TESTING CONSULTING 

### Report To: D o ver Industrial Ch rome, Inc
. 292 9 N. CampbdI Avenue 

### Chic ago IL 606 I 8 ATTiS: 

### Mr. Arid Schrodt I NC
.



### Pr -ojcct T ype: S.ack Test Analysis f o r Chromium Emissi o ns 

### IDENTIFICATION OF MATERIAL:**D~lIlcL** J. Bell**En~ln..-erJl~ S~**  .... lcc::l 3 15S S. Kolin A**~e. a.lc~:.o**  IL 606!l-4l1S9 Ph o ne: 773_25-1_1406 F , LX; 77l_Z$.l_6G61


### Repo rt D : lt e : 8/ 28 /9 7 Pr 'oj ec t N umber: 

### 06-629 Pr o j ec t In ce ption: 71l1 /9 7

Seven (7) so.rr:ple bottles, fr om 

### 306A air testing, id e ntified below: 

### PRO CE D UR E , D ove r Indusm21 Chr ome is a j ob shop electroplating facility. The facility contains 8 hard chromium plating tanks. Tank #4 is no[ op erati o nal. The test was performed with six of the seven tank s in use. The specificoperating conditions are shm vn in Attac h ment B. 

### Th e test conditions are represe:lt:nive of maximum operating conditions
. Tests were performed on rh e two s t acks that exhaust chr omi um emis s ions simu ltan eously. Both stacks had been modified to meet the criteria for an acceptable sampling point. Testing waS performed in stra igh t se c ti o ns of exho.usl duct following the blowers
. The sampling location on the east stack was 1 6 inches from the end of the stack and 68 inches from t he transition to the blower (See Diagram A). The stack has a diamete r of 32 inch e s. This sampling l oc ation is theref ore 0. 5 duct diameters upstream of the final exit point and 

### 2.1 duct diameters downstream from the flow disrurbance of the transition. The sampling lo cat ion on the west stack was 1 8 inches from th e end of the stack and 90 in ches from the transition to the blower (See Diagram A). The sta c k i s rectangular 

### ( 3 0 " x 4 0") and has an equivalent duct diameter o f 

### 3-1.3 inches. This sampling loc ari o n is theref o re 

### 0.53 duct diameters upstream of the final exit point and 

### 2
. 63 duct diameters down stream from the fl ow di stu r ba n ce of the transition. These sampling sites therefore meet the 

### 2
. 0/0. 5 duct diame te r criteria, as specified in secrion 

### 2.1 of USEPA Meth od 1 

### (40CFR Part 

### 60, Appendix A ). There were 

### 12 sampling points on two traverses, for a total of 

### 24 sampling points, as pe r Method 1 section 2.2.1 and 

### 2.3.1 for the e:lst stack and 

### 25 sampl in g points in a 5 x 5 grid as pe r sec ti on 

### 2.3.2 fo r the west stack. The tests were performed o n July 11 , 1997 by Mr. Daniel 

### J. Bell, Mr. David Caskey, and Mr. Nathan Green of Scientific Control Lab ora tories. An TEPA offici al was not present. All analyses were perf o rmed in accordance with the EPAIlEPA approved test procedures as 

### specified in 40 CFR, pan 63, Method 306A
. N ote : I: is OUf polky t o**k:~p ~Op** **IU** of**~p r1** **S** for six r.\ o nth ,. The daL:l is hpt On**m~** for up to**thre~** yean.. S.ur.ples (if**3ppli~3blc )**  Jf': kept for**:~re~** .... ed;s
. S3rr:pln th3t 3rt b=:d o us .... ill be returned to the**~Ii~nt.** If Ihls**pol i~y**  poses"**dim~ulry.** plnn**eonl3~t** us to m:I);e othcr**3=ng~m~~ts .**  I f repro ducd. our rep o rt.**mu~t** be**n:prot!u~cd** completely
. Any un3uthor'..l:d**;I.!I~r.ltion** of tllis**~port illvJlid31~S**  lhe**CO~le~t.**Pa'! e 2

Scientific ContTol Labs, Inc., is a certified lab o ratory for analysis of potable water (IEPA Cen. #100183), and a certified lab oratory f or wastewater analysis (State of Washing ton Cert. #C165 , State of Wisc o nsin DNR #9 9 8 09 1 9 3 0). This means we have a quality co ntrol program in effect and that this quality c o mr o l pr o grum is monit o red and reviewed annually by the certifying a g encies
. 

### RE SU LTS: The s:lmples were analyzed by atomic abs o rpti o n graphite furnace f o r the detection of t otal chromium.

S A MPLE 1.0
. TE ST CONC. I
TE ST TRL-ti. # I 0
. 057 mgfL EAST STACK 7111197 TEST TRI.U li2 0.058 m gIL EA ST STACK 7 / 11 /97 TEST TRL"-l. #3 0
. 165 m gfL EAST STACK 7/1 1 /97 TEST TlUAL ' 1 0.081 mgfL WEST ST A CK 7 / 11 / 97 TE ST TRIAL #2 0
. 088 mgfL WE ST STACK 7/11 / 97 TEST TRL"-l. "3 0.102 mgfL WE ST STACK 7/1 1 /97 

### BLANK 0.003 m gIL Analyzed by SCL 2 As calcul:ued by SCL (see attached ) 3 Lim it for existing small sourc es ACTUAL EM I SS IO N LIM I T J EM I SS I ON: 0
. 0 088 m g/ds cm 0.03 m gldscm

0
. 0103 m g/dscm 0
. 03 mgldscm

0.026 1 mgldscm 0.03 mgldscm

0
. 014 7 mgfdscm 0.03 mgJdscm

0.0171 mgldscm 0.03 mgfdscm

0.0 170 m gfdscm 0.03 mgfdscm

NA NA

Leak te sts were co n ducted before and after each test run and found to be less than 0.02 

### fr / min. The presence of cyclonic flow was checked at each samp l ing l ocatio n and th e average angle of misalignment was f o und to be 2.5 degrees for th e e ast stack and 3.0 degrees for the west stack
. Since the average ang l e of misalignment was less than 20 degrees, the amoun t of cyclonic flow is acceptable.

Not .: It is o u r polic), to keep cop i es of**~por:s** f o r six month s. The d 3t.:1 IS hpt on tile for up to three ),C31"!
. Samples (if applit3blc) arc hpl for**tb~~** ....... k s. Samples tb31 no: bJoZ.:ml o us ....i ll be reNmed 10 lhe eli=n!. If ! his policy p o ses a dif1icully. ple3se (OplaC! liS t o make o lh.;**lI~ £.** **.n lS.**  If r:: produe e :!
. o ut r::;:o o r: . :nU S! b
. rep rod u c e d co m p! etely
. All Y U03uth o rUcd a! t O:r.I1 io n o f lbis repon ill valid.llcs lb. ( o nt = lI!.

# ~ CL. J.


# .... c.**J.~** •• 

### oc"elf,u Page 3

CONTRO LABORATORIES, INC.


### Mist suppressant is being used to reduce airborne chromic acid mists. Surface tension is being monitored to ensure that the proper concentration of mist suppresant is maintained in the plating solution. Surface tension measurements were taken during testing and are shown in Attachment B SUPPLEMENTAL CALCULATIOr-;S FOR DOVER INDUSTRIAL CHROME, INC. Equation (taken from Method 306A, FR 

### 1125/95, Pg. 4992):

Where: Cc:r =Concentration in stack gas in mg/dscm Mc:r=Amount of Cr in sample from stack sampling in micrograms Tm 

