### Ony xEnvironmenta l Service s Sauget , Illmoi s «



# Evaluationo

f Metals , an

d PCDD/PCD F Emission s for Incinerator

s 2and4

ENS R Corporatio n Januar y2004 Documen tNumbe r10002-008-10 0

### E N H
CONTENT S
1. 0 INTRODUCTIO N 1- 1 1. 1 Progra m Summar y1- 1 1. 2 Fiel d Progra m Schedul e 1- 1
2. 0 SUMMAR YO FRESULT S 2- 1 2. 1 Introductio n 2- 1 2. 2 Stac k

Emissio n Result s fo rUnit4 , Conditio n 1 2- 1 2. 3 Stac k

Emissio n Result s fo rUnit4 , Conditio n 2 2- 1 2. 4 Stac k

Emissio n Result s fo rUni t2 2- 2 3. 0 SAMPLIN G AN D ANALYTICA LPROCEDURE S 3- 1 3. 1 Samplin g Procedure s 3- 1 3.1. 1 Velocity , Moistur e an d Fixe d Ga s Determination s 3- 1 3.1. 2 PCDD/PCD FSamplin g 3- 1 3.1. 3 Metal s Samplin g .3- 1 3. 2 Analytica l Procedure s 3- 2 3.2. 1 PCDD/PCD FAnalyse s .. . 3- 2 3.2. 2 Metal s Analyse s 3- 2
4. 0 QUALIT YASSURANC E 4- 1 4. 1 Introductio n 4- 1 4. 2 Stac k

Samplin g QA/Q C 4- 1 4. 3 Chain-of-Custod y4- 2 4. 4 Analytica l QA/Q C 4- 2 4.4. 1 Analysi s fo rMetal s 4- 2 4.4. 2 Analysi s fo rPCDDs/PCDF s 4- 3

C:\Document s an d Settirtgs\cdoolittle\M

yDocuments\Onyx\090

3 testing\Ony xj 1 

### January , 200 4 090 3 data\090 3 Ony xTes tProgram.do c

### CONTENT S - CONTINUE D

APPENDICE S
A- Fiel d Dat aSheet s B - Proces s Fee d an d Operatin g Condition s C - Fiel d Equipmen tCalibratio n Form s D - Analytica l Dat aReport s

C:\Document s an d Settings\cdoolittle\M

yDocuments\Onyx\090

3 teslinglOny x090 3 j j data\090 3 Ony xTes tProgranrudo c January , 200 4m m . 

### LIS TO FTABLE S
Tabl e 2- 1 Summar yo fPCDD/PCD FEmission s fo rUni t4 , Conditio n 1 , TE Q Basi s 2- 3 Tabl e 2- 2 Summar yo fMetal s Emission s fo rUnit4 , Conditio n 1 -Targe tMetal s 2- 4 Tabl e 2- 3 Summar yo fPCDD/PCD FEmission s fo rUni t4 , Conditio n 2 , TE Q Basi s 2- 6 Tabl e 2- 4 Summar yo fMetal s Emission s fo rUni t4 , Conditio n 2 -Targe tMetal s 2- 7 Tabl e 2- 5 Summar yo fPCDD/PCD FEmission s fo rUni t2 , TE Q Basi s 2- 9 Tabl e 2- 6 Summar yo fMetal s Emission s fo rUnit2 -Targe tMetal s 2-1 0

C:\Doojmen s an d Settings\aJoolittle\M

yDocuments\Onyx\090

3 testing\Ony x 090 3 dala\090 3 Ony xTes tProgram.do c ii i January , 200 4mrERNAT/OAIAL


### 1. 0 INTRODUCTIO N

1. 1 Progra m Summar y ENS R Internationa l wa s retaine d b yOny xEnvironmenta l Services , Sauget , Illinoi s t o conduc t stac k ga s emissio n samplin g durin g th e wee k o fSeptembe r15 , 2003 , o n tw o incinerator s a tth e facility
. Th e Uni t4 tes tprogra m wa s intende d to evaluat e incinerato rperformanc e whil e varyin g th e mercur yan d powdere d activate d carbo n feedrates
. Therefore , Uni t4 wa s teste d unde rtw o separat e operatin g conditions , alow-mercury/low-carbo n feedrat e conditio n an d ahigh mercury/high-carbo n feedrat e condition
. Fo rth e firs tUni t4 tes tconditio n (Mod e 1) , mercur ywa s fe d a t0.05 5 Ibs/h ran d 6 Ibs/h rfo ractivate d carbon
. Fo rth e secon d Uni t4 tes tcondition , mercur y wa s fe d a t0.18 6 Ibs/h ran d 2 0 Ibs/h rfo ractivate d carbon
. Uni t2 an d Uni t4 wer e bot h teste d fo rdioxin s an d furan s i n accordanc e wit h EP AMetho d 0023 , an d si x(6 ) metals 1 

### i n accordanc e wit h EP AMetho d 29
. Stac k flow s wer e determine d b ypito t tube/wate rmanomete ra s parto fth e actua l samplin g process . Stac k moistur e wa s determine d b y measurin g th e volum e gaine d i n th e samplin g trai n durin g sampling
. Oxyge n an d carbo n dioxid e wer e determine d b ycollectin g aTedia rba g sampl e followe d b yORSA Tanalysis
. Metho d 0023 Asample s wer e labeled , package d an d shippe d followin g accepte d protocol s t o Alt a Analytical , E l Dorad o Hills , C Afo rth e dioxi n an d fura n analysis
. Metho d 2 9 sample s wer e labeled , package d an d shippe d followin g accepte d protocol s t o Sever n &Tren tLaboratorie s o f Sacramento , CA
. I n additio n t o progra m samples , ENS R prepare d tw o fiel d blank s fo ranalysis , on e fo reac h sampl e train
. 1. 2 Fiel d Progra m Schedul e Th e tes twa s complete d ove rafive-da ytim e fram e a s follows : Septembe r1 5 - Trave l t o th e sit e an d se tu p o n stac k o fUni t4 ; Septembe r1 6 - Complete d Ru n 1 &2 o n Uni t4 Conditio n 1 ; Septembe r1 7 - Complete d Ru n 3 o n Uni t4 Conditio n 1 , an d Run s 2 &3 , o n Uni t4 , Conditio n 2 ; Septembe r1 6 - Complete d Ru n 3 o n Uni t4 Conditio n 2 , an d Ru n 1 onTJni t2 ; Septembe r1 9 - Complete d Ru n 2 &3 o n Uni t2 , prepare d sample s fo rshipment , departe d site
.

1 Thes e metal s included : arsenic , beryllium , cadmium , chromium , lead , an d mercury .



### C:\Documenl s an d Setinos\cdot>Iitte\M

yDocuments\Onyx\090

3 testing\Ony x090 3 data\090 3 Ony xTes tProgram.do c 1- 1 January , 200 4

### ENSR
. /HTERHJir/ONAL 

### 2. 0 SUMMAR YO FRESULT S

2. 1 Introductio n Thi s sectio n summarize s the tes tprogra m results
. Th e dat apresente d her e include s only , stac k emission s data
. Wast e fee d an d proces s dat arelate d t o thi s progra m ar e include d i n Appendi xB o f thi s report
. 2. 2 Stac k

Emissio n Result s fo rUni t4 , Conditio n 1 Asummar yo fth e PCDD/PCD Fan d Metal s emissio n result s fo rUnit s 4 , Conditio n 1 ar e include d i n Table s 2- 1 an d 2-2 , respectively
. Thes e result s indicat e that : Th e PCDD/PCD Femission s fo rUni t4 , Conditio n 1 (averag e emission s fo rth e thre e tes tru n se t wer e 0.0 5 ng/m 3 

### ) ar e belo wthe HW C MAC Temissio n standar d o f0. 2 ng/m 3

### (correcte d t o 7 % 0 2 

### ) ; Th e LV M an d SV M metal s emission s fo rUni t4 , Conditio n 1 (averag e emission s fo rth e thre e tes t ru n se twer e <3 1 pg/m 3

### fo rLVM s an d 19 9 pg/m 3

### fo rSVMs ) wer e lowe rtha n th e ne wHW C MAC T emissio n standard s o f9 7 pg/m 3

### an d 24 0 pg/m 3

### (correcte d t o 7 % 0 2 

### ) fo rLVM s an d SVM s respectively ;
« Th e mercuryemission s fo rUnit4 , Conditio n 1 (averag e fo rth e thre e tes tru n se twer e 26 7 pg/m 3 

### ) wer e highe rtha n the ne wHW C MAC Temissio n standar d o f13 0 pg/m 3


### . 2. 3 Stac k

Emissio n Result s fo rUni t4 , Conditio n 2 Asummar yo fth e PCDD/PCD Fan d Metal s emissio n result s fo rUnit s 4 , Conditio n 2 ar e include d i n Table s 2- 3 an d 2-4 , respectively
. Thes e result s indicat e that :

•Th e PCDD/PCD Femission s fo rUni t4 , Conditio n 2 (averag e emission s fo rth e thre e tes tru n se t wer e 0.0 4 ng/m 3 

### ) ar e belo wth e HW C MAC Temissio n standar d o f0. 2 ng/m 3

### (correcte d t o 7 % 0 2 

### ) ;

. Th e LV M an d SV M metal s emission s fo rUni t4 , Conditio n 2 (averag e emission s fo rth e thre e tes t ru n se twer e <36 pg/m 3

### fo rLVM s an d 22 0 pg/m 3

### fo rSVMs ) wer e lowe rtha n the ne wHW C MAC T emissio n standard s o f9 7 pg/m 3

### an d 24 0 pg/m 3

### (correcte d t o 7 % 0 2 

### ) fo rLVM s an d SVM s respectively ;

•Th e mercuryemission s fo rUni t4 , Conditio n 2 (averag e fo rth e thre e tes tru n se twer e 55 3 pg/m 3 

### ) wer e highe rtha n th e ne wHW C MAC Temissio n standar d o f13 0 pg/m 3


### .

C:\Document s an d SetIings\cdoolitle\M

yDocuments\Onyx\090

3 tesling\Ony x090 3 data\090 3 Ony xTes tPrograrado c 2- 1 January , 200 4

### ENSR
. INT0RNAT/ONAL 

### 2. 4 Stac k

Emissio n Result s fo rUni t2 Asummaryofth e PCDD/PCD Fan d Metal s emissio n result s fo rUnit s 2 ar e include d i n Table s 2- 5 an d 2-6 , respectively
. Thes e results indicat e that :

•Th e PCDD/PCD Femission s fo rUnit2 (averag e emission s fo rthe thre e tes tru n se twer e 0.2 2 ng/m 3 

### ) ar e highe rtha n th e HW C MAC Temissio n standar d o f0.2 0 ng/m 3

### (correcte d t o 7 % 0 2 

### ) ;

•Th e LV M an d SV M metal s emission s fo rUnit2 (averag e emission s fo rth e thre e tes tru n se twer e <2. 7 pg/m 3

### fo rLVM s an d 3. 7 pg/m 3

### fo rSVMs ) wer e lowe rtha n th e ne wHW C MAC Temissio n standard s o f9 7 pg/m 3

### an d 24 0 pg/m 3

### (correcte d t o 7 % 0 2 

### ) fo rLVM s an d SVM s respectively ;

•Th e mercuryemission s fo rUnit2 (averag e fo rth e thre e tes tru n se twer e 5 8 pg/m 3 

### ) wer e lowe r tha n th e ne wHW C MAC Temissio n standar d o f13 0 pg/m 3


### .

C:\Documenl s an d Settinos\cdoolittle\M

yDocuments\Onyx\090

3 testing\Ony x090 3 data\090 3 Ony xTes tProgram.do c 2- 2 January , 200 4

### ElH t WTERHATIOHAL 

### Tabl e 2- 1 Summar yo fPCDD/PCD FEmission s fo rUni t4 , Conditio n 1 , TE Q Basi s Ru n No . C1-R 1 C1-R 2 C1-R3 Dat e 16-Sep-0 3 16-Sep-03 17-Sep-0 3 Star tTime 101 5 164 5 80 0 Stop Time 135 3 195 3 110 9 Units Sample Volum e dsc f 126.78 4 117.63 4 114.38 3 Sample Volum e m 3 3.5 9 3.3 3 3.2 4 Moistur e Content %v/ v 37. 9 39. 8 40. 0 0 2Cone . % v/ v(dry ) 13.0 0 13.0 0 12.7 0 C0 2Cone . %v/ v(dry ) 5.0 0 5.20 5.5 0 Isokinetic

s % 10 2 10 2 99 Stack Flowrat e dscfm 18,87 9 18,79 6 18,79 7 PCD D / PCD FParameter

s TE F(a

) pg/sample ng/ m TEQ 3 pg/sample ng/mTE Q pg/'iamp l ng/mTE Q 2,3,7,8-TCD D 1.0 0 8 2.3E-03 1 3 3.9E-03 1 2 3.7E-0 3 1,2,3,7,8-PeCD D 0.5 0 4

2 5.8E-03 3 5 5.3E-03 27 4.2E-03 1,2,3,4,7,8-HxCD D 0.1 0 45 1.2E-0 3 4

4 1.3E-0

3 3

1 9.6E-0

4 1,2,3,6,7,8-HxCD D 0.1 0 59 1.7E-0 3 6

6 2.0E-03 4 5 1.4E-0

3 1,2,3,7,8,9-HxCD D 0.1 0 49 1.4E-0 3 35 1.OE-0 3 28 8.7E-0 4 1,2,3,4,6,7,8-HpCD D 0.0 1 26

4 7.3E-04 24 9 7.5E-04 15 7 4.8E-04 OCD D 0.0 0 225 6.3E-05 18 9 5.7E-05 15 0 4.6E-05 2,3,7,8-TCD F 0.1 0 30 8.2E-04 28 8.4E-04 2 4 7.3E-0

4 1,2,3,7,8-PeCD F 0.0 5 50 7.0E-0 4 30 4.5E-04 27 4.2E-04 2,3,4,7,8-PeCD F 0.5 0 6

1 8.6E-03 46 6.9E-03 3 9 6. 1 E-0

3 1,2,3,4,7,8-HxCD F 0.1 0 10 1 2.8E-03 5 0 1.5E-0

3 3

1 9.5E-0

4 1,2,3,6,7,8-HxCD F 0.1 0 9 8 2.7E-03 4 2 1.3E-0

3 2

9 9.0E-0

4 2,3,4,6,7,8-HxCD F 0.1 0 10 2 2.8E-03 47 1.4E-0 3 3

2 9.8E-0

4 1,2,3,7,8,9-HxCD F 0.1 0 25 7.0E-04 1 8 5.4E-04 1 6 4.9E-04 1,2,3,4,6,7,8-HpCD F 0.0 1 46

3 1.3E-0

3 13

9 4.2E-04 10 4 3.2E-0

4 1,2,3,4,7,8,9-HpCD F 0.0 1 10

0 2.8E-04 26 7.9E-05 1 6 4.9E-05 OCD F 0.0 0 32

0 8.9E-05 59 1.8E-0 5 6

9 2. 1 E-0

5 TOTA LTCDD 0.0 0 1,36

6 0.0E+O

0 1,45

1 O.OE+0

0 91 0 O.OE+0 0 TOTA LPeCD D 0.0 0 1,41 7 0.0E+0 0 1,51 0 O.OE+0 0 1,01 9 O.OE+0 0 TOTA LHxCD D 0.0 0 1,54

2 0.0E+0

0 1,64

8 O.OE+0

0 1,00

0 O.OE+0

0 TOTA LHpCD D 0.0 0 557 O.OE+0 0 51 2 0.0E+0 0 33

6 O.OE+0

0 TOTALTCD F 0.0 0 3,52

6 0.0E+0

0 4,45

7 O.OE+0

0 3,14

9 0.0E+0

0 TOTA LPeCD F 0.0 0 84

6 O.OE+0

0 801 O.OE+0 0 51 9 0.0E+0 0 TOTA LHxCD F 0.0 0 89

5 0.0E+0

0 39

4 O.OE+0

0 23

8 0.0E+0

0 TOTA LHpCD F 0.0 0 84

2 0.0E+0

0 18

0 0.0E+0

0 14

7 O.0E+0

0 TOTA LTEQ s (ng/m 3

) 0.0 3 0.0 3 0.0 2 TOTA LTEQ s (ng/m 3@7 %0 2 ) 0.0 6 0.0 5 0.0 4 TOTA LTEQ s (g/s

) = 3.0E-1 0 2.5E-1 0 2.0E-1 0 (a ) U.S.EP A(1989

) Toxi c Equivalenc

yFacto r


### C.IDocument s an d SettingstaloolittieWl

yDocuments\Onyx\090

3 testingVOny x090 3 daB\090 3 Ony xTes tProgratado c 2- 3 January , 200 4

### Tabl e 2- 2 Summar yo fMetal s Emission s fo rUni t4 , Conditio n 1 -Targe tMetal s
L o wVolatil e Metal s Emission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e A s 35. 7 21. 3 15. 2 24. 1 B e <0.1 9 <0.1 9 <0.1 9 <0.1 9 C r 6.0 7 8.9 2 5.2 6 6.7 5 Tota l LV M <42. 0 <30. 4 <20. 7 <31. 0

LV M Regulator yStandar d = 9 7 micrograms/ m 3

Semi-Volatil e Meta l Emission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e P b 135. 8 253. 7 202. 8 197. 4 C d 2.5 4 1.1 5 0.3 2 1.3 3 Tota l SV M 138. 3 254. 8 203. 1 198. 7

SV M RegulatoryStandar d = 24 0 micrograms/m 3


### Mercur yEmission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e H g 212. 6 358. 5 228. 5 266. 6 Mercur yRegulatoryStandar d = 13 0 micrograms/m 3

— 

### . , , , ,

C:\Document s an d SettingstadooffitleW

yDocuments\Onyx\090

3 testing\Ony x050 3 Uat3\090 3 Ony xTes tProgranxdo c 2- 4 January
. 200 4WTERNATlONAi. 

