### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC General Company and Facility** 

**Information**

**Instructions**

Please complete this worksheet for your parent company and PVC production facility

.

**Parent Company General Information**

Parent Company

Name:

Address:

City:

Country: USA

Size of Com pany

(approximate number of employees including all subsidiaries, branches, and related establishments owned):

**PVC Production Facility General Information**

Facility Name:

Facility Address:

Facility City:

Facility Technical Contact Name:

Technical Contact Telephone Number:

Technical Contact Email:

Number of employees attached to the PVC production facility: 103 9 Peach Tree Hill Road Formosa Plastics Corporation USA

302.836.2256

kbennett@fdde.fpcusa.com Formosa Plastics Corporation DE

780 Schoolhouse Road

Delaware City

KimBennett Livingston

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater** 

State: NJ Zip Code: 7039

Size of Com pany

(approximate number of employees including all subsidiaries, branches, and related establishments owned):

State: DE Zip Code: 19706

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Treatment Sy** **stem Information Update**

**Instructions**

2. Also complete the additional supplemental questions to Form C-1-c.

**FORM C-1-c PROCESS EQUIPMENT - WA** **STEWA TER STEA** **M STRIPPER**

Process Unit ID: P1 E2 Plant

Process Equipment ID: U27 Wastewater Feed Rate (lb/hr): Feed Temperature (°F): Feed Inlet Pressure (psia): Liquid Loading Rate (liters/m2): SteamFeed Rate (lb/hr): Steamto Feed Ratio (kg steam/liter of wastewater): Operating Temperature (°F): 160 Operating Pressure (psig): 15 Total Number of Stages: Overall Calculated Tray Efficiency: Stripping Factor: Flow configuration (countercurrent, cocurrent): Number of Actual Trays: Colum n Height (meters):

Year Equipment Installed: Equipment Currently

Regulated Under (cite regulations): 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessary below.

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater** 

**Form C-1-c Supplemental Questions**

Please also provide the stripper feed rate in liters per hour, or liters for batch strippers:

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, please provide those values: 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessaryPlease also provide the stripper feed rate in liters per hour, or liters for batch strippers: liters/hour 26,495 liters

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, please provide those values:

liters/hour (max design) 44,285 liters (max design) 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessary

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Treatment Sy** **stem Information Update**

**Instructions**

2. Also complete the additional supplemental questions to Form C-1-c.

**FORM C-1-c PROCESS EQUIPMENT - WA** **STEWA TER STEA** **M STRIPPER**

Process Unit ID: S2 Plant

Process Equipment ID: U63 Wastewater Feed Rate (lb/hr): Feed Temperature (°F): Feed Inlet Pressure (psia): Liquid Loading Rate (liters/m2): SteamFeed Rate (lb/hr): Steamto Feed Ratio (kg steam/liter of wastewater): Operating Temperature (°F): 170 Operating Pressure (psig): 15 Total Number of Stages: Overall Calculated Tray Efficiency: Stripping Factor: Flow configuration (countercurrent, cocurrent): Number of Actual Trays: Colum n Height (meters):

Year Equipment Installed: Equipment Currently

Regulated Under (cite regulations): 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessary below.

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater** 

**Form C-1-c Supplemental Questions**

Please also provide the stripper feed rate in liters per hour, or liters for batch strippers:

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, please provide those values: 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessaryPlease also provide the stripper feed rate in liters per hour, or liters for batch strippers: liters/hour 18,925 liters

If the above stripper feed rate or capacity does not equal the maximum design rate or capacity, please provide those values:

liters/hour (max design) 31,542 liters (max design) 1. A copy

of your facility's responses on Form C-1-c of the August 21, 2009 CAA section 114 request were included with the CAA Section 114 request letter dated November XX, 2012. Please review those previous responses and update if necessary

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Stream Information** 

**Instructions**

1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process wastewater treatment system. 2. Complete a row in Table 2 below for each PVC process wastewater stream that exits a PVC production process wastewater treatment system. 3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC production facility

.

**Table 1. Process Wastewater Streams Not Treated by a PVC Process Wastewater Treatment System 1**  **3**

P1 E2 Plant

S2 Plant **2**

Pum p seal water (non VCM contact)

Pum p seal water (non VCM contact) **PVC Process Unit ID**  **Name of PVC Process Wastewater Stream PVC Process**  **Wastewater Stream ID** **Table 2. Process Wastewater Streams Exiting a PVC Process Wastewater Treatment System 1**  **2 3**  **4 5**  **6**

**Min** P1 E2 Plant E2 Production Unit SteamStripping Batch E2WW-1 0 S2 Plant S2 Production SteamStripping Batch S2WW-1 0

**Table 3. PVC Process Wastewater Destination Codes Table**

Wastewater treatment system Discharge without treatment by pipeline, sewer, or other conveyance to surface water Discharge to POTW , no treatment Discharge to PrOTW , no treatment Zero discharge or alternative disposal method Recycle to process Other

**Table 4. Non-PVC Production Process Wastewater Streams Entering a PVC Process Wastewater Treatment System**
**2 3** 

**Min Ma** **x**

**PVC Process Wastewater Stream Flow Rate**

**Process Wastewater Stream Flow Rate**

**(gallons per day) Destination Description**  **PVC Process Wastewater**  **Treatment System ID**  **PVC Process Unit ID**  **PVC Process Wastewater**  **Stream ID Ty** **pe of Process Wastewater**  **Treatment System**

**Source of Process Wastewater Stream**

**1 Is this** 
**process wastewater**  **treatment system batch**  **or continuous operation?** 

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater** 

1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process wastewater treatment system. 2. Complete a row in Table 2 below for each PVC process wastewater stream that exits a PVC production process wastewater treatment system. 3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC production facility

.

**Table 1. Process Wastewater Streams Not Treated by a PVC Process Wastewater Treatment System 4**  **5 6**  **7 8** 

**Min Ma** **x Av** **erage**

0 10080 8880 Estimated 360

0 17280 17280 Estimated 360 **PVC Process Wastewater Stream Flow Rate**

**(gallons per day) Flow Rate**  **Determination Me** **thod Operating Days Per**  **Year 7**  **8 9**  **10 11** 

**Ma x**  **Av erage**  7000 7000 Estimated 60 WWT 5000 5000 Estimated 96 WWT

**Code**
WWT Provide name of the wastewater treatment system SW Provide name of outfall POTWRAW Provide name of POTW PrOTWRAW Provide name of PrOTW ZEROALT Describe method RECYC Describe where in the process the stream is recycled OTHER Describe

**Table 4. Non-PVC Production Process Wastewater Streams Entering a PVC Process Wastewater Treatment System**
**4 5**  **6 7** 

**Av erage**  **Flow Rate**

**Determination Me** **thod PVC Process**  **Wastewater Treatment**  **System ID PVC Process Wastewater Stream Flow Rate** 

**(gallons per day) Flow Rate**  **Determination Me** **thod**

**Operating Days Per Year**  **Process Wastewater Stream Flow Rate**

**(gallons per day) Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2**  **PVC Process Wastewater Stream**  **Destination Code**

(Refer to Table 3 below) **Operating Days Per Year** 1. Complete a row in Table 1 below for each PVC process wastewater stream generated within the PVC production facility that exits a piece of PVC production process equipment and is not treated by a PVC production process wastewater treatment system.

3. In Table 4, please provide the source, flow rates, and the ID of the PVC process wastewater treatment system for each stream that enters a PVC process wastewater treatment system but that does not originate from the PVC production facility

.

