Instructions for filling the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil 

fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently 

supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or 

if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Carbon 

Monoxide, Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi-Volatile Organic 

HAPs, Sulfur Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total Dissolved Solids (TDS), and Total 

Suspended Solids (TSS). You must complete 3 separate sampling events for each of the requested constituents. This 

spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using 

separate copies of this spreadsheet. Fields shaded in yellow are required. All cells that are shaded in light green are 

populated using drop-down lists. You do not need to populate cells shaded in gray, as they are automatically populated 

from the Boiler Information worksheet. Please Do Not modify the structure of this spreadsheet by adding or subtracting 

rows, columns, cells. Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 

2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each 

spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test 

results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent 

family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 and 

Hg+2, or if the Ontario-Hydro Method was used, you would need to enter Hg0, HgP, and Hg+2. However, both the Speciated 

Volatile Organic HAP and Speciated Semi-Volatile Organic HAP worksheets allow you to use a drop-down provided in the 

Constituent field to define as many records as needed to record each HAP that you have results for. General instructions 

follow for these worksheets:

Boiler Operation Information

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units of measure 

(deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field.

2. Please provide the values of all requested parameters for each of the 3 sample testing periods in the Sample 1, Sample 

2, and Sample 3 fields.

3. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop-downs in the Fuel Type Selection field. 

You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 3 fields. 

If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 

2. Please enter the unit of measure using the drop down provided.

3. Please enter the test method used to determine the fuel input rate.

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure, while 

others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million 

BTU) and ppmvd @ 7% O2(parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both.

2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. 

Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010).

3. Please provide any other information that you feel may be important in the Other Supporting Information field.

4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also 

enter these data.
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1
Control Device Configuraton

Listed (by boiler) in Question 16 (page 17) of the questionnaire
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2 Sample 3

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3

Emission Test Results

CO Emission Rate 

Sample 1 

(lb/MMBtu)

CO Emission Rate 

Sample 1 

(ppmvd @ 7% O2)

CO Emission Rate 

Sample 2 

(lb/MMBtu)
Unit of Measure

Other Supporting 

Information

1000 lb/hr

MMBtu/hr

N/A

%

Unit of Measure

Fuel Flow 

Measurement 

Method

Other Supporting 

Information

CO Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

CO Emission Rate 

Sample 3 

(lb/MMBtu)

CO Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used 

(ex. U.S. EPA

Method 10A)

Other Supporting 

Information
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2 Sample 3

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3

Emission Test Results

Formaldehyde 

Emission Rate 

Sample 1 

(lb/MMBtu)

Formaldehyde 

Emission Rate 

Sample 1 

(ppmvd @ 7% O2)

Formaldehyde 

Emission Rate 

Sample 2 

(lb/MMBtu)
Unit of Measure

Other Supporting 

Information

1000 lb/hr

MMBtu/hr

N/A

%

Unit of Measure

Fuel Flow 

Measurement 

Method

Other Supporting 

Information

Formaldehyde 

Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

Formaldehyde 

Emission Rate 

Sample 3 

(lb/MMBtu)

Formaldehyde 

Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA

Method 320)
Other Supporting 

Information
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2

Date of Testing 3/26/2010 3/26/2010

Steam Output (1000 lb/hr) 2061 2009

Total Heat Input (MMBtu/hr) 3765 3630

Basis (Wet/Dry) Wet Wet

Exhaust Steam % Moisture 6.29 4.87

Exhaust Flow Rate (acfm or dscfm) 1,38,596 1,370,578

Exhaust Temperature (deg C or deg F) 223 223

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

bituminous 3765 3630

Emission Test Results

Methane Emission Rate 

Sample 1

 (lb/MMBtu)

Methane Emission Rate 

Sample 1

(ppmvd @ 7% O2)

0.00031 0.472
Sample 3 Unit of Measure

Other Supporting 

Information

3/26/2010

2011 1000 lb/hr

3601 MMBtu/hr

Wet N/A

4.83 %

1,362,005 acfm

223 deg F

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow Measurement 

Method

Other Supporting 

Information

3601 MMBtu/hr F-Factor CEMS Data

Methane Emission Rate 

Sample 2 

(lb/MMBtu)

Methane Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

Methane Emission Rate 

Sample 3 

(lb/MMBtu)

Methane Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

0.0003 0.468 0.0003 0.465
Test Method Used

(ex. U.S. EPA

Method 18)

Other Supporting 

Information

U.S. EPA Method 18 Run 1 BDL, Run 2 BDL, Run 3 BDL
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2 Sample 3

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3

Emission Test Results

SO2 Emission Rate 

Sample 1

 (lb/MMBtu)

SO2 Emission Rate 

Sample 1

(ppmvd @ 7% O2)

SO2 Emission Rate 

Sample 2 

(lb/MMBtu)
Unit of Measure

Other Supporting 

Information

1000 lb/hr

MMBtu/hr

N/A

%

Unit of Measure

Fuel Flow 

Measurement Method

Other Supporting 

Information

SO2 Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

SO2 Emission Rate 

Sample 3 

(lb/MMBtu)

SO2 Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA

Method 6)
Other Supporting 

Information
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 3

Date of Testing 3/23/2010 3/23/2010

Steam Output (1000 lb/hr) 2027.546 2015.931

Total Heat Input (MMBtu/hr) 3606.197 3599.339

Basis (Wet/Dry) Dry Dry

Exhaust Steam % Moisture 5.5 6.5

Exhaust Flow Rate (acfm or dscfm) 867953 843587

Exhaust Temperature (deg C or deg F) 65 58

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

bituminous 3606.197 3599.339

Run 1 Run 3

Emission Test Results

Total Vapor Phase 

Mercury Emission Rate 

Sample 1

 (lb/MMBtu)

Total Vapor Phase 

Mercury Emission Rate 

Sample 2 

(lb/MMBtu)

3.37E-06 3.53E-06

Data Sheets and QA/QC Documentation

trap ID Section 1 

1A AU 007975 256.1

1B AU 007837 548.7

3A AU007999 282.5

3B AU007806 546.5

5A AU007956 242.4

5B AU007984 515.9

Start

1A 3/23/2010 9:00

1B 3/23/2010 9:00

3A 3/23/2010 15:15

3B 3/23/2010 15:15

Summary of Hg Collected on Sorbent Traps via M

Run ID

Appartioned Mass (ng)

Individual Sorbent Tube Emis

Run ID Test Date Run Time
5A 3/24/2010 10:15

5B 3/24/2010 10:15

Averages

Average R Vol. diff (%)

1A

1B 62.412 -1.12%

3A

3B 62.412 0.43%

5A

5B 62.412 0.39%

% Limit

1A 1.171417415

1B 0.546746856

3A 0.991150442

3B 0.512351327

5A 1.031353135

5B 0.387672029

Summary of M30B Quality Assurance Checks

Run ID Volume Sampled (dscm)

Run ID

Sorbent Trap Breakthrough (B)

≤ 10% of Section 1 Hg 

mass for Hg conc. >1 

μg/dscm: or ≤ 20% of 

Section 1 for Hg conc.≤1 

μg/dscm
Sample 5 Unit of Measure

Other Supporting 

Information

3/24/2010

2007.338 1000 lb/hr

3576.488 MMBtu/hr

Dry N/A

6.1 %

852628 dscfm

76 deg F

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow 

Measurement 

Method

Other Supporting 

Information

3576.488 MMBtu/hr F-Factor From CEMS

Run 5

Total Vapor Phase 

Mercury Emission Rate 

Sample 3 

(lb/MMBtu)

Test Method Used

(ex. U.S. EPA Method 

30B)

Other Supporting 

Information

3.21E-06 U.S. EPA Method 30B ADL, Run 1- 3.37E-06, ADL, Run 3- 3.53E-06, ADL, Run 5- 3.21E-06

5 runs were performed but runs 1, 3, and 5 were reported

Total Mass (ng)

Section 2 Sections 1+2 (ng)

3 259.1 0 259.1

3 551.7 302.13 249.57

2.8 285.3 0 285.3

2.8 549.3 302.13 247.17

2.5 244.9 0 244.9

2 518 302.13 215.87

Stop per tube per run per tube

11:00 4.1 4.1

11:00 3.95 3.95

17:19 4.5 4.5

17:19 3.93 3.93

 of Hg Collected on Sorbent Traps via Method 30B

Initial Spike (ng) Total Non-spike

Individual Sorbent Tube Emission Summary, Method 30B

Run Time Hg Emissions(lb/Tbtu) Hg Emissions (lb/hr)
12:15 3.96 3.96

12:15 3.51 3.51

3.991666667

Limit Abs. diff. % Limit

Crec R (%) by Run R (%) by program Limit

1.863354037 ≥10 % RD mass for 

Hg conc. >1 

μg/dscm: or ≤20% 

RD or ≤0.2 μg/dscm 

abs.diff. for Hg conc. 

≤1 μg/dscm

0.57 6.761565836

91.94

Average Recovery, 

between 85 and 

115% 4.22 88.01

 M30B Quality Assurance Checks

Paired Trap Agreement (RD)

≤20% of field recovery

test

0.15

4.46 90.84

0.45 6.024096386

Measured Spike Recovery ( R )

4.63 96.97
un 3- 3.53E-06, ADL, Run 5- 3.21E-06

 1, 3, and 5 were reported

(ug)

0.2591

0.24957

0.2853

0.24717

0.2449

0.21587

per run per tube per run

Hg Emissions (lb/yr)*

Total Non-spike

Hg Emissions (lb/hr)
#DIV/0! #DIV/0!

