Attachment C

Tables
Table 1: Sample Specific Information

Sample ID

Date

Composited/

Collected Type

Composite

Volume

(barrels)

Grab

Volume1

(barrels)

Grab

Location2

Date/Time

Collected3 Physical Des

North Q1 7/2/2010 Waste 50 12.5 1 7/2/2010

12.5 2 08:5012.5 312.5 4

North Q2 7/1/2010 Waste 50 12.5 5 7/1/2010

12.5 6 14:4512.5 712.5 8

North Q3 7/1/2010 Waste 50 12.5 9 7/1/2010

12.5 10 13:5012.5 1112.5 12

North Q4 7/1/2010 Waste 50 12.5 13 7/1/2010

12.5 14 12:5012.5 1512.5 16

South Q1 7/1/2010 Waste 50 12.5 17 7/1/2010

12.5 18 08:4512.5 1912.5 20

South Q2 7/1/2010 Waste 50 12.5 21 7/1/2010

12.5 22 09:5512.5 2312.5 24
Table 1: Sample Specific Information (continued)

Sample ID

Date

Composited/

Collected Type

Composite

Volume

(barrels)

Grab

Volume1

(barrels)

Grab

Location2

Date/Time

Collected3 Physical Des

South Q3 7/1/2010 Waste 50 12.5 25 7/1/2010

12.5 26 11:05

South Q32 7/1/2010 Field

Duplicate

12.5 27

12.5 28

South Q4 7/1/2010 Waste 50 12.5 29 7/1/2010

12.5 30 11:5512.5 3112.5 32

1 Grab samples were collected with a vacuum truck. As such, specific volumes at each sampling point were not measur

sample material was collected from the top of the sludge to the bottom of the tank (i.e., a full vertical profile). The va

are based on the assumptions that approximately 50 barrels of material were collected in each tank quarter and that 

contributed 25% of the 50 barrels.

2 Grab locations correlate with the numbers on Figure 7.

3 Collection dates/times are those for sludge recovery from the tanks via vacuum truck.

4 Sample material was collected with a vacuum truck from under several feet of water. Therefore, a physical character

material at each location was not performed.
Table 2: Sample Identifiers and Types

Field ID Lab ID Sample Type

North Q1 1007142‐09 Waste

North Q2 1007142‐08 Waste

North Q3 1007142‐07 Waste

North Q4 1007142‐06 Waste

North Q4 (TCLP Basic) 1007294‐04 Waste

North Q4 (TCLP Neutral) 1007294‐03 Waste

South Q1 1007142‐01 Waste

South Q1 (TCLP Basic) 1007294‐02 Waste

South Q1 (TCLP Neutral) 1007294‐01 Waste

South Q2 1007142‐02 Waste

South Q3 1007142‐03 Waste

South Q32 1007142‐04 Replicate

South Q4 1007142‐05 Waste

TB070110A (Trip Blank) 1007142‐10 Trip Blank

Trip Blank 2 1007142‐11 Trip Blank

   
Table 3: Sample Preparation Methods

Analysis1 Total/TCLP

Preparation

Method

Mercury Total SW‐846 7471A

TCLP SW‐846 1311

SW‐846 3010A

Metals Total SW‐846 3050A

TCLP SW‐846 1311

SW‐846 3010A

Semivolatile Organics Total SW‐846 3541

TCLP SW‐846 1311

SW‐846 3510

Volatile Organics TCLP SW‐846 1311

NOTE:    Method 1311 was modified to include basic and

neutral extraction fluids in addition to the method described

acidic extraction fluid.

1    Preparation methods are presented per notations in the

analytical data packages (Attachment E).    Preparation

methods are not reported for all analyses.  It is assumed that

the preparation methods for those analyses are included in

the analytical method.
Table 4: Dates Associated with Sample Analyses

TestNo Test Name Collected

Totals TCLP (Acid) TC

Prepared Analyzed Analyst TCLP Prepared Analyzed Analyst TCLP Prepar

North Q1EPA 160.3 Moisture 7/2/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/2/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/2/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/2/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/2/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJSW‐846 7471A Mercury 7/2/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/2/2010  ‐‐  7/14/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/2/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/14/2010 ACNSW‐846 9014 Cyanide 7/2/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/2/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/2/2010  ‐‐  7/12/2010 HNNorth Q2EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJSW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/13/2010 ACNSW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HNNorth Q3EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJSW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/13/2010 ACNSW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HN
Table 4: Dates Associated with Sample Analyses (continued

TestNo Test Name Collected

Totals TCLP (Acid) TC

Prepared Analyzed Analyst TCLP Prepared Analyzed Analyst TCLP Prepar

North Q4EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJ 7/13/2010 7/13/20SW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJ 7/13/2010 7/15/20SW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PC 7/13/2010 SW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/14/2010 ACN 7/13/2010 7/13/20SW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HNSouth Q1EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/12/2010 JCJ 7/13/2010 7/13/20SW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJ 7/13/2010 7/15/20SW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PC 7/13/2010 SW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/13/2010 ACN 7/13/2010 7/13/20SW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/9/2010 HNSouth Q2EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/1/2010  ‐‐  7/14/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/13/2010 ACNSW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HN
Table 4: Dates Associated with Sample Analyses (continued

TestNo Test Name Collected

Totals TCLP (Acid) TC

Prepared Analyzed Analyst TCLP Prepared Analyzed Analyst TCLP Prepar

South Q3EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJSW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/13/2010 ACNSW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HNSouth Q32EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJSW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/14/2010 ACN 7/9/2010 7/9/2010 7/13/2010 ACNSW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HNSouth Q4EPA 160.3 Moisture 7/1/2010  ‐‐  7/7/2010 JLCEPA 1664 Oil & Grease 7/1/2010  ‐‐  7/19/2010 JLCSM4500 S2‐F Sulfide 7/1/2010  ‐‐  7/9/2010 HNSW‐846 1030 Ignitability 7/1/2010  ‐‐  7/12/2010 JLCSW‐846 6020 Metals 7/1/2010 7/12/2010 7/12/2010 SKS 7/12/2010 7/12/2010 7/13/2010 JCJSW‐846 7471A Mercury 7/1/2010 7/13/2010 7/13/2010 JCJ 7/12/2010 7/12/2010 7/12/2010 JCJSW‐846 8260 VOCs 7/1/2010  ‐‐  7/13/2010 WLR 7/9/2010 7/15/2010 PCSW‐846 8270 SVOCs 7/1/2010 7/7/2010 7/13/2010 ACN 7/9/2010 7/9/2010 7/14/2010 ACNSW‐846 9014 Cyanide 7/1/2010  ‐‐  7/14/2010 IABSW‐846 9045B pH 7/1/2010  ‐‐  7/8/2010 IABSW‐846 Chap. 7 Reactivity 7/1/2010  ‐‐  7/12/2010 HN
Table 5: Surrogate Recoveries – Volatile Organics

Sample ID Dilution

TCLP Total

DCE BFB DBFM T DCE BFB DBFM T

70‐125% 72‐125% 71‐125% 75‐125% 70‐128% 73‐126% 71‐128% 73‐127%

North Q1

20 99.4 94.4 101 91.6  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  113 106 104 97.9

North Q2

20 102 96.7 104 100  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  108 100 100 100

North Q3

20 95.3 97 99.6 105  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  107 104 103 98.7

North Q4

20 98.7 103 104 111  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  108 101 102 99.4

North Q4

(TCLP Basic) 20 106 96.7 103 100  ‐‐  ‐‐  ‐‐  ‐‐ 

North Q4

(TCLP Neutral) 20 104 93.9 101 95.9  ‐‐  ‐‐  ‐‐  ‐‐ 

South Q1

20 98.5 104 101 107  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  111 101 112 105

10  ‐‐  ‐‐  ‐‐  ‐‐  102 102 101 100

1250  ‐‐  ‐‐  ‐‐  ‐‐  98.3 94.7 99.7 91.8

South Q1

(TCLP Basic) 20 106 97.2 102 99  ‐‐  ‐‐  ‐‐  ‐‐ 

South Q1

(TCLP Neutral) 20 92.1 92.2 97.5 93.8  ‐‐  ‐‐  ‐‐  ‐‐ 

South Q2

20 101 101 107 109  ‐‐  ‐‐  ‐‐  ‐‐ 

10  ‐‐  ‐‐  ‐‐  ‐‐  101 101 94.3 100

1250  ‐‐  ‐‐  ‐‐  ‐‐  94.2 98.8 99.1 99.7

South Q3

20 98 101 101 102  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  115 101 98.7 97.9

South Q32

20 98.7 96.9 101 102  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  108 96.9 95.6 101

10  ‐‐  ‐‐  ‐‐  ‐‐  98.9 96.6 96.3 97.6

South Q4

20 106 104 109 102  ‐‐  ‐‐  ‐‐  ‐‐ 

1  ‐‐  ‐‐  ‐‐  ‐‐  106 99.4 96.3 99.7

Trip Blank 2 95.6 92 94.7 98.9

DCE = 1,2‐Dichloroethane‐d4

BFB = 4‐Bromofluorobenzene

DBFM = Dibromofluoromethane

T = Toluene‐d8
Table 6: Surrogate Recoveries – Semivolatile Organics

Sample ID Dilution

TCLP Total

2‐FBP 2‐FP 4‐TP NB P TBP 2‐FBP 2‐FP 4‐TP 

48‐

120%

20‐

120%

51‐

135%

41‐

120%

20‐

120%

36‐

126%

43‐

125%

37‐

125%

32‐

125%

North Q1 1 76.7 66.1 77 72.2 66 101 69.8 50.1 83.9 North Q2 1 64.9 52.5 79.3 61.4 59.7 88.7 72 58.7 79.9 North Q3

1 64.6 47.1 70.4 55.2 51.5 84.4 76.2 55.2 76.4 

5  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐  87.4 78.8 50.8 81 

North Q4

1 83.3 71.6 78.5 78.5 70.6 87 78.9 52.1 76.3 

5  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐  80.7 73.9 47.2 80.3 

North Q4(TCLP Basic) 1 70.6 57.2 66.1 66.6 54.8  ‐‐  ‐‐  ‐‐  ‐‐  North Q4(TCLP Neutral) 1 67.7 47.7 74.2 60.4 57.3  ‐‐  ‐‐  ‐‐  ‐‐  South Q1 1 68.8 53.7 80.1 62.9 63.5 84.2 73.3 52.5 77.4 South Q1(TCLP Basic) 1 72.4 59.4 81 71.7 67.1  ‐‐  ‐‐  ‐‐  ‐‐  South Q1(TCLP Neutral) 1 80.2 66.4 77 78.1 64.9  ‐‐  ‐‐  ‐‐  ‐‐  South Q2

1 66.4 51.3 81.6 57.7 58.4 89 77.6 53.7 78.8 

4  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐  87 75.2 49.9 77.9 

South Q3

1 57.3 50.6 75.3 56.7 56.7 97.5 101 48.4 75.9 

5  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐  89.8 80.3 45.7 86.3 

South Q32

1 67.3 55.5 74.9 66.3 58.4 88.9 91.5 52.4 69.7 

5  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐  73 61.6 40.2 64.4 

South Q4

1 71 61.7 79.8 66.7 73.3 93 79.6 52 79.6 

5  ‐‐  ‐‐  ‐‐  ‐‐  ‐‐  88 73.4 48.9 79.1 

TBP = 2,4,6‐Tribromophenol 2‐FP = 2‐Fluorophenol NB = Nitrobenzene‐d52‐FBP = 2‐Fluorobiphenyl 4‐TP = 4‐Terphenyl‐d14 P = Phenol‐d6
Table 7: MS/MSD Results – Sample South Q2

Spiked

Analyte

Un‐Spiked

Detected

Value

Spike

Value Units

MS MSD

RPD

Result %R Result %R 

Oil & Grease 4336 1600 mg/kg 3960 ‐23.5 3072 ‐79 25.3 Mercury 0.000004 0.005 mg/L 0.00522 104 0.0052 104 0.384 Mercury 569.3 354/339.6 ug/kg 856.6 81.2 876.1 90.4 2.24 Arsenic 0.04601 0.5 mg/L 0.5367 98.1 0.5489 101 2.25 Barium 0.623 0.5 mg/L 1.106 96.6 1.139 103 2.94 Cadmium  ‐0.002424 0.5 mg/L 0.4774 96 0.496 99.7 3.82 Chromium  ‐0.0004273 0.5 mg/L 0.4766 95.4 0.488 97.7 2.36 Lead 0.002698 0.5 mg/L 0.4829 96 0.4988 99.2 3.24 Selenium 0.001765 0.5 mg/L 0.4994 99.5 0.535 107 6.88 Silver  ‐0.001257 0.5 mg/L 0.4609 92.4 0.4711 94.5 2.19 Antimony 0.005452 0.5 mg/L 0.5157 102 0.5185 103 0.541 Beryllium  ‐0.001797 0.5 mg/L 0.4762 95.6 0.5017 101 5.22 Cobalt 0.000833 0.5 mg/L 0.4739 94.6 0.4737 94.6 0.0422 Nickel 0.1379 0.5 mg/L 0.5798 88.4 0.5962 91.7 2.79 Vanadium 0.007156 0.5 mg/L 0.5038 99.3 0.5008 98.7 0.597 Zinc 0.004523 0.5 mg/L 0.5121 102 0.5158 102 0.72 Arsenic 23.82 9.615/9.524 mg/kg 31.34 78.1 31.39 79.5 0.172 Barium 76.6 9.615/9.524 mg/kg 88.81 127 86.79 107 2.3 Cadmium 0.6739 9.615/9.524 mg/kg 9.169 88.4 9.119 88.7 0.549 Chromium 22.42 9.615/9.524 mg/kg 29.7 75.7 31.3 93.3 5.25 Cobalt 5.865 9.615/9.524 mg/kg 13.31 77.4 13.63 81.5 2.38 Lead 12.88 9.615/9.524 mg/kg 21.95 94.3 22.18 97.6 1.04 Nickel 47.18 9.615/9.524 mg/kg 53.39 64.7 52.56 56.5 1.57 Selenium 7.68 9.615/9.524 mg/kg 15.82 84.6 15.23 79.3 3.79 
Table 7: MS/MSD Results – Sample South Q2 (continued)

Spiked

Analyte

Un‐Spiked

Detected

Value

Spike

Value Units

MS MSD

RPD

Result %R Result %R 

Silver 0.04209 9.615/9.524 mg/kg 7.975 82.5 7.92 82.7 0.692 Vanadium 22.54 9.615/9.524 mg/kg 30.42 82 30.22 80.6 0.673 Zinc 475.6 9.615/9.524 mg/kg 471.9 ‐38.1 481.9 66.3 2.09 Beryllium 0.04753 9.615/9.524 mg/kg 8.958 92.7 8.911 93.1 0.518 2,4‐Dimethylphenol 3332/3328 ug/kg 3060 97.8 2935 88.2 4.19 2,4‐Dinitrophenol 3332/3328 ug/kg 1739 52.2 1916 57.6 9.67 2,4‐Dinitrotoluene 1666/1664 ug/kg 1913 115 1947 117 1.77 2‐Methylphenol 39.91 3332/3328 ug/kg 2960 87.6 2817 83.4 4.95 3&4‐Methylphenol 83.39 4998/4992 ug/kg 4632 91 4306 84.6 7.28 4‐Nitrophenol 3332/3328 ug/kg 3486 105 3029 91 14 Acenaphthene 1129 1666/1664 ug/kg 2462 80 2224 65.8 10.2 Anthracene 1056 1666/1664 ug/kg 2870 109 2326 76.3 20.9 Benz(a)anthracene 236.2 1666/1664 ug/kg 1582 80.8 1602 82.1 1.26 Benzo(a)pyrene 245.5 1666/1664 ug/kg 1820 94.5 1738 89.7 4.65 Benzo(b)fluoranthene 105.5 1666/1664 ug/kg 1436 79.9 1175 64.3 20 Benzo(k)fluoranthene 57.65 1666/1664 ug/kg 2015 117 1989 116 1.31 Bis(2‐ethylhexyl)phthalate 329.8 1666/1664 ug/kg 1987 99.4 1785 87.5 10.7 Butyl benzyl phthalate 1666/1664 ug/kg 1630 97.9 1560 93.8 4.41 Chrysene 667.3 1666/1664 ug/kg 2403 104 2131 88 12 Dibenz(a,h)anthracene 66.85 1666/1664 ug/kg 1746 101 1595 91.8 9.03 Diethyl phthalate 1666/1664 ug/kg 1572 94.4 1440 86.5 8.76 Dimethyl phthalate 1666/1664 ug/kg 1486 89.2 1401 84.2 5.86 Di(n)butyl phthalate 1666/1664 ug/kg 1638 98.3 1599 96.1 2.39 Di(n)octyl phthalate 20.09 1666/1664 ug/kg 1702 101 1700 101 0.137 
Table 7: MS/MSD Results – Sample South Q2 (continued)

Spiked

Analyte

Un‐Spiked

Detected

Value

Spike

Value Units

MS MSD

RPD

Result %R Result %R 

Fluoranthene 427.2 1666/1664 ug/kg 2364 116 2071 98.8 13.2 Fluorene 2609 1666/1664 ug/kg 3824 72.9 3796 71.3 0.725 Indeno(1,2,3‐cd)pyrene 101.4 1666/1664 ug/kg 1371 76.2 1205 66.3 12.9 Nitrobenzene 1666/1664 ug/kg 1455 87.3 1380 83 5.27 Phenanthrene 6641 1666/1664 ug/kg 7851 72.6 6260 ‐22.9 22.5 Phenol 69.92 3332/3328 ug/kg 2772 81.1 2632 77 5.2 Pyrene 1844 1666/1664 ug/kg 2988 68.6 2898 63.3 3.06 Pyridine 1666/1664 ug/kg 800.8 48.1 783.4 47.1 2.2 Quinoline 1666/1664 ug/kg 1795 108 1678 101 6.74 2,4‐Dimethylphenol 100 ug/L 84.97 85 82.73 82.7 2.67 2,4‐Dinitrophenol 100 ug/L 71.09 71.1 77.54 77.5 8.67 2,4‐Dinitrotoluene 50 ug/L 41.85 83.7 41.75 83.5 0.22 2‐Methylphenol 100 ug/L 77.39 77.4 76.88 76.9 0.665 3&4‐Methylphenol 1.348 150 ug/L 123.7 81.6 119.6 78.9 3.37 4‐Nitrophenol 100 ug/L 76.33 76.3 81.14 81.1 6.11 Acenaphthene 5.135 50 ug/L 50.2 90.1 48.85 87.4 2.73 Anthracene 50 ug/L 46.96 93.9 45.63 91.3 2.87 Benz(a)anthracene 50 ug/L 45.13 90.3 45.58 91.2 0.991 Benzo(a)pyrene 50 ug/L 45.1 90.2 43.79 87.6 2.94 Benzo(b)fluoranthene 50 ug/L 49.14 98.3 47.78 95.6 2.81 Benzo(k)fluoranthene 50 ug/L 43.82 87.6 44.25 88.5 0.974 Bis(2‐ethylhexyl)phthalate 50 ug/L 46.93 93.9 45.57 91.1 2.95 Butyl benzyl phthalate 50 ug/L 46.86 93.7 45.8 91.6 2.28 Chrysene 50 ug/L 47.27 94.5 44.33 88.7 6.42 
Table 7: MS/MSD Results – Sample South Q2 (continued)

Spiked

Analyte

Un‐Spiked

Detected

Value

Spike

Value Units

MS MSD

RPD

Result %R Result %R 

Dibenz(a,h)anthracene 50 ug/L 47.64 95.3 46.05 92.1 3.39 Diethyl phthalate 50 ug/L 41.23 82.5 41.24 82.5 0.037 Dimethyl phthalate 50 ug/L 41.47 82.9 40.14 80.3 3.25 Di(n)butyl phthalate 50 ug/L 47.22 94.4 44.64 89.3 5.62 Di(n)octyl phthalate 50 ug/L 45.34 90.7 46 92 1.44 Fluoranthene 50 ug/L 47.52 95 44.57 89.1 6.41 Fluorene 8.492 50 ug/L 51.08 85.2 49.87 82.8 2.39 Indeno(1,2,3‐cd)pyrene 50 ug/L 45.81 91.6 45.02 90 1.73 Nitrobenzene 50 ug/L 42.04 84.1 40.72 81.4 3.2 Phenanthrene 13.98 50 ug/L 59.01 90.1 53.25 78.5 10.3 Phenol 1.898 100 ug/L 77.53 75.6 73.6 71.7 5.2 Pyrene 50 ug/L 44.74 89.5 43.91 87.8 1.86 Pyridine 50 ug/L 33.32 66.6 33.92 67.8 1.8 Quinoline 50 ug/L 44.02 88 43.54 87.1 1.1 1,1,1‐Trichloroethane 500 ug/kg 477.8 95.6 381.4 76.3 22.4 1,1‐Dichloroethane 500 ug/kg 506.6 101 444.1 88.8 13.1 1,1‐Dichloroethene 500 ug/kg 508.3 102 420.7 84.1 18.9 1,2‐Dibromoethane 500 ug/kg 535.4 107 411.5 82.3 26.2 1,2‐Dichlorobenzene 500 ug/kg 472.3 94.5 298.1 59.6 45.2 1,2‐Dichloroethane 500 ug/kg 503.4 101 454.6 90.9 10.2 1,3‐Dichlorobenzene 500 ug/kg 460.9 92.2 292 58.4 44.9 1,4‐Dichlorobenzene 500 ug/kg 476.5 95.3 300.8 60.2 45.2 1,4‐Dioxane 10000 ug/kg 12540 125 12120 121 3.43 2‐Butanone 1000 ug/kg 1299 130 1142 114 12.8 
Table 7: MS/MSD Results – Sample South Q2 (continued)

Spiked

Analyte

Un‐Spiked

Detected

Value

Spike

Value Units

MS MSD

RPD

Result %R Result %R 

Benzene 11.2 500 ug/kg 508.2 99.4 418.9 81.5 19.3 Carbon disulfide 1000 ug/kg 974.1 97.4 725.2 72.5 29.3 Chlorobenzene 500 ug/kg 471.2 94.2 327.2 65.4 36.1 Chloroform 500 ug/kg 501.9 100 438.4 87.7 13.5 Ethylbenzene 302.4 500 ug/kg 598 59.1 627.9 65.1 4.87 Methyl tert‐butyl ether 500 ug/kg 545.5 109 515.7 103 5.63 Naphthalene 3721 500 ug/kg 1975 ‐349 3512 ‐41.8 56 Styrene 500 ug/kg 499.7 99.9 355 71 33.9 Tetrachloroethane 33.52 500 ug/kg 475.7 88.4 347.7 62.8 31.1 Toluene 289.5 500 ug/kg 615.1 65.1 696 81.3 12.3 Trichloroethene 500 ug/kg 538.2 108 459.6 91.9 15.8 Xylenes, total 2490 1500 ug/kg 2455 ‐2.31 3367 58.5 31.3 Naphthalene 85.95 1000 ug/kg 1106 102 1119 85.95 1.24 1,1,1‐Trichloroethane 1000 ug/L 890.4 89 936.5 93.6 5.04 1,1‐Dichloroethane 1000 ug/L 1051 105 961.8 96.2 8.86 1,1‐Dichloroethene 1000 ug/L 898.3 89.8 945.8 94.6 5.14 1,2‐Dibromoethane 1000 ug/L 1019 102 983 98.3 3.58 1,2‐Dichlorobenzene 1000 ug/L 997.9 99.8 930.9 93.1 6.94 1,2‐Dichloroethane 1000 ug/L 1051 105 1032 103 1.74 1,3‐Dichlorobenzene 1000 ug/L 922.1 92.2 924.5 92.4 0.256 1,4‐Dichlorobenzene 1000 ug/L 937.5 93.8 926.4 92.6 1.2 1,4‐Dioxane 20000 ug/L 17630 88.2 20670 103 15.9 2‐Butanone 2000 ug/L 2132 107 2040 102 4.42 Benzene 1000 ug/L 954.1 95.4 987.8 98.8 3.47 
Table 7: MS/MSD Results – Sample South Q2 (continued)

Spiked

Analyte

Un‐Spiked

Detected

Value

Spike

Value Units

MS MSD

RPD

Result %R Result %R 

Carbon disulfide 2000 ug/L 1780 89 1940 97 8.58 Chlorobenzene 1000 ug/L 903.5 90.4 911.9 91.2 0.921 Chloroform 1000 ug/L 1050 105 960.1 96 8.92 Ethylbenzene 1000 ug/L 885.4 88.5 901.7 90.2 1.82 Methyl tert‐butyl ether 1000 ug/L 994 99.4 1021 102 2.66 Naphthalene 85.95 1000 ug/L 1106 102 1119 103 1.24 Styrene 1000 ug/L 952.5 95.2 916.5 91.7 3.85 Tetrachloroethane 1000 ug/L 741.5 74.2 855.8 85.6 14.3 Toluene 11.04 1000 ug/L 911.4 90 940.5 92.9 3.15 Trichloroethene 1000 ug/L 893.8 89.4 920.5 92 2.94 Xylenes, total 56.84 3000 ug/L 2759 90.1 2739 89.4 0.726 Cyanide (9014) 0.9341 9.191/9.18 mg/kg 9.191 89.8 9.18 89.8 0.12 Cyanide (9010) 0.005 0.2 mg/L 0.188 91.5  ‐‐  ‐‐  ‐‐  Sulfide 96.8 1075 mg/kg 553.6 42.5 553.6 96.8 0 Cyanide, reactive 250 mg/kg 234.9 94 234.9 94 0 MS = Matrix Spike

MSD = Duplicate Matrix Spike%R = Percent Recovery

RPD = Relative Percent Difference
Table 8: Total Analytical Results

Analyte North Q1 North Q2 North Q3 North Q4 South Q1 South Q2 South Q3 

Sulfide 72.8 H 72.8 H 48.8 H 145 H 133 H 96.8 H 84.8 H Cyanide 3.13 J 1.72 J 1.2 U 1.3 U 1.4 U 2.03 J 7.72 Cyanide, Amenable 1.4 U 1.6 U 1.2 U 1.3 U 1.4 U 1.2 U 3.09 J Mercury 0.416 0.274 0.205 0.428 0.972 1.24 1.46 Antimony 1.89 1.13 J 0.55 U 0.939 J 1.8 1.87 1.04 J Arsenic 22.1 28.6 12.9 30.4 60.1 51.7 38 Barium 181 135 61.4 125 196 166 130 Beryllium 0.13 U 0.12 U 0.11 U 0.11 U 0.11 U 0.11 U 0.11 U Cadmium 0.484 J 0.794 J 0.286 J 0.976 J 1.26 1.46 1.25 Chromium 23.7 30.4 11.5 28.9 152 48.7 37.8 Cobalt 6.61 8.23 3.54 6.12 24.4 12.7 9.9 Lead 15.7 15.8 5.79 14.1 43.1 28 23 Nickel 29.8 42.9 16.4 42.4 212 102 87.7 Selenium 20.9 14.9 3.91 9.46 100 16.7 13.7 Silver 0.1 U 0.095 U 0.088 U 0.087 U 0.16 J 0.0913 J 0.086 U Vanadium 28.5 43.3 17.3 36.4 114 48.9 38.1 Zinc 358 997 227 659 1010 1140 922 Percent Moisture1 62.4 62.6 57.4 57.3 57.4 53.9 58.7 Oil and Grease 9970 1730 921 1360 2710 9410 3090 pH2 9.17 8.76 8.58 8.86 10 10.2 9.53 Reactive Cyanide 23 U 23 U 23 U 23 U 23 U 23 U 23 U Reactive Sulfide 14 U 14 U 14 U 14 U 14 U 14 U 14 U 2,4‐Dimethylphenol 0.098 U 0.099 U 0.087 U 0.086 U 0.087 U 0.08 U 0.13 U 2,4‐Dinitrophenol 0.17 U 0.17 U 0.15 U 0.15 U 0.15 U 0.14 U 0.23 U 2,4‐Dinitrotoluene 0.16 U 0.16 U 0.14 U 0.14 U 0.14 U 0.13 U 0.22 U 2‐Methylphenol 0.096 U 0.096 U 0.085 U 0.1 J 0.085 U 0.087 J 0.17 J 
Table 8: Total Analytical Results (continued)

Analyte North Q1 North Q2 North Q3 North Q4 South Q1 South Q2 South Q3 

3&4‐Methylphenol 1.6 0.17 U 0.15 U 0.23 J 0.15 U 0.18 J 0.47 J 4‐Nitrophenol 0.16 U 0.16 U 0.14 U 0.14 U 0.14 U 0.13 U 0.22 U Acenaphthene 1.5 2.1 4.3 4.2 0.52 2.5 8 Anthracene 1 1.7 2.9 4.4 0.42 2.3 18 Benz(a)anthracene 0.22 J 0.24 J 0.49 0.56 0.14 J 0.51 3.6 Benzo(a)pyrene 0.23 J 0.27 J 0.52 0.59 0.093 J 0.53 1.5 Benzo(b)fluoranthene 0.08 U 0.1 J 0.18 J 0.14 J 0.07 U 0.23 J 0.6 J Benzo(k)fluoranthene 0.13 J 0.1 J 0.28 J 0.2 J 0.07 U 0.13 J 0.66 Bis(2‐ethylhexyl)

phthalate 0.5 0.55 0.78 0.87 0.22 J 0.72 1.8 

Butyl benzyl phthalate 0.08 U 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U Chrysene 0.23 J 0.8 1.6 1.5 0.24 J 1.4 4.2 Dibenz(a,h)anthracene 0.08 U 0.08 U 0.17 J 0.07 U 0.099 J 0.15 J 0.11 U Diethyl phthalate 0.08 U 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U Dimethyl phthalate 0.08 U 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U Di‐n‐butyl phthalate 0.08 U 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U Di‐n‐octyl phthalate 0.19 J 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U Fluoranthene 0.08 U 0.65 1.7 1.6 0.21 J 0.93 3.8 Fluorene 2.8 3.4 8.3 8.6 0.83 5.7 19 Indeno(1,2,3‐cd)pyrene 0.08 U 0.08 U 0.07 U 0.16 J 0.11 J 0.22 J 0.44 J Nitrobenzene 0.088 U 0.088 U 0.077 U 0.077 U 0.077 U 0.072 U 0.12 U Phenanthrene 8.1 11 27 27 2.8 15 62 Phenol 0.32 J 0.08 U 0.084 J 0.11 J 0.07 U 0.15 J 0.22 J Pyrene 2 2.5 4.8 6.5 0.6 4 9.7 Pyridine 0.08 U 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U Quinoline 0.08 U 0.08 U 0.07 U 0.07 U 0.07 U 0.065 U 0.11 U 
Table 8: Total Analytical Results (continued)

Analyte North Q1 North Q2 North Q3 North Q4 South Q1 South Q2 South Q3 

1,1,1‐Trichloroethane 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,1‐Dichloroethane 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,1‐Dichloroethene 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,2‐Dibromoethane 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,2‐Dichlorobenzene 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,2‐Dichloroethane 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,3‐Dichlorobenzene 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,4‐Dichlorobenzene 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U 1,4‐Dioxane 0.053 U 0.053 U 0.047 U 0.047 U 0.047 U 0.43 U 0.048 U 2‐Butanone 0.083 0.029 0.032 0.0033 U 0.12 0.03 U 0.043 Benzene 0.0035 J 0.0088 J 0.031 0.0076 J 0.018 0.024 J 0.0072 J Carbon disulfide 0.0083 J 0.0027 U 0.0023 U 0.0023 U 0.0023 U 0.022 U 0.0024 U Chlorobenzene 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U Chloroform 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U Ethylbenzene 0.11 0.033 0.045 0.035 0.24 0.66 0.14 Methyl tert‐butyl ether 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U Naphthalene 0.086 0.46 0.39 0.11 90 83 0.34 Styrene 0.0013 U 0.0013 U 0.0012 U 0.0012 U 0.0012 U 0.011 U 0.0012 U Tetrachloroethene 0.04 0.037 0.03 0.025 0.072 0.073 J 0.042 Toluene 0.068 0.037 0.11 0.052 0.3 0.63 0.17 Trichloroethene 0.0027 J 0.0021 J 0.003 J 0.004 J 0.0076 J 0.011 U 0.0071 J Xylenes, Total 0.46 0.25 0.37 0.25 7.6 5.4 0.77 Ignitability, Solid3 Negative Negative Negative Negative Negative Negative Negative 

Unless otherwise noted, units are mg/kg‐dry.

1 Units for percent moisture are weight percent.

2 Units for pH are standard units.

3 There are no units for ignitability.
Table 9: TCLP Analytical Results

Analyte North Q1 North Q2 North Q3 North Q4

North Q4

(TCLP Basic)

North Q4

(TCLP Neutral) South Q1

South Q1

(TCLP Basic)

(T

Cyanide Mercury 0.000042 U 0.000042 U 0.000042 U 0.000042 U 0.000042 U 0.000042 U 0.000042 U 0.000052 J 0Arsenic 0.0144 J 0.0543 0.157 0.0586 0.114 0.0195 J 0.0118 J 0.107 Barium 1.12 0.836 1.07 0.706 0.0359 J 0.0467 J 0.621 0.0457 J Cadmium 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U Chromium 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U 0.006 U Lead 0.004 U 0.004 U 0.004 U 0.00452 J 0.004 U 0.004 U 0.00535 J 0.00431 J 0Selenium 0.025 U 0.025 U 0.025 U 0.025 U 0.0265 J 0.025 U 0.025 U 0.18 Silver 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U Antimony 0.005 U 0.005 U 0.005 U 0.00537 J 0.00729 J 0.00504 J 0.005 U 0.00743 J Beryllium 0.003 U 0.003 U 0.003 U 0.003 U 0.003 U 0.003 U 0.003 U 0.003 U Cobalt 0.00737 J 0.005 U 0.00592 J 0.005 U 0.005 U 0.005 U 0.005 U 0.00614 J Nickel 0.116 0.0287 J 0.173 0.068 0.0148 J 0.014 U 0.132 0.0317 J Vanadium 0.00956 J 0.015 J 0.0202 J 0.0121 J 0.13 0.0113 J 0.007 U 0.055 Zinc 0.0881 0.025 U 0.0595 0.025 U 0.0377 J 0.025 U 0.0436 J 0.227 2,4‐Dimethylphenol 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 2,4‐Dinitrophenol 0.0014 U 0.0014 U 0.0014 U 0.0014 U 0.0014 U 0.0014 U 0.0014 U 0.0014 U 2,4‐Dinitrotoluene 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 2‐Methylphenol 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 3&4‐Methylphenol 0.024 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.0052 0.001 U 4‐Nitrophenol 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U 0.0019 U Acenaphthene 0.0019 J 0.0031 J 0.0036 J 0.0033 J 0.003 J 0.0043 J 0.002 J 0.0009 U Anthracene 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0017 J 0.0006 U 0.0006 U Benz(a)anthracene 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U Benzo(a)pyrene 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U Benzo(b)fluoranthene 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U Benzo(k)fluoranthene 0.0009 U 0.0009 U 0.0009 U 0.0009 U 0.0009 U 0.0009 U 0.0009 U 0.0009 U Bis(2‐ethylhexyl)

phthalate 0.0033 U 0.0033 U 0.0033 U 0.0033 U 0.0033 U 0.0033 U 0.0033 U 0.0033 U 

Butyl benzyl phthalate 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U 0.0007 U Chrysene 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U Dibenz(a,h)anthracene 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U Diethyl phthalate 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U Dimethyl phthalate 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U Di‐n‐butyl phthalate 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U Di‐n‐octyl phthalate 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 
Table 9: TCLP Analytical Results (continued)

Analyte North Q1 North Q2 North Q3 North Q4

North Q4

(TCLP Basic)

North Q4

(TCLP Neutral) South Q1

South Q1

(TCLP Basic)

(

Fluoranthene 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0035 J 0.0005 U 0.0005 U Fluorene 0.003 J 0.005 0.0064 0.0054 0.0053 0.0081 0.0031 J 0.0014 J Indeno(1,2,3‐cd)pyrene 0.0013 U 0.0013 U 0.0013 U 0.0013 U 0.0013 U 0.0013 U 0.0013 U 0.0013 U Nitrobenzene 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U 0.0008 U Phenanthrene 0.0047 J 0.0084 0.011 0.009 0.0096 0.018 0.0053 0.0024 J Phenol 0.0033 J 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0032 J 0.0005 U Pyrene 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0005 U 0.0026 J 0.0005 U 0.0005 U Pyridine 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Quinoline 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 0.0006 U 1,1,1‐Trichloroethane 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,1‐Dichloroethane 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,1‐Dichloroethene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,2‐Dibromoethane 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,2‐Dichlorobenzene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,2‐Dichloroethane 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,3‐Dichlorobenzene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,4‐Dichlorobenzene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 1,4‐Dioxane 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2‐Butanone 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U Benzene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Carbon disulfide 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U Chlorobenzene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Chloroform 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Ethylbenzene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Methyl tert‐butyl ether 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Naphthalene 0.044 J 0.01 U 0.01 U 0.032 J 0.01 U 0.01 U 0.056 J 0.044 J Styrene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Tetrachloroethene 0.012 U 0.012 U 0.012 U 0.012 U 0.012 U 0.012 U 0.012 U 0.012 U Toluene 0.017 J 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.013 J 0.02 J Trichloroethene 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Xylenes, Total 0.071 J 0.03 U 0.03 U 0.03 U 0.03 U 0.03 U 0.068 J 0.065 J 
Table 10: ALS Equipment

Item Description Manufacturer/Model

GC with FID (FID #2)    HP 5890A, HP7673 Injector   

GC with FID/FPD (FID #1)    HP 5890A, HP7673A Injector   

GC with FID (FID#3)    HP 5890A Series II, HP7673A Injector   

GC with FID (FID #4) / with Headspace

Analyzer   

HP 5890A Series II / HTA HT280T Headspace

Autosampler   

GC with FID, Dual Thu‐put (FID#7 / #8)    Agilent 6890N, Dual Column/FID   

GC with FID, Dual Thu‐put (FID#10 / #11)    Agilent 6890N, Dual Column/FID   

GC with FID (FID#6‐ GRO)    HP 5890 Series II,   

Purge & Trap Conc, for GRO    OI 4560 (for FID #6)   

Purge & Trap Concentrator    OI 4552 Autosampler (for FID 6 )   

GC with FID (FID#9‐ GRO)    Agilent 6890 GC   

Purge & Trap Concentrator    Tekmar 3100 (for FID #9 – GRO)  

Closed Loop Multi‐sampler    OI 4552 Multi‐sampler (FID#9)   

GC Dual PID (BTEX 1&2)    HP 5890 Series II   

Purge & Trap Concentrator    Tekmar 3000 (BTEX 1&2)  

Closed Loop Multi‐sampler    Varian Archon Sampler (BTEX 1&2)   

GC Dual PID (BTEX 3&4)    HP 5890 Series II   

Closed Loop Multi‐sampler    Varian Archon Sampler (BTEX 3&4)   