### Tabl e 2-2 , Continue d Summar yo fMetal s Emission s fo rUni t4 Conditio n 1
Ru n No . ' U4-C1-R 1 U4-C1-R 2 U4-C1-R3 Dat e 16-Sep-0 3 16-Sep-0

3 17-Sep-0

3 Star tTim e Unit s 101 5 164 5 80

0 Stop Time 130 9 192

3 103

9 AVG S SamDlin q Parameter

s - Barometric Pressur

e in . Hg 29.7 0 29.7

0 29.7

0 29.7

0 Volume Metere

d dc f 108.71 3 105.73 4 99.98

6 104.81 1 Sample Volume dsc f 100.851 99.059 96.24 7 98.71 9 Moistur e % v/ v 38.8 39. 1 39.4 39. 1 0 2a tStac k %dr y 13.0

0 13.0

0 12.7

0 12.9

0 Avg . Stac k

Temp . ° F 40 9 40

7 401 40 5 Stack Flowrat e dscf m 18,75

7 18,56

3 18,81 3 18,71 1 Isokinetic s % 10 4 10

3 9

9 10

2 Arseni c (As) - LV M Quantit yCollecte

d pg 58.3 0 34.1 0 24.6 0 39.0

0 Stack Cone . @ 7

% 0 2 pg/m 3 35.7 3 21.27 15.2 2 24.0

7 Stack Emissio n Rat

e Ib/hr 1.43E-0 3 8.45E-0

4 6.36E-0

4 9.72E-0

4 Berylliu m (Be

) - LV M Quantit yCollecte

d pg < 0.31 < 0.31 < 0.31 < 0.31 Stack Cone . @ 7

% 0 2 pg/m 3 < 0.1 9 < 0.1 9 < 0.1 9 < 0.1 9 Stack Emissio n Rat

e Ib/hr 7.63E-0 6 < 7.68E-06 < 8.0 1 E-06 < 7.78E-0

6 Tota l Chromiu m ier) • - LV M Quantit yCollecte

d pg 9.9 0 14.3

0 8.50 10.9 0 Stack Cone . @7

% 0 2 pg/m 3 6.0 7 8.9

2 5.26 6.7 5 Stack Emissio n Rat

e ib/h r 2.44E-0 4 3.54E-0

4 2.20E-0

4 2.73E-0

4 Cadmiu m (Cd) - SV M Quantit yCollecte

d pg 4.1 4 1.8 4 0.51 2.1 6 Stack Cone . @ 7

% 0 2 pg/m 3 2.5 4 1.1 5 0.3 2 1.3

3 Stack Emissio n Rat

e Ib/hr 1.02E-0 4 4.56E-05 1.32E-0 5 5.35E-0

5 Lea d (Pb) - SV M Quantit yCollecte

d p g 221.61 406.6 1 327.61 318.61 Stack Cone . @ 7

% 0 2 pg/m 3 135.8 0 253.6

7 202.7

5 197.41 Stack Emissio n Rat

e Ib/hr 5.45E-0 3 1.0

1 E-0 2 8.47E-0

3 8.00E-0

3 Mercur y(Hq ) - V M Quantit yCollecte

d pg 347.0 574. 6 369. 3 430.3 — Stack Cone . @ 7

% 0 2 pg/m 3 212.6 358.5 228. 5 266.6 Stack Emissio n Rat

e Ib/hr 8.54E-0 3 1.42E-0

2 9.55E-0

3 1.08E-0

2



### C:\Document s an d Seffings\crirjolrtt)eWl

yDocurnents\Onyx\090

3 testing\Ony x090 3 data\090 3 Ony xTes tProgram.do c 2- 5 January , 200 4INTERNATIONAL 

### Tabl e 2- 3 Summar yo fPCDD/PCD FEmission s fo rUni t4 , Conditio n 2 , TE Q Basi s Ru n No . C2-R 1 C2-R2 C2-R3 Dat e 17-Sep-0 3 17-Sep-0 3 18-Sep-0 3 Star tTim e 114 5 154 0 81 0 Stop Tim e 150 4 184 9 111 8 Units Sample Volume dsc f 111.251 111.67 3 112.92 9 Sample Volume m 3 3.1 5 3.1 6 3.2 0 Moistur e Conten

t % v/

v 40.0 40.7 39.2 O 2Cone . % v/ v(dry ) 12.5 0 12.1 0 13.0 0 C0 2Cone . % v/ v(dry ) 5.2 0 5.5 0 4.2 0 Isokinetic s % 9 9 10 1 9 9 Stack Flowrat e dscfm 18,39 4 18,08 8 18,61 6 PCD D / PCD FParameter

s TE F(a

) pg/sample ng/nrTE Q pg/sample ng/mTE Q pg/sample ng/nfTE Q 2,3,7,8-TCD D 1.0 0 1 1 3.4E-0 3 1 5 4.6E-0 3 1 4 4.2E-0 3 1,2,3,7,8-PeCD D 0.5 0 2

7 4.3E-0

3 3

8 6.0E-0

3 45 7.1E-0 3 1,2,3,4,7,8-HxCD D 0.1 0 3 2 1.OE-0

3 3

0 9.6E-0

4 25 7.7E-0 4 1,2,3,6,7,8-HxCD D 0.1 0 4 2 1.3E-0

3 2

7 8.4E-0

4 40 1.2E-0 3 1,2,3,7,8,9-HxCD D 0.1 0 3 2 1.OE-0

3 3

4 1.

1 E-0 3 27 8.4E-0 4 1,2,3,4,6,7,8-HpCD D 0.0 1 18

1 5.8E-0

4 23

7 7.5E-0

4 17

6 5.5E-0

4 OCD D 0.0 0 13

4 4.3E-05 15 6 4.9E-05 41 1.3E-0 5 2,3,7,8-TCD F 0.1 0 1 9 6.1 E-0 4 2

7 8.5E-0

4 20 6.4E-0 4 1,2,3,7,8-PeCD F 0.0 5 2

4 3.8E-0

4 3

6 5.7E-0

4 3

0 4.7E-0

4 2,3,4,7,8-PeCD F 0.5 0 4

0 6.3E-0

3 4

6 7.3E-0

3 40 6.2E-0 3 1,2,3,4,7,8-HxCD F 0.1 0 2 4 7.7E-0

4 3

3 1.

1 E-0 3 46 1.4E-0 3 1,2,3,6,7,8-HxCD F 0.1 0 2 8 9.0E-0

4 3

7 1.2E-0

3 36 1.1E-0 3 2,3,4,6,7,8-HxCD F 0.1 0 3 2 1.OE-0

3 41 1.3E-0 3 49 1.5E-0 3 1,2,3,7,8,9-HxCD F 0.1 0 7 2.1 E-0 4 1 1 3.4E-0 4 9 3.0E-0 4 1,2,3,4,6,7,8-HpCD F 0.0 1 3

5 1.

1 E-0 4 11 8 3.7E-0 4 4

3 1.3E-0

4 1,2,3,4,7,8,9-HpCD F 0.0 1 1 4 4.6E-05 1 7 5.3E-0 5 1 6 4.9E-0 5 OCD F 0.0 0 5

3 1.7E-0

5 6

0 1.9E-0

5 9

0 2.8E-0

5 TOTALTCD D 0.0 0 1,12

8 0.0E+0

0 1,48

9 0.0E+0

0 97

8 0.0E+0

0 TOTA LPeCD D 0.0 0 1,19

8 0.0E+0

0 1,59

8 O.OE+0

0 98

1 0.0E+0

0 TOTA LHxCD D 0.0 0 1,25

7 0.0E+0

0 1,56

5 O.0E+0

0 1,08

5 0.0E+0

0 TOTA LHpCD D 0.0 0 38

1 O.OE+0

0 52

4 0.0E+0

0 36

3 0.0E+0

0 TOTALTCD F 0.0 0 3,79

8 0.0E+0

0 4,89

9 0.0E+0

0 3,51 0 0.0E+0 O TOTA LPeCD F 0.0 0 66

5 0.0E+0

0 86

6 0.0E+0

0 67

4 O.OE+0

0 TOTA LHxCD F 0.0 0 26

4 0.0E+0

0 35

3 O.OE+0

0 38

9 O.OE+0

0 TOTA LHpCD F 0.0 0 7

4 0.0E+0

0 14

7 0.0E+0

0 17

8 O.OE+0

0 TOTA LTEQ s (ng/m') = 0.0 2 0.0 3 0.0 3 TOTA LTEQ s (ng/m 3@7 % 0 2 ) = 0.0 4 0.0 4 0.0 5 TOTA LTEQ s (g/s

) = 1.9E-1 0 2.3E-1 0 2.3E-1 0 | (a ) U.S.EP A(1989

) Toxi c Equivalenc

yFactor


### C:\Document s an d Settings\cdootittle\M

yDocuments\Onyx\090

3 testimony * 090 3 2- 6 data\09O 3 Ony xTes tProgram.do c January , 200 4ENSR . WTERHAr/OAIAL 

### Tabl e 2- 4 Summar yo fMetal s Emission s fo rUni t4 , Conditio n 2 -Targe tMetal s

L o wVolatil e Metal s Emission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e A s 12. 4 11. 1 63. 9 29. 1 B e <0.2 4 <0.2 3 <0.2 5 <0.2 4 C r 6.0 6 6.2 5 7.5 3 6.6 2 Tota l LV M <18. 7 <17. 5 <71. 7 <36. 0

LV M RegulatoryStandar d = 9 7 micrograms/ m 3


### Semi-Volatil e Meta l Emission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e P b 210. 1 249. 9 198. 5 219. 5 C d 0.3 1 0.2 7 0.5 1 0.3 6 Tota l SV M 210. 4 250. 1 199. 0 219. 8

SV M RegulatoryStandar d = 24 0 micrograms/m 3


### Mercur yEmission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e H g 468. 5 902. 1 288. 7 553. 1 Mercur yRegulatoryStandar d = 13 0 micrograms/m 3



### C:\Docgment s an d Settings\cdoolrttle\M

yDocuments\Onyx\090

3 testingVOny x090 3 data\090 3 Ony xTes tProgram.do c 2- 7 January , 200 4INTERNATIONAL 

### Tabl e 2-4 , Continue d Summar yo fMetal s Emission s fo rUni t4 Conditio n 2 - Ru n No . Ru n 1 Ru n 2 Run 3 Dat e 17-Sep-0 3 17-Sep-0

3 18-Sep-0

3 Star tTime Unit s 114

5 154

0 081 0 Stop Time 143 4 181 9 104 8 AVG S Samolin a Parameter

s - Barometric Pressur

e in . Hg 29.6 0 29.6

0 29.5

5 29.58 Volum e Metere d dc f 81.45

2 82.62

9 81.27

8 81.78

6 Sample Volume dsc f 75.76

4 76.39

0 77.09

6 76.41 7 Moistur e % v/ v 39.8 40. 7 38.9 39. 8 0 2a tStack %dr y 12.5

0 12.1 0 13.0 0 12.5

3 Avg . Stack

Temp . ° F 40 4 40

9 40

5 40

6 Stack Flowrat e dscfm 18,41 0 17,86 7 18,70

8 18,32

8 Isokinetic s % 99 10 3 10

0 10

1 Arseni c (As) - LV M Quantit yCollecte

d p g 16.1 0 15.2 0 79.7

0 37.0

0 Stack Cone . @ 7

% 0 2 pg/m 3 12.3 6 11.0

5 63.8

9 29.1 0 Stack Emissio n Rat

e Ib/hr 5.17E-0 4 4.70E-04 2.56E-0 3 1.18E-0

3 Berylliu m (Be

) - LV M Quantit yCollecte

d p g < 0.31 < 0.31 < 0.3 1 < 0.31 Stack Cone . @ 7

% 0 2 pg/m 3 < 0.2 4 < 0.2

3 < 0.2

5 < 0.2

4 Stack Emissio n Rat

e lb/h r 9.96E-06 < 9.59E-06 < 9.95E-0 6 < 9.84E-06 Tota l Chromiu m (Cr

) — LV M Quantit yCollecte

d P 9 7.9

0 8.6

0 9.4

0 8.6

3 Stack Cone . @ 7

% 0 2 pg/m 3 6.0 6 6.2

5 7.5

3 6.6

2 Stack Emissio n Rat

e Ib/hr 2.54E-04 2.66E-0 4 3.02E-0

4 2.74E-0

4 Cadmiu m (Cd) - SV M Quantit yCollecte

d P 9 0.4

0 0.3

7 0.6

3 0.4

7 Stack Cone . @7

% 0 2 pg/m 3 0.31 0.2 7 0.51 0.3 6 Stack Emissio n Rat

e Ib/hr 1.29E-0 5 1.14E-0

5 2.02E-0

5 1.48E-0

5 Lead (Pb

) - SV M Quantit yCollecte

d P 9 273.61 343.61 247.61 288.28 Stack Cone . @7

% 0 2 pg/m 3 210.0 5 249.8

7 198.4

8 219.4

7 Stack Emissio n Rat

e Ib/hr 8.79E-0 3 1.06E-0

2 7.95E-0

3 9.12E-0

3 Mercur y(Hq ) - V M Quantit yCollecte

d pg 610.3 1240.5 3S0. 1 737.0 Stack Cone . @ 7

% 0 2 pg/m 3 468. 5 902. 1 288.7 553. 1 Stack Emissio n Rat

e Ib/hr 1.96E-0 2 3.84E-0

2 1.16E-0

2 2.32E-0

2



### C:\Document s an d Settings\cdoolfttie\M

yDocuments\Onyx\050

3 testingVOny x090 3 data\090 3 Ony xTes tProgram.do c 2- 8 January , 200 4INTERNATIONAL 

