

Narrative:

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Analyte Result Limt Batch

Reporting

Units Dilution Prepared Analyzed Method Analyst 

Particulate FgimrotFurn 1/2

1008107-01 (Solid) 16-Aug-10 00:00

Date Sampled

Qualifier

Metals

Arsenic BRL 0.96 mg/kg 20 A008172 31-Aug-10 02-Sep-10 SW 846 6020 AK

Beryllium BRL 0.96 " " " " " " AK

Cadmium 15 0.96 " " " " 02-Sep-10 " AK

Cobalt 12 0.96 " " " " " " AK

Chromium 130 2.5 " 50 " " 02-Sep-10 SW846 6020 AK

SW846 

7471A

Mercury 0.06 0.02 " 1 A008170 31-Aug-10 31-Aug-10 AK

Manganese 800 10 " 200 A008172 31-Aug-10 01-Sep-10 SW846 6020 AK

Nickel 67 1.0 " 20 " " 02-Sep-10 " AK

Lead 170 2.4 " 50 " " 02-Sep-10 SW 846 6020 AK

Antimony 11 0.96 " 20 " " 02-Sep-10 " AK

Selenium BRL 0.96 " " " " " " AK

Wet Chemistry

BRL SW846 

7196A

Hexavalent Chromium 0.50 mg/kg 1 A008154 27-Aug-10 27-Aug-10 RLL

% Solids 98.6 % " A008151 25-Aug-10 25-Aug-10 EPA 160.3 ROZ

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Analyte Result Limt Batch

Reporting

Units Dilution Prepared Analyzed Method Analyst 

Clean Lime

1008107-02 (Solid) 16-Aug-10 00:00

Date Sampled

Qualifier

Metals

Arsenic BRL 0.93 mg/kg 20 A008172 31-Aug-10 02-Sep-10 SW 846 6020 AK

Beryllium BRL 0.93 " " " " " " AK

Cadmium BRL 0.93 " " " " 02-Sep-10 " AK

Cobalt BRL 0.93 " " " " " " AK

Chromium 3.4 1.0 " " " " 02-Sep-10 SW846 6020 AK

BRL SW846 

7471A

Mercury 0.02 " 1 A008170 31-Aug-10 31-Aug-10 AK

Manganese 51 2.5 " 50 A008172 31-Aug-10 01-Sep-10 SW846 6020 AK

Nickel 11 1.0 " 20 " " 02-Sep-10 " AK

Lead BRL 0.93 " " " " 02-Sep-10 SW 846 6020 AK

Antimony BRL 0.93 " " " " 02-Sep-10 " AK

Selenium BRL 0.93 " " " " " " AK

Wet Chemistry

BRL SW846 

7196A

Hexavalent Chromium 0.50 mg/kg 1 A008154 27-Aug-10 27-Aug-10 RLL

% Solids 99.3 % " A008151 25-Aug-10 25-Aug-10 EPA 160.3 ROZ

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Metals - Quality Control

Qualifier

Batch A008170 - SW846 7471A

Blank (A008170-BLK1) Prepared & Analyzed: 31-Aug-10

Mercury BRL 0.02 mg/kg AK

LCS (A008170-BS1) Prepared & Analyzed: 31-Aug-10

Mercury 0.18 0.02 mg/kg 0.167 107 78-122 AK

LCS Dup (A008170-BSD1) Prepared & Analyzed: 31-Aug-10

Mercury 0.17 0.02 mg/kg 0.167 105 78-122 1.94 20 AK

Duplicate (A008170-DUP1) Source: 1008106-01 Prepared & Analyzed: 31-Aug-10

Mercury 0.74 0.03 mg/kg 0.71 4.39 20 AK

Post Spike (A008170-PS1) Source: 1008106-01 Prepared & Analyzed: 31-Aug-10

Mercury 1.0 0.03 mg/kg 0.307 0.71 109 70-130 AK

Post Spike (A008170-PS2) Source: 1008106-01 Prepared & Analyzed: 31-Aug-10

Mercury 1.0 0.03 mg/kg 0.307 0.71 111 70-130 AK

Batch A008172 - EPA 3050 Modified

Blank (A008172-BLK1) Prepared: 31-Aug-10 Analyzed: 02-Sep-10

Beryllium BRL 1.0 mg/kg AK

Antimony BRL 1.0 " AK

Manganese BRL 2.5 " AK

Cobalt BRL 1.0 " AK

Cadmium BRL 1.0 " AK

Selenium BRL 1.0 " AK

Nickel BRL 1.0 " AK

Chromium BRL 1.0 " AK

Lead BRL 1.0 " AK

Arsenic BRL 1.0 " AK

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Metals - Quality Control

Qualifier

Batch A008172 - EPA 3050 Modified

LCS (A008172-BS1) Prepared: 31-Aug-10 Analyzed: 02-Sep-10

Cadmium 47 1.0 mg/kg 50.0 94.5 80-120 AK

Cobalt 47 1.0 " 50.0 93.7 80-120 AK

Chromium 47 1.0 " 50.0 93.9 80-120 AK

Arsenic 47 1.0 " 50.0 94.8 0-120 AK

Manganese 49 2.5 " 50.0 97.2 80-120 AK

Beryllium 47 1.0 " 50.0 94.5 80-120 AK

Selenium 48 1.0 " 50.0 95.9 80-120 AK

Nickel 48 1.0 " 50.0 96.8 80-120 AK

Antimony 50 1.0 " 50.0 99.9 80-120 AK

Lead 46 1.0 " 50.0 93.0 80-120 AK

LCS Dup (A008172-BSD1) Prepared: 31-Aug-10 Analyzed: 02-Sep-10

Chromium 48 1.0 mg/kg 50.0 95.7 80-120 1.96 20 AK

Beryllium 49 1.0 " 50.0 97.2 80-120 2.75 20 AK