**9 10** 

DP501A&B Various process pumps

SC302A&B, SC304A&B, SP303A&B, SP503A&B Various process pumps **Originating PVC Process Equipment ID**  **Originating PVC Process Equipment Description** **12 13** 

Site WWT Yes Site WWT Yes

Provide name of the wastewater treatment system

Describe where in the process the stream is recycled

**Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2 Is this PVC process wastewater**  **stream exposed to the atmosphere at any point between the outlet of**  **the PVC process wastewater treatment system and its**  **destination? As** **sociated Destination Information** 

(Refer to Table 3 below)**11 12** 

WWT Site WWT

WWT Site WWT **As sociated Destination Information**  **PVC Process Wastewater Stream Destination Code** 

(Refer to Table 3 below)**Process Wastewater Destination Details to Provide in Column 12 of Table 1 and Column 11 of Table 2**

**If your response in Column 3 is "Other" then please provide a description of the process wastewaetr treatment system**  **14 13** 

Yes

Yes **Is this PVC process wastewater stream exposed to the atmosphere**  **at any point between the originating PVC process equipment**  **and its destination? If your response in Column 3 is "Other" then please provide a description of the process wastewaetr** 

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Sampling and A** **naly sis Data** 

**Instructions**

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Com plete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed. 4. Enter any

other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below. 4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column. 5. Enter any

notes or additional information relevant to the sampling or analysis.

**Company Facility**  **PVC Process Wastewater Treatment Sy stem ID** 

**CA S No.**  **HA P** 

107211 Ethylene glycol 67561 Methanol 75070 Acetaldehyde 50000 Formaldehyde 51285 2,4-dinitrophenol 98862 Acetophenone 117817 Bis(2-ethylhexyl) phthalate (DEHP) 123319 Hydroquinone 108952 Phenol 79345 1,1,2,2-tetrachloroethane 106990 1,3-butadiene 540841 2,2,4-trimethylpentane 71432 Benzene 108907 Chlorobenzene 67663 Chloroform 126998 Chloroprene 98828 Cumene 75003 Ethyl chloride (Chloroethane) 100414 Ethylbenzene 107062 Ethylene dichloride (1,2-Dichloroethane) 75343 Ethylidene dichloride (1,1-Dichloroethane) **Resin Type (suspension, dispersion, bulk, etc.) -->**74873 Methyl chloride (Chloromethane) 75092 Methylene chloride 110543 n-Hexane 108883 Toluene 71556 Methyl chloroform (1,1,1-Trichloroethane) 79005 1,1,2-Trichloroethane 108054 Vinyl acetate 593602 Vinyl bromide 75014 Vinyl chloride 75354 Vinylidene chloride (1,1-Dichloroethylene) 1330207 Xylenes (isomers and mixtures)

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Sampling and A** **naly sis Data** 

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Com plete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed. 4. Enter any

other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below. 4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column. 5. Enter any

notes or additional information relevant to the sampling or analysis.

Formosa Plastics Corporation USA Formosa Plastics Corporation DE

P1 E2 Plant

1/11/2013 - 1/14/2013 01-E2-A-01-07-2013 JB25020-1

**An alysis M** **ethod Concentration**  **(ppmw) Non-Detect?** 

SW-846-8015C 10 Non-detect SW-846-8015C 13.2 SW-846-8315A 2.38 SW-846-8315A 4.11 SW-846-8270D 0.017 Non-detect SW-846-8270D 0.00029 Non-detect SW-846-8270D 0.0006 Non-detect SW-846-8270D R SW-846-8270D 0.0013 Non-detect SW-846-8260B 0.0021 Non-detect SW-846-8260B 0.019 Non-detect SW-846-8260B 0.0023 Non-detect SW-846-8260B 0.0024 Non-detect SW-846-8260B 0.0023 Non-detect SW-846-8260B 0.002 Non-detect SW-846-8260B 0.0021 Non-detect SW-846-8260B 0.0045 Non-detect SW-846-8260B 0.0147 SW-846-8260B 0.0023 Non-detect SW-846-8260B 0.0026 Non-detect SW-846-8260B 0.0011 Non-detect **An alysis Date -->** 

**Lab Sample ID --> Lab Report ID -->**  **Stream Temperature (degrees F) -->** 179.3 **Flow Rate Determination Method -->** Estimated **Stream Flow Rate (gallons per minute) -->** 140.1 **Sample Date -->** 01/07/13 **Resin Type (suspension, dispersion, bulk, etc.) -->** em ulsionSW-846-8260B 0.0147

SW-846-8260B 0.007 Non-detect SW-846-8260B 0.0046 Non-detect SW-846-8260B 0.0023 Non-detect SW-846-8260B 0.0024 Non-detect SW-846-8260B 0.0029 Non-detect SW-846-8260B 0.011 Non-detect SW-846-8260B 0.0027 Non-detect EPA Method 107 0.4639 SW-846-8260B 0.0019 Non-detect SW-846-8260B 0.0024 Non-detect1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Com plete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed.

4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column.

1/11/2013 - 1/14/2013 01-E2-B-01-07-2013 JB25020-2 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 21.5 4.02 2.94 0.017 Non-detect 0.00029 Non-detect 0.0015 Rejected R Rejected 0.0013 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0265 0.0023 Non-detect 0.0026 Non-detect 0.0011 Non-detect 179.3 Estimated Estimated 140.1 01/07/13

emulsion **1 2** 0.008 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 3.99 0.0027 Non-detect 1.276 0.0019 Non-detect 0.0024 Non-detect1/14/2013 - 1/22/2013 1/14/2013 - 1/17/2013

02-E2-A-01-10-2013 02-E2-B-01-10-2013 JB25021-1 JB25021-2 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 66 J-Estimated Value 65.2 7.04 7.74 0.19 J-Estimated Value 0.272 0.66 Non-detect R 0.011 Non-detect 0.0014 Non-detect 0.023 Non-detect 0.0029 Non-detect R Rejected R 0.051 Non-detect 0.0064 Non-detect 0.0021 Non-detect 0.0054 Non-detect 0.019 Non-detect 0.048 Non-detect 0.0023 Non-detect 0.0056 Non-detect 0.0024 Non-detect 0.0059 Non-detect 0.0023 Non-detect 0.0057 Non-detect 0.002 Non-detect 0.0051 Non-detect 0.0021 Non-detect 0.0052 Non-detect 0.0045 Non-detect 0.011 Non-detect 0.0227 0.018 0.0023 Non-detect 0.0057 Non-detect 0.0026 Non-detect 0.0065 Non-detect 0.0011 Non-detect 0.0027 Non-detect 159.2 159.2 Estimated Estimated 103 103 01/10/13

em ulsion em ulsion 01/10/13 **3**0.015 0.0132 0.007 Non-detect 0.018 Non-detect 0.0046 Non-detect 0.012 Non-detect 0.0023 Non-detect 0.0057 Non-detect 0.0024 Non-detect 0.0059 Non-detect 0.0029 Non-detect 0.0072 Non-detect 4.2 6.28 0.0027 Non-detect 0.0067 Non-detect 1.5788 1.2314 0.0019 Non-detect 0.0048 Non-detect 0.0024 Non-detect 0.006 Non-detect1/16/2013 - 1/21/2013 03-E2-A-01-14-2013 JB25022-1 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 0.045 Non-detect 9.14 J-Estimated Value 0.013 J-Estimated Value 0.017 Non-detect 0.00029 Non-detect 0.00059 Non-detect Rejected R Rejected 0.0013 Non-detect 0.0054 Non-detect 0.048 Non-detect 0.0056 Non-detect 0.0059 Non-detect 0.0057 Non-detect 0.0051 Non-detect 0.0052 Non-detect 0.011 Non-detect 0.0066 Non-detect 0.0057 Non-detect 0.0065 Non-detect 0.0027 Non-detect 156.8 Estimated Estimated 92.3 emulsion 01/14/13 **4 5** 0.0285 0.018 Non-detect 0.012 Non-detect 0.0057 Non-detect 0.0059 Non-detect 0.0072 Non-detect 0.0408 0.0067 Non-detect

Non-detect 0.0048 Non-detect 0.006 Non-detect1/16/2013 - 1/21/2013 1/29/2013 - 2/5/2013

03-E2-B-01-14-2013 04-E2-A-01-23-2013 JB25022-2 JB25023-4 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 0.045 Non-detect 93 9.08 7.04 0.0246 J-Estimated Value 0.228 0.017 Non-detect 0.17 Non-detect 0.00029 Non-detect 0.0029 Non-detect 0.00059 Non-detect 0.0059 Non-detect R Rejected R 0.0013 Non-detect 0.013 Non-detect 0.0054 Non-detect 0.0021 Non-detect 0.048 Non-detect 0.019 Non-detect 0.0056 Non-detect 0.0023 Non-detect 0.0059 Non-detect 0.0024 Non-detect 0.0057 Non-detect 0.0023 Non-detect 0.0051 Non-detect 0.002 Non-detect 0.0052 Non-detect 0.0021 Non-detect 0.011 Non-detect 0.0045 Non-detect 0.0066 Non-detect 0.0026 Non-detect 0.0057 Non-detect 0.0023 Non-detect 0.0065 Non-detect 0.0026 Non-detect 0.0027 Non-detect 0.0011 Non-detect 156.8 159.1 Estimated Estimated 92.3 113.4 em ulsion em ulsion 01/14/13 01/23/13 **6**0.0099 0.0118 0.018 Non-detect 0.007 Non-detect 0.012 Non-detect 0.0046 Non-detect 0.0057 Non-detect 0.0023 Non-detect 0.0059 Non-detect 0.0024 Non-detect 0.0072 Non-detect 0.0029 Non-detect 0.86 0.011 Non-detect 0.0067 Non-detect 0.0027 Non-detect

Non-detect 0.1344 0.0048 Non-detect 0.0019 Non-detect 0.006 Non-detect 0.0024 Non-detect1/29/2013 - 2/5/2013 04-E2-B-01-23-2013 JB25023-5 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 96.9 J-Estimated Value 7.87 J-Estimated Value 0.241 0.17 Non-detect 0.0029 Non-detect 0.0059 Non-detect Rejected R Rejected 0.013 Non-detect 0.0021 Non-detect R Rejected 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0119 0.0023 Non-detect 0.0026 Non-detect 0.0011 Non-detect 159.1 Estimated Estimated 113.4 emulsion 01/23/13 **7 8** 0.0021 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.0027 Non-detect 0.4777 0.0019 Non-detect 0.0024 Non-detect2/4/2013 - 2/7/2013 2/4/2013 - 2/7/2013

05-E2-A-01-31-2013 05-E2-B-01-31-2013 JB25024-4 JB25024-5 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 0.01 Non-detect 47.9 56 3.82 J-Estimated Value 3.42 0.219 J-Estimated Value 0.268 0.017 Non-detect 0.017 Non-detect 0.00029 Non-detect 0.00029 Non-detect 0.00059 Non-detect 0.00059 Non-detect R Rejected R 0.0013 Non-detect 0.0013 Non-detect 0.0021 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0026 Non-detect 0.0097 0.0023 Non-detect 0.0023 Non-detect 0.0026 Non-detect 0.0026 Non-detect 0.0011 Non-detect 0.0011 Non-detect 157.1 157.1 Estimated Estimated 178.8 178.8 em ulsion em ulsion 01/31/13 01/31/13 **9**0.0021 Non-detect 0.0021 Non-detect 0.007 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.011 Non-detect 0.0027 Non-detect 0.0027 Non-detect 1.6468 0.4591 0.0019 Non-detect 0.0019 Non-detect 0.0024 Non-detect 0.0024 Non-detect2/11/2013 - 2/23/2013 06-E2-A-02-07-2013 JB25025-1 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 0.045 Non-detect J-Estimated Value 8.47 J-Estimated Value J-Estimated Value 0.0756 J-Estimated Value 0.017 Non-detect 0.00029 Non-detect 0.0052 Rejected R Rejected 0.0013 Non-detect 0.00021 Non-detect 0.0019 Non-detect 0.00023 Non-detect 0.00024 Non-detect 0.00023 Non-detect 0.0002 Non-detect 0.00021 Non-detect 0.00045 Non-detect 0.00026 Non-detect 0.00023 Non-detect 0.00026 Non-detect 0.00011 Non-detect 158.6 Estimated Estimated 171.3 emulsion 02/07/13 **11 10** 0.0094 0.0007 Non-detect 0.00046 Non-detect 0.00023 Non-detect 0.00024 Non-detect 0.00029 Non-detect 0.251 0.00027 Non-detect 0.3055 0.00019 Non-detect 0.00024 Non-detect2/11/2013 - 2/23/2013 2/14/2013 - 2/23/2013

06-E2-B-02-07-2013 07-E2-A-02-12-2013 JB25025-2 JB25026-6 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 0.045 Non-detect 0.045 Non-detect 9.69 J-Estimated Value 6.46 0.0881 J-Estimated Value 0.0209 0.017 Non-detect 0.017 Non-detect 0.00029 Non-detect 0.00029 Non-detect 0.00059 Non-detect 0.00059 Non-detect R Rejected R 0.0013 Non-detect 0.0013 Non-detect 0.00021 Non-detect 0.011 Non-detect 0.0019 Non-detect 0.095 Non-detect 0.00023 Non-detect 0.011 Non-detect 0.00024 Non-detect 0.012 Non-detect 0.00023 Non-detect 0.011 Non-detect 0.0002 Non-detect 0.01 Non-detect 0.00021 Non-detect 0.01 Non-detect 0.00045 Non-detect 0.022 Non-detect 0.0297 0.0637 0.00023 Non-detect 0.011 Non-detect 0.0041 0.013 Non-detect 0.00011 Non-detect 0.0053 Non-detect 158.8 158.6 Estimated Estimated 171.3 183.9 em ulsion em ulsion 02/12/13 02/07/13 **12**0.0154 0.0491 0.0007 Non-detect 0.035 Non-detect 0.00046 Non-detect 0.023 Non-detect 0.00023 Non-detect 0.011 Non-detect 0.00024 Non-detect 0.012 Non-detect 0.00029 Non-detect 0.014 Non-detect 3.76 39.9 0.00027 Non-detect 0.013 Non-detect 1.0615 2.1305 0.00019 Non-detect 0.0096 Non-detect 0.00024 Non-detect 0.012 Non-detect2/14/2013 - 2/24/2013 07-E2-B-02-12-2013 JB25026-7 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 0.045 Non-detect J-Estimated Value 6.11 J-Estimated Value 0.0175 0.017 Non-detect 0.00029 Non-detect 0.00059 Non-detect Rejected R Rejected 0.0013 Non-detect 0.011 Non-detect 0.095 Non-detect 0.011 Non-detect 0.012 Non-detect 0.011 Non-detect 0.01 Non-detect 0.01 Non-detect 0.022 Non-detect 0.0487 0.011 Non-detect 0.013 Non-detect 0.0053 Non-detect 158.8 Estimated Estimated 183.9 emulsion 02/12/13 **13 14** 0.0484 0.035 Non-detect 0.023 Non-detect 0.011 Non-detect 0.012 Non-detect 0.014 Non-detect 38.5 0.013 Non-detect 1.9344 0.0096 Non-detect 0.012 Non-detect2/18/2013 - 2/27/2013 2/18/2013 - 2/28/2013

08-E2-A-02-14-2013 08-E2-B-02-14-2013 JB25027-4 JB25027-5 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 0.045 Non-detect 0.045 Non-detect 58.4 60.3 0.6 J-Estimated Value 0.61 R 0.17 Non-detect 3.08 2.56 0.0059 Non-detect 0.0059 Non-detect R Rejected R 0.013 Non-detect 0.013 Non-detect 2.1 Non-detect 2.1 Non-detect 19 Non-detect 19 Non-detect 2.3 Non-detect 2.3 Non-detect 2.4 Non-detect 2.4 Non-detect 2.3 Non-detect 2.3 Non-detect 2 Non-detect 2 Non-detect 2.1 Non-detect 2.1 Non-detect 4.5 Non-detect 4.5 Non-detect 2.6 Non-detect 2.6 Non-detect 2.3 Non-detect 2.3 Non-detect 2.6 Non-detect 2.6 Non-detect 1.1 Non-detect 1.1 Non-detect 160.5 160.5 Estimated Estimated 113.6 113.6 02/14/13

em ulsion em ulsion 02/14/13 **15**2.1 Non-detect 2.1 Non-detect 7 Non-detect 7 Non-detect 4.6 Non-detect 4.6 Non-detect 2.3 Non-detect 2.3 Non-detect 2.4 Non-detect 2.4 Non-detect 2.9 Non-detect 2.9 Non-detect 10700 10900 2.7 Non-detect 2.7 Non-detect Non-detect Non-detect 1.9 Non-detect 1.9 Non-detect 2.4 Non-detect 2.4 Non-detect2/27/2013 - 3/25/2013 09-E2-A-02-25-2013 JB25028-4 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 3050 6.7 J-Estimated Value J-Estimated Value R Rejected 0.083 Non-detect 0.0014 Non-detect 0.0029 Non-detect Rejected 0.025 Non-detect 0.0064 Non-detect 0.21 Non-detect 1.9 Non-detect 0.23 Non-detect 0.24 Non-detect 0.23 Non-detect 0.2 Non-detect 0.21 Non-detect 0.45 Non-detect 1.28 0.23 Non-detect 0.26 Non-detect 0.11 Non-detect 160.6 Estimated 159.1 Estimated 02/25/13

emulsion **16 17** 0.798 0.7 Non-detect 0.46 Non-detect 0.23 Non-detect 0.24 Non-detect 0.29 Non-detect 176 0.27 Non-detect 18.1496 0.19 Non-detect 0.24 Non-detect2/27/2013 - 3/8/2013 3/11/2013 - 3/16/2013

09-E2-B-02-25-2013 10-E2-A-03-07-2013 JB25028-5 JB25029-4 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 2700 82.8 7.19 J-Estimated Value 6.19 0.0074 J-Estimated Value 0.14 0.017 Non-detect 0.017 Non-detect 0.00029 Non-detect 0.00029 Non-detect 0.00059 Non-detect 0.0013 0.005 Non-detect R 0.0013 Non-detect 0.0013 Non-detect 0.21 Non-detect 0.0021 Non-detect 1.9 Non-detect 0.019 Non-detect 0.23 Non-detect 0.0023 Non-detect 0.24 Non-detect 0.0024 Non-detect 0.23 Non-detect 0.0023 Non-detect 0.2 Non-detect 0.002 Non-detect 0.21 Non-detect 0.0021 Non-detect 0.45 Non-detect 0.0045 Non-detect 1.37 0.0026 Non-detect 0.23 Non-detect 0.0023 Non-detect 0.26 Non-detect 0.006 0.11 Non-detect 0.0011 Non-detect 160.6 159.2 159.1 181 Estimated Estimated em ulsion 02/25/13 03/07/13

em ulsion **18**0.765 0.0101 0.7 Non-detect 0.007 Non-detect 0.46 Non-detect 0.0046 Non-detect 0.23 Non-detect 0.0023 Non-detect 0.24 Non-detect 0.0024 Non-detect 0.29 Non-detect 0.0029 Non-detect 197 2.28 0.27 Non-detect 0.0027 Non-detect 15.4083 Non-detect 0.19 Non-detect 0.0019 Non-detect 0.24 Non-detect 0.0024 Non-detect3/11/2013 - 3/16/2013 10-E2-B-03-07-2013 JB25029-5 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 76.3 J-Estimated Value 6.95 J-Estimated Value 0.126 J-Estimated Value 0.017 Non-detect 0.00029 Non-detect 0.0093 Rejected R Rejected 0.0013 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0101 0.0023 Non-detect 0.0089 0.0011 Non-detect 159.2 Estimated Estimated emulsion 181 03/07/13 **19 20** 0.0231 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 6.38 0.0027 Non-detect 0.5051 0.0019 Non-detect 0.0024 Non-detect3/15/2013 - 3/18/2013 3/15/2013 - 3/18/2013

11-E2-A-03-12-2013 11-E2-B-03-12-2013 JB25030-4 JB25030-5 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 102 76.9 7.35 6.26 0.295 0.259 0.17 Non-detect 0.17 Non-detect 0.0029 Non-detect 0.0029 Non-detect 0.0059 Non-detect 0.0059 Non-detect R Rejected R 0.013 Non-detect 0.013 Non-detect 0.0021 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.002 Non-detect R Rejected R 0.0045 Non-detect 0.0045 Non-detect 0.0252 0.0266 0.0023 Non-detect 0.0023 Non-detect 0.0078 0.0085 0.0011 Non-detect 0.0011 Non-detect 165.1 165.1 Estimated Estimated em ulsion em ulsion 174.6 174.6 03/12/13 03/12/13 **21**0.0171 0.0181 0.007 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.0029 Non-detect 2.2 2.79 0.0027 Non-detect 0.0027 Non-detect

Non-detect 0.304 0.0019 Non-detect 0.0019 Non-detect 0.0024 Non-detect 0.0024 Non-detect3/21/2013 - 4/4/2013 12-E2-A-03-18-2013 JB25031-4 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect J-Estimated Value 0.045 Non-detect 7.14 J-Estimated Value 0.0406 J-Estimated Value 0.033 Non-detect 1.47 0.0012 Non-detect Rejected R Rejected 0.0026 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0041 Non-detect Rejected 0.0042 Non-detect 0.0089 Non-detect 0.0475 0.0046 Non-detect 0.0102 0.0021 Non-detect 158.9 Estimated Estimated emulsion 58.4 03/18/13 **22 23** 0.0274 0.014 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0057 Non-detect 112 0.0054 Non-detect 0.8333 0.0038 Non-detect 0.0048 Non-detect3/21/2013 - 4/4/2013 4/1/2013 - 4/8/2013

12-E2-B-03-18-2013 13-E2-A-03-27-2013 JB25031-5 JB25032-4 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 0.045 Non-detect 22.4 6.41 J-Estimated Value 3.1 0.0434 J-Estimated Value 0.161 0.033 Non-detect 0.017 Non-detect 1.29 0.00029 Non-detect 0.0012 Non-detect 0.00059 Non-detect R Rejected R 0.0026 Non-detect 0.0013 Non-detect 0.0043 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0041 Non-detect 0.0041 Non-detect 0.0042 Non-detect 0.0042 Non-detect 0.0089 Non-detect 0.0089 Non-detect 0.0476 0.0479 0.0046 Non-detect 0.0046 Non-detect 0.009 0.0109 0.0021 Non-detect 0.0021 Non-detect 158.9 154.7 196.2 Estimated Estimated em ulsion em ulsion 58.4 03/27/13 **24** 03/18/130.0281 0.0329 0.014 Non-detect 0.014 Non-detect 0.0093 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0047 Non-detect 0.0057 Non-detect 0.0057 Non-detect 114 0.022 Non-detect 0.0054 Non-detect 0.0054 Non-detect 0.6553 0.5743 0.0038 Non-detect 0.0038 Non-detect 0.0048 Non-detect 0.0048 Non-detect4/1/2013 - 4/8/2013 13-E2-B-03-27-2013 JB25032-5 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 47 4.19 J-Estimated Value 0.252 0.017 Non-detect 0.00029 Non-detect 0.00059 Non-detect Rejected R Rejected 0.0013 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0041 Non-detect 0.0042 Non-detect 0.0089 Non-detect 0.0467 0.0046 Non-detect 0.0105 0.0021 Non-detect 154.7 Estimated Estimated emulsion 196.2 **25** 03/27/13 **26**0.0295 0.014 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0057 Non-detect 0.022 Non-detect 0.0054 Non-detect 0.5793 0.0038 Non-detect 0.0048 Non-detect4/4/2013 - 4/8/2013 4/4/2013 - 4/8/2013

14-E2-A-04-01-2013 14-E2-B-04-01-2013 JB25033-4 JB25033-5 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 36.5 37.2 4.01 4.88 0.342 0.444 0.017 Non-detect 0.017 Non-detect 0.00029 Non-detect 0.00029 Non-detect 0.00059 Non-detect 0.00059 Non-detect 0.005 Non-detect 0.005 Non-detect 0.0013 Non-detect 0.0013 Non-detect 0.0011 Non-detect 0.0011 Non-detect 0.0095 Non-detect 0.0095 Non-detect 0.0011 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0012 Non-detect 0.0011 Non-detect 0.0011 Non-detect 0.001 Non-detect 0.001 Non-detect 0.001 Non-detect 0.001 Non-detect 0.0022 Non-detect 0.0022 Non-detect 0.0013 Non-detect 0.0108 0.0011 Non-detect 0.0011 Non-detect 0.0013 Non-detect 0.0013 Non-detect 0.00053 Non-detect 0.00053 Non-detect 159.8 159.8 133.7 Estimated Estimated em ulsion em ulsion 133.7 04/01/13 04/01/13 **27**0.001 Non-detect 0.0031 0.0035 Non-detect 0.0035 Non-detect 0.0023 Non-detect 0.0023 Non-detect 0.0011 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0012 Non-detect 0.0014 Non-detect 0.0014 Non-detect 0.0056 Non-detect 0.0056 Non-detect 0.0013 Non-detect 0.0013 Non-detect 0.4078 0.5673 0.00096 Non-detect 0.00096 Non-detect 0.0012 Non-detect 0.0012 Non-detect4/12/13-4/24/13 15-E2-A-04-08-2013 JB25034-4 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 53.1 2.67 0.137 0.017 Non-detect 0.00029 Non-detect 0.0018J 0.005 Non-detect 0.0098 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0026 Non-detect 0.0023 Non-detect 4.6J 0.0011 Non-detect 159.6 128.1 Estimated Estimated emulsion 04/08/13 **29 28** 0.0021 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.0027 Non-detect 0.1639 0.0019 Non-detect 0.0024 Non-detect4/12/13-4/24/13

15-E2-B-04-08-2013 JB25034-5 **Concentration (ppmw)**  **Non-Detect? Note(s)** 

10 Non-detect 30.7 2.63 0.156 0.017 Non-detect 0.00029 Non-detect 0.00059 Non-detect 0.005 Non-detect 0.0013 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0026 Non-detect 0.0023 Non-detect 4.5J 0.0011 Non-detect 159.6 128.1 Estimated em ulsion 04/08/13 **30**0.0021 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.0027 Non-detect 0.1591 0.0019 Non-detect 0.0024 Non-detect

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Sampling and A** **naly sis Data** 

**Instructions**

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Com plete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed. 4. Enter any

other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below. 4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column. 5. Enter any

notes or additional information relevant to the sampling or analysis.

**Company Facility**  **PVC Process Wastewater Treatment Sy stem ID** 

**CA S No.**  **HA P** 

107211 Ethylene glycol 67561 Methanol 75070 Acetaldehyde 50000 Formaldehyde 51285 2,4-dinitrophenol 98862 Acetophenone 117817 Bis(2-ethylhexyl) phthalate (DEHP) 123319 Hydroquinone 108952 Phenol 79345 1,1,2,2-tetrachloroethane 106990 1,3-butadiene 540841 2,2,4-trimethylpentane 71432 Benzene 108907 Chlorobenzene 67663 Chloroform 126998 Chloroprene 98828 Cumene 75003 Ethyl chloride (Chloroethane) 100414 Ethylbenzene 107062 Ethylene dichloride (1,2-Dichloroethane) 75343 Ethylidene dichloride (1,1-Dichloroethane) **Resin Type (suspension, dispersion, bulk, etc.) -->**74873 Methyl chloride (Chloromethane) 75092 Methylene chloride 110543 n-Hexane 108883 Toluene 71556 Methyl chloroform (1,1,1-Trichloroethane) 79005 1,1,2-Trichloroethane 108054 Vinyl acetate 593602 Vinyl bromide 75014 Vinyl chloride 75354 Vinylidene chloride (1,1-Dichloroethylene) 1330207 Xylenes (isomers and mixtures)

### November 8, 2012 CA **A Section 114 - Poly** 

**viny l Chloride and Copoly** **mers (PVC) Production Process Wastew ater**  **PVC Production Process Wastew ater Sampling and A** **naly sis Data** 

1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Com plete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed. 4. Enter any

other HAP expected to be present (that are not listed in Table 10 to Subpart HHHHHHH of Part 63) in the table below. 4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column. 5. Enter any

notes or additional information relevant to the sampling or analysis.

Formosa Plastics Corporation USA Formosa Plastics Corporation DE

S2 Plant

1/21/2013 - 1/30/2013 01-S2-A-01-17-2013 JB26756-1

**An alysis M** **ethod Concentration**  **(ppmw) Non-Detect?** 

SW-846-8015C 10 Non-detect SW-846-8015C 2.61 SW-846-8315A 0.0985 SW-846-8315A 0.0661 SW-846-8270D 0.17 Non-detect SW-846-8270D 0.0029 Non-detect SW-846-8270D 0.0059 Non-detect SW-846-8270D R SW-846-8270D 0.013 Non-detect SW-846-8260B 0.0054 Non-detect SW-846-8260B 0.048 Non-detect SW-846-8260B 0.0056 Non-detect SW-846-8260B 0.0059 Non-detect SW-846-8260B 0.0057 Non-detect SW-846-8260B 0.0051 Non-detect SW-846-8260B 0.0052 Non-detect SW-846-8260B 0.011 Non-detect SW-846-8260B 0.0066 Non-detect SW-846-8260B 0.0057 Non-detect SW-846-8260B 0.0065 Non-detect SW-846-8260B 0.0027 Non-detect **Sample Date -->** 01/17/13 **Resin Type (suspension, dispersion, bulk, etc.) -->** em ulsion

**Stream Flow Rate (gallons per minute) -->** 104.5 **Flow Rate Determination Method -->** Estimated

**Lab Sample ID --> Lab Report ID -->**  **An alysis Date -->**  **Stream Temperature (degrees F) -->** 184.2SW-846-8260B 0.0052 Non-detect

SW-846-8260B 0.018 Non-detect SW-846-8260B 0.012 Non-detect SW-846-8260B 0.0057 Non-detect SW-846-8260B 0.0059 Non-detect SW-846-8260B 0.0072 Non-detect SW-846-8260B 0.028 Non-detect SW-846-8260B 0.0067 Non-detect EPA Method 107 Non-detect SW-846-8260B 0.0048 Non-detect SW-846-8260B 0.006 Non-detect1. Complete the table below for each PVC process wastewater steam exiting a process wastewater treatment system that was sampled and analyzed. Com plete one worksheet for each single stream (make copies of this worksheet if necessary). 2. Enter the PVC process wastewater treatment system ID for the stream that was sampled and analyzed. The ID must match the IDs listed in Table 2 of the "Stream Info" worksheet. 3. Complete columns 1 through 30. Enter the sample date, resin type, stream flow rate, basis for flow rate determination, stream temperature, sample type, analysis date, lab report ID, and lab sample ID. Enter the concentration results for each HAP listed.

4. For compounds that were not detected, indicate as such in the "Non-Detect?" column and provide the method detection limit, in ppmw, in the "Concentration (ppmw)" column.

1/21/2013 - 1/30/2013 01-S2-B-01-17-2013 JB26756-2 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 2.82 0.161 0.0971 0.17 Non-detect 0.0029 Non-detect 0.0059 Non-detect Rejected R Rejected 0.013 Non-detect 0.0011 Non-detect 0.0095 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0011 Non-detect 0.001 Non-detect 0.001 Non-detect 0.0022 Non-detect 0.0013 Non-detect 0.0011 Non-detect 0.0013 Non-detect 0.00053 Non-detect **1 2**  01/17/13

emulsion 104.5 Estimated Estimated 184.20.001 Non-detect 0.0035 Non-detect 0.0023 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0014 Non-detect 0.0056 Non-detect 0.0013 Non-detect

Non-detect 0.00096 Non-detect 0.0012 Non-detect1/21/2013 - 1/30/2013 1/21/2013 - 1/30/2013

02-S2-A-01-17-2013 02-S2-B-01-17-2013 JB25021-5 JB25021-6 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 5.85 6.96 0.983 1.06 0.361 0.366 0.017 Non-detect 0.017 Non-detect 0.00029 Non-detect 0.00029 Non-detect 0.00059 Non-detect 0.00059 Non-detect R Rejected R 0.0013 Non-detect 0.0013 Non-detect 0.00021 Non-detect 0.00021 Non-detect 0.0019 Non-detect 0.0019 Non-detect 0.00023 Non-detect 0.00023 Non-detect 0.00026 0.00029 0.00023 Non-detect 0.00023 Non-detect 0.0002 Non-detect 0.0002 Non-detect 0.00021 Non-detect 0.00021 Non-detect 0.00045 Non-detect 0.00045 Non-detect 0.002 0.0022 0.00023 Non-detect 0.00023 Non-detect 0.00026 Non-detect 0.00026 Non-detect 0.00011 Non-detect 0.00011 Non-detect **3** 01/17/13 01/17/13

em ulsion em ulsion 124.7 124.7 Estimated Estimated 182.4 182.40.00046 0.00021 Non-detect 0.0007 Non-detect 0.0007 Non-detect 0.00046 Non-detect 0.00046 Non-detect 0.00023 Non-detect 0.00023 Non-detect 0.00024 Non-detect 0.00024 Non-detect 0.00029 Non-detect 0.00029 Non-detect 0.0011 Non-detect 0.0011 Non-detect 0.00027 Non-detect 0.00027 Non-detect 0.1313 0.1124 0.00019 Non-detect 0.00019 Non-detect 0.00024 Non-detect 0.00024 Non-detect1/24/2013 - 1/30/2013 03-S2-A-01-21-2013 JB25022-3 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 3.19 1.1 Non-detect J-Estimated Value 2 Non-detect 1.7 Non-detect 0.029 Non-detect 0.059 Non-detect Rejected R Rejected 0.13 Non-detect 0.0054 Non-detect 0.048 Non-detect 0.0056 Non-detect 0.0059 Non-detect 0.0057 Non-detect 0.0051 Non-detect 0.0052 Non-detect 0.011 Non-detect 0.0066 Non-detect 0.0057 Non-detect 0.0065 Non-detect 0.0027 Non-detect **5 4**  01/21/13

emulsion 108.3 Estimated Estimated 185.20.0052 Non-detect 0.018 Non-detect 0.012 Non-detect 0.0057 Non-detect 0.0059 Non-detect 0.0072 Non-detect 0.028 Non-detect 0.0067 Non-detect 0.1111 0.0048 Non-detect 0.006 Non-detect1/24/2013 - 1/30/2013 1/24/2013 - 1/30/2013

03-S2-B-01-21-2013 04-S2-A-01-21-2013 JB25022-4 JB25023-1 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 2.66 13.4 0.18 Non-detect 4.42 0.34 Non-detect 0.111 1.7 Non-detect 1.7 Non-detect 0.029 Non-detect 0.029 Non-detect 0.059 Non-detect 0.059 Non-detect R Rejected R 0.13 Non-detect 0.13 Non-detect 0.0054 Non-detect 0.0011 Non-detect 0.048 Non-detect 0.0095 Non-detect 0.0056 Non-detect 0.0011 Non-detect 0.0059 Non-detect 0.0012 Non-detect 0.0057 Non-detect 0.0011 Non-detect 0.0051 Non-detect 0.001 Non-detect 0.0052 Non-detect 0.001 Non-detect 0.011 Non-detect 0.0022 Non-detect 0.0066 Non-detect 0.0013 Non-detect 0.0057 Non-detect 0.0011 Non-detect 0.0065 Non-detect 0.0013 Non-detect 0.0027 Non-detect 0.00053 Non-detect **6** 01/21/13 01/21/13

em ulsion em ulsion 108.3 176.5 Estimated Estimated 185.2 184.10.0052 Non-detect 0.001 Non-detect 0.018 Non-detect 0.0035 Non-detect 0.012 Non-detect 0.0023 Non-detect 0.0057 Non-detect 0.0011 Non-detect 0.0059 Non-detect 0.0012 Non-detect 0.0072 Non-detect 0.0014 Non-detect 0.028 Non-detect 0.0056 Non-detect 0.0067 Non-detect 0.0013 Non-detect 0.1004 0.1018 0.0048 Non-detect 0.00096 Non-detect 0.006 Non-detect 0.0012 Non-detect1/24/2013 - 1/30/2013 04-S2-B-01-21-2013 JB25023-2 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 12.1 3.74 0.1 1.7 Non-detect 0.029 Non-detect 0.178 Rejected R Rejected 0.13 Non-detect 0.0011 Non-detect 0.0095 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0011 Non-detect 0.001 Non-detect 0.001 Non-detect 0.0022 Non-detect 0.0013 Non-detect 0.0011 Non-detect 0.0013 Non-detect 0.00053 Non-detect **7 8**  01/21/13

emulsion 176.5 Estimated Estimated 184.10.001 Non-detect 0.0035 Non-detect 0.0023 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0014 Non-detect 0.0056 Non-detect 0.0013 Non-detect 0.0969 0.00096 Non-detect 0.0012 Non-detect2/1/2013 - 2/5/2013 2/1/2013 - 2/5/2013

05-S2-A-01-29-2013 05-S2-B-01-29-2013 JB25024-1 JB25024-2 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 26.1 21 23.3 26.5 0.179 0.212 17 Non-detect 17 Non-detect 0.29 Non-detect 0.29 Non-detect 0.59 Non-detect 0.59 Non-detect 5 Non-detect 5 Non-detect 1.3 Non-detect 1.3 Non-detect 0.0054 Non-detect 0.0054 Non-detect 0.048 Non-detect 0.048 Non-detect 0.0056 Non-detect 0.0056 Non-detect 0.0059 Non-detect 0.0059 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.0051 Non-detect 0.0051 Non-detect 0.0052 Non-detect 0.0052 Non-detect 0.011 Non-detect 0.011 Non-detect 0.0066 Non-detect 0.0066 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.0065 Non-detect 0.0065 Non-detect 0.0027 Non-detect 0.0027 Non-detect **9** 01/29/13 01/29/13

em ulsion em ulsion 109.3 109.3 Estimated Estimated 175.2 175.20.0052 Non-detect 0.0052 Non-detect 0.018 Non-detect 0.018 Non-detect 0.012 Non-detect 0.012 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.0059 Non-detect 0.0059 Non-detect 0.0072 Non-detect 0.0072 Non-detect 0.028 Non-detect 0.028 Non-detect 0.0067 Non-detect 0.0067 Non-detect 2.1224 1.7713 0.0048 Non-detect 0.0048 Non-detect 0.006 Non-detect 0.006 Non-detect2/4/2013 - 2/11/2013 06-S2-A-02-01-2013 JB25026-1 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 5.54 1.01 0.0728 1.7 Non-detect 0.029 Non-detect 0.059 Non-detect R Rejected 0.13 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0041 Non-detect 0.0042 Non-detect 0.0089 Non-detect 0.0052 Non-detect 0.0046 Non-detect 0.0052 Non-detect 0.0021 Non-detect **10 11**  02/01/13

emulsion 133.4 Estimated Estimated 185.20.0041 Non-detect 0.014 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0057 Non-detect 0.022 Non-detect 0.0054 Non-detect 0.3329 0.0038 Non-detect 0.0048 Non-detect2/4/2013 - 2/11/2013 2/11/2013 - 2/20/2013

06-S2-B-02-01-2013 07-S2-A-02-06-2013 JB25026-2 JB25026-4 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 5.16 1.22 0.55 Non-detect 0.87 Non-detect 1 Non-detect 1.6 Non-detect 1.7 Non-detect 17 Non-detect 0.029 Non-detect 0.29 Non-detect 0.059 Non-detect 0.59 Non-detect R Rejected R 0.13 Non-detect 1.3 Non-detect 0.0043 Non-detect 0.0021 Non-detect 0.038 Non-detect 0.019 Non-detect 0.0045 Non-detect 0.0023 Non-detect 0.0047 Non-detect 0.0024 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0041 Non-detect 0.002 Non-detect 0.0042 Non-detect 0.0021 Non-detect 0.0089 Non-detect 0.0045 Non-detect 0.0052 Non-detect 0.0026 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0052 Non-detect 0.0026 Non-detect 0.0021 Non-detect 0.0011 Non-detect **12** 02/01/13 02/06/13

em ulsion em ulsion 133.4 144.5 Estimated Estimated 157.8 185.20.0041 Non-detect 0.0021 Non-detect 0.014 Non-detect 0.007 Non-detect 0.0093 Non-detect 0.0046 Non-detect 0.0045 Non-detect 0.0023 Non-detect 0.0047 Non-detect 0.0024 Non-detect 0.0057 Non-detect 0.0029 Non-detect 0.022 Non-detect 0.011 Non-detect 0.0054 Non-detect 0.0027 Non-detect 0.3831 0.3223 0.0038 Non-detect 0.0019 Non-detect 0.0048 Non-detect 0.0024 Non-detect2/11/2013 - 2/20/2013 07-S2-B-02-06-2013 JB25026-5 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 1.13 1.3 Non-detect 2.4 Non-detect 17 Non-detect 0.29 Non-detect 0.59 Non-detect Rejected R Rejected 1.3 Non-detect 0.0011 Non-detect 0.0095 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0011 Non-detect 0.001 Non-detect 0.001 Non-detect 0.0022 Non-detect 0.0013 Non-detect 0.0011 Non-detect 0.0013 Non-detect 0.00053 Non-detect **13 14**  02/06/13

emulsion 144.5 Estimated Estimated 157.80.001 Non-detect 0.0035 Non-detect 0.0023 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0014 Non-detect 0.0056 Non-detect 0.0013 Non-detect 0.2677 0.00096 Non-detect 0.0012 Non-detect2/14/2013 - 2/23/2013 2/14/2013 - 2/23/2013

08-S2-A-02-11-2013 08-S2-B-02-11-2013 JB25027-1 JB25027-2 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 7.11 9.21 1.15 J-Estimated Value 1.12 0.0565 0.0515 0.17 Non-detect 0.17 Non-detect 0.0029 Non-detect 0.0029 Non-detect 0.0059 Non-detect 0.0059 Non-detect R Rejected R 0.013 Non-detect 0.013 Non-detect 0.0043 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0041 Non-detect 0.0041 Non-detect 0.0042 Non-detect 0.0042 Non-detect 0.0089 Non-detect 0.0089 Non-detect 0.0052 Non-detect 0.0052 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0052 Non-detect 0.0052 Non-detect 0.0021 Non-detect 0.0021 Non-detect **15** 02/11/13 02/11/13

em ulsion em ulsion 88.3 88.3 Estimated Estimated 184.3 184.30.0041 Non-detect 0.0041 Non-detect 0.014 Non-detect 0.014 Non-detect 0.0093 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0047 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.022 Non-detect 0.022 Non-detect 0.0054 Non-detect 0.0054 Non-detect 0.137 0.1321 0.0038 Non-detect 0.0038 Non-detect 0.0048 Non-detect 0.0048 Non-detect2/21/2013 - 3/4/2013 09-S2-A-02-19-2013 JB25028-1 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 19 J-Estimated Value 9.16 0.144 J-Estimated Value 3.3 Non-detect 0.057 Non-detect 0.12 Non-detect Rejected 1 Non-detect 0.26 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0041 Non-detect 0.0042 Non-detect 0.0089 Non-detect 0.0279 0.0046 Non-detect 0.0052 Non-detect 0.0021 Non-detect **17 16**  02/19/13

emulsion 185.3 Estimated Estimated 185.40.0041 Non-detect 0.014 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0057 Non-detect 0.022 Non-detect 0.0054 Non-detect 0.6792 0.0038 Non-detect 0.0048 Non-detect2/21/2013 - 3/4/2013 3/4/2013 - 3/13/2013

09-S2-B-02-19-2013 10-S2-A-02-27-2013 JB25028-2 JB25029-1 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 14.4 4.85 9.68 0.597 0.159 J-Estimated Value R 3.3 Non-detect R 0.057 Non-detect 0.00033 Non-detect 0.12 Non-detect 0.00067 Non-detect 1 Non-detect R 0.26 Non-detect R 0.0043 Non-detect 0.0011 Non-detect 0.038 Non-detect 0.0095 Non-detect 0.0045 Non-detect 0.0011 Non-detect 0.0047 Non-detect 0.0012 Non-detect 0.0046 Non-detect 0.0011 Non-detect 0.0041 Non-detect 0.001 Non-detect 0.0042 Non-detect 0.001 Non-detect 0.0089 Non-detect 0.0022 Non-detect 0.0052 Non-detect 0.0013 Non-detect 0.0046 Non-detect 0.0011 Non-detect 0.0052 Non-detect 0.0013 Non-detect 0.0021 Non-detect 0.00053 Non-detect **18** 02/19/13 02/27/13

em ulsion em ulsion 185.3 181.4 Estimated Estimated 185.4 184.70.0041 Non-detect 0.001 Non-detect 0.014 Non-detect 0.0035 Non-detect 0.0093 Non-detect 0.0023 Non-detect 0.0045 Non-detect 0.0011 Non-detect 0.0047 Non-detect 0.0012 Non-detect 0.0057 Non-detect 0.0014 Non-detect 0.022 Non-detect 0.0056 Non-detect 0.0054 Non-detect 0.0013 Non-detect 0.2911 0.244 0.0038 Non-detect 0.00096 Non-detect 0.0048 Non-detect 0.0012 Non-detect3/4/2013 - 3/13/2013 10-S2-B-02-27-2013 JB25029-2 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 5.02 J-Estimated Value 0.59 J-Estimated Value Rejected R Rejected Rejected R Rejected R Rejected R Rejected Rejected R Rejected Rejected R Rejected 0.0011 Non-detect 0.0095 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0011 Non-detect 0.001 Non-detect 0.001 Non-detect 0.0022 Non-detect 0.0013 Non-detect 0.0011 Non-detect 0.0013 Non-detect 0.00053 Non-detect **19 20**  02/27/13

emulsion 181.4 Estimated Estimated 184.70.001 Non-detect 0.0035 Non-detect 0.0023 Non-detect 0.0011 Non-detect 0.0012 Non-detect 0.0014 Non-detect 0.0056 Non-detect 0.0013 Non-detect 0.1863 0.00096 Non-detect 0.0012 Non-detect3/4/2013 - 3/13/2013 3/4/2013 - 3/13/2013