### Tabl e 2- 5 Summar yo fPCDD/PCD FEmission s fo rUni t2 , TE Q Basi s

Ru n No . R 1 R2 R3 Dat e 18-Sep-0 3 19-Sep-0 3 19-Sep-0 3 Star tTime 144 5 83 0 125 0 Stop Tim e 184 9 114 2 160 1 Units Sample Volume dsc f 109.37 3 120.21 9 112.85 4 Sample Volume m 3 3.1 0 3.4 0 3.2 0 Moistur e Conten

t %v/

v 45. 6 42. 8 43. 9 0 2Cone . %v/ v(dry ) 12.1 0 12.1 0 11.5 0 C0 2Cone . %v/ v(dry ) 6.7 0 6.7 0 6.7 0 Isokinetic s % 99 9 6 9 7 Stack Flowrat e dscfm 7,628 8,68 5 8,05 7 PCD D / PCD FParameter

s TE F(a

) pg/sample ng/ m TE Q pg/sample ng/ m TEQ 3 pg/sample ng/m 3TE Q 2,3,7,8-TCD D 1.0 0 2

0 6.6E-03 1 3 3.7E-0 3 1 5 4.7E-03 1,2,3,7,8-PeCD D 0.5 0 10

7 1.7E-0

2 45 6.6E-03 4 3 6.7E-0

3 1,2,3,4,7,8-HxCD D 0.1 0 10 6 3.4E-03 53 1.6E-0 3 4

0 1.3E-0

3 1,2,3,6,7,8-HxCD D 0.1 0 19 8 6.4E-03 8 8 2.6E-03 8 4 2.6E-0

3 1,2,3,7,8,9-HxCD D 0.1 0 12 6 4. 1 E-03 6 7 2.0E-03 1 1 3.5E-0 4 1,2,3,4,6,7,8-HpCD D 0.0 1 65

6 2. 1 E-03 38 3 1.1 E-0

3 35

2 1.1E-0

3 OCD D 0.0 0 46

8 1.5E-0

4 31 4 9.2E-05 30 9 9.7E-0

5 2,3,7,8-TCD F 0.1 0 26 0 8.4E-03 12 8 3.8E-03 9 4 2.9E-0

3 1,2,3,7,8-PeCD F 0.0 5 40

7 6.6E-03 15 9 2.3E-03 12 9 2.0E-0

3 2,3,4,7,8-PeCD F 0.5 0 79

4 1.3E-01 369 5.4E-0 2 26

6 4.2E-0

2 1,2,3,4,7,8-HxCD F 0.1 0 53 5 1.7E-0

2 235 6.9E-03 16 4 5.1E-0

3 1,2,3,6,7,8-HxCD F 0.1 0 42 0 1.4E-0

2 18

4 5.4E-03 14 0 4.4E-03 2,3,4,6,7,8-HxCD F 0.1 0 73 3 2.4E-02 281 8.3E-03 19 9 6.2E-0

3 1,2,3,7,8,9-HxCD F 0.1 0 19 6 6.3E-03 76 2.2E-03 5 8 1.8E-0

3 1,2,3,4,6,7,8-HpCD F 0.0 1 81 1 2.6E-03 451 1.3E-0 3 35

3 1.1E-0

3 1,2,3,4,7,8,9-HpCD F 0.01 17 0 5.5E-04 61 1.8E-0 4 6

1 1.9E-0

4 OCD F 0.0 0 20

6 6.7E-05 10 1 3.0E-05 11 7 3.7E-0 5 TOTALTCD D 0.0 0 4,56

3 0.0E+0

0 1,97

3 O.OE+0

0 1,54

3 0.0E+0

0 TOTA LPeCD D 0.0 0 5,03

4 0.0E+0

0 2,02

4 0.0E+0

0 1,70

6 0.0E+0

0 TOTALHxCD D 0.0 0 6,16

1 0.0E+0

0 2,57

8 0.0E+0

0 2,55

0 0.0E+0

0 TOTA LHpCD D 0.0 0 1,41 5 0.0E+0 0 82

3 0.0E+0

0 73

9 O.OE+0

0 TOTALTCD F 0.0 0 10,50

4 0.0E+0

0 5.10

3 O.OE+0

0 3,89

4 0.0E+0

0 TOTA LPeCD F 0.0 0 10,10

6 0.0E+0

0 4,02

5 O.OE+0

0 2,84

4 0.0E+0

0 TOTA LHxCD F 0.0 0 7,73

5 0.0E+0

0 2,56

5 O.OE+0

0 1,83

3 O.OE+0

0 TOTA LHpCD F 0.0 0 1,84

9 0.0E+0

0 63

4 0.0E+0

0 62

6 O.OE+0

0 TOTA LTEQ s (ng/m 5

) 0.25 0.1 0 0.0 8 TOTA LTEQ s (ng/m 3@ 7 %0 2 )
-= 0.39 0.1 6 0.1 2 TOTA LTEQ s (y/s) = 8.9E-1 0 4.2E-1 0 3.1E-1 0 (a ) U.S.EP A(1989

) Toxi c Equivalenc

yFactor


### C:\Documenl s an d Sertings\cdooIirite\M

yDocuments\Onyx\090

3 testing\Ony x090 3 dala\090 3 Ony xTestProgram.do

c 2- 9 January , 200 4

## H MIMIC. , \ INTERNATIONAL 

### Tabl e 2-6 , Continue d Summar yo fMetal s Emission s fo rUni t2
Ru n No . Ru n 1 Ru n 2 Ru n 3 Dat e 18-Sep-0 3 19-Sep-0

3 19-Sep-0

3 Star tTim e Unit s 144

5 83

0 125

0 Stop Tim e 181 0 111 2 153 1 AVG S Samolin q Parameter

s - Barometric Pressur

e in . H g 29.5 5 29.6

0 29.6

0 29.58 Volum e Metere

d dc f 85.391 84.76 3 82.28

8 84.14

7 Sampl e Volume dsc f 78.120 83.40 5 79.85

2 80.45

9 Moistur e % v/ v 44.5 42.4 43.4 43.4 0 2a tStac k %dr y 12.1 0 12.1 0 11.5 0 11.9

0 Avg . Stac k

Temp . ° F 38 2 36

8 37

2 37

4 Stac k Flowrat e dscfm 5,38 1 5,84

0 5,54

9 5,59

0 Isokinetic s % 9 9 9

7 9

8 9

8 Arseni c (As

) - LV M Quantit yCollecte

d M 9 1.9

0 2.3

0 0.9

6 1.7

2 Stac k Cone . @ 7

% 0 2 pg/m ' 1.3 5 1.5

3 0.6

3 1.1 7 Stac k Emissio n Rat

e Ib/hr 1.73E-0 5 2.13E-0

5 8.82E-0

6 1.58E-0

5 Berylliu m (Be

) - LV M Quantit yCollecte

d P 9 < 0.31 < 0.31 < 0.31 < 0.31 Stac k Cone . @ 7

% 0 2 pg/m 3 < 0.2 2 < 0.21 < 0.2 0 < 0.21 Stac k Emissio n Rat

e Ib/hr 2.82E-06 < 2.87E-06 < 2.85E-0 6 < 2.85E-06 Tota l Chromiu m (Cr

) - LV M Quantit yCollecte

d pg 1.6 0 1.9

0 2.3

0 1.9

3 Stac k Cone . @ 7

% 0 2 pg/m 3 1.1 4 1.2 7 1.5

0 1.3

0 Stac k Emissio n Rat

e Ib/hr 1.46E-0 5 1.76E-0

5 2.1 1 E-0

5 1.78E-0

5 Cadmiu m (Cd) - SV M Quantit yCollecte

d pg 0.31 0.2 8 0.1 6 0.2 5 Stac k Cone . @ 7

% 0 2 pg/m 3 0.2 2 0.1 9 0.1 0 0.1 7 Stac k Emissio n Rat

e lb/h r 2.82E-06 2.59E-06 1.47E-0 6 2.30E-06 Lea d (Pb ) - SV M Quantit yCollecte

d p g 4.01 6.0 1 5.8

1 5.2

8 Stac k Cone . @ 7

% 0 2 pg/m 3 2.8 5 4.0

0 3.7

9 3.5

5 Stac k Emission Rat

e Ib/hr 3.65E-05 5.57E-0 5 5.34E-0

5 4.85E-0

5 Mercur y(Hq ) - V M Quantit yCollecte

d p g 118.4, 104.0 32.8 85. 1 Stac k Cone . @ 7

% 0 2 pg/m 3 84.2 69.3 21. 4 58.3 Stac k Emissio n Rat

e Ib/hr 1.08E-0 3 9.63E-0

4 3.01 E-0

4 7.81 E-0

4 g/sec 1.36E-0

4 1.2

1 E-04 3.80E-0

5 9.84E-0

5



### C:\Document s an d Setmgs\cdoolitleW

yDocuments\Onyx\090

3 testing\Ony x090 3 2-1 1 datat>90 3 Ony xTes tProgram.do c January , 200 4EHS R /HTERAMrrOHAL 

### Tabl e 2- 6 Summar yo fMetal s Emission s fo rUni t2 -Targe tMetal s
L o wVolatil e Metal s Emission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e A s 1. 4 1. 5 0.6 3 1. 2 B e <0.2 2 <0.2 1 <0.2 0 <0.2 1 C r 1.1 4 1.2 7 1.5 0 1.3 0 Tota l LV M <2. 7 <3. 0 <2. 3 <2. 7

LV M Regulator yStandar d = 9 7 micrograms/ m 3


### Semi-Volatil e Meta l Emission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e P b 2. 9 4. 0 3. 8 3. 5 C d 0.2 2 0.1 9 0.1 0 0.1 7 Tota l SV M 3. 1 4. 2 3. 9 3. 7

SV M RegulatoryStandar d = 24 0 micrograms/m 3



### Mercur yEmission s - micrograms/m 3 

### Metal s Run l Run 2 Run 3 Averag e H g 84. 2 69. 3 21. 4 58. 3 MercuryRegulator yStandar d = 13 0 micrograms/m 3



### C:\Documen1 s an d Settings\cdoolitfe\M

yDocumenl5\0nyx\090

3 testingXOny x090 3 dala\090 3 Ony xTes tProgram.do c 2-1 0 January , 200 4

### ENSR
. MTeRNATIONAL 

### 3. 0 SAMPLIN G AN D ANALYTICA LPROCEDURE S

3. 1 Samplin g Procedure s Severa l differen tsamplin g an d monitorin g technique s wer e use d t o provid e th e require d dat at o mee t th e goal s o fthi s tes tprogram . Triplicat e run s wer e conducte d o n Uni t4 a ttw o condition s establishe d b yOnyx
. Triplicat e testin g wa s als o conducte d o n Uni t2 a tproces s condition s establishe d b yOnyx
. Th e samplin g activities describe d belo wwer e conducte d durin g al l runs . Al l fiel d activities wer e documente d i n accordanc e with EP Aaccepte d procedure s an d copie s o fal l fiel d note s an d dat a sheet s ar e include d i n Appendi xAo fthi s report
. 3.1. 1 Velocity , Moistur e an d Fixe d Ga s Determination s Ga s strea m velocit yan d temperatur e wer e determine d i n conjunctio n with eac h manua l samplin g method
. Atyp e "S " pito ttub e connecte d t o a n incline d wate rmanomete rwa s use d t o determin e velocit yhea d o fth e flu e ga s a teac h duc ttravers e poin ta s specifie d i n EP AReferenc e Metho d 2
. Th e temperatur e profil e o fthe flu e ga s a teac h duc ttravers e poin twa s obtaine d b ytakin g reading s wit h a thermocoupl e an d pyromete rconcurren twith th e velocit yhea d measurements
. Moistur e conten twa s determine d a s specifie d i n EP AMetho d 4
. Velocit yan d temperatur e measuremen tprofile s wer e establishe d prio rt o testin g t o ai d i n sampl e trai n set-up
. Sample s fo rth e determinatio n o fth e fixe d ga s compositio n (0 2

### an d C0 2 

### ) wer e collecte d usin g th e integrate d ba g techniqu e detaile d i n EP A Referenc e Metho d 3
. 3.1. 2 PCDD/PCD FSamplin g Samplin g fo rdioxin s an d furan s wa s complete d i n accordanc e with EP AMetho d 0023 A(EP ASW 846)
. Sample s wer e collecte d fo rseparat e fronthal fan d bac k hal fanalysis
. O n Uni t#4 , eac h samplin g ru n wa s 3 hour s i n duratio n coverin g 1 2 samplin g point s a t1 5 minute s pe rpoint
. O n Uni t#2 , eac h samplin g ru n wa s 3 hour s i n duratio n coverin g 1 2 samplin g point s a t1 5 minute s pe rpoint
. Set u p an d recover yschematic s fo rth e Metho d 0023 Atrai n ar e include d i n Appendi xB
. 3.1. 3 Metal s Samplin g Th e EP AMultipl e Metal s Trai n (EP AMetho d 2 9 a s specifie d i n 4 0 CF R 6 0 Appendi xA ) wa s utilize d durin g the testin g progra m fo rthe collectio n o fthe followin g metals : arsenic , beryllium , cadmium , chromium , lead , mercury)
. Eac h ru n wa s 2-h ri n duratio n coverin g 1 2 samplin g point s a t1 0 minute s pe rpoint
. Set-u p an d recoveryschematic s forth e multimetal s trai n ar e include d i n Appendi xB
.

C:\Document s an d SetlinQS\cdooli1t!e\M

yDocuments\Onyx\090

3 testing\Ony x090 3 data\090 3 Ony xTes ! Program.do c 3- 1 January , 200 4/NTERNAT/ONAL



### 3. 2 Analytica l Procedure s 3.2. 1 PCDD/PCD FAnalyse s Metho d 002 3 sample s wer e analyze d b yEP AMetho d 829 0 (hig h resolutio n GC/MS)
. Th e trai n fraction s recovere d fo ranalysi s o fPCDDs/PCDF s includ e th e fronthal frinses, th e particulat e filte ran d th e XA D resi n trap
. Whil e separat e fronthal fan d bac k analytica l result s wer e obtained , th e result s fo r eac h sampl e fractio n wer e combine d int o asingl e analytica l resul tfo reac h run . PCDD/PCD F analyse s wer e performe d b yAlt aAnalytica l Laboratory , Inc
. i n E l Dorad o Hills , CA
. 3.2. 2 Metal s Analyse s Metal s analyse s fo rth e wast e fee d sample s wer e complete d usin g tw o separat e procedures
. First , sample s wer e prepare d an d analyze d fo rarsenic , beryllium , cadmium , chromium , an d lea d a s specifie d i n EP AMetho d 602 0 (ICP-MS) , SW846 , 3 r d

### Edition
. Mercur ywa s analyze d vi ametho d 7471A
. Metal s analyse s wer e performe d b ySever n &Tren tLaboratories , Sacramento , CA
.

CADocument s an d Settings\cdoolittte\M

yDocuments\Onyx\090

3 lesting\Ony x090 3 data\090 3 Ony xTes tProgram.do c 3- 2 January , 2004INTERNATIONAL


### 4. 0 QUALIT YASSURANC E

4. 1 Introductio n Thi s sectio n present s th e result s o fal l QA/Q C measure s implemente d durin g th e fiel d samplin g progra m an d al l phase s o fsubsequen tanalysis
. Dat agenerate d fo rth e progra m ar e judge d t o b e vali d a s overal l accurac yan d precisio n result s ar e consisten twith genera l objectives
. Analytica l QA/Q C dat aar e presente d t o supportal l sampl e result s use d fo rdeterminin g complianc e wit h performanc e criteri ao remissio n standards
. 4. 2 Stac k

Samplin g QA/Q C Th e stac k

samplin g progra m incorporate d avariet yo fmeasure s t o ensur e tha tsoun d dat awoul d b e obtained
. Al l sample s wer e collecte d a tth e stac k samplin g location s a s planne d an d i n accordanc e wit h applicabl e method procedures
. On e fiel d blan k fo reac h pollutan twa s als o submitte d fo ranalysi s alon g wit h progra m samples
. Samplin g QA/Q C measur e fo rthi s progra m include d calibratio n o fal l applicabl e samplin g equipmen t use d a s describe d below
. Fiel d equipmen twer e calibrate d accordin g t o EP Aprocedure s specifie d i n EPA-600/4-77-027 b (Augus t1977 ) an d 4 0 CF R 60 , Method s 1-5 , a s wel l a s manufacturer' s specifications
. 1 ) Dr yGa s Meter s an d Orific e Meter s (EP AMetho d 5 Type)
. Th e dryga s meter s fo ral l samplin g train s wer e calibrate d agains tawe ttes tmete rtha tha d bee n calibrate d agains taspirometer
. Th e orific e meter s wer e calibrate d agains tth e we ttes tmete ran d checke d agains tth e dryga s mete rt o whic h the ywer e attached
. Mete rboxe s ar e calibrate d annuall yan d the n verifie d b yus e ofth e alternativ e Metho d 5 post-tes tcalibratio n procedure
. Thi s procedur e i s base d o n th e principal s o f th e optiona l pretes torific e mete rcoefficien tchec k outline d i n Sectio n 4.4. 1 o fMetho d 5
. Th e averag e Y-valu e obtaine d b ythi s metho d mus tb e withi n 5 % o fth e initia l Y-value
. Th e calculation s provide d wit h th e dat asheet s i n Appendi xC sho wtha tthi s criterio n wa s me tfo reac h isokineti csamplin g trai n use d o n thi s program . Al l annua l calibratio n form s ar e provide d i n Appendi xC
. 2 ) Samplin g Nozzles
. Eac h glas s nozzl e i s calibrate d with amicromete rprio rt o testin g an d identifie d wit h auniqu e identificatio n number
. Th e intema l diamete ro feac h nozzl e i s measure d t o 0.00 1 inche s alon g thre e point s o fth e circumferenc e wit h adia l vernie rcalipe ran d th e thre e measurement s ar e the n averaged
. 3 ) Balance
. Th e analytica l balanc e use d i n the fiel d t o determin e initia l an d fina l silic age l weight s i s calibrate d agains tClas s M weight s provide d b ythe Mettle rCorporation
. 4 ) Thermocouples
. Typ e Kthermocouple s i n eac h mete rcontro l box , heate d sampl e box , impinge r umbilica l connecto ran d sampl e probe s ar e calibrate d agains tAST M mercury-in-glas s C:\Document s an d SettingstaJoolittleWl

yDocuments\Onyxl090

3 lesting\Ony x090 3 data\090 3 Ony xTes tProgram.do c 4- 1 January , 2004

### EN5 R INTERNATIONAL. 

### thermometer s a tthre e points : a n ic e bath , ambien ttemperatur e an d aboilin g wate rbath
. Calibratio n dat aar e provide d i n Appendi xC
. 5 ) Pito tTube
. Eac h S-typ e stainles s stee l pito ttub e use d i s designe d t o mee tgeometri c configuration s a s define d i n EP AMetho d 2
. Dat asheet s ar e provide d i n Appendi xC
. 4. 3 Chain-of-Custod y Chain-of-custod yprocedure s wer e followe d fo ral l sample s a s follows :

•Eac h isokineti ctrai n wa s set-u p an d recovere d i n aclea n are aadjacen tt o th e incinerators
. » Sample s wer e collected , seale d an d labele d appropriately
. •Al l sample s wer e packe d i n bubbl e wra p o rothe rabsorben tmateria l an d place d i n eithe r sampl e cooler s o rappropriat e DO Tshippin g package s (dangerou s good s items)
. •Al l sample s wer e subsequentl yshippe d vi aPriorit yOvernigh tFed
. E xservic e t o th e designate d laboratory
. 4. 4 Analytica l QA/Q C Dat aQualit yIndicator s (DQI's ) wer e utilize d throughou tthe progra m t o asses s th e validit yo fanalytica l data
. Thi s sectio n provide s arevie wo fthes e indicator s an d th e subsequen timpac to n the analytica l data
. 4.4. 1 Analysi s fo rMetal s Evaluatio n o fth e validit yo fmetal s dat aresultin g fro m th e analysi s o fth e Metho d 006 0 samplin g trai n sample s wa s base d o n th e followin g tw o set s o fDQI's :

•Recoverie s o finternal , pre-spik e an d alternat e recoverystandard s adde d t o th e sample s prior t o sampling
. Recoverie s o fthes e standard s ar e include d wit h othe rSever n &Tren t Laboratorie s dat ai n Appendi xD
.
•Result s o fanalyse s o ffiel d an d metho d blan k sample s fo rmetals
. Thes e result s ar e include d i n Appendi xD
. O n th e basi s o fthes e Q C results , n o sampl e analyse s wer e rejecte d an d al l th e dat awer e determine d t o b e valid
. Completenes s wa s therefor e determine d t o b e 100 % fo ral l metal s result s fro m al l samples
. Dat aqualit yindicator s (DQIs ) wer e utilize d throughou tth e progra m t o asses s the validit yo fth e analytica l data
. Thi s sectio n provide s arevie wo fthes e indicator s an d th e subsequen timpac to n th e analytica l data
.

C:\Docuroent e an d SettinastadoolittleWl

yDocuments\Onyx\090

3 tes!ing\Ony x090 3 aata\090 3 Ony xTes tProgram.do c 4- 2 January , 2004

# ENSR . INTERNATIONAL 

### 4.4. 2 Analysi s fo rPCDDs/PCDF s Evaluatio n o fthe validit yo fth e PCDD/PCD Fdat aresultan tfro m th e analysi s o fth e Metho d 2 3 samplin g trai n sample s wa s base d o n fou rset s o fDQIs
. Thes e were :

•Recoverie s o fintemal , pre-spik e an d alternat e recoverystandard s adde d t o th e sample s prio rt o sampling
.
•Result s o fanalysi s o fLaboratoryContro l Sample s (LCS ) fo rth e 1 7 PCDD/PCD Fisomer s liste d i n EP AMetho d 23
.
•Result s o fanalyse s o ffiel d an d metho d blan k sample s fo rPCDD/PCDFs
. Thes e result s ar e include d wit h th e Alt aAnalytica l Dat aRepor tinclude d i n Appendi xD
. Base d o n thes e Q C results , recoverie s o ftw o nativ e analyte s (2,3,6,7,8-HxCD Fan d 1,2,3,7,8,9-HxCDF ) wer e outsid e o fAlta' s limi ti n the Ongoin g Precisio n an d Recover y(OPR ) sample
. Thes e limit s ar e recommende d only , an d ar e no tdesignate d b yth e method
. N o sampl e analyse s wer e rejected , an d al l dat awer e determine d t o b e valid
.

C:\Document s an d SetingstadooMeNM

yDocuments\Onyx\090

3 lesting\Ony x090 3 4- 3 data\090 3 Ony xTes tPrograrado c January , 2004INTERNATIONAL



### APPENDI XA FIEL D DAT ASHEET S

C:\Doctment s an d Sstinos\cdoolit!!e\M

yDocumenB\Ony>;\090

3 testfncAOny xO90 3 d3taWppendix

### Covere.do

c January2004

### Uni t4 , Conditio n 1 PCDD/PCD FFIEL D DAT A

S:\STACKU0B\20D3tonyxRP\repoiWl ysheets.** : 

### Novembe r200 3Metho d 0023 ASamplin g Parameter s UNI T4 - Conditio n 1-R M 0023 A 

### Ru n No
. C1-R 1 C1-R 2 C1-R 3 Dat e 16-Sep-0 3 16-Sep-0 3 17-Sep-0 3 Star tTim e Unit s 101 5 164 5 80 0 Sto p Tim e 135 3 195 3 110 9 AVG S Nozzl e Diamete r inche s 0.29 1 0.28 0 0.28 0 0.28 4 Barometri cPressur e in
. H g 29.7 0 29.7 0 29.6 0 29.6 7 Ne tSamplin g Tim e min
. 180. 0 180. 0 180. 0 180. 0 Volum e Metere d dc f 136.25 6 125.63 2 119.06 6 126.98 5 Avg
. DG M Temp
. ° F 95. 8 91. 8 75. 8 87. 8 Av g Delt aH i n H 2 

### 0 2.1 6 1.8 0 1.6 3 1.8 6 Av g Delt aH in
. H g 0.158 7 0.132 4 0.120 1 0.137 1 D G M Calibratio n Facto r — 

### 0.981 4 0.981 4 0.981 4 0.981 4 G a s Sampl e Volum e dsc f 126.78 4 117.63 4 114.38 3 119.60 0 Tota l Wate rCollecte d m L 1639. 5 1648. 1 1620. 6 1636. 1 Volum e o fWate rVapo r sc f 77.30 2 77.70 8 76.41 1 77.14 1 Moistur e (measured ) % v/v 37. 9 39. 8 40. 0 39. 2 Moistur e ( @ saturation ) % v/v 100. 8 100. 9 101. 2 101. 0 Dr yMol e Fraction , 100-% M ~ 

### 0.621 2 0.602 2 0.599 5 0.607 6 C 0 2

### a tStac k %dr y 5.0 0 5.2 0 5.5 0 5.2 3 0 2

### a tStac k %dr y 13.0 0 13.0 0 12.7 0 12.9 0 C O + N 2 

### % dr y 82.0 0 81.8 0 81.8 0 81.8 7 Dr yMolecula rWeigh t Ib/lb-mol e 29.3 2 29.3 5 29.3 9 29.3 5 We tMolecula rWeigh t Ib/lb-mol e 25.0 3 24.8 4 24.8 3 24.9 0 Exces s Ai ra tStac k 

### % 150. 3 151. 2 142. 8 148. 1 Stac k Diamete r inche s 48. 0 48. 0 48. 0 48. 0 Stac k Are a sq . in
. 1809. 6 1809. 6 1809. 6 1809. 6 Stati cPressur e i n H 2 

### 0 -0.4 2 -0.5 2 -0.5 2 -0.4 9 Stac k Pressur e in
. H g 29.6 7 29.6 6 29.5 6 29.6 3 Avg
. Stac k

Temp
. 406. 4 408. 3 400. 7 405. 1 Avg
. Sqroo to fDelt aP — 

### 0.859 8 0.880 7 0.882 1 0.874 2 S D E Averag e ~ 

### 25.30 9 25.95 3 25.87 9 25.71 4 Pito tCoefficien t 

# - 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 4,00 2 4,12 0 4,11 6 4,08 0 Stac k Flowrat e we tacf m 50,28 9 51,77 9 51,72 8 51,26 6 Stac k Flowrat e we tscf m 30,39 0 31,21 3 31,35 4 30,98 6 Stac k Flowrat e dscf m 18,87 9 18,79 6 18,79 7 18,82 4 Isokinetic s 

### % 10 2 10 2 9 9 10 1 Mete rBo xNo
. ~ 

### 8010 2 8010 2 8010 2 

# - Delt aH @ in
. H g 2.059 0 2.059 0 2.059 0 Fiel d Q AYq c — 

### 1.03 6 1.02 3 1.01 4 1.02 5 [Deviation ] Pre- Y 

### % 5.6 % 4.2 % 3.4 % 4.4 % S:\STACK\JOB\2003\onyxRP\xldala\Sep t03\[M2 3 U 4 Cl .xlsJTOTALDF

S

### UNI T4 - Conditio n 1-R M 0023 A

P T RU N 1AVGS - -PCDDs/ 1 >CDFs RU N 2 AVG S - -PCDDs/PCDF s RU N 3 AVG S - -PCDDs/PCDF s P T DP SQR T DP DG M



### IN DGM 

### OU T D H STAC K

TEM P DP SQR T DP DGM



### IN DGM

OU T DH STAC K TEM P DP SQR T D P DG M



### IN DG M

OU T D H STAC K TEM P 

### a 1 0.6

5 0 .806 2 6 7 6

5 2.50 39 9 0.61 0.781 0 9 6 9

5 1.5

0 399 0.59 0.768 1 6 3 6

2 1.2

0 390 

### a 2 0.7

3 0.854

4 9

1 

### 8

2 2.7

0 40

5 0.7

7 

### 0 .877 5 9

3 9

3 1.8

0 401 0.7 3 0.854

4 69 6 5 1.5

0 39

2 

### a 3 0.8

5 0.922

0 

### 9 3 8

5 3.1 0 412 0.8 5 0.922

0 9

2 9

1 2.0

0 40

8 0.8

5 0.922

0 7

3 67 1.8 0 40

3 a4 

### 0.8

5 0.922

0 9

6 8

8 3.1 0 413 0.8 4 0.916

5 9

3 9

1 2.0

0 408 0.9 0 0.948

7 76 7 0 1.9

0 40

7 

### a 5 0.7

4 0.860

2 

### 9 4 9

3 1.8

0 412 0.8 7 0.932

7 9

3 9

0 2.1 0 40 7 0.8

0 0.894

4 7

8 7

2 1.7

0 406 

### a 6 0.6

3 

### 0 .793 7 10

6 9

4 1.6

0 40

6 0.8

5 0.922

0 9

2 8

9 2.0

0 40

7 0.7

5 0.8660 8 0 7

4 1.6

0 40

4 

### a 7 0.6

0 0 .774 6 10 3 9

7 1 .4

0 40

6 0.5

7 0.755

0 9

2 9

2 1.4

0 40

2 0.59 0.768 1 7 6 7

5 1.2

0 391 

### a 8 0.7

0 0.836

7 

### 10 9 9

8 

### 1.8

0 40

5 0.71 0.842 6 9

2 8

8 1.6

0 40

8 0.7

5 0.866

0 8

1 76 1.6 0 400 

### a 9 0.7

8 0.883

2 

### 11 0 10 1 2.0

0 40

8 0.8

6 0.927

4 9

5 8

9 1.9

0 413 0.8 2 0.905

5 8

3 7

8 1.7

0 400 

### al O 0.8

5 0.922

0 

### 11 1 10 3 2.1 0 410 0.8 8 0.938 1 9 4 8

9 1.9

0 415 0.9 0 0.948

7 8

5 8

0 1.9

0 40

4 

### a1 1 0.7

2 0.848

5 10

3 10

2 1.8

0 401 0.8 2 0.905

5 9

4 8

8 1.8

0 41 6 0.8 8 0.938 1 8 6 8

1 1.8

0 406 

### a1 2 0.8

0 0.894

4 10

5 10

2 2.0

0 40

0 0.7

2 0.848

5 9

4 8

8 1.6

0 41 6 0.8 2 0.905

5 8

6 8

3 1.7

0 40

5 AV G 0.7 4 0.859 8 95. 8 2.1 6 40 6 0.7 8 0.880 7 91. 8 1.80 40 8 0.7 8 0.882 1 75. 8 1.6 3 40 1

### P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T •'•asA o..<- *x /••S / A .. . Samplin gTrai n Ru nNumbe

rU'f Cj • /?. i Clien t FncHlt yLocatio

n Sourc e Dnf e Operato r Slac kDia. - in. Star tTim e Slo p lim e Barometri cPressur eJ'/
. /£*



### KH SialicPressur e(+/- ) ~ Probe/Pito

lNumbe r^C A i-,^

—£ Plto tCoemden

tQ t

S} y FillerBo xNo. • Mete rBo xNo.

