### Name: Gary Kowalczyk

Title: General Manager Martin Plant Company: Florida Power & Light Sign Date: 7/29/2010 Name: Thomas K. Graham Title: Director of Operations Company:Air Hygiene International, Inc. Sign Date: 6/9/2010 Permitted Facility Representative / Date Testing Company Representative / Date



## Martin Energy Center, Unit #2, Information Collection Request Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Tuesday, February 15, 2011 Page 1 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Facility Information: Martin Energy Center 21900 SW Warfield Boulevard, SR 710

Indiantown FL34956 Contact:Augie De La Vega Phone: (305) 242-3896 Fax: Email: augie.de.la.vega@fpl.com Testing Company: Air Hygiene International, Inc. 5634 S. 122nd East Ave, Suite F

Tulsa OK74146 Contact:Thomas Graham Phone:(918) 307-8865 Fax: (918) 307-9131 Email: tom@airhygiene.com

Air Permit Number: 0850001-018-AV Permitted Source ID/Name: Foster Wheeler, Wall Fired Boiler PMR2 Permitted Maximum Process Rate: 863.3 MW Max. Normal Operation Process Rate: 800 MW Target Process Test Rate 800 MW

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Florida Power and Light Company (FPL) operates two oil fired electric utility steam generating units of Foster Wheeler design, designated as Units PMR1 and PMR2. The facility is located at 21900 Southwest Warfield Boulevard, State Route 710 in Indiantown, Florida. Unit PMR1 and PMR2 are of identical design and consists of two wall fired boilers and ancillary equipment designed to generate 863.3 megawatts (MW) of electricity each with rated heat inputs of 8,650 million British thermal units per hour (MMBtu/hr) based on high heating value (HHV). Fuel oil consumption is rated at 600,000 pounds per hour. Unit PMR1 and PMR2 utilize low nitrogen oxide (NOx) burner technology to control NOx emissions and cyclone separators to control particulate matter (PM) emissions. Emission testing will be conducted from platforms on the independent stacks of each unit. Industry/SCC/NAIS221112

Sampling Location Information:

Test Parameter Information: AFS #:0850001 FRS #:110008320566

SCC / Description10100401 External Combustion Boilers - Electric Generation - Residual Oil - Grade 6 Oil: Normal Firing

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width PMR2 - D/F 357.4 4524 876 4 0 24 0 0 PMR2 - Gases357.4 4524 876 4 0 1 0 0 PMR2 - Metals357.4 4524 876 4 0 24 0 0 PMR2 - PM 357.4 4524 876 4 0 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location Regulation Description Compound Limit Unit Not applicable.



### Tuesday, February 15, 2011 Page 2 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location % H2O Method 1 - 4 3 480 24 PMR2 - D/F 2,3,7,8-TCDD Method 23 3 480 24 PMR2 - D/F 1,2,3,7,8-PeCDD Method 23 3 480 24 PMR2 - D/F 1,2,3,4,7,8-HxCDD Method 23 3 480 24 PMR2 - D/F 1,2,3,6,7,8-HxCDD Method 23 3 480 24 PMR2 - D/F 1,2,3,7,8,9-HxCDD Method 23 3 480 24 PMR2 - D/F 1,2,3,4,6,7,8-HpCDD Method 23 3 480 24 PMR2 - D/F OCDD Method 23 3 480 24 PMR2 - D/F 2,3,7,8-TCDF Method 23 3 480 24 PMR2 - D/F 1,2,3,7,8-PeCDF Method 23 3 480 24 PMR2 - D/F 2,3,4,7,8-PeCDF Method 23 3 480 24 PMR2 - D/F 1,2,3,4,7,8-HxCDF Method 23 3 480 24 PMR2 - D/F 1,2,3,6,7,8-HxCDF Method 23 3 480 24 PMR2 - D/F 2,3,4,6,7,8-HxCDF Method 23 3 480 24 PMR2 - D/F 1,2,3,7,8,9-HxCDF Method 23 3 480 24 PMR2 - D/F 1,2,3,4,6,7,8-HpCDF Method 23 3 480 24 PMR2 - D/F 1,2,3,4,7,8,9-HpCDF Method 23 3 480 24 PMR2 - D/F OCDF Method 23 3 480 24 PMR2 - D/F Total Dioxins Method 23 3 480 24 PMR2 - D/F Total Furans Method 23 3 480 24 PMR2 - D/F 3,3',4,4'-TCB (PCB77) Method 23 3 480 24 PMR2 - D/F 3,4,4',5-TCB (PCB81) Method 23 3 480 24 PMR2 - D/F 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 24 PMR2 - D/F 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 24 PMR2 - D/F 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 24 PMR2 - D/F 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 24 PMR2 - D/F 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 24 PMR2 - D/F 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 24 PMR2 - D/F
2,3',4,4',5,5'-HxCB (PCB167)Method 23 3 480 24 PMR2 - D/F 3,3',4,4',5,5'-HxCB (PCB169)Method 23 3 480 24 PMR2 - D/F 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 24 PMR2 - D/F

O2 Method 3A O2 3 480 24 PMR2 - D/F Co2 Method 3A CO2 3 480 24 PMR2 - D/F % H2O Method 1 - 4 3 120 1 Determined after initial stratification test PMR2 - Gases

Carbon Monoxide Method 10 3 120 1 Determined after initial stratification test PMR2 - Gases
Total organic compounds

(TOC) as Propane Method 25A 3 120 1 Determined after initial stratification test PMR2 - Gases

O2 Method 3A O2 3 120 1 Determined after initial stratification test PMR2 - Gases

Co2 Method 3A CO2 3 120 1 Determined after initial stratification test PMR2 - Gases

Sulfur Dioxide Method 6C 3 120 1 Determined after initial stratification test PMR2 - Gases
Nitrogen oxides (NOx) Method 7E 3 120 1 Determined after initial stratification test PMR2 - Gases

% H2O Method 1 - 4 3 240 24 PMR2 - MetalsSelenium Method 29 3 240 24 PMR2 - MetalsManganese Method 29 3 240 24 PMR2 - Metals


### Tuesday, February 15, 2011 Page 3 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. PM Run All - reduced to 2 hour runs to avoid high vacuum, did not pull required volumes.
PM Run 3 - oily substance in organic backhalf.

Lead Method 29 3 240 24 PMR2 - MetalsFilterable Particulate Method 29 3 240 24 PMR2 - MetalsCobalt Method 29 3 240 24 PMR2 - MetalsCadmium Method 29 3 240 24 PMR2 - MetalsChromium Method 29 3 240 24 PMR2 - MetalsNickel Method 29 3 240 24 PMR2 - MetalsCo2 Method 3A CO2 3 240 24 PMR2 - MetalsO2 Method 3A O2 3 240 24 PMR2 - Metals% H2O Method 1 - 4 3 120 12 Run times vary based on method calculations PMR2 - PM

Filterable Particulate OTM - 27/28 3 120 12 Run times vary based on method calculations PMR2 - PM

Filterable PM2.5 OTM - 27/28 3 120 12 Run times vary based on method calculations PMR2 - PM
Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 120 12 Run times vary based on method calculations PMR2 - PM
Organic Condensible

Particulate OTM - 27/28 3 120 12 Run times vary based on method calculations PMR2 - PM

Total PM2.5 OTM - 27/28 3 120 12 Run times vary based on method calculations PMR2 - PM

Total Particulate OTM - 27/28 3 120 12 Run times vary based on method calculations PMR2 - PM

O2 Method 3A O2 3 120 12 Run times vary based on method calculations PMR2 - PM

Co2 Method 3A CO2 3 120 12 Run times vary based on method calculations PMR2 - PM



### Tuesday, February 15, 2011 Page 4 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Sampling / Stack Data Results Summary


### Location PMR2 - D/F - Method 23 Average Run Number PMR2-23-1 PMR2-23- 2 PMR2-23-3

Test Date 4/13/2010 4/14/2010 4/15/2010 Run Start Time 8:30:00 AM 8:20:00 AM 8:29:00 AM

Run Finish Time 4:30:00 PM4:20:00 PM 4:29:00 PM Net Run Time, minutes 480 480 480 Dry Gas Meter Volume Sampled, dscf 366.702 307.304 312.237 328.748 Moisture Content of Stack Gas, % 9.58 10.01 9.57 9.720 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 13.82 13.81 13.89 13.840 Oxygen, % 4.04 4.13 4 4.057 Average Stack Gas Temperature, °F 323.63 325.50 327.00 325.377 Dry Volumetric Flow Rate, dry scfm 1,551,963.01,325,062.4 1,342,738.01,406,587.80 0 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,563,661.52,197,901.8 2,218,384.42,326,649.23 3 Percent Isokinetic of Sampling Rate, % 100.6 98.7 99.0 99.433 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Location PMR2 - Gases - Method 10 Average Run Number 2-CO-1 2-CO-2 2-CO-3
Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.00 0 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Fuel Type Oil Oil Oil
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 5 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 25A Average Run Number 2-THC-1 2-THC-2 2-THC-3
Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.00 0 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Fuel Type Oil Oil Oil
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Location PMR2 - Gases - Method 3A CO2 Average Run Number 2-CO2-1 2-CO2-2 2-CO2-3
Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.00 0 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Fuel Type Oil Oil Oil
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 6 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 3A O2 Average Run Number 2-O2-1 2-O2-2 2-O2-3
Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.00 0 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Fuel Type Oil Oil Oil
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Location PMR2 - Gases - Method 6C Average Run Number 2-SO2-1 2-SO2-2 2-SO2-3
Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.00 0 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Fuel Type Oil Oil Oil
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 7 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 7E Average Run Number 2-NOx-1 2-NOx-2 2-NOx-3
Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.00 0 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Fuel Type Oil Oil Oil
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Location PMR2 - Metals - Method 29 Average Run Number PMR2-29-1 PMR2-29- 2 PMR2-29-3

Test Date 4/13/2010 4/13/2010 4/14/2010 Run Start Time 9:20:00 AM2:10:00 PM11:06:00 AM Run Finish Time 1:20:00 PM6:10:00 PM 3:06:00 PM Net Run Time, minutes 240 240 240 Dry Gas Meter Volume Sampled, dscf 181.467 162.907 194.024 179.466 Moisture Content of Stack Gas, % 10.35 10.19 9.83 10.123 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 13.82 13.82 13.81 13.817 Oxygen, % 4.04 4.04 4.13 4.070 Average Stack Gas Temperature, °F 317.88 324.17 326.92 322.990 Dry Volumetric Flow Rate, dry scfm 1,566,802.61,372,399.4 1,636,364.71,525,188.90 0 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,591,250.22,279,414.0 2,708,293.32,526,319.16 7 Percent Isokinetic of Sampling Rate, % 98.6 101.1 101.0 100.233 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 8 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - PM - OTM - 27/28 Average Run Number PMR2- 27/28-1 PMR2-

27/28-2 PMR2-

27/28-3
Test Date 4/12/2010 4/12/2010 4/14/2010 Run Start Time 2:38:00 PM6:49:00 PM 8:23:00 AM Run Finish Time 5:34:00 PM9:30:00 PM10:56:00 AM Net Run Time, minutes 129 126 127 Dry Gas Meter Volume Sampled, dscf 44.745 42.447 43.709 43.634 Moisture Content of Stack Gas, % 9.54 9.43 9.45 9.473 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 13.82 13.82 13.89 13.843 Oxygen, % 4.04 4.04 4 4.027 Average Stack Gas Temperature, °F 314.58 313.58 324.00 317.387 Dry Volumetric Flow Rate, dry scfm 1,390,346.01,407,916.1 1,455,776.51,418,012.86 7 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,266,873.72,293,626.4 2,395,203.02,318,567.70 0 Percent Isokinetic of Sampling Rate, % 107.7 103.3 102.1 104.367 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 9 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Emissions Summary


### Location: PMR2 - D/F - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000081 0.00000000559 0.0000000039 0.000 lb/mmBtuO2 5.55E-13 4.59E-13 3.13E-13 0.000 ng/dscm 7.80E-04 6.42E-04 4.41E-04 0.001 ng/dscm@7%O2 6.43E-04 5.32E-04 3.63E-04 0.001 

### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000096 0.0000000062 0.0000000011 0.000 lb/mmBtuO2 6.58E-13 5.09E-13 8.83E-14 0.000 ng/dscm 9.25E-04 7.13E-04 1.24E-04 0.001 ng/dscm@7%O2 7.63E-04 5.91E-04 1.02E-04 0.000 

### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000023 0.0000000029 0.0000000014 0.000 lb/mmBtuO2 1.58E-13 2.38E-13 1.12E-13 0.000 ng/dscm 2.22E-04 3.33E-04 1.58E-04 0.000 ng/dscm@7%O2 1.83E-04 2.76E-04 1.30E-04 0.000 

### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000024 0.0000000023 0.0000000012 0.000 lb/mmBtuO2 1.64E-13 1.89E-13 9.63E-14 0.000 ng/dscm 2.31E-04 2.64E-04 1.36E-04 0.000 ng/dscm@7%O2 1.90E-04 2.19E-04 1.12E-04 0.000 

### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000017 0.0000000014 0.0000000026 0.000 lb/mmBtuO2 1.16E-13 1.15E-13 2.09E-13 0.000 ng/dscm 1.64E-04 1.61E-04 2.94E-04 0.000 ng/dscm@7%O2 1.35E-04 1.33E-04 2.42E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000033 0.0000000016 0.0000000012 0.000 lb/mmBtuO2 2.26E-13 1.31E-13 9.63E-14 0.000 ng/dscm 3.18E-04 1.84E-04 1.36E-04 0.000 ng/dscm@7%O2 2.62E-04 1.53E-04 1.12E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDF Average



### Tuesday, February 15, 2011 Page 10 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000016 0.0000000015 0.00000000095 0.000 lb/mmBtuO2 1.10E-13 1.23E-13 7.62E-14 0.000 ng/dscm 1.54E-04 1.72E-04 1.07E-04 0.000 ng/dscm@7%O2 1.27E-04 1.43E-04 8.80E-05 0.000 

### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000000236 0.0000000016 0.0000000012 0.000 lb/mmBtuO2 1.62E-13 1.31E-13 9.63E-14 0.000 ng/dscm 2.27E-04 1.84E-04 1.36E-04 0.000 ng/dscm@7%O2 1.87E-04 1.53E-04 1.12E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000018 0.0000000014 0.0000000011 0.000 lb/mmBtuO2 1.23E-13 1.15E-13 8.83E-14 0.000 ng/dscm 1.73E-04 1.61E-04 1.24E-04 0.000 ng/dscm@7%O2 1.43E-04 1.33E-04 1.02E-04 0.000 

### Compound: 1,2,3,7,8-PeCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000025 0.000000002 0.0000000014 0.000 lb/mmBtuO2 1.71E-13 1.64E-13 1.12E-13 0.000 ng/dscm 2.41E-04 2.30E-04 1.58E-04 0.000 ng/dscm@7%O2 1.99E-04 1.91E-04 1.30E-04 0.000 

### Compound: 1,2,3,7,8-PeCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000000327 0.0000000017 0.000000001 0.000 lb/mmBtuO2 2.24E-13 1.40E-13 8.02E-14 0.000 ng/dscm 3.15E-04 1.95E-04 1.13E-04 0.000 ng/dscm@7%O2 2.60E-04 1.62E-04 9.29E-05 0.000 

### Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000027 0.000000003 0.0000000018 0.000 lb/mmBtuO2 1.85E-13 2.46E-13 1.44E-13 0.000 ng/dscm 2.60E-04 3.45E-04 2.04E-04 0.000 ng/dscm@7%O2 2.14E-04 2.86E-04 1.68E-04 0.000 

### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000146 0.0000000071 0.0000000051 0.000 lb/mmBtuO2 1.00E-12 5.83E-13 4.09E-13 0.000 ng/dscm 1.41E-03 8.16E-04 5.77E-04 0.001 ng/dscm@7%O2 1.16E-03 6.76E-04 4.75E-04 0.001



