# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\3362475579673333196\[EPA-HQ-OAR-2013-0290-DRAFT-0051.xls]El Paso-Glost-Emission Calc** Date: 12/1/14

Plant name: Dal Tile Location: FACID: Test date: 12/13-14/2010 UNITID: Equipment: Bisque Roller Kilns (RK-1, RK-2, RK-5, RK-6) Control device: None Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 16.8 157.8 19,500 12.766 1.25E-09 2.8559 9.7069.46E-05 #DIV/0!

2 16.7 144.7 17,578 11.213 1.20E-09 2.7355 8.9688.17E-05 #DIV/0! 3 16.9 153.6 18,485 10.610 1.07E-09 2.4394 8.47677.66E-05 #DIV/0! Average 16.8 152.0 18,521 1.17E-09 2.6769 9.0508.43E-05#DIV/0! #DIV/0! TEQ 1 M23 16.8 157.8 19,500 0.156107 1.53E-11 0.034923 0.118687 1.16E-06 #DIV/0!

2 16.7 144.7 17,578 0.124753 1.33E-11 0.030435 0.0997759.09E-07 #DIV/0! 3 16.9 153.6 18,485 0.123817 1.24E-11 0.028468 0.0989268.94E-07 #DIV/0! Average 16.8 152.0 18,521 1.37E-11 0.031275 0.1057969.87E-07#DIV/0! #DIV/0! Notes: El Paso, TX

1 of 1

### DIOXIN-FURAN PARTICLE CATCH

Measured wt, ng Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Compound Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.593 0.523 0.476 Total TCDD 593 523 476 Total TCDD 593 523 476 Total PeCDD 1.06 0.891 0.735 Total PeCDD 1060 891 735 Total PeCDD 1060 891 735 Total HxCDD 1.24 1.23 1.16 Total HxCDD 1240 1230 1160 Total HxCDD 1240 1230 1160 Total HpCDD 2.21 1.93 1.68 Total HpCDD 2210 1930 1680 Total HpCDD 2210 1930 1680 Total OCDD 7.54 6.56 6.45 Total OCDD 7540 6560 6450 Total OCDD 7540 6560 6450

Total dioxins 12.643 11.134 10.501 Total TCDF 0.0634 0.0338 0.0507 Total TCDF 63.4 33.8 50.7 Total TCDF 63.4 33.8 50.7 Total PeCDF 0.0326 0.0213 0.0308 Total PeCDF 32.6 21.3 30.8 Total PeCDF 32.6 21.3 30.8 Total HxCDF 0.0161 0.0144 0.0116 Total HxCDF 16.1 14.4 11.6 Total HxCDF 16.1 14.4 11.6 Total HpCDF 0.00528 0.0026 0.00742 Total HpCDF 5.28 2.6 7.42 Total HpCDF 5.28< 2.6 7.42 Total OCDF 0.0058 0.0068 0.0081 Total OCDF 5.8 6.8 8.1 Total OCDF < M, U 5.8< U 6.8< M, J, R 8.1

Total furans 0.12318 0.0789 0.10862 TOTAL CDD/CDF 12.76618 11.212910.60962

Measured wt, ng TEQ, ng Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.038 0.029 0.033 0.038 0.029 0.033 1 2,3,7,8-TCDD 38 29 33 2,3,7,8-TCDD < M, R 38< M, R 29< M, R 33 1,2,3,7,8 PeCDD 0.0806 0.0648 0.061 0.0806 0.0648 0.061 1 1,2,3,7,8-PeCDD 80.6 64.8 61 1,2,3,7,8-PeCDD M 80.6 M 64.8 M, R 61 1,2,3,4,7,8 HxCDD 0.0571 0.0463 0.04120.00571 0.004630.00412 0.1 1,2,3,4,7,8-HxCDD 57.1 46.3 41.2 1,2,3,4,7,8-HxCDD 57.1 46.3 41.2 1,2,3,6,7,8 HxCDD 0.0735 0.0583 0.05880.007350.005830.00588 0.1 1,2,3,6,7,8-HxCDD 73.5 58.3 58.8 1,2,3,6,7,8-HxCDD 73.5 58.3 58.8 1,2,3,7,8,9 HxCDD 0.1 0.0868 0.0761 0.01 0.008680.00761 0.1 1,2,3,7,8,9-HxCDD 100 86.8 76.1 1,2,3,7,8,9-HxCDD 100 86.8 76.1 1,2,3,4,6,7,8 HpCDD 0.822 0.729 0.6650.008220.007290.00665 0.01 1,2,3,4,6,7,8-HpCDD 822 729 665 1,2,3,4,6,7,8-HpCDD 822 729 665 Total OCDD 7.54 6.56 6.450.002260.001970.00194 0.0003 OCDD 7540 6560 6450 OCDD 7540 6560 6450 Total CDD congeners 8.7112 7.5742 7.3851 0.15214 0.1222 0.1202 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.007 0.00291 0.00652 0.00070.000290.00065 0.1 2,3,7,8-TCDF 7 2.91 6.52 2,3,7,8-TCDF < M, R 7 M, J 2.91 M 6.52 1,2,3,7,8 PeCDF 0.00387 0.0025 0.003740.00012 7.5E-050.00011 0.03 1,2,3,7,8-PeCDF 3.87 2.5 3.74 1,2,3,7,8-PeCDF M, J 3.87< M, J, R 2.5 J 3.74 2,3,4,7,8 PeCDF 0.00676 0.0037 0.005860.002030.00111 0.00176 0.3 2,3,4,7,8-PeCDF 6.76 3.7 5.86 2,3,4,7,8-PeCDF M, J 6.76< M, J, R 3.7 M, J 5.86 1,2,3,4,7,8 HxCDF 0.00288 0.0028 0.00220.000290.000280.00022 0.1 1,2,3,4,7,8-HxCDF 2.88 2.8 2.2 1,2,3,4,7,8-HxCDF M, J 2.88< M, J, R 2.8< M, J, R 2.2 1,2,3,6,7,8 HxCDF 0.0029 0.00306 0.00260.000290.00031 0.00026 0.1 1,2,3,6,7,8-HxCDF 2.9 3.06 2.6 1,2,3,6,7,8-HxCDF < M, J, R 2.9 M, J 3.06< M, J, R 2.6 2,3,4,6,7,8 HxCDF 0.00282 0.0025 0.00290.000280.000250.00029 0.1 2,3,4,6,7,8-HxCDF 2.82 2.5 2.9 2,3,4,6,7,8-HxCDF M, J 2.82 M, J 2.5< M, J, R 2.9 1,2,3,7,8,9 HxCDF 0.00184 0.0017 0.0021 0.000180.000170.00021 0.1 1,2,3,7,8,9-HxCDF 1.84 1.7 2.1 1,2,3,7,8,9-HxCDF J 1.84< M, U 1.7< U 2.1 1,2,3,4,6,7,8 HpCDF 0.00528 0.0045 0.00742 5.3E-05 4.5E-05 7.4E-05 0.01 1,2,3,4,6,7,8-HpCDF 5.28 4.5 7.42 1,2,3,4,6,7,8-HpCDF M, J 5.28< M, J, R 4.5 M, J 7.42 1,2,3,4,7,8,9 HpCDF 0.0022 0.0026 0.0043 2.2E-05 2.6E-05 4.3E-05 0.01 1,2,3,4,7,8,9-HpCDF 2.2 2.6 4.3 1,2,3,4,7,8,9-HpCDF< M, U 2.2< U 2.6< M, J, R 4.3 Total OCDF 0.0058 0.0068 0.0081 1.7E-06 2E-06 2.4E-06 0.0003 OCDF 5.8 6.8 8.1 OCDF < M, U 5.8< U 6.8< M, J, R 8.1 Total CDF congeners 0.04135 0.03307 0.045740.003960.002560.00362 **TOTAL CDD/CDF (TEQ)** 8.75255 7.60727 7.430840.15611 0.124750.12382

M indicates that a peak has been manually integrated U indicates that this compound was not detected above the MDL J indicates that a target analyte was detected below the LQL R indicates that the ion abundance ratio for this compounds did not meet the acceptance criterion. Measured wt, pg Measured wt, pg Measured wt, pg

Measured wt, pg

EPA-HQ-OAR-2013-0290-DRAFT-0051 El Paso-Bisque D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\3362475579673333196\[EPA-HQ-OAR-2013-0290-DRAFT-0051.xls]El Paso-Glost-Emission Calc** Date: 12/1/14

