April 20, 2012 

Mr. Howard Gilberg 

Guida, Slavich and Flores, P.C. 

750 North St. Paul Street, Suite 200 

Dallas, Texas 75201 

Re: Emissions Testing Report – Tile MACT ICR Report 

 - American Marazzi Tile - Multiple Sources - Methods 1, 2, 3, 3A, 4, 5, 23 and 29 

 Sunnyvale, Texas 

 Entec Project No.: 210269 

Dear Mr. Gilberg, 

Please find the attached two (2) hard copies and a CD with a PDF copy of the Tile MACT ICR 

Emissions Testing for Spray Dryer No. 3, Kiln No. 4, Kiln 5 - Upper Chamber and Press Dryer 

No. 10. Testing was conducted at the American Marazzi Tile facility located in Sunnyvale, 

Texas on December 2-3 and 6-7, 2010. A PDF copy of this report has been or will be sent to 

you by email for your records.

This report is the sole property of Guida, Slavich and Flores, P.C. and no additional copies have 

been sent to any other entity. 

We appreciate the opportunity to perform this project for you and hope to be of assistance to 

you in the future. If you have any questions please call 205-358-1011. 

Sincerely, 

Entec Services, Inc. 

John T. Sutton 
EMISSIONS TESTING 

TILE MACT ICR 

ON 

SPRAY DRYER NO. 3, ROLLER KILN NO. 4, 

ROLLER KILN 5–UPPER CHANNEL 

AND PRESS DRYER NO. 10 

AMERICAN MARAZZI TILE, INC. 

DECEMBER 2-3 AND 6-7, 2010 

PROJECT NO.: 210269 

Prepared for 

GUIDA, SLAVICH & FLORES, P.C. 

750 North St. Paul Street, Suite 200 

Dallas, Texas 75201 

ENTEC SERVICES, INC.

30 Monroe Drive 

Pelham, Alabama 35124 

(205) 358-1011 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 2 of 29

EMISSIONS TESTING 

TILE MACT ICR 

ON 

SPRAY DRYER NO. 3, KILN NO. 4, 

ROLLER KILN 5 – UPPER CHANNEL 

AND PRESS DRYER NO. 10 

AMERICAN MARAZZI TILE, INC. 

CONDUCTED ON 

DECEMBER 2-3 AND 6-7, 2010 

I certify that I have personally examined and am familiar with the information 

contained herein. Based on my inquiries of the individuals immediately responsible for 

obtaining the information, I believe the contents of this report deliverable to be true, 

accurate, and complete, to the best of my knowledge. 

Entec Project No. 210269 Report Submitted: April 20, 2012 

Completed By: Reviewed By: 

________________________________ ___________________________________ 

W. Keith Poole 

Manager, Reporting Division 

Troy Burrows 

QA / QC Manager 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 3 of 29

TABLE OF CONTENTS 

SECTION PAGE

1.0 EXECUTIVE SUMMARY ....................................................................................... 6 

2.0 SUMMARY OF TEST RESULTS .......................................................................... 7 

 2.1 SAMPLING ISSUES AND METHOD DEVIATIONS .................................. 7 

3.0 PROCESS DESCRIPTION ................................................................................. 17 

 3.1 CONTROL EQUIPMENT DESCRIPTION ............................................... 18 

4.0 REFERENCE METHOD TEST PROCEDURES ................................................. 19 

4.1 US EPA REFERENCE TEST METHOD 1 – 

 TRAVERSE POINT LAYOUT .................................................................. 19 

4.2 US EPA REFERENCE TEST METHOD 2 – VELOCITY ......................... 19 

4.3 US EPA REFERENCE TEST METHOD 3 – DRY GAS MOLECULAR 

 WEIGHT .................................................................................................. 19 

4.4 US EPA REFERENCE TEST METHOD 3A – DRY GAS MOLECULAR 

 WEIGHT .................................................................................................. 20 

4.5 US EPA REFERENCE TEST METHOD 4 – MOISTURE CONTENT ..... 20 

4.6 US EPA REFERENCE TEST METHOD 23 – DIOXINS FURANS 

 DETERMINATION ................................................................................... 20 

4.7 US EPA REFERENCE TEST METHOD 5 WITH 29- PARTICULATE AND 

 METALS. ................................................................................................ 20 

5.0 QA / QC PROCEDURES..................................................................................... 29 

 

6.0 CALIBRATION PROCEDURES .......................................................................... 29 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 4 of 29

LIST OF APPENDICES 

APPENDIX PAGE 

A RAW TEST DATA AND EMISSIONS CALCULATION 

 SPRAY DRYER NO. 3 – US EPA METHODS 1 - 4 AND 23 ................................ 1 

B RAW TEST DATA AND EMISSIONS CALCULATION 

 KILN NO. 4 – US EPA METHODS 1 – 4 AND 29 ............................................... 16 

C RAW TEST DATA AND EMISSIONS CALCULATION 

 KILN 5-UPPER CHANNEL .................................................................................. 30 

 C.1 US EPA METHODS 1 - 4, 5 AND 29 ......................................................... 31 

 C.2 US EPA METHODS 1 – 4 and 23 .............................................................. 43 

D RAW TEST DATA AND EMISSIONS CALCULATION 

 PRESS DRYER NO. 10 – US EPA METHODS 1 – 4 AND 23 ............................ 61 

E OPERATIONAL AND PRODUCTION DATA ....................................................... 76 

F QA/QC DOCUMENTS AND CHECKLISTS ......................................................... 78 

G LABORATORY CHAINS OF CUSTODY ........................................................... 108 

H LABORATORY DATA ....................................................................................... 116 

 H.1 PARTICULATE MATTER AND MULTIPLE METALS ............................ 117 

 H.2 DIOXINS/FURANS ................................................................................ 128 

I CALIBRATION DATA ........................................................................................ 144 

J QSTI CERTIFICATIONS ................................................................................... 162 

K EXAMPLE CALCULATIONS AND NOMENCLATURE ..................................... 166 

L EPA ICR DOCUMENTS .................................................................................... 178 

 L.1 EPA LETTER AND ENCLOSURES 1 AND 2 ........................................ 179 

 L.2 ENCLOSURES 3 through 9 AND TABLE 1.1 ........................................ 186 

 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

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LIST OF TABLES 

TABLE PAGE 

2-1 EMISSIONS SUMMARY – SPRAY DRYER NO. 3 – METHODS 1-4 AND 23 ...... 8 

2-2 EMISSIONS SUMMARY – ROLLER KILN NO. 4 – METHODS 1-4 AND 23 ...... 10 

2-3 EMISSIONS SUMMARY – KILN 5 UPPER CHANNEL – METHODS 1-4, 5 

 AND 29 ................................................................................................................ 12 

2-4 EMISSIONS SUMMARY – KILN 5 UPPER CHANNEL – METHODS 1-4 AND 23 

 ................................................................................................................. 14 

2-5 EMISSIONS SUMMARY – PRESS DRYER NO. 10 – METHODS 1-4 AND 23 .. 15 

LIST OF FIGURES 

FIGURE PAGE 

4-1 TRAVERSE POINT LAYOUT – SPRAY DRYER NO. 3 ...................................... 23 

4-2 TRAVERSE POINT LAYOUT – ROLLER KILN NO. 4 ........................................ 24 

4-3 TRAVERSE POINT LAYOUT – KILN 5 UPPER CHANNEL ............................... 25 

4-4 TRAVERSE POINT LAYOUT – PRESS DRYER NO. 10 .................................... 26 

4-5 METHOD 23 SAMPLE TRAIN DIAGRAM ........................................................... 27 

4-6 METHOD 5 / 29 SAMPLE TRAIN DIAGRAM ...................................................... 28
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 6 of 29

1.0 EXECUTIVE SUMMARY

On March 12, 2010 the U. S. Environmental Protection Agency (US EPA) issued an 

Information Collection Request (the Tile ICR) to American Marazzi Tile, Inc. Within the Tile ICR, 

Enclosure 2 specified the emission sources and pollutants that were required to be tested and 

Enclosure 3, Table 1.1 Summary of Ceramic Tile Source Test Methods and Alternate Methods, 

specified the test methods and parameters for each pollutant to be tested. These enclosures are 

included as attachments to this report and can be located in Appendix L. 

Although the ICR requested that testing be performed for PM 2.5 and condensable PM, 

these tests were not performed due to an agreement reached between the tile industry and the 

US EPA. The Test Protocol that was submitted and approved reflects this, as there is no 

discussion of these tests. Additionally, because of production issues, Kiln 4 (RK-4) was tested in 

lieu of Kiln 1 (RK-1) and the upper channel of the double layer kiln (RK-5U) was tested in lieu of 

the lower channel (RK-5L). These changes were coordinated with the EPA prior to the testing. 

 On April 13, 2010, the Tile Council of North America (TCNA), through the offices of Guida, 

Slavich and Flores contracted with Entec Services to perform this testing at all TCNA member 

companies who had received the ICR. 

Testing was conducted at American Marazzi Tile on December 2-3 and 6-7, 2010 by Mr. 

Lynn Beane, Mr. Kevin Rosenberg, Mr. Chuck Duncan IV, Mr. Eric Groth, Mr. Lalan Kirby and 

Mr. Ryan Fogg of Entec Services, Inc. Representing American Marazzi Tile was Mr. Steve 

Wiederwax who coordinated testing with plant production personnel. 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 7 of 29

2.0 SUMMARY OF TEST RESULTS 

 Emission testing was conducted on the following sources utilizing US EPA methods 1, 2, 

3, 3A, 4, 5, 23 and 29 of 40 CFR 60, Appendix A as indicated in the table below. 

ICR ID Source Name/Control Device Test Methods 

SD-3 Spray Dryer No. 3/Fabric Filter 1, 2, 3, 3a, 4, 23 

RK-4 Kiln No. 4/No control device 1, 2, 3, 3a, 4, 5, 29 

RK-5U Roller Kiln 5-Upper channel /No control device 1, 2, 3, 3a, 4, 5, 23, 29 

DC-10 Press Dryer No. 10/ No control device 1, 2, 3, 3a, 4, 23 

2.1 SAMPLING ISSUES AND METHOD DEVIATIONS 

 No difficulties or problems were encountered during sampling on the above sources. The 

emissions test summaries on the following pages gives a detailed summary of each test. No 

process data was provided thus emissions are not reported in kg/MG of product. The Company 

will submit process data and corresponding calculations as CBI (confidential business 

information) under separate cover. 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 8 of 29
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 9 of 29

 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 10 of 29

Table 2-2

Emissions Summary

Test Performed For: Testing Performed By: 

Sunnyvale, TX Birmingham Division 

Source(s) Tested: Roller Kiln No. 4 (RK-4) Project Manager: 

Test Condition: Operating Conditions - ICR Tile MACT Lynn Beane 

Test(s) Performed:

Run Number Run 1 Run 2 Run 3 Average

Date of Run 12/6/10 12/7/10 12/7/10 3 Runs

Times, Pollutant Runs (Began - Ended) 1230-1635 0735 - 1137 1210 - 1613 -

Oxygen Conc., % (dry basis) 13.3 13.1 13.2 13.2

Carbon Dioxide Conc. % (dry basis) 4.8 4.9 4.8 4.8

Molecular Weight Of Stack Gas 29.29 29.30 29.29 29.30

Molecular Weight Of Stack Gas 28.01 27.98 27.96 27.98

Isokinetic Sampling Rate % 102.71 99.48 98.67 -

Stack Temperature o

F 480.3 473.4 473.2 475.6

Stack Temperature o

C 249.1 245.2 245.1 246.5

Moisture Content %, v / v 11.33 11.63 11.85 11.60

Average Stack Gas Velocity mps 11.91 12.20 11.80 11.97

Stack Gas Flow @ Actual Conditions acmm 348 356 345 350

Stack Gas Flow @ Standard Conditions scmm 195 200 194 197

Stack Gas Flow @ Dry Standard Conditions dscmm 173 177 171 174

Particulate Conc. @ STP mg / dscm 12.01 10.93 14.56 12.50

Antimony Conc. @ STP mg / dscm 4.73E-04 3.98E-04 5.70E-04 4.80E-04

Arsenic Conc. @ STP mg / dscm 2.01E-02 1.77E-02 2.34E-02 2.04E-02

Beryllium Conc. @ STP mg / dscm 4.78E-05 1.02E-04 6.39E-05 7.12E-05

Cadmium Conc. @ STP mg / dscm 3.04E-03 3.98E-03 5.65E-03 4.22E-03

Chromium Conc. @ STP mg / dscm 1.86E-02 1.60E-02 2.80E-02 2.09E-02

Cobalt Conc. @ STP mg / dscm 3.59E-04 4.81E-04 1.78E-04 3.39E-04

Lead Conc. @ STP mg / dscm 3.84E-02 1.94E-02 6.89E-02 4.22E-02

Manganese Conc. @ STP mg / dscm 7.23E-03 2.47E-02 7.75E-03 1.32E-02

Mercury Conc. @ STP mg / dscm 1.08E-02 1.17E-02 1.18E-02 1.14E-02

Nickel Conc. @ STP mg / dscm 1.53E-03 1.85E-03 1.34E-03 1.57E-03

Selenium Conc. @ STP mg / dscm 2.80E-01 2.59E-01 4.01E-01 3.14E-01

Total Metals Conc. @ STP mg / dscm 3.81E-01 3.56E-01 5.49E-01 4.29E-01

American Marazzi Tile

Methods 1-4, 5 and 29 (Metric)
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 11 of 29