### "HOlOjL LEA KCHECK S I n "H g INITIA L VAC . /S~In . MI D VAC . glO

III . FINA L VAC , / VIn . CF MQ.QCs ? CF M

### Q OC I

INIT . PITO T FINALPITOV O Orific eCoefficien

t(Y)Q,<?S/ y Delt aII ®

### J.A<r?a Nozzl eSize/No . Q ,3/.? /

JVc a XA D Thermocoupl

eID: Im p FILTE RDAT A NUMBER " TAR E "

. — "Ei?"!!'!.?.?.. 10

/. IMPWGE RVOI,< S 

### .iNix.
. /f <•:>. FINA L



### 5

SILIC A GE L 

### ^ 1 Orsa t 

### o z Jf. 0 13.0 r. o i3. o ,5- 0 i 'i . O Fina lPurg eRnte
_ Fina lP H SAMPL E POINT CLOC K

HM r TJEA D

Deliai 1li t'w t ORIFIC E 

### MintRVO l Drlliill.ii iw

c VOM'Mi " STAC K 

### TEMPERATUR E READINGS
. ° F PROB E ORGANI C

OVE Ni

MOPMJ 3 IM P GA S METE R I K OC T VACUU M to. Hi t COMMENT S 

### AI ^ 2
. 2 <,?:, ft?1

/(a ,-7 Y 2j L 

### 2A. 7 . o 

### 5 U
_ 85 " 

### *to, a, (j>Q 6 ^ 

### 22 L . £ 1

/SS 

### /ro p . / ' ( F .. .

/ y 

### r<rj
. o ±£ 4 L4&a> JLS/ /<o 9
UL 

### 2XL 22— ? r 

### so/ vol 

### SO -Z S3. o 

### T,<S~ /7 a /P.o /£S)o

J-CI&"f- /tilt* '/J/2. - / '

### E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin gTrai n

### ..-CfXiA RunNumbe

r

### O c 

### /-C/ Clien t Facilit yLocutio

n Sourc e Dat e Operato r Barometri cPressur

e

### Jl°l.'}C> Stati cPressur e(+•/- ) —Q ,S~,2. Probe/Pito

tNumber

_ Pito tCoerriclen

t Filte rBo xNo. _ Mete rBo xNo . LEA KCHECK S i n"H g INITIA L VAC . /.<T MI D VAC . ~ - FINA L VAC . / 7 CF MQ .QO M CF M

INIT . PITOT FINA L P1T0X> >

FILTE RDAT A Stac kDia.-In . 

### •Y8" Delt aII ®

### J?.&Syc> NUMBE R TAR E Star tTim e 

### JIMS'

/"li** Nozzl eSize/No . ^ ^SC " ^
_ Slo p Tim e /8 /< T /9 .T - 3 XAD Thermocoupl eBJ : IMPINGE R VOL'S . INIT .
--o o FTNAt. .

SILIC A GE L Wi Orsa t



### 13 ° 4 " > I3T.0

Fina lPurg eRat e SAMPL E POIN T li(l ( K

TIM E 

### vt.ixicm

1IEA & I'ell

### il'.iuwc ORIFIC E

Mr.iFi noi, . ttrlt.iH, II I w

t UA S M IIE R 

### TEMPERATUR E READINGS
. ° F — ' • 

### ^ililMII.^M. i

PDM P VACUU M 

### taift COMMENT S SAMPL E POIN T li(l ( K

TIM E 

### vt.ixicm

1IEA & I'ell

### il'.iuwc ORIFIC E

Mr.iFi noi, . ttrlt.iH, II I w

t 10LUM E ft* STIC K PMOBf r OVF V ORGANIC .

MODUL E ; ; . GA S METER.. . 

### ^ililMII.^M. i PDM P VACUU M 

### taift COMMENT S SAMPL E POIN T li(l ( K

TIM E 

### vt.ixicm

1IEA & I'ell

### il'.iuwc ORIFIC E

Mr.iFi noi, . ttrlt.iH, II I w

t 10LUM E ft* STIC K PMOBf r OVF V ORGANIC .

MODUL E I M P I N O U T 

### ^ililMII.^M. i PDM P VACUU M 

### taift COMMENT S 

### O 6.(of /..< r cct T %r V . 6 

### /s cb.77 / . S Vr> / 

### cT y s?<r 7. 2 

### J2.S~ Jo O. 8

^ T 

### .<v.r . s v 8 „7c5 V 

### (of ' 4 / ^ . o Vc ">8 ' 

### £5-1 ir » r 

### (s-2 9 / /v.sr •S " ,*! . / JV^ . 6 / 

### JT 7 9R /t5~. 0 

### <f » vsr o . 

### as ' T 7 C )


### . f V£> 7 ^Vc i 

### 3H1 6 V 6 6 

### <?J / J " o 

## ^ / 9 o o.>5- ? 

### S?a./</</ yo; > 

### .^tSTo- <2YY 6 ' 7 

### /f>^ 9X /J.o < 2 /<\< P
. 7 / ?V9
. <s ~ <ZSY .T V J " 7 

### / ?„. a • 3 /£o &o9. Y JSZ> XV 7 6 c 

### S~ 1



### / irr ' / • J •y^ y 

### 3SY &a 1Y 6 " 

### /^Z > 3 . 

### JT-

Z JYO &C3 v 5 T 

### YY ti > 

### /os- /.G > 

### aa Ce (



## - , . 1

### E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n Ru n Numbe r Clien t Facilit yLocatio n Sourc e Dal e Operato r Stac k Dia . StartTime Sto p Time Barometri c Pressure

### j ?9v ^ 

### C> Stati c Pressure (+/-

) —O m T*A . Sachet XC Probe/Pito tNumbe rX- / S Plto tCoemcleii t Filte rBo xNo . Mete rBo xNo . 

### o.-zy LEA KCHECK S I n "H g INITIA L VAC . / &In . MI D VAC . In . FINA L VAC . / 6 In . C F M 0,00 / C F M• — 

### //iff- a C F M O.Ct ) < INIT . PITO T FINA L PIT O 

### •III
. Orific e Coefficien t(Y ) (?,/?> ' ' / Delt a H @ J) , Nozzl e Size/No . 

### t?,£gT> FILTE RDAT A

XA D Thermocoupl e ID : p'/

J ?jy K NUMBER * 

### mmm IM I INGL KVO l S USlf r



### a PINA L

•3 -

SILIC AGE L Fina l Purg eRate
_ VUIP I I. I'OI Nr CLOC K

TIM E VEtocrr v

11EA& I»elll P inw t ORIFIC E

MI.IfeR\O I l>ill» H i n w

e HASMI-TF R 

### TEMPERATUR E READINGS
. " F v1 - ""ii'iriimn r PUM P VACOO M COMMENT S VUIP I I. I'OI Nr CLOC K

TIM E VEtocrr v

11EA& I»elll P inw t ORIFIC E

MI.IfeR\O I l>ill» H i n w

e TfOJLUM

E 

### w .STACK . PROB E OVE N ORGANI C MOtrtJL E GASMETgf t ""ii'iriimn r PUM P VACOO M COMMENT S VUIP I I. I'OI Nr CLOC K

TIM E VEtocrr v

11EA& I»elll P inw t ORIFIC E

MI.IfeR\O I l>ill» H i n w

e TfOJLUM

E 

### w .STACK . PROB E OVE N ORGANI C MOtrtJL E IMl - I N OU T ""ii'iriimn r PUM P VACOO M COMMENT S 

### A/ o.;r ? /.A 6SA77 7 ,7*£> v . o 

### X A T 0,7 J Ar ,2Y 7 j/. a $ 

### O , 5ks " 

### A8 f/tfn"/. (£> YoS AST) «#5C > ,5" 7 7 3 - f- 0 

### 7 /Z,£> J.<\ C

O S ' O , / l



### /o'7 .2</V 6>d Mc 7o /v.o
o <i.C

> 

### /

7 / n 9 0 . 

### ' 7 79, /3.a 76' 0
. 7iS " "zC o 

### 7 V C.S9 /
. - 1 7/6
. feV1 <?? / £</</ 

### «^? » 7 £ ^ r " JL 

### 0.7JT /.(« 7/9
. < 7 7t ^ /3.Q /lo Cs.VJ /

7 7 ^

?
. 3 

# 1 , 3 7S * Y<y.a <3
. A9 A'<9 ,

### V
. 2 y / :r v .9 9 /.T.cs

, r /-TT ) 

### 7 ^ 3US
. f Yo(f> & / 

### ^ / V I 

### / ^ r 7<&o.< r ^?y y /s. s~ RlHsf c Orsa

t 0 2 

### sx

i-i'

### Uni t4 , Conditio n 1 MULTI-METAL S FIEL D DAT A

S:VSTACKJOB\2003\onyxBP\repoiWlysheels.doc

### Metho d 2 9 Metal s Samplin g Parameter s UNI T4 - Conditio n 1 Ru n No . U4-C1-R 1 U4-C1-R 2 U4-C1-R 3 Dat e 16-Sep-0 3 16-Sep-0 3 17-Sep-0 3 StartTim e Unit s 101 5 164 5 80 0 Sto p Tim e 130 9 192 3 103 9 AVG S Nozzl e Diamete r inche s 0.31 5 0.31 5 0.31 5 0.31 5 Barometri c Pressur e in . H g 29.7 0 29.7 0 29.7 0 29.7 0 Ne tSamplin g Tim e min . 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dc f 108.71 3 105.73 4 99.98 6 104.81 1 Avg . DG M Temp . ° F 94. 9 89. 3 74. 3 86. 1 Av g Delt a H i n H 2 0 2.8 3 2.6 9 2.4 5 2.6 6 Av g Delt a H in . H g 0.207 7 0.197 9 0.180 1 0.195 3 DG M Calibratio n Facto r 

# - 0.975 3 0.975 3 0.975 3 0.975 3 Ga s Sampl e Volum e dsc f 100.85 1 99.05 9 96.24 7 98.71 9 Tota l Wate rCollecte d m L 1355. 5 1350. 3 1327. 0 1344. 3 Volum e ofWate rVapo r sc f 63.91 2 63.66 7 62.56 8 63.38 2 Moistur e (measured ) % V/ V 38. 8 39. 1 39. 4 39. 1 Moistur e ( @ saturation ) % v/v 100. 8 100. 9 100. 9 100. 9 Dr yMol e Fraction , 100-% N 0.612 1 0.608 7 0.606 0 0.609 0 C 0 2at Stac k %dr y 5.0 0 5.2 0 5.5 0 5.2 3 0 2at Stac k %dr y 13.0 0 13.0 0 12.7 0 12.9 0 C O + N 2 % dry 82.0 0 81.8 0 81.8 0 81.8 7 Dr yMolecula rWeigh t Ib/lb-mol e 29.3 2 29.3 5 29.3 9 29.3 5 We tMolecula rWeigh t Ib/lb-mol e 24.9 3 24.9 1 24.9 0 24.9 1 Exces s Ai rat Stac k % 150. 3 151. 2 142. 8 148. 1 Stac k Diamete r inche s 48. 0 48. 0 48. 0 48. 0 Stac k Are a sq . in . 1809. 6 1809. 6 1809. 6 1809. 6 Stati c Pressur e i n H 2 0 -0.4 2 -0.5 2 -0.5 2 -0.4 9 Stac k Pressur e in . H g 29.6 7 29.6 6 29.6 6 29.6 6 Avg . Stac k

Temp . ° F 408. 7 406. 8 400. 8 405. 4 Avg . Sqroo tofDelt a P — 0.866 3 0.861 0 0.873 3 0.866 9 SD E Averag e 25.53 3 25.34 9 25.62 2 25.50 1 PitotCoefficien t — 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 4,04 6 4,01 8 4,06 3 4,04 2 Stac k Flowrat e wetacf m 50,84 1 50,49 8 51,05 1 50,79 7 Stac k Flowrat e we tscf m 30,64 3 30,49 3 31,04 2 30,72 6 Stac k Flowrat e dscf m 18,75 7 18,56 3 18,81 3 18,71 1 Isokinetic s % 10 4 10 3 9 9 10 2 Mete rBo xNo . ~ 8060 4 8060 4 8060 4 — Delt a H @ i n H 2 0 2.004 7 2.004 7 2.004 7 

# - Fiel d Q AYq c ~ 1.002 5 1.000 7 0.995 4 0.999 5 [Deviation ] Pre- Y % 2.79 % 2.60 % 2.06 % 2.48 % 

### S:\STACK\JOB\2003\onyxRP\xldata\Sep t03\[M2 9 U 4 C 1 .xlsJEMISSpg

l

### Uni t4 - Conditio n 1-RM2 9 RU N I AVG S - - METAL S RU N 2 AVG S - - METAL S RUN 3 AVGS--METAL S 

### P T Delt aP SQR

T Deli aP DG

M I N DG M OU T Delt aH STAC

K TEM P Deli aP SQR

T Deli aP DG

M I N DG M OU T Delt aH STAC

K TEM P Delt aP SQR

T Delt aP DG

M IN DG

M OU T Delt aH STAC

K TEM P a 1 0.7 6 0.871 8 6

8 6 7 2.8 0 40 6 0.6 7 0.818

5 9 2 9 1 2.5 0 40 2 0.7 4 0.860

2 6 3 6 2 2.4 0 395
. a 2 0.8 2 0.905

5 9 3 8 3 3.0 0 40 7 0.8 2 0.905

5 9 1 9 0 3.0 0 40 4 0.81 0.900

0 7 0 6 5 2.6 0 39 7 a 3 0.9 2 0.959

2 9 6 8 5 3.4 0 40 9 0.9 4 0.969

5 9 1 8 9 3.5 0 40 8 0.8 7 0.932

7 7 3 6 7 2.8 0 401 a 4 0.9 2 0.959

2 9 8 8 7 3.4 0 41 0 0.8

3 0.911 0 9

2 8 9 3.1 0 40

9 0.8 4 0.916

5 7 4 6 8 2.7 0 40 4 a 5 0.7 5 0.866

0 10 2 9 0 2.8 0 41 0 0.4

8 0.692

8 9 3 9 0 1.8 0 40 9 0.7 6 0.871 8 7

6 7 0 2.4 0 40 4 a 6 0.6 2 0.787

4 10 2 9 1 2.3 0 40 5 0.5 8 0.761 6 9

2 9 0 2.1 0 40

5 0.6 0 0.774

6 7 7 71 1.9

0 40 0 a 7 0.6 3 0.793

7 9 4 9 2 2.3 0 40 9 0.7 8 0.883

2 8 6 8 5 2.9 0 40 0 0.6 6 0.812

4 7 5 7 4 2.1 0 40

2 a 8 0.7 5 0.866

0 9 9 9 4 2.8 0 40 6 0.8 0 0.894

4 8 7 8 5 3.0 0 40 8 0.81 0.900

0 7 8 7 5 2.6 0 401 a 9 0.8 2 0.905

5 10 6 9 6 3.1 0 40

8 0.8 6 0.927

4 9 0 8 6 2.9 0 41 3 0.8

5 0.922

0 8 0 7 6 2.7 0 40 2 a1 0 0.8

0 0.894

4 11 0 9

8 3.1 0 41 0 0.8 8 0.9381 9

1 8 6 3.0 0 41 3 0.8

3 0.911 0 8

2 7 8 2.7 0 40 3 a1 1 0.7

5 0.866

0 11 2 10

1 2.9 0 41 2 0.7

2 0.848

5 9 1 8 6 2.4 0 41 1 0.7

6 0.871 8 8

4 7 9 2.4 0 401 at 2 0.5 2 0.721 1 11 1 10 2 2.0 0 41 2 0.61 0.781 0 9 2 8 7 2.1 0 40

0 0.6 5 0.806

2 8 5 8 0 2.1 0 40

0 b l 0.000

0 0.000 0 0.000 0 b 2 0.000

0 0.000 0 0.000 0 b 3 0.000

0 0.000 0 0.000 0 b 4 0.000

0 0.000 0 0.000 0 b 5 0.000

0 0.000 0 0.000 0 b 6 0.000

0 0.000 0 0.000 0 b 7 0.000

0 0.000 0 0.000 0 b 8 0.000

0 0.000 0 0.000 0 b 9 0.000

0 0.000 0 0.000 0 b1 0 0.000

0 0.000 0 0.000 0 b l 1 0.000

0 0.000 0 0.000 0 b1 2 0.000

0 0.000 0 0.000 0

A V G 0.7 6 0.866 3 94. 9 2.8 3 40 9 0.7 5 0.861 0 89. 3 2.6 9 40 7 0.7 7 0.873 3 74. 3 2.4 5 40 1

### E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Traii i Ru n Numbe r£J V" C ^ Clien tt3 -^y> t Facilit yLocatio n vS^^-fig:/ -7~£ - Soui-ce Date _ Operato r£1$ Slac k Dia . - In . ¥ff " StartTim e Sto p Tim e 

### &3L Barometri c Pressure/c v Stati c Pressure(+/•

) —^>,y 2 Probe/Pito tNumbe r^ r *--^ » Plto tCoemden t£>. fp V Filte rBoxNo . /y^ 7/ Mete rBoxNo . 

### "g&Ccl'/ LEA KCHECK S i n "H g INITIA L VAC . /S"

In . MI D VAC . In . In . 

### C F Ma>coz C F M FINA LVAC . /J j INIT. PITO T . CFMC. gtf < FINA LPITOTi^T -- n Orific eCoefriclen t(V)Q , * 7 V^ J Delt a H @ ^.OP y? Nozzl eSize/No . _ XA D Thermocoupl c ID : Im p Outle tT C ID : FILTE RDAT A AN 'tlMnER TAR E 

### * , IMPINGERVOL'S . INIT,


### 0 SCO FINAL, .

SILICA GE L 

### 3IZ I VACUU M RiHsK l

I S / O D 

### 7 « H Orsa t



### -C o

Co /3.t > Ina lPurg eRat e 'Ina lP H SAMPL E POINT CLOC K

TIM E •VELOCITY

De'Li Pln* c ORIFIC E

METt RVO L ijeltaH , nin e UASMETS R

VOV'M K ft*' STAC K TEMPERATUR E READINGS . » F PROB E OVE N ORGANI C MODUL E IMP GA S METE R ^ I N OU T COMMENT S 

### o77T< ,A&L &5L 

### 4JL

3iQ 3 7 ^- T ?LY7 3 - J 

### 2 ^ Jo ycu. 7 W 7 yo-o < 7 

### 22L 3L 7/ o ;,.s\s~ £ 5 1 i 2 . 

### yos: ZOe L 

### . 2 / P& <i,/<r 

### W,8 '/<3<P JS/ ^ 2 , ?9 o 

### S o SCS(b 2&- 7 9

a 

### .go . 4 , / 'Ye ? Sr ; o - a r 

### GO ILL.

### & P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n Ru n Numbe r Clien t Facilit yLocatio n Sourc e Dal e Operato r StackDIa,-In . ~ l/ $ " StartTim e Sto p Tim ? Barometri c Pressure »29
. Co O Stati c Pressure (+/-

) -(lb. SSL Probe/Pito tNumbe r

### yCfJ'-^~ -X Pilo tCoemden tQ tft/ Filte rBo i No . 

### Wff-J. I Mete rBo xNo . &Qtt Q>

l ( LEA KCHECK S I n "H g

INITIA L VAC . /s T MI D VAC . FINA L VAC . J<i CF M0.00 3 CF M CFMO.Of U INIT . PITO T/ FINA L PlTOTi ^ C Orific e Coefnden t(Y ) c > Delt a I I @ Nozzl e Size/No . 

### -ml- FILTE RDAT A



### Q.3/J XA D Thermocoupl e ID : / ( NUMBE R TAR E IMPINGE RVOL'S . INIT. FINA L „

4 3 3

Z E E

SILIC A GE L Orsa t 

### QOl 0 2

ia- 7
Fina l Purg eRat e
1 AM PII . i oir . 1 CLOC K

TIM E V M OT n

HEA D Del l it* , 11

1 w t 

### ouir u K MfI*R\O I IM l iH .lnw c OA< - M I If R 

### TEMPERATUR E READINGS
. ° F POM P VACl'O M COMMENT S 1 AM PII . i oir . 1 CLOC K

TIM E V M OT n

HEA D Del l it* , 11

1 w t 

### ouir u K MfI*R\O I IM l iH .lnw c VOLUM E



### (V STA < K PROB E OVE N ORGANI C MODUL E GA &M .Ktl - H POM P VACl'O M COMMENT S 1 AM PII . i oir . 1 CLOC K

TIM E V M OT n

HEA D Del l it* , 11

1 w t 

### ouir u K MfI*R\O I IM l iH .lnw c VOLUM E



### (V STA < K PROB E OVE N ORGANI C MODUL E IM P It * POM P VACl'O M COMMENT S
O 

### o.7Y J.Y /oa. ?xo £V/ -?jr r 

### .M/A <S>. 5 /• J A . 

### 8 7 <J.Y& \ 7c 3 

### 6v T <Z.(S 3 ,.?-<

3 

### (S.U

7 St.* //7. v5 " 

### 2Y?



# - ,5 7 •2 ? 6 7 9 . 0 

### H 3 o 

### O
. ft V .0 .7 /,2C>.3 •/£>< / 

### 2STs> 7 V ^ 8 - 

### Q. O S O , 7 Co 

### a,H y o y 

### <3CT 3 ' sz, 7G 7 £ 5 

### L Sn «. CoO / , 9 V V ^ JIY 6 « r & 7 / 7 . 0 

### A1 (oO 3-1 )SC.), 07 ,25b - 7 r 7</ 7. O 

### ;2 O.S 7 7 ? 7S ° 1
. 6

« ? 

### ifO 0 . a r 

### 2.'7 /&7 , . '-f 7 6 ? . 0 v 

### /o r vtf.'? 

### .P. 7 /76>.C> . c ?

t ) ~ 

### /Od 0 . 7 ^ 

### /8Y. K ^ Y 7 fiY 7 9 s.«r " 

### G / / o 7 . / /«?.? , O 

### Yco c ? y r 5?.5 ~ 3 . 0 

### /olO — — I

### i

E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin gTrai n Ru nNumbe

r Clien t Facilit yLocatio n Sourc e Date Operato r Barometri cPressur

eJ9.7Q Stati cPressur

e(+/- ) —

### Q.^SH. Probe/Pito

tNumbe r Plto tCoefficien

tO

&</ Filte rBo xNo .

### /7?fi~J/ Mete rBo xNo. gfcVS O <f LEA KCHECK S I n"H g INITIA L VAC . SS~In

. MIUVAC . In . FINAL VAC . /Q

In

. CF M

INIT. PITOT "FINA L PITCHf- V

FILTERDAT A Slac kDin. - In

. 

### Yt" Delt aI I@ a o V7 NUMBE R TAR E Star tTim e Nozzl eSize/No . O t -QlQ 6? Sto p Tim e XAD Thermocoupl eID : ^SyCA IWI'lNl.F RVOL' S INIT .



### - o o» 

### sa>a> FTNAL .

O k 

### £10

SILICA PE L SAMPI1 . 

### roin i ( iOf

K TIM E 

### v i i ocn v

II I\\ ) Hella Pn tVr c OriFIC E M lIERVOI Dfllall.in-w c GAS. METE R 

### TEMPERATUR E READINGS
. ° F PUM; P VACUU M COMMA S SAMPI1 . 

### roin i ( iOf

K TIM E 

### v i i ocn v

II I\\ ) Hella Pn tVr c OriFIC E M lIERVOI Dfllall.in-w c VOLUM E

« » STACK . PROB E OVE N ORGANI C MODULI ! IM

P GA S METE R PUM; P VACUU M COMMA S SAMPI1 . 

### roin i ( iOf

K TIM E 

### v i i ocn v

II I\\ ) Hella Pn tVr c OriFIC E M lIERVOI Dfllall.in-w c VOLUM E

« » STACK . PROB E OVE N ORGANI C MODULI ! IM

P I

N OU T PUM; P

VACUU M COMMA S
A1 

### o O.(o7 J.S? 

### v c 

### ;ycic< - </OJL A T I M / A 92. 6>.ST ,x 3
. 

### o /'OiM ,cT " J S 7 I 

### >r / 9 / ?<? 

### 0,99 / OS7o 

### jss X 9 9,,5 " y .<?

o /O&J.

### o- AGO Sl> 

### Sf 9 y o O .

### </F /03J .S" 

### 9< > fn . 

### c5

~ i-> 

### o..«v a y & r ac 0 o 

### 5 7 A O 0.7 8 /CWC . 7S I 

### jsst
%
.... 

### 7 0 Cb. KCi /eX ^S. fo 

### Y

a* 

### jss- 9 . o 3 O .

### <T

6 /c 5<£>.r \ 1 2,5£> <YX * t T 

### 9 o C U T .<?. . C l /6?</. / 

### V/J SiVC J7SX- 

### 9 / 5 ~ :),Z 2 3LM /av.S,&~ H / i A S l 

### YJ y / cT. O Co <ZU.n 

### o . ^ ,r?, / YOQ 

### ^ y y 6^/ 

### IT 7 • 

### -to?"? , <^ 7 Orsat 

### mm

### Uni t4 , Conditio n 2 PCDD/PCD FFIEL D DAT AMetho d0023 A Samplin gParameter s Uni t4 - Conditio n2-R M0023 A 

### Ru n No
. C2-R 1 C2-R 2 C2-R 3 Dat e 17-Sep-0 3 17-Sep-0 3 18-Sep-0 3 Star tTim e Unit s 114 5 154 0 81 0 Sto p Tim e 150 4 184 9 111 8 AVG S Nozzl e Diamete r inche s 0.28 0 0.28 0 0.28 0 0.28 0 Barometri cPressur e in
. H g 29.6 0 29.6 0 29.5 5 29.5 8 Ne tSamplin g Tim e min
. 180. 0 180. 0 180. 0 180. 0 Volum e Metere d dc f 119.50 6 120.29 5 118.75 9 119.52 0 Avg
. DG M Temp
. ° F 92. 9 94. 5 80. 3 89. 2 Av g Delt aH i n H 2 

### 0 1.6 1 1.6 3 1.6 0 1.6 1 Av g Delt aH in
. H g 0.118 3 0.120 1 0.117 6 0.118 7 D G M Calibratio n Facto r ~ 

### 0.981 4 0.981 4 0.981 4 0.981 4 G a s Sampl e Volum e dsc f 111.25 1 111.67 3 112.92 9 111.95 1 Tota l Wate rCollecte d m L 1571. 0 1626. 7 1542. 1 1579. 9 Volum e o fWate rVapo r sc f 74.07 3 76.69 9 72.71 0 74.49 4 Moistur e (measured ) % v/v 40. 0 40. 7 39. 2 40. 0 Moistur e ( @ saturation ) % v/v 101. 2 101. 2 101. 4 101. 3 Dr yMol e Fraction , 100-% M — 

### 0.600 3 0.592 8 0.608 3 0.600 5 C 0 2

### a tStac k %dr y 5.2 0 5.5 0 4.2 0 4.9 7 0 2

### a tStac k %dr y 12.5 0 12.1 0 13.0 0 12.5 3 C O + N 2 

### % dr y 82.3 0 82.4 0 82.8 0 82.5 0 Dr yMolecula rWeigh t Ib/lb-mol e 29.3 3 29.3 6 29.1 9 29.3 0 We tMolecula rWeigh t Ib/lb-mol e 24.8 0 24.7 4 24.8 1 24.7 8 Exces s Ai ra tStac k % 135. 5 125. 3 146. 7 135. 9 Stac k Diamete r inche s 48. 0 48. 0 48. 0 48. 0 Stac k Are a sq . in
. 1809. 6 1809. 6 1809. 6 1809. 6 Stati cPressur e i n H 2 

### 0 -0.5 1 -0.5 4 -0.5 0 -0.5 2 Stac k Pressur e in
. H g 29.5 6 29.5 6 29.5 1 29.5 5 Avg
. Stac k

Temp
. ° F 404. 7 408. 3 404. 3 405. 7 Avg
. Sqroo to fDelt aP 

### - - 0.863 6 0.860 7 0.863 1 0.862 5 S D E Averag e 

# - 25.39 6 25.36 0 25.37 5 25.37 7 Pito tCoefficien t ~ 

### 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 4,04 1 4,04 1 4,04 1 4,04 1 Stac k Flowrat e we tacf m 50,78 6 50,78 5 50,78 0 50,78 4 Stac k Flowrat e we tscf m 30,64 2 30,51 2 30,60 2 30,58 5 Stac k Flowrat e dscf m 18,39 4 18,08 8 18,61 6 18,36 6 Isokinetic s % 9 9 10 1 9 9 10 0 Mete rBo xNo
. — 

### 8010 2 8010 2 8010 2 ~ 

### Delt aH @ in
. H g 2.059 0 2.059 0 2.059 0 ~ 

### Fiel d Q AYq c — 

### 1.02 0 1.02 2 1.01 5 1.01 9 [Deviation ] Pre- Y 

### % 3.9 % 4.i % 3.4 % 3.8 % S:\STACKVIOB\2003\onyxRP\xldata\Sep t03\[M2 3 U 4 C2.xls]AVG SP T

a6 

### b 3 b 5 b 6 AV G DP

0.6 2 0.6 9 0.8 2 0.8 6 0.81 0.7 5 0.6 0 0.7 5 0.8 0 0.33 0.80 0.6 5
0.7 5 

### Uni t4 - Conditio n 2-R M 0023 A

RU N 1 AVG S - - PCDDs/PCDF s SQR T DP 0,787 4 0.830 7 0.9055 0.927 4 0.900 0 0.866 0 0.774 6 0.866 0 0.894 4 0.911 0 0.894 4 0.806 2
0.863 6 DG M

I N 8 3 8 7 9 2 9 3 9 5 9 8 9 7 9 8 99 99 9 9
92. 9 DG M

OU T 8 3 8 4 8 7 8 9 90 9 2 9 4 9 4 9 5 9 5 9 5 9 5 DH

1.3 0 1.4 0 1.7 0 1.8 0 1.7 0 1.6 0 1.3 0 1.7 0 1.8 0 1.8 0 1.8 0 1.4 0 

### 1.6 1 STAC K

TEM P 40 0 40 0 40 4 40 5 406 40 8 39 8 40 3 40 5 409 41 1 40 7
40 5 DP

0.6 3 0.7 4 0.8 2 0.83 . 0.8 3 0.6 8 0.4 6 0.6 5 0.8 6 0.8 4 0.8 6 0.7 5 RU N 2 AVG S - - PCDDs/PCDF s

0.7 5 SQR T

DP 0.793 7 0.860 2 0.905 5 0.911 0 0.911 0 0.824 6 0.678 2 0.806 2 0.927 4 0.916 5 0.927 4 0.866 0
0.860 7 DGM

I N 9 2 9 5 9 7 9 7 9 7 9 7 9 4 9 6 9 7
_ 9 6 9 7 9 7
94. 5 DGM

OU T 9 2 9 2 9 3 9 4 9 4 9 4 9 4 9 3 9 3 9 2 9 2 9 2 D

H 1.4 0 1.6 0 1.8 0 1.8 0 1.8 0 1.5 0 1.0 0 1.4 0 1.9 0 1.8 0 1.9 0 1.7 0
1.63 STAC K

TEM P 40 0 40 7 41 1 412 412 412 40 2 40 3 41 0 412 41 0 40 8
40 8 DP

0.4 5 0.6 8 0.8 0 0.8 6 0.91 0.8 5 0.5 5 0.7 0 0.8 4 0.8 4 0.8 4 0.7 0
0.7 5 RU N 3 AVG S - - PCDDs/PCDF s

SQR T D P 0.670 8 0.824 6 0.894 4 0.927 4 0.9539 0.922 0 0.741 6 0.836 7 0.916 5 0.916 5 0.916 5 0.836 7
0.863 1 DG M

I N 67 76 78 7 9 8 3 8 4 8 1 8 7 8 6 8 8 9 0 9 1
80. 3 DG M

OU T 6 6 70 7 2 7 4 76 7 8 8 0 8 4 8 2 83 85 86 D H

1.0 0 1.4 0 1.7 0 1.8 0 1.9 0 1.8 0 1.2 0 1.5 0 1.8 0 1.8 0 1.8 0 1.5 0
1.6 0 STAC K

TEM P 400 40 2 40 3 40 4 40 4 40 5 40 0 40 0 40 7 40 8 409 409
40 4

### P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n Ru n Numbe r Clien t Facilit yLocatio n Sourc e Date Operato r Slac k Ola . - lu . StartTime Sto p Tim e Barometri c Pressure o j *? . t^j i Q

•7 T — Siali c Pressure (+/- ) —O. S'I Scrtcif l <••»/•

•TL Probe/Pilo tNumber_ Pilo tCoeriicicu t Filte rBoxNo . _ Mete rBoxNo . LEA KCHECK S I n "H g INITIA L VAC . MI U VAC . FINA L VAC . /$ ~

+ INIT . PITO T C F M - CFMfl.tSO /


### //yrAte' Y Orific e Coefficien t(Y)C? . 9?/* ^ Delt a H ® 

### J?.j>S?'a Noul e Slie/No . 

### &,J.8C> FINA L PITOT><^- T FILTE RDAT A

XA D Thermocoupl e II) : XAf?- £S~ Ini p Outle tTCID : NUMBE R STARK; : )MHN<.lH\OL S INIT , C 3 FINAL. . 

