-..

Docket No. A-92-45

Item IXc-B-l

MEMORANDUM

TO: Group IV Polymers and Resins Docket A-92-45

FROM: Keith Barnett, EPAJOAQPSIESDIOCG

DATE: December 2000

SUBJECT: Final Analysis ofEquipment Leak Program for PET Facilities Subject 10 the

Group IV Polymers and Resins NESHAP

Based on comments received on the June 8, 1999, proposed denial of petitions for

reconsideration on the Group IV equipment leak provisions as they apply to PET facilities, a final

equipment leak analysis (hereafter referred to as the December 2000 analysis) has been

developed. This memo presents the results of the December 2000 analysis and summarizes the

changes that have been made to the previous analysis entitled "Equipment Leak Analysis for

PET Facilities Subject to the Group IV Polymers and Resins NESHAP," October 26, 1998,

which may be found in Docket A-92-45 as Item VIc-B-l (hereafter referred to as the October

1998 analysis). Table 1 summarizes the changes made to the October 1998 analysis.

RESULTS

Table 2 presents the results ofthe December 2000 analysis by subcategory and compares

the results with those presented in the October 1998 analysis (i.e., Docket Item Vlc-B-I). As

seen in Table 2, the October 1998 analysis cost effectiveness ratios range from $1,400 to $2,300

per Mg of HAP emission reduction. The cost effectiveness ratios of the equipment leak program

under the December 2000 analysis range from $1,800 to $3,600 per Mg of HAP emission

reduction.

Appendix A presents the cost effectiveness values for each ofthe individual facilities by

subcategory. Appendix B presents the facility specific cost spreadsheets for the December 2000

analysis. Appendix C presents the facility specific emissions and emission reduction spreadsheets

for the December 2000 analysis.

DISCUSSION

The following paragraphs discuss the changes made to the October 1998 analysis.

1
TABLE 1. SUMMARY OF CHANGES MADE TO OCTOBER 1998 ANALYSIS

ITEM DESCRIPTION OF CHANGE

Monitoring Costs Increased initial monitoring costs for pumps. valves. and connectors in

gas/vapor or light liquid service.

Eastman Kodak. Rochester Incorporated compliance with 6 NYCRR Part 236 into baseline.

Tennessee Eastman and Carolina Incorporated new data on leak frequencies and emission factors for

Eastman components subject to Method 21 monitoring.

DuPont conneclors in gas/vapor Incorporated new data on emission factors for conneClors in gas/vapor or

or light liquid service light liquid service for DuPont.

Monitoring periods Decreased expected monitoring frequency for (I) connectors at all facilities.

(2) valves in gas/vapor service at Carolina Eastman. and (3) valves in light

liquid service at ICI-Fayetteville.

In-House vs Subcontraclor Applied the 500 or fewer components subject to Method 21 rule for using

personnel in-house personnel to those facilities in which during anyone month 500 or

fewer components subject to Method 21 would be monitored.

Facilities that did not provide Estimated leak frequencies and emission factors for components subject to

company- or facility-specific data Method 21 at facilities for which company- or facility-specific data were not

for components subject to provided using company- or facility-specific data provided by other

Method 21 monitoring companies.

TABLE 2 SUMMARY OF COST EFFECrIVENESS RESULTS

($/Mg of emission' reduction)

Subcategory October 1998 Analysis December 2000 Analysis

DMT-Balch 2.291 3.600

DMT-Continuous 1,401 2,991

TPA-Conlinuous 1.769 1.821

TPA-Batch 1,812 1.812

2
Initial Monitoring Cost Changes

Table 3 summarizes the changes made to the initial monitoring costs for pumps in light

liquid service, valves in gas or light liquid service, and connectors in gas or light liquid service.

As seen in Table 3, the cost per component for initial monitoring for these components were

increased from $4.65 to $17.70 per component when using a subcontractor and from either $0.75

or $3.75 to $16.50 per component when using in-house personnel. No changes were made to any

of the other cost components.

TABLE 3. INITIAL MONITORING COST CHANGES

($ per component)

October 1998 Analysis December 2000 Analysis

Component Subcontractor In-House Subcontractor In-House

Personnel Personnel Personnel Personnel

Pumps, light liquid service 4.65 3.75

Valves, gas service

Valves, light liquid service 17.70 16.50 4.65 0.75

Connectors, gas service

Connectors, light liquid service

Eastman Kodak - Rochester. New York

Based on comments from Eastman Kodak, their Rochester, New York, facility is subject

to 6 NYCRR Part 236 - Synthetic Organic Chemical Manufacturing Facility Component Leaks

(see Appendix D). The cost for c,!mplying with Part 236 was calcqlated and the incremental cost

for complying with the Group IV equipment leak program was then calculated.

TABLE4. mCREMENTALCOST~CTIVENESSFOR

EASTMAN KODAK'S ROCHESTER FACILITY

Annual Costs ($) Rule Requirement Annual Emission Cost Effectiveness ($JMg of

Reduction (Mglyr) emission reduction)

Part 236 8,079 2.47 3,271

Group IV Resins 12,675 3.02 4,197

Increments 4,596 0.55 8,356

3
Tennessee Eastman and Carolina Eastman Facilities

Based on comments and data supplied by Tennessee Eastman and Carolina Eastman, the

revised analysis incorporates new emission factors and leak frequencies for their facilities. Table

5 presents these new emission factors and leak f~uencies. The following paragraphs discuss

the derivation of these factors and leak frequencies.

Uncontrolled Emission Leak Factors: These values were taken or derived from

spreadsheets submi.tted b~ Eastm~n..N?te that Eastmans'su~m~ttal showed a rate of 0.00143 for

pumps in light liqUid service, which IS Incorrect based on their Excel spreadsheet. The correct

value is 0.01433 lbs/hr/component.

Total Number of Components: These were determined based on the Excel spreadsheets

provided by Eastman.

Number of Components Leaking Above the nON Definition: For valves and

connectors, 500 ppm is the leak definition used. For pumps, 5,000 ppm is the leak definition

used for polymerizing monomers, which would be applicable to PET facilities. The 1,000 ppm is

shown for comparison. The number of leakers were determined from th~ Excel spreadsheets by

sorting from low to high on the screening values and then counting the number of components at

or above the leak definition level.

Percent Leakers: This is simply the number of components leaking divided by the total

number of components.

Subsequent Leak Rate: For those components whose initial percent leak rate is less than

the subsequent leak rate attributable to the HON program, the subsequent leak 'rate was assumed

to be the same as the initial leak rate. For Valves, light liquid service at Tennessee Eastman and

for pumps, light liquid service at Carolina Eastman, the initial leak rates were higher than the

HON's subsequent leak rate. For valves, light liquid service, the HON's subsequent leak rate of

2% was used. For pumps, light liquid service at Carolina Eastman, an extrapolation was used.

The HON reports initial and subsequent leak rates of 17.1% and 8.04% with a leak definition of

1,000 ppm. Since the relevant leak definition for PET facilities is 5,000 ppm, the subsequent

leak frequency was extrapolated as follows: 8.93% x (8.04/17.1) =4.2%.

Subsequent Emission }'actor: For those components whose subsequent leak rate

was assumed to be the same as the initial leak rate, the following assumptions were made: (1)

the same percentage of components found to be not leaking continued to be non-leaking and

emitting at the same rate for the entire monitoring period and for the entire year, (2) the same

percentage of components found leaking at the start were found leaking each monitoring period

for the year, and (3) the leaking components would increase linearly during each monitoring

period, resulting in emissions occurring over the year at one-half the uncontrolled leaker

emission factor.

4
TABLE 5. EASTMAN EMISSION FACTORS AND LEAK FREQUENCIES

UncontroJled Emission Factor Number of Percent Subsequent Non-Leak

Components Leakers Subsequent (Ibslhr/component) Total and Leak Rates (%)

Component Number of Leaking (0/0) Emission

aboveHON Rate (lbslhrl

AU Non-Iekaing Leaking Components Leak Non- Leakers component)

Components Components Components Definition

Initial leakers

Tennessee Eastman

Pumps. light liquid 0.00385 0.0023053 0.308644 198 1at 5,000 0.51 99.49 0.51 0.00308

ppm

Valves, gas/vapor 0.00030 0.00008985 0.01444 538 8 1.49 98.51 1.49 0.000196

Valves. light liquid 0.00082 0.00030118 0.02176 3,893 94 2.415 98.00 2.00 0.000513

Connectors (gas/vapor 0.00038 0.00022085 0.036043 14,138 63 0.44 99.56 0.44 0.000299 and light liquid)

Carolina Eastman

9 at 1,000 16.1 at 5.000

Pumps. light liquid 0.01433 0.00313 0.1287 56 ppm ppm:

at 5.000 0.00570 5 at 5.000 8.93 95.8 ppm: 4.2

ppm

Valves. gas/vapor 0.000026 0.00002 0.00168466 300 1 0.33 99.67 0.33 0.ססOO227

Valves, light liquid 0.00013 0.00006454 0.00418874 1,318 20 1.52 98.48 1.52 0.0000954

Connectors (gas/vapor

and light liquid) 0.000047 O.OOOOtS86 0.011634 4.906 13 0.265 99.735 0.265 0.0000312

5
For valves, light liquid service at Tennessee Eastman, 98% of the valves were assumed

to be non-leaking each monitoring period at the average leak rate for those valves found to be not

leaking at the initial monitoring and 2% of the valves were assumed to be leaking each

monitoring period at one-half the average leak rate for those valves found to be leaking at the

initial monitoring. (The one-half assumption is equivalent to leaking at the full average leak rate

for leakers starting at the mid-way point in each monitoring period or for 4,380 hours per year.)

For pumps, light liquid service at Carolina Eastman. 95.8% of the pumps were

assumed to be non-leaking each monitoring at the average leak rate for those pumps found to be

not leaking at the initial monitoring and 4.2% of the pumps were assumed to be leaking each

monitoring period at one-half the average leak rate for those pumps found to be leaking at the

initial monitoring. (The one-half assumption is equivalent to leaking at the full average leak rate

for leakers starting at the mid-way point in each monitoring period or for 4,380 hours per year.)

The subsequent emission factors arc calculated using the following equation:

(% non-leakers x non-Ieaker emission factor) + (% leakers x leaker emission factor x 0.5)

DuPont Connectors in Gas/Vapor Service or Light Liquid Service

DuPont identified an average emission factor of 0.00022 Ibs/hr/component for connectors

in gaslvapor or light liquid service. DuPont noted that according to their data the was no

statistical difference between initial and subsequent leak frequencies for these connectors. As for

components at Eastman facilities that showed the same initial and subsequent leak frequencies,

an average emission factor was developed to estimate emissions that would occur between

subsequent monitoring event. The average emission factor developed is 0.00014

Ibs/hr/component. This factor was derived as follows:

1. An initial leak frequency of 0.52 percent was assigned to these connectors. This leak

frequency is the average of the reported leak frequencies for these connectors from Tennessee

Eastman, Carolina Eastman. and ICI-Fayetteville [(0.265 + 0.44 + 0.86)/3 =0.52).

2. Subsequent leak frequency was assumed to be 0.5 percent, which is the expected

subsequent leak frequency for these components under the rule. This subsequent leak frequency

is essentially identical to DuPont's assertion that they found no statistical difference between

initial and subsequent leak frequencies.

3. Non-Ieaker and leaker emission factors that correspond to the initial leak rate of

0.00022 Ibs/hr/component were calculated by first assuming the ratio ofthe leakers' leak rate to

the non-Ieakers' leak rate is the same as the average ratio found at Tennessee Eastman and

Carolina Eastman. The ratios at these two companies are 163.2 for Carolina Eastman and 733.55

for Tennessee Eastman, yielding an average ratio of 448.37. Next, the following equation was

solved to deterinine the leak rate for each non-leaking connector:

6
Non-leaker emission rate = 0.00022 =0.00006596 lbslhr/component

0.99478 + (0.00522 x 448.37)

The leaker emission rate =0.00006596 x 448.37 =0.02958 lbslhr/component

4. The average emission factor was then calculated as follows:

(0.OOO06596 x 0.99478) + (0.02958 x 0.005 x 0.5) =0.0001396lbs/hr/component

These initial emission and subsequent average emission factors and leak frequencies were

applied to all DuPont facilities in the December 2000 analysis.

In-House versus Subcontractor Personnel

In the December 2000 analysis. the detennination of whether a facility would use inhouse personnel or subcontractor personnel is based on the estimated number of components that

would be monitored in anyone month. Ifthis number is equal to or less than 500 components.

the facility is assumed to use in-house personnel. If this number is greater than 500 components.

the facility is assumed to use subcontractor personnel. Table 6 summarizes the estimated

maximum number of components that would be subject to Method 21 monitoring in anyone

month period.

In calculating this number of components. the monitoring period for connectors in ,

gas/vapor or light liquid service was estimated to be once every four years. Thus. one quarter of

the total number of connectors in gas/vapor or light liquid service would be monitored each year.

Within each year. it was assumed that one quarter ofthese components would be monitored each

quarter. For example, if a facility has 800 connectors in gas/vapor or light liqUid service, 200 of

these connectors would be monitored each year over four years. Within each year, 50 connectors

would be monitored in each of four months (to correspond to the quarterly mOnitoring of valves).

Leak Frequencies and Emission Factors for "Other Facilities"

In the December 2000 analysis, uncontro]]ed emission factors and initial leak frequencies

identified by specific companies for specific components subject to Method 21 monitoring were

extended to the other facilities that did not identify leak frequencies and emission factors specific

to their facilities or to components not addressed by companies that did submit company- or

facility-specific infonnation. In general, initial leak frequencies, subsequent leak frequencies.

and uncontrolled emission rates were calculated as averages of reported initial leak frequencies,

subsequent leak frequencies. and uncontrolled emission rates. Then, ratios ofleaker emission

factors to non-Ieaker emission factors were calculated based on Carolina Eastman and Tennessee

Eastman data. Lastly, the subsequent average emission factor was calculated using the same

equation shown earlier for DuPont connectors. Controlled emission factors for several Hoechsl

Celanese and ICI-Fayetteville components were also re-estimated using this procedure.

Appendix E presents a spreadsheet showing these calculations.

7
TABLE 6. ESTIMAnON OF MAXnvruM: NUMBER OF COfvlPONENTS TO MONITOR IN ONE MONTH

Total Number of Personnel to be

Valves. light Connectors. Components to Used to Conduct

Pumps, gas/vapor and Company Location Process light liquid Valves, gas liquid Monitor in One Method 21

light liquid Month MonitorinR

3M Decatur DMT-B 4 66 18 14.3 162 In-House

3M Greenville DMT-B 2 34 40 7.4 83 In-House

BASF Lowland DMT-B 8 135 160 29.4 332 In-House

Eastman Kodak Rochester DMT-B 4 75 89 16.4 184 In-House

Hoechst Shelby DMT-B 0 37 146 30.8 214 In-House

Celanese

DMT-B 4 431 116 21.3 572

Hoechsl Spartanburg

DMT-C 14 204 250 142.1 610

Celanese TPA.c 0 8 0 0.0 8

Totals 18 643 366 163.3 1190 Subcontractor

leI Fayetteville DMT-B 24 0 350 80.3 454 In-House

leI Hopewell DMT-B 3 59 70 12.8 145 In-House

DMT-B 1 25 30 5.4 61

Shell Pt. Pleasant TPA-C 32 20 46 7.4 105

TPA-B 0 0 0 0.0 0

Totals 33 45 76 12.8 167 In-House

DMT-B 16 0 167 0.0 183

Tennessee Kingsport DMT-C 34 16 808 242.1 1100

Eastman TPA-C 2 14 86 29.4 131

Totals 52 30 1061 271.4 1414 Subcontractor

DMT-C 20 68 511 118.4 717

Carolina Eastman Columbia TPA-C 0 153 0 21.6 175

Totals 20 221 511 140 892 Subcontractor

DuPont Brevard DMT-C 2 10 57 17.8 87 In-House

DMT-C 39 158 886 278.1 1361 - DuPont Cape Fear TPA-C 22 13 32 . 4.9 72

Totals 61 171 918 283 1433 . Subcontractor

DuPont Circleville DMT-C 10 42 234 73.3 359 In-House

8

L
(

TABLE 6. ESTIMATION OF MAXIMUM NUMBER OF COMPONENTS TO MONITOR IN ONE MONTH

(concluded)

(

\

Connectorst

Total Number of Personnel to be

Company Location Process Pumps. Valves. gas

Valves, light gas/vapor and Components to Used to Conduct

light liquid liquid Monitor in One Method 21

light liquid Month Monitorin2

DMT-C 9 36 202 63.4 310

DuPont Cooper River TPA-C 31 19 45 7.1 102

Totals 40 S5 247 70.5 413 In-House

DuPont Florence DMT-C 19 77 434 136.1 666 Subcontractor

DMT-C 13 54 304 95.3 466

DuPont Kinston lPA-C 28 17 41 6.4 92

Totals 41 71 345 101.75 559 Subcontractor

DuPont Old Hickory DMT-C 12 50 ~80 88.0

Hoechst

430 In·House

Celanese Greer TPA.c 0 4 0 2.2 6 In-House

Hoechst Salisbury Celanese TPA-C S6 112 O. 17.5 186 In-House

Wellman TPA-C 0 5 0 0.0 5 In-House

YKK TPA-C 8 0 8 1.0 17 In-House

9
Table 7 presents the initial and subsequent leak frequencies used for components subject

to Method 21 at all facilities in the current revised analysis and compares them to those used in

the October 1998 analysis. Table 8 presents the uncontrolled and controlled emission factors

used for components subject to Method 21 at an facilities in the current revised analysis and

compares them to those used in the October 1998 analysis.

Monitoring PeriodUnder the rule, if the leak frequency for valves in gas/vapor service is less than or equal

to 1.0 percent but greater than 0.5 percent, the monitoring period is twice per year. Based on data

submitted, a leak frequency of 0.91 percent for these components were calculated for the "other

facilities." Therefore, for the "other facilities" the December 2000 analysis uses a monitoring

frequency oftwice per year for these components.

Under the rule, if the leak frequency for valves in gas/vapor service is less than or equal

to 0.5 percent but greater than 0.25 percent, the monitoring period is once per year. Based on

data submitted, Carolina Eastman reports a leak frequency of 0.33 percent for these components.

Therefore, for Carolina Eastman the December 2000 analysis uses a monitoring frequency of

once per year for these components.

Under the rule, if the leak frequency for valves in light liquid service is less than or equal

to 1 percent, the monitoring period is twice per year. Based on data submitted, ICI-FayetteviJIe ..I

reports a leak frequency of 0.86 percent for these components. Therefore, for ICI-Fayetteville the

December 2000 analysis uses a monitoring frequency oftwice per year for these components.

Under the rule, if the leak frequency for connectors in ~as/vapor or light liquid service is

less than or equal to 0.5 percent, the monitoring period can be once every four years. In the

December 2000 analysis, this once every four year period for monitoring has been used for all

facilities.

10
TABLE 7. SUMMARY OF LEAK FREQUENCIES (%)

Initial Subsequent

Component CompanylFacility October 1998 December October 1998 December

Analysis 2000 Analysis 2000

Analysis Analysis

Valves. gas/vapor HC facilities 2.35 2.35 2.00 2.00

Eastman - Kingsport 1.6 1.49 2.00 1.49

Carolina Eastman 0 0.33 0 0.33

All Others 13.6 1.39 2.00 0.91

Valves. light liquid HC facilities 2.5 2.5 2.00 2.00

Eastman - Kingsport 1.7 2.415 2.00 2.00

Carolina Eastman 0 1.52 0 1.52

ICI-Fayetteville 0.86 0.86 Q.86 0.86

All Others 8.5 1.824 2.00 1.46

Pumps. light liquid HC facilities 8.68 8.68 8.04 4.2

Eastman - Kingsport 3.65 0.51 3.65 0.51

Carolina Eastman 8.73 8.93 8.04 4.2

ICI-Fayetteville 16.7 16.7 8.04 8.04

All Others 17.1 8.71 8.04 4.2

Connectors. HC facilities 0.86 0.86 0.5 0.5

gas/vapor and light Eastman - Kingsport 0.47 0.44 0.5 0.44 liquid

Carolina Eastman 0.33 0.265· 0.5 0.265

DuPont 3.9 0.52 0.5 0.5

ICI-Fayetteville 0.86 0.86 0.5 0.5

All Others 3.9 0.61 0.5 0.5

II
TABLE 8. SUMMARY OF EMISSION FACTORS (Ibs/hr/component)

Uncontrolled

Controlled (Ibslhrlcomponent) (Ibslhr/component)

Component CompanylFaciJity

October 1998 December December October 1998

Analysis 2000

Analysis 2000

Analysis Analysis

Valves, gas/vapor HC facilities 0.002303 0.002303 0.001 0.0013385

Eastman - Kingsport 0.00158 0.00030 0.001 0.000196

Carolina Eastman 0 0.000026. 0 0.ססOO227

All Others 0.0131 0.000876 0.001 0.000516

Valves. light liquid HC facilities 0.00266 0.00266 0.0011 0.0011266

Eastman - Kingsport 0.001835 0.00082 0.0011 0.000513

Carolina Eastman 0 0.00013 0 0.0000954

ICI-Fayetteville 0.000955 0.000955 0.000955 0.0005285

All Others 0.00887 0.001141 0.0011 0.0004931

Pumps, light liquid HC facilities 0.022685 0.022685 0.011 0.0074535

Eastman - Kingsport 0.01013 0.00385 0.01013 0.00308

Carolina Eastman 0.022792 0.01433 0.011 0.00571

ICI-Fayetteville 0.04269 0.04269 0.011 . 0.01226

All Others 0.0438 0.020889 0.011 0.0068948

Connectors, HC facilities 0.000923 0.000923 0.000286 0.0004029

gas/vapor and light

liquid Eastman - Kingsport 0.000523 0.00038 0.000286 0:000299

Carolina Eastman 0.000164 0.000041 0.000164 0.0000312

DuPont 0.00403 0.00022 0.000286 0.0001396

ICI-Fayetteville 0.000926 0.000926 0.000286 0.0004042

All Others 0.00403 0.0005 0.000286 0.0002837

12
APPENDIX A

DETAll.ED COST EFFECTIVENESS SUMMARIES BY FACILITY AND SUBCATEGORY
DECEMBER 2000 COST EFFECTIVENESS SUMMARY

Annual Emission Cost Cost

Company Location Costs Reduction Effectivness Effectiveness

from October .,.)

DMT- Batch 2000 Analysis

3M Decatur $12,262 2.91 $4,214

3M Greenville $9,324 1.53 $6,094

BASF Lowland $18,425 5.76 $3,199

EK Rochester $4,596 0.55 $8,356

Hoeschst Celanese Shelby $10,218 2.19 $4,666

Hoeschst Celanese Spartanburg $30,136 14.67 $2,054

ICI Fayetteville $31,125 6.16 $5,053

ICI Hopewell $11,609 2.78 $4,176

Shell PI. Pleasant $4,328 1.37 $3,159

Tennessee Eastman Kingsport $10,015 1.53 $6,545

TOTALS $142,037 39.45 $3,600 $2,291

DMT Continuous

Carolina Eastman Columbia $n,366 31.71 $2,440

DuPont Brevard $11,212 2.63 $4,263

DuPont Cape Fear $113,794 39.96 $2,848

DuPont Circleville $27,356 10.62 $2,576

DuPont Cooper River $24,030 9.20 $2,612

DuPont Florence $71,352 19.80 $3,604

DuPont Kinston $54,947 13.45 $4,085

DuPont Old Hickory $30,887 12.14 $2,544

Hoeschst Celanese Spartanburg $50,658 15.20 $3,333

Tennessee Eastman Kingsport $93,740 30.94 $3,030 -..I

TOTALS $555,342 185.65 $2,991 $1,401

TPA Continuous

Carolina Eastman Columbia $14,928 66.99 $223

DuPont Cape Fear $17,603 4.92 $3,578

DuPont Cooper River $28,065 7.24 $3,876

DuPont Kinston $24,447 6.84 $3,574

Hoechst Celanese Greer $10,441 1.47 $7,102

Hoechst-Celanese Salisbury $55,640 8.97 $6,203

Hoeschst Celanese Spartanburg $1,089 0.03 $36,307

Shell PI. Pleasant $28,751 7.40 $3,885

Tennessee Eastman Kingsport $9,413 5.85 $1,609

Wellman $31,252 15.83 $1,974

YKK $11,038 2.20 $5,017

TOTALS $232,667 127.74 $1,821 $1,769

TPA Batch

Shell PI. Pleasant $4,911 2.71 $1,812 $1,812

J

....,

CosUnl.xls
APPENDIXB

FACll..ITY SPECIFIC COST SPREADSHEETS FOR DECEMBER 2000 ANALYSIS
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