Table 2-2, continued

Emissions Summary

Test Performed For: Testing Performed By: 

Sunnyvale, TX Birmingham Division 

Source(s) Tested: Roller Kiln No. 4 (RK-4) Project Manager: 

Test Condition: Operating Conditions - ICR Tile MACT Lynn Beane 

Test(s) Performed:

Run Number Run Run Run Average

Date of Run 12/6/10 12/7/10 12/7/10 3 Runs

Particulate Conc. @ 7% Oxygen mg / dscmc 22.1 19.4 26.3 22.58

Antimony Conc. @ 7% Oxygen mg / dscmc 8.70E-04 7.04E-04 1.03E-03 8.68E-04

Arsenic Conc. @ 7% Oxygen mg / dscmc 3.70E-02 3.14E-02 4.23E-02 3.69E-02

Beryllium Conc. @ 7% Oxygen mg / dscmc 8.79E-05 1.81E-04 1.16E-04 1.28E-04

Cadmium Conc. @ 7% Oxygen mg / dscmc 5.59E-03 7.04E-03 1.02E-02 7.62E-03

Chromium Conc. @ 7% Oxygen mg / dscmc 3.42E-02 2.84E-02 5.06E-02 3.77E-02

Cobalt Conc. @ 7% Oxygen mg / dscmc 6.60E-04 8.52E-04 3.22E-04 6.11E-04

Lead Conc. @ 7% Oxygen mg / dscmc 7.06E-02 3.43E-02 1.24E-01 7.65E-02

Manganese Conc. @ 7% Oxygen mg / dscmc 1.33E-02 4.38E-02 1.40E-02 2.37E-02

Mercury Conc. @ 7% Oxygen mg / dscmc 1.99E-02 2.07E-02 2.13E-02 2.06E-02

Nickel Conc. @ 7% Oxygen mg / dscmc 2.81E-03 3.27E-03 2.41E-03 2.83E-03

Selenium Conc. @ 7% Oxygen mg / dscmc 5.16E-01 4.59E-01 7.26E-01 5.67E-01

Total Metals Conc. @ 7% Oxygen mg / dscmc 7.01E-01 6.30E-01 9.92E-01 7.74E-01

Particulate Emissions kg / hr 1.25E-01 1.16E-01 1.49E-01 1.30E-01

Antimony Emissions kg / hr 4.92E-06 4.22E-06 5.84E-06 5.00E-06

Arsenic Emissions kg / hr 2.09E-04 1.88E-04 2.40E-04 2.12E-04

Beryllium Emissions kg / hr 4.97E-07 1.08E-06 6.55E-07 7.45E-07

Cadmium Emissions kg / hr 3.16E-05 4.22E-05 5.79E-05 4.39E-05

Chromium Emissions kg / hr 1.93E-04 1.70E-04 2.87E-04 2.17E-04

Cobalt Emissions kg / hr 3.73E-06 5.11E-06 1.83E-06 3.56E-06

Lead Emissions kg / hr 4.00E-04 2.06E-04 7.06E-04 4.37E-04

Manganese Emissions kg / hr 7.52E-05 2.63E-04 7.95E-05 1.39E-04

Mercury Emissions kg / hr 1.13E-04 1.24E-04 1.21E-04 1.19E-04

Nickel Emissions kg / hr 1.59E-05 1.96E-05 1.37E-05 1.64E-05

Selenium Emissions kg / hr 2.92E-03 2.75E-03 4.11E-03 3.26E-03

Total Metals Emissions kg / hr 3.96E-03 3.78E-03 5.63E-03 4.46E-03

American Marazzi Tile

Methods 1-4, 5 and 29 (Metric)
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 12 of 29

Table 2-3

Emissions Summary

Test Performed For: Testing Performed By: 

Sunnyvale, TX Birmingham Division 

Source(s) Tested: Roller Kiln 5 Upper Channel (RK-5U) Project Manager: 

Test Condition: Operating Conditions - ICR Tile MACT Lynn Beane 

Test(s) Performed:

Run Number Run 1 Run 2 Run 3 Average

Date of Run 12/6/10 12/7/10 12/7/10 3 Runs

Times, Pollutant Runs (Began - Ended) 1000-1410 0737-1151 1255-1701 -

Oxygen Conc., % (dry basis) 19.3 19.3 19.0 19.2

Carbon Dioxide Conc. % (dry basis) 0.9 0.9 1.0 0.9

Molecular Weight Of Stack Gas g/g-mole 28.91 28.92 28.92 28.92

Molecular Weight Of Stack Gas g/g-mole 28.59 28.55 28.57 28.57

Isokinetic Sampling Rate % 93.93 99.12 98.85 -

Stack Temperature o

F 231.8 224.5 236.8 231.1

Stack Temperature o

C 111.0 107.0 113.8 110.6

Moisture Content %, v / v 2.98 3.37 3.20 3.18

Average Stack Gas Velocity mps 16.75 16.36 16.87 16.66

Stack Gas Flow @ Actual Conditions acmm 795 776 800 790

Stack Gas Flow @ Standard Conditions scmm 602 601 609 604

Stack Gas Flow @ Dry Standard Conditions dscmm 585 581 589 585

Particulate Conc. @ STP mg / dscm 2.20 3.41 2.81 2.81

Antimony Conc. @ STP mg / dscm 8.86E-05 1.01E-04 1.67E-04 1.19E-04

Arsenic Conc. @ STP mg / dscm 6.91E-03 9.58E-03 7.54E-03 8.01E-03

Beryllium Conc. @ STP mg / dscm 7.68E-05 5.88E-05 5.81E-05 6.46E-05

Cadmium Conc. @ STP mg / dscm 1.86E-04 1.25E-04 1.82E-04 1.64E-04

Chromium Conc. @ STP mg / dscm 8.47E-03 9.46E-03 9.00E-03 8.98E-03

Cobalt Conc. @ STP mg / dscm 6.69E-05 4.12E-05 5.15E-05 5.32E-05

Lead Conc. @ STP mg / dscm 5.68E-03 5.10E-03 5.01E-03 5.26E-03

Manganese Conc. @ STP mg / dscm 2.11E-03 9.43E-04 1.02E-03 1.36E-03

Mercury Conc. @ STP mg / dscm 4.82E-03 8.21E-03 6.07E-03 6.36E-03

Nickel Conc. @ STP mg / dscm 1.73E-03 7.96E-04 9.14E-04 1.15E-03

Selenium Conc. @ STP mg / dscm 2.39E-01 3.23E-01 2.75E-01 2.79E-01

Total Metals Conc. @ STP mg / dscm 2.69E-01 3.57E-01 3.05E-01 3.10E-01

American Marazzi Tile

Methods 1-4, 5 and 29 (Metric)
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 13 of 29

Table 2-3, continued

Emissions Summary

Test Performed For: Testing Performed By: 

Sunnyvale, TX Birmingham Division 

Source(s) Tested: Roller Kiln 5 Upper Channel (RK-5U) Project Manager: 

Test Condition: Operating Conditions - ICR Tile MACT Lynn Beane 

Test(s) Performed:

Run Number Run Run Run Average

Date of Run 12/6/10 12/7/10 12/7/10 3 Runs

Particulate Conc. @ 7% Oxygen mg / dscmc 19.1 29.1 20.7 22.96

Antimony Conc. @ 7% Oxygen mg / dscmc 7.70E-04 8.61E-04 1.23E-03 9.53E-04

Arsenic Conc. @ 7% Oxygen mg / dscmc 6.00E-02 8.17E-02 5.54E-02 6.57E-02

Beryllium Conc. @ 7% Oxygen mg / dscmc 6.68E-04 5.02E-04 4.27E-04 5.32E-04

Cadmium Conc. @ 7% Oxygen mg / dscmc 1.62E-03 1.07E-03 1.34E-03 1.34E-03

Chromium Conc. @ 7% Oxygen mg / dscmc 7.36E-02 8.06E-02 6.62E-02 7.35E-02

Cobalt Conc. @ 7% Oxygen mg / dscmc 5.81E-04 3.51E-04 3.79E-04 4.37E-04

Lead Conc. @ 7% Oxygen mg / dscmc 4.93E-02 4.35E-02 3.69E-02 4.32E-02

Manganese Conc. @ 7% Oxygen mg / dscmc 1.83E-02 8.04E-03 7.51E-03 1.13E-02

Mercury Conc. @ 7% Oxygen mg / dscmc 4.18E-02 7.00E-02 4.46E-02 5.22E-02

Nickel Conc. @ 7% Oxygen mg / dscmc 1.50E-02 6.79E-03 6.72E-03 9.52E-03

Selenium Conc. @ 7% Oxygen mg / dscmc 2.08E+00 2.75E+00 2.02E+00 2.28E+00

Total Metals Conc. @ 7% Oxygen mg / dscmc 2.34E+00 3.05E+00 2.24E+00 2.54E+00

Particulate Emissions kg / hr 7.73E-02 1.19E-01 9.93E-02 9.85E-02

Antimony Emissions kg / hr 3.11E-06 3.52E-06 5.90E-06 4.18E-06

Arsenic Emissions kg / hr 2.42E-04 3.34E-04 2.67E-04 2.81E-04

Beryllium Emissions kg / hr 2.70E-06 2.05E-06 2.06E-06 2.27E-06

Cadmium Emissions kg / hr 6.54E-06 4.36E-06 6.43E-06 5.78E-06

Chromium Emissions kg / hr 2.97E-04 3.29E-04 3.18E-04 3.15E-04

Cobalt Emissions kg / hr 2.34E-06 1.43E-06 1.82E-06 1.87E-06

Lead Emissions kg / hr 1.99E-04 1.78E-04 1.77E-04 1.85E-04

Manganese Emissions kg / hr 7.40E-05 3.29E-05 3.61E-05 4.77E-05

Mercury Emissions kg / hr 1.69E-04 2.86E-04 2.15E-04 2.23E-04

Nickel Emissions kg / hr 6.07E-05 2.77E-05 3.23E-05 4.03E-05

Selenium Emissions kg / hr 8.38E-03 1.13E-02 9.72E-03 9.79E-03

Total Metals Emissions kg / hr 9.44E-03 1.25E-02 1.08E-02 1.09E-02

American Marazzi Tile

Methods 1-4, 5 and 29 (Metric)
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

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American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

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American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

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American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

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3.0 PROCESS DESCRIPTION 

No production data is included in this report. The Company will submit process data and 

corresponding calculations as CBI (confidential business information) under separate cover. 

Nonmetallic Mineral Processing 

This includes the receipt of the raw materials by truck (shale, clay, nepheline syenite, 

feldspar, talc, recycled glass, and sand) and their storage in the raw material storage area. 

These materials are moved by a front-end loader to the appropriate plant and loaded into a feed 

hopper. For Plant 1 with the exception of the shale and clay, these materials are metered 

directly out onto a conveyor system that transports the material to storage silos. The shale and 

clay material is processed through a crusher prior to being conveyed to a storage silo. From the 

storage silos, raw materials are transported by conveyors to surge hoppers that feed the 

individual continuous mills. Within Plant 2 these materials are loaded into a feed hopper and 

then metered directly onto a conveyor belt and transported to surge hoppers that feed the 

continuous mill. Once fed into a continuous ball mill water is added and then milled to the 

desired consistency and viscosity creating a mud like slurry called “slip.” Upon completion of 

the milling process, the slip is pumped in to a concrete slip tank where it is stored before spray 

drying 

Spray Drying 

The slip is then pumped, at high pressure, into one of three spray dryers (atomizer) 

through a series of nozzles that cause the slip to be sprayed as a fine mist into an enclosed hot 

air stream that dries the slip to a fine powder with low moisture content. This prill is transported 

via conveyor systems to the prill silos. The spray dryers are fueled by natural gas. 

Tile Drying 

The individual pressed tiles are transported by roller conveyor to either a horizontal or 

vertical five channel roller dryer to further reduce the moisture content of individual pressed tiles. 

These dried tiles are referred to as “green tile” and this drying process provides the green tiles 

with sufficient strength to undergo glazing and transfer to the kilns. Press dryers are fueled by 

natural gas. 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 18 of 29

Firing 

This step involves heating of the tiles to vitrify (make glass-like) and fuse (bond) the 

glaze material permanently to the surface of the tile body. The green tiles are fed into a fast fire 

roller kiln and fired according to a predetermined temperature curve that exposes the tiles to a 

maximum temperature of approximately 2,000°F and then cooled rapidly by an indirect cooling 

system. This process results in the formation of an attractive product in which the glazing 

materials and tile body are fused permanently together. Natural gas is used as fuel to heat the 

kilns. 

3.1 Control Equipment Description 

Spray Dryer 3 (SD-3) is controlled by a Eurofilter Model FD 1080-18-3000 Dust 

Collector. The Press Dryer (DC-10), Kiln RK-4 (RK-4) and Roller Kiln 5 Upper Chamber 

(RK-5U) are uncontrolled sources. 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 19 of 29

4.0 REFERENCE METHOD TEST PROCEDURES 

 Emission rates were determined using US EPA Reference Test Methods 1, 2, 3, 3A, 4, 

5, 23 and 29 of US EPA 40 CFR 60, Appendix A. Calibration and quality assurance procedures 

of US EPA 40 CFR Part 60, Appendix A and the “Quality Assurance Handbook for Air Pollution 

Measurement System” Volume III Stationary Source-Specific Methods were followed throughout 

the duration of field and laboratory testing for all methods. The most current version for each 

method (as described in the Federal Register) was used. 

 

4.1 US EPA REFERENCE TEST METHOD 1 - TRAVERSE POINT LAYOUT 

For Information on stack dimensions, traverse points, distance to disturbance and other 

relevant data, refer to the drawings presented in Figures 4-1 through 4-4, “Stack Drawing and 

Traverse Point Location”. 

 

4.2 US EPA REFERENCE TEST METHOD 2 - VELOCITY

The velocity of each gas stream was determined according to USEPA Reference 

Method 2 by reading the instantaneous velocity head with an inclined manometer at each 

sampling point with a calibrated S-type pitot. The stack pressure was measured with the static 

side of an S-type pitot tube. A calibrated pyrometer was used to measure stack temperature at 

each sampling point. All test data, worksheets, and spreadsheets presenting the calculations 

are included in Appendices A - D. Calibration procedures for the velocity equipment are located 

in Section 6.0 of this report. Pitot tube, thermocouple, and other measurement device 

calibration worksheets used for the test series are presented in Appendix I. 

4.3 US EPA REFERENCE TEST METHOD 3 - DRY GAS MOLECULAR WEIGHT-CARBON 

 DIOXIDE 

Dry Gas molecular weight (carbon dioxide) was determined using US EPA Reference 

Test Method 3 (Fyrite Method). A sample of the flue gas was extracted from the gas stream 

during each test. These samples were analyzed with a Fyrite gas analyzer. The molecular 

weight of the gas was calculated using the moisture, oxygen and carbon dioxide content, and 

the measured stack gas temperature. 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 20 of 29

4.4 US EPA REFERENCE TEST METHOD 3A - MOLECULAR WEIGHT 

 DETERMINATION-INSTRUMENTAL ANALYSIS- OXYGEN 

The oxygen concentration was determined using US EPA Reference Test Method 3A. A 

sample of the flue gas was extracted from the gas stream during each test. Moisture was 

removed from the sample and the dry sample was then analyzed with an instrumental gas 

analyzer. The molecular weight of the gas was calculated using the moisture, oxygen and 

carbon dioxide content and the measured stack gas temperature. 

4.5 US EPA REFERENCE TEST METHOD 4 - MOISTURE CONTENT 

The moisture content used for calculating the gas stream flow rate was determined by 

measuring the moisture in a series of glass impingers and silica gel impinger gravimetrically with 

an analytical balance with a tolerance of 0.1 g. The volume of gas drawn was corrected to dry 

standard conditions. The dry gas meter and thermocouple calibration forms are contained in 

Appendix I. 

4.6 US EPA REFERENCE TEST METHOD 23 - DIOXIN-FURAN DETERMINATION 

This method is applicable to the determination of polychlorinated dibenzo-p-dioxins 

(PCDD's) and polychlorinated dibenzofurans (PCDF's) from stationary sources. A sample is 

withdrawn from the gas stream isokinetically and collected in the sample probe, on a glass fiber 

filter, and on a packed column of adsorbent material. The sample cannot be separated into a 

particle vapor fraction. The PCDD's and PCDF's are extracted from the sample, separated by 

high resolution gas chromatography, and measured by high resolution mass spectrometry. 

4.7 US EPA REFERENCE TEST METHOD 5 WITH METHOD 29 – PARTICULATE AND 

METALS DETERMINATION 

 The particulate/multiple metals sample train consisted of a heated stainless steel sample 

probe with a glass liner equipped with an S-type pitot tube and thermocouple. The probe was 

attached to a sample module consisting of a heated filter compartment, which houses the in-line 

filter holder equipped with a pre-weighed quartz filter for the collection of the particulate, and a 

series of glass impingers to collect metals and determine moisture. The sample module was 

connected to a control module by means of an umbilical cord. The control module consisted of a 

dry gas meter, calibrated orifice, leak free pump, two inclined manometers, and temperature 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 21 of 29

controllers for the heated filter compartment, the probe, and a thermocouple indicator to monitor 

the required temperatures during the testing. 

 Gas samples were collected as follows: the sample gas was drawn through the sampling 

probe isokinetically and passed through a 3-inch quartz filter on to which particulate matter was 

deposited. The sample gas was then passed through a series of ice-cooled impingers. The first 

and second impingers contained exactly 100 ml each of an absorbing solution (5% HNO3 10% 

H2O2). The third impinger was empty. The fourth and fifth impingers contained exactly 100 ml 

each of acidic KMnO4 absorbing solution. The sixth impinger contained exactly 250 g of silica 

gel, which absorbs any remaining moisture. These impingers were placed in an ice-bath to 

maintain a maximum exit temperature of 68o

 F. The sample gas then passed through a vacuum 

pump followed by a dry gas meter. The dry gas meter integrated the sample gas flow 

throughout the duration of the test. A calibrated orifice attached to the outlet of the dry gas 

meter provided real time flow rate data. 

 A representative gas sample was acquired by sampling for equal periods of time at the 

centroid of a number of equal area regions in the exhaust stack. The sampling rate was 

adjusted at each test point maintaining an isokinetic sampling condition. 

 After the sampling was complete, the filter was removed and placed in a storage 

container. The nozzle, probe liner, and inlet side of the filter holder were quantitatively washed 

with exactly 100 ml of reagent grade acetone and stored in a marked and sealed container. The 

nozzle, probe liner, and inlet side of the filter holder were rinsed again with 0.1N HNO3 and 

placed into another marked and sealed container. The nozzle and probe liner were then rinsed 

with DI water and followed by another acetone rinse. These rinses were not retained and were 

a QA/QC step to ensure clean glassware prior to starting another run. The liquids from the first 

and second impingers were weighed and added to a third marked and sealed container. The 

back half of the filter holder and these two impingers were rinsed with exactly 100 ml of 0.1N 

HNO3 and the rinses were added to the same container. The contents of the third impinger were 

weighed and then rinsed with exactly 100 ml of 0.1N HNO3 and the rinses were placed in a 

fourth marked and sealed container. The liquids from the fourth and fifth impingers were 

weighed and added to a fifth marked and sealed container. These impingers were first rinsed 

with exactly 100 ml of fresh KMnO4, and then exactly 100 ml of distilled water and the rinses 

were added to the sample container. All the samples were transferred to our laboratory for 

particulate determination and shipment to ALS Laboratory Group for metals analysis. The fourth 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 22 of 29

and fifth impingers were then rinsed with a total of 25ml of 8N HCI; this was added to 200ml of 

DI water in a sixth marked container and sealed. The sixth impinger was weighed to determine 

moisture catch of the silica gel. 
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 23 of 29

Client: American Marazzi Tile Job No. :

Source: Spray Dryer 3 (SD-3) Input By:

P Port Type Nipple Port Diameter

Stack Properties: Inches Feet

Stack Diameter (inside), inches: 71.75 5.98

Stack Height (grade to test platform), feet: 50.00

Stack 

Diameters

740.0 10.31

320.0 4.46 12 12

Point No.

1 1.5 8.0

2 4.8 11.3

3 8.5 15.0

4 12.7 19.2

5 17.9 24.4

6 25.5 32.0

7 46.2 52.7

8 53.8 60.3

9 59.1 65.6

10 63.3 69.8

11 66.9 73.4

12 70.2 76.7

* Adjusted points diameter > 24" no point closer than 1.0 inch

* Adjusted points diameter < 24" no point closer than 0.5 inch

Stack Diameters between 12-24 inches minimum points are 8 ; 

4 points per port if the 8 / 2 diameters downstream and

upstream criteria is met.

Figure 4-1

Entec Services, Inc

30 Monroe Drive, Pelham, Alabama 35124

Type of Traverse: Velocity (V) or Particulate (P):

2

STACK DRAWING & TRAVERSE POINT LOCATION

Total Number of Traverse Points:

6

28.078

 'After' Flow Disturbance, Distance (A):

Stack Area, Ft2

:

24

Length of Port, inches:

Inches

Inside Stack

 'Before' Flow Disturbance, Distance (B):

210269

Chuck Duncan IV

Outside Nipple

Number of Points per port / traverse:

Number of Ports:

Inches

6.50

INCHES

71.75 INCHES

INCHES

320.0

740.0
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 24 of 29

Client: American Marazzi Tile Job No. :

Source: Roller Kiln No. 4 (RK-4) Input By:

P Port Type Flange Port Diameter

Stack Properties: Inches Feet

Stack Diameter (inside), inches: 31 2.58

Stack Height (grade to test platform), feet: 50.00

Stack 

Diameters

240.0 7.74

129.0 4.16 12 12

* The port length was different from A side to B side. Therefore, the test crew established probe markings flush with stack wall.

Point No.

1 1.0 *adjusted 1.0

2 2.1 2.1

3 3.7 3.7

4 5.5 5.5

5 7.8 7.8

6 11.0 11.0

7 20.0 20.0

8 23.3 23.3

9 25.5 25.5

10 27.3 27.3

11 28.9 28.9

12 30.0 *adjusted 30.0

* Adjusted points diameter > 24" no point closer than 1.0 inch

* Adjusted points diameter < 24" no point closer than 0.5 inch

Stack Diameters between 12-24 inches minimum points are 8 ; 

4 points per port if the 8 / 2 diameters downstream and

upstream criteria is met.

24

INCHES

Outside Nipple

Inches

Length of Port, inches:* 0.00

31.0 INCHES

INCHES

129.0

240.0

Inches

Inside Stack

 'Before' Flow Disturbance, Distance (B):

5.241

STACK DRAWING & TRAVERSE POINT LOCATION

 'After' Flow Disturbance, Distance (A):

Type of Traverse: Velocity (V) or Particulate (P):

2

Total Number of Traverse Points:

Number of Points per port / traverse:

Number of Ports:

Stack Area, Ft2

:

210269

Chuck Duncan IV

6

Figure 4-2

Entec Services, Inc

30 Monroe Drive, Pelham, AL 35124
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 25 of 29

Client: American Marazzi Tile Job No. :

Source: Roller Kiln 5 Upper Channel (RK-5U) Input By:

P Port Type Flange Port Diameter

Stack Properties: Inches Feet

Stack Diameter (inside), inches: 39.5 3.29

Stack Height (grade to test platform), feet: 100.00

Stack 

Diameters

600.0 15.19

300.0 7.59 12 12

Point No.

1 1.0 *adjusted 7.0

2 2.6 8.6

3 4.7 10.7

4 7.0 13.0

5 9.9 15.9

6 14.1 20.1

7 25.4 31.4

8 29.6 35.6

9 32.5 38.5

10 34.8 40.8

11 36.9 42.9

12 38.5 *adjusted 44.5

* Adjusted points diameter > 24" no point closer than 1.0 inch

* Adjusted points diameter < 24" no point closer than 0.5 inch

Stack Diameters between 12-24 inches minimum points are 8 ; 

4 points per port if the 8 / 2 diameters downstream and

upstream criteria is met.

Figure 4-3

Entec Services, Inc

30 Monroe Drive, Pelham, AL 35124

Type of Traverse: Velocity (V) or Particulate (P):

2

STACK DRAWING & TRAVERSE POINT LOCATION

Total Number of Traverse Points:

6

8.510

 'After' Flow Disturbance, Distance (A):

Stack Area, Ft2

:

24

Length of Port, inches:

Inches

Inside Stack

 'Before' Flow Disturbance, Distance (B):

210269

Kevin Rosenberg

Outside Nipple

Number of Points per port / traverse:

Number of Ports:

Inches

6.00

INCHES

39.5 INCHES

INCHES

300.0

600.0
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 26 of 29

Client: American Marazzi Tile Job No. :

Source: Press Dryer 10 (DC-10) Input By:

P Port Type Nipple Port Diameter

Stack Properties: Inches Feet

Stack Diameter (inside), inches: 19.0 1.58

Stack Height (grade to test platform), feet: 50.00

Stack 

Diameters

600.0 31.58

42.0 2.21 12 12

Point No.