11-S2-A-02-28-2013 11-S2-B-02-28-2013 JB25030-1 JB25030-2 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 6.14 5.17 5.95 J-Estimated Value 6.24 0.0421 J-Estimated Value 0.0507 0.17 Non-detect 0.17 Non-detect 0.0029 Non-detect 0.0029 Non-detect 0.0109 0.0059 Non-detect R Rejected R 0.013 Non-detect 0.013 Non-detect 0.0043 Non-detect 0.0043 Non-detect 0.038 Non-detect 0.038 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0047 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0041 Non-detect 0.0041 Non-detect 0.0042 Non-detect 0.0042 Non-detect 0.0089 Non-detect 0.0089 Non-detect 0.0052 Non-detect 0.0052 Non-detect 0.0046 Non-detect 0.0046 Non-detect 0.0052 Non-detect 0.0052 Non-detect 0.0021 Non-detect 0.0021 Non-detect **21** 02/28/13 0/28/2013

em ulsion em ulsion 149.2 149.2 Estimated Estimated 184.5 184.50.0041 Non-detect 0.0041 Non-detect 0.014 Non-detect 0.014 Non-detect 0.0093 Non-detect 0.0093 Non-detect 0.0045 Non-detect 0.0045 Non-detect 0.0047 Non-detect 0.0047 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.022 Non-detect 0.022 Non-detect 0.0054 Non-detect 0.0054 Non-detect 0.3659 0.4436 0.0038 Non-detect 0.0038 Non-detect 0.0048 Non-detect 0.0048 Non-detect3/18/2013 - 4/12/2013 12-S2-A-03-14-2013 JB25031-1 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 6.09 J-Estimated Value 3.56 Resample value lab ID: JB25031-7 J-Estimated Value 1.11 Resample value lab ID: JB25031-7 0.17 Non-detect 0.0029 Non-detect 0.0059 Non-detect Rejected R Rejected 0.013 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0026 Non-detect 0.0023 Non-detect 0.0026 Non-detect 0.0011 Non-detect **22 23**  03/14/13

emulsion 193.1 Estimated Estimated 182.70.0021 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.0027 Non-detect 0.2036 0.0019 Non-detect 0.0024 Non-detect3/18/2013 - 4/12/2013 3/21/2013 - 4/9/2013

12-S2-B-03-14-2013 13-S2-A-03-19-2013 JB25031-2 JB25032-1 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 6.04 5.72 3.63 Resample value lab ID: JB25031-8 0.73 Non-detect 1.12 Resample value lab ID: JB25031-8 1.4 Non-detect 0.17 Non-detect 0.83 Non-detect 0.0029 Non-detect 0.014 Non-detect 0.0059 Non-detect 0.029 Non-detect R Rejected R 0.013 Non-detect 0.064 Non-detect 0.0021 Non-detect 0.0054 Non-detect 0.019 Non-detect 0.048 Non-detect 0.0023 Non-detect 0.0056 Non-detect 0.0024 Non-detect 0.0059 Non-detect 0.0023 Non-detect 0.0057 Non-detect 0.002 Non-detect 0.0051 Non-detect 0.0021 Non-detect 0.0052 Non-detect 0.0045 Non-detect 0.011 Non-detect 0.0026 Non-detect 0.0066 Non-detect 0.0023 Non-detect 0.0057 Non-detect 0.0026 Non-detect 0.0065 Non-detect 0.0011 Non-detect 0.0027 Non-detect **24** 03/14/13 03/19/13

em ulsion em ulsion 193.1 162.3 Estimated Estimated 182.7 158.20.0021 Non-detect 0.0052 Non-detect 0.007 Non-detect 0.018 Non-detect 0.0046 Non-detect 0.012 Non-detect 0.0023 Non-detect 0.0057 Non-detect 0.0024 Non-detect 0.0059 Non-detect 0.0029 Non-detect 0.0072 Non-detect 0.011 Non-detect 0.028 Non-detect 0.0027 Non-detect 0.0067 Non-detect 0.1892 0.2229 0.0019 Non-detect 0.0048 Non-detect 0.0024 Non-detect 0.006 Non-detect3/21/2013 - 4/9/2013 13-S2-B-03-19-2013 JB25032-2 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 5.29 1.07 0.0373 0.83 Non-detect 0.014 Non-detect 0.029 Non-detect Rejected R Rejected 0.064 Non-detect 0.0054 Non-detect 0.048 Non-detect 0.0056 Non-detect 0.0059 Non-detect 0.0057 Non-detect 0.0051 Non-detect 0.0052 Non-detect 0.011 Non-detect 0.0066 Non-detect 0.0057 Non-detect 0.0065 Non-detect 0.0027 Non-detect **25 26**  03/19/13

emulsion 162.3 Estimated Estimated 158.20.0052 Non-detect 0.018 Non-detect 0.012 Non-detect 0.0057 Non-detect 0.0059 Non-detect 0.0072 Non-detect 0.028 Non-detect 0.0067 Non-detect 0.1304 0.0048 Non-detect 0.006 Non-detect4/1/2013 - 4/8/2013 4/1/2013 - 4/8/2013

14-S2-A-03-27-2013 14-S2-B-03-27-2013 JB25033-1 JB25033-2 **Concentration (ppmw)**  **Non-Detect? Note(s)**  **Concentration (ppmw)**  **Non-Detect?**

10 Non-detect 10 Non-detect 11.1 9.11 6.13 5.95 0.068 Non-detect 0.068 Non-detect R Rejected R 0.0029 Non-detect 0.0029 Non-detect 0.0059 Non-detect 0.0059 Non-detect R Rejected R R Rejected R 0.0054 Non-detect 0.0054 Non-detect 0.048 Non-detect 0.048 Non-detect 0.0056 Non-detect 0.0056 Non-detect 0.0059 Non-detect 0.0059 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.0051 Non-detect 0.0051 Non-detect 0.0052 Non-detect 0.0052 Non-detect 0.011 Non-detect 0.011 Non-detect 0.0066 Non-detect 0.0066 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.0065 Non-detect 0.0065 Non-detect 0.0027 Non-detect 0.0027 Non-detect **27** 03/27/13 03/27/13

em ulsion em ulsion 169.6 169.6 Estimated Estimated 185.4 185.40.0052 Non-detect 0.0052 Non-detect 0.018 Non-detect 0.018 Non-detect 0.012 Non-detect 0.012 Non-detect 0.0057 Non-detect 0.0057 Non-detect 0.0059 Non-detect 0.0059 Non-detect 0.0072 Non-detect 0.0072 Non-detect 0.028 Non-detect 0.028 Non-detect 0.0067 Non-detect 0.0067 Non-detect 0.0865 0.0899 0.0048 Non-detect 0.0048 Non-detect 0.006 Non-detect 0.006 Non-detect4/4/2013-4/8/2013 15-S2-A-04-01-2013 JB25034-1 **Note(s) Concentration**  **(ppmw) Non-Detect?**  **Note(s)**

10 Non-detect 5.73 0.501 0.0868 Rejected 1.7 Non-detect 0.029 Non-detect 0.059 Non-detect Rejected 0.5 Non-detect Rejected 0.13 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0026 Non-detect 0.0023 Non-detect 0.0026 Non-detect 0.0011 Non-detect **29 28**  04/01/13

emulsion 166.5 Estimated Estimated 1850.0021 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.0027 Non-detect Non-detect 0.0019 Non-detect 0.0024 Non-detect4/4/2013-4/8/2013

15-S2-B-04-01-2013 JB25034-2 **Concentration (ppmw)**  **Non-Detect? Note(s)** 

10 Non-detect 6.71 0.54 0.0887 1.7 Non-detect 0.029 Non-detect 0.059 Non-detect 0.5 Non-detect 0.13 Non-detect 0.0021 Non-detect 0.019 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0023 Non-detect 0.002 Non-detect 0.0021 Non-detect 0.0045 Non-detect 0.0026 Non-detect 0.0023 Non-detect 0.0026 Non-detect 0.0011 Non-detect **30** 04/01/13

em ulsion 166.5 Estimated 1850.0021 Non-detect 0.007 Non-detect 0.0046 Non-detect 0.0023 Non-detect 0.0024 Non-detect 0.0029 Non-detect 0.011 Non-detect 0.0027 Non-detect Non-detect 0.0019 Non-detect 0.0024 Non-detect