62.921

62.145

62.17 Spiked

62.4120 Average R

63.109

62.28

62.352

62.5803 Non Spiked



EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Emission Test Results Mercury Species

Mercury Emission Rate 

Sample 1

 (lb/MMBtu)

Hg0

Hg+2

HgP
Sample 3 Unit of Measure

Other Supporting 

Information

1000 lb/hr

MMBtu/hr

N/A

%

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow 

Measurement 

Method

Other Supporting 

Information

Mercury Emission Rate 

Sample 2 

(lb/MMBtu)

Mercury Emission Rate 

Sample 3 

(lb/MMBtu)

Test Method Used

(ex. ASTM Method 

D6784)

Other Supporting 

Information
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 3/26/2010 3/26/2010 3/26/2010

Steam Output (1000 lb/hr) 2060 2008 2011 1000 lb/hr

Total Heat Input (MMBtu/hr) 3765 3629 3601 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 6.34 4.91 4.86 %

Exhaust Flow Rate (acfm or dscfm) 1372494 1374789 1372135 acfm

Exhaust Temperature (deg C or deg F) 342 343 343 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow 

Measurement 

Method

Other Supporting 

Information

bituminous 3765 3629 3601 MMBtu/hr F-Factor From CEMS

Compound 

(use drop down to define for as many 

rows as needed)

Volatile Organic HAP 

Emission Rate Sample 

1 

(lb/MMBtu)

Volatile Organic HAP 

Emission Rate Sample 

1 

(ug/dscm @ 7% O2)

Volatile Organic 

HAP Emission Rate 

Sample 2 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 2

(ug/dscm @ 7%

O2)

Volatile Organic 

HAP Emission 

Rate Sample 3 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 3

(ug/dscm @ 7%

O2) Test Method Used Other Supporting Information

Dichlorodifluoromethane 1.295E-06 1.434 1.041E-06 1.167 1.524E-06 1.703 U.S. EPA Method 0031 with SWDDL Run 1,25.4,49.01,20.38,24.82,[<3] DLL Run 2, 32.4,13.65,13.14,37.91,[<3] DLL Run 3 39.48,14.82,22.43,68.46,[<3] -846 Method 8260B

1,2-Chloro-1,1,2,2-Tetrafluoroethane 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Chloromethane 5.521E-05 42.453 1.152E-04 90.326 1.913E-03 1504.640 U.S. EPA Method 0031 with SWDLL Run 1, 2864.34,1287.34,604.98,467.66,[<3] DLL Run 2, 7795.47,1241.92,921.82,1120.96,[<3] DLL Run 3 105178.6,78009.23,1553.02,1260.92,[<3] -846 Method 8260B

Vinyl chloride 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,3-Butadiene 3.099E-07 0.238 5.773E-07 0.452 1.804E-05 14.193 U.S. EPA Method 0031 with SWDLL Run 1, 12.62,9.56,1.16,[<3],[<3] Run 2, 24.78,[<3],15.09,9.65,[<3] DLL Run 3 202.33,1516.55,15.72,16.96,[<3] -846 Method 8260B

Bromomethane 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Chloroethane 3.660E-07 0.281 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],22.65,[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Trichloromonofluoromethane 1.615E-06 1.242 2.173E-06 1.703 6.522E-07 0.513 U.S. EPA Method 0031 with SWDLL Run 1, 19.44,73.81,18.21,38.47,[<3] DLL Run 2, 116.19,17.04,9.19,63.58,[<3] DLL Run 3 23.19,4.61,23.52,9.1,[<3] -846 Method 8260B

1,1-Dichloroethane 1.271E-06 0.978 4.375E-06 3.429 1.595E-06 1.254 U.S. EPA Method 0031 with SWDLL Run 1, 7.9,14.43,27.65,67.39,[<3] DLL Run 2, 91.7,97.95,75.79,152.33,[<3] DLL Run 3 71.24,3.89,14.42,62.53,[<3] -846 Method 8260B

1-1,2-trichloro-1,2,2-trifluoroethane 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Ethanol 2.273E-05 17.475 4.420E-05 34.641 1.832E-05 14.414 U.S. EPA Method 0031 with SWADL Run 1, 354.4, 640.48, 570.57, 584.24, 2.08 ADL Run 2, 2161.2,491.41,504.77,1089.47, 4.68 ADL Run 3 508.87,412.22,535.45,322.65,2.68 -846 Method 8260B

Carbon disulfide 1.489E-05 11.447 3.991E-05 31.286 8.095E-06 6.367 U.S. EPA Method 0031 with SWADL Run 1 152.53, 603.29, 235.67, 414.87, 3.18 DLL Run 2, 2757.91,[<3],126.95,943.81,7.13 ADL Run 3 310.06,41.26,352.09,80.35,3.37 -846 Method 8260B

Isopropyl alcohol 1.465E-07 0.113 1.783E-06 1.398 2.062E-07 0.162 U.S. EPA Method 0031 with SWDLL Run 1, [<3],[<3],[<3],[<3],1.87 BDL Run 2, [<3],156.18,[<3],[<3],6.3 DLL Run 3, [<3],[<3],[<3],[<3],8.05 -846 Method 8260B

Methylene chloride 1.855E-04 142.593 2.396E-04 187.805 8.356E-05 65.729 U.S. EPA Method 0031 with SWADL Run 1 2525.04,8697.07,3538.05,2794.64,3.04 ADL Run 2 12120.39,1700.84,872.76,8323.5,26.48 ADL Run 3 3083.24,990.17,3085.42,931.99,34.65 -846 Method 8260B

Acetone 1.867E-04 143.559 1.850E-04 145.017 1.195E-04 93.976 U.S. EPA Method 0031 with SWADL Run 1 3522.58,6596.2,4526.24,3017.65,14.22 ADL Run 2 6574.33,1817.87,3143.67,6209.02,48.98 ADL Run 3 3793.2,3363.9,2997.86,1411.91,50.52 -846 Method 8260B

trans-1,2-Dichloroethene 1.603E-07 0.123 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWDLL Run 1 [<3],3.18,[<3], [<3],[<3]BDL Run 2 [<3],[<3],[<3],[<3][<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Hexane 1.584E-07 0.122 3.871E-06 3.034 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2 282.69,80.6,[<3],[<3],[<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Methyl-t-butyl either (MTBE) 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,1-Dichloroethene 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Vinyl acetate 1.182E-05 9.086 2.493E-06 1.954 1.095E-05 8.616 U.S. EPA Method 0031 with SWDLL Run 1, 369.55,52.54,680.35,13.37,[<3] ADL Run 2 70.64,30.26,79.86,56.0,[<3] DLL Run 3 94.2,413.14,545.36,9.4,[<3] -846 Method 8260B

cis-1,2-dichloroethene 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Cyclohexane 1.953E-07 0.150 5.814E-07 0.456 2.306E-07 0.181 U.S. EPA Method 0031 with SWDLL Run 1 [<3],6.49,[<3], [<3] ,[<3] DLL Run 235.92,[<3],4.44,9.56,[<3] DLL Run 3 [<3],6.57,6.85,[<3],[<3] -846 Method 8260B

Chloroform 1.135E-07 0.087 3.921E-07 0.307 1.276E-07 0.100 U.S. EPA Method 0031 with SWDLL Run 1 1.74,2.53,1.77,1.71,[<3] DLL Run 2 27.29,2.08,1.52,3.82,[<3] DLL Run 3 2.15,1.7,2.56,[<3],[<3] -846 Method 8260B

Ethyl acetate 3.575E-06 2.749 6.130E-06 4.805 2.285E-06 1.797 U.S. EPA Method 0031 with SWDLL Run 1 82.19,74.74,59.17,119.35,[<3] DLL Run 2 236.17,143.07,96.46,110.86,[<3] DLL Run 3 79.25,16.95,69.69,53.26,[<3] -846 Method 8260B

Teteahydrofuran 9.597E-07 0.738 1.583E-06 1.240 1.080E-06 0.849 U.S. EPA Method 0031 with SWDLL Run 1 23.68,18.43,22.74,23.03,[<3], Run 2 78.41,14.65,30.94,25.21,[<3] DLL Run 3 36.62,21.25,26.17,17.94,[<3] -846 Method 8260B

1,1,1-Trichloroethane 1.584E-07 0.122 2.556E-07 0.200 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1 [<3],[<3],[<3],[<3][<3] DLL Run 2 12.58,[<3],[<3],[<3],[<3], BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Carbon tetrachloride 1.797E-07 0.138 1.928E-07 0.151 1.445E-07 0.114 U.S. EPA Method 0031 with SWDLL Run 1 5.47,2.8,2.55,3.19,[<3] DLL Run 2 5.87,[<3],2.85,3.82,[<3] DLL Run 3 3.42,[<3],2.67,1.96,[<3] -846 Method 8260B

2-Butanone (MEK) 6.211E-06 4.776 1.085E-05 8.506 5.699E-06 4.483 U.S. EPA Method 0031 with SWDLL Run 1 148.98,138.77,[<3],294.3,[<3] DLL Run 2 472.39,382.83,182.45,[<3],[<3] DLL Run 3 202.42,137.99,126.41,83.97,[<3] -846 Method 8260B

Heptane 1.584E-07 0.122 1.560E-07 0.122 5.024E-07 0.395 U.S. EPA Method 0031 with SWBDL Run 1 [<3],[<3],[<3],[<3],[<3] BDL Run 2 [<3],[<3],[<3],[<3],[<3] DLL Run 3 [<3],36.85,[<3],[<3],[<3] -846 Method 8260B

Benzene 8.951E-06 6.882 1.110E-05 8.700 1.755E-05 13.803 U.S. EPA Method 0031 with SWDLL Run 1 165.13,123.22,391.62,164.44,[<3] DLL Run 2 391.33,140.57,390.27,142.31,[<3] DLL Run 3 240.37,1028.9,318.57,115.44,[<3] -846 Method 8260B

1,2-Dichloroethane 1.651E-06 1.269 2.182E-06 1.711 3.946E-06 3.104 U.S. EPA Method 0031 with SWDLL Run 1 [<3],[<3],6.72,140.58,[<3] DLL Run 2 17.55,43.41,128.19,17.74,[<3] DLL Run 3 [<3],[<3],132.0,242.75,[<3] -846 Method 8260B

Tetrachloroethylene 1.420E-07 0.109 1.759E-07 0.138 1.350E-07 0.106 U.S. EPA Method 0031 with SWDLL Run 1 1.44,[<3],[<3],[<3],[<3] DLL Run 2 [<3],[<3],4.92,[<3],[<3] DLL Run 3 1.13,[<3],[<3],[<3],[<3] -846 Method 8260B

1,2-Dichloropropane 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Bromodichloromethane 1.745E-07 0.134 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWDLL Run 1 [<3],[<3],4.52,[<3],[<3] BDL Run 2 [<3],[<3],[<3],[<3],[<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,4-Dioxane 1.366E-04 105.007 1.366E-04 107.084 1.216E-04 95.669 U.S. EPA Method 0031 with SWDLL Run 1 2841.41,2551.49,3822.14,3711.71,[<3] DLL Run 2 4381.59,2756.56,3104.15,2894.16,[<3] DLL 4217.52,1020.63,3856.55,2729.02,[<3] -846 Method 8260B

cis-1,3-Dichloropropene 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Toluene 3.798E-06 2.920 1.233E-05 9.663 1.769E-06 1.392 U.S. EPA Method 0031 with SWDLL Run 1 25.17,39.41,44.54,247.44,[<3] DLL Run 2 540.37,316.17,43.62,282.45,[<3] DLL Run 3 51.93,57.75,42.8,16.55,[<3] -846 Method 8260B

4-Methyl-2-pentanone (MIBK) 7.996E-07 0.615 2.156E-06 1.690 5.145E-07 0.405 U.S. EPA Method 0031 with SWDLL Run 1 40.98,18.65,10.07,[<3],[<3] DLL Run 2 145.47,43.38,12.54,[<3],[<3] DLL Run 3 23.62,[<3],17.41,[<3],[<3] -846 Method 8260B

1-1,3-dichloropropene 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Tetrachloroethylene 1.584E-07 0.122 1.855E-07 0.145 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1 [<3],[<3],[<3],[<3],[<3] DLL Run 2 6.07,2.77,[<3],[<3],[<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,1,2-Trichloroethane 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Dibromochloromethane 1.584E-07 0.122 1.570E-07 0.123 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1 [<3],[<3],[<3],[<3],[<3] DLL Run 2 [<3],2.25,[<3],3.85,[<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,2-Dichloroethane 2.418E-07 0.186 1.967E-07 0.154 1.574E-07 0.124 U.S. EPA Method 0031 with SWDLL Run 1 [<3],[<3],[<3],10.89,[<3] DLL Run 2 [<3],[<3],6.92,[<3],[<3] DLL Run 3 [<3],[<3],[<3],3.31,[<3] -846 Method 8260B

2-Hexanone 7.517E-06 5.780 5.735E-06 4.495 2.446E-06 1.924 U.S. EPA Method 0031 with SWDLL Run 1 189.19,60.09,210.97,248.42,[<3] DLL Run 2 202.81,200.96,88.6,56.16,[<3] DLL Run 3 69.32,66.12,56.29,43.13,[<3] -846 Method 8260B

Ethylbenzene 8.762E-07 0.674 1.804E-06 1.414 3.801E-07 0.299 U.S. EPA Method 0031 with SWDLL Run 1 10.71,16.75,14.8,37.7,[<3] DLL Run 2 81.95,41.91,13.03,33.59,[<3] DLL Run 3 12.55,1.32,13.26,6.83,[<3] -846 Method 8260B

Chlorobenzene 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

m/p-Xylene 1.584E-07 0.122 4.727E-07 0.370 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1 [<3],[<3],[<3],[<3],[<3] DLL Run 2 33.46,[<3],[<3],[<3],[<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

o-Xylene 6.807E-07 0.523 1.928E-06 1.511 3.712E-07 0.292 U.S. EPA Method 0031 with SWDLL Run 1 6.2,11.9,8.8,34.55,[<3] DLL Run 2 100.1,41.42,8.28,32.6,[<3] DLL Run 3 8.04,13.74,7.84,3.48,[<3] -846 Method 8260B

Styrene 1.593E-07 0.122 3.714E-07 0.291 1.726E-06 1.358 U.S. EPA Method 0031 with SWDLL Run 1 [<3],[<3],[<3],3.08,[<3] DLL Run 2 23.51,1.46,21.9,5.85,[<3] DLL Run 3 8.01,130.99,20.67,5.19,[<3] -846 Method 8260B

Tribromomethane 1.584E-07 0.122 1.691E-07 0.133 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,1,2,2-Tetrachloroethane 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1-ethyl-4-methybenzene 1.584E-07 0.122 7.179E-07 0.563 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1 [<3],[<3],[<3],[<3],[<3] DLL Run 2 43.06,16.98,[<3],[<3],[<3] BDL Run 3 [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,3,5-trimethylbenzene 3.139E-07 0.241 5.974E-07 0.468 2.335E-07 0.184 U.S. EPA Method 0031 with SWDLL Run 1 3.71,3.43,4.51,15.07,[<3] DLL Run 2 26.26,11.26,5.75,11.19,[<3] DLL Run 3 5.99,4.86,5.35,3.51,[<3] -846 Method 8260B

1,2,4-trimethlbenzene 4.621E-07 0.355 1.309E-06 1.026 1.502E-07 0.118 U.S. EPA Method 0031 with SWDLL Run 1 2.82,3.19,3.4,31.34,[<3] DLL Run 2 68.58,26.79,3.56,23.96,[<3] DLL Run 3 3.62,2.65,3.47,1.87,[<3] -846 Method 8260B

1,3-Dichlorobenzene 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,4-Difluorobenzene (IS) 1.584E-07 0.122 1.560E-07 0.122 1.543E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

Benzyl chloride 2.919E-06 2.244 3.777E-06 2.960 1.531E-05 12.041 U.S. EPA Method 0031 with SWDLL Run 1 62.43,40.87,167.05,[<3],[<3] DLL Run 2 96.25,[<3],258.0,[<3],[<3] DLL Run 3 71.76,1222.28,151.18,40.34,[<3] -846 Method 8260B

1,2-Dichlorobenzene 1.584E-07 0.122 1.560E-07 0.122 1.557E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,1,2,3,4-hexachloro-1,3-butadiene 1.584E-07 0.122 1.560E-07 0.122 1.557E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B

1,2,4-Trichlorobenzene 1.584E-07 0.122 1.560E-07 0.122 1.557E-07 0.121 U.S. EPA Method 0031 with SWBDL Run 1, [<3],[<3],[<3],[<3],[<3] BDL Run 2, [<3],[<3],[<3],[<3],[<3] BDL Run 3, [<3],[<3],[<3],[<3],[<3] -846 Method 8260B
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2

Date of Testing 3/26/2010 3/26/2010

Steam Output (1000 lb/hr) 2060 2008

Total Heat Input (MMBtu/hr) 3765 3629

Basis (Wet/Dry) Dry Dry

Exhaust Steam % Moisture 6.34 4.91

Exhaust Flow Rate (acfm or dscfm) 1372494 1374789

Exhaust Temperature (deg C or deg F) 342 343

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

bituminous 3765 3629

Compound 

(use drop down to define for as 

many rows as needed)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 1 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 1 

(ug/dscm @ 7% O2)

Naphthalene 5.474E-09 0.0042

2-Methylnaphthalene 1.446E-09 0.0011

Acenaphthylene 1.446E-09 0.0011

Acenaphthylene (CCC) 1.446E-09 0.0011

Fluorene 1.446E-09 0.0011

Phenanthrene 1.446E-09 0.0011

Anthracene 1.446E-09 0.0011

Fluoranthene 1.446E-09 0.0011

Pyrene 1.446E-09 0.0011

Benz(a)anthracene 1.446E-09 0.0011

Chrysene 1.446E-09 0.0011

Benzo(b)fluoranthene 1.446E-09 0.0011

Benzo(k)fluoranthene 1.446E-09 0.0011

Benzo(e)pyrene 1.446E-09 0.0011

Benzo(a)pyrene CCC 1.446E-09 0.0011

Perylene 1.446E-09 0.0011

Indeno(1,2,3-cd)pyrene 1.446E-09 0.0011

Dibenz(a,h)anthracene 1.446E-09 0.0011

Benzo(g,h,i)perylene 1.446E-09 0.0011

N-Nitrosodimethylamine 1.116E-07 0.1238

Phenol 1.427E-07 0.1099

Aniline 1.003E-07 0.0772

Bis(2-chloroisopropyl) ether 1.139E-07 0.0877

2-Chlorophenol 9.021E-08 0.0694

1,3-Dichlorobenzene 8.067E-08 0.0621
1,4-Dichlorobenzene 7.633E-08 0.0588

Benzyl alcohol 1.012E-07 0.0779

1,2-Dichlorobenzene 8.067E-08 0.0621

2-Methylphenol 9.801E-08 0.0755

3/4-Methylphenol 8.529E-08 0.0657

N-Nitrosodi-n-propylamine 1.203E-07 0.0926

Hexachloroethane 9.136E-08 0.0703

Nitrobenzene 1.180E-07 0.0908

Isophorone 1.081E-07 0.0832

2,4-Dimethylphenol 1.052E-07 0.0810

2-Nitrophenol 9.686E-08 0.0746

Bis(2-chloroethoxy)methane 1.058E-07 0.0815

2,4-Dichlorophenol 9.425E-08 0.0726

1,2,4-Trichlorobenzene 8.934E-08 0.0688

4-Chloroaniline 1.226E-07 0.0944

Hexachlorobutadiene 8.818E-08 0.0679

4-Chloro-3-methylphenol 9.570E-08 0.0737

1-Methylnaphthalene 8.876E-08 0.0683

Hexachlorocyclopentadiene 1.174E-06 0.9037

2,4,6-Trichlorophenol 1.067E-07 0.0821

2,4,5-Trichlorophenol 7.806E-08 0.0601

2-Chloronaphthalene 9.425E-08 0.0726

1,4-Dinitrobenzene 9.715E-08 0.0748

Dimethyl phthalate 1.171E-07 0.0901

1,3-Dinitrobenzene 1.183E-07 0.0910

2,6-Dinitrotoluene 1.122E-07 0.0864

1,2-Dinitrobenzene 1.125E-07 0.0866

2,4-Dinitrophenol 7.315E-07 0.5631

4-Nitrophenol 8.356E-07 0.6433

2,4-Dinitrotoluene 1.162E-07 0.0895

Dibenzofuran 9.946E-08 0.0766

2,3,5,6-Tetrachlorophenol 1.099E-07 0.0846

2,3,4,6-Tetrachlorophenol 1.012E-07 0.0779

Diethyl phthalate 1.475E-07 0.1135

4-Chlorophenyl phenyl ether 1.090E-07 0.0839

4,6-Dinitro-2-methylphenol 7.459E-07 0.5743

N-Nitrosodiphenylamine 1.035E-07 0.0797

Azobenzene 1.434E-07 0.1104

4-Bromophenyl phenyl ether 9.686E-08 0.0746

Hexachlorobenzene 7.893E-08 0.0608

Pentachlorophenol 8.182E-08 0.0630

Carbazole 1.021E-07 0.0786

Di-n-butyl phthalate 1.501E-07 0.1155

Benzidine 3.296E-06 2.5374

Butyl benzyl phthalate 1.171E-07 0.0901

3,3'-Dimethoxybenzidine 1.558E-06 1.1997

Bis(2-ethylhexyl) phthalate 1.073E-07 0.0826

3,3'-Dichlorobenzidine 1.353E-06 1.0417

Di-n-octyl phthalate 9.310E-08 0.0717




Sample 3 Unit of Measure

Other Supporting 

Information

3/26/2010

2011 1000 lb/hr

3601 MMBtu/hr

Dry N/A

4.86 %

1372135 acfm

343 deg F

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow Measurement 

Method

3601 MMBtu/hr F-Factor

Semi-Volatile Organic HAP 

Emission Rate 

Sample 2 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 2 

(ug/dscm @ 7% O2)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 3 

(lb/MMBtu)

5.202E-09 0.0041 4.693E-09

1.418E-09 0.0011 1.454E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.426E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.418E-09 0.0011 1.413E-09

1.095E-07 0.1230 1.091E-07

1.407E-07 0.1104 1.342E-07

9.841E-08 0.0772 9.806E-08

1.117E-07 0.0877 1.113E-07

8.849E-08 0.0694 8.817E-08

7.913E-08 0.0621 7.885E-08
7.487E-08 0.0588 7.461E-08

9.927E-08 0.0779 9.891E-08

7.913E-08 0.0621 7.885E-08

9.615E-08 0.0755 9.580E-08

8.367E-08 0.0657 8.337E-08

1.180E-07 0.0926 1.176E-07

8.962E-08 0.0703 8.930E-08

1.157E-07 0.0908 1.153E-07

1.061E-07 0.0832 1.057E-07

1.032E-07 0.0810 1.029E-07

9.501E-08 0.0746 9.467E-08

1.038E-07 0.0815 1.034E-07

9.246E-08 0.0726 9.213E-08

8.764E-08 0.0688 8.733E-08

1.203E-07 0.0944 1.198E-07

8.650E-08 0.0679 8.619E-08

9.388E-08 0.0737 9.354E-08

8.707E-08 0.0683 8.676E-08

1.151E-06 0.9037 1.147E-06

1.047E-07 0.0821 1.043E-07

7.658E-08 0.0601 7.630E-08

9.246E-08 0.0726 9.213E-08

9.529E-08 0.0748 9.496E-08

1.149E-07 0.0901 1.145E-07

1.160E-07 0.0910 1.156E-07

1.100E-07 0.0864 1.097E-07

1.103E-07 0.0866 1.099E-07

7.175E-07 0.5631 7.150E-07

8.196E-07 0.6433 8.167E-07

1.140E-07 0.0895 1.136E-07

9.756E-08 0.0766 9.722E-08

1.078E-07 0.0846 1.074E-07

9.927E-08 0.0779 9.891E-08

1.446E-07 0.1135 1.441E-07

1.069E-07 0.0839 1.065E-07

7.317E-07 0.5743 7.291E-07

1.015E-07 0.0797 1.012E-07

1.407E-07 0.1104 1.402E-07

9.501E-08 0.0746 9.467E-08

7.743E-08 0.0608 7.715E-08

8.026E-08 0.0630 7.998E-08

1.001E-07 0.0786 9.976E-08

1.472E-07 0.1155 1.467E-07

3.233E-06 2.5374 3.222E-06

1.149E-07 0.0901 1.145E-07

1.529E-06 1.1997 1.523E-06

2.573E-07 0.2020 1.048E-07

1.327E-06 1.0417 1.323E-06

9.132E-08 0.0717 9.100E-08




Other Supporting Information

Plant Data

Semi-Volatile Organic HAP 

Emission Rate 

Sample 3 

(ug/dscm @ 7% O2) Test Method Used

0.0037 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0011 U.S. EPA Method 0010 with SW-846 Method 8270D

0.1222 U.S. EPA Method 0010 with SW-846 Method 8270D

0.1057 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0772 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0877 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0694 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0621 U.S. EPA Method 0010 with SW-846 Method 8270D
0.0588 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0779 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0621 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0755 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0657 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0926 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0703 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0908 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0832 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0810 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0746 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0815 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0726 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0688 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0944 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0679 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0737 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0683 U.S. EPA Method 0010 with SW-846 Method 8270D

0.9037 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0821 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0601 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0726 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0748 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0901 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0910 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0864 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0866 U.S. EPA Method 0010 with SW-846 Method 8270D

0.5631 U.S. EPA Method 0010 with SW-846 Method 8270D

0.6433 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0895 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0766 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0846 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0779 U.S. EPA Method 0010 with SW-846 Method 8270D

0.1135 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0839 U.S. EPA Method 0010 with SW-846 Method 8270D

0.5743 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0797 U.S. EPA Method 0010 with SW-846 Method 8270D

0.1104 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0746 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0608 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0630 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0786 U.S. EPA Method 0010 with SW-846 Method 8270D

0.1155 U.S. EPA Method 0010 with SW-846 Method 8270D

2.5374 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0901 U.S. EPA Method 0010 with SW-846 Method 8270D

1.1997 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0826 U.S. EPA Method 0010 with SW-846 Method 8270D

1.0417 U.S. EPA Method 0010 with SW-846 Method 8270D

0.0717 U.S. EPA Method 0010 with SW-846 Method 8270D




Other Supporting Information

DLL Run 1, FH 1.55,BH .937,Cond [.050] DLL Run 2, FH .079,BH .995,Cond [.050] DLL Run 3, FH .082,BH .94,Cond [.050]

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] DLL Run 3, FH [.050],BH .054,Cond [.

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] DLL Run 3, FH [.050],BH .051,Cond [.

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [.050],BH [.050],Cond [.050] BDL Run 2, FH [.050],BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond 

BDL Run 1, FH [3.86],BH [3.86],Cond [3.86] BDL Run 2, FH [3.86],BH [3.86],Cond [3.86] BDL Run 3, FH [3.86],BH [3.86],Cond 

DLL Run 1, FH [3.25],BH 8.31,Cond [3.25] DLL Run 2, FH [3.25],BH 8.38,Cond [3.25] DLL Run 3, FH [3.25],BH 7.75,Cond [3.25

BDL Run 1, FH [3.47],BH [3.47],Cond [3.47] BDL Run 2, FH [3.47],BH [3.47],Cond [3.47] BDL Run 3, FH [3.47],BH [3.47],Cond 

BDL Run 1, FH [3.94],BH [3.94],Cond [3.94] BDL Run 2, FH [3.94],BH [3.94],Cond [3.94] BDL Run 3, FH [3.94],BH [3.94],Cond 

BDL Run 1, FH [3.12],BH [3.12],Cond [3.12] BDL Run 2, FH [3.12],BH [3.12],Cond [3.12] BDL Run 3, FH [3.12],BH [3.12],Cond 

BDL Run 1, FH [2.79],BH [2.79],Cond [2.79] BDL Run 2, FH [2.79],BH [2.79],Cond [2.79] BDL Run 3, FH [2.79],BH [2.79],Cond 
BDL Run 1, FH [2.64],BH [2.64],Cond [2.64] BDL Run 2, FH [2.64],BH [2.64],Cond [2.64] BDL Run 3, FH [2.64],BH [2.64],Cond 

BDL Run 1, FH [3.50],BH [3.50],Cond [3.50] BDL Run 2, FH [3.50],BH [3.50],Cond [3.50] BDL Run 3, FH [3.50],BH [3.50],Cond 

BDL Run 1, FH [2.79],BH [2.79],Cond [2.79] BDL Run 2, FH [2.79],BH [2.79],Cond [2.79] BDL Run 3, FH [2.79],BH [2.79],Cond 

BDL Run 1, FH [3.39],BH [3.39],Cond [3.39] BDL Run 2, FH [3.39],BH [3.39],Cond [3.39] BDL Run 3, FH [3.39],BH [3.39],Cond 

BDL Run 1, FH [2.95],BH [2.95],Cond [2.95] BDL Run 2, FH [2.95],BH [2.95],Cond [2.95] BDL Run 3, FH [2.95],BH [2.95],Cond 

BDL Run 1, FH [4.16],BH [4.16],Cond [4.16] BDL Run 2, FH [4.16],BH [4.16],Cond [4.16] BDL Run 3, FH [4.16],BH [4.16],Cond 

BDL Run 1, FH [3.16],BH [3.16],Cond [3.16] BDL Run 2, FH [3.16],BH [3.16],Cond [3.16] BDL Run 3, FH [3.16],BH [3.16],Cond 

BDL Run 1, FH [4.08],BH [4.08],Cond [4.08] BDL Run 2, FH [4.08],BH [4.08],Cond [4.08] BDL Run 3, FH [4.08],BH [4.08],Cond 

BDL Run 1, FH [3.74],BH [3.74],Cond [3.74] BDL Run 2, FH [3.74],BH [3.74],Cond [3.74] BDL Run 3, FH [3.74],BH [3.74],Cond 

BDL Run 1, FH [3.64],BH [3.64],Cond [3.64] BDL Run 2, FH [3.64],BH [3.64],Cond [3.64] BDL Run 3, FH [3.64],BH [3.64],Cond 

BDL Run 1, FH [3.35],BH [3.35],Cond [3.35] BDL Run 2, FH [3.35],BH [3.35],Cond [3.35] BDL Run 3, FH [3.35],BH [3.35],Cond 

BDL Run 1, FH [3.66],BH [3.66],Cond [3.66] BDL Run 2, FH [3.66],BH [3.66],Cond [3.66] BDL Run 3, FH [3.66],BH [3.66],Cond 

BDL Run 1, FH [3.26],BH [3.26],Cond [3.26] BDL Run 2, FH [3.26],BH [3.26],Cond [3.26] BDL Run 3, FH [3.26],BH [3.26],Cond 

BDL Run 1, FH [3.09],BH [3.09],Cond [3.09] BDL Run 2, FH [3.09],BH [3.09],Cond [3.09] BDL Run 3, FH [3.09],BH [3.09],Cond 

BDL Run 1, FH [4.24],BH [4.24],Cond [4.24] BDL Run 2, FH [4.24],BH [4.24],Cond [4.24] BDL Run 3, FH [4.24],BH [4.24],Cond 

BDL Run 1, FH [3.05],BH [3.05],Cond [3.05] BDL Run 2, FH [3.05],BH [3.05],Cond [3.05] BDL Run 3, FH [3.05],BH [3.05],Cond 

BDL Run 1, FH [3.31],BH [3.31],Cond [3.31] BDL Run 2, FH [3.31],BH [3.31],Cond [3.31] BDL Run 3, FH [3.31],BH [3.31],Cond 

BDL Run 1, FH [3.07],BH [3.07],Cond [3.07] BDL Run 2, FH [3.07],BH [3.07],Cond [3.07] BDL Run 3, FH [3.07],BH [3.07],Cond 

BDL Run 1, FH [40.60],BH [40.60],Cond [40.60] BDL Run 2, FH [40.60],BH [40.60],Cond [40.60] BDL Run 3, FH [40.60],BH [4

BDL Run 1, FH [3.69],BH [3.69],Cond [3.69] BDL Run 2, FH [3.69],BH [3.69],Cond [3.69] BDL Run 3, FH [3.69],BH [3.69],Cond 

BDL Run 1, FH [2.70],BH [2.70],Cond [2.70] BDL Run 2, FH [2.70],BH [2.70],Cond [2.70] BDL Run 3, FH [2.70],BH [2.70],Cond 

BDL Run 1, FH [3.26],BH [3.26],Cond [3.26] BDL Run 2, FH [3.26],BH [3.26],Cond [3.26] BDL Run 3, FH [3.26],BH [3.26],Cond 

BDL Run 1, FH [3.36],BH [3.36],Cond [3.36] BDL Run 2, FH [3.36],BH [3.36],Cond [3.36] BDL Run 3, FH [3.36],BH [3.36],Cond 

BDL Run 1, FH [4.05],BH [4.05],Cond [4.05] BDL Run 2, FH [4.05],BH [4.05],Cond [4.05] BDL Run 3, FH [4.05],BH [4.05],Cond 

BDL Run 1, FH [4.09],BH [4.09],Cond [4.09] BDL Run 2, FH [4.09],BH [4.09],Cond [4.09] BDL Run 3, FH [4.09],BH [4.09],Cond 

BDL Run 1, FH [3.88],BH [3.88],Cond [3.88] BDL Run 2, FH [3.88],BH [3.88],Cond [3.88] BDL Run 3, FH [3.88],BH [3.88],Cond 

BDL Run 1, FH [3.89],BH [3.89],Cond [3.89] BDL Run 2, FH [3.89],BH [3.89],Cond [3.89] BDL Run 3, FH [3.89],BH [3.89],Cond 

BDL Run 1, FH [25.30],BH [25.30],Cond [25.30] BDL Run 2, FH [25.30],BH [25.30],Cond [25.30] BDL Run 3, FH [25.30],BH [25

BDL Run 1, FH [28.90],BH [28.90],Cond [28.90] BDL Run 2, FH [28.90],BH [28.90],Cond [28.90] BDL Run 3, FH [28.90],BH [28

BDL Run 1, FH [4.02],BH [4.02],Cond [4.02] BDL Run 2, FH [4.02],BH [4.02],Cond [4.02] BDL Run 3, FH [4.02],BH [4.02],Cond 

BDL Run 1, FH [3.44],BH [3.44],Cond [3.44] BDL Run 2, FH [3.44],BH [3.44],Cond [3.44] BDL Run 3, FH [3.44],BH [3.44],Cond 

BDL Run 1, FH [3.80],BH [3.80],Cond [3.80] BDL Run 2, FH [3.80],BH [3.80],Cond [3.80] BDL Run 3, FH [3.80],BH [3.80],Cond 

BDL Run 1, FH [3.50],BH [3.50],Cond [3.50] BDL Run 2, FH [3.50],BH [3.50],Cond [3.50] BDL Run 3, FH [3.50],BH [3.50],Cond 

BDL Run 1, FH [5.10],BH [5.10],Cond [5.10] BDL Run 2, FH [5.10],BH [5.10],Cond [5.10] BDL Run 3, FH [5.10],BH [5.10],Cond 

BDL Run 1, FH [3.77],BH [3.77],Cond [3.77] BDL Run 2, FH [3.77],BH [3.77],Cond [3.77] BDL Run 3, FH [3.77],BH [3.77],Cond 

BDL Run 1, FH [25.80],BH [25.80],Cond [25.80] BDL Run 2, FH [25.80],BH [25.80],Cond [25.80] BDL Run 3, FH [25.80],BH [25

BDL Run 1, FH [3.58],BH [3.58],Cond [3.58] BDL Run 2, FH [3.58],BH [3.58],Cond [3.58] BDL Run 3, FH [3.58],BH [3.58],Cond 

BDL Run 1, FH [4.96],BH [4.96],Cond [4.96] BDL Run 2, FH [4.96],BH [4.96],Cond [4.96] BDL Run 3, FH [4.96],BH [4.96],Cond 

BDL Run 1, FH [3.35],BH [3.35],Cond [3.35] BDL Run 2, FH [3.35],BH [3.35],Cond [3.35] BDL Run 3, FH [3.35],BH [3.35],Cond 

BDL Run 1, FH [2.73],BH [2.73],Cond [2.73] BDL Run 2, FH [2.73],BH [2.73],Cond [2.73] BDL Run 3, FH [2.73],BH [2.73],Cond 

BDL Run 1, FH [2.83],BH [2.83],Cond [2.83] BDL Run 2, FH [2.83],BH [2.83],Cond [2.83] BDL Run 3, FH [2.83],BH [2.83],Cond 

BDL Run 1, FH [3.53],BH [3.53],Cond [3.53] BDL Run 2, FH [3.53],BH [3.53],Cond [3.53] BDL Run 3, FH [3.53],BH [3.53],Cond 

BDL Run 1, FH [5.19],BH [5.19],Cond [5.19] BDL Run 2, FH [5.19],BH [5.19],Cond [5.19] BDL Run 3, FH [5.19],BH [5.19],Cond 

BDL Run 1, FH [114.0],BH [114.0],Cond [114.0] BDL Run 2, FH [114.0],BH [114.0],Cond [114.0] BDL Run 3, FH [114.0],BH [114

BDL Run 1, FH [4.05],BH [4.05],Cond [4.05] BDL Run 2, FH [4.05],BH [4.05],Cond [4.05] BDL Run 3, FH [4.05],BH [4.05],Cond 

BDL Run 1, FH [53.9],BH [53.9],Cond [53.9] BDL Run 2, FH [53.9],BH [53.9],Cond [53.9] BDL Run 3, FH [53.9],BH [53.9],Cond 

BDL Run 1, FH [8.71],BH [8.71],Cond [8.71] DLL Run 2, FH [8.71],BH 24.8,Cond [8.71] BDL Run 3, FH [8.71],BH [8.71],Cond [8

BDL Run 1, FH [46.8],BH [46.8],Cond [46.8] BDL Run 2, FH [46.8],BH [46.8],Cond [46.8] BDL Run 3, FH [46.8],BH [46.8],Cond 

BDL Run 1, FH [3.22],BH [3.22],Cond [3.22] BDL Run 2, FH [3.22],BH [3.22],Cond [3.22] BDL Run 3, FH [3.22],BH [3.22],Cond 




95,Cond [.050] DLL Run 3, FH .082,BH .94,Cond [.050]

BH [.050],Cond [.050] DLL Run 3, FH [.050],BH .054,Cond [.050]

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] DLL Run 3, FH [.050],BH .051,Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [.050],Cond [.050] BDL Run 3, FH [.050],BH [.050],Cond [.050] 

BH [3.86],Cond [3.86] BDL Run 3, FH [3.86],BH [3.86],Cond [3.86]

 8.38,Cond [3.25] DLL Run 3, FH [3.25],BH 7.75,Cond [3.25]

BH [3.47],Cond [3.47] BDL Run 3, FH [3.47],BH [3.47],Cond [3.47]

BH [3.94],Cond [3.94] BDL Run 3, FH [3.94],BH [3.94],Cond [3.94]

BH [3.12],Cond [3.12] BDL Run 3, FH [3.12],BH [3.12],Cond [3.12]

BH [2.79],Cond [2.79] BDL Run 3, FH [2.79],BH [2.79],Cond [2.79]
BH [2.64],Cond [2.64] BDL Run 3, FH [2.64],BH [2.64],Cond [2.64]

BH [3.50],Cond [3.50] BDL Run 3, FH [3.50],BH [3.50],Cond [3.50]

BH [2.79],Cond [2.79] BDL Run 3, FH [2.79],BH [2.79],Cond [2.79]

BH [3.39],Cond [3.39] BDL Run 3, FH [3.39],BH [3.39],Cond [3.39]

BH [2.95],Cond [2.95] BDL Run 3, FH [2.95],BH [2.95],Cond [2.95]

BH [4.16],Cond [4.16] BDL Run 3, FH [4.16],BH [4.16],Cond [4.16] 

BH [3.16],Cond [3.16] BDL Run 3, FH [3.16],BH [3.16],Cond [3.16] 

BH [4.08],Cond [4.08] BDL Run 3, FH [4.08],BH [4.08],Cond [4.08] 

BH [3.74],Cond [3.74] BDL Run 3, FH [3.74],BH [3.74],Cond [3.74]

BH [3.64],Cond [3.64] BDL Run 3, FH [3.64],BH [3.64],Cond [3.64]

BH [3.35],Cond [3.35] BDL Run 3, FH [3.35],BH [3.35],Cond [3.35]

BH [3.66],Cond [3.66] BDL Run 3, FH [3.66],BH [3.66],Cond [3.66]

BH [3.26],Cond [3.26] BDL Run 3, FH [3.26],BH [3.26],Cond [3.26]

BH [3.09],Cond [3.09] BDL Run 3, FH [3.09],BH [3.09],Cond [3.09] 

BH [4.24],Cond [4.24] BDL Run 3, FH [4.24],BH [4.24],Cond [4.24]

BH [3.05],Cond [3.05] BDL Run 3, FH [3.05],BH [3.05],Cond [3.05] 

BH [3.31],Cond [3.31] BDL Run 3, FH [3.31],BH [3.31],Cond [3.31]

BH [3.07],Cond [3.07] BDL Run 3, FH [3.07],BH [3.07],Cond [3.07] 

.60],BH [40.60],Cond [40.60] BDL Run 3, FH [40.60],BH [40.60],Cond [40.60] 

BH [3.69],Cond [3.69] BDL Run 3, FH [3.69],BH [3.69],Cond [3.69] 

BH [2.70],Cond [2.70] BDL Run 3, FH [2.70],BH [2.70],Cond [2.70]

BH [3.26],Cond [3.26] BDL Run 3, FH [3.26],BH [3.26],Cond [3.26]

BH [3.36],Cond [3.36] BDL Run 3, FH [3.36],BH [3.36],Cond [3.36]

BH [4.05],Cond [4.05] BDL Run 3, FH [4.05],BH [4.05],Cond [4.05] 

BH [4.09],Cond [4.09] BDL Run 3, FH [4.09],BH [4.09],Cond [4.09]

BH [3.88],Cond [3.88] BDL Run 3, FH [3.88],BH [3.88],Cond [3.88]

BH [3.89],Cond [3.89] BDL Run 3, FH [3.89],BH [3.89],Cond [3.89]

30],BH [25.30],Cond [25.30] BDL Run 3, FH [25.30],BH [25.30],Cond [25.30]

90],BH [28.90],Cond [28.90] BDL Run 3, FH [28.90],BH [28.90],Cond [28.90]

BH [4.02],Cond [4.02] BDL Run 3, FH [4.02],BH [4.02],Cond [4.02] 

BH [3.44],Cond [3.44] BDL Run 3, FH [3.44],BH [3.44],Cond [3.44]

BH [3.80],Cond [3.80] BDL Run 3, FH [3.80],BH [3.80],Cond [3.80]

BH [3.50],Cond [3.50] BDL Run 3, FH [3.50],BH [3.50],Cond [3.50]

BH [5.10],Cond [5.10] BDL Run 3, FH [5.10],BH [5.10],Cond [5.10]

BH [3.77],Cond [3.77] BDL Run 3, FH [3.77],BH [3.77],Cond [3.77]

80],BH [25.80],Cond [25.80] BDL Run 3, FH [25.80],BH [25.80],Cond [25.80]

BH [3.58],Cond [3.58] BDL Run 3, FH [3.58],BH [3.58],Cond [3.58]

BH [4.96],Cond [4.96] BDL Run 3, FH [4.96],BH [4.96],Cond [4.96]

BH [3.35],Cond [3.35] BDL Run 3, FH [3.35],BH [3.35],Cond [3.35]

BH [2.73],Cond [2.73] BDL Run 3, FH [2.73],BH [2.73],Cond [2.73]

BH [2.83],Cond [2.83] BDL Run 3, FH [2.83],BH [2.83],Cond [2.83]

BH [3.53],Cond [3.53] BDL Run 3, FH [3.53],BH [3.53],Cond [3.53]

BH [5.19],Cond [5.19] BDL Run 3, FH [5.19],BH [5.19],Cond [5.19]

4.0],BH [114.0],Cond [114.0] BDL Run 3, FH [114.0],BH [114.0],Cond [114.0] 

BH [4.05],Cond [4.05] BDL Run 3, FH [4.05],BH [4.05],Cond [4.05] 

BH [53.9],Cond [53.9] BDL Run 3, FH [53.9],BH [53.9],Cond [53.9]

H 24.8,Cond [8.71] BDL Run 3, FH [8.71],BH [8.71],Cond [8.71] 

BH [46.8],Cond [46.8] BDL Run 3, FH [46.8],BH [46.8],Cond [46.8]

BH [3.22],Cond [3.22] BDL Run 3, FH [3.22],BH [3.22],Cond [3.22]
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2 Sample 3

Date of Testing 3/24/2010 3/25/2010 3/25/2010

Steam Output (1000 lb/hr) 2009.764 2006.384 2013.48

Total Heat Input (MMBtu/hr) 3585.775 3515.212 3487.327

Basis (Wet/Dry) Dry Dry Dry

Exhaust Steam % Moisture 11.12 11.07 10.98

Exhaust Flow Rate (acfm or dscfm) 1,381,510 1,366,012 1,376,386

Exhaust Temperature (deg C or deg F) 344 334 343

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3

bituminous 464 485 480

Emission Test Results

Hydrogen Cyanide 

Emission Rate 

Sample 1

 (lb/MMBtu)

Hydrogen Cyanide 

Emission Rate 

Sample 2 

(lb/MMBtu)

Hydrogen Cyanide 

Emission Rate 

Sample 3 

(lb/MMBtu)

[<1.56E-05] [<3.61E-05] [<3.57E-05]
Unit of Measure

Other Supporting 

Information

1000 lb/hr

MMBtu/hr

N/A

%

acfm

deg F

Unit of Measure

Fuel Flow 

Measurement 

Method

MMBtu/hr F-Factor

Test Method Used

(ex. U.S. EPA Conditional Test Method 033)

Other Supporting 

Information

U.S. EPA Conditional Test Method 033 (CTM-033) BDL Run 1, [<1.56E-05], BDL Run 2, [<3.61E-05], BDL Run 3, [<3.57E-05]

pH Run 1@15 min 11.5, @30 min 14.0, @ 45 min 13.5, @ 60 min 13.0

pH Run 2@15 min 14.0, @30 min 14.0, @ 45 min 14.0, @ 60 min 14.0

pH Run 3@15 min 11.4, @30 min 14.0, @ 45 min 12.4, @ 60 min 11.4

The HCN was sampled using CTM 033 with

6 normal NaOH and an additional impinger for one 

hour per the clarification given by the USEPA in

FAQ Number 10. http://www.epa.gov/ttn/emc/ctm/ctm-033.pdf
Other Supporting Information

Plant Data

 [<1.56E-05], BDL Run 2, [<3.61E-05], BDL Run 3, [<3.57E-05]

15 min 11.5, @30 min 14.0, @ 45 min 13.5, @ 60 min 13.0

15 min 14.0, @30 min 14.0, @ 45 min 14.0, @ 60 min 14.0

15 min 11.4, @30 min 14.0, @ 45 min 12.4, @ 60 min 11.4

as sampled using CTM 033 with

aOH and an additional impinger for one 

 clarification given by the USEPA in

er 10. http://www.epa.gov/ttn/emc/ctm/ctm-033.pdf
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Emission Test Results Constituent

Consitutent Emission Rate 

Sample 1

 (%)

O2

CO2
Sample 3 Unit of Measure

Other Supporting 

Information

1000 lb/hr

MMBtu/hr

N/A

%

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow 

Measurement Method

Other Supporting 

Information

Consitutent Emission Rate 

Sample 2 

(%)

Consitutent Emission Rate 

Sample 3 

(%)

Test Method Used

(ex. U.S. EPA Method 

3B)

Other Supporting 

Information
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Emission Test Results Constituent

Nitrogen Oxides Emission Rate 

Sample 1 

(lb/MMBtu)

NO

NO2
Sample 3 Unit of Measure Other Supporting Information

1000 lb/hr

MMBtu/hr

N/A

%

Fuel Input Rate 

Sample 3 Unit of Measure Fuel Flow Measurement Method

Nitrogen Oxides Emission Rate 

Sample 1

(ppmvd @ 7% O2)

Nitrogen Oxides Emission Rate 

Sample 2 

(lb/MMBtu)

Nitrogen Oxides Emission Rate 

Sample 2

(ppmvd @ 7% O2)
Other Supporting Information

Nitrogen Oxides Emission Rate 

Sample 3 

(lb/MMBtu)

Nitrogen Oxides Emission Rate 

Sample 3

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA Method 7)
Other Supporting 

Information
EIA Facility Code Facility Name Boiler ID

628 Crystal River Unit 1

Parameter Sample 1 Sample 2

Date of Testing

Steam Output (1000 lb/hr)

Total Heat Input (MMBtu/hr)

Basis (Wet/Dry)

Exhaust Steam % Moisture

Exhaust Flow Rate (acfm or dscfm)

Exhaust Temperature (deg C or deg F)

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Emission Test Results Constituent

Constituent Emission 

Rate Sample 1 

(mg solids/liter)

Total Dissolved Solids (TDS)

Total Suspended Solids (TSS)
Sample 3 Unit of Measure

1000 lb/hr

MMBtu/hr

N/A

%

Fuel Input Rate 

Sample 3 Unit of Measure

Constituent Emission Rate 

Sample 2 

(mg solids/liter)

Constituent Emission Rate 

Sample 3 

(mg solids/liter)
Other Supporting Information

Fuel Flow Measurement Method

Test Method Used

(ex. Standard Test Method for Filterable and Nonfilterable Matter in Water ASTM 

D5907)
Other Supporting 

Information

Other Supporting 

Information





Fuel

anthracite

bituminous

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C)

synfuel

petroleum coke

other

Relative to Control Device

Upstream

Downstream

Fuel Input Units of Measure

MMBtu/hr

standard cubic feet per minute (scfm)

gallon/minute

lb/hour

ton/day

Exhaust Flow Rate Units of Measure

acfm

dscfm

Exhaust Temperature Units of Measure

deg C

deg F

Test Method Used for Fuel Input Rate

F-Factor

gas fuel meter

boiler efficiency calculation

Other

CO Test Method

U.S. EPA Method 10A

U.S. EPA Method 10B
Formaldehyde Test Method

U.S. EPA Method 320

CH4 Test Method

U.S. EPA Method 18

U.S. EPA Method 320

SO2 Test Method

U.S. EPA Method 6

Hg Test Method

U.S. EPA Method 30B

Speciated Volatile Organic HAP Method

U.S. EPA Method 0031 with SW-846 Method 8260B

Speciated Semi-Volatile Organic HAP Method

U.S. EPA Method 0010 with SW-846 Method 8270D

HCN Test Method

U.S. EPA Conditional Test Method 033 (CTM-033)

O2/CO2 Test Method

U.S. EPA Method 3B

NOX Test Method

U.S. EPA Method 7

U.S. EPA Method 7A

U.S. EPA Method 7B

U.S. EPA Method 7C

U.S. EPA Method 7D

TDS/TSS Test Method

Standard Test Method for Filterable and Nonfilterable Matter in Water ASTM D5907

Standard Methods of the Examination of Water and Wastewater Method 2540B

Control Configuration
Listed (by boiler) in Question 16 (page 17) of the questionnaire

Listed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICR

Hg Ontario Hydro Test Method

ASTM Method D6784


Constituent CAS

Acetone 67-64-1

Acetonitrile 75-05-8

Acrolein (Propenal) 107-02-8

Acrylonitrile 107-13-1

Allyl alcohol 107-18-6

Allyl chloride 107-05-1

Azobenzene

Benzene 71-43-2

Benzyl chloride 100-44-7

Bis(2-chloroethyl)sulfide 505-60-2

Bromoacetone 598-31-2

Bromochloromethane 74-97-5

Bromodichloromethane 75-27-4

4-Bromofluorobenzene (surr) 460-00-4

Bromoform 75-25-2

Bromomethane 74-83-9

1,3-Butadiene 106-99-0

n-Butanol 71-36-3

2-Butanone (MEK) 78-93-3

t-Butyl alcohol 75-65-0

Carbazole

Carbon disulfide 75-15-0

Carbon tetrachloride 56-23-5

Chloral hydrate 302-17-0

1,2-Chloro-1,1,2,2-Tetrafluoroethane 76-14-2

Chlorobenzene 108-90-7

Chlorobenzene-d (IS)

Chlorodibromomethane 124-48-1

Chloroethane 75-00-3

2-Chloroethanol 107-07-3

2-Chloroethyl vinyl ether 110-75-8

Chloroform 67-66-3

Chloromethane 74-87-3

Chloroprene 126-99-8

3-Chloropropionitrile 542-76-7

Crotonaldehyde 4170-30-3

Cyclohexane 110-82-7

1,2-Dibromo-3-chloropropane 96-12-8

1,2-Dibromoethane 106-93-4

Dibromochloromethane 124-48-1

Dibromomethane 74-95-3

1,2-Dichlorobenzene 95-50-1

1,3-Dichlorobenzene 541-73-1

1,4-Dichlorobenzene 106-46-7

1,4-Dichlorobenzene-d (IS)

cis-1,4-Dichloro-2-butene 1476-11-5

trans-1,4-Dichloro-2-butene 110-57-6

Dichlorodifluoromethane 75-71-8

1,1-Dichloroethane 75-34-3

1,2-Dichloroethane 107-06-2

1,2-Dichloroethane-d (surr)

Speciated Volatile Organic HAPs
1,1-Dichloroethene 75-35-4

cis-1,2-dichloroethene 156-59-2

trans-1,2-Dichloroethene 156-60-5

1,2-Dichloropropane 78-87-5

1,3-Dichloro-2-propanol 96-23-1

1-1,3-dichloropropene 1006-02-6

cis-1,3-Dichloropropene 10061-01-5

trans-1,3-Dichloropropene 10061-02-6

1,2,3,4-Diepoxybutane 1464-53-5

Diethyl ether 60-29-7

1,4-Difluorobenzene (IS) 540-36-3

1,4-Dioxane 123-91-1

Epichlorohydrin 106-89-8

Ethanol 64-17-5

1-ethyl-4-methybenzene 622-96-8

Ethyl acetate 141-78-6

Ethylbenzene 100-41-4

Ethylene oxide 75-21-8

Ethyl methacrylate 97-63-2

Fluorobenzene (IS) 462-06-6

Heptane 142-82-5

Hexachlorobutadiene 87-68-3

1,1,2,3,4-hexachloro-1,3-butadiene 87-68-3

Hexachloroethane 67-72-1

Hexane 11/5/2003

2-Hexanone 591-78-6

2-Hydroxypropionitrile 78-97-7

Iodomethane 74-88-4

Isobutyl alcohol 78-83-1

Isopropyl alcohol 67-63-0

Isopropylbenzene 98-82-8

Malononitrile 109-77-3

Methacrylonitrile 126-98-7

Methanol 67-56-1

Methylene chloride 75-09-2

Methyl methacrylate 80-62-6

Methyl-t-butyl either (MTBE) 1634-04-4

4-Methyl-2-pentanone (MIBK) 108-10-1

Naphthalene 91-20-3

Nitrobenzene 98-95-3

2-Nitropropane 79-46-9

N-Nitroso-di-n-butylamine 924-16-3

Paraldehyde 123-63-7

Pentachloroethane 76-01-7

2-Pentanone 107-87-9

2-Picoline 109-06-8

1-Propanol 71-23-8

2-Propanol 67-63-0

Propargyl alcohol 107-19-7

$-Propiolactone 57-57-8

Propionitrile (ethyl cyanide) 107-12-0

n-Propylamine 107-10-8

Pyridine 110-86-1

Styrene 100-42-5
1,1,1,2-Tetrachloroethane 630-20-6

lectronic ICR 1,1,2,2-Tetrachloroethane 79-34-5

Tetrachloroethylene 127-18-4

Teteahydrofuran 109-99-9

2,3,4,6-Tetrchlorophenol

Toluene 108-88-3

Toluene-d (surr) 2037-26-5

o-Toluidine 95-53-4

Tribromomethane 75-25-2

1-1,2-trichloro-1,2,2-trifluoroethane 76-13-1

1,2,4-Trichlorobenzene 120-82-1

1,1,1-Trichloroethane 71-55-6

1,1,2-Trichloroethane 79-00-5

Trichloroethylene 79-01-6

Trichlorofluoromethane 75-69-4

Trichloromonofluoromethane 75-69-4

1,2,3-Trichloropropane 96-18-4

1,3,5-trimethylbenzene 108-67-8

1,2,4-trimethlbenzene 95-63-6

Vinyl acetate 108-05-4

Vinyl chloride 75-01-4

m/p-Xylene 95-47-6

o-Xylene 95-47-6

m-Xylene 108-38-3

p-Xylene 106-42-3


Speciated Semi-volatile Organic HAPs

Constituent CAS

Acenaphthene 83-32-9

Acenaphthylene 208-96-8

Acetophenone 98-86-2

2-Acetylaminofluorene 53-96-3

1-Acetyl-2-thiourea 591-08-2

Aldrin 309-00-2

2-Aminoanthraquinone 117-79-3

Aminoazobenzene 60-09-3

4-Aminobiphenyl 92-67-1

3-Amino-9-ethylcarbazole 132-32-1

Anilazine 101-05-3

Aniline 62-53-3

o-Anisidine 90-04-0

Anthracene 120-12-7

Aramite 140-57-8

Aroclor 1016 12674-11-2

Aroclor 1221 11104-28-2

Aroclor 1232 11141-16-5

Aroclor 1242 53469-21-9

Aroclor 1248 12672-29-6

Aroclor 1254 11097-69-1

Aroclor 1260 11096-82-5

Azinphos-methyl 86-50-0

Barban 101-27-9

Benzidine 92-87-5

Benzoic acid 65-85-0

Benz(a)anthracene 56-55-3

Benzo(b)fluoranthene 205-99-2

Benzo(k)fluoranthene 207-08-9

Benzo(g,h,i)perylene 191-24-2

Benzo(a)pyrene 50-32-8

p-Benzoquinone 106-51-4

Benzyl alcohol 100-51-6

α-BHC 319-84-6

β-BHC 319-85-7

δ-BHC 319-86-8

γ-BHC (Lindane) 58-89-9

Bis(2-chloroethoxy)methane 111-91-1

Bis(2-chloroethyl) ether 111-44-4

Bis(2-chloroisopropyl) ether 39638-32-9

Bis(2-ethylhexyl) phthalate 117-81-7

4-Bromophenyl phenyl ether 101-55-3

Bromoxynil 1689-84-5

Butyl benzyl phthalate 85-68-7

Captafol 2425-06-1

Captan 133-06-2
Carbaryl 63-25-2

Carbofuran 1563-66-2

Carbophenothion 786-19-6

Chlordane (NOS) 57-74-9

Chlorfenvinphos 470-90-6

4-Chloroaniline 106-47-8

Chlorobenzilate 510-15-6

5-Chloro-2-methylaniline 95-79-4

4-Chloro-3-methylphenol 59-50-7

3-(Chloromethyl)pyridine hydrochloride 6959-48-4

1-Chloronaphthalene 90-13-1

2-Chloronaphthalene 91-58-7

2-Chlorophenol 95-57-8

4-Chloro-1,2-phenylenediamine 95-83-0

4-Chloro-1,3-phenylenediamine 5131-60-2

4-Chlorophenyl phenyl ether 7005-72-3

Chrysene 218-01-9

Coumaphos 56-72-4

p-Cresidine 120-71-8

Crotoxyphos 7700-17-6

2-Cyclohexyl-4,6-dinitro-phenol 131-89-5

4,4'-DDD 72-54-8

4,4'-DDE 72-55-9

4,4'-DDT 50-29-3

Demeton-O 298-03-3

Demeton-S 126-75-0

Diallate (cis or trans) 2303-16-4

2,4-Diaminotoluene 95-80-7

Dibenz(a,j)acridine 224-42-0

Dibenz(a,h)anthracene 53-70-3

Dibenzofuran 132-64-9

Dibenzo(a,e)pyrene 192-65-4

1,2-Dibromo-3-chloropropane 96-12-8

Di-n-butyl phthalate 84-74-2

Dichlone 117-80-6

1,2-Dichlorobenzene 95-50-1

1,3-Dichlorobenzene 541-73-1

1,4-Dichlorobenzene 106-46-7

3,3'-Dichlorobenzidine 91-94-1

2,4-Dichlorophenol 120-83-2

2,6-Dichlorophenol 87-65-0

Dichlorovos 62-73-7

Dicrotophos 141-66-2

Dieldrin 60-57-1

Diethyl phthalate 84-66-2

Diethylstilbestrol 56-53-1
Diethyl sulfate 64-67-5

Dimethoate 60-51-5

3,3'-Dimethoxybenzidine 119-90-4

Dimethylaminoazobenzene 60-11-7

7,12-Dimethylbenz(a)-anthracene 57-97-6

3,3'-Dimethylbenzidine 119-93-7

α,α-Dimethylphenethylamine 122-09-8

2,4-Dimethylphenol 105-67-9

Dimethyl phthalate 131-11-3

1,2-Dinitrobenzene 528-29-0

1,3-Dinitrobenzene 99-65-0

1,4-Dinitrobenzene 100-25-4

4,6-Dinitro-2-methylphenol 534-52-1

2,4-Dinitrophenol 51-28-5

2,4-Dinitrotoluene 121-14-2

2,6-Dinitrotoluene 606-20-2

Dinocap 39300-45-3

Dinoseb 88-85-7

Diphenylamine 122-39-4

5,5-Diphenylhydantoin 57-41-0

1,2-Diphenylhydrazine 122-66-7

Di-n-octyl phthalate 117-84-0

Disulfoton 298-04-4

Endosulfan I 959-98-8

Endosulfan II 33213-65-9

Endosulfan sulfate 1031-07-8

Endrin 72-20-8

Endrin aldehyde 7421-93-4

Endrin ketone 53494-70-5 X X ND X X 53494-70-5

EPN 2104-64-5

Ethion 563-12-2

Ethyl carbamate 51-79-6

Ethyl methanesulfonate 62-50-0

Famphur 52-85-7

Fensulfothion 115-90-2

Fenthion 55-38-9

Fluchloralin 33245-39-5

Fluoranthene 206-44-0

Fluorene 86-73-7

2-Fluorobiphenyl (surr) 321-60-8

2-Fluorophenol (surr) 367-12-4

Heptachlor 76-44-8

Heptachlor epoxide 1024-57-3

Hexachlorobenzene 118-74-1

Hexachlorobutadiene 87-68-3

Hexachlorocyclopentadiene 77-47-4
Hexachloroethane 67-72-1

Hexachlorophene 70-30-4

Hexachloropropene 1888-71-7

Hexamethylphosphoramide 680-31-9

Hydroquinone 123-31-9

Indeno(1,2,3-cd)pyrene 193-39-5

Isodrin 465-73-6

Isophorone 78-59-1

Isosafrole 120-58-1

Kepone 143-50-0

Leptophos 21609-90-5

Malathion 121-75-5

Maleic anhydride 108-31-6

Mestranol 72-33-3

Methapyrilene 91-80-5

Methoxychlor 72-43-5

3-Methylcholanthrene 56-49-5

4,4'-Methylenebis (2-chloroaniline) 101-14-4

4,4'-Methylenebis(N,N-dimethylaniline) 101-61-1

Methyl methanesulfonate 66-27-3

2-Methylnaphthalene 91-57-6

Methyl parathion 298-00-0

2-Methylphenol 95-48-7

3-Methylphenol 108-39-4

4-Methylphenol 106-44-5

Mevinphos 7786-34-7

Mexacarbate 315-18-4

Mirex 2385-85-5

Monocrotophos 6923-22-4

Naled 300-76-5

Naphthalene 91-20-3

1,4-Naphthoquinone 130-15-4

1-Naphthylamine 134-32-7

2-Naphthylamine 91-59-8

Nicotine 54-11-5

5-Nitroacenaphthene 602-87-9

2-Nitroaniline 88-74-4

3-Nitroaniline 99-09-2

4-Nitroaniline 100-01-6

5-Nitro-o-anisidine 99-59-2

Nitrobenzene 98-95-3

4-Nitrobiphenyl 92-93-3

Nitrofen 1836-75-5

2-Nitrophenol 88-75-5

4-Nitrophenol 100-02-7

5-Nitro-o-toluidine 99-55-8

Nitroquinoline-1-oxide 56-57-5

N-Nitrosodi-n-butylamine 924-16-3

N-Nitrosodiethylamine 55-18-5

N-Nitrosodimethylamine 62-75-9

N-Nitrosodiphenylamine 86-30-6

N-Nitrosodi-n-propylamine 621-64-7

N-Nitrosomethylethylamine 10595-95-6

N-Nitrosomorpholine 59-89-2

N-Nitrosopiperidine 100-75-4
N-Nitrosopyrrolidine 930-55-2

Octamethyl pyrophosphoramide 152-16-9

4,4'-Oxydianiline 101-80-4

Parathion 56-38-2

Pentachlorobenzene 608-93-5

Pentachloronitrobenzene 82-68-8

Pentachlorophenol 87-86-5

Phenacetin 62-44-2

Phenanthrene 85-01-8

Phenobarbital 50-06-6

Phenol 108-95-2

1,4-Phenylenediamine 106-50-3

Phorate 298-02-2

Phosalone 2310-17-0

Phosmet 732-11-6

Phosphamidon 13171-21-6

Phthalic anhydride 85-44-9

2-Picoline (2-Methylpyridine) 109-06-8

Piperonyl sulfoxide 120-62-7

Pronamide 23950-58-5

Propylthiouracil 51-52-5

Pyrene 129-00-0

Resorcinol 108-46-3

Safrole 94-59-7

Strychnine 57-24-9

Sulfallate 95-06-7

Terbufos 13071-79-9

1,2,4,5-Tetrachlorobenzene 95-94-3

2,3,4,6-Tetrachlorophenol 58-90-2

Tetrachlorvinphos 961-11-5

Tetraethyl dithiopyrophosphate 3689-24-5

Tetraethyl pyrophosphate 107-49-3

Thionazine 297-97-2

Thiophenol (Benzenethiol) 108-98-5

Toluene diisocyanate 584-84-9

o-Toluidine 95-53-4

Toxaphene 8001-35-2

1,2,4-Trichlorobenzene 120-82-1

2,4,5-Trichlorophenol 95-95-4

2,4,6-Trichlorophenol 88-06-2

Trifluralin 1582-09-8

2,4,5-Trimethylaniline 137-17-7

Trimethyl phosphate 512-56-1

1,3,5-Trinitrobenzene 99-35-4

Tris(2,3-dibromopropyl) phosphate 126-72-7

Tri-p-tolyl phosphate 78-32-0

O,O,O-Triethyl phosphorothioate 126-68-1