Arsenic 49 1.0 " 50.0 97.6 0-120 2.95 20 AK

Cobalt 48 1.0 " 50.0 96.4 80-120 2.86 25 AK

Lead 49 1.0 " 50.0 98.0 80-120 5.30 20 AK

Cadmium 49 1.0 " 50.0 97.8 80-120 3.37 20 AK

Antimony 53 1.0 " 50.0 106 80-120 6.10 20 AK

Manganese 50 2.5 " 50.0 99.3 80-120 2.13 20 AK

Nickel 49 1.0 " 50.0 99.0 80-120 2.28 20 AK

Selenium 51 1.0 " 50.0 102 80-120 5.97 20 AK

Duplicate (A008172-DUP1) Source: 1008105-03 Prepared: 31-Aug-10 Analyzed: 02-Sep-10

Antimony BRL 0.92 mg/kg BRL 20 AK

Cadmium BRL 0.92 " BRL 20 AK

Arsenic 1.1 0.92 " 1.0 7.77 20 AK

Lead BRL 0.92 " BRL 20 AK

Nickel 19 1.0 " 19 1.09 20 AK

Cobalt 1.1 0.92 " 1.1 0.469 20 AK

Beryllium BRL 0.92 " BRL 20 AK

Manganese 140 2.5 " 150 6.83 20 AK

Selenium BRL 0.92 " BRL 20 AK

Chromium 1.3 1.0 " 1.4 3.61 20 AK

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Metals - Quality Control

Qualifier

Batch A008172 - EPA 3050 Modified

Matrix Spike (A008172-MS1) Source: 1008105-03 Prepared: 31-Aug-10 Analyzed: 02-Sep-10

Arsenic 43 0.95 mg/kg 47.4 1.0 88.1 80-120 AK

Antimony 47 0.95 " 47.4 BRL 98.3 80-120 AK

Selenium 39 0.95 " 47.4 BRL 82.7 80-120 AK

Cobalt 45 0.95 " 47.4 1.1 93.2 80-120 AK

Lead 49 0.95 " 47.4 BRL 103 80-120 AK

Manganese 190 2.5 " 47.4 150 95.9 80-120 AK

Cadmium 44 0.95 " 47.4 BRL 93.0 80-120 AK

Nickel 63 1.0 " 47.4 19 92.5 80-120 AK

Chromium 46 1.0 " 47.4 1.4 94.2 80-120 AK

Beryllium 41 0.95 " 47.4 BRL 86.6 80-120 AK

Matrix Spike Dup (A008172-MSD1) Source: 1008105-03 Prepared: 31-Aug-10 Analyzed: 02-Sep-10

Lead 51 1.0 mg/kg 49.8 BRL 103 80-120 5.06 20 AK

Antimony 50 1.0 " 49.8 BRL 100 80-120 6.94 20 AK

Nickel 67 1.0 " 49.8 19 96.7 80-120 6.56 20 AK

Chromium 50 1.0 " 49.8 1.4 97.2 80-120 7.67 20 AK

Selenium 41 1.0 " 49.8 BRL 82.8 80-120 5.04 25 AK

Cadmium 47 1.0 " 49.8 BRL 93.9 80-120 5.84 20 AK

Arsenic 46 1.0 " 49.8 1.0 89.4 80-120 6.18 20 AK

Manganese 200 2.5 " 49.8 150 107 80-120 3.95 20 AK

Cobalt 48 1.0 " 49.8 1.1 94.7 80-120 6.32 20 AK

Beryllium 43 1.0 " 49.8 BRL 86.5 80-120 4.71 20 AK

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Analyst 

Wet Chemistry - Quality Control

Qualifier

Batch A008154 - Alkaline Prep

Blank (A008154-BLK1) Prepared & Analyzed: 27-Aug-10

Hexavalent Chromium BRL 0.50 mg/kg RLL

LCS (A008154-BS1) Prepared & Analyzed: 27-Aug-10

Hexavalent Chromium 9.4 0.50 mg/kg 10.0 94.2 90-110 RLL

Duplicate (A008154-DUP1) Source: 1008106-01 Prepared & Analyzed: 27-Aug-10

Hexavalent Chromium BRL 0.50 mg/kg BRL 10 RLL

Matrix Spike (A008154-MS1) Source: 1008107-01 Prepared & Analyzed: 27-Aug-10

Hexavalent Chromium 9.8 0.50 mg/kg 10.0 BRL 97.7 90-110 RLL

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.
AMERICAN ANALYTICAL LABORATORIES, INC

 ANALYTICAL SCIENCES  AKRON OPERATIONS 

Project:

Project Number:

Project Manager:

Reported:

Aleris Recycling, Inc. - Coldwater, MI

267 N Fillmore Rd Subpart RRR 114 Request

Gary C. Barnett

Subpart RRR 114 Request

Coldwater, MI 49036 03-Sep-10 10:59

Notes and Definitions 

Sample results reported on a dry weight basis

RPD Relative Percent Difference

dry

NR Not Reported

BRL Analyte NOT DETECTED at or above the reporting limit

DET Analyte DETECTED

Reporting Limit - also the lower limit of quantitation (LLOQ). This value

 changes if the standard dilution or concentration of the sample is deviated from

 during sample preparation/analysis. Often it is the lowest linear standard for 

 applicable methods.

American Analytical Laboratories, Inc. - Akron The results in this report apply to the samples analyzed in accordance with the chain of 

custody document. This analytical report must be reproduced in its entirety.