### i I E RlftSfc . 

### t25 - 3 £

SILIC A PE L 

### TTTr

V Orsa

t OA . 

## £>

Fina l Purg e Rnte
_ Fina l P H SAMI'l t POIN I < H Xh

TIM E VKLQC1T V HEA D ItelldlMl l \lt ORIFIC E

.MI.IFRVO I 

### I ) IllK .llKf l O A S Mnu t

VOLUM E SlAC k 

### TEMPERATUR E READINGS
. ° F
PROB E 0V £ N ORtiANI C MODUL E I M P GASMETE R I N O W PUM P

YACOU M roMMFNr s 

### o <3. 6 2 

### Ma ~3vo TTT gv 3 7 Q /JT ' 2 1 

### ;?9c :3 . c > 

### YG»Y ' 7 S T UL 799, 

### <p Yt>r E y £ 2T1 / 3 A

_ L 

### c?
. J73~



# 131 57t3
. 2-

.ay?. ? 

### Mo, 3 

### .M zjy__ yg> r

a s y a r vof

### i lit - Vo7
_ 

### 3*£Y_



### £Y* M l — < 9 

## /< * / A O E E

/ / • c T 

### / / , o r

### E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T
Barometri c Pressure

### $frS S*" " Samplin g Trai n Ru n Numbe r Clien tCX^VX Facilit yLocatio n Sourc e Dat e Operato r Stac k Dia.-Iii . StartTim e Sto p Tim e Stati c Pressure «/- ) —d ,J"fc > Probe/Pilo tNumbe rC'.S'""/ — Pito tCoefficien t0. ' Filte rBo i No . Mete rBoxNo . CF M LEA KCHECK S I n "H g INITIA L VAC , /

S~InMI D VAC . ^ - In . FINA L VAC . I

In , + INIT . PITO T-^FINA L P1T C CFMQ.QC K CFMfl . CC

f

Orific e Coefncien t(Y ) CP.^y/ y Dtl u 1 1 

### @ Ag>.Ty<= > Nozzl e Size/No . C.?.^?y^ > FILTE RDAT A

XA D Tliermocoupl e ID;^C4^p . eg. IDit . €> 

### /OO
m m .

FINAl i 7 92* 

### 17 6

SILICA GE L RlNsR .

3 7 Orsa t

C o i

13- ° 

# \>.r Fina l Purg e Rat e
J .U1P I t pon s i ' !.() { K

11M K VMoci n

HEA D Dtl'l P llfc t ORiriL L

MI'.IF R\O I Del l til . I n IT

C LASMHU t ^-i— " ^ 

### TEMPERATUR E RE A 3INGS
. ° F • H I f MiWimu L PUM P VACUU M > « * ,COMMENTS ,' J .U1P I t pon s i ' !.() { K

11M K VMoci n

HEA D Dtl'l P llfc t ORiriL L

MI'.IF R\O I Del l til . I n IT

C •VOLIIM T

fl ' STAC K PROB E OVF N ORGANI C MODUL E I M P I I ..GAS M I N BTE R

O U T f

MiWimu L PUM P VACUU M > « * ,COMMENTS ,' / ? / 

### O .</.* - /
. O 

### / /
. 7 *1 jyy ^ (nCs> 

### 8 , a

/ . r /.< / / I . n Y£>£ JW2. ,2</7 •SXo 

### ^• y 7C 

### 70s 3 

### o Sto 

### /
. 7 

## %.& St? 

### 7& 7J ? w o 

### V O Bio 

### A ? ' 3 7 . ( .2</9 J ,<r/> 

### J^ 2 '7 9 • ? y /£". O a / 

### 7.9 - Yew 2V2 

### ^7 " 7<

### 5 » / T T

k 6 

### o.a r fi> 6 

### 8 ? /l T.JT

^ f l - 

### 9a /:,; > ' 7CY.7Y2 y a o *?y y 6 ( 

### 3 / / / . C j 3 7Q .Y Y a o 

### ?? 7 ^ y

/xc> 

### * S
. / Y£>7 

### § J i y 7 9
. & .^y' 7 . C 7 

### /7. O yo? , ,2YC ( 

### /7, 0 h
. T o i f ' ^ " fc3.e>."f Y d ? 2YY J Z ?«3 , </9 d — - • —

„

••

iE P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T



### Ac-/- , y c Samplin gTrai nM.X&A RunNumbe

r-

C-Z- 'R.JL 

### <•'»«»<O^H-K Facilit yLocalion'~S < <-

Lft; |< Sourc e Dal e__ OperalorfjQ SlackDia . - in . •' ' SlartTlme/'f/ l Slo p Tim e/'/V p

### /ft</9 Us?/*? Barometri cPressur e

### J?- 1 

### ?. &O Stati cPressur e(+/- ) Q . v g~ V Probe/Pito

tNumbe r,JU,T'£-£ Plto lCoefficien

td). ^ Filte rBo xNo. Hj$-iT~ Mete rBo xNo . LEA KCHECK S I n"Hg INITIA L VAC . /J ~In

. CF M0.003 . MI D VAC . • —

In , CF M FINAL VAC . /O

in. CF Mfri C O 3
Orinc eCoefficien

t(V ) Q , 9 g/ y DeliaH @ 

### ^.0,Sf<i Nozzl eSize/No . tf.-Zff- D

SZO/GZ- lNIT.PITOIV . FINAL PITO*-"^ - FILTE RDAT A
XA D Thermocoupl

eID : Im p PulletT C ID ; £-2\2S~ IMPINGERVOL'S . .INIT , 

### 0 'Ci O FINAL ; BINS E 

### " 7 c o

SILICA GE L Fina lP H 

### 4 ^ Orsa

t ycb'ii :

p . /

e SU1I( t I'OIN I CLOC K TIM S VELOCIT Y

HEA D Del lil' . I nwt! ORIFIC E M lI f RYO l l>ellulf.iri<r

c CASMF.IE K YOl.VM R « » TEMPERATUR E READINGS . ° F

STACK , PROB E OVE N ORCANI C MODUL E IM P I N 

### PUM P

VACUU M COMMENT S z o : 

### wt/ c v?r ) 

### •/to o A S P 2 2 1 

### 3 T SI ? 3 £ 7/ Q r& 

### tLLL 2X1 MS X £ L 

### 66 7<sr /o<\ /AQ L&SL
/ &?. r 

### i t / . y



### /
. o

i t 92 .0

,1 

## i?/V v >y^, o 

### '<n, -7

y p ^ ^ y ? ,3, 3 i v. x2yz
_ 

### JL<£3L 2HCe £V7 (h

2 6LL.
6?6 tt- <£><e M l S z £ 2
_

'.M'l'MIMMI lMil lIt'l lUl lHi t11 ! U11 1 tl II IIII I• 1 1

### Uni t4 , Conditio n 2 MULT I METAL S FIEL D DAT A

S:\STACKUOB\2003\onyxRP\repolMlysheels.dK ; Novembe r2003

### Metho d 2 9 Metal s Samplin g Parameter s UNI T4 - Conditio n 2 Ru n No
. Ru n 1 Ru n 2 Ru n 3 Dat e 17-Sep-0 3 17-Sep-0 3 18-Sep-0 3 Star tTim e Unit s 1145 154 0 081 0 Sto p Tim e 1434 181 9 104 8 AVG S Nozzl e Diamete r inche s 0.28 2 0.28 2 0.28 2 0.28 2 Barometri cPressur e in
. H g 29.6 0 29.6 0 29.5 5 29.5 8 NetSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dc f 81.45 2 82.62 9 81.27 8 81.78 6 Avg
. DG M Temp
. ° F 89. 9 93. 3 78. 3 87. 1 Av g Delt aH i n H 2 

### 0 1.60 1.60 1.58 1.59 Av g Delt aH in
. H g 0.117 6 0.117 6 0.116 4 0.1172 DG M Calibratio n Facto r — 

### 0.975 3 0.975 3 0.975 3 0.975 3 Ga s Sampl e Volum e dsc f 75.76 4 76.39 0 77.09 6 76.41 7 Tota l Wate rCollecte d m L 1060. 8 1113. 9 1041. 5 1072. 1 Volum e o

fWate rVapo r scf 50.01 7 52.52 0 49.10 7 50.54 8 Moisture (measured ) % v/ v 39. 8 40. 7 38. 9 39. 8 Moisture ( @ saturation ) % v/ v 101. 2 101. 2 101. 4 101. 3 Dr yMol e Fraction , 100-%r v 

# - 0.602 3 0.592 6 0.610 9 0.601 9 C 0 2

### a tStac k %dry 5.2 0 5.5 0 4.2 0 4.9 7 0 2

### a tStac k % dr y 12.5 0 12.1 0 13.0 0 12.5 3 C O + N 2 

### % dr y 82.3 0 82.4 0 82.8 0 82.5 0 Dr yMolecula rWeigh t Ib/lb-mol e 29 .3 3 29.3 6 29 .1 9 29.3 0 WetMolecula rWeigh t Ib/lb-mol e 24.8 3 24.7 3 24.8 4 24.8 0 Exces s Ai ra

tStac k o

/ 10 

### 135. 5 125. 3 146. 7 135. 9 Stac k Diamete r inche s 48. 0 48. 0 48. 0 48. 0 Stac k Are a sq . in
. 1809. 6 1809. 6 1809. 6 1809. 6 Stati cPressur e i n H 2 

### 0 -0.5 1 -0.5 4 -0.5 0 -0.5 2 Stac k Pressur e in
. H g 29.5 6 29.5 6 29.5 1 29.5 5 Avg
. Stac k

Temp
. ° F 404. 3 408. 8 404. 8 406. 0 Avg
. Sqrooto

fDelt aP



# - 0.861 7 0.850 7 0.864 6 0.859 0 SD E Averag e


# - 25.33 3 25.07 4 25.42 5 25.27 7 PitotCoefficien t



# - 0.84 0.84 0.84 0.84 Stac k Ga s Velocity afp m 4,03 0 3,99 6 4,04 7 4,02 4 Stac k Flowrate wetacf m 50,63 8 50,21 3 50,85 2 50,56 8 Stac k Flowrate wetscf m 30,56 4 30,15 1 30,62 4 30,44 6 Stac k Flowrat e dscf m 18,41 0 17,86 7 18,70 8 18,32 8 Isokinetic s % 

### 9 9 103 10 0 10 1 Mete rBo xNo
. 

# - 8060 4 8060

4 8060

4 — 

### Delt aH @ i n H 2 

### 0 2 .0047 2.0047 2.004 7 

# - Fiel d Q A Yq c ~ 1.005 5 0.9936 0.9950 0.9980 

### [Deviation ] Pre- Y % 3.09% 1.88 % 2.02% 

### 2 .33 % S:\STACKUOB\2003\onyxRP\xldata\Sep t03\[M2 9 U 4 C2.xls)EMISSpg 1E P AISOKINETI C SAMPLIN G -

### FIEL D DAT ASHEE T Samplin g Trai n °l Hu n Numbe r Cllcn l Facilit yLocatio n Sourc e Dnl e Operato r SlackPla . - lu . StartTime Sto p TliiH ' 

### 0

,0 VX
JLLY. 

### 9 fr// a

:i 

## JU1 Barometri c Pressure (j> Q Stati c Pressure (+/-

) 

### "-Q.<S"I Probe/Pilo tMumbe r^AlS; S~~Z. Plto tCoefficien tC*,,^ f Filte rBoxNo . 

### h/B~Xl Meie rBoxNo . 

### 20 (i >0' / LEA KCHECK S I n "H g INITIA L VAC . In . MH ) VAC . 111.. FINA L VAC . ^. O In .

+ INIT . PITO T CFMQ.Oo l CFM(I > ,OC

I CFM O .O i I
"FINA L PITOTv^ - 

### tlSL //v,i ~ iZT?

/& V t2t? y/M.G /f.i<j OriUc e Coefnclen l (Y)Q t <37tC 7 Delt a II ®

J?.0O</Y Nozzl e Size/No . C^ff X FILTERDAT A NUMBER ; 

### mmm IMPlNUltVO I S 1NIT , FlNAl i

C J SCO 

## J2J-

T

Fina l Purg e Ral e
S A MPi t I'DI N I CLOC K

1IM T VIIOCH V

HEA D Uclll l litt i ORIFIC E

M l IfRUl l Htlt«H,lii <T c HA S M r

### i ti t 

### TEMPERATUR E READINGS
. ° F PUM P VACy« M tnllt f COMMENT S S A MPi t I'DI N I CLOC K

1IM T VIIOCH V

HEA D Uclll l litt i ORIFIC E

M l IfRUl l Htlt«H,lii <T c WI.l'V L



## r r STAC K PB O II P OVk N ORGANI C 1 MODULI - j r

\I P . I N KXE R O C T PUM P

VACy« M tnllt f COMMENT S
A| O 

### O. (oX / V 2 /<•> 

### 0

. 79 / , 7 ,<CJZ 

## ? y <3 -Vo ) 

### V 0..&V - 

## sir " -xi •-4? — , — » • • <:/ &

... . 

