Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

4072 Pulliam 8 

### subbituminous

### Fuel Type 2 Fuel Type 3 Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte



### 4072 Pulliam 8 As Received Higher Heating Value 

### 4072 Pulliam 8 As Received % Moisture 

### 4072 Pulliam 8 As Received % Ash 

### 4072 Pulliam 8 As Received % Sulfur 

### 4072 Pulliam 8 Dry basis Higher Heating Value 

### 4072 Pulliam 8 Dry basis % Ash 

### 4072 Pulliam 8 Dry basis % Sulfur 

### 4072 Pulliam 8 Dry basis Antim ony 

### 4072 Pulliam 8 Dry basis Arsenic 

### 4072 Pulliam 8 Dry basis Bery llium 

### 4072 Pulliam 8 Dry basis Cadmium 

### 4072 Pulliam 8 Dry basis Chlorine 

### 4072 Pulliam 8 Dry basis Chromium 

### 4072 Pulliam 8 Dry basis Cobalt 

### 4072 Pulliam 8 Dry basis Fluorine 

### 4072 Pulliam 8 Dry basis Lead 

### 4072 Pulliam 8 Dry basis Manganese 

### 4072 Pulliam 8 Dry basis Mercury 

### 4072 Pulliam 8 Dry basis Nickel 

### 4072 Pulliam 8 Dry basis Selenium

### An alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865-07

ASTM D4239 ASTM D5865-07

ASTM D4239 ASTM D6357, ASTM D5987 ASTM D6357, ASTM D5987 ASTM D6357, ASTM D5987 ASTM D6357, ASTM D5987 ASTM D6721 ASTM D6357, ASTM D5987 ASTM D6357, ASTM D5987 ASTM D5987 ASTM D6357, ASTM D5987 ASTM D6357, ASTM D5987 ASTM D6722 ASTM D6357, ASTM D5987 ASTM D6357, ASTM D5987EIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

### 4072 Pulliam 8 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Run 1 (20101711) 

### 4/6/2010 4/6/2010 8339.00 Btu/lb Run 2 (20101712) 4/7/2010 4/7/2010 8477.00 Btu/lb Run 3 (20101713) 4/8/2010 4/8/2010 8407.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.94 4.66 0.32 11903 Btu/lb 6.65 0.46 28.79 4.51 0.21 11904 Btu/lb 6.34 0.3 29.32 4.44 0.2 11894 Btu/lb 6.28 0.29Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 37 ppm 0.068 μg/g 0.202 μg/g 1.4 μg/g 0.244 20 ppm 0.082 μg/g 0.154 μg/g 1.08 μg/g 0.257 17 ppm 0.072 μg/g 0.131 μg/g 0.941 μg/g 0.252Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g 0.0832 μg/g 4.98 μg/g 2.66 μg/g 23.5 μg/g μg/g 0.0718 μg/g 3.92 μg/g 2.69 μg/g 10.7 μg/g μg/g 0.0745 μg/g 3.79 μg/g 2.82 μg/g 9.05 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 4.8 μg/g <1 μg/g 68.2 ppm 1.72 μg/g 29.94 3.81 μg/g <1 μg/g 69.4 ppm 1.69 μg/g 28.79 3.61 μg/g <1 μg/g 75.5 ppm 1.65 μg/g 29.32 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 52.61 6.65 40.74 67.42 3.93 1.5 0.46 52.03 6.34 41.63 67.41 3.71 1.45 0.3 51.94 6.28 41.78 68.11 3.94 1.37 0.29 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 20.04 20.79 20.01EIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

### 4072 Pulliam 8 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 

### Run 1 (20101711) 

### 4/6/2010 4/6/2010 8339.00 Btu/lb Run 2 (20101712) 4/7/2010 4/7/2010 8477.00 Btu/lb Run 3 (20101713) 4/8/2010 4/8/2010 8407.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.94 4.66 0.32 11903 Btu/lb 6.65 0.46 28.79 4.51 0.21 11904 Btu/lb 6.34 0.3 29.32 4.44 0.2 11894 Btu/lb 6.28 0.29Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 37 ppm 0.068 μg/g 0.202 μg/g 1.4 μg/g 0.244 20 ppm 0.082 μg/g 0.154 μg/g 1.08 μg/g 0.257 17 ppm 0.072 μg/g 0.131 μg/g 0.941 μg/g 0.252Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g 0.0832 μg/g 4.98 μg/g 2.66 μg/g 23.5 μg/g μg/g 0.0718 μg/g 3.92 μg/g 2.69 μg/g 10.7 μg/g μg/g 0.0745 μg/g 3.79 μg/g 2.82 μg/g 9.05 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 4.8 μg/g <1 μg/g 68.2 ppm 1.72 μg/g 3.81 μg/g <1 μg/g 69.4 ppm 1.69 μg/g 3.61 μg/g <1 μg/g 75.5 ppm 1.65 μg/g

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 29.94 52.61 6.65 40.74 67.42 3.93 1.5 0.46 28.79 52.03 6.34 41.63 67.41 3.71 1.45 0.3 29.32 51.94 6.28 41.78 68.11 3.94 1.37 0.29 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 20.04 20.79 20.01EIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

### 4072 Pulliam 8 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Run 1 (20101714) 

### 4/9/2010 4/9/2010 8348.00 Btu/lb Run 2 (20101715) 4/9/2010 4/9/2010 8399.00 Btu/lb Run 3 (20101716) 4/9/2010 4/9/2010 8485.00 Btu/lb Run 2 (20101717) 4/10/2010 4/10/2010 8214.00 Btu/lb Run 3 (20101718) 4/10/2010 4/10/2010 8243.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 29.81 4.49 0.23 11894 Btu/lb 6.39 0.33 29.62 4.41 0.24 11934 Btu/lb 6.27 0.34 28.92 4.43 0.25 11937 Btu/lb 6.23 0.35 30.64 5.09 0.32 11842 Btu/lb 7.34 0.46 30.21 5.23 0.36 11811 Btu/lb 7.5 0.51Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 29.81 29.62 28.92 30.64 30.21 Proximate Analy

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 50.32 6.39 43.29 68.05 3.81 1.36 0.33 20.06 51.44 6.27 42.29 67.3 3.84 1.31 0.34 20.94 51.04 6.23 42.73 68.12 3.81 1.17 0.35 20.32 52.18 7.34 40.48 67.34 3.95 1.15 0.46 19.76 53.31 7.5 39.19 66.88 3.99 1.15 0.51 19.97 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HAPs Test Group 

### 4072 Pulliam 8

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm