Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.EIA

Facility Code Facility Name Boiler ID Fuel Type 1

10373 Hanford CB1302 petroleum cokeFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

10373 Hanford CB1302 As Received Higher Heating Value 10373 Hanford CB1302 As Received % Moisture 10373 Hanford CB1302 As Received % Ash 10373 Hanford CB1302 As Received % Sulfur 10373 Hanford CB1302 Dry basis Higher Heating Value 10373 Hanford CB1302 Dry basis % Ash 10373 Hanford CB1302 Dry basis % Sulfur 10373 Hanford CB1302 Dry basis Antim ony 10373 Hanford CB1302 Dry basis Arsenic 10373 Hanford CB1302 Dry basis Beryllium 10373 Hanford CB1302 Dry basis Cadmium 10373 Hanford CB1302 Dry basis Chlorine 10373 Hanford CB1302 Dry basis Chromium 10373 Hanford CB1302 Dry basis Cobalt 10373 Hanford CB1302 Dry basis Fluorine 10373 Hanford CB1302 Dry basis Lead 10373 Hanford CB1302 Dry basis Manganese 10373 Hanford CB1302 Dry basis Mercury 10373 Hanford CB1302 Dry basis Nickel 10373 Hanford CB1302 Dry basis SeleniumAnalysis M ethod for each Analyte

(example: ASTM D5865-04)

ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D6721-01 ASTM D 6357 ASTM D 6357 ASTM D6721-96 ASTM D 6357 ASTM D 6357 ASTM D 6722 ASTM D 6357 SW7740EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10373 Hanford CB1302 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 591-7 5/20/2010 5/20/2010 14765.00 Btu/lb 592-8 5/20/2010 5/20/2010 14659.00 Btu/lb 593-9 5/20/2010 5/20/2010 15005.00 Btu/lb 594-10 5/21/2010 5/21/2010 14857.00 Btu/lb 595-11 5/21/2010 5/21/2010 14944.00 Btu/lb 596-12 5/21/2010 5/21/2010 14978.00 Btu/lb 597-13 5/22/2010 5/22/2010 14881.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.66 3.15 3.36 14863 Btu/lb 3.17 3.39 0.77 2.47 3.33 14773 Btu/lb 2.49 3.36 0.69 1.83 3.31 15108 Btu/lb 1.84 3.34 0.77 3.01 3.55 14973 Btu/lb 3.03 3.58 0.66 2.26 3.39 15043 Btu/lb 2.27 3.41 0.62 2.24 3.31 15071 Btu/lb 2.25 3.33 0.68 2.9 3.46 14983 Btu/lb 2.92 3.49Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)

<1 μg/g <1 μg/g <0.2 <1 μg/g <1 μg/g <0.2 <1 μg/g <1 μg/g <0.2 <0.02 μg/gBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units

μg/g <0.2 μg/g 6 μg/g <2 μg/g 3 μg/g μg/g <0.2 μg/g 6 μg/g <2 μg/g 2 μg/g μg/g <0.2 μg/g 5 μg/g <2 μg/g 2 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 0.66 0.77 0.69 771 μg/g <1 μg/g 6 μg/g 0.77 767 μg/g <1 μg/g 7 μg/g 0.66 762 μg/g <1 μg/g 7 μg/g 0.62 0.68 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 11.49 3.17 85.34 86.4 3.35 3.09 3.39 10.87 2.49 86.64 87.39 3.42 3.1 3.36 11.22 1.84 86.94 87.6 3.64 3.13 3.34 11.28 3.03 85.69 86.43 3.57 3.1 3.58 11.36 2.27 86.37 87.1 3.56 3.09 3.41 10.68 2.25 87.07 87.07 3.58 3.1 3.33 11.58 2.92 85.5 86.76 3.56 3.1 3.49 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

0.6 0.24 0.45 0.29 0.57 0.67 0.17EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10373 Hanford CB1302 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 584-1 5/18/2010 5/18/2010 14663.00 Btu/lb 585-2 5/18/2010 5/18/2010 14858.00 Btu/lb 586-3 5/18/2010 5/18/2010 14816.00 Btu/lb 587-4 5/19/2010 5/19/2010 14839.00 Btu/lb 589-5 5/19/2010 5/19/2010 14928.00 Btu/lb 590-6 5/19/2010 5/19/2010 14756.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.73 3.47 3.24 14771 Btu/lb 3.49 3.26 0.78 2.81 3.22 14974 Btu/lb 2.83 3.24 0.75 3.15 3.25 14929 Btu/lb 3.17 3.27 0.81 3.33 3.3 14960 Btu/lb 3.35 3.33 0.77 3.62 3.53 15044 Btu/lb 3.64 3.56 0.69 2.58 3.32 14859 Btu/lb 2.6 3.35Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)

260 ppm 250 ppm 280 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units

<20 ppm <20 ppm <20 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

0.73 10.99 3.49 85.52 85.95 3.39 3.05 3.26 0.78 10.25 2.83 86.92 86.45 3.39 3.08 3.24 0.75 10.96 3.17 86.55 86.55 3.4 3.06 3.27 0.81 10.7 3.35 85.95 85.92 3.35 3.05 3.33 0.77 11.32 3.64 85.04 85.61 3.35 3.11 3.56 0.69 10.38 2.6 87.02 86.94 3.38 3.1 3.35 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 0.86 1.01 0.55 1 0.73 0.63EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10373 Hanford CB1302 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 584-1 5/18/2010 5/18/2010 14663.00 Btu/lb 585-2 5/18/2010 5/18/2010 14858.00 Btu/lb 586-3 5/18/2010 5/18/2010 14816.00 Btu/lb 587-4 5/19/2010 5/19/2010 14839.00 Btu/lb 589-5 5/19/2010 5/19/2010 14928.00 Btu/lb 590-6 5/19/2010 5/19/2010 14756.00 Btu/lb 591-7 5/20/2010 5/20/2010 14765.00 Btu/lb 592-8 5/20/2010 5/20/2010 14659.00 Btu/lb 593-9 5/20/2010 5/20/2010 15005.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.73 3.47 3.24 14771 Btu/lb 3.49 3.26 0.78 2.81 3.22 14974 Btu/lb 2.83 3.24 0.75 3.15 3.25 14929 Btu/lb 3.17 3.27 0.81 3.33 3.3 14960 Btu/lb 3.35 3.33 0.77 3.62 3.53 15044 Btu/lb 3.64 3.56 0.69 2.58 3.32 14859 Btu/lb 2.6 3.35 0.66 3.15 3.36 14863 Btu/lb 3.17 3.39 0.77 2.47 3.33 14773 Btu/lb 2.49 3.36 0.69 1.83 3.31 15108 Btu/lb 1.84 3.34Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)

260 ppm 250 ppm 280 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 0.73 <20 ppm 0.78 <20 ppm 0.75 <20 ppm 0.81 0.77 0.69 0.66 0.77 0.69 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 10.99 3.49 85.52 85.95 3.39 3.05 3.26 0.86 10.25 2.83 86.92 86.45 3.39 3.08 3.24 1.01 10.96 3.17 86.55 86.55 3.4 3.06 3.27 0.55 10.7 3.35 85.95 85.92 3.35 3.05 3.33 1 11.32 3.64 85.04 85.61 3.35 3.11 3.56 0.73 10.38 2.6 87.02 86.94 3.38 3.1 3.35 0.63 11.49 3.17 85.34 86.4 3.35 3.09 3.39 0.6 10.87 2.49 86.64 87.39 3.42 3.1 3.36 0.24 11.22 1.84 86.94 87.6 3.64 3.13 3.34 0.45 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 10373 Hanford CB1302 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 584-1 5/18/2010 5/18/2010 14663.00 Btu/lb 585-2 5/18/2010 5/18/2010 14858.00 Btu/lb 586-3 5/18/2010 5/18/2010 14816.00 Btu/lb 587-4 5/19/2010 5/19/2010 14839.00 Btu/lb 589-5 5/19/2010 5/19/2010 14928.00 Btu/lb 590-6 5/19/2010 5/19/2010 14756.00 Btu/lb 591-7 5/20/2010 5/20/2010 14765.00 Btu/lb 592-8 5/20/2010 5/20/2010 14659.00 Btu/lb 593-9 5/20/2010 5/20/2010 15005.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 0.73 3.47 3.24 14771 Btu/lb 3.49 3.26 0.78 2.81 3.22 14974 Btu/lb 2.83 3.24 0.75 3.15 3.25 14929 Btu/lb 3.17 3.27 0.81 3.33 3.3 14960 Btu/lb 3.35 3.33 0.77 3.62 3.53 15044 Btu/lb 3.64 3.56 0.69 2.58 3.32 14859 Btu/lb 2.6 3.35 0.66 3.15 3.36 14863 Btu/lb 3.17 3.39 0.77 2.47 3.33 14773 Btu/lb 2.49 3.36 0.69 1.83 3.31 15108 Btu/lb 1.84 3.34Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)

260 ppm 250 ppm 280 ppmBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 0.73 <20 ppm 0.78 <20 ppm 0.75 <20 ppm 0.81 0.77 0.69 0.66 0.77 0.69 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 10.99 3.49 85.52 85.95 3.39 3.05 3.26 0.86 10.25 2.83 86.92 86.45 3.39 3.08 3.24 1.01 10.96 3.17 86.55 86.55 3.4 3.06 3.27 0.55 10.7 3.35 85.95 85.92 3.35 3.05 3.33 1 11.32 3.64 85.04 85.61 3.35 3.11 3.56 0.73 10.38 2.6 87.02 86.94 3.38 3.1 3.35 0.63 11.49 3.17 85.34 86.4 3.35 3.09 3.39 0.6 10.87 2.49 86.64 87.39 3.42 3.1 3.36 0.24 11.22 1.84 86.94 87.6 3.64 3.13 3.34 0.45 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm