Name of Method:

Organization ID No. (as in ASTM D XXXX-XX):

Laboratory Name:

Laboratory Street Address:

Laboratory City:

Laboratory State:

Laboratory Zip code:

Laboratory Contact Person:

Laboratory Contact Phone Number

Laboratory Contact Facsimile Number

Laboratory Contact E-mail Address

Is 1,000 ppm Sulfur Precision Criterion Met?

standard deviation

Laboratory Test Identification Number Date Time Test Result 

(ppm)

REQUIRED DATA MISSING

Confidential Business Information Claim. A company may assert a business confidentiality claim covering 

the information contained in this submission. If no such claim is made the information may be made 

available to the public by EPA without further notice. All questions of confidentiality will be handled 

pursuant to 40 CFR Part 2. Is confidentiality claimed for the information in this submission? (Note: 

Please answer by typing "Yes" or "No" in the adjacent cell.)

1,000 ppm Sulfur Precision Criterion - a standard deviation less than 18.07 ppm, computed from the results of a minimum 

tests made over 20 days on samples taken from a single homogenous commerically available ECA Marine fuel with a sulfur r

1,000 ppm. The 20 results must be a series of tests with a sequential record of the analyses and no omissions. A lab facility 

given sample or test result only if the exclusion is for a valid reason under good laboratory practices and it maintains records 

sample and test results and the reason for excluding them.

1,000 ppm ECA Marine Fuel Sulfur Precision Demonstration [ECA0300 (insert form number):OMB # 2060-0308 Expire

REQUIRED DATA MISSING

Test Method

Laboratory Identification

Data Entry QC Check on Test 

Result

DATA REQUIRED IN CELL D20

DATA REQUIRED IN CELL D21

DATA REQUIRED IN CELL D22

DATA REQUIRED IN CELL D23

DATA REQUIRED IN CELL D24

DATA REQUIRED IN CELL D25

DATA REQUIRED IN CELL D26

DATA REQUIRED IN CELL D27

DATA REQUIRED IN CELL D28

DATA REQUIRED IN CELL D29

DATA REQUIRED IN CELL D30

DATA REQUIRED IN CELL D31

DATA REQUIRED IN CELL D32

from the results of a minimum of 20 repeat 

ECA Marine fuel with a sulfur range of 700 to 

nd no omissions. A lab facility may exclude a 

ctices and it maintains records regarding the 

ber):OMB # 2060-0308 Expires 1/31/2016]
DATA REQUIRED IN CELL D33

DATA REQUIRED IN CELL D34

DATA REQUIRED IN CELL D35

DATA REQUIRED IN CELL D36

DATA REQUIRED IN CELL D37

DATA REQUIRED IN CELL D38

DATA REQUIRED IN CELL D39
1,000 ppm ECA Marine Fuel Sulfur Accuracy Demonstration [ECA0300 (insert EPA External form number):OMB # 2060

Name of Method:

Organization ID No. (as in ASTM D XXXX-XX):

Laboratory Name:

Laboratory Street Address:

Laboratory City:

Laboratory State:

Laboratory Zip code:

Laboratory Contact Person:

Laboratory Contact Phone Number

Laboratory Contact Facsimile Number

Laboratory Contact E-mail Address

Is 300-400 ppm Sulfur Accuracy Criterion 

Met?

Arithmetic Average (ppm)

Vendor Name of Gravimetric Standard

Lot Identification Number of Gravimetric 

Standard

Accepted Reference Value (ARV) of 

Gravimetric Standard (ppm)

Difference between Arithmetic Average and 

ARV of Gravimetric Standard

Laboratory Test Identification Number Date Time

Test 

Result 

(ppm)

300 to 400 ppm Accuracy Criterion - the arithmetic average of a continuous series of at least 10 tests performed on a 

commercially available gravimetric sulfur standard in the range of 300 to 400 ppm sulfur shall not differ from the accepted 

reference value (ARV) of that standard by more than 13.55 ppm. Individual test results shall be compensated for any known 

chemical interferences.

REQUIRED DATA MISSING

REQUIRED DATA MISSING

REQUIRED DATA MISSING

gravimetric sulfur standard

Test Method

0

0

Laboratory Identification

0

0

0

0

Confidential Business Information Claim. A company may assert a business confidentiality claim covering the information cont

claim is made the information may be made available to the public by EPA without further notice. All questions of confidentiality 

Part 2. Is confidentiality claimed for the information in this submission? (Note: Please answer by typing "Yes" or "No" in the ad

0

0

0

0

0

Accuracy Criterion for 300-400 ppm

Is 900-1,000 ppm Sulfur 

Accuracy Criterion Met?

Arithmetic Average (ppm)

Vendor Name of 

Gravimetric Standard

Concentration QC Check on ARV Lot Identification Number 

of Gravimetric Standard

ARV TOO LOW IN CONCENTRATION

Accepted Reference Value 

(ARV) of Gravimetric 

Standard (ppm)

Difference between 

Arithmetic Average and 

ARV of Gravimetric 

Standard

Data Entry QC Check on Test Result Laboratory Test 

Identification Number Date Time

DATA REQUIRED IN CELL D26

DATA REQUIRED IN CELL D27

us series of at least 10 tests performed on a 

0 ppm sulfur shall not differ from the accepted 

 test results shall be compensated for any known 

900 to 1,000 ppm Accuracy Criterion - the arithmetic average of a contin

tests performed on a commercially available gravimetric sulfur standard in 

sulfur shall not differ from the accepted reference value (ARV) of that stan

Individual test results shall be compensated for any known chemical interfe

REQUIRED DATA MISSING

REQUIRED DATA MISSING

REQUIRED DATA MISSING

gravimetric sulfur standard

Accuracy Criterion for 900-1,000 ppm

ss confidentiality claim covering the information contained in this submission. If no such 

without further notice. All questions of confidentiality will be handled pursuant to 40 CFR 

ote: Please answer by typing "Yes" or "No" in the adjacent cell.)
DATA REQUIRED IN CELL D28

DATA REQUIRED IN CELL D29

DATA REQUIRED IN CELL D30

DATA REQUIRED IN CELL D31

DATA REQUIRED IN CELL D32

DATA REQUIRED IN CELL D33

DATA REQUIRED IN CELL D34

DATA REQUIRED IN CELL D35
Concentration QC Check on ARV

ARV TOO LOW IN 

CONCENTRATION

Test 

Result 

(ppm)

Data Entry QC Check on Test 

Result

DATA REQUIRED IN CELL J26

DATA REQUIRED IN CELL J27

 arithmetic average of a continuous series of at least 10 

 gravimetric sulfur standard in the range of 900 to 1000 ppm 

rence value (ARV) of that standard by more than 13.55 ppm. 

 for any known chemical interferences.

D DATA MISSING

D DATA MISSING

D DATA MISSING
DATA REQUIRED IN CELL J28

DATA REQUIRED IN CELL J29

DATA REQUIRED IN CELL J30

DATA REQUIRED IN CELL J31

DATA REQUIRED IN CELL J32

DATA REQUIRED IN CELL J33

DATA REQUIRED IN CELL J34

DATA REQUIRED IN CELL J35
 OMB Control Number: 2060-0308

Name of Method:

Organization ID No. (as in ASTM D XXXX-XX):

Laboratory Name:

Laboratory Street Address:

Laboratory City:

Laboratory State:

Laboratory Zip code:

Laboratory Contact Person:

Laboratory Contact Phone Number

Laboratory Contact Facsimile Number

Laboratory Contact E-mail Address

No

Is 15 ppm Sulfur Precision Criterion Met?

standard deviation

Laboratory Test Identification Number Date Time Test Result 

(ppm)

Data Entry QC Check on Test 

Result

######### 1/26/2013 8:00 AM 755.000 OK

######### 1/27/2013 8:00 AM 780.000 OK

######### 1/28/2013 8:00 AM 765.000 OK

######### 1/29/2013 8:00 AM 750.000 OK

######### 1/30/2013 8:00 AM 745.000 OK

######### 2/1/2013 8:00 AM 760.000 OK

######### 2/2/2013 8:00 AM 763.000 OK

######### 2/3/2013 8:00 AM 772.000 OK

######### 2/5/2013 8:00 AM 749.000 OK

######### 2/6/2013 8:00 AM 730.000 OK

######### 2/7/2013 8:00 AM 740.000 OK

######### 2/8/2013 8:00 AM 760.000 OK

######### 2/9/2013 8:00 AM 745.000 OK

######### 2/10/2013 8:00 AM 750.000 OK

######### 2/11/2013 8:00 AM 756.000 OK

######### 2/12/2013 8:00 AM 763.000 OK

######### 2/13/2013 8:00 AM 765.000 OK

######### 2/14/2013 8:00 AM 763.000 OK

######### 2/15/2013 8:00 AM 777.000 OK

######### 2/16/2013 8:00 AM 750.000 OK

EPA External No. 5900-352

202-343-2801

sopata.joe@epa.gov

PASSED

12.42

Confidential Business Information Claim. A company may assert a business 

confidentiality claim covering the information contained in this submission. If no such 

claim is made the information may be made available to the public by EPA without 

further notice. All questions of confidentiality will be handled pursuant to 40 CFR Part 2. 

Is confidentiality claimed for the information in this submission? (Note: Please answer 

by typing "Yes" or "No" in the adjacent cell.)

1,000 ppm Sulfur Precision Criterion - a standard deviation less than 18.07 ppm, computed from the results of a minimum 

of 20 repeat tests made over 20 days on samples taken from a single homogenous commerically available ECA Marine fuel 

with a sulfur range of 700 to 1,000 ppm. The 20 results must be a series of tests with a sequential record of the analyses 

and no omissions. A lab facility may exclude a given sample or test result only if the exclusion is for a valid reason under 

good laboratory practices and it maintains records regarding the sample and test results and the reason for excluding them.

202-343-9034

1,000 ppm ECA Marine Fuel Sulfur Precision Demonstration [ECA030] Expires 1/31/2016

Test Method

Standard Test Method for Sulfur in Petroleum Products by Wavelength 

ASTM D2622-10

Laboratory Identification

USEPA National and Vehicle Fuels Emissions Laboratory/OAR

2565 Plymouth Road, Mailcode AATSG

Ann Arbor

Michigan

48105

Joe Sopata
1,000 ppm ECA Marine Fuel Sulfur Accuracy Demonstration [ECA0300 (insert EPA external form number):OMB # 2060

Name of Method:

Organization ID No. (as in ASTM D XXXX-XX):

Laboratory Name:

Laboratory Street Address:

Laboratory City:

Laboratory State:

Laboratory Zip code:

Laboratory Contact Person:

Laboratory Contact Phone Number

Laboratory Contact Facsimile Number

Laboratory Contact E-mail Address

Is 300-400 ppm Sulfur Accuracy Criterion 

Met?

Arithmetic Average (ppm)

Vendor Name of Gravimetric Standard

Lot Identification Number of Gravimetric 

Standard

Accepted Reference Value (ARV) of 

Gravimetric Standard (ppm)

Difference between Arithmetic Average and 

ARV of Gravimetric Standard

Laboratory Test Identification Number Date Time Test Result 

(ppm)

######### 1/28/2013 8:00 AM 352.000

ALDS45678

350.00

2

PASSED

352.00

NIST

sopata.joe@epa.gov

Accuracy Criterion for 300-400 ppm

gravimetric sulfur standard

Confidential Business Information Claim. A company may assert a business confidentiality claim covering the information cont

submission. If no such claim is made the information may be made available to the public by EPA without further notice. All qu

confidentiality will be handled pursuant to 40 CFR Part 2. Is confidentiality claimed for the information in this submission? (Not

typing "Yes" or "No" in the adjacent cell.)

300 to 400 ppm Accuracy Criterion - the arithmetic average of a continuous series of at least 10 tests performed 

on a commercially available gravimetric sulfur standard in the range of 300 to 400 ppm sulfur shall not differ from the 

accepted reference value (ARV) of that standard by more than 13.55 ppm. Individual test results shall be 

compensated for any known chemical interferences.

202-343-2801

Test Method

Standard Test Method for Sulfur in Petroleum Products by Wavelength Dispers

ASTM D2622-10

Laboratory Identification

USEPA National and Vehicle Fuels Emissions Laboratory/OAR

2565 Plymouth Road, Mailcode AATSG

Ann Arbor

Michigan

48105

Joe Sopata

202-343-9034
######### 1/28/2013 8:30 AM 354.000

######### 1/28/2013 9:00 AM 350.000

######### 1/28/2013 9:30 AM 348.000

######### 1/28/2013 10:00 AM 340.000

######### 1/28/2013 10:30 AM 360.000

######### 1/28/2013 11:00 AM 356.000

######### 1/28/2013 11:30 AM 357.000

######### 1/28/2013 12:00 PM 352.000

######### 1/28/2013 12:30 PM 351.000
No

Is 900-1000 ppm Sulfur 

Accuracy Criterion Met?

Arithmetic Average (ppm)

Vendor Name of 

Gravimetric Standard

Concentration QC Check on ARV Lot Identification Number 

of Gravimetric Standard

OK

Accepted Reference Value 

(ARV) of Gravimetric 

Standard (ppm)

Difference between 

Arithmetic Average and 

ARV of Gravimetric 

Standard

Data Entry QC Check on Test 

Result

Laboratory Test 

Identification Number Date Time

Test 

Result 

(ppm)

OK ######### 1/29/2013 8:00 AM 960.000

ALDS53478

950.00

1.7

PASSED

951.70

NIST

Accuracy Criterion for 900-1000 ppm

gravimetric sulfur standard

usiness confidentiality claim covering the information contained in this 

vailable to the public by EPA without further notice. All questions of 

iality claimed for the information in this submission? (Note: Please answer by

ntinuous series of at least 10 tests performed 

f 300 to 400 ppm sulfur shall not differ from the 

ppm. Individual test results shall be 

900 to 1000 ppm Accuracy Criterion - the arithmetic average of a continuous series 

10 tests performed on a commercially available gravimetric sulfur standard in the rang

to 1000 ppm sulfur shall not differ from the accepted reference value (ARV) of that sta

more than 13.55 ppm. Individual test results shall be compensated for any known che

interferences.

 for Sulfur in Petroleum Products by Wavelength Dispersive X-ray Fluorescence 

Vehicle Fuels Emissions Laboratory/OAR

Mailcode AATSG
OK ######### 1/29/2013 8:30 AM 940.000

OK ######### 1/29/2013 9:00 AM 942.000

OK ######### 1/29/2013 9:30 AM 962.000

OK ######### 1/29/2013 10:00 AM 953.000

OK ######### 1/29/2013 10:30 AM 957.000

OK ######### 1/29/2013 11:00 AM 949.000

OK ######### 1/29/2013 11:30 AM 950.000

OK ######### 1/29/2013 12:00 PM 956.000

OK ######### 1/29/2013 12:30 PM 948.000
Concentration QC Check on ARV

OK

Data Entry QC Check on Test 

Result

OK

metic average of a continuous series of at least 

ravimetric sulfur standard in the range of 900 

ed reference value (ARV) of that standard by

 be compensated for any known chemical 
OK

OK

OK

OK

OK

OK

OK

OK

OK