1 0.5 adjusted 5.3

2 1.3 6.0

3 2.2 7.0

4 3.4 8.1

5 4.8 9.5

6 6.8 11.5

7 12.2 17.0

8 14.3 19.0

9 15.6 20.4

10 16.8 21.5

11 17.7 22.5

12 18.5 adjusted 23.3

* Adjusted points diameter > 24" no point closer than 1.0 inch

* Adjusted points diameter < 24" no point closer than 0.5 inch

Stack Diameters between 12-24 inches minimum points are 8 ; 

4 points per port if the 8 / 2 diameters downstream and

upstream criteria is met.

Figure 4-4

Entec Services, Inc

30 Monroe Drive, Pelham, AL 35124

Type of Traverse: Velocity (V) or Particulate (P):

2

STACK DRAWING & TRAVERSE POINT LOCATION

Total Number of Traverse Points:

3

1.969

 'After' Flow Disturbance, Distance (A):

Stack Area, Ft2:

24

Length of Port, inches:

Inches

Inside Stack

 'Before' Flow Disturbance, Distance (B):

210269

Kevin Rosenberg

Outside Nipple

Number of Points per port / traverse:

Number of Ports:

Inches

4.75

INCHES

19.0 INCHES

INCHES

42.0

600.0
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 27 of 29
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 28 of 29
American Marazzi Tile, Inc. – Sunnyvale, TX Project No. 210269 

Page 29 of 29

5.0 QA / QC PROCEDURES 

Specific Quality Assurance / Quality Control (QA / QC) procedures were adhered to 

during this test project to provide valid and scientifically defensible data. For any environmental 

field and laboratory measurement, a degree of uncertainty exists in the data due to inherent 

limitations of the measurement systems employed. Entec Services, Inc. objective of the QA / 

QC program is to produce data of known precision, accuracy, representation, completeness, 

and comparability. Special Entec-designed QA/QC checklists are contained in Appendix F. 

6.0 CALIBRATION PROCEDURES 

 All of the emission testing equipment used was calibrated according to the procedures 

outlined in the EPA 40 CFR Part 60 Appendix “A” and the Quality Assurance Handbook for Air 

Pollution Measurement Systems, Volume III, EPA-600/4-94-038c. Complete calibration records 

are located in the appendix of this report. 
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 1 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 2 of 215
Client: 

Source: Spray Dryer 3 (SD-3)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0821-1229 1422-1829 0802-1207 -

Sampling Time  minutes 240 240 240 240

Stack Area As Ft2 28.08 28.08 28.08 -

Barometric Pressure Pbar in. Hg 29.75 29.75 30.07 29.910

Stack Static Pressure Pg in. H20 -0.40 -0.40 -0.40 -0.40

Pitot Tube Correction factor Cp - 0.84 0.84 0.84 -

Meter Correction Factor Y - 1.010 1.010 1.010 -

Meter Delta H @ H@ in. H20 1.905 1.905 1.905 1.905

Nozzle Diameter Dn inches 0.243 0.243 0.243 -

Meter Volume Vm dcf 149.195 157.492 151.328 152.672

Meter Temperature tm o

F 67.4 81.0 69.8 72.7

Avg. Orifice Delta H H in. H20 1.34 1.47 1.37 1.39

Impingers Weight Gain (Moisture) Wimp grams 587.5 586.8 596.2 590.2

Silica Gel Impinger Weight Gain (Moisture) Wsg grams 40.4 36.4 42.6 39.8

Oxygen Concentration, % (dry basis) O2 % 18.5 18.6 19.3 18.80

Carbon Dioxide Concentration, % (dry basis) CO2 % 1.2 1.1 1.1 1.14

Avg. Sq. Rt. of Delta P sqrt P in. H20 1/2 0.754 0.781 0.764 0.766

Stack Temperature ts o

F 215.1 215.6 214.8 215.2

2, 3, 7, 8 - TCDD pg 4.1 4.7 3.0 3.9

1, 2, 3, 7, 8 - PeCDD pg 1.2 1.5 1.2 1.3

1, 2, 3, 4, 7, 8 - HxCDD pg 1.9 1.4 1.3 1.5

1, 2, 3, 6, 7, 8 - HxCDD pg 1.7 1.2 1.2 1.4

1, 2, 3, 7, 8, 9 - HxCDD pg 1.8 1.3 1.3 1.5

1, 2, 3, 4, 6, 7, 8 - HpCDD pg 5.5 3.9 3.0 4.1

OCDD pg 59 71 44 57.8

2, 3, 7, 8 - TCDF pg 1.4 1.8 2.0 1.7

1, 2, 3, 7, 8 - PeCDF pg 0.84 1.10 0.92 0.95

2, 3, 4, 7, 8 - PeCDF pg 0.87 1.10 0.9 0.96

210269

Chuck Duncan IV

American Marazzi Tile, Inc Job No.:

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Run Number

Field Data

Data Input By:

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 3 of 215
Client: 

Source: Spray Dryer 3 (SD-3)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/02/10 12/02/10 12/03/10 All Runs

210269

Chuck Duncan IV

American Marazzi Tile, Inc Job No.:

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Run Number

Field Data

Data Input By:

1, 2, 3, 4, 7, 8 - HxCDF pg 0.74 0.97 0.57 0.76

1, 2, 3, 6, 7, 8 - HxCDF pg 0.66 0.87 0.51 0.68

2, 3, 4, 6, 7, 8 - HxCDF pg 0.70 0.92 0.54 0.72

1, 2, 3, 7, 8, 9 - HxCDF pg 0.81 1.10 0.62 0.84

1, 2, 3, 4, 6, 7, 8 - HpCDF pg 0.85 0.94 1.10 0.96

1, 2, 3, 4, 7, 8, 9 - HpCDF pg 1.0 0.81 0.86 0.9

OCDF pg 1.6 2.1 0.9 1.6

Other - TCDD pg 29.8 29.6 3.6 21.0

Other - PeCDD pg 4.8 3.2 1.7 3.2

Other - HxCDD pg 3.2 1.8 2.0 2.3

Other - HpCDD pg 5.0 1.3 4.9 3.8

Other - TCDF pg 1.4 1.8 2.0 1.7

Other - PeCDF pg 2.28 1.10 0.92 1.43

Other - HxCDF pg 0.81 1.10 0.62 0.84

Other - HpCDF pg 1.0 0.81 0.9 0.9

Total Dioxans pg 117.6 120.7 23.2 87.2

Total Furans pg 15.0 16.5 13.4 15.0

Total Dioxans and Furans pg 132.5 137.3 36.6 102.1

Indicates values below the detection limit (BDL).

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 4 of 215
Client:

Source: Spray Dryer 3 (SD-3)

Formulas Symbol Units Calculated Data QC'd by Keith Poole

Run Numbers - - 1 2 3 AVERAGE

Test Date(s) - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0821-1229 1422-1829 0802-1207 -

1. Stack Pressure = Pbar + Pg / 13.6 Ps in. Hg 29.72 29.72 30.04 29.83

2. Meter Pressure = Pbar + DH / 13.6 Pm in. Hg 29.85 29.86 30.17 29.96

3. Standard Meter Volume = 17.64* Y* (Vm/Tm)* (Pbar + DH / 13.6) Vm(std) dscf 150.503 154.933 153.591 153.009

4a. Standard Volume of Water Vapor Condensed =0.04706*Wimp Vwc(std) scf 27.648 27.615 28.057 27.773

4b. Standard Volume of Water Collected in Silica Gel =0.04715*Wsg Vwsg(std) scf 1.905 1.716 2.009 1.877

5. Moisture Fraction =(Vwc(std) + Vwsg(std))/(Vwc(std) + Vwsg(std) + Vm(std)) Bws fraction 0.1641 0.1592 0.1637 0.1623

6. Moisture Fraction @ Saturation (Theoretical) =10[6.6911-(3144/(ts+390.86)]/Ps TBws fraction 1.0000 1.0000 1.0000 1.0000

7. Standard Water Volume @ Saturation (Theoretical) =Vm(std) * (TBws)/(1-TBws) TVW(std) scf 150.50 154.93 153.59 153.01

8. Volume of Water @ Saturation (Theoretical) =TVw(std)/0.04707 TVlc ml 3197.4 3291.6 3263.0 3250.7

9. Molecular Weight of Stack Gas (dry) = 0.32*(O2)+ 0.44*(CO2)+0.28*(100-(O2)-(CO2)) Md lb / lb-mole 28.932 28.922 28.948 28.934

10. Molecular Weight of Stack Gas (wet) = Md*(1-Bws)+18.0*(Bws) Ms lb / lb-mole 27.138 27.183 27.156 27.159

11. Average Stack Gas Velocity = 85.49*Cp*(sqrt DP)avg*SQRT((Ts) / (Ps*Mw)) vs ft / s 49.555 51.28 49.92 50.25

12. Stack Gas Flow @ Actual Conditions = 60*vs*As Qa acfm 83,486 86,387 84,107 84,660

13. Stack Gas Flow @ Standard Conditions = Qa*(Tstd/Ts)*(Ps/Pstd) Qs scfm 64,831 67,034 66,050 65,972

14. Stack Gas Flow @ Dry Standard Conditions = Qa*(1-Bws)*(Tstd/Ts)*(Ps/Pstd) Qstd dscfm 54,190 56,364 55,237 55,264

15 2 3 7 8 TCDD C t ti *( / 12)/ ( ) C /d f 4 20E 13 4 68E 13 3 01E 13 3 97E 13

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: Chuck Duncan IV

American Marazzi Tile, Inc Job No.: 210269

15a. 2, 3, 7, 8 - TCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.20E-13 4.68E-13 3.01E-13 3.97E-13

15b. 1, 2, 3, 7, 8 - PeCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.23E-13 1.49E-13 1.21E-13 1.31E-13

15c. 1, 2, 3, 4, 7, 8 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.95E-13 1.39E-13 1.31E-13 1.55E-13

15d. 1, 2, 3, 6, 7, 8 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.74E-13 1.20E-13 1.21E-13 1.38E-13

15e. 1, 2, 3, 7, 8, 9 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.85E-13 1.29E-13 1.31E-13 1.48E-13

15f. 1, 2, 3, 4, 6, 7, 8 - HpCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 5.62E-13 3.88E-13 3.01E-13 4.17E-13

15g. OCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 6.01E-12 7.06E-12 4.40E-12 5.82E-12

15h. 2, 3, 7, 8 - TCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.44E-13 1.79E-13 2.01E-13 1.75E-13

15i. 1, 2, 3, 7, 8 - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.61E-14 1.10E-13 9.24E-14 9.60E-14

15j. 2, 3, 4, 7, 8 - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.92E-14 1.10E-13 9.04E-14 9.64E-14

15k. 1, 2, 3, 4, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.59E-14 9.66E-14 5.73E-14 7.66E-14

15l. 1, 2, 3, 6, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 6.77E-14 8.66E-14 5.12E-14 6.85E-14

15m. 2, 3, 4, 6, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.18E-14 9.16E-14 5.42E-14 7.25E-14

15n. 1, 2, 3, 7, 8, 9 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.30E-14 1.10E-13 6.23E-14 8.50E-14

15o. 1, 2, 3, 4, 6, 7, 8 - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.71E-14 9.36E-14 1.11E-13 9.71E-14

15p. 1, 2, 3, 4, 7, 8, 9 - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.03E-13 8.07E-14 8.64E-14 8.99E-14

15q. OCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.64E-13 2.11E-13 9.34E-14 1.56E-13

15r. Other - TCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.06E-12 2.95E-12 3.58E-13 2.12E-12

15s. Other - PeCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.88E-13 3.14E-13 1.69E-13 3.23E-13

15t. Other - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.29E-13 1.75E-13 2.04E-13 2.36E-13

15u. Other - HpCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 5.15E-13 1.29E-13 4.95E-13 3.80E-13

15v. Other - TCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.44E-13 1.79E-13 2.01E-13 1.75E-13

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 5 of 215
Client:

Source: Spray Dryer 3 (SD-3)

Formulas Symbol Units Calculated Data QC'd by Keith Poole

Run Numbers - - 1 2 3 AVERAGE

Test Date(s) - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0821-1229 1422-1829 0802-1207 -

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: Chuck Duncan IV

American Marazzi Tile, Inc Job No.: 210269

15w. Other - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.34E-13 1.10E-13 9.24E-14 1.45E-13

15x. Other - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.30E-14 1.10E-13 6.23E-14 8.50E-14

15y. Other - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.03E-13 8.07E-14 8.64E-14 8.99E-14

15z. Total Dioxans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.21E-11 1.20E-11 2.33E-12 8.80E-12

15aa. Total Furans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.53E-12 1.65E-12 1.34E-12 1.51E-12

15ab. Total Dioxans and Furans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.36E-11 1.37E-11 3.67E-12 1.03E-11