Plant name: Dal Tile Location: FACID: Test date: 12/15-16/2010 UNITID: Equipment: Glost Roller Kilns (RK-7, RK-8, RK-11, RK-12) Control device: None Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 19.5 114.8 13,758 

# 0.414 5.57E-11 0.1274 1.2382.98E-06 #DIV/0!

2 19.7 112.6 13,992 

# 0.447 6.12E-11 0.1401 1.5583.33E-06 #DIV/0! 3 17.3 117.9 13,858 

# 0.338 4.43E-11 0.1013 0.38572.39E-06 #DIV/0! Average 18.8 115.1 13,869 5.37E-11 0.1229 1.0612.90E-06#DIV/0! #DIV/0! TEQ 1 M23 19.5 114.8 13,758 

# 0.010230 1.37E-12 0.003146 0.0305777.35E-08 #DIV/0!

2 19.7 112.6 13,992 

# 0.008482 1.16E-12 0.002660 0.0295776.32E-08 #DIV/0! 3 17.3 117.9 13,858 

# 0.009380 1.23E-12 0.002809 0.0106996.62E-08 #DIV/0! Average 18.8 115.1 13,869 1.26E-12 0.002872 0.0236186.76E-08#DIV/0! #DIV/0! Notes: El Paso, TX

1 of 1DIOXIN-FURAN PARTICLE CATCH

Measured wt, ng Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Compound Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.00491 0.0019 0.00561 Total TCDD 4.91 1.9 5.61 Total TCDD 4.91 1.9 5.61 Total PeCDD 0.00864 0.0201 0.0114 Total PeCDD 8.64 20.1 11.4 Total PeCDD 8.64 20.1 11.4 Total HxCDD 0.0338 0.0175 0.0191 Total HxCDD 33.8 17.5 19.1 Total HxCDD 33.8 17.5 19.1 Total HpCDD 0.0743 0.0749 0.0668 Total HpCDD 74.3 74.9 66.8 Total HpCDD 74.3 74.9 66.8 Total OCDD 0.267 0.306 0.202 Total OCDD 267 306 202 Total OCDD 267 306 202

Total dioxins 0.38865 0.4204 0.30491 Total TCDF 0.0037 0.0108 0.0077 Total TCDF 3.7 10.8 7.7 Total TCDF < 3.7 10.8 7.7 Total PeCDF 0.00676 0.0035 0.00573 Total PeCDF 6.76 3.5 5.73 Total PeCDF 6.76 3.5 5.73 Total HxCDF 0.00562 0.00248 0.00813 Total HxCDF 5.62 2.48 8.13 Total HxCDF 5.62 2.48 8.13 Total HpCDF 0.0027 0.0023 0.00642 Total HpCDF 2.7 2.3 6.42 Total HpCDF < 2.7 2.3 6.42 Total OCDF 0.0068 0.0073 0.0053 Total OCDF 6.8 7.3 5.3 Total OCDF < U 6.8 < U 7.3 < U 5.3

Total furans 0.02558 0.02638 0.03328 TOTAL CDD/CDF 0.41423 0.44678 0.33819

Measured wt, ng TEQ, ng Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.0032 0.0019 0.0021 0.0032 0.0019 0.0021 1 2,3,7,8-TCDD 3.2 1.9 2.1 2,3,7,8-TCDD < U 3.2 < U 1.9 < U 2.1 1,2,3,7,8 PeCDD 0.00321 0.00314 0.00371 0.00321 0.003140.00371 1 1,2,3,7,8-PeCDD 3.21 3.14 3.71 1,2,3,7,8-PeCDD M, J 3.21 M, J 3.14 M, J 3.71 1,2,3,4,7,8 HxCDD 0.00258 0.0032 0.00230.000260.000320.00023 0.1 1,2,3,4,7,8-HxCDD 2.58 3.2 2.3 1,2,3,4,7,8-HxCDD M, J 2.58 < M, U 3.2 < M, U 2.3 1,2,3,6,7,8 HxCDD 0.0018 0.00318 0.00280.000180.000320.00028 0.1 1,2,3,6,7,8-HxCDD 1.8 3.18 2.8 1,2,3,6,7,8-HxCDD < M, J, R 1.8 M, J 3.18 < M, J, R 2.8 1,2,3,7,8,9 HxCDD 0.0054 0.0035 0.004840.000540.000350.00048 0.1 1,2,3,7,8,9-HxCDD 5.4 3.5 4.84 1,2,3,7,8,9-HxCDD < M, J, R 5.4 < M, J, R 3.5 M, J 4.84 1,2,3,4,6,7,8 HpCDD 0.0326 0.0336 0.02940.000330.000340.00029 0.01 1,2,3,4,6,7,8-HpCDD 32.6 33.6 29.4 1,2,3,4,6,7,8-HpCDD M, J, R 32.6 M 33.6 M 29.4 Total OCDD 0.267 0.306 0.202 8E-05 9.2E-05 6.1E-05 0.0003 OCDD 267 306 202 OCDD 267 306 M 202 Total CDD congeners 0.31579 0.35452 0.247150.007790.006460.00716 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.0037 0.0022 0.00580.000370.000220.00058 0.1 2,3,7,8-TCDF 3.7 2.2 5.8 2,3,7,8-TCDF < U 3.7 < U 2.2 < U 5.8 1,2,3,7,8 PeCDF 0.0019 0.0025 0.0016 5.7E-05 7.5E-05 4.8E-05 0.03 1,2,3,7,8-PeCDF 1.9 2.5 1.6 1,2,3,7,8-PeCDF < M, U 1.9 < U 2.5 < U 1.6 2,3,4,7,8 PeCDF 0.0033 0.0035 0.00260.000990.001050.00078 0.3 2,3,4,7,8-PeCDF 3.3 3.5 2.6 2,3,4,7,8-PeCDF < J, R 3.3 M, J 3.5 < J, R 2.6 1,2,3,4,7,8 HxCDF 0.00289 0.0013 0.00140.000290.000130.00014 0.1 1,2,3,4,7,8-HxCDF 2.89 1.3 1.4 1,2,3,4,7,8-HxCDF M, J 2.89 < U 1.3 < M, J, R 1.4 1,2,3,6,7,8 HxCDF 0.0022 0.0011 0.0020.000220.00011 0.0002 0.1 1,2,3,6,7,8-HxCDF 2.2 1.1 2 1,2,3,6,7,8-HxCDF < M, J, R 2.2 < U 1.1 < M, J, R 2 2,3,4,6,7,8 HxCDF 0.00273 0.00248 0.00270.000270.000250.00027 0.1 2,3,4,6,7,8-HxCDF 2.73 2.48 2.7 2,3,4,6,7,8-HxCDF M, J 2.73 M, J 2.48 < M, J, R 2.7 1,2,3,7,8,9 HxCDF 0.0016 0.0014 0.00130.000160.000140.00013 0.1 1,2,3,7,8,9-HxCDF 1.6 1.4 1.3 1,2,3,7,8,9-HxCDF < U 1.6 < U 1.4 < U 1.3 1,2,3,4,6,7,8 HpCDF 0.0048 0.0028 0.00581 4.8E-05 2.8E-05 5.8E-05 0.01 1,2,3,4,6,7,8-HpCDF 4.8 2.8 5.81 1,2,3,4,6,7,8-HpCDF < J, R 4.8 < M, J, R 2.8 M, J 5.81 1,2,3,4,7,8,9 HpCDF 0.0027 0.0023 0.0014 2.7E-05 2.3E-05 1.4E-05 0.01 1,2,3,4,7,8,9-HpCDF 2.7 2.3 1.4 1,2,3,4,7,8,9-HpCDF < U 2.7 < U 2.3 < M, U 1.4 Total OCDF 0.0068 0.0073 0.0053 2E-06 2.2E-06 1.6E-06 0.0003 OCDF 6.8 7.3 5.3 OCDF < U 6.8 < U 7.3 < U 5.3 Total CDF congeners 0.03262 0.02688 0.02991 0.002440.002030.00222 **TOTAL CDD/CDF (TEQ)** 0.34841 0.3814 0.277060.010230.008480.00938

M indicates that a peak has been manually integrated U indicates that this compound was not detected above the MDL J indicates that a target analyte was detected below the LQL R indicates that the ion abundance ratio for this compounds did not meet the acceptance criterion. Measured wt, pg Measured wt, pg

Measured wt, pg Measured wt, pg

EPA-HQ-OAR-2013-0290-DRAFT-0051 El Paso-Glost D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\3362475579673333196\[EPA-HQ-OAR-2013-0290-DRAFT-0051.xls]El Paso-Glost-Emission Calc** Date: 12/1/14

Plant name: Dal Tile Location: FACID: Test date: 12/13-14/2010 UNITID: Equipment: Tile Dryer Control device: None Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 17.5 165.8 637 1.025 9.54E-11 0.2183 0.8822.36E-07 #DIV/0!

2 17.6 156.0 629 1.191 1.18E-10 0.2697 1.1262.88E-07 #DIV/0! 3 17.4 153.1 618 0.887 8.94E-11 0.2046 0.81482.15E-07 #DIV/0! Average 17.5 158.3 628 1.01E-10 0.2308 0.9412.46E-07#DIV/0! #DIV/0! TEQ 1 M23 17.5 165.8 637 0.007405 6.89E-13 0.001577 0.006372 1.71E-09 #DIV/0!

2 17.6 156.0 629 0.006949 6.87E-13 0.001573 0.006566 1.68E-09 #DIV/0! 3 17.4 153.1 618 0.004470 4.51E-13 0.001031 0.004106 1.08E-09 #DIV/0! Average 17.5 158.3 628 6.09E-13 0.001394 0.005681 1.49E-09#DIV/0! #DIV/0! Notes: El Paso, TX

1 of 1DIOXIN-FURAN PARTICLE CATCH

Measured wt, ng Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Compound Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.0024 0.0012 0.00098 Total TCDD 2.4 1.2 0.98 Total TCDD < 2.4 < 1.2 0.98 Total PeCDD 0.0018 0.0166 0.007 Total PeCDD 1.8 16.6 7 Total PeCDD < 1.8 16.6 7 Total HxCDD 0.0192 0.0235 0.0241 Total HxCDD 19.2 23.5 24.1 Total HxCDD 19.2 23.5 24.1 Total HpCDD 0.134 0.12 0.0942 Total HpCDD 134 120 94.2 Total HpCDD 134 120 94.2 Total OCDD 0.856 1.02 0.751 Total OCDD 856 1020 751 Total OCDD 856 1020 751

Total dioxins 1.0134 1.1813 0.87728 Total TCDF 0.0017 0.00154 0.00167 Total TCDF 1.7 1.54 1.67 Total TCDF < 1.7 1.54 1.67 Total PeCDF 0.0015 0.0011 0.0012 Total PeCDF 1.5 1.1 1.2 Total PeCDF < 1.5 < 1.1 1.2 Total HxCDF 0.0014 0.0012 0.00093 Total HxCDF 1.4 1.2 0.93 Total HxCDF < 1.4 < 1.2 0.93 Total HpCDF 0.0022 0.0016 0.0016 Total HpCDF 2.2 1.6 1.6 Total HpCDF < 2.2 < 1.6 1.6 Total OCDF 0.0049 0.0047 0.0042 Total OCDF 4.9 4.7 4.2 Total OCDF <U 4.9 <U 4.7 <U 4.2

Total furans 0.0117 0.01014 0.0096 TOTAL CDD/CDF 1.0251 1.19144 0.88688

Measured wt, ng TEQ, ng Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.0024 0.0012 0.00098 0.0024 0.00120.00098 1 2,3,7,8-TCDD 2.4 1.2 0.98 2,3,7,8-TCDD <U 2.4 <U 1.2 <U 0.98 1,2,3,7,8 PeCDD 0.0018 0.0027 0.00124 0.0018 0.00270.00124 1 1,2,3,7,8-PeCDD 1.8 2.7 1.24 1,2,3,7,8-PeCDD <M, U 1.8 M, J 2.7 M, J 1.24 1,2,3,4,7,8 HxCDD 0.0039 0.003 0.00170.00039 0.00030.00017 0.1 1,2,3,4,7,8-HxCDD 3.9 3 1.7 1,2,3,4,7,8-HxCDD <U 3.9 <U 3 <U 1.7 1,2,3,6,7,8 HxCDD 0.0035 0.0027 0.00150.000350.000270.00015 0.1 1,2,3,6,7,8-HxCDD 3.5 2.7 1.5 1,2,3,6,7,8-HxCDD <U 3.5 <U 2.7 <M, U 1.5 1,2,3,7,8,9 HxCDD 0.0043 0.0068 0.003920.000430.000680.00039 0.1 1,2,3,7,8,9-HxCDD 4.3 6.8 3.92 1,2,3,7,8,9-HxCDD <M, J, U 4.3 <M, J, R 6.8 M, J 3.92 1,2,3,4,6,7,8 HpCDD 0.0563 0.0552 0.0421 0.000560.000550.00042 0.01 1,2,3,4,6,7,8-HpCDD 56.3 55.2 42.1 1,2,3,4,6,7,8-HpCDD M 56.3 M 55.2 M 42.1 Total OCDD 0.856 1.02 0.751 0.000260.00031 0.00023 0.0003 OCDD 856 1020 751 OCDD 856 1020 M 751 Total CDD congeners 0.9282 1.0916 0.802440.006190.00601 0.00358 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.0017 0.0012 0.00130.000170.000120.00013 0.1 2,3,7,8-TCDF 1.7 1.2 1.3 2,3,7,8-TCDF <U 1.7 <U 1.2 <U 1.3 1,2,3,7,8 PeCDF 0.0015 0.0011 0.0012 4.5E-05 3.3E-05 3.6E-05 0.03 1,2,3,7,8-PeCDF 1.5 1.1 1.2 1,2,3,7,8-PeCDF <U 1.5 <U 1.1 <U 1.2 2,3,4,7,8 PeCDF 0.0015 0.0011 0.00120.000450.000330.00036 0.3 2,3,4,7,8-PeCDF 1.5 1.1 1.2 2,3,4,7,8-PeCDF <U 1.5 <M, U 1.1 <U 1.2 1,2,3,4,7,8 HxCDF 0.0013 0.0011 0.000850.000130.00011 8.5E-05 0.1 1,2,3,4,7,8-HxCDF 1.3 1.1 0.85 1,2,3,4,7,8-HxCDF <U 1.3 <U 1.1 <U 0.85 1,2,3,6,7,8 HxCDF 0.0011 0.00098 0.000760.00011 9.8E-05 7.6E-05 0.1 1,2,3,6,7,8-HxCDF 1.1 0.98 0.76 1,2,3,6,7,8-HxCDF <U 1.1 <U 0.98 <U 0.76 2,3,4,6,7,8 HxCDF 0.0012 0.001 0.00081 0.00012 0.0001 8.1E-05 0.1 2,3,4,6,7,8-HxCDF 1.2 1 0.81 2,3,4,6,7,8-HxCDF <M, U 1.2 <U 1 <U 0.81 1,2,3,7,8,9 HxCDF 0.0014 0.0012 0.000930.000140.00012 9.3E-05 0.1 1,2,3,7,8,9-HxCDF 1.4 1.2 0.93 1,2,3,7,8,9-HxCDF <U 1.4 <U 1.2 <U 0.93 1,2,3,4,6,7,8 HpCDF 0.0027 0.0013 0.0013 2.7E-05 1.3E-05 1.3E-05 0.01 1,2,3,4,6,7,8-HpCDF 2.7 1.3 1.3 1,2,3,4,6,7,8-HpCDF <M, J, R 2.7 <U 1.3 <U 1.3 1,2,3,4,7,8,9 HpCDF 0.0022 0.0016 0.0016 2.2E-05 1.6E-05 1.6E-05 0.01 1,2,3,4,7,8,9-HpCDF 2.2 1.6 1.6 1,2,3,4,7,8,9-HpCDF <U 2.2 <U 1.6 <U 1.6 Total OCDF 0.0049 0.0047 0.0042 1.5E-06 1.4E-06 1.3E-06 0.0003 OCDF 4.9 4.7 4.2 OCDF <U 4.9 <U 4.7 <U 4.2 Total CDF congeners 0.0195 0.01528 0.014150.001220.000940.00089 **TOTAL CDD/CDF (TEQ)** 0.9477 1.10688 0.816590.00741 0.006950.00447

M indicates that a peak has been manually integrated U indicates that this compound was not detected above the MDL J indicates that a target analyte was detected below the LQL R indicates that the ion abundance ratio for this compounds did not meet the acceptance criterion. Measured wt, pg Measured wt, pg

Measured wt, pg Measured wt, pg

EPA-HQ-OAR-2013-0290-DRAFT-0051 El Paso Tile Dry D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\3362475579673333196\[EPA-HQ-OAR-2013-0290-DRAFT-0051.xls]El Paso-Glost-Emission Calc** Date: 12/1/14

Plant name: Dal Tile Location: FACID: Test date: 4/28-29/2011 UNITID: Equipment: Spry Dryer No. 1 Control device: Wet Scrubber Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 18.0 148.8 20,663 31.410 3.26E-09 7.4528 35.9702.62E-04 #DIV/0!

2 17.6 150.0 20,055 36.139 3.72E-09 8.5086 35.4102.90E-04 #DIV/0! 3 17.4 147.1 20,273 26.215 2.75E-09 6.2925 25.06172.17E-04 #DIV/0! Average 17.7 148.6 20,330 3.24E-09 7.4180 32.1472.56E-04#DIV/0! #DIV/0! TEQ 1 M23 18.0 148.8 20,663 0.051535 5.34E-12 0.012228 0.0590174.29E-07 #DIV/0!

2 17.6 150.0 20,055 0.060735 6.25E-12 0.014300 0.0595104.87E-07 #DIV/0! 3 17.4 147.1 20,273 0.041417 4.34E-12 0.009941 0.0395943.42E-07 #DIV/0! Average 17.7 148.6 20,330 5.31E-12 0.012156 0.0527074.20E-07#DIV/0! #DIV/0! Notes: El Paso, TX

1 of 1DIOXIN-FURAN PARTICLE CATCH

Measured wt, ng Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Compound Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.0778 0.0765 0.0504 Total TCDD 77.8 76.5 50.4 Total TCDD 77.8 76.5 50.4 Total PeCDD 0.206 0.236 0.16 Total PeCDD 206 236 160 Total PeCDD 206 236 160 Total HxCDD 0.617 0.65 0.437 Total HxCDD 617 650 437 Total HxCDD 617 650 437 Total HpCDD 1.7 1.97 1.36 Total HpCDD 1700 1970 1360 Total HpCDD 1700 1970 1360 Total OCDD 28.8 33.2 24.2 Total OCDD 28800 33200 24200 Total OCDD 28800 33200 24200

Total dioxins 31.4008 36.1325 26.2074 Total TCDF 0.00094 0.000650.000808 Total TCDF 0.94 0.65 0.808 Total TCDF < 0.94 < 0.65 0.808 Total PeCDF 0.0012 0.00096 0.00083 Total PeCDF 1.2 0.96 0.83 Total PeCDF < 1.2 < 0.96 < 0.83 Total HxCDF 0.00099 0.00066 0.00078 Total HxCDF 0.99 0.66 0.78 Total HxCDF < 0.99 < 0.66 < 0.78 Total HpCDF 0.0015 0.0012 0.0011 Total HpCDF 1.5 1.2 1.1 Total HpCDF < 1.5 < 1.2 < 1.1 Total OCDF 0.00487 0.0032 0.0045 Total OCDF 4.87 3.2 4.5 Total OCDF M, J 4.87 < M, U 3.2 < M, J, R 4.5

Total furans 0.0095 0.006670.008018 TOTAL CDD/CDF 31.410336.1391726.21542

Measured wt, ng TEQ, ng Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.004 0.0048 0.0033 0.004 0.0048 0.0033 1 2,3,7,8-TCDD 4 4.8 3.3 2,3,7,8-TCDD < M, R 4 < M, R 4.8 < M, J, R 3.3 1,2,3,7,8 PeCDD 0.0187 0.0228 0.0149 0.0187 0.0228 0.0149 1 1,2,3,7,8-PeCDD 18.7 22.8 14.9 1,2,3,7,8-PeCDD M, J 18.7 M 22.8 M, J 14.9 1,2,3,4,7,8 HxCDD 0.0213 0.0271 0.01770.002130.00271 0.00177 0.1 1,2,3,4,7,8-HxCDD 21.3 27.1 17.7 1,2,3,4,7,8-HxCDD 21.3 M 27.1 J 17.7 1,2,3,6,7,8 HxCDD 0.0302 0.0343 0.02360.003020.003430.00236 0.1 1,2,3,6,7,8-HxCDD 30.2 34.3 23.6 1,2,3,6,7,8-HxCDD 30.2 M 34.3 23.6 1,2,3,7,8,9 HxCDD 0.0678 0.0766 0.05240.006780.007660.00524 0.1 1,2,3,7,8,9-HxCDD 67.8 76.6 52.4 1,2,3,7,8,9-HxCDD 67.8 M 76.6 52.4 1,2,3,4,6,7,8 HpCDD 0.739 0.873 0.5930.007390.008730.00593 0.01 1,2,3,4,6,7,8-HpCDD 739 873 593 1,2,3,4,6,7,8-HpCDD 739 M 873 593 Total OCDD 28.8 33.2 24.20.008640.009960.00726 0.0003 OCDD 28800 33200 24200 OCDD 28800 33200 24200 Total CDD congeners 29.681 34.2386 24.90490.050660.060090.04076 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.00094 0.000650.000808 9.4E-05 6.5E-05 8.1E-05 0.1 2,3,7,8-TCDF 0.94 0.65 0.808 2,3,7,8-TCDF < U 0.94 < U 0.65 M, J 0.808 1,2,3,7,8 PeCDF 0.0012 0.00095 0.00082 3.6E-05 2.9E-05 2.5E-05 0.03 1,2,3,7,8-PeCDF 1.2 0.95 0.82 1,2,3,7,8-PeCDF < U 1.2 < U 0.95 < U 0.82 2,3,4,7,8 PeCDF 0.0012 0.00096 0.000830.000360.000290.00025 0.3 2,3,4,7,8-PeCDF 1.2 0.96 0.83 2,3,4,7,8-PeCDF < U 1.2 < U 0.96 < U 0.83 1,2,3,4,7,8 HxCDF 0.00091 0.00062 0.00072 9.1E-05 6.2E-05 7.2E-05 0.1 1,2,3,4,7,8-HxCDF 0.91 0.62 0.72 1,2,3,4,7,8-HxCDF < U 0.91 < U 0.62 < U 0.72 1,2,3,6,7,8 HxCDF 0.0008 0.00054 0.000630.00008 5.4E-05 6.3E-05 0.1 1,2,3,6,7,8-HxCDF 0.8 0.54 0.63 1,2,3,6,7,8-HxCDF < U 0.8 < U 0.54 < U 0.63 2,3,4,6,7,8 HxCDF 0.00087 0.00058 0.00069 8.7E-05 5.8E-05 6.9E-05 0.1 2,3,4,6,7,8-HxCDF 0.87 0.58 0.69 2,3,4,6,7,8-HxCDF < U 0.87 < U 0.58 < U 0.69 1,2,3,7,8,9 HxCDF 0.00099 0.00066 0.00078 9.9E-05 6.6E-05 7.8E-05 0.1 1,2,3,7,8,9-HxCDF 0.99 0.66 0.78 1,2,3,7,8,9-HxCDF < U 0.99 < U 0.66 < U 0.78 1,2,3,4,6,7,8 HpCDF 0.0012 0.0011 0.00084 1.2E-05 1.1E-05 8.4E-06 0.01 1,2,3,4,6,7,8-HpCDF 1.2 1.1 0.84 1,2,3,4,6,7,8-HpCDF < U 1.2 < M, J, R 1.1 < U 0.84 1,2,3,4,7,8,9 HpCDF 0.0015 0.0012 0.0011 1.5E-05 1.2E-05 1.1E-05 0.01 1,2,3,4,7,8,9-HpCDF 1.5 1.2 1.1 1,2,3,4,7,8,9-HpCDF < U 1.5 < U 1.2 < U 1.1 Total OCDF 0.00487 0.0032 0.0045 1.5E-06 9.6E-07 1.4E-06 0.0003 OCDF 4.87 3.2 4.5 OCDF M, J 4.87 < M, U 3.2 < M, J, R 4.5 Total CDF congeners 0.01448 0.010460.0117180.000880.000650.00066 **TOTAL CDD/CDF (TEQ)** 29.6954834.2490624.916620.051540.060740.04142

M indicates that a peak has been manually integrated U indicates that this compound was not detected above the MDL J indicates that a target analyte was detected below the LQL R indicates that the ion abundance ratio for this compounds did not meet the acceptance criterion. Measured wt, pg Measured wt, pg

Measured wt, pg Measured wt, pg

EPA-HQ-OAR-2013-0290-DRAFT-0051 El Paso Spray Dr D-F Data 12/1/2014