Purge & Trap    Tekmar 3000   

GC Dual ECD (ECD 1&2)    HP 5890 Series II, HP7673 Injector   

GC Dual ECD (ECD 3&4)    HP 5890 Series II, HP7673 Injector   

GC Dual ECD (ECD 5&6)    HP 5890 Series II, HP7673 Injector   

GC Dual ECD (ECD 7&8)    Agilent 6890N, dual micro ECDs,   Agilent 7683B

Injector  

GC Dual ECD (ECD 9&10)    HP 5890 Series II, HP7673 Injector   

GC/MSD (VOA1)    HP5890 Series II with HP5972A MSD   

Closed Loop Multi‐sampler    Varian Archon Multi‐sampler (VOA1)   

Purge & Trap Concentrator    HP Purge and Trap (VOA 1)   

GC/MSD II (VOA2)    Agilent 6890 GC with 5973A MSD   

Closed Loop Multi‐sampler    Varian Archon Multi‐sampler (VOA2)   

Purge & Trap Concentrator    Tekmar Dohrmann Velocity (VOA2)   

GC/MSD II (VOA3)    HP5890 Series II with HP5972A MSD   

Closed Loop Multi‐sampler    Varian Archon Multi‐sampler (VOA3)   

Purge & Trap Concentrator    Tekmar Dohrmann 3100 (VOA3)   

GC/MSD II (VOA4)    Agilent 6890 GC with 5973 Inert MSD  

Closed Loop Multi‐sampler    Varian Archon Multi‐sampler (VOA4)   

Purge & Trap Concentrator    Tekmar Dohrmann Velocity (VOA4)   

GC/MSD II (VOA5)    Agilent 6890 GC with 5975 Inert MSD  

   
Table 10: ALS Equipment (continued)

Item Description Manufacturer/Model

Closed Loop Multi‐sampler    Tekmar/Dohrmann SOLATek (VOA5)  

Purge & Trap Concentrator    Tekmar Dohrmann Velocity (VOA5)   

GC/MSD II (VOA5)    Agilent 6890 GC with 5975 Inert MSD  

Closed Loop Multi‐sampler    Varian Archom (VOA5)   

Purge & Trap Concentrator    Tekmar Dohrmann Velocity (VOA5)   

GC/MSD II (SV2)    Agilent 6890 Plus with 5973 MSD  

GC/MSD III (SV3)    Agilent 6890 Plus with 5973 MSD  

GC/MSD IV (SV4)    Agilent 6890 Plus with 5973 MSD  

GC/MSD V (SV5)    Agilent 6890 Plus with 5973 MSD   

Soxtec Extraction Unit (1)    Model 2055 (Total Ext. Capacity = 6)   

Soxtec Extraction Unit (2)    Model 2055 (Total Ext. Capacity = 6)   

HPLC – with UV and   Fluorescence

detectors    Agilent 1100 Series HPLC, with autosampler  

UV/VIS   Shimadzu UV‐2450   

Ion Chromatograph    Dionex ICS‐3000   

ICP/MS    Agilent 7500 Series ORC  

ICP/MS    Agilent 7500 Series ORCE   

ICP/MS    Agilent 7500 Series ORCE   

Mercury Analyzer    CETAC Technologies M‐6000A  

TOC Analyzer (for waters)    OI 1010 TOC Analyzer & Autosampler   

TOC Analyzer (for soils)    OI TOC Solids Analyzer   

Cyanide Distillation    Environmental Express 10 position   

Ammonia Distillation    Environmental Express 10 position   

Vortex    Fisher Genie 2   

Stirrer    Labline Multi Magnestir  

Centrifuge (4)    IES   

Water Bath   Precision  

Nitrogen Evaporator   Organomation N‐Evap  

Turbo Vap II (2 units)    Caliper Life Sciences, Turbo Vap II   

3‐D Shaker    Glass‐col   

Multi‐tube Vortexer    VWR VX 2500  

GPC    OI Analytical Autoprep 2000   

Furnace    Thermodyne  

Furnace    Thermodyne  

Sonicator Ultrasonic    Heat System XL   

Ultrasonic Bath (3)    Branson 2200   

Hot Plate (2)    Corning PC 104   

Hot Block Digesters (2)    Environmental Express   

   
Table 10: ALS Equipment (continued)

Item Description Manufacturer/Model

Hot Block Digesters (2)    Environmental Express   

Analytical balances (6)    Mettler AE 200 (2), Mettler AE 163(2), Fisher

A160, Cahn Micro‐balance (1)   

Analytical balance    Ohaus ScoutPro 400g   

Analytical balance    Shimadzu UniBlock AUX220   

Specific Ion/pH Meter (2)    Fisher Accumet AR‐50   

Specific Ion/pH Meter    Fisher Accumet AR‐50   

PH Meter    Mettler Toledo SevenEasy  

ZHE Extraction Units (9)    Environmental Express   

Top Loading balance (1)    Mettler 4400   

Top Loading balance (1)    Denver Instruments APX‐1502   

Forced Air Oven    VWR FM 1390   

Drying Oven (2)    VWR Model 1326   

Full Size Refrigerator/Freezer (3)    Labline Explosion Proof   

13' x 40'   Walk‐in Refrigerator    Thermo‐Kool   

8' x 10'   Walk‐in Refrigerator    NorLake   

8' x 10'   Walk‐in Freezer    NorLake   

Refrigerators (5)    Various   

Freezer (3)    Hussmann/Tappan  

ELIMS Database    e‐LIMS   

Computer Servers (4)    HP and Compaq   

Computer Server (Target)    e‐Lab Analytical, Inc.   

SQL Server (eLIMS)    e‐Lab Analytical, Inc.