20a. 2, 3, 7, 8 - TCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 2.43E-12 2.83E-12 2.62E-12 2.63E-12

20b. 1, 2, 3, 7, 8 - PeCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 7.13E-13 9.03E-13 1.05E-12 8.88E-13

20c. 1, 2, 3, 4, 7, 8 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.13E-12 8.43E-13 1.13E-12 1.04E-12

20d. 1, 2, 3, 6, 7, 8 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.01E-12 7.22E-13 1.05E-12 9.26E-13

20e. 1, 2, 3, 7, 8, 9 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.07E-12 7.82E-13 1.13E-12 9.95E-13

20f. 1, 2, 3, 4, 6, 7, 8 - HpCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 3.25E-12 2.35E-12 2.62E-12 2.74E-12

20g. OCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 3.48E-11 4.27E-11 3.82E-11 3.86E-11

20h. 2, 3, 7, 8 - TCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 8.31E-13 1.08E-12 1.75E-12 1.22E-12

20i. 1, 2, 3, 7, 8 - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.99E-13 6.62E-13 8.03E-13 6.55E-13

20j 2 3 4 7 8 P CDF t ti dj t d t 7% O2 20j. 2, 3, 4, 7, 8 - PeCDF concentration adjusted to 7% O2 =C * ((20 9 7)/(20 9 %O2)) Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr /d f sc c 5 17E 13 5.17E-13 6 62E 13 6.62E-13 7 85E 13 7.85E-13 6 55E 13 6.55E-13

20k. 1, 2, 3, 4, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.39E-13 5.84E-13 4.97E-13 5.07E-13

20l. 1, 2, 3, 6, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 3.92E-13 5.24E-13 4.45E-13 4.54E-13

20m. 2, 3, 4, 6, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.16E-13 5.54E-13 4.71E-13 4.80E-13

20n. 1, 2, 3, 7, 8, 9 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.81E-13 6.62E-13 5.41E-13 5.61E-13

20o. 1, 2, 3, 4, 6, 7, 8 - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.05E-13 5.66E-13 9.60E-13 6.77E-13

20p. 1, 2, 3, 4, 7, 8, 9 - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.94E-13 4.88E-13 7.51E-13 6.11E-13

20q. OCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 9.50E-13 1.28E-12 8.12E-13 1.01E-12

20r. Other - TCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.77E-11 1.78E-11 3.11E-12 1.29E-11

20s. Other - PeCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 2.83E-12 1.90E-12 1.47E-12 2.06E-12

20t. Other - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.91E-12 1.06E-12 1.77E-12 1.58E-12

20u. Other - HpCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 2.98E-12 7.82E-13 4.30E-12 2.69E-12

20v. Other - TCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 8.31E-13 1.08E-12 1.75E-12 1.22E-12

20w. Other - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.35E-12 6.62E-13 8.03E-13 9.40E-13

20x. Other - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.81E-13 6.62E-13 5.41E-13 5.61E-13

20y. Other - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.94E-13 4.88E-13 7.51E-13 6.11E-13

20z. Total Dioxans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 6.98E-11 7.27E-11 2.02E-11 5.42E-11

20aa. Total Furans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 8.88E-12 9.96E-12 1.17E-11 1.02E-11

20ab. Total Dioxans and Furans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 7.87E-11 8.26E-11 3.19E-11 6.44E-11

21a. 2, 3, 7, 8 - TCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.95E-10 2.26E-10 1.43E-10 1.88E-10

21b. 1, 2, 3, 7, 8 - PeCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.71E-11 7.22E-11 5.71E-11 6.21E-11

21c. 1, 2, 3, 4, 7, 8 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 9.05E-11 6.74E-11 6.18E-11 7.32E-11

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 6 of 215
Client:

Source: Spray Dryer 3 (SD-3)

Formulas Symbol Units Calculated Data QC'd by Keith Poole

Run Numbers - - 1 2 3 AVERAGE

Test Date(s) - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0821-1229 1422-1829 0802-1207 -

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: Chuck Duncan IV

American Marazzi Tile, Inc Job No.: 210269

21d. 1, 2, 3, 6, 7, 8 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 8.10E-11 5.77E-11 5.71E-11 6.53E-11

21e. 1, 2, 3, 7, 8, 9 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 8.57E-11 6.25E-11 6.18E-11 7.00E-11

21f. 1, 2, 3, 4, 6, 7, 8 - HpCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.61E-10 1.88E-10 1.43E-10 1.97E-10

21g. OCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.79E-09 3.41E-09 2.08E-09 2.76E-09

21h. 2, 3, 7, 8 - TCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.67E-11 8.66E-11 9.51E-11 8.28E-11

21i. 1, 2, 3, 7, 8 - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.00E-11 5.29E-11 4.38E-11 4.56E-11

21j. 2, 3, 4, 7, 8 - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.14E-11 5.29E-11 4.28E-11 4.57E-11

21k. 1, 2, 3, 4, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.52E-11 4.67E-11 2.71E-11 3.63E-11

21l. 1, 2, 3, 6, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.14E-11 4.19E-11 2.43E-11 3.25E-11

21m. 2, 3, 4, 6, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.33E-11 4.43E-11 2.57E-11 3.44E-11

21n. 1, 2, 3, 7, 8, 9 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.86E-11 5.29E-11 2.95E-11 4.03E-11

21o. 1, 2, 3, 4, 6, 7, 8 - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.05E-11 4.52E-11 5.23E-11 4.60E-11

21p. 1, 2, 3, 4, 7, 8, 9 - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.76E-11 3.90E-11 4.09E-11 4.25E-11

21q. OCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 7.62E-11 1.02E-10 4.42E-11 7.41E-11

21r. Other - TCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.42E-09 1.42E-09 1.69E-10 1.00E-09

21 Oth P CDD M E i i 21s. Other - PeCDD Mass Emissions = (60/7000)* *Q d (60/7000)*cs*Qsd PMR lb / h sr 2 27E 10 2.27E-10 1 52E 10 1.52E-10 7 99E 11 7.99E-11 1 53E 10 1.53E-10

21t. Other - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.53E-10 8.47E-11 9.66E-11 1.11E-10

21u. Other - HpCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.39E-10 6.25E-11 2.34E-10 1.79E-10

21v. Other - TCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.67E-11 8.66E-11 9.51E-11 8.28E-11

21w. Other - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.09E-10 5.29E-11 4.38E-11 6.84E-11

21x. Other - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.86E-11 5.29E-11 2.95E-11 4.03E-11

21y. Other - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.76E-11 3.90E-11 4.09E-11 4.25E-11

21z. Total Dioxans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.60E-09 5.81E-09 1.10E-09 4.17E-09

21aa. Total Furans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 7.12E-10 7.96E-10 6.35E-10 7.14E-10

21ab. Total Dioxans and Furans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.31E-09 6.60E-09 1.74E-09 4.88E-09

22. Volume collected through nozzle =Ts/Ps*[0.002669*Vlc+ Vm*Y*Pm/Tm] Vn acf 231.800 237.393 233.801 234.331

23. Particulate Matter (FH Filterable PM Conc., actual cond.) =0.01543*mn/Vn ca gr / acf 0.00000 0.00000 0.00000 0.00000

24. Isokinetic Sampling Rate, Percent = 100*Vn / (60*vs*An*q) I % 100.86 99.83 100.98 100.56

Post Meter Orifice Cal. (EMC ALT-009 Yqa) yqa 1.0122 1.0173 1.0093 1.013

% Difference, (Calibration must be within 5% of original Y-factor) -0.29%

Indicates values below the detection limit (BDL).

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 7 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269

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American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 31 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 32 of 215
Client: 

Source: Roller Kiln 5 Upper Channel (RK-5U)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/06/10 12/07/10 12/07/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 1000-1410 0737-1151 1255-1701 -

Sampling Time  minutes 240 240 240 240

Stack Area As Ft2 8.51 8.51 8.51 -

Barometric Pressure Pbar in. Hg 29.75 30.08 30.08 29.998

Stack Static Pressure Pg in. H20 -0.42 -0.52 -0.51 -0.49

Pitot Tube Correction factor Cp - 0.84 0.84 0.84 -

Meter Correction Factor Y - 1.002 1.002 1.002 -

Meter Delta H @ H@ in. H20 1.878 1.878 1.878 1.878

Nozzle Diameter Dn inches 0.215 0.240 0.240 -

Meter Volume Vm dcf 135.062 174.487 181.913 163.821

Meter Temperature tm o

F 56.8 57.6 73.1 62.5

Avg. Orifice Delta H H in. H20 1.11 1.77 1.85 1.58

Impingers Weight Gain (Moisture) Wimp grams 69.2 103.0 94.0 88.7

Silica Gel Impinger Weight Gain (Moisture) Wsg grams 20.8 30.4 34.0 28.4

Oxygen Concentration, % (dry basis) O2 % 19.30 19.27 19.01 19.19

Carbon Dioxide Concentration, % (dry basis) CO2 % 0.87 0.92 1.01 0.93

Avg. Sq. Rt. of Delta P sqrt P in. H20 1/2 0.848 0.837 0.856 0.847

Stack Temperature ts o

F 231.8 224.5 236.8 231.1

Particulate Matter Mass (FH Filterable PM) mn mg 8.6 17.4 14.5 13.5

MSb μg 0.55 0.52 0.86 0.64

MAs μg 27.0 48.9 38.9 38.2

MBe μg 0.3 0.3 0.3 0.3

MCd μg 0.73 0.69 0.94 0.79

MCr μg 33.1 48.2 46.5 42.6

MCo μg 0.46 0.41 0.47 0.45

MPb μg 22.2 26.0 25.9 24.7

MMn μg 8.24 4.81 5.27 6.11

MHg μg 18.8 41.9 31.3 30.7

MNi μg 6.76 4.06 4.72 5.18

Mse μg 933 1647 1419 1333

μg 1,050.8 1,823.0 1,574.5 1482.75

*Beryllium was not detected on this source. The number above represents the summation of the detection limits.

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Antimony (Sb)

Arsenic (As)

Run Number

Field Data

Data Input By:

210269

Kevin Rosenberg

American Marazzi Tile, Inc. Job No.:

Beryllium (Be)*

Total Metals collected

Selenium (Se)

Mercury (Hg)

Nickel (Ni)

Cadmium (Cd)

Chromium (Cr, total)

Lead (Pb)

Manganese (Mn)

Cobalt (Co)

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 33 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated Data QC'd by 

Run Number - - 1 23 AVETest Date - - 12/06/10 12/07/10 12/07/10 AlTimes, Pollutant Runs (Began - Ended) - Military Time 1000-1410 0737-1151 1255-1701 1. Stack Pressure = Ps*25.4 Ps mm. Hg 754.9 763.1 763.1 72. Meter Pressure = Pm*25.4 Pm mm. Hg 757.7 767.3 767.5 73. Standard Meter Volume =Vm(std) * 0.02831685 Vm(std) dscm 3.904 5.099 5.163 44a. Standard Volume of Water Vapor Condensed =0.04706*Wimp Vwc(std) scm 0.092 0.137 0.125 04b. Standard Volume of Water Collected in Silica Gel =0.04715*Wsg Vwsg(std) scm 0.028 0.041 0.045 05. Moisture Fraction =(Vwc(std) + Vwsg(std))/(Vwc(std) + Vwsg(std) + Vm(std)) Bws fraction 0.0298 0.0337 0.0320 09. Molecular Weight of Stack Gas (dry) = 0.32*(O2)+ 0.44*(CO2)+0.28*(100-(O2)-(CO2)) Md g / g-mole 28.91 28.92 28.92 210. Molecular Weight of Stack Gas (wet) = Md*(1-Bws)+18.0*(Bws) Ms g / g-mole 28.59 28.55 28.57 211. Average Stack Gas Velocity = 85.49*Cp*(sqrt DP)avg*SQRT((Ts) / (Ps*Mw)) vs m / s 16.75 16.36 16.87 112. Stack Gas Flow @ Actual Conditions = vs*As Qa acmm 795 776 800 13. Stack Gas Flow @ Standard Condition = Qa*(Tstd/Ts)*(Ps/Pstd) Qs scmm 602 601 609 14. Stack Gas Flow @ Dry Standard Condition = Qa*(1-Bws)*(Tstd/Ts)*(Ps/Pstd) Qstd, d dscmm 585 581 589 15. Particulate Matter (FH Filterable PM Conc. @ STP) =mn/Vm(std) cs mg / dscm 2.20 3.41 2.81 215. Antimony Conc. @ STP =0.001*mn/Vm(std) cSb mg / dscm 1.40E-04 1.01E-04 1.67E-04 1.315. Arsenic Conc. @ STP =0.001*mn/Vm(std) cAs mg / dscm 6.91E-03 9.58E-03 7.54E-03 8.015. Beryllium Conc. @ STP =0.001*mn/Vm(std) cBe mg / dscm 7.68E-05 5.88E-05 5.81E-05 6.415. Cadmium Conc. @ STP =0.001*mn/Vm(std) cCd mg / dscm 1.86E-04 1.35E-04 1.82E-04 1.615. Chromium Conc. @ STP =0.001*mn/Vm(std) cCr mg / dscm 8.47E-03 9.46E-03 9.00E-03 8.915. Cobalt Conc. @ STP =0.001*mn/Vm(std) cCo mg / dscm 1.18E-04 8.04E-05 9.03E-05 9.615. Lead Conc. @ STP =0.001*mn/Vm(std) cPb mg / dscm 5.68E-03 5.10E-03 5.01E-03 5.215. Manganese Conc. @ STP =0.001*mn/Vm(std) cMn mg / dscm 2.11E-03 9.43E-04 1.02E-03 1.315. Mercury Conc. @ STP =0.001*mn/Vm(std) cHg mg / dscm 4.82E-03 8.21E-03 6.07E-03 6.315. Nickel Conc. @ STP =0.001*mn/Vm(std) cNi mg / dscm 1.73E-03 7.96E-04 9.14E-04 1.115. Selenium Conc. @ STP =0.001*mn/Vm(std) cSe mg / dscm 2.39E-01 3.23E-01 2.75E-01 2.715.Total Metals Conc. @ STP =0.001*mn/Vm(std) cTSM mg / dscm 0.2692 0.3575 0.3050 015. Particulate Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cs7 mg / dscmc 1.91E+01 2.91E+01 2.07E+01 2.315. Antimony Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cSb mg / dscmc 0.0012 0.0009 0.0012 1.115. Arsenic Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cAs mg / dscmc 0.0600 0.0817 0.0554 6.515. Beryllium Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cBe mg / dscmc 0.0007 0.0005 0.0004 5.315. Cadmium Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cCd mg / dscmc 0.0016 0.0012 0.0013 1.3

Description

Kevin Rosen

CALCULATED TEST DATA - Metric Units

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

American Marazzi Tile, Inc. 210269

Data Input By:

Job No.:

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 34 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated Data QC'd by 

Run Number - - 1 23 AVETest Date - - 12/06/10 12/07/10 12/07/10 Al

Description

Kevin Rosen

CALCULATED TEST DATA - Metric Units

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

American Marazzi Tile, Inc. 210269

Data Input By:

Job No.:

15. Chromium Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cCr mg / dscmc 0.0736 0.0806 0.0662 7.315. Cobalt Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cCo mg / dscmc 0.0010 0.0007 0.0007 7.915. Lead Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cPb mg / dscmc 0.0493 0.0435 0.0369 4.315. Manganese Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cMn mg / dscmc 0.0183 0.0080 0.0075 1.115. Mercury Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cHg mg / dscmc 0.0419 0.0700 0.0446 5.215. Nickel Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cNi mg / dscmc 0.0150 0.0068 0.0067 9.515. Selenium Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cSe mg / dscmc 2.0755 2.7547 2.0218 2.215.Total Metals Conc. @ 7% Oxygen =Cs * ((20.9-7)/(20.9-%O2)) cTSM mg / dscmc 2.3382 3.0486 2.2428 2.521. Particulate Emissions = (0.000001)*cs*Qsd PMR kg / hr 0.0773 0.1189 0.0993 017. Antimony Emissions = (0.000001)*CSb*Qsd Sb-kg/hr kg / hr 4.905E-06 3.519E-06 5.898E-06 4.717. Arsenic Emissions = (0.000001)*CAs*Qsd As-kg/hr kg / hr 2.423E-04 3.338E-04 2.666E-04 0.017. Beryllium Emissions = (0.000001)*CBe*Qsd Be-kg/hr kg / hr 2.695E-06 2.050E-06 2.055E-06 0.017. Cadmium Emissions = (0.000001)*CCd*Qsd Cd-kg/hr kg / hr 6.540E-06 4.701E-06 6.433E-06 0.017. Chromium Emissions = (0.000001)*CCr*Qsd Cr-kg/hr kg / hr 2.972E-04 3.294E-04 3.183E-04 0.017. Cobalt Emissions = (0.000001)*CCo*Qsd Co-kg/hr kg / hr 4.141E-06 2.801E-06 3.192E-06 0.017. Lead Emissions = (0.000001)*CPb*Qsd Pb-kg/hr kg / hr 1.992E-04 1.775E-04 1.773E-04 0.017. Manganese Emissions = (0.000001)*CMn*Qsd Mn-kg/hr kg / hr 7.402E-05 3.286E-05 3.610E-05 0.017. Mercury Emissions = (0.000001)*CHg*Qsd Hg-kg/hr kg / hr 1.691E-04 2.861E-04 2.147E-04 0.017. Nickel Emissions = (0.000001)*CNi*Qsd Ni-kg/hr kg / hr 6.073E-05 2.774E-05 3.233E-05 0.017. Selenium Emissions = (0.000001)*CSe*Qsd Se-kg/hr kg / hr 8.379E-03 1.125E-02 9.723E-03 0.017. Total Metals Emissions = (0.000001)*CTSM*Qsd TSM-kg/hr kg / hr 0.00944 0.01246 0.01079 0.022. Volume collected through nozzle =Ts/Ps*[0.002669*Vlc+ Vm*Y*Pm/Tm] Vn acm 5.308 6.814 7.010 624. Isokinetic Sampling Rate, Percent = 100*Vn / (60*vs*An*q) I % 93.93 99.12 98.85 9Post Meter Orifice Cal. (EMC ALT-009 Yqa) yqa 1.0172 0.9886 0.9831 0% Difference, (Calibration must be within 5% of original Y-factor) 0

Beryllium was not detected in any of the three samples. Results are calculated at the detection limit.

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 35 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269

Report Appendix Page 36 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 37 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269

Report Appendix Page 38 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 39 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 40 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 41 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 42 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 43 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 44 of 215
Client: 

Source: Roller Kiln 5 Upper Channel (RK-5U)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/06/10 12/07/10 12/07/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 1000-1411 0739-1153 1257-1700 -

Sampling Time  minutes 240 240 240 240

Stack Area As Ft2 8.51 8.51 8.51 -

Barometric Pressure Pbar in. Hg 29.75 30.08 30.08 29.998

Stack Static Pressure Pg in. H20 -0.42 -0.51 -0.51 -0.49

Pitot Tube Correction factor Cp - 0.84 0.84 0.84 -

Meter Correction Factor Y - 0.977 0.977 0.977 -

Meter Delta H @ H@ in. H20 1.725 1.725 1.725 1.725

Nozzle Diameter Dn inches 0.235 0.235 0.235 -

Meter Volume Vm dcf 165.079 173.963 172.930 170.657

Meter Temperature tm o

F 56.0 52.3 65.5 57.9

Avg. Orifice Delta H H in. H20 1.45 1.63 1.57 1.55

Impingers Weight Gain (Moisture) Wimp grams 66.5 86.2 83.4 78.7

Silica Gel Impinger Weight Gain (Moisture) Wsg grams 34.1 36.3 39.4 36.6

Oxygen Concentration, % (dry basis) O2 % 19.30 19.27 19.01 19.19

Carbon Dioxide Concentration, % (dry basis) CO2 % 0.87 0.92 1.01 0.93

Avg. Sq. Rt. of Delta P sqrt P in. H20 1/2 0.838 0.841 0.827 0.835

Stack Temperature ts o

F 232.4 226.4 237.4 232.1

2, 3, 7, 8 - TCDD pg 160.0 208.0 199.0 189.0

1, 2, 3, 7, 8 - PeCDD pg 258.0 332.0 348.0 312.7

1, 2, 3, 4, 7, 8 - HxCDD pg 119.0 144.0 141.0 134.7

1, 2, 3, 6, 7, 8 - HxCDD pg 220.0 267.0 236.0 241.0

1, 2, 3, 7, 8, 9 - HxCDD pg 478.0 639.0 561.0 559.3

1, 2, 3, 4, 6, 7, 8 - HpCDD pg 2,780.0 3,940.0 3,280.0 3333.3

OCDD pg 40,500 57,600 53,100 50400.0

2, 3, 7, 8 - TCDF pg 45.8 67.9 61.2 58.3

1, 2, 3, 7, 8 - PeCDF pg 8.88 12.50 12.20 11.19

2, 3, 4, 7, 8 - PeCDF pg 38.40 44.90 41.7 41.67

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Run Number

Field Data

Data Input By:

210269

Kevin Rosenberg

American Marazzi Tile, Inc. Job No.:

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 45 of 215
Client: 

Source: Roller Kiln 5 Upper Channel (RK-5U)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/06/10 12/07/10 12/07/10 All Runs

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Run Number

Field Data

Data Input By:

210269

Kevin Rosenberg

American Marazzi Tile, Inc. Job No.:

1, 2, 3, 4, 7, 8 - HxCDF pg 9.03 10.90 12.00 10.64

1, 2, 3, 6, 7, 8 - HxCDF pg 4.80 5.30 5.93 5.34

2, 3, 4, 6, 7, 8 - HxCDF pg 7.30 8.66 9.75 8.57

1, 2, 3, 7, 8, 9 - HxCDF pg 1.00 1.70 2.11 1.60

1, 2, 3, 4, 6, 7, 8 - HpCDF pg 5.60 8.00 6.64 6.75

1, 2, 3, 4, 7, 8, 9 - HpCDF pg 1.2 1.70 2.20 1.7

OCDF pg 10.2 13.1 15.9 13.1

Other - TCDD pg 1,620.0 1,922.0 1,761.0 1767.7

Other - PeCDD pg 3,312.0 4,048.0 3,642.0 3667.3

Other - HxCDD pg 4,713.0 6,080.0 5,352.0 5381.7

Other - HpCDD pg 4,050.0 5,540.0 4,950.0 4846.7

Other - TCDF pg 191.2 272.1 270.8 244.7

Other - PeCDF pg 102.72 111.60 124.10 112.81

Other - HxCDF pg 34.07 30.84 43.31 36.07

Other - HpCDF pg 0.9 4.73 4.3 3.3

Total Target Analytes Dibenzo-p-dioxins pg 58,210 80,720 73,570 70,833

Total Target Analytes Dibenzofurans pg 461 594 612 556

Total Target Analytes Dibenzo-p-dioxins and Dibenzofurans pg 58,671 81,314 74,182 71,389

Indicates values below the detection limit (BDL).

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 46 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated D

Run Numbers - - 1 2 Test Date(s) - - 12/06/10 12/07/10 Times, Pollutant Runs (Began - Ended) - Military Time 1000-1411 0739-1153 1. Stack Pressure = Pbar + Pg / 13.6 Ps in. Hg 29.72 30.04 2. Meter Pressure = Pbar + DH / 13.6 Pm in. Hg 29.86 30.20 3. Standard Meter Volume = 17.64* Y* (Vm/Tm)* (Pbar + DH / 13.6) Vm(std) dscf 164.697 176.813 4a. Standard Volume of Water Vapor Condensed =0.04706*Wimp Vwc(std) scf 3.129 4.057 4b. Standard Volume of Water Collected in Silica Gel =0.04715*Wsg Vwsg(std) scf 1.608 1.712 5. Moisture Fraction =(Vwc(std) + Vwsg(std))/(Vwc(std) + Vwsg(std) + Vm(std)) Bws fraction 0.0280 0.0316 9. Molecular Weight of Stack Gas (dry) = 0.32*(O2)+ 0.44*(CO2)+0.28*(100-(O2)-(CO2)) Md g / g-mole 28.911 28.918 10. Molecular Weight of Stack Gas (wet) = Md*(1-Bws)+18.0*(Bws) Ms g / g-mole 28.606 28.573 11. Average Stack Gas Velocity = 85.49*Cp*(sqrt DP)avg*SQRT((Ts) / (Ps*Mw)) vs ft / s 54.296 54.03 12. Stack Gas Flow @ Actual Conditions = 60*vs*As Qa acfm 27,723 27,586 13. Stack Gas Flow @ Standard Conditions = Qa*(Tstd/Ts)*(Ps/Pstd) Qs scfm 20,990 21,298 14. Stack Gas Flow @ Dry Standard Conditions = Qa*(1-Bws)*(Tstd/Ts)*(Ps/Pstd) Qstd dscfm 20,403 20,625 15a. 2, 3, 7, 8 - TCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.50E-11 1.82E-11 15b. 1, 2, 3, 7, 8 - PeCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.42E-11 2.90E-11 15c. 1, 2, 3, 4, 7, 8 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.11E-11 1.26E-11 15d. 1, 2, 3, 6, 7, 8 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.06E-11 2.33E-11 15e. 1, 2, 3, 7, 8, 9 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.48E-11 5.58E-11 15f. 1, 2, 3, 4, 6, 7, 8 - HpCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.60E-10 3.44E-10 

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: 

American Marazzi Tile, Inc. Job No.: 

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 47 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated D

Run Numbers - - 1 2 Test Date(s) - - 12/06/10 12/07/10 

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: 

American Marazzi Tile, Inc. Job No.: 

15g. OCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.79E-09 5.03E-09 15h. 2, 3, 7, 8 - TCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.29E-12 5.93E-12 15i. 1, 2, 3, 7, 8 - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.32E-13 1.09E-12 15j. 2, 3, 4, 7, 8 - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.60E-12 3.92E-12 15k. 1, 2, 3, 4, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.46E-13 9.51E-13 15l. 1, 2, 3, 6, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.50E-13 4.63E-13 15m. 2, 3, 4, 6, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 6.84E-13 7.56E-13 15n. 1, 2, 3, 7, 8, 9 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 9.37E-14 1.48E-13 15o. 1, 2, 3, 4, 6, 7, 8 - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 5.25E-13 6.98E-13 15p. 1, 2, 3, 4, 7, 8, 9 - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.12E-13 1.48E-13 15q. OCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 9.56E-13 1.14E-12 15r. Other - TCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.52E-10 1.68E-10 15s. Other - PeCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.10E-10 3.53E-10 15t. Other - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.42E-10 5.31E-10 15u. Other - HpCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.79E-10 4.83E-10 15v. Other - TCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.79E-11 2.37E-11 15w. Other - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 9.62E-12 9.74E-12 15x. Other - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 3.19E-12 2.69E-12 15y. Other - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 8.53E-14 4.13E-13 

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 48 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated D

Run Numbers - - 1 2 Test Date(s) - - 12/06/10 12/07/10 

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: 

American Marazzi Tile, Inc. Job No.: 

15z. Total Dioxans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 5.45E-09 7.04E-09 15aa. Total Furans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 4.32E-11 5.18E-11 15ab. Total Dioxans and Furans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 5.50E-09 7.10E-09 20a. 2, 3, 7, 8 - TCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 1.30E-10 1.55E-10 20b. 1, 2, 3, 7, 8 - PeCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 2.10E-10 2.47E-10 20c. 1, 2, 3, 4, 7, 8 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 9.69E-11 1.07E-10 20d. 1, 2, 3, 6, 7, 8 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 1.79E-10 1.99E-10 20e. 1, 2, 3, 7, 8, 9 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.89E-10 4.76E-10 20f. 1, 2, 3, 4, 6, 7, 8 - HpCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 2.26E-09 2.93E-09 20g. OCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.30E-08 4.29E-08 20h. 2, 3, 7, 8 - TCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.73E-11 5.05E-11 20i. 1, 2, 3, 7, 8 - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 7.23E-12 9.30E-12 20j. 2, 3, 4, 7, 8 - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.13E-11 3.34E-11 

20k. 1, 2, 3, 4, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 7.35E-12 8.11E-12 20l. 1, 2, 3, 6, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.91E-12 3.94E-12 20m. 2, 3, 4, 6, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 5.94E-12 6.44E-12 20n. 1, 2, 3, 7, 8, 9 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 8.14E-13 1.27E-12 20o. 1, 2, 3, 4, 6, 7, 8 - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 4.56E-12 5.95E-12 20p. 1, 2, 3, 4, 7, 8, 9 - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 9.77E-13 1.27E-12 

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 49 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated D

Run Numbers - - 1 2 Test Date(s) - - 12/06/10 12/07/10 

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: 

American Marazzi Tile, Inc. Job No.: 

20q. OCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 8.30E-12 9.75E-12 20r. Other - TCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 1.32E-09 1.43E-09 20s. Other - PeCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 2.70E-09 3.01E-09 20t. Other - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.84E-09 4.52E-09 20u. Other - HpCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.30E-09 4.12E-09 20v. Other - TCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 1.56E-10 2.02E-10 20w. Other - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 8.36E-11 8.31E-11 20x. Other - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 2.77E-11 2.30E-11 20y. Other - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 7.41E-13 3.52E-12 20z. Total Dioxans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 4.74E-08 6.01E-08 20aa. Total Furans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 3.75E-10 4.42E-10 

20ab. Total Dioxans and Furans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) C7%O2 gr / dscfc 4.78E-08 6.05E-08 

21a. 2, 3, 7, 8 - TCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.70E-09 3.31E-09 21b. 1, 2, 3, 7, 8 - PeCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.35E-09 5.29E-09 21c. 1, 2, 3, 4, 7, 8 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.01E-09 2.29E-09 21d. 1, 2, 3, 6, 7, 8 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.71E-09 4.25E-09 21e. 1, 2, 3, 7, 8, 9 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 8.06E-09 1.02E-08 21f. 1, 2, 3, 4, 6, 7, 8 - HpCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.69E-08 6.28E-08 21g. OCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.83E-07 9.18E-07 

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 50 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated D

Run Numbers - - 1 2 Test Date(s) - - 12/06/10 12/07/10 

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: 

American Marazzi Tile, Inc. Job No.: 

21h. 2, 3, 7, 8 - TCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 7.72E-10 1.08E-09 21i. 1, 2, 3, 7, 8 - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.50E-10 1.99E-10 21j. 2, 3, 4, 7, 8 - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.47E-10 7.15E-10 21k. 1, 2, 3, 4, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.52E-10 1.74E-10 21l. 1, 2, 3, 6, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 8.09E-11 8.44E-11 21m. 2, 3, 4, 6, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.23E-10 1.38E-10 21n. 1, 2, 3, 7, 8, 9 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.69E-11 2.71E-11 21o. 1, 2, 3, 4, 6, 7, 8 - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 9.44E-11 1.27E-10 21p. 1, 2, 3, 4, 7, 8, 9 - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.02E-11 2.71E-11 21q. OCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.72E-10 2.09E-10 21r. Other - TCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.73E-08 3.06E-08 21s. Other - PeCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.58E-08 6.45E-08 21t. Other - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 7.94E-08 9.69E-08 21u. Other - HpCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.83E-08 8.83E-08 21v. Other - TCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.22E-09 4.33E-09 21w. Other - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.73E-09 1.78E-09 21x. Other - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.74E-10 4.91E-10 21y. Other - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.53E-11 7.54E-11 21z. Total Dioxans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 9.81E-07 1.29E-06 

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 51 of 215
Client:

Source: Roller Kiln 5 Upper Channel (RK-5U)

Formulas Symbol Units Calculated D

Run Numbers - - 1 2 Test Date(s) - - 12/06/10 12/07/10 

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

Description

Data Input By: 

American Marazzi Tile, Inc. Job No.: 

21aa. Total Furans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 7.77E-09 9.46E-09 21ab. Total Dioxans and Furans Emissions = (60/7000)*cs*Qsd PMR lbs / hr 9.89E-07 1.30E-06 22. Volume collected through nozzle =Ts/Ps*[0.002669*Vlc+ Vm*Y*Pm/Tm] Vn acf 223.698 236.395 24. Isokinetic Sampling Rate, Percent = 100*Vn / (60*vs*An*q) I % 94.99 100.88 Post Meter Orifice Cal. (EMC ALT-009 Yqa) yqa 0.9912 0.9884 % Difference, (Calibration must be within 5% of original Y-factor) 

Indicates values below the detection limit (BDL).

American Marazzi Tile, Inc. Sunnyvale, TX

Project No. 210269

Report Appendix Page 52 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269

Report Appendix Page 53 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 54 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269

Report Appendix Page 55 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 56 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269

Report Appendix Page 57 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 58 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 59 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 60 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 61 of 215
American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 62 of 215
Client: 

Source: Press Dryer 10 (DC-10)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0735-1139 1255-1700 0735-1138 -

Sampling Time  minutes 240 240 240 240

Stack Area As Ft2 1.97 1.97 1.97 -

Barometric Pressure Pbar in. Hg 29.75 29.75 30.07 29.910

Stack Static Pressure Pg in. H20 -0.18 -0.18 -0.20 -0.19

Pitot Tube Correction factor Cp - 0.84 0.84 0.84 -

Meter Correction Factor Y - 1.002 1.002 1.002 -

Meter Delta H @ H@ in. H20 1.878 1.878 1.878 1.878

Nozzle Diameter Dn inches 0.300 0.300 0.300 -

Meter Volume Vm dcf 167.103 168.552 163.954 166.536

Meter Temperature tm o

F 58.2 80.6 65.1 68.0

Avg. Orifice Delta H H in. H20 1.57 1.48 1.48 1.51

Impingers Weight Gain (Moisture) W grams 351 9 408 2 433 1 397 7

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Run Number

Field Data

Data Input By:

210269

Kevin Rosenberg

American Marazzi Tile, Inc. Job No.:

Impingers Weight Gain (Moisture) Wimp grams 351.9 408.2 433.1 397.7

Silica Gel Impinger Weight Gain (Moisture) Wsg grams 43.1 38.8 35.6 39.2

Oxygen Concentration, % (dry basis) O2 % 18.80 18.80 18.72 18.77

Carbon Dioxide Concentration, % (dry basis) CO2 % 0.95 0.95 0.99 0.96

Avg. Sq. Rt. of Delta P sqrt P in. H20 1/2 0.507 0.493 0.496 0.499

Stack Temperature ts o

F 216.5 222.1 218.5 219.0

2, 3, 7, 8 - TCDD pg 2.5 2.2 1.5 2.1

1, 2, 3, 7, 8 - PeCDD pg 1.6 1.6 1.5 1.6

1, 2, 3, 4, 7, 8 - HxCDD pg 1.8 1.7 1.3 1.6

1, 2, 3, 6, 7, 8 - HxCDD pg 1.6 1.5 1.2 1.4

1, 2, 3, 7, 8, 9 - HxCDD pg 1.7 2.2 2.0 2.0

1, 2, 3, 4, 6, 7, 8 - HpCDD pg 8.3 10.4 10.1 9.6

OCDD pg 215 233 210 219.3

2, 3, 7, 8 - TCDF pg 1.2 1.6 1.8 1.5

1, 2, 3, 7, 8 - PeCDF pg 0.84 0.92 0.74 0.83

2, 3, 4, 7, 8 - PeCDF pg 0.82 0.90 1.0 0.91

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 63 of 215
Client: 

Source: Press Dryer 10 (DC-10)

Symbol Units Test Data QC'd by Keith Poole

- - 1 2 3AVERAGE

Test Date - - 12/02/10 12/02/10 12/03/10 All Runs

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

INPUT DATA

Run Number

Field Data

Data Input By:

210269

Kevin Rosenberg

American Marazzi Tile, Inc. Job No.:

1, 2, 3, 4, 7, 8 - HxCDF pg 0.81 0.81 0.56 0.73

1, 2, 3, 6, 7, 8 - HxCDF pg 0.72 0.73 0.50 0.65

2, 3, 4, 6, 7, 8 - HxCDF pg 0.76 0.77 0.53 0.69

1, 2, 3, 7, 8, 9 - HxCDF pg 0.88 0.88 0.61 0.79

1, 2, 3, 4, 6, 7, 8 - HpCDF pg 1.42 0.60 1.40 1.14

1, 2, 3, 4, 7, 8, 9 - HpCDF pg 1.7 0.74 0.61 1.0

OCDF pg 3.3 1.3 1.3 2.0

Other - TCDD pg 1.6 5.4 3.4 3.5

Other - PeCDD pg 1.5 7.4 4.4 4.4

Other - HxCDD pg 1.8 1.7 12.4 5.3

Other - HpCDD pg 13.8 1.3 13.2 9.4

Other - TCDF pg 1.2 1.6 2.9 1.9

Other - PeCDF pg 0.84 0.92 0.74 0.83 

Other - HxCDF pg 0.88 0.88 0.61 0.79

Other - HpCDF pg 1.5 0.74 1.5 1.2

Total Dioxans pg 252.4 270.1 263.8 262.1

Total Furans pg 16.9 5.4 7.0 9.8

Total Dioxans and Furans pg 269.3 275.5 270.8 271.9

Indicates values below the detection limit (BDL).