### =Dry gas meter temperature, 

### OF Y m 

### =Dry gas meter correct.ion factor V m 

### =Dry gas meter volume in 

### ff P bar 

### =Barometric pressure in inches of Hg
Dover Indtlstrial Chrome, Inc. Results East Stack-Trial #1: 

### (377 ml in test trial #1 sample) 0.057- 0.003 mgIL 

## = 0.054 mgIL Mer 

## = (0.054 mgIL)x(0.377 L) 

## = 0.0204 mg x 1000 micrograms/mg = 20.36 micrograms 

### Tm 

## = 93.1 OF Y m 

### = 1.03 (see calculation below) 

### Vm = (2.319 m J 

### )(35.3 

### trIm') = 

### 81.86 

## tr P bv 

### = 30.35
Cc:r = (20.36) (93.1 

### + 460) = 0.0088 mg/dscm (499.8)( 1.03)(81.86)(30.35) Dover Industrial Chrome, Inc. Results East Stack-Trial #2: 

### (433 ml in test trial #2 sample) 0.058-0.003 mgIL = 0.055 mgIL Mer 

# = (0.055 mgIL)x(0.433 L) 

## = 0.0238 mg x 1000 micrograms/mg 

# = 23.82 micrograms Tm 

## = 94.8 

### OF Ym 

### =1.03 (see calculation below) 

### Vm = (2.329 m 3 

### )(35.3 

### tr/m3) = 

### 82.21 

### ff P bar 

## = 30.35 Note: It is our**poli~** 10 keep copies of Rpons (or six monlhs. The dal:l is kepi on file for up to three yean. Samples (if appli=le)**~** kept for three weeks. Samples thai are hazardous will be returned 10 the clienL If this**poli~** poses a difficulty, pleuc contact us to make olher anangemenlS. If reproduced. our report. musl be reproduced complelely. Any unauthorized alteration of this report invalidates the conleaL

### Cer 

## = (23.82) (94.8 

### + 460) = 

### 0.0103 mg/dscm (499.8)( 1.03)(82.21 )(30.35)
Dover Industrial Chrome, Inc. Results East Stack-Trial #3: (378 rol in test trial #3 sample) 0.165

- 0.003 mgIL 

## = 0.162 mgIL 

### Mer 

## = (0.162 mgIL)x(0.378 L) 

## = 0.0612 mg x 1000 micrograms/mg 

## = 61.24 micrograms Tm = 

### 94.3 

### OF Y m 

### =1.03 (see calculation below) Vm 

## = (2.361 m 3 

### )(35.3 fe/m') 

## = 83.34 ft3 

### Pilar 

## = 30.35 

### Cer 

## = (61.24) (94.3 + 

### 460) = 

### 0.0261 mg/dscm (499.8)( 1.03)(83.34)(30.35) Dover Industrial Chrome, Inc. Results West Stack-Trial #1: (362 rol in test trial #1 sample) 0.081

- 0.003 mgIL 

## = 0.078 mg/L 

### Mer 

## = (0.078 mg/L)x(0.362 L) = _ 

### 0.0282 mg x 1000 micrograms/mg = 

### 28.24 micrograms Tm 

## = 94.5 

### OF Ym 

## = 0.982 (see calculation below) Vm = 

### (2.022 m3 

### )(35.3 ftl/m 3 ) 

## = 71.38 

### tr P bar = 

### 30.35 

### Cer = 

### (28.24) (94.5 

### + 460) = 

### 0.0147 mg/dscm (499.8)(0.982)(71.38)(30.35) Dover Industrial Chrom.e, Inc. Results West Stack-Trial #2: (390 ml 

### in test trial #2 sample) 0.088-.003 mg/L 

## = 0.085 mgIL 

### Mer 

## = (0.085 mg/L)x(0.390 L) 

## = 0.0332 mg x 1000 micrograms/mg = 

### 33.15 micrograms Tm 

## = 97.4 

### OF Y m 

### = 

### 0.982 (see calculation below) Vm 

## = (2.051 m3

### )(35.3 £r/m3 ) = 

### 72.40**f~** 

### Pilar 

## = 30.35 

### Ccr = 

### (33.15) (97.4 

### + 460) 

## = 0.0171 mg/dscm (499.8)(0.982)(72.40)(30.35)
Note: It is our policy to keep copies of**~pons** for six months. The data is kepi 00 file for up to**th~e** years. Samples (if applicable)**~** kept for**th~** weeks. Samples that are hazatdous will be feNmed to the cIienL If this policy poses a difficulty, please contact us 10 make other arrangements. If reproduced. our**~port.** must be n:produced completely. Any unauthorized a1ter:atioD of this report invalidates the conleDL

# .~ CI. },**~c-. .l.~**  

### dct.en.u

CONTROU LABORATORIES, INC.


### Dover Industrial Chrome, Inc. Results West Stack-Trial #3: 

### (335 ml in test trial #3 sample) 0.102-.003 mg/L 

## = 0.099 mg/L 

### Mer 

# = (0.099 mgIL)x(0.335 

### L) 

## = 0.0332 mg 

### x 1000 micrograms/mg 

# = 33.17 micrograms 

### Tm = 

### 97.1 

### of Y m 

## = 0.982 (see calculation below) Vm 

## = (2.063 m 3 

### )(35.3 tr/m 3 ) 

## = 72.82 

## tr P

bar 

## = 30.35 

# ea 

## = (33,17) (97,1 

### + 460) 

## = 0.0170 mg/dscm 

### (499.8)(0.982)(72.82)(30.35) Quality Control Data: 

### Sample: Duplicate: Spike: LFB::\ 

### LRB:**~**

# ~ 11.41 ppb 10.51 ppb, relative percent difference 

## = 8.21 % 15.30 ppb, 97.3% spike recovery 26,51 ppb, 106% recovery

2.02 ppb, method detection limit = 

### 2.00 ppb
Calculation for Post Test Gas Meter Calibration: 

## - 

## ...

The meters were run for 6 minutes with a critical orifice that allows 0.75 cfm. 

### GAS METER USED ON EAST STACK The gas meter used on the .east stack recorded a volume of 4.6643 

### ftl. The average temperature was 93.0 and the barometric pressure was 30.35 in. of mercury. To correct tostandard conditions:

where: Vm(SId) 

## = (K1)(VJ 

## k+**(~HI13,6)** 

### from EPA Method 5 

## Tm

Kl = 

### 17.64 Vm 

## = volume of gas recorded from post test in 

## ff P b2r 

## = barometric pressure in inches of mercury Note: It is our policy to keep copies of reports for six monlhs. The dau is kepI on file for up 10**th~c** yean. Samples (if applicable) arc kept for thR:C weeks. Samples thai**a~** hazardous will be**~lUmed** to the clienL If this polic;y poses Ii difficulty, please contact us to make other arr.lngements. If reproduced, our report. must be R:produced completely, Any unauthorized llIteratioD of this report iovalidates the conlenL

# ·~ .:£ CL J "'C.

### J..~ oct.el£u Page 6

CONTROU LABORATORIES, INC. 

### ill**~** average pressure differential across the orifice in inches of water provided on orifice calibration sheet T m 

## = temperature in degrees R Vm(std) = 

### C17.64)(4.6643)( 30.35 

### + (1.8/13.6)] 

### 93.0+ 460

_ . Vm(sld) 

## = 4.5353 

### ff
To calculate the standard volume of air passed through the critical orifice: VCI($Id) 

## = K' 

### .[T amb 

### where: K' 

## = factor from orifice calibration sheet provided with critical orifice by manufacturer Pilat = 

### barometric pressure in inches of mercury e 

## = time in minutes T:amb 

## = temperature in degrees R 0.5933 (30.1)(6) .[547.25 V Cl(Sld) 

## = 4.5803 

### ff the Y value for the post test is then: 

### Y m (after laI) =**~$Id)** 

### V m(Sld) 

### Y m(after test) 

## = 4.5803 4.5353

Ym(manu) 

### Y m(after laI) 

## = 1.039· 1.010 = 1.029



### • As provided on the meter calibration sheet provided with the meter by the manufacturer

Note: It is our policy 10 keep copies of repons for six months. The data is kept on file for up 10 three years. Samples (if**app1i~le)** arc kept Cor three weeks. Samples that ale hazardous will be returned to tbe clienl. If this policy poses a difficulty, please CODlaet us 10 make other amlDgemenlS. If reproduced. our report, must be reproduced completely. Any unauthorized a\lenltion oC this report invalidates the contenl.

# ®<
CI. 

### 1

.... C.**.l.~ dC'~l£u**  Page 7 CCNTRCLl I..ABCRATCRIES. INC.**Si~ce** 

### the Y value is between 0.95 and 1.05, the gas meter is acceptable. GAS METER USED ON WEST STACK The gas meter used on the west stack recorded a volume of 4.7703 

## fr. The average temperature was 95.8 and the barometric pressure was 30.35 in. of mercury. To correct to standard conditions:
Vm(Sld) 

## = (17.64)(4.7703)[ 30.35 

### + n.8113.6)] 95.8+ 460 V m(std) 

## = 4.6150 

# re
the Y value for the post test is then: 

### Y

m (:after \eSt) = YatSld) 

### V m(Sld) 

### Y

m(:after lese) 

## = 4.5803 4.6150 

### Y m(aftcr ICSI) 

## = 0.992



## = 0.974· 0.992 = 0.982


### ·As provided on the meter calibration sheet provided with the meter by the manufacturer Since the Y value is between 0.95 and 1.05, the gas meter is acceptable. 

### CONCLUSION: The tests were conducted to demonstrate compliance with the National Emissions Standard for Hazardous Air pollutants (NESHAP),. The results of these perfonnance tests indicate that Dover Industrial Chrome meets the small source emission limit of 0.030 mg/dscm. Ongoing compliance will be demonstrated by recording the surface tension of the chromium plating solutions. Dover Industrial Chrome will be considered to be in compliance as long as the surface tension remains below those values recorc.ted during the performance tests.

Note: It is our policy to keep copies of repons for six. months. The data is kept on file for up to three yeIUS. Samples (if applicable) are kept for three wee""'- Samples that are bazanlous will be returned to the clienL If this policy poses a difficulty. please CODtact us to make otber arrangements. If reproduced, our report. must be reproduced completely. Any unauthorized alteration of this report invalidates the content.· 

### .'

# ~ CL. } 

# ... c .**.s.~** •• oC£tn.u**Pa~e** 

### 8

CONTRO L.A80RATCRIEB, INC.
I certify that the above results are, to the best of my knowledge, true and accurate. If you have any questions please call me. SCIENTIFI.s.-CONTROL LABORATORIES, INC. By

# ~,~//~ /. 

## ,. Daniel 1. Bell 

### CERTIFICATION: 

### The above statements and report were subscribed and sworn to before me this '

DB:db 

### CN06629A TWENTY EIGHTH 

### day of AUGUST, 1997.

# ~rX~ Notary Public "OFFICIAL SEAL" 

### LAURA L. CAIRO Notary Public, State of Illinois My Commission Expires 3/612001

,Note: It is our polit;)' to keep copies of reports for six months. The data is kept on file for up to three years. Samples (if applicable) :ate kept for three weeks. Samples that are hazardous will be returned to the clienL If this policy poses a difficulty, please conlact us to m:ake other amngemenlS. If reproduced. our repOTt. must be reproduced completely. Any unauthorized altel'Btion of Ibis report invalidates tbc conlcnLt' 

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.. r:tE i'LI. : 77347SQ008 Jul. 19 1997 03:29=1'1 Pl 

### DOVER INDUSTRIAL CHROME. INC. 2929 N. Campbell Ave. 

### Chicago, JL 60618 July 18, 1997 Scientific Control Laboratories. Inc. 3158 South Kolin Ave. Chicago.IL 60623-4889 Attn: Dan Bell 

# A........ r/c ;.;jw :::'"/'

--- 

## TS -II
.. -**~J** 

### 7"

Re: Data relating to July 11. 1997 chromium emission testing. Six of seven chrome plating tanks were in operation on July 11. We alternately use either #5 tank or #7 tank, depending upon the work size, but we never use both at once. We pump solution from one to the other as needed and connect one rectifier the the particular tank selected. (Note that at this time we do not have a 

### #4 tank in operation). Tank # Volume Surface Tension Ampere Hours 1 

### 2 3 4 5 6 

### 7 8 before 

### 7529 27.9 838g 

### 22.4 

### 1.5989 27.S not installed not operational 

### 712 9 27.0 

### 1,036g 28.8 373g 24.8 after 

### 29.3 22.0 

### 28.3 27.2 30.3 25.2 during testing

. 36.850



### 19,292



### 9,600 2,050 32.300

3.500 103,592 total If there is any further information required, please let me know. Sincerely yours,

# ~~£,/,,--- Ariel G. Schrodt. Ph
.. D. President 

### Phone: 773-478-2022 Fax: 773-478-0008 e-mail: tvjdover@mcs.com3158 S. KOLIN AVENUE 

### CHICAGO, IL 60623-400n TEL (312) 254-2t106 

### FAX (312) 254-66fJ 

### 1 

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