### Tuesday, February 15, 2011 Page 11 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.000000376 0.000000257 0.000000197 0.000 lb/mmBtuO2 2.58E-11 2.11E-11 1.58E-11 0.000 ng/dscm 3.62E-02 2.95E-02 2.23E-02 0.029 ng/dscm@7%O2 2.98E-02 2.45E-02 1.83E-02 0.024 

### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000259 0.00000002 0.0000000165 0.000 lb/mmBtuO2 1.77E-12 1.64E-12 1.32E-12 0.000 ng/dscm 2.49E-03 2.30E-03 1.87E-03 0.002 ng/dscm@7%O2 2.05E-03 1.91E-03 1.54E-03 0.002 

### Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000392 0.0000000201 0.0000000187 0.000 lb/mmBtuO2 2.68E-12 1.65E-12 1.50E-12 0.000 ng/dscm 3.78E-03 2.31E-03 2.12E-03 0.003 ng/dscm@7%O2 3.12E-03 1.91E-03 1.74E-03 0.002 

### Compound: 2,3',4,4',5-PeCB (PCB118) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000104 0.000000773 0.00000058 0.000 lb/mmBtuO2 7.12E-11 6.35E-11 4.65E-11 0.000 ng/dscm 1.00E-01 8.88E-02 6.56E-02 0.085 ng/dscm@7%O2 8.24E-02 7.36E-02 5.40E-02 0.070 

### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000002 0.0000000185 0.0000000119 0.000 lb/mmBtuO2 1.37E-12 1.52E-12 9.55E-13 0.000 ng/dscm 1.93E-03 2.13E-03 1.35E-03 0.002 ng/dscm@7%O2 1.59E-03 1.77E-03 1.11E-03 0.001 

### Compound: 2,3,4,6,7,8-HxCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000029 0.0000000015 0.00000000097 0.000 lb/mmBtuO2 1.99E-13 1.23E-13 7.78E-14 0.000 ng/dscm 2.79E-04 1.72E-04 1.10E-04 0.000 ng/dscm@7%O2 2.30E-04 1.43E-04 9.05E-05 0.000 

### Compound: 2,3,4,7,8-PeCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000039 0.0000000016 0.00000000093 0.000 lb/mmBtuO2 2.67E-13 1.31E-13 7.46E-14 0.000



### Tuesday, February 15, 2011 Page 12 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 ng/dscm 3.76E-04 1.84E-04 1.05E-04 0.000 ng/dscm@7%O2 3.10E-04 1.53E-04 8.64E-05 0.000 

### Compound: 2,3,7,8-TCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000024 0.000000002 0.0000000019 0.000 lb/mmBtuO2 1.64E-13 1.64E-13 1.52E-13 0.000 ng/dscm 2.31E-04 2.30E-04 2.15E-04 0.000 ng/dscm@7%O2 1.90E-04 1.91E-04 1.77E-04 0.000 

### Compound: 2,3,7,8-TCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.000000005 0.000000002 0.0000000013 0.000 lb/mmBtuO2 3.42E-13 1.64E-13 1.04E-13 0.000 ng/dscm 4.82E-04 2.30E-04 1.47E-04 0.000 ng/dscm@7%O2 3.97E-04 1.91E-04 1.21E-04 0.000 

### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000000235 0.00000000079 0.0000000013 0.000 lb/mmBtuO2 1.61E-13 6.49E-14 1.04E-13 0.000 ng/dscm 2.26E-04 9.08E-05 1.47E-04 0.000 ng/dscm@7%O2 1.86E-04 7.53E-05 1.21E-04 0.000 

### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000031 0.0000000031 0.0000000028 0.000 lb/mmBtuO2 2.12E-13 2.55E-13 2.25E-13 0.000 ng/dscm 2.99E-04 3.56E-04 3.17E-04 0.000 ng/dscm@7%O2 2.47E-04 2.95E-04 2.61E-04 0.000 

### Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.000000131 0.0000000958 0.0000000675 0.000 lb/mmBtuO2 8.97E-12 7.87E-12 5.42E-12 0.000 ng/dscm 1.26E-02 1.10E-02 7.64E-03 0.010 ng/dscm@7%O2 1.04E-02 9.12E-03 6.28E-03 0.009 

### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000000804 0.00000000538 0.00000000424 0.000 lb/mmBtuO2 5.51E-13 4.42E-13 3.40E-13 0.000 ng/dscm 7.74E-04 6.18E-04 4.80E-04 0.001 ng/dscm@7%O2 6.38E-04 5.12E-04 3.95E-04 0.001 

### Compound: OCDD Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3


### Tuesday, February 15, 2011 Page 13 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Mass_mg 0.000000022 0.0000000048 0.0000000224 0.000 lb/mmBtuO2 1.51E-12 3.94E-13 1.80E-12 0.000 ng/dscm 2.12E-03 5.52E-04 2.53E-03 0.002 ng/dscm@7%O2 1.75E-03 4.58E-04 2.08E-03 0.001 

### Compound: OCDF Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.0000000062 0.0000000047 0.0000000116 0.000 lb/mmBtuO2 4.25E-13 3.86E-13 9.31E-13 0.000 ng/dscm 5.97E-04 5.40E-04 1.31E-03 0.001 ng/dscm@7%O2 4.92E-04 4.48E-04 1.08E-03 0.001 

### Compound: Total Dioxins Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000004306 0.00000001989 0.0000000332 0.000 lb/mmBtuO2 2.95E-12 1.63E-12 2.66E-12 0.000 ng/dscm 4.15E-03 2.29E-03 3.76E-03 0.003 ng/dscm@7%O2 3.42E-03 1.90E-03 3.09E-03 0.003 

### Compound: Total Furans Average RunNumber PMR2-23-1 PMR2-23-2 PMR2-23-3 Mass_mg 0.00000003827 0.0000000249 0.00000002295 0.000 lb/mmBtuO2 2.62E-12 2.05E-12 1.84E-12 0.000 ng/dscm 3.69E-03 2.86E-03 2.60E-03 0.003 ng/dscm@7%O2 3.04E-03 2.37E-03 2.14E-03 0.003



### Location: PMR2 - Gases - Method 10 Compound: Carbon Monoxide Average Run 2-CO-1 2-CO-2 2-CO-3 lb/mmBtuO2 4.60E-01 4.55E-01 5.49E-01 0.488 ppm 5.52E+02 5.51E+02 6.66E+02 589.667 ppm@7%O2 4.58E+02 4.53E+02 5.47E+02 486.000



### Location: PMR2 - Gases - Method 25A Compound: Total organic compounds (TOC) as Average Run 2-THC-1 2-THC-2 2-THC-3 lb/mmBtuO2 1.22E-03 2.22E-04 3.75E-04 0.001 ppm 9.26E-01 1.70E-01 2.89E-01 0.462 ppm@7%O2 7.68E-01 1.40E-01 2.37E-01 0.382



### Location: PMR2 - Gases - Method 6C Compound: Sulfur Dioxide Average Run 2-SO2-1 2-SO2-2 2-SO2-3 lb/mmBtuO2 4.69E-01 5.96E-01 6.29E-01 0.565 ppm 2.46E+02 3.15E+02 3.33E+02 298.000 ppm@7%O2 2.04E+02 2.59E+02 2.73E+02 245.333



### Tuesday, February 15, 2011 Page 14 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010

Location: PMR2 - Gases - Method 7E 

### Compound: Nitrogen oxides (NOx) Average Run 2-NOx-1 2-NOx-2 2-NOx-3 lb/mmBtuO2 2.96E-01 2.97E-01 2.98E-01 0.297 ppm 2.16E+02 2.19E+02 2.20E+02 218.333 ppm@7%O2 1.79E+02 1.80E+02 1.81E+02 180.000



### Location: PMR2 - Metals - Method 29 

### Compound: Antimony Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.326 0.144 0.36 0.277 Elb/hr 3.72E-01 1.60E-01 4.02E-01 0.311 lb/mmBtuO2 4.51E-05 2.22E-05 4.69E-05 0.000 mg/dscm 6.35E-02 3.12E-02 6.55E-02 0.053 mg/dscm@7%O2 5.24E-02 2.57E-02 5.43E-02 0.044 

### Compound: Arsenic Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.0178 0.012 0.0249 0.018 Elb/hr 2.03E-02 1.34E-02 2.78E-02 0.021 lb/mmBtuO2 2.46E-06 1.85E-06 3.24E-06 0.000 mg/dscm 3.46E-03 2.60E-03 4.53E-03 0.004 mg/dscm@7%O2 2.85E-03 2.14E-03 3.75E-03 0.003 

### Compound: Beryllium Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.00162 0.00117 0.00188 0.002 Elb/hr 1.85E-03 1.30E-03 2.10E-03 0.002 lb/mmBtuO2 2.24E-07 1.80E-07 2.45E-07 0.000 mg/dscm 3.15E-04 2.54E-04 3.42E-04 0.000 mg/dscm@7%O2 2.60E-04 2.09E-04 2.83E-04 0.000 

### Compound: Cadmium Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.000659 0.00044 0.000586 0.001 Elb/hr 7.53E-04 4.90E-04 6.54E-04 0.001 lb/mmBtuO2 9.12E-08 6.78E-08 7.63E-08 0.000 mg/dscm 1.28E-04 9.54E-05 1.07E-04 0.000 mg/dscm@7%O2 1.06E-04 7.87E-05 8.87E-05 0.000 

### Compound: Chromium Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.0439 0.0275 0.0404 0.037 Elb/hr 5.01E-02 3.06E-02 4.51E-02 0.042 lb/mmBtuO2 6.08E-06 4.24E-06 5.26E-06 0.000 mg/dscm 8.54E-03 5.96E-03 7.35E-03 0.007



### Tuesday, February 15, 2011 Page 15 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 mg/dscm@7%O2 7.04E-03 4.91E-03 6.09E-03 0.006 

### Compound: Cobalt Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.229 0.114 0.261 0.201 Elb/hr 2.62E-01 1.27E-01 2.91E-01 0.227 lb/mmBtuO2 3.17E-05 1.76E-05 3.40E-05 0.000 mg/dscm 4.46E-02 2.47E-02 4.75E-02 0.039 mg/dscm@7%O2 3.68E-02 2.04E-02 3.94E-02 0.032 

### Compound: Filterable Particulate Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 167.8 52.2 194.9 138.300 Elb/hr 1.92E+02 5.82E+01 2.17E+02 155.733 lb/mmBtuO2 2.32E-02 8.05E-03 2.54E-02 0.019 mg/dscm 3.27E+01 1.13E+01 3.55E+01 26.500 mg/dscm@7%O2 2.70E+01 9.32E+00 2.94E+01 21.907 

### Compound: Lead Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.0727 0.0368 0.0687 0.059 Elb/hr 8.30E-02 4.10E-02 7.66E-02 0.067 lb/mmBtuO2 1.01E-05 5.67E-06 8.94E-06 0.000 mg/dscm 1.42E-02 7.98E-03 1.25E-02 0.012 mg/dscm@7%O2 1.17E-02 6.58E-03 1.04E-02 0.010 

### Compound: Manganese Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.296 0.168 0.338 0.267 Elb/hr 3.38E-01 1.87E-01 3.77E-01 0.301 lb/mmBtuO2 4.10E-05 2.59E-05 4.40E-05 0.000 mg/dscm 5.76E-02 3.64E-02 6.15E-02 0.052 mg/dscm@7%O2 4.75E-02 3.00E-02 5.10E-02 0.043 

### Compound: Nickel Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 2.77 1.36 3.12 2.417 Elb/hr 3.16E+00 1.52E+00 3.48E+00 2.720 lb/mmBtuO2 3.83E-04 2.10E-04 4.06E-04 0.000 mg/dscm 5.39E-01 2.95E-01 5.68E-01 0.467 mg/dscm@7%O2 4.44E-01 2.43E-01 4.71E-01 0.386 

### Compound: Selenium Average RunNumber PMR2-29-1 PMR2-29-2 PMR2-29-3 Mass_mg 0.00954 0.00766 0.0258 0.014 Elb/hr 1.09E-02 8.54E-03 2.88E-02 0.016 lb/mmBtuO2 1.32E-06 1.18E-06 3.36E-06 0.000 mg/dscm 1.86E-03 1.66E-03 4.70E-03 0.003


### Tuesday, February 15, 2011 Page 16 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010

Process Run Data mg/dscm@7%O2 1.53E-03 1.37E-03 3.90E-03 0.002



### Location: PMR2 - PM - OTM - 27/28 Compound: Filterable Particulate Average RunNumber PMR2-27/28-2 PMR2-27/28-3 PMR2-27/28-1 Mass_mg 41.75 43.427 37.825 41.001 lb/mmBtuO2 2.47E-02 2.49E-02 2.12E-02 0.024 

### Compound: Filterable PM2.5 Average RunNumber PMR2-27/28-1 PMR2-27/28-2 PMR2-27/28-3 Mass_mg 24.95 38.475 38.125 33.850 lb/mmBtuO2 1.40E-02 2.28E-02 2.19E-02 0.020 

### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber PMR2-27/28-1 PMR2-27/28-2 PMR2-27/28-3 Mass_mg 2.995 5.859 1.79 3.548 lb/mmBtuO2 1.68E-03 3.47E-03 1.03E-03 0.002 

### Compound: Organic Condensible Particulate Average RunNumber PMR2-27/28-1 PMR2-27/28-2 PMR2-27/28-3 Mass_mg 3.988 3.406 31.306 12.900 lb/mmBtuO2 2.24E-03 2.02E-03 1.79E-02 0.007 

### Compound: Total Particulate Average RunNumber PMR2-27/28-1 PMR2-27/28-2 PMR2-27/28-3 Mass_mg 44.807 51.015 76.524 57.449 lb/mmBtuO2 2.52E-02 3.02E-02 4.39E-02 0.033 

### Compound: Total PM2.5 Average RunNumber PMR2-27/28-1 PMR2-27/28-2 PMR2-27/28-3 Mass_mg 31.932 47.74 71.221 50.298 lb/mmBtuO2 1.79E-02 2.82E-02 4.08E-02 0.029



### Tuesday, February 15, 2011 Page 17 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Process Run Data



### Run Name Value UOM Comments Target Value 1 Residual Oil (No. 6) Burned 56990 gal/hr Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 4/13/2010; Start - 15:25; End - 17:24 0



### 10Residual Oil (No. 6) Burned 56486 gal/hr Method 027/028; Run PM-1; Date - 4/12/2010; Start - 14:38; End - 17:34 0

11Residual Oil (No. 6) Burned 56457 gal/hr Method 027/028; Run PM-2; Date - 4/12/2010; Start - 18:49; End - 21:30 0

12Residual Oil (No. 6) Burned 57570 gal/hr Method 027/028; Run PM-3; Date - 4/14/2010; Start - 08:23; End - 10:56 0

2 Residual Oil (No. 6) Burned 57005 gal/hr Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 4/13/2010; Start - 17:43; End - 19:42 0

3 Residual Oil (No. 6) Burned 57474 gal/hr Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 4/13/2010; Start - 19:52; End - 21:51 0



### 4 Residual Oil (No. 6) Burned 57101 gal/hr Method 23; Run D/F-1; Date - 4/13/2010; Start - 08:30; End - 17:13 0

5 Residual Oil (No. 6) Burned 57570 gal/hr Method 23; Run D/F-2; Date - 4/14/2010; Start - 08:20; End - 17:00 0

6 Residual Oil (No. 6) Burned 57218 gal/hr Method 23; Run D/F-3; Date - 4/15/2010; Start - 08:29; End - 16:56 0

7 Residual Oil (No. 6) Burned 57101 gal/hr Method 29; Run M-1; Date - 4/13/2010; Start - 09:20; End - 13:48 0



### Tuesday, February 15, 2011 Page 18 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 8 Residual Oil (No. 6) Burned 57042 gal/hr Method 29; Run M-2; Date - 4/13/2010; Start - 14:10; End - 18:48 0

9 Residual Oil (No. 6) Burned 57599 gal/hr Method 29; Run M-3; Date - 4/14/2010; Start - 11:06; End - 15:36 0

1 Average Heat Input 7184 MMBtu/hr Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 4/13/2010; Start - 15:25; End - 17:24 0



### 10Average Heat Input 7121 MMBtu/hr Method 027/028; Run PM-1; Date - 4/12/2010; Start - 14:38; End - 17:34 0

11Average Heat Input 7133 MMBtu/hr Method 027/028; Run PM-2; Date - 4/12/2010; Start - 18:49; End - 21:30 0

12Average Heat Input 72585 MMBtu/hr Method 027/028; Run PM-3; Date - 4/14/2010; Start - 08:23; End - 10:56 0

2 Average Heat Input 7187 MMBtu/hr Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 4/13/2010; Start - 17:43; End - 19:42 0

3 Average Heat Input 7245 MMBtu/hr Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 4/13/2010; Start - 19:52; End - 21:51 0



### 4 Average Heat Input 7199 MMBtu/hr Method 23; Run D/F-1; Date - 4/13/2010; Start - 08:30; End - 17:13 0

5 Average Heat Input 7258 MMBtu/hr Method 23; Run D/F-2; Date - 4/14/2010; Start - 08:20; End - 17:00 0

6 Average Heat Input 7213 MMBtu/hr Method 23; Run D/F-3; Date - 4/15/2010; Start - 08:29; End - 16:56 0



### Tuesday, February 15, 2011 Page 19 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 7 Average Heat Input 7199 MMBtu/hr Method 29; Run M-1; Date - 4/13/2010; Start - 09:20; End - 13:48 0

8 Average Heat Input 7191 MMBtu/hr Method 29; Run M-2; Date - 4/13/2010; Start - 14:10; End - 18:48 0

9 Average Heat Input 7262 MMBtu/hr Method 29; Run M-3; Date - 4/14/2010; Start - 11:06; End - 15:36 0

1 Steam Output 5191 1000 lb Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 4/13/2010; Start - 15:25; End - 17:24 0



### 10Steam Output 5147 1000 lb Method 027/028; Run PM-1; Date - 4/12/2010; Start - 14:38; End - 17:34 0

11Steam Output 5141 1000 lb Method 027/028; Run PM-2; Date - 4/12/2010; Start - 18:49; End - 21:30 0

12Steam Output 5214 1000 lb Method 027/028; Run PM-3; Date - 4/14/2010; Start - 08:23; End - 10:56 0

2 Steam Output 5173 1000 lb Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 4/13/2010; Start - 17:43; End - 19:42 0

3 Steam Output 5184 1000 lb Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 4/13/2010; Start - 19:52; End - 21:51 0

4 Steam Output 5176 1000 lb Method 23; Run D/F-1; Date - 4/13/2010; Start - 08:30; End - 17:13 0

5 Steam Output 5194 1000 lb Method 23; Run D/F-2; Date - 4/14/2010; Start - 08:20; End - 17:00 0



### Tuesday, February 15, 2011 Page 20 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 6 Steam Output 5150 1000 lb Method 23; Run D/F-3; Date - 4/15/2010; Start - 08:29; End - 16:56 0

7 Steam Output 5170 1000 lb Method 29; Run M-1; Date - 4/13/2010; Start - 09:20; End - 13:48 0

8 Steam Output 5189 1000 lb Method 29; Run M-2; Date - 4/13/2010; Start - 14:10; End - 18:48 0

9 Steam Output 5187 1000 lb Method 29; Run M-3; Date - 4/14/2010; Start - 11:06; End - 15:36 0

1 Unit Gross Electrical Output 802 MWg Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 4/13/2010; Start - 15:25; End - 17:24 0



### 10Unit Gross Electrical Output 800 MWg Method 027/028; Run PM-1; Date - 4/12/2010; Start - 14:38; End - 17:34 0

11Unit Gross Electrical Output 800 MWg Method 027/028; Run PM-2; Date - 4/12/2010; Start - 18:49; End - 21:30 0

12Unit Gross Electrical Output 803 MWg Method 027/028; Run PM-3; Date - 4/14/2010; Start - 08:23; End - 10:56 0

2 Unit Gross Electrical Output 802 MWg Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 4/13/2010; Start - 17:43; End - 19:42 0

3 Unit Gross Electrical Output 803 MWg Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 4/13/2010; Start - 19:52; End - 21:51 0

4 Unit Gross Electrical Output 802 MWg Method 23; Run D/F-1; Date - 4/13/2010; Start - 08:30; End - 17:13 0



### Tuesday, February 15, 2011 Page 21 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 5 Unit Gross Electrical Output 803 MWg Method 23; Run D/F-2; Date - 4/14/2010; Start - 08:20; End - 17:00 0

6 Unit Gross Electrical Output 799 MWg Method 23; Run D/F-3; Date - 4/15/2010; Start - 08:29; End - 16:56 0

7 Unit Gross Electrical Output 802 MWg Method 29; Run M-1; Date - 4/13/2010; Start - 09:20; End - 13:48 0

8 Unit Gross Electrical Output 802 MWg Method 29; Run M-2; Date - 4/13/2010; Start - 14:10; End - 18:48 0

9 Unit Gross Electrical Output 802 MWg Method 29; Run M-3; Date - 4/14/2010; Start - 11:06; End - 15:36 0

1 Unit Net Electric Generation 774 MWn Methods 6c, 7e, 10, and 25a; Run RM-1 and FTIR-1; Date - 4/13/2010; Start - 15:25; End - 17:24 0



### 10Unit Net Electric Generation 771 MWn Method 027/028; Run PM-1; Date - 4/12/2010; Start - 14:38; End - 17:34 0

11Unit Net Electric Generation 771 MWn Method 027/028; Run PM-2; Date - 4/12/2010; Start - 18:49; End - 21:30 0

12Unit Net Electric Generation 773 MWn Method 027/028; Run PM-3; Date - 4/14/2010; Start - 08:23; End - 10:56 0

2 Unit Net Electric Generation 773 MWn Methods 6c, 7e, 10, and 25a; Run RM-2 and FTIR-2; Date - 4/13/2010; Start - 17:43; End - 19:42 0

3 Unit Net Electric Generation 773 MWn Methods 6c, 7e, 10, and 25a; Run RM-3 and FTIR-3; Date - 4/13/2010; Start - 19:52; End - 21:51 0



### Tuesday, February 15, 2011 Page 22 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010

APCD Run Data

Process Lab Run Data 4 Unit Net Electric Generation 774 MWn Method 23; Run D/F-1; Date - 4/13/2010; Start - 08:30; End - 17:13 0

5 Unit Net Electric Generation 774 MWn Method 23; Run D/F-2; Date - 4/14/2010; Start - 08:20; End - 17:00 0

6 Unit Net Electric Generation 771 MWn Method 23; Run D/F-3; Date - 4/15/2010; Start - 08:29; End - 16:56 0

7 Unit Net Electric Generation 774 MWn Method 29; Run M-1; Date - 4/13/2010; Start - 09:20; End - 13:48 0

8 Unit Net Electric Generation 774 MWn Method 29; Run M-2; Date - 4/13/2010; Start - 14:10; End - 18:48 0

9 Unit Net Electric Generation 774 MWn Method 29; Run M-3; Date - 4/14/2010; Start - 11:06; End - 15:36 0



### Run Name Value UOM Comments Target Value 1 LOW NOX BURNERS 194NOx Emissions 0


### 2 LOW NOX BURNERS 194NOx Emissions 0
3 LOW NOX BURNERS 195NOx Emissions 0
1 CYCLONE SEPARATORS 10.6 Opacity 0


### 2 CYCLONE SEPARATORS 10.7 Opacity 0
3 CYCLONE SEPARATORS 12.2 Opacity 0

Run Name Value UOM Comments 

### 1 Fuel Higher Heating Value 18500 Btu/lb 1 Fuel Moisture 0.794 % 1 Fuel Mercury Content 0.001 mg/kg 1 Fuel Chlorine Content 835 mg/kg 

### 1 Fuel Fluorine Content 40 mg/kg 1 Fuel Antimony Content 1.5 mg/kg 1 Fuel Arsenic Content 0.1 mg/kg 

### 1 Fuel Beryllium Content 0.01 mg/kg
Tuesday, February 15, 2011 Page 23 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 1 Fuel Cadmium Content 0.006 mg/kg 

### 1 Fuel Chromium Content 0.081 mg/kg 1 Fuel Cobalt Content 1.2 mg/kg 1 Fuel Lead Content 0.35 mg/kg 1 Fuel Manganese Content 1.5 mg/kg 

### 1 Fuel Nickel Content 12.8 mg/kg 1 Fuel Selenium Content 0.03 mg/kg 1 Fuel Sulfur Content 6550 mg/kg 

### 1 Fuel Proximate Analysis (Carbon) 88.38 % 1 Fuel Proximate Analysis (Hydrogen) 10.32 % 1 Fuel Proximate Analysis (Nitrogen) 0.5 % 1 Fuel Proximate Analysis (Oxygen) 0.5 % 

### 1 Fuel Proximate Analysis (Sulfur) 0.592 % 2 Fuel Higher Heating Value 18500 Btu/lb 2 Fuel Moisture 1.13 % 

### 2 Fuel Mercury Content 0.002 mg/kg 2 Fuel Chlorine Content 107 mg/kg 2 Fuel Fluorine Content 40 mg/kg 2 Fuel Antimony Content 1.5 mg/kg 

### 2 Fuel Arsenic Content 0.092 mg/kg 2 Fuel Beryllium Content 0.01 mg/kg 2 Fuel Cadmium Content 0.007 mg/kg 

### 2 Fuel Chromium Content 0.08 mg/kg 2 Fuel Cobalt Content 1.1 mg/kg 2 Fuel Lead Content 0.35 mg/kg 2 Fuel Manganese Content 1.5 mg/kg 

### 2 Fuel Nickel Content 12.6 mg/kg 2 Fuel Selenium Content 0.03 mg/kg 2 Fuel Sulfur Content 6480 mg/kg 

### 2 Fuel Proximate Analysis (Carbon) 88.03 % 2 Fuel Proximate Analysis (Hydrogen) 10.25 % 2 Fuel Proximate Analysis (Nitrogen) 0.5 % 2 Fuel Proximate Analysis (Oxygen) 0.5 % 

### 2 Fuel Proximate Analysis (Sulfur) 0.647 % 3 Fuel Higher Heating Value 18500 Btu/lb 3 Fuel Moisture 1.33 % 

### 3 Fuel Mercury Content 0.002 mg/kg 3 Fuel Chlorine Content 91.7 mg/kg 3 Fuel Fluorine Content 400 mg/kg 3 Fuel Antimony Content 1.5 mg/kg 

### 3 Fuel Arsenic Content 0.075 mg/kg 3 Fuel Beryllium Content 0.012 mg/kg 3 Fuel Cadmium Content 0.007 mg/kg



### Tuesday, February 15, 2011 Page 24 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 3 Fuel Chromium Content 0.078 mg/kg 

### 3 Fuel Cobalt Content 1.2 mg/kg 3 Fuel Lead Content 0.35 mg/kg 3 Fuel Manganese Content 1.5 mg/kg 3 Fuel Nickel Content 12.6 mg/kg 

### 3 Fuel Selenium Content 0.03 mg/kg 3 Fuel Sulfur Content 6430 mg/kg 3 Fuel Proximate Analysis (Carbon) 87.84 % 

### 3 Fuel Proximate Analysis (Hydrogen) 10.33 % 3 Fuel Proximate Analysis (Nitrogen) 0.54 % 3 Fuel Proximate Analysis (Oxygen) 0.5 % 3 Fuel Proximate Analysis (Sulfur) 0.652 %



### Tuesday, February 15, 2011 Page 25 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010 Sampling / Stack Data Results Detail


### Location PMR2 - D/F - Method 23 Average Run Number PMR2-23-1 PMR2-23-2 PMR2-23-3 Test Date 4/13/2010 4/14/2010 4/15/2010 Run Start Time 8:30:00 AM8:20:00 AM 8:29:00 AM Run Finish Time 4:30:00 PM4:20:00 PM 4:29:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 480 480 480 Nozzle Diameter, inches 0.25 0.25 0.25 0.250 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.002 0.979 1.002 0.994 Barometric Pressure, inches of Mercury 29.85 29.94 29.97 29.920 Average Orifice Meter Differential, inches H2O 2.04 1.41 1.53 1.660 Dry Gas Meter Volume Sampled, cubic feet 375.190 318.400 317.890 337.160 Average Dry Gas Meter Temperature, °F 82.75 77.79 81.56 80.700 Dry Gas Meter Volume Sampled, dscf 366.702 307.304 312.237 328.748 Total Moisture Liquid collected, g 825 726.5 701.8 751.100 Volume of Water Vapor, standard cubic feet 38.83 34.20 33.03 35.353 Moisture Content of Stack Gas, % 9.58 10.01 9.57 9.720 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9042 0.8999 0.9043 0.903 Carbon Dioxide, % 13.82 13.81 13.89 13.840 Oxygen, % 4.04 4.13 4 4.057 Carbon Monoxide & Nitrogen, % 82.14 82.06 82.11 82.103 Fuel Factor 1.22 1.21 1.22 Dry Molecular Weight, lb/lb-Mole 30.37 30.37 30.38 30.373 Wet Molecular weight, lb/lb-Mole 29.18 29.13 29.20 29.170 Flue Gas Static Pressure, inches of H2O -1.7 -1.7 -1.7 -1.700 Absolute Flue Gas Pressure, inches of Mercury 29.73 29.82 29.85 29.800 Average Stack Gas Temperature, °F 323.63 325.50 327.00 325.377 Average Velocity Head, inches of H2O 0.8075770879 273630.592948567

0946170.604940115

158624 0.668
Average Stack Gas Velocity, feet/second 61.33 52.58 53.07 55.660 Stack Cross-Sectional Area, square feet 696.685 696.685 696.685 696.685 Dry Volumetric Flow Rate, dry scfm 1,551,963.0 1,325,062.4 1,342,738.01,406,587.8 00 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,563,661.5 2,197,901.8 2,218,384.42,326,649.2 33 Percent Isokinetic of Sampling Rate, % 100.6 98.7 99.0 99.433 Percent Excess Air, % 22.9 23.6 22.6 23.033 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Round Duct Diameter, inches 357.4 357.4 357.4 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 26 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 10 Average Run Number 2-CO-1 2-CO-2 2-CO-3 Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM 5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Fuel Factor 1.32 1.32 1.32 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.0 00 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Analyzer Make THERMO THERMO THERMO Analyzer Model 48i 48i 48i Analyzer Serial Number INST-CO0017 INST-CO0017 INST-CO0017 Operating Range 1109 1109 1109 1,109.000 Operating Units ppm ppm ppm No. Readings/Avg. 240 240 240 240.000 Calibration Set 5 5 5 5.000 Calibration Pre Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Pre Zero Cylinder Instrument Response 5.86 6.51 7.94 6.770 Calibration Pre Zero Cylinder Bias 0.41 0.47 0.6 0.493 Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID ALM042523- COALM042523

-COALM042523-

CO Calibration Pre High Cylinder Instrument Response 559 551.7 542.06 550.920 Calibration Pre High Cylinder Bias 0.27 -0.39 -1.26 -0.460 Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Post Zero Cylinder Instrument Response 6.51 7.94 6.24 6.897 Calibration Post Zero Cylinder Bias 0.47 0.6 0.44 0.503 Calibration Post Zero Cylinder Drift 0.06 0.13 0.16 0.117 Calibration Post High Cylinder ID ALM042523- COALM042523

-COALM042523-

CO Calibration Post High Cylinder Instrument Response 551.7 542.06 543.01 545.590 Calibration Post High Cylinder Bias -0.39 -1.26 -1.17 -0.940 Calibration Post High Cylinder Drift 0.66 0.879.000000000 00001E-02 0.540
Cavg 557.94 549.08 656.16 587.727 Cavg Units ppmvd ppmvd ppmvd Cgas 551.5892 551.2381 665.5015 589.443 Cgas Units ppmvd ppmvd ppmvd Fuel Type Oil Oil Oil Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000 Cgasw 0 0 0 0.000 Cgasw Units ppmvw ppmvw ppmvw



### Tuesday, February 15, 2011 Page 27 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 25A Average Run Number 2-THC-1 2-THC-2 2-THC-3 Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM 5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Fuel Factor 1.32 1.32 1.32 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.0 00 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Analyzer Make VIG VIG VIG Analyzer Model 20 20 20 20.000 Analyzer Serial Number INST-TH0007 INST-TH0007 INST-TH0007 Operating Range 50 50 50 50.000 Operating Units ppm ppm ppm No. Readings/Avg. 240 240 240 240.000 Calibration Set 6 6 6 6.000 Calibration Pre Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Pre Zero Cylinder Instrument Response -0.09 0.09 0.53 0.177 Calibration Pre Zero Cylinder Bias 0 0.36 1.24 0.533 Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID CC115743 CC115743 CC115743 Calibration Pre High Cylinder Instrument Response 14.45 14.45 14.21 14.370 Calibration Pre High Cylinder Bias -0.06 -0.06 -0.54 -0.220 Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Post Zero Cylinder Instrument Response 0.09 0.53 0.41 0.343 Calibration Post Zero Cylinder Bias 0.36 1.24 1 0.867 Calibration Post Zero Cylinder Drift 0.36 0.88 0.24 0.493 Calibration Post High Cylinder ID CC115743 CC115743 CC115743 Calibration Post High Cylinder Instrument Response 14.45 14.21 14.32 14.327 Calibration Post High Cylinder Bias -0.06 -0.54 -0.32 -0.307 Calibration Post High Cylinder Drift 0 0.48 0.22 0.233 Cavg 0.84 0.46 0.72 0.673 Cavg Units ppmvw ppmvw ppmvw Cgas 0.9259 0.1704 0.2886 0.462 Cgas Units ppmvd ppmvd ppmvd Fuel Type Oil Oil Oil Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000 Cgasw 0.8370934256 055360.154065620

5420830.260964117

433853 0.417
Cgasw Units ppmvw ppmvw ppmvw



### Tuesday, February 15, 2011 Page 28 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 3A CO2 Average Run Number 2-CO2-1 2-CO2-2 2-CO2-3 Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM 5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Fuel Factor 1.32 1.32 1.32 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.0 00 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Analyzer Make THERMO THERMO THERMO Analyzer Model 410i 410i 410i Analyzer Serial Number INST-C2-0010 INST-C2- 0010 INST-C2-

0010 Operating Range 19.3 19.3 19.3 19.300 Operating Units % % % No. Readings/Avg. 240 240 240 240.000 Calibration Set 2 2 2 2.000 Calibration Pre Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Pre Zero Cylinder Instrument Response 0.06 0.29 0.16 0.170 Calibration Pre Zero Cylinder Bias 0.26 1.45 0.78 0.830 Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID AAL12025- CO2AAL12025-

CO2 AAL12025-

CO2 Calibration Pre High Cylinder Instrument Response 8.8 8.92 8.85 8.857 Calibration Pre High Cylinder Bias -0.52 0.1 -0.26 -0.227 Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Post Zero Cylinder Instrument Response 0.29 0.16 0.07 0.173 Calibration Post Zero Cylinder Bias 1.45 0.78 0.31 0.847 Calibration Post Zero Cylinder Drift 1.19 0.67 0.47 0.777 Calibration Post High Cylinder ID AAL12025- CO2AAL12025-

CO2 AAL12025-

CO2 Calibration Post High Cylinder Instrument Response 8.92 8.85 8.86 8.877 Calibration Post High Cylinder Bias 0.1 -0.26 -0.21 -0.123 Calibration Post High Cylinder Drift 0.62 0.36 0.05 0.343 Cavg 13.77 13.7 13.59 13.687 Cavg Units %vd %vd %vd Cgas 13.9159 13.8329 13.7063 13.818 Cgas Units %vd %vd %vd Fuel Type Oil Oil Oil Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000 Cgasw 0 0 0 0.000 Cgasw Units %vw %vw %vw



### Tuesday, February 15, 2011 Page 29 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 3A O2 Average Run Number 2-O2-1 2-O2-2 2-O2-3 Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM 5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Fuel Factor 1.32 1.32 1.32 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.0 00 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Analyzer Make THERMO THERMO THERMO Analyzer Model 42i-HL 42i-HL 42i-HL Analyzer Serial Number INST-N2-0002 INST-N2- 0002 INST-N2-

0002 Operating Range 21.1 21.1 21.1 21.100 Operating Units % % % No. Readings/Avg. 240 240 240 240.000 Calibration Set 1 1 1 1.000 Calibration Pre Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Pre Zero Cylinder Instrument Response 0.16 0.24 0.45 0.283 Calibration Pre Zero Cylinder Bias 0.9 1.28 2.27 1.483 Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID AAL12025-O2AAL12025- O2 AAL12025-

O2 Calibration Pre High Cylinder Instrument Response 12 12.04 12.18 12.073 Calibration Pre High Cylinder Bias -0.28 -0.09 0.57 0.067 Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Post Zero Cylinder Instrument Response 0.24 0.45 0.36 0.350 Calibration Post Zero Cylinder Bias 1.28 2.27 1.85 1.800 Calibration Post Zero Cylinder Drift 0.38 0.99 0.42 0.597 Calibration Post High Cylinder ID AAL12025-O2AAL12025- O2 AAL12025-

O2 Calibration Post High Cylinder Instrument Response 12.04 12.18 12.12 12.113 Calibration Post High Cylinder Bias -0.09 0.57 0.28 0.253 Calibration Post High Cylinder Drift 0.19 0.66 0.29 0.380 Cavg 4.25 4.23 4.25 4.243 Cavg Units %vd %vd %vd Cgas 4.1459 3.9956 3.9612 4.034 Cgas Units %vd %vd %vd Fuel Type Oil Oil Oil Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000 Cgasw 0 0 0 0.000 Cgasw Units %vw %vw %vw



### Tuesday, February 15, 2011 Page 30 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 6C Average Run Number 2-SO2-1 2-SO2-2 2-SO2-3 Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM 5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Fuel Factor 1.32 1.32 1.32 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.0 00 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Analyzer Make THERMO THERMO THERMO Analyzer Model 43i-HL 43i-HL 43i-HL Analyzer Serial Number INST-S2-0005 INST-S2- 0005 INST-S2-

0005 Operating Range 959 959 959 959.000 Operating Units ppm ppm ppm No. Readings/Avg. 240 240 240 240.000 Calibration Set 3 3 3 3.000 Calibration Pre Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Pre Zero Cylinder Instrument Response 1.78 3.32 3.56 2.887 Calibration Pre Zero Cylinder Bias 0.16 0.33 0.35 0.280 Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID CC66246 CC66246 CC66246 Calibration Pre High Cylinder Instrument Response 422.1 417 410.32 416.473 Calibration Pre High Cylinder Bias -0.82 -1.36 -2.05 -1.410 Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Post Zero Cylinder Instrument Response 3.32 3.56 2.55 3.143 Calibration Post Zero Cylinder Bias 0.33 0.35 0.25 0.310 Calibration Post Zero Cylinder Drift 0.17 0.02 0.1 0.097 Calibration Post High Cylinder ID CC66246 CC66246 CC66246 Calibration Post High Cylinder Instrument Response 417 410.32 411.11 412.810 Calibration Post High Cylinder Bias -1.36 -2.05 -1.97 -1.793 Calibration Post High Cylinder Drift 0.54 0.697.999999999 99998E-02 0.437
Cavg 242.26 305.64 320.48 289.460 Cavg Units ppmvd ppmvd ppmvd Cgas 246.0333 315.2981 333.2628 298.198 Cgas Units ppmvd ppmvd ppmvd Fuel Type Oil Oil Oil Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000 Cgasw 0 0 0 0.000 Cgasw Units ppmvw ppmvw ppmvw



### Tuesday, February 15, 2011 Page 31 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Gases - Method 7E Average Run Number 2-NOx-1 2-NOx-2 2-NOx-3 Test Date 4/13/2010 4/13/2010 4/13/2010 Run Start Time 3:25:22 PM 5:43:22 PM 7:52:18 PM Run Finish Time 5:24:52 PM7:42:52 PM 9:51:48 PM Carbon Dioxide, % 13.91 13.84 13.71 13.820 Oxygen, % 4.15 4 3.97 4.040 Fuel Factor 1.32 1.32 1.32 Dry Volumetric Flow Rate, dry scfm 1551695 1551695 15516951,551,695.0 00 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Moisture, % 9.59 9.59 9.59 9.590 Analyzer Make THERMO THERMO THERMO Analyzer Model 42i-HL 42i-HL 42i-HL Analyzer Serial Number INST-N2-0002 INST-N2- 0002 INST-N2-

0002 Operating Range 1110 1110 1110 1,110.000 Operating Units ppm ppm ppm No. Readings/Avg. 240 240 240 240.000 Calibration Set 4 4 4 4.000 Calibration Pre Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Pre Zero Cylinder Instrument Response 1.12 1.68 4.97 2.590 Calibration Pre Zero Cylinder Bias 0.02 0.07 0.37 0.153 Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID ALM042523- NOxALM042523

-NOxALM042523-

NOx Calibration Pre High Cylinder Instrument Response 538.2 528.2 521.78 529.393 Calibration Pre High Cylinder Bias -1.33 -2.23 -2.81 -2.123 Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID ALM031337ALM031337ALM031337 Calibration Post Zero Cylinder Instrument Response 1.68 4.97 3.98 3.543 Calibration Post Zero Cylinder Bias 0.07 0.37 0.28 0.240 Calibration Post Zero Cylinder Drift 0.05 0.3 0.09 0.147 Calibration Post High Cylinder ID ALM042523- NOxALM042523

-NOxALM042523-

NOx Calibration Post High Cylinder Instrument Response 528.2 521.78 526.22 525.400 Calibration Post High Cylinder Bias -2.23 -2.81 -2.41 -2.483 Calibration Post High Cylinder Drift 0.9 0.58 0.4 0.627 Cavg 211.37 212.23 213.1 212.233 Cavg Units ppmvd ppmvd ppmvd Cgas 215.9714 219.0506 219.6581 218.227 Cgas Units ppmvd ppmvd ppmvd Fuel Type Oil Oil Oil Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000 Cgasw 0 0 0 0.000 Cgasw Units ppmvw ppmvw ppmvw



### Tuesday, February 15, 2011 Page 32 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - Metals - Method 29 Average Run Number PMR2-29-1 PMR2-29-2 PMR2-29-3 Test Date 4/13/2010 4/13/2010 4/14/2010 Run Start Time 9:20:00 AM 2:10:00 PM11:06:00 AM Run Finish Time 1:20:00 PM 6:10:00 PM 3:06:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 240 240 240 Nozzle Diameter, inches 0.25 0.25 0.25 0.250 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.979 0.979 1.002 0.987 Barometric Pressure, inches of Mercury 29.85 29.91 30 29.920 Average Orifice Meter Differential, inches H2O 1.99 1.53 2.27 1.930 Dry Gas Meter Volume Sampled, cubic feet 188.950 170.460 197.410 185.607 Average Dry Gas Meter Temperature, °F 79.60 82.73 82.73 81.687 Dry Gas Meter Volume Sampled, dscf 181.467 162.907 194.024 179.466 Total Moisture Liquid collected, g 445.2 392.6 449.6 429.133 Volume of Water Vapor, standard cubic feet 20.96 18.48 21.16 20.200 Moisture Content of Stack Gas, % 10.35 10.19 9.83 10.123 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.8965 0.8981 0.9017 0.899 Carbon Dioxide, % 13.82 13.82 13.81 13.817 Oxygen, % 4.04 4.04 4.13 4.070 Carbon Monoxide & Nitrogen, % 82.14 82.14 82.06 82.113 Fuel Factor 1.22 1.22 1.21 Dry Molecular Weight, lb/lb-Mole 30.37 30.37 30.37 30.370 Wet Molecular weight, lb/lb-Mole 29.09 29.11 29.15 29.117 Flue Gas Static Pressure, inches of H2O -1.7 -1.7 -1.7 -1.700 Absolute Flue Gas Pressure, inches of Mercury 29.73 29.79 29.88 29.800 Average Stack Gas Temperature, °F 317.88 324.17 326.92 322.990 Average Velocity Head, inches of H2O 0.8284654510 414280.637761063

4785170.901006123

011436 0.789
Average Stack Gas Velocity, feet/second 61.99 54.53 64.79 60.437 Stack Cross-Sectional Area, square feet 696.685 696.685 696.685 696.685 Dry Volumetric Flow Rate, dry scfm 1,566,802.6 1,372,399.4 1,636,364.71,525,188.9 00 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,591,250.2 2,279,414.0 2,708,293.32,526,319.1 67 Percent Isokinetic of Sampling Rate, % 98.6 101.1 101.0 100.233 Percent Excess Air, % 22.9 22.9 23.6 23.133 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Round Duct Diameter, inches 357.4 357.4 357.4 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 33 of 34

### Martin Energy Center, Unit #2, Information Collection Request
7/29/2010
Location PMR2 - PM - OTM - 27/28 Average Run Number PMR2-27/28-1 PMR2- 27/28-2PMR2-27/28-

3 Test Date 4/12/2010 4/12/2010 4/14/2010 Run Start Time 2:38:00 PM 6:49:00 PM 8:23:00 AM Run Finish Time 5:34:00 PM 9:30:00 PM10:56:00 AM Net Traversing Points 12 12 12 Net Run Time, minutes 129 126 127 Nozzle Diameter, inches 0.172 0.172 0.172 0.172 Pitot Tube Coefficient 0.8 0.8 0.8 0.800 Dry Gas Meter Calibration Factor 1.002 1.002 1.002 1.002 Barometric Pressure, inches of Mercury 29.88 29.83 29.94 29.883 Average Orifice Meter Differential, inches H2O 0.39 0.39 0.39 0.390 Dry Gas Meter Volume Sampled, cubic feet 45.670 43.400 44.190 44.420 Average Dry Gas Meter Temperature, °F 79.79 79.83 75.75 78.457 Dry Gas Meter Volume Sampled, dscf 44.745 42.447 43.709 43.634 Total Moisture Liquid collected, g 100.2 93.8 96.9 96.967 Volume of Water Vapor, standard cubic feet 4.72 4.42 4.56 4.567 Moisture Content of Stack Gas, % 9.54 9.43 9.45 9.473 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9046 0.9057 0.9055 0.905 Carbon Dioxide, % 13.82 13.82 13.89 13.843 Oxygen, % 4.04 4.04 4 4.027 Carbon Monoxide & Nitrogen, % 82.14 82.14 82.11 82.130 Fuel Factor 1.22 1.22 1.22 Dry Molecular Weight, lb/lb-Mole 30.37 30.37 30.38 30.373 Wet Molecular weight, lb/lb-Mole 29.19 29.20 29.21 29.200 Flue Gas Static Pressure, inches of H2O -1.7 -1.7 -1.7 -1.700 Absolute Flue Gas Pressure, inches of Mercury 29.76 29.71 29.82 29.763 Average Stack Gas Temperature, °F 314.58 313.58 324.00 317.387 Average Velocity Head, inches of H2O 0.7050553763 143120.721868404

1953710.779776047

186202 0.736
Average Stack Gas Velocity, feet/second 54.23 54.87 57.30 55.467 Stack Cross-Sectional Area, square feet 696.685 696.685 696.685 696.685 Dry Volumetric Flow Rate, dry scfm 1,390,346.0 1,407,916.1 1,455,776.51,418,012.8 67 Actual Wet Volumetric Flue Gas Flow Rate, acfm 2,266,873.7 2,293,626.4 2,395,203.02,318,567.7 00 Percent Isokinetic of Sampling Rate, % 107.7 103.3 102.1 104.367 Percent Excess Air, % 22.9 22.9 22.6 22.800 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Round Duct Diameter, inches 357.4 357.4 357.4 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 1032010,320.000 Fc 1420 1420 1420 1,420.000



### Tuesday, February 15, 2011 Page 34 of 34