# Attachment C

TablesTable1:SampleSpecificInformationSampleIDDateComposited/CollectedTypeCompositeVolume(barrels)GrabVolume1(barrels)GrabLocation2Date/TimeCollected3PhysicalDescription4NorthQ17/2/2010Waste5012.517/2/201008:5012.5212.5312.54NorthQ27/1/2010Waste5012.557/1/201014:4512.5612.5712.58NorthQ37/1/2010Waste5012.597/1/201013:5012.51012.51112.512NorthQ47/1/2010Waste5012.5137/1/201012:5012.51412.51512.516SouthQ17/1/2010Waste5012.5177/1/201008:4512.51812.51912.520SouthQ27/1/2010Waste5012.5217/1/201009:5512.52212.52312.524Table1:SampleSpecificInformation(continued)SampleIDDateComposited/CollectedTypeCompositeVolume(barrels)GrabVolume1(barrels)GrabLocation2Date/TimeCollected3PhysicalDescription4SouthQ37/1/2010Waste5012.5257/1/201011:0512.526SouthQ327/1/2010FieldDuplicate12.52712.528SouthQ47/1/2010Waste5012.5297/1/201011:5512.53012.53112.5321Grabsampleswerecollectedwithavacuumtruck.Assuch,specificvolumesateachsamplingpointwerenotmeasured.Instead,samplematerialwascollectedfromthetopofthesludgetothebottomofthetank(i.e.,afullverticalprofile).Thevaluesgivenherearebasedontheassumptionsthatapproximately50barrelsofmaterialwerecollectedineachtankquarterandthateachgrabcontributed25%ofthe50barrels.2GrablocationscorrelatewiththenumbersonFigure7.3Collectiondates/timesarethoseforsludgerecoveryfromthetanksviavacuumtruck.4Samplematerialwascollectedwithavacuumtruckfromunderseveralfeetofwater.Therefore,aphysicalcharacterizationofthematerialateachlocationwasnotperformed.

# Table 2: Sample Identifiers and Types

Field ID Lab ID Sample Type

North Q1 

# 1007142

‐ 09 Waste

North Q2 

# 1007142

‐ 08 Waste

North Q3 

# 1007142

‐ 07 Waste

North Q4 

# 1007142

‐ 06 Waste

North Q4 (TCLP Basic) 

# 1007294

‐ 04 Waste

North Q4 (TCLP Neutral) 

# 1007294

‐ 03 Waste

South Q1 

# 1007142

‐ 01 Waste

South Q1 (TCLP Basic) 

# 1007294

‐ 02 Waste

South Q1 (TCLP Neutral) 

# 1007294

‐ 01 Waste

South Q2 

# 1007142

‐ 02 Waste

South Q3 

# 1007142

‐ 03 Waste

South Q32 

# 1007142

‐ 04 Replicate

South Q4 

# 1007142

‐ 05 Waste

TB070110A (Trip Blank) 

# 1007142

‐ 10 Trip Blank

Trip Blank 2 

# 1007142

‐ 11 Trip Blank

# Table 3: Sample Preparation Methods

Analysis 1 

# Total/TCLP Preparation

Method

Mercury Total SW

‐ 846 7471A

TCLP SW

‐ 846 1311

SW

‐ 846 3010A

Metals Total SW

‐ 846 3050A

TCLP SW

‐ 846 1311

SW

‐ 846 3010A

Semivolatile Organics Total SW

‐ 846 3541

TCLP SW

‐ 846 1311

SW

‐ 846 3510

Volatile Organics TCLP SW

‐ 846 1311

NOTE: Method 1311 was modified to include basic and

neutral extraction fluids in addition to the method described

acidic extraction fluid.

1 Preparation methods are presented per notations in the

analytical data packages (Attachment E). Preparation

methods are not reported for all analyses. It is assumed that

the preparation methods for those analyses are included in

the analytical method.Table4:DatesAssociatedwithSampleAnalysesTestNoTestNameCollectedTotalsTCLP(Acid)TCLP(Base)TCLP(Neutral)PreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystNorthQ1EPA160.3Moisture7/2/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/2/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/2/2010‐‐7/9/2010HNSW‐8461030Ignitability7/2/2010‐‐7/12/2010JLCSW‐8466020Metals7/2/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJSW‐8467471AMercury7/2/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/2/2010‐‐7/14/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/2/20107/7/20107/13/2010ACN7/9/20107/9/20107/14/2010ACNSW‐8469014Cyanide7/2/2010‐‐7/14/2010IABSW‐8469045BpH7/2/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/2/2010‐‐7/12/2010HNNorthQ2EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/13/2010ACNSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HNNorthQ3EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/13/2010ACNSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HNTable4:DatesAssociatedwithSampleAnalyses(continued)TestNoTestNameCollectedTotalsTCLP(Acid)TCLP(Base)TCLP(Neutral)PreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystNorthQ4EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJ7/13/20107/13/20107/14/2010ALR7/13/20107/13/20107/14/2010ALRSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJ7/13/20107/15/20107/16/2010JCJ7/13/20107/15/20107/16/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PC7/13/20107/16/2010PC7/13/20107/16/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/14/2010ACN7/13/20107/13/20107/13/2010KMB7/13/20107/13/20107/13/2010KMBSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HNSouthQ1EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/12/2010JCJ7/13/20107/13/20107/14/2010ALR7/13/20107/13/20107/14/2010ALRSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJ7/13/20107/15/20107/16/2010JCJ7/13/20107/15/20107/16/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PC7/13/20107/16/2010PC7/13/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/13/2010ACN7/13/20107/13/20107/13/2010KMB7/13/20107/13/20107/13/2010KMBSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/9/2010HNSouthQ2EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/12/2010JCJSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/1/2010‐‐7/14/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/13/2010ACNSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HNTable4:DatesAssociatedwithSampleAnalyses(continued)TestNoTestNameCollectedTotalsTCLP(Acid)TCLP(Base)TCLP(Neutral)PreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystTCLPPreparedAnalyzedAnalystSouthQ3EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/13/2010ACNSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HNSouthQ32EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/14/2010ACN7/9/20107/9/20107/13/2010ACNSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HNSouthQ4EPA160.3Moisture7/1/2010‐‐7/7/2010JLCEPA1664Oil&Grease7/1/2010‐‐7/19/2010JLCSM4500S2‐FSulfide7/1/2010‐‐7/9/2010HNSW‐8461030Ignitability7/1/2010‐‐7/12/2010JLCSW‐8466020Metals7/1/20107/12/20107/12/2010SKS7/12/20107/12/20107/13/2010JCJSW‐8467471AMercury7/1/20107/13/20107/13/2010JCJ7/12/20107/12/20107/12/2010JCJSW‐8468260VOCs7/1/2010‐‐7/13/2010WLR7/9/20107/15/2010PCSW‐8468270SVOCs7/1/20107/7/20107/13/2010ACN7/9/20107/9/20107/14/2010ACNSW‐8469014Cyanide7/1/2010‐‐7/14/2010IABSW‐8469045BpH7/1/2010‐‐7/8/2010IABSW‐846Chap.7Reactivity7/1/2010‐‐7/12/2010HN

# Table 5: Surrogate Recoveries

– Volatile Organics

Sample ID Dilution TCLP Total

DCE BFB DBFM T DCE BFB DBFM T

70

‐ 125% 72

‐ 125% 71

‐ 125% 75

‐ 125% 70

‐ 128% 73

‐ 126% 71

‐ 128% 73

‐ 127%

North Q1 20 99.4 94.4 101 91.6

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 113 106 104 97.9

North Q2 20 102 96.7 104 100

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 108 100 100 100

North Q3 20 95.3 97 99.6 105

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 107 104 103 98.7

North Q4 20 98.7 103 104 111

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 108 101 102 99.4

North Q4

(TCLP Basic) 

# 20 106 96.7 103 100

‐‐  ‐‐  ‐‐  ‐‐

North Q4

(TCLP Neutral) 

# 20 104 93.9 101 95.9

‐‐  ‐‐  ‐‐  ‐‐

South Q1 20 98.5 104 101 107

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 111 101 112 105

10

‐‐  ‐‐  ‐‐  ‐‐ 102 102 101 100

1250

‐‐  ‐‐  ‐‐  ‐‐ 98.3 94.7 99.7 91.8

South Q1

(TCLP Basic) 

# 20 106 97.2 102 99

‐‐  ‐‐  ‐‐  ‐‐

South Q1

(TCLP Neutral) 

# 20 92.1 92.2 97.5 93.8

‐‐  ‐‐  ‐‐  ‐‐

South Q2 20 101 101 107 109

‐‐  ‐‐  ‐‐  ‐‐

10

‐‐  ‐‐  ‐‐  ‐‐ 101 101 94.3 100

1250

‐‐  ‐‐  ‐‐  ‐‐ 94.2 98.8 99.1 99.7

South Q3 20 98 101 101 102

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 115 101 98.7 97.9

South Q32 20 98.7 96.9 101 102

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 108 96.9 95.6 101

10

‐‐  ‐‐  ‐‐  ‐‐ 98.9 96.6 96.3 97.6

South Q4 20 106 104 109 102

‐‐  ‐‐  ‐‐  ‐‐

1

‐‐  ‐‐  ‐‐  ‐‐ 106 99.4 96.3 99.7

Trip Blank 2 95.6 92 94.7 98.9

DCE = 1,2

‐ Dichloroethane

‐ d 4



# BFB = 4

‐ Bromofluorobenzene

DBFM = Dibromofluoromethane

T = Toluene

‐ d 8Table6:SurrogateRecoveries–SemivolatileOrganicsSampleIDDilutionTCLPTotal2‐FBP2‐FP4‐TPNBPTBP2‐FBP2‐FP4‐TPNBP48‐120%20‐120%51‐135%41‐120%20‐120%36‐126%43‐125%37‐125%32‐125%37‐125%40‐125%NorthQ1176.766.17772.26610169.850.183.96758.3NorthQ2164.952.579.361.459.788.77258.779.971.266.9NorthQ3164.647.170.455.251.584.476.255.276.475.364.95‐‐  ‐‐  ‐‐  ‐‐  ‐‐87.478.850.88174.168.6NorthQ4183.371.678.578.570.68778.952.176.374.963.45‐‐  ‐‐  ‐‐  ‐‐  ‐‐80.773.947.280.363.664.1NorthQ4(TCLPBasic)170.657.266.166.654.8‐‐  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐NorthQ4(TCLPNeutral)167.747.774.260.457.3‐‐  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐SouthQ1168.853.780.162.963.584.273.352.577.462.258.1SouthQ1(TCLPBasic)172.459.48171.767.1‐‐  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐SouthQ1(TCLPNeutral)180.266.47778.164.9‐‐  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐SouthQ2166.451.381.657.758.48977.653.778.873.964.44‐‐  ‐‐  ‐‐  ‐‐  ‐‐8775.249.977.965.957.4SouthQ3157.350.675.356.756.797.510148.475.975.965.45‐‐  ‐‐  ‐‐  ‐‐  ‐‐89.880.345.786.368.161SouthQ32167.355.574.966.358.488.991.552.469.773.364.75‐‐  ‐‐  ‐‐  ‐‐  ‐‐7361.640.264.454.945.4SouthQ417161.779.866.773.39379.65279.674.963.75‐‐  ‐‐  ‐‐  ‐‐  ‐‐8873.448.979.166.963.7TBP=2,4,6‐Tribromophenol2‐FP=2‐FluorophenolNB=Nitrobenzene‐d52‐FBP=2‐Fluorobiphenyl4‐TP=4‐Terphenyl‐d14P=Phenol‐d6Table7:MS/MSDResults–SampleSouthQ2SpikedAnalyteUn‐SpikedDetectedValueSpikeValueUnitsMSMSDRPDControlLimitsResult%RResult%RRecoveryRPDOil&Grease43361600mg/kg3960‐23.53072‐7925.380‐12020Mercury0.0000040.005mg/L0.005221040.00521040.38475‐12520Mercury569.3354/339.6ug/kg856.681.2876.190.42.2485‐11520Arsenic0.046010.5mg/L0.536798.10.54891012.2575‐12525Barium0.6230.5mg/L1.10696.61.1391032.9475‐12525Cadmium‐0.0024240.5mg/L0.4774960.49699.73.8275‐12525Chromium‐0.00042730.5mg/L0.476695.40.48897.72.3675‐12525Lead0.0026980.5mg/L0.4829960.498899.23.2475‐12525Selenium0.0017650.5mg/L0.499499.50.5351076.8875‐12525Silver‐0.0012570.5mg/L0.460992.40.471194.52.1975‐12525Antimony0.0054520.5mg/L0.51571020.51851030.54175‐12525Beryllium‐0.0017970.5mg/L0.476295.60.50171015.2275‐12525Cobalt0.0008330.5mg/L0.473994.60.473794.60.042275‐12525Nickel0.13790.5mg/L0.579888.40.596291.72.7975‐12525Vanadium0.0071560.5mg/L0.503899.30.500898.70.59775‐12525Zinc0.0045230.5mg/L0.51211020.51581020.7275‐12525Arsenic23.829.615/9.524mg/kg31.3478.131.3979.50.17275‐12525Barium76.69.615/9.524mg/kg88.8112786.791072.375‐12525Cadmium0.67399.615/9.524mg/kg9.16988.49.11988.70.54975‐12525Chromium22.429.615/9.524mg/kg29.775.731.393.35.2575‐12525Cobalt5.8659.615/9.524mg/kg13.3177.413.6381.52.3875‐12525Lead12.889.615/9.524mg/kg21.9594.322.1897.61.0475‐12525Nickel47.189.615/9.524mg/kg53.3964.752.5656.51.5775‐12525Selenium7.689.615/9.524mg/kg15.8284.615.2379.33.7975‐12525Table7:MS/MSDResults–SampleSouthQ2(continued)SpikedAnalyteUn‐SpikedDetectedValueSpikeValueUnitsMSMSDRPDControlLimitsResult%RResult%RRecoveryRPDSilver0.042099.615/9.524mg/kg7.97582.57.9282.70.69275‐12525Vanadium22.549.615/9.524mg/kg30.428230.2280.60.67375‐12525Zinc475.69.615/9.524mg/kg471.9‐38.1481.966.32.0975‐12525Beryllium0.047539.615/9.524mg/kg8.95892.78.91193.10.51875‐125252,4‐Dimethylphenol3332/3328ug/kg306097.8293588.24.1955‐125302,4‐Dinitrophenol3332/3328ug/kg173952.2191657.69.6740‐125302,4‐Dinitrotoluene1666/1664ug/kg191311519471171.7755‐125302‐Methylphenol39.913332/3328ug/kg296087.6281783.44.9555‐120303&4‐Methylphenol83.394998/4992ug/kg463291430684.67.2855‐120304‐Nitrophenol3332/3328ug/kg34861053029911450‐13030Acenaphthene11291666/1664ug/kg246280222465.810.255‐12030Anthracene10561666/1664ug/kg2870109232676.320.955‐12030Benz(a)anthracene236.21666/1664ug/kg158280.8160282.11.2655‐12530Benzo(a)pyrene245.51666/1664ug/kg182094.5173889.74.6555‐12030Benzo(b)fluoranthene105.51666/1664ug/kg143679.9117564.32055‐12530Benzo(k)fluoranthene57.651666/1664ug/kg201511719891161.3155‐13030Bis(2‐ethylhexyl)phthalate329.81666/1664ug/kg198799.4178587.510.755‐12530Butylbenzylphthalate1666/1664ug/kg163097.9156093.84.4155‐12530Chrysene667.31666/1664ug/kg24031042131881255‐12530Dibenz(a,h)anthracene66.851666/1664ug/kg1746101159591.89.0355‐12030Diethylphthalate1666/1664ug/kg157294.4144086.58.7655‐12030Dimethylphthalate1666/1664ug/kg148689.2140184.25.8655‐12030Di(n)butylphthalate1666/1664ug/kg163898.3159996.12.3955‐12530Di(n)octylphthalate20.091666/1664ug/kg170210117001010.13755‐13030Table7:MS/MSDResults–SampleSouthQ2(continued)SpikedAnalyteUn‐SpikedDetectedValueSpikeValueUnitsMSMSDRPDControlLimitsResult%RResult%RRecoveryRPDFluoranthene427.21666/1664ug/kg2364116207198.813.255‐12530Fluorene26091666/1664ug/kg382472.9379671.30.72555‐12030Indeno(1,2,3‐cd)pyrene101.41666/1664ug/kg137176.2120566.312.955‐12530Nitrobenzene1666/1664ug/kg145587.31380835.2755‐12030Phenanthrene66411666/1664ug/kg785172.66260‐22.922.555‐12030Phenol69.923332/3328ug/kg277281.12632775.250‐12030Pyrene18441666/1664ug/kg298868.6289863.33.0655‐12530Pyridine1666/1664ug/kg800.848.1783.447.12.230‐12030Quinoline1666/1664ug/kg179510816781016.7455‐130302,4‐Dimethylphenol100ug/L84.978582.7382.72.6753‐115302,4‐Dinitrophenol100ug/L71.0971.177.5477.58.6747‐115302,4‐Dinitrotoluene50ug/L41.8583.741.7583.50.2256‐115302‐Methylphenol100ug/L77.3977.476.8876.90.66553‐115303&4‐Methylphenol1.348150ug/L123.781.6119.678.93.3748‐115304‐Nitrophenol100ug/L76.3376.381.1481.16.1126‐13330Acenaphthene5.13550ug/L50.290.148.8587.42.7357‐11530Anthracene50ug/L46.9693.945.6391.32.8756‐11530Benz(a)anthracene50ug/L45.1390.345.5891.20.99153‐11530Benzo(a)pyrene50ug/L45.190.243.7987.62.9457‐11530Benzo(b)fluoranthene50ug/L49.1498.347.7895.62.8154‐11730Benzo(k)fluoranthene50ug/L43.8287.644.2588.50.97450‐11530Bis(2‐ethylhexyl)phthalate50ug/L46.9393.945.5791.12.9550‐11530Butylbenzylphthalate50ug/L46.8693.745.891.62.2851‐11530Chrysene50ug/L47.2794.544.3388.76.4258‐11530Table7:MS/MSDResults–SampleSouthQ2(continued)SpikedAnalyteUn‐SpikedDetectedValueSpikeValueUnitsMSMSDRPDControlLimitsResult%RResult%RRecoveryRPDDibenz(a,h)anthracene50ug/L47.6495.346.0592.13.3956‐11530Diethylphthalate50ug/L41.2382.541.2482.50.03757‐11530Dimethylphthalate50ug/L41.4782.940.1480.33.2556‐11530Di(n)butylphthalate50ug/L47.2294.444.6489.35.6254‐11530Di(n)octylphthalate50ug/L45.3490.746921.4449‐11530Fluoranthene50ug/L47.529544.5789.16.4158‐11530Fluorene8.49250ug/L51.0885.249.8782.82.3956‐11530Indeno(1,2,3‐cd)pyrene50ug/L45.8191.645.02901.7351‐11530Nitrobenzene50ug/L42.0484.140.7281.43.240‐12430Phenanthrene13.9850ug/L59.0190.153.2578.510.357‐11530Phenol1.898100ug/L77.5375.673.671.75.238‐11530Pyrene50ug/L44.7489.543.9187.81.8651‐11530Pyridine50ug/L33.3266.633.9267.81.834‐11530Quinoline50ug/L44.028843.5487.11.152‐116301,1,1‐Trichloroethane500ug/kg477.895.6381.476.322.479‐124301,1‐Dichloroethane500ug/kg506.6101444.188.813.175‐124301,1‐Dichloroethene500ug/kg508.3102420.784.118.980‐122301,2‐Dibromoethane500ug/kg535.4107411.582.326.279‐120301,2‐Dichlorobenzene500ug/kg472.394.5298.159.645.279‐120301,2‐Dichloroethane500ug/kg503.4101454.690.910.273‐121301,3‐Dichlorobenzene500ug/kg460.992.229258.444.979‐120301,4‐Dichlorobenzene500ug/kg476.595.3300.860.245.277‐120301,4‐Dioxane10000ug/kg12540125121201213.4365‐132302‐Butanone1000ug/kg1299130114211412.865‐13030Table7:MS/MSDResults–SampleSouthQ2(continued)SpikedAnalyteUn‐SpikedDetectedValueSpikeValueUnitsMSMSDRPDControlLimitsResult%RResult%RRecoveryRPDBenzene11.2500ug/kg508.299.4418.981.519.379‐12030Carbondisulfide1000ug/kg974.197.4725.272.529.380‐12430Chlorobenzene500ug/kg471.294.2327.265.436.179‐12030Chloroform500ug/kg501.9100438.487.713.578‐12030Ethylbenzene302.4500ug/kg59859.1627.965.14.8780‐12230Methyltert‐butylether500ug/kg545.5109515.71035.6376‐12130Naphthalene3721500ug/kg1975‐3493512‐41.85671‐12830Styrene500ug/kg499.799.93557133.978‐12430Tetrachloroethane33.52500ug/kg475.788.4347.762.831.180‐12130Toluene289.5500ug/kg615.165.169681.312.379‐12030Trichloroethene500ug/kg538.2108459.691.915.880‐12130Xylenes,total24901500ug/kg2455‐2.31336758.531.380‐12030Naphthalene85.951000ug/kg1106102111985.951.2471‐128301,1,1‐Trichloroethane1000ug/L890.489936.593.65.0480‐120201,1‐Dichloroethane1000ug/L1051105961.896.28.8676‐120201,1‐Dichloroethene1000ug/L898.389.8945.894.65.1473‐124201,2‐Dibromoethane1000ug/L101910298398.33.5880‐120201,2‐Dichlorobenzene1000ug/L997.999.8930.993.16.9480‐120201,2‐Dichloroethane1000ug/L105110510321031.7478‐120201,3‐Dichlorobenzene1000ug/L922.192.2924.592.40.25680‐130201,4‐Dichlorobenzene1000ug/L937.593.8926.492.61.280‐120201,4‐Dioxane20000ug/L1763088.22067010315.950‐158202‐Butanone2000ug/L213210720401024.4258‐13220Benzene1000ug/L954.195.4987.898.83.4773‐12120Table7:MS/MSDResults–SampleSouthQ2(continued)SpikedAnalyteUn‐SpikedDetectedValueSpikeValueUnitsMSMSDRPDControlLimitsResult%RResult%RRecoveryRPDCarbondisulfide2000ug/L1780891940978.5868‐14120Chlorobenzene1000ug/L903.590.4911.991.20.92180‐12020Chloroform1000ug/L1050105960.1968.9280‐12020Ethylbenzene1000ug/L885.488.5901.790.21.8280‐12020Methyltert‐butylether1000ug/L99499.410211022.6673‐12120Naphthalene85.951000ug/L110610211191031.2465‐12720Styrene1000ug/L952.595.2916.591.73.8580‐12020Tetrachloroethane1000ug/L741.574.2855.885.614.379‐13020Toluene11.041000ug/L911.490940.592.93.1580‐12020Trichloroethene1000ug/L893.889.4920.5922.9480‐12020Xylenes,total56.843000ug/L275990.1273989.40.72680‐12020Cyanide(9014)0.93419.191/9.18mg/kg9.19189.89.1889.80.1275‐12530Cyanide(9010)0.0050.2mg/L0.18891.5‐‐  ‐‐  ‐‐75‐125‐‐Sulfide96.81075mg/kg553.642.5553.696.8021‐8150Cyanide,reactive250mg/kg234.994234.994050‐15035MS=MatrixSpikeMSD=DuplicateMatrixSpike%R=PercentRecoveryRPD=RelativePercentDifferenceTable8:TotalAnalyticalResultsAnalyteNorthQ1NorthQ2NorthQ3NorthQ4SouthQ1SouthQ2SouthQ3SouthQ32SouthQ4Sulfide72.8H72.8H48.8H145H133H96.8H84.8H109H24.8HCyanide3.13J1.72J1.2U1.3U1.4U2.03J7.724.51.2UCyanide,Amenable1.4U1.6U1.2U1.3U1.4U1.2U3.09J1.2U1.2UMercury0.4160.2740.2050.4280.9721.241.460.8150.353Antimony1.891.13J0.55U0.939J1.81.871.04J1.110.87JArsenic22.128.612.930.460.151.73840.631.2Barium18113561.4125196166130133135Beryllium0.13U0.12U0.11U0.11U0.11U0.11U0.11U0.1U0.1UCadmium0.484J0.794J0.286J0.976J1.261.461.251.241.07Chromium23.730.411.528.915248.737.838.730.7Cobalt6.618.233.546.1224.412.79.99.667.56Lead15.715.85.7914.143.1282323.516.6Nickel29.842.916.442.421210287.772.747.3Selenium20.914.93.919.4610016.713.712.78.49Silver0.1U0.095U0.088U0.087U0.16J0.0913J0.086U0.084U0.08UVanadium28.543.317.336.411448.938.139.431.7Zinc35899722765910101140922901740PercentMoisture162.462.657.457.357.453.958.757.455.7OilandGrease997017309211360271094103090194003780pH29.178.768.588.861010.29.539.569.54ReactiveCyanide23U23U23U23U23U23U23U23U23UReactiveSulfide14U14U14U14U14U14U14U14U14U2,4‐Dimethylphenol0.098U0.099U0.087U0.086U0.087U0.08U0.13U0.087U0.083U2,4‐Dinitrophenol0.17U0.17U0.15U0.15U0.15U0.14U0.23U0.15U0.14U2,4‐Dinitrotoluene0.16U0.16U0.14U0.14U0.14U0.13U0.22U0.14U0.14U2‐Methylphenol0.096U0.096U0.085U0.1J0.085U0.087J0.17J0.084U0.13JTable8:TotalAnalyticalResults(continued)AnalyteNorthQ1NorthQ2NorthQ3NorthQ4SouthQ1SouthQ2SouthQ3SouthQ32SouthQ43&4‐Methylphenol1.60.17U0.15U0.23J0.15U0.18J0.47J0.15U0.494‐Nitrophenol0.16U0.16U0.14U0.14U0.14U0.13U0.22U0.14U0.14UAcenaphthene1.52.14.34.20.522.583.42.7Anthracene11.72.94.40.422.31823.6Benz(a)anthracene0.22J0.24J0.490.560.14J0.513.60.650.49Benzo(a)pyrene0.23J0.27J0.520.590.093J0.531.50.450.59Benzo(b)fluoranthene0.08U0.1J0.18J0.14J0.07U0.23J0.6J0.25J0.18JBenzo(k)fluoranthene0.13J0.1J0.28J0.2J0.07U0.13J0.660.23J0.26JBis(2‐ethylhexyl)phthalate0.50.550.780.870.22J0.721.80.680.88Butylbenzylphthalate0.08U0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UChrysene0.23J0.81.61.50.24J1.44.21.41.7Dibenz(a,h)anthracene0.08U0.08U0.17J0.07U0.099J0.15J0.11U0.17J0.068UDiethylphthalate0.08U0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UDimethylphthalate0.08U0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UDi‐n‐butylphthalate0.08U0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UDi‐n‐octylphthalate0.19J0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UFluoranthene0.08U0.651.71.60.21J0.933.80.07U1.3Fluorene2.83.48.38.60.835.71986.2Indeno(1,2,3‐cd)pyrene0.08U0.08U0.07U0.16J0.11J0.22J0.44J0.16J0.16JNitrobenzene0.088U0.088U0.077U0.077U0.077U0.072U0.12U0.077U0.074UPhenanthrene8.11127272.815621718Phenol0.32J0.08U0.084J0.11J0.07U0.15J0.22J0.07U0.22JPyrene22.54.86.50.649.73.84.7Pyridine0.08U0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UQuinoline0.08U0.08U0.07U0.07U0.07U0.065U0.11U0.07U0.068UTable8:TotalAnalyticalResults(continued)AnalyteNorthQ1NorthQ2NorthQ3NorthQ4SouthQ1SouthQ2SouthQ3SouthQ32SouthQ41,1,1‐Trichloroethane0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,1‐Dichloroethane0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,1‐Dichloroethene0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,2‐Dibromoethane0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,2‐Dichlorobenzene0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,2‐Dichloroethane0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,3‐Dichlorobenzene0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,4‐Dichlorobenzene0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011U1,4‐Dioxane0.053U0.053U0.047U0.047U0.047U0.43U0.048U0.047U0.045U2‐Butanone0.0830.0290.0320.0033U0.120.03U0.0430.0430.036Benzene0.0035J0.0088J0.0310.0076J0.0180.024J0.0072J0.0140.0094JCarbondisulfide0.0083J0.0027U0.0023U0.0023U0.0023U0.022U0.0024U0.0023U0.0023UChlorobenzene0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011UChloroform0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011UEthylbenzene0.110.0330.0450.0350.240.660.140.160.083Methyltert‐butylether0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011UNaphthalene0.0860.460.390.1190830.341.90.0064JStyrene0.0013U0.0013U0.0012U0.0012U0.0012U0.011U0.0012U0.0012U0.0011UTetrachloroethene0.040.0370.030.0250.0720.073J0.0420.0410.042Toluene0.0680.0370.110.0520.30.630.170.260.11Trichloroethene0.0027J0.0021J0.003J0.004J0.0076J0.011U0.0071J0.0068J0.0061JXylenes,Total0.460.250.370.257.65.40.771.20.7Ignitability,Solid3NegativeNegativeNegativeNegativeNegativeNegativeNegativeNegativeNegativeUnlessotherwisenoted,unitsaremg/kg‐dry.1Unitsforpercentmoistureareweightpercent.2UnitsforpHarestandardunits.3Therearenounitsforignitability.Table9:TCLPAnalyticalResultsAnalyteNorthQ1NorthQ2NorthQ3NorthQ4NorthQ4(TCLPBasic)NorthQ4(TCLPNeutral)SouthQ1SouthQ1(TCLPBasic)SouthQ1(TCLPNeutral)SouthQ2SouthQ3SouthQ32SouthQ4Cyanide0.003UHMercury0.000042U0.000042U0.000042U0.000042U0.000042U0.000042U0.000042U0.000052J0.000042U0.000042U0.000042U0.000042U0.000042UArsenic0.0144J0.05430.1570.05860.1140.0195J0.0118J0.1070.0149J0.046J0.05690.06020.0596Barium1.120.8361.070.7060.0359J0.0467J0.6210.0457J0.08470.6230.6240.6690.645Cadmium0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006UChromium0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006U0.006ULead0.004U0.004U0.004U0.00452J0.004U0.004U0.00535J0.00431J0.00508J0.004U0.004U0.004U0.004USelenium0.025U0.025U0.025U0.025U0.0265J0.025U0.025U0.180.05420.025U0.025U0.025U0.025USilver0.007U0.007U0.007U0.007U0.007U0.007U0.007U0.007U0.007U0.007U0.007U0.007U0.007UAntimony0.005U0.005U0.005U0.00537J0.00729J0.00504J0.005U0.00743J0.005U0.00545J0.00548J0.005U0.005UBeryllium0.003U0.003U0.003U0.003U0.003U0.003U0.003U0.003U0.003U0.003U0.003U0.003U0.003UCobalt0.00737J0.005U0.00592J0.005U0.005U0.005U0.005U0.00614J0.005U0.005U0.005U0.005U0.005UNickel0.1160.0287J0.1730.0680.0148J0.014U0.1320.0317J0.014U0.1380.10.1140.047JVanadium0.00956J0.015J0.0202J0.0121J0.130.0113J0.007U0.0550.007U0.00716J0.00801J0.0103J0.0125JZinc0.08810.025U0.05950.025U0.0377J0.025U0.0436J0.2270.1660.025U0.025U0.025U0.025U2,4‐Dimethylphenol0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U2,4‐Dinitrophenol0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U0.0014U2,4‐Dinitrotoluene0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U2‐Methylphenol0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U0.001U3&4‐Methylphenol0.0240.001U0.001U0.001U0.001U0.001U0.00520.001U0.001U0.0013J0.001U0.001U0.001U4‐Nitrophenol0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019U0.0019UAcenaphthene0.0019J0.0031J0.0036J0.0033J0.003J0.0043J0.002J0.0009U0.0009U0.00510.0023J0.0021J0.0034JAnthracene0.0006U0.0006U0.0006U0.0006U0.0006U0.0017J0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006UBenz(a)anthracene0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005UBenzo(a)pyrene0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006UBenzo(b)fluoranthene0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007UBenzo(k)fluoranthene0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009U0.0009UBis(2‐ethylhexyl)phthalate0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033U0.0033UButylbenzylphthalate0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007U0.0007UChrysene0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008UDibenz(a,h)anthracene0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008UDiethylphthalate0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005UDimethylphthalate0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005UDi‐n‐butylphthalate0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005UDi‐n‐octylphthalate0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006UTable9:TCLPAnalyticalResults(continued)AnalyteNorthQ1NorthQ2NorthQ3NorthQ4NorthQ4(TCLPBasic)NorthQ4(TCLPNeutral)SouthQ1SouthQ1(TCLPBasic)SouthQ1(TCLPNeutral)SouthQ2SouthQ3SouthQ32SouthQ4Fluoranthene0.0005U0.0005U0.0005U0.0005U0.0005U0.0035J0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005UFluorene0.003J0.0050.00640.00540.00530.00810.0031J0.0014J0.0006U0.00850.0048J0.004J0.0057Indeno(1,2,3‐cd)pyrene0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013U0.0013UNitrobenzene0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008U0.0008UPhenanthrene0.0047J0.00840.0110.0090.00960.0180.00530.0024J0.0005U0.0140.00880.00710.01Phenol0.0033J0.0005U0.0005U0.0005U0.0005U0.0005U0.0032J0.0005U0.0005U0.0019J0.0005U0.0005U0.0005UPyrene0.0005U0.0005U0.0005U0.0005U0.0005U0.0026J0.0005U0.0005U0.0005U0.0005U0.0005U0.0005U0.0005UPyridine0.002U0.002U0.002U0.002U0.002U0.002U0.002U0.002U0.002U0.002U0.002U0.002U0.002UQuinoline0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U0.0006U1,1,1‐Trichloroethane0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,1‐Dichloroethane0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,1‐Dichloroethene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,2‐Dibromoethane0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,2‐Dichlorobenzene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,2‐Dichloroethane0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,3‐Dichlorobenzene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,4‐Dichlorobenzene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U1,4‐Dioxane2U2U2U2U2U2U2U2U2U2U2U2U2U2‐Butanone0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02UBenzene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UCarbondisulfide0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02U0.02UChlorobenzene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UChloroform0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UEthylbenzene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UMethyltert‐butylether0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UNaphthalene0.044J0.01U0.01U0.032J0.01U0.01U0.056J0.044J0.01U0.086J0.062J0.059J0.04JStyrene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UTetrachloroethene0.012U0.012U0.012U0.012U0.012U0.012U0.012U0.012U0.012U0.012U0.012U0.012U0.012UToluene0.017J0.01U0.01U0.01U0.01U0.01U0.013J0.02J0.016J0.011J0.014J0.015J0.01UTrichloroethene0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01U0.01UXylenes,Total0.071J0.03U0.03U0.03U0.03U0.03U0.068J0.065J0.03U0.057J0.055J0.045J0.03U

# Table 10: ALS Equipment

Item Description Manufacturer/Model

GC with FID (FID #2) HP 5890A, HP7673 Injector

GC with FID/FPD (FID #1) HP 5890A, HP7673A Injector

GC with FID (FID#3) HP 5890A Series II, HP7673A Injector

GC with FID (FID #4) / with Headspace

Analyzer HP 5890A Series II / HTA HT280T Headspace

Autosampler

GC with FID, Dual Thu

‐ put (FID#7 / #8) Agilent 6890N, Dual Column/FID

GC with FID, Dual Thu

‐ put (FID#10 / #11) Agilent 6890N, Dual Column/FID

GC with FID (FID#6

‐ GRO) HP 5890 Series II,

Purge & Trap Conc, for GRO OI 4560 (for FID #6)

Purge & Trap Concentrator OI 4552 Autosampler (for FID 6 )

GC with FID (FID#9

‐ GRO) Agilent 6890 GC

Purge & Trap Concentrator Tekmar 3100 (for FID #9

– GRO)

Closed Loop Multi

‐ sampler OI 4552 Multi

‐ sampler (FID#9)

GC Dual PID (BTEX 1&2) HP 5890 Series II

Purge & Trap Concentrator Tekmar 3000 (BTEX 1&2)

Closed Loop Multi

‐ sampler Varian Archon Sampler (BTEX 1&2)

GC Dual PID (BTEX 3&4) HP 5890 Series II

Closed Loop Multi

‐ sampler Varian Archon Sampler (BTEX 3&4)

Purge & Trap Tekmar 3000

GC Dual ECD (ECD 1&2) HP 5890 Series II, HP7673 Injector

GC Dual ECD (ECD 3&4) HP 5890 Series II, HP7673 Injector

GC Dual ECD (ECD 5&6) HP 5890 Series II, HP7673 Injector

GC Dual ECD (ECD 7&8) Agilent 6890N, dual micro ECDs, Agilent 7683B

Injector

GC Dual ECD (ECD 9&10) HP 5890 Series II, HP7673 Injector

GC/MSD (VOA1) HP5890 Series II with HP5972A MSD

Closed Loop Multi

‐ sampler Varian Archon Multi

‐ sampler (VOA1)

Purge & Trap Concentrator HP Purge and Trap (VOA 1)

GC/MSD II (VOA2) Agilent 6890 GC with 5973A MSD

Closed Loop Multi

‐ sampler Varian Archon Multi

‐ sampler (VOA2)

Purge & Trap Concentrator Tekmar Dohrmann Velocity (VOA2)

GC/MSD II (VOA3) HP5890 Series II with HP5972A MSD

Closed Loop Multi

‐ sampler Varian Archon Multi

‐ sampler (VOA3)

Purge & Trap Concentrator Tekmar Dohrmann 3100 (VOA3)

GC/MSD II (VOA4) Agilent 6890 GC with 5973 Inert MSD

Closed Loop Multi

‐ sampler Varian Archon Multi

‐ sampler (VOA4)

Purge & Trap Concentrator Tekmar Dohrmann Velocity (VOA4)

GC/MSD II (VOA5) Agilent 6890 GC with 5975 Inert MSD

# Table 10: ALS Equipment (continued)

Item Description Manufacturer/Model

Closed Loop Multi

‐ sampler Tekmar/Dohrmann SOLATek (VOA5)

Purge & Trap Concentrator Tekmar Dohrmann Velocity (VOA5)

GC/MSD II (VOA5) Agilent 6890 GC with 5975 Inert MSD

Closed Loop Multi

‐ sampler Varian Archom (VOA5)

Purge & Trap Concentrator Tekmar Dohrmann Velocity (VOA5)

GC/MSD II (SV2) Agilent 6890 Plus with 5973 MSD

GC/MSD III (SV3) Agilent 6890 Plus with 5973 MSD

GC/MSD IV (SV4) Agilent 6890 Plus with 5973 MSD

GC/MSD V (SV5) Agilent 6890 Plus with 5973 MSD

Soxtec Extraction Unit (1) Model 2055 (Total Ext. Capacity = 6)

Soxtec Extraction Unit (2) Model 2055 (Total Ext. Capacity = 6)

HPLC

– with UV and Fluorescence

detectors Agilent 1100 Series HPLC, with autosampler

UV/VIS Shimadzu UV

‐ 2450

Ion Chromatograph Dionex ICS

‐ 3000

ICP/MS Agilent 7500 Series ORC

ICP/MS Agilent 7500 Series ORCE

ICP/MS Agilent 7500 Series ORCE

Mercury Analyzer CETAC Technologies M

‐ 6000A

TOC Analyzer (for waters) OI 1010 TOC Analyzer & Autosampler

TOC Analyzer (for soils) OI TOC Solids Analyzer

Cyanide Distillation Environmental Express 10 position

Ammonia Distillation Environmental Express 10 position

Vortex Fisher Genie 2

Stirrer Labline Multi Magnestir

Centrifuge (4) IES

Water Bath Precision

Nitrogen Evaporator Organomation N

‐ Evap

Turbo Vap II (2 units) Caliper Life Sciences, Turbo Vap II

3

‐ D Shaker Glass

‐ col

Multi

‐ tube Vortexer VWR VX 2500

GPC OI Analytical Autoprep 2000

Furnace Thermodyne

Furnace Thermodyne

Sonicator Ultrasonic Heat System XL

Ultrasonic Bath (3) Branson 2200

Hot Plate (2) Corning PC 104

Hot Block Digesters (2) Environmental Express

# Table 10: ALS Equipment (continued)

Item Description Manufacturer/Model

Hot Block Digesters (2) Environmental Express

Analytical balances (6) Mettler AE 200 (2), Mettler AE 163(2), Fisher

A160, Cahn Micro

‐ balance (1)

Analytical balance Ohaus ScoutPro 400g

Analytical balance Shimadzu UniBlock AUX220

Specific Ion/pH Meter (2) Fisher Accumet AR

‐ 50

Specific Ion/pH Meter Fisher Accumet AR

‐ 50

PH Meter Mettler Toledo SevenEasy

ZHE Extraction Units (9) Environmental Express

Top Loading balance (1) Mettler 4400

Top Loading balance (1) Denver Instruments APX

‐ 1502

Forced Air Oven VWR FM 1390

Drying Oven (2) VWR Model 1326

Full Size Refrigerator/Freezer (3) Labline Explosion Proof

13' x 40' Walk

‐ in Refrigerator Thermo

‐ Kool

8' x 10' Walk

‐ in Refrigerator NorLake

8' x 10' Walk

‐ in Freezer NorLake

Refrigerators (5) Various

Freezer (3) Hussmann/Tappan

ELIMS Database e

‐ LIMS

Computer Servers (4) HP and Compaq

Computer Server (Target) e

‐ Lab Analytical, Inc.

SQL Server (eLIMS) e

‐ Lab Analytical, Inc.