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 64 of 215
Client:

Source: Press Dryer 10 (DC-10)

Formulas Symbol Units Calculated Data QC'd by: Keith Poole

Run Numbers - - 1 2 3AVERAGE

Test Date(s) - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0735-1139 1255-1700 0735-1138 -

1. Stack Pressure = Pbar + Pg / 13.6 Ps in. Hg 29.74 29.74 30.06 29.84

2. Meter Pressure = Pbar + DH / 13.6 Pm in. Hg 29.87 29.86 30.18 29.97

3. Standard Meter Volume = 17.64* Y* (Vm/Tm)* (Pbar + DH / 13.6) Vm(std) dscf 170.291 164.621 166.610 167.174

4a. Standard Volume of Water Vapor Condensed =0.04706*Wimp Vwc(std) scf 16.560 19.210 20.382 18.717

4b. Standard Volume of Water Collected in Silica Gel =0.04715*Wsg Vwsg(std) scf 2.032 1.829 1.679 1.847

5. Moisture Fraction =(Vwc(std) + Vwsg(std))/(Vwc(std) + Vwsg(std) + Vm(std)) Bws fraction 0.0984 0.1133 0.1169 0.1096

9. Molecular Weight of Stack Gas (dry) = 0.32*(O2)+ 0.44*(CO2)+0.28*(100-(O2)-(CO2)) Md lb / lb-mole 28.904 28.904 28.907 28.905

10. Molecular Weight of Stack Gas (wet) = Md*(1-Bws)+18.0*(Bws) Ms lb / lb-mole 27.831 27.668 27.632 27.710

11. Average Stack Gas Velocity = 85.49*Cp*(sqrt DP)avg*SQRT((Ts) / (Ps*Mw)) vs ft / s 32.944 32.23 32.18 32.45

12. Stack Gas Flow @ Actual Conditions = 60*vs*As Qa acfm 3,892 3,808 3,801 3,834

13. Stack Gas Flow @ Standard Conditions = Qa*(Tstd/Ts)*(Ps/Pstd) Qs scfm 3,018 2,928 2,971 2,972

14. Stack Gas Flow @ Dry Standard Conditions = Qa*(1-Bws)*(Tstd/Ts)*(Ps/Pstd) Qstd dscfm 2,721 2,597 2,623 2,647

15a. 2, 3, 7, 8 - TCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.27E-13 2.06E-13 1.39E-13 1.91E-13

15b. 1, 2, 3, 7, 8 - PeCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.45E-13 1.53E-13 1.39E-13 1.46E-13

15c. 1, 2, 3, 4, 7, 8 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.63E-13 1.59E-13 1.20E-13 1.48E-13

15d. 1, 2, 3, 6, 7, 8 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.45E-13 1.41E-13 1.11E-13 1.32E-13

15e. 1, 2, 3, 7, 8, 9 - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.54E-13 2.06E-13 1.85E-13 1.82E-13

15f 1 2 3 4 6 7 8 - HpCDD Concentrations =15 43*(m /10e12)/Vm(std) C gr / dscf 7 52E-13 9 75E-13 9 35E-13 8 87E-13

Description

Data Input By: Kevin Rosenberg

American Marazzi Tile, Inc. Job No.: 210269

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

15f. 1, 2, 3, 4, 6, 7, 8 - HpCDD Concentrations =15.43 (mn/10e )/Vm(std) Cs gr / dscf 7.52E-13 9.75E-13 9.35E-13 8.87E-13

15g. OCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.95E-11 2.18E-11 1.94E-11 2.03E-11

15h. 2, 3, 7, 8 - TCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.09E-13 1.50E-13 1.67E-13 1.42E-13

15i. 1, 2, 3, 7, 8 - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.61E-14 8.62E-14 6.85E-14 7.70E-14

15j. 2, 3, 4, 7, 8 - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.43E-14 8.44E-14 9.26E-14 8.38E-14

15k. 1, 2, 3, 4, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.34E-14 7.59E-14 5.19E-14 6.71E-14

15l. 1, 2, 3, 6, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 6.52E-14 6.84E-14 4.63E-14 6.00E-14

15m. 2, 3, 4, 6, 7, 8 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 6.89E-14 7.22E-14 4.91E-14 6.34E-14

15n. 1, 2, 3, 7, 8, 9 - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.97E-14 8.25E-14 5.65E-14 7.29E-14

15o. 1, 2, 3, 4, 6, 7, 8 - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.29E-13 5.62E-14 1.30E-13 1.05E-13

15p. 1, 2, 3, 4, 7, 8, 9 - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.54E-13 6.94E-14 5.65E-14 9.33E-14

15q. OCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.99E-13 1.22E-13 1.20E-13 1.80E-13

15r. Other - TCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.45E-13 5.08E-13 3.14E-13 3.22E-13

15s. Other - PeCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.35E-13 6.95E-13 4.03E-13 4.11E-13

15t. Other - HxCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.63E-13 1.59E-13 1.15E-12 4.90E-13

15u. Other - HpCDD Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.25E-12 1.22E-13 1.22E-12 8.65E-13

15v. Other - TCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.09E-13 1.50E-13 2.65E-13 1.75E-13

15w. Other - PeCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.61E-14 8.62E-14 6.85E-14 7.70E-14

15x. Other - HxCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 7.97E-14 8.25E-14 5.65E-14 7.29E-14

15y. Other - HpCDF Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.36E-13 6.94E-14 1.39E-13 1.15E-13

15z. Total Dioxans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.29E-11 2.53E-11 2.44E-11 2.42E-11

15aa. Total Furans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 1.53E-12 5.10E-13 6.49E-13 8.96E-13

15ab. Total Dioxans and Furans Concentrations =15.43*(mn/10e12)/Vm(std) Cs gr / dscf 2.44E-11 2.58E-11 2.51E-11 2.51E-11

20a. 2, 3, 7, 8 - TCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.50E-12 1.36E-12 8.86E-13 1.25E-12

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 65 of 215
Client:

Source: Press Dryer 10 (DC-10)

Formulas Symbol Units Calculated Data QC'd by: Keith Poole

Run Numbers - - 1 2 3AVERAGE

Test Date(s) - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0735-1139 1255-1700 0735-1138 -

Description

Data Input By: Kevin Rosenberg

American Marazzi Tile, Inc. Job No.: 210269

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

20b. 1, 2, 3, 7, 8 - PeCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 9.60E-13 1.01E-12 8.86E-13 9.52E-13

20c. 1, 2, 3, 4, 7, 8 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.08E-12 1.05E-12 7.68E-13 9.67E-13

20d. 1, 2, 3, 6, 7, 8 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 9.60E-13 9.31E-13 7.09E-13 8.66E-13

20e. 1, 2, 3, 7, 8, 9 - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.02E-12 1.36E-12 1.18E-12 1.19E-12

20f. 1, 2, 3, 4, 6, 7, 8 - HpCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.98E-12 6.45E-12 5.96E-12 5.80E-12

20g. OCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.29E-10 1.45E-10 1.24E-10 1.33E-10

20h. 2, 3, 7, 8 - TCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 7.20E-13 9.93E-13 1.06E-12 9.25E-13

20i. 1, 2, 3, 7, 8 - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.04E-13 5.71E-13 4.37E-13 5.04E-13

20j. 2, 3, 4, 7, 8 - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.92E-13 5.58E-13 5.91E-13 5.47E-13

20k. 1, 2, 3, 4, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.86E-13 5.03E-13 3.31E-13 4.40E-13

20l. 1, 2, 3, 6, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.32E-13 4.53E-13 2.95E-13 3.93E-13

20m. 2, 3, 4, 6, 7, 8 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 4.56E-13 4.78E-13 3.13E-13 4.15E-13

20n. 1, 2, 3, 7, 8, 9 - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.28E-13 5.46E-13 3.60E-13 4.78E-13

20o. 1, 2, 3, 4, 6, 7, 8 - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 8.52E-13 3.72E-13 8.27E-13 6.84E-13

20p. 1, 2, 3, 4, 7, 8, 9 - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.02E-12 4.59E-13 3.60E-13 6.13E-13

20q. OCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.98E-12 8.07E-13 7.68E-13 1.18E-12

20r. Other - TCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 9.60E-13 3.36E-12 2.00E-12 2.11E-12

20s Other - PeCDD concentration adjusted to 7% O2 20s. Other - PeCDD concentration adjusted to 7% O2 =Cs * ((20 9-7)/(20 9-%O2)) ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc gr / dscfc 8 94E-13 8.94E-13 4 60E-12 4.60E-12 2 57E-12 2.57E-12 2 69E-12 2.69E-12

20t. Other - HxCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.08E-12 1.05E-12 7.32E-12 3.15E-12

20u. Other - HpCDD concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 8.28E-12 8.07E-13 7.79E-12 5.63E-12

20v. Other - TCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 7.20E-13 9.93E-13 1.69E-12 1.13E-12

20w. Other - PeCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.04E-13 5.71E-13 4.37E-13 5.04E-13

20x. Other - HxCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 5.28E-13 5.46E-13 3.60E-13 4.78E-13

20y. Other - HpCDF concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 9.00E-13 4.59E-13 8.86E-13 7.48E-13

20z. Total Dioxans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.51E-10 1.68E-10 1.56E-10 1.58E-10

20aa. Total Furans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.01E-11 3.38E-12 4.14E-12 5.88E-12

20ab. Total Dioxans and Furans concentration adjusted to 7% O2 =Cs * ((20.9-7)/(20.9-%O2)) c%O2 gr / dscfc 1.61E-10 1.71E-10 1.60E-10 1.64E-10

21a. 2, 3, 7, 8 - TCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.28E-12 4.59E-12 3.12E-12 4.33E-12

21b. 1, 2, 3, 7, 8 - PeCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.38E-12 3.40E-12 3.12E-12 3.30E-12

21c. 1, 2, 3, 4, 7, 8 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.80E-12 3.55E-12 2.71E-12 3.35E-12

21d. 1, 2, 3, 6, 7, 8 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.38E-12 3.13E-12 2.50E-12 3.00E-12

21e. 1, 2, 3, 7, 8, 9 - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.59E-12 4.59E-12 4.16E-12 4.12E-12

21f. 1, 2, 3, 4, 6, 7, 8 - HpCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.75E-11 2.17E-11 2.10E-11 2.01E-11

21g. OCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 4.54E-10 4.86E-10 4.37E-10 4.59E-10

21h. 2, 3, 7, 8 - TCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.54E-12 3.34E-12 3.75E-12 3.21E-12

21i. 1, 2, 3, 7, 8 - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.77E-12 1.92E-12 1.54E-12 1.75E-12

21j. 2, 3, 4, 7, 8 - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.73E-12 1.88E-12 2.08E-12 1.90E-12

21k. 1, 2, 3, 4, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.71E-12 1.69E-12 1.17E-12 1.52E-12

21l. 1, 2, 3, 6, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.52E-12 1.52E-12 1.04E-12 1.36E-12

21m. 2, 3, 4, 6, 7, 8 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.61E-12 1.61E-12 1.10E-12 1.44E-12

21n. 1, 2, 3, 7, 8, 9 - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.86E-12 1.84E-12 1.27E-12 1.66E-12

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Client:

Source: Press Dryer 10 (DC-10)

Formulas Symbol Units Calculated Data QC'd by: Keith Poole

Run Numbers - - 1 2 3AVERAGE

Test Date(s) - - 12/02/10 12/02/10 12/03/10 All Runs

Times, Pollutant Runs (Began - Ended) - Military Time 0735-1139 1255-1700 0735-1138 -

Description

Data Input By: Kevin Rosenberg

American Marazzi Tile, Inc. Job No.: 210269

ENTEC Services, Inc.

30 Monroe Drive, Pelham, AL 35124

CALCULATED TEST DATA - English Units

21o. 1, 2, 3, 4, 6, 7, 8 - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.00E-12 1.25E-12 2.92E-12 2.39E-12

21p. 1, 2, 3, 4, 7, 8, 9 - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.59E-12 1.54E-12 1.27E-12 2.14E-12

21q. OCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 6.97E-12 2.71E-12 2.71E-12 4.13E-12

21r. Other - TCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.38E-12 1.13E-11 7.06E-12 7.25E-12

21s. Other - PeCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.15E-12 1.55E-11 9.06E-12 9.22E-12

21t. Other - HxCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.80E-12 3.55E-12 2.58E-11 1.11E-11

21u. Other - HpCDD Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.92E-11 2.71E-12 2.75E-11 1.98E-11

21v. Other - TCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 2.54E-12 3.34E-12 5.96E-12 3.94E-12

21w. Other - PeCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.77E-12 1.92E-12 1.54E-12 1.75E-12

21x. Other - HxCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 1.86E-12 1.84E-12 1.27E-12 1.66E-12

21y. Other - HpCDF Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.17E-12 1.54E-12 3.12E-12 2.61E-12

21z. Total Dioxans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.33E-10 5.63E-10 5.49E-10 5.49E-10

21aa. Total Furans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 3.56E-11 1.13E-11 1.46E-11 2.05E-11

21ab. Total Dioxans and Furans Mass Emissions = (60/7000)*cs*Qsd PMR lbs / hr 5.69E-10 5.75E-10 5.64E-10 5.69E-10

22. Volume collected through nozzle =Ts/Ps*[0.002669*Vlc+ Vm*Y*Pm/Tm] Vn acf 243.514 241.338 241.362 242.071

24. Isokinetic Sampling Rate, Percent = 100*Vn / (60*vs*An*q) I % 104.57 105.93 106.12 105.54

Post Meter Orifice Cal. (EMC ALT-009 Yqa) yqa 0.9795 0.9625 0.9697 0.971

% Difference, (Calibration must be within 5% of original Y-factor) 3.14%

Indicates values below the detection limit (BDL).

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Sunnyvale, TX

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December 2-3, 6-7, 2010

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Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

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this report.

American Marazzi Tile, Inc. 

Sunnyvale, TX

Project No. 210269 Tile MACT ICR Testing 

December 2-3, 6-7, 2010

Report Appendix Page 215 of 215