### T~.h*.l ^(? w 

### / 0 «-d.rtrf <
— • — 

## , , —
, 

### ,223. 2 VJ T , 

# - r. . — • y o O , 

### 7<1

s 

### /.a y o y c2V<i 

# % 7 0 

### 6 o O . 

### '7 & / , <o -yo< y I'lQ,,,., , 

### te •2. 

## o . W /.X YoS > > 

### 5 ^ 

## 9 3 <i , o 

### .3 

## 0
. # o /.V 

## .2jx.r
. & yd 

## 7 r r

### ,& 9 o 

### 7.7 YQb ^ y <> y (*.o 

## < T /<D O 

## 0.7J ' J/7 270, i 

## y o 7 o ?y ? it s 9 y 

# IS 6 0 (r> / / a 0.5* 7 

## /.:< 27 7. X 

## y o / V r 

### 283,339 . — — 

### 1 

### 4 

## mm 7W 7^- Orsa t

I>. <

### Uni t4 - Conditio n 2-Mult i Metal s RU N1 AVG S - - METAL S RU N2 AVG S - - METAL S RU N3 AVG S - - METAL S P T Delt a P SQR T Delt a P DG M

I N DG M

OU T Deli a H STAC K TEM P Delt a P SQR T Deli a P DG M

I N DG M

OU T Delt a H STAC K TEM P Delt a P SQR T Deli a P DG M

I N DG M

OU T Delt a H STAC K TEM P a l 0.6 8 0.824 6 8 2 8 1 1.4 0 40 1 0.7 2 0.848 5 9 1 9 1 1.6 0 40 1 0.6 8 0.824 6 6 9 6 7 1.5 0 40 2 a 2 0.7 9 0.888 8 8 4 8 3 1.7 0 40 0 0.7 7 0.877 5 9 3 9 1 1.7 0 41 0 0.7 8 0.883 2 7 4 7 0 1.6 0 40 3 a 3 0.8 2 0.905 5 8 6 8 4 1.7 0 40 1 0.8 2 0.905 5 9 5 9 2 1.8 0 41 0 0.8 6 0.927 4 7 6 7 2 1.8 0 40 4 a 4 0.8 2 0.905 5 8 8 8 5 1.7 0 40 4 0.8 2 0.905 5 9 8 9 3 1.8 0 41 2 0.8 4 0.916 5 7 8 7 3 1.8 0 40 4 a 5 0.7 6 0.871 8 9 1 8 9 1.6 0 40 9 0.7 0 0.836 7 10 0 9 4 1.5 0 41 3 0.7 0 0.836 7 7 9 7 4 1.5 0 40 6 a 6 0.5 9 0.768 1 9 3 9 0 1.2 0 40 4 0.5 7 0.755 0 10 1 9 6 1.3 0 40 6 0.5 8 0.761 6 8 0 7 6 1.2 0 40 4 a7 0.7 6 0.871 8 9 4 9 3 1.6 0 40 4 0.6 3 0.793 7 9 2 9 1 1.4 0 40 8 0.8 0 0.894 4 7 8 7 8 1.7 0 40 3 a B 0.8 2 0.905 5 9 4 9 3 1.8 0 40 8 0.7 2 0.848 5 9 2 9 1 1.6 0 41 0 0.8 0 0.894 4 8 2 7 9 1.7 0 40 6 a 9 0.8 0 0.894 4 9 5 9 3 1.8 0 40 7 0.8 4 0.916 5 9 3 9 1 1.8 0 41 1 0.8 1 0.900 0 8 4 8 1 1.7 0 40 5 a1 0 0.7 8 0.883 2 9 4 9 2 1.7 0 40 6 0.8 4 0.916 5 9 3 9 1 1.8 0 41 2 0.8 3 0.911 0 8 5 8 2 1.7 0 40 7 a1 1 0.7 5 0.866 0 9 4 9 3 1.7 0 40 7 0.7 1 0.842 6 9 3 9 1 1.6 0 41 2 0.7 8 0.883 2 8 7 8 3 1.6 0 40 9 a1 2 0.5 7 0.755 0 9 4 9 2 1.3 0 40 1 0.5 8 0.761 6 9 4 9 1 1.3 0 40 0 0.5 5 0.741 6 8 8 8 4 1.2 0 40 5 b 1 0.000 0 0.000 0 0.000 0 b 2 0.000 0 0.000 0 0.000 0 b 3 0.000 0 0.000 0 0.000 0 b4 0.000 0 0.000 0 0.000 0 b 5 0.000 0 0.000 0 0.000 0 b 6 0.000 0 0.000 0 0.000 0 b 7 0.000 0 0.000 0 0.000 0 b 8 0.000 0 0.000 0 0.000 0 b 9 0.000 0 0.000 0 0.000 0 b1 0 0.000 0 0.000 0 0.000 0 b1 1 0.000 0 0.000 0 0.000 0 b1 2 0.000 0 0.000 0 0.000 0


### AV G 0 .75 0 .861 7 89. 9 

### 1.60 40 4 0 .73 

### 0.850 7 93.3 

### 1.60 40 9 | | 0.7 5 0.864 6 78 . 3 

### 1.58 40 5

### : P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n 

### .sL1<2 c



### } Ru n Numbe r Clien t0, 0 YX 0 *4-CA-RSL Facilit yLocatio n Ci>\n.c 1 > fTL

### UH1 Sourc e Dnl e Optrnlo r Stac k Din.-In , Startlim e Barometri c Pressure ,Q>Q Stati c Pressure (+/-

) * •Q,S¥ Probe/Pito tNumbe r

### .X-(J~-,^~-~Z. Plto tCoemden tQ Filte rBoxNo . /// j -J / Mete rBo xNo . 

### f£&(W LEA KCHECK S l u "H g INITIA L VAC . In . MI D VAC . III. . lu . CFMO.OQ 3 C F M * FINA L VAC . CFM<3,t3 6 (
INIT . PITO T 

### Jill /<T¥o u/t Orific e Coefficien t, 9 AS ? ? Delt a H @

### .2.06'/7 Noul e Size/No . + FINA L PlTO 'g ^ FILTE RDAT A I S UMBER : STARE S IM l INI.L R VO L 1 INIT. 

## J2
_ z o o

V

### tS C l FI

NA t
I f 

### Juv>

uro- /oo Orsa t



### mm I* ?

Im p Outle tT C ID : 1f Fina l P H SAMPL E roir , i (I OC K

HMf c VELOCIT Y

HEA D Dtln l litw c OriFlC E

MlIMtVO L DrltnH.l u w

c OA S M TI fi t 

### TEMPERATUR E READINGS . ° F niM P VACUU M h-m . COMMENT S SAMPL E roir , i (I OC K

HMf c VELOCIT Y

HEA D Dtln l litw c OriFlC E

MlIMtVO L DrltnH.l u w

c VOLUM E

f f S I U k rjioiii . OVE N ORGANI C MODUL E ...\.GAS.MET.;ER . niM P VACUU M h-m . COMMENT S SAMPL E roir , i (I OC K

HMf c VELOCIT Y

HEA D Dtln l litw c OriFlC E

MlIMtVO L DrltnH.l u w

c VOLUM E

f f S I U k rjioiii . OVE N ORGANI C MODUL E I M P I N otr r niM P VACUU M h-m . COMMENT S

, 3 / O O./J i J s t 'f i «•/& / AJ/ A 

### 4 / a /£> 

### cb .~77 7 Y / O ,<r v 

### ^ / c\. V3L 

### / . fr 

### ^7/7 Y / o .QSV s y ck.o ."KO Ci.

### 82 / . ,?<W . 

### V Y/JL J V Y ? f r § 3 ci. o YO a.T' o 3/J. Y Y l Z Z l Y & a / o o 9<Y G > 

### n ,<?7 / . 3 C ?/9 . / VOCr> a m J O T 

### S ~3 A/ GO n . (oC? 

### / y YCW XYCs a s 7 s . O c 2 7 0 r \ , 7 J i 

### 7- 6 3*/ , 7 H/<5 a s z <s* v 9 / / . , 0 S O 6 , W 

## /. £ V / / < / r / o 0 . S V 

### / ^ * er - Y/JL .OYT a r Y .cx - 

### 93 J - / o o 3.7 / as;?,, ^ Y/JL 2 . Y Y 6 7 / 0 

## / , YOO ors p /•io . 3 <J><<> , 

### Va? ? 4

•

VMiiiiiiiiri^nifTn-rr

pV

E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T iMPlNOfc R VOL'S , Orsa t Samplin g Trail l 

### AiZtl Barometri c Pressure

### tS /iOO I EA KCHECK S I n "H e

S1TIALVAC . /J T In . CF M 1 lNH . I I INA L RlNS E CO Z

### I 02 . Ku n Numbe r( VV- C i ! - AL ? Stati c Pressure W-) - ft. <7i

V

EA KCHECK S I n "H e S1TIALVAC . /J T In . CF M 1 CHen l 

### O. OyX Probe/Pilo tNumbe r

### ^US'S'"2. MI D VAC . In , CF M •- • •?4 r Facilit yLocatio n S'W,, ; { ,T i Pilo tCoefficien td>.^Y FINA L VAC . ( n lit . CFMrt.rtrt t Sourc e C" / FlllerBoxNo . 

### M&~Jll + NIT , PITO Tc. —

FINA L PIT ( + C 3 D«l e

### Illti/oS Mete rBoxNo . 

### jfCY„r>V' 1 + NIT , PITO Tc. —

FINA L PIT ( 

### /OO Opernto r/\i 5 Orific e Coefficien t(Y )

### 0.°ll<;3 FILTE R DAT A ^ « 

### /OQ Slac k Dia.-In . Vft " Delt o H @,?.00 ' / 7 MUMBER TAR E StartTim e CTSlQ Nozzl e Size/No . 

### 0.2.9JL . . . Slo p Tim e

### Cfl/O

SO</51 XA D Thermocoupl e ID : 

### ^Cj / SJ St i ICAGL L Fina l Pure ' Rat e * "

_ M,ImpOulletTCID : CZ- ? Filia l P H JtAMl' I I W I M C l OCI v

TIM E V rI OCIIV

HEA D l»el l IP , i n 1V

1 ORIHC P MI.IH ? VO L DelliH.iiin c UA S M rlil t 

### TEMPERATUR E READINGS
. ° FI PUM P

v ' COMMENTS , ; JtAMl' I I W I M C l OCI v

TIM E V rI OCIIV

HEA D l»el l IP , i n 1V

1 ORIHC P MI.IH ? VO L DelliH.iiin c U>LUM F ft ' S1A < K PROi m 

### OMtORGANI C MODUL E llllllll l 

### mmmmmm VACUO M v ' COMMENTS , ; JtAMl' I I W I M C l OCI v

TIM E V rI OCIIV

HEA D l»el l IP , i n 1V

1 ORIHC P MI.IH ? VO L DelliH.iiin c U>LUM F ft ' S1A < K PROi m 

### OMtORGANI C MODUL E IM P

### j I N OU T | m . 

### a * v ' COMMENTS , ; 

### A1 C J 

### o.Wii 7.S 

### yoj. ,2 < W 

### C n 

### <7 SL. ./<. > . . 

### r>.7V /, (a 3?X. 7 JVC, K Y7 7 V 70 . r . o 

### J. zs-o.sj- 3iT2- 3 y y \ 

### Yy 76, 7JZ H ;?f?? - 7 

### <yoY Yl 75 ? 7R o ~ y o t T ? y . 

### Y<?6> 

### £Z> 7 9 7Y L> A- ? <Yo</ J2Y? y<? 7& v..« r 

### R 1 CoO 7.7 Yo?. Y / j2 

### AYY CoY ? * A 

### •70 0 . s o 

### J.7 VA/ ,/ 

### ;3Y8 Y<%

SO 7. 7 yj?/ 

### y <7dsST ,ar, ? 

### <]o /. 7 ^s* . < / 

### Yo? fr.r 0 ^ j ? 

### /oo / ,c i V £.r . Y 

### Yd>9 2 S-7 

### ayc S3 2? ,<f > . . //£ > 

### /.a m.- s YtiST as? J2S* •Ma p 

### /JLO 1 - — \

• UAIUJ1 ~INTERNATIONAL



### Uni t2 PCDD/PCD FFIEL D DAT A

S:\STACKVJOB\2003VonyxRP\repoilMlysheels.do c Novembe r200 3Metho d 0023 A Samplin gParameter s Uni t2 

### Ru n No
. R 1 R 2 R 3 Dat e 18-Sep-0 3 19-Sep-0 3 19-Sep-0 3 Star tTim e Unit s 144 5 83 0 125 0 Sto p Tim e 184 9 114 2 160 1 AVG S Nozzl e Diamete r inche s 0.43 0 0.43 0 0.43 0 0.43 0 Barometri cPressur e in
. H g 29.5 5 29.6 0 29.6 0 29.5 8 Ne tSamplin g Tim e min
. 180. 0 180. 0 180. 0 180. 0 Volum e Metere d dc f 121.06 2 121.47 9 116.10 8 119.55 0 Avg
. DG M Temp
. ° F 108. 7 60. 3 69. 5 79. 5 Av g Delt aH i n H 2 

### 0 1.5 9 1.7 4 1.5 6 1.6 3 Av g Delt aH in
. H g 0.117 0 0.128 1 0.114 6 0.119 9 D G M Calibratio n Facto r — 

### 0.981 4 0.981 4 0.981 4 0.981 4 G a s Sampl e Volum e dsc f 109.37 3 120.21 9 112.85 4 114.14 9 Tota l Wate rCollecte d m L 1944. 1 1910. 7 1875. 2 1910. 0 Volum e o fWate rVapo r sc f 91.66 4 90.09 0 88.41 6 90.05 7 Moistur e (measured ) % v/ v 45. 6 42. 8 43. 9 44. 1 Moistur e ( @ saturation ) % v/ v 101. 1 101. 1 101. 0 101. 1 Dr yMol e Fraction , 100-% M 

### - - 0.544 0 0.571 6 0.560 7 0.558 8 C 0 2

### a tStac k %dr y 6.7 0 6.7 0 6.7 0 6.7 0 0 2

### a tStac k % dr y 12.1 0 12.1 0 11.5 0 11.9 0 C O + N 2 

### %dr y 81.2 0 81.2 0 81.8 0 81.4 0 Dr yMolecula rWeigh t Ib/lb-mol e 29.5 6 29.5 6 29.5 3 29.5 5 We tMolecula rWeigh t Ib/lb-mol e 24.2 9 24.6 1 24.4 7 24.4 5 Exces s Ai ra tStac k 

### % 129. 6 129. 6 113. 9 124. 4 Stac k Diamete r inche s 48. 0 48. 0 48. 0 48. 0 Stac k Are a sq . in
. 1809. 6 1809. 6 1809. 6 1809. 6 Stati cPressur e i n H 2 

### 0 0.4 5 0.1 1 0.2 0 0.2 5 Stac k Pressur e in
. H g 29.5 8 29.6 1 29.6 1 29.6 0 Avg
. Stac k

Temp
. ° F 381. 8 367. 1 372. 1 373. 7 Avg
. Sqroo to fDelt aP ~ 

### 0.385 7 0.416 8 0.394 2 0.398 9 S D E Averag e — 

### 11.19 2 11.98 8 11.37 2 11.51 8 Pito tCoefficien t ~ 

### 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocit y afp m 1,79 9 1,91 4 1,82 1 1,84 5 Stac k Flowrat e we tacf m 22,61 0 24,05 1 22,87 8 23,18 0 Stac k Flowrat e we tscf m 14,02 2 15,19 4 14,36 9 14,52 8 Stac k Flowrat e dscf m 7,62 8 8,68 5 8,05 7 8,12 4 Isokinetic s 

### % 9 9 9 6 9 7 9 7 Mete rBo xNo
. ~ 

### 8010 2 8010 2 8010 2 ~ 

### Delt aH @ in
. H g 2.059 0 2.059 0 2.059 0 — 

### Fiel d Q AYq c — 

### 1.01 3 1.00 9 1.00 8 1.01 0 [Deviation ] Pre- Y 

### % 3.2 % 2.8 % 2.7 % 2.9 % S:\STACKUOB\2003\onyxRP\xldata\Sep t03\[M2 3 U2.xls]TEQ S

### Uni t2

P T RU N1 AVG S - - PCDDs/PCDF s RUN2AVGS - - PCDDs/PCDFs RUN3 AVG S - PCDDs/PCDF s P T D P SQR T D P DG M

I N DG M

O U T D H STAC K TEM P D P SQR T D P DG M

I N DG M

OU T D H STAC K TEM P D P SQR T D P DG M

I N D G M

O U T D H STAC K TEM P a1 0.1 7 0.412 3 9 5 9 5 1.8 0 38 2 0.19 0.435 9 5 9 5 8 1.9 0 36 7 0.1 4 0.374 2 6 3 6 2 1.4 0 36 7 a Z 0.1 8 0.424 3 10 3 9 7 1.9 0 38 2 0.1 8 0.424 3 6 3 6 0 1.8 0 37 0 0.1 4 0.374 2 6 7 6 3 1.4 0 37 3 a 3 0.1 5 0.387 3 10 7 10 3 1.6 0 38 2 0.1 9 0.435 9 6 0 5 8 1.9 0 36 9 0.1 6 0.400 0 6 7 6 5 1.6 0 37 5 a 4 0.1 3 0.360 6 11 1 10 7 1.4 0 38 3 0.1 9 0.435 9 6 1 5 8 1.9 0 36 8 0.1 8 0.424 3 6 8 6 5 1.8 0 37 3 a5 0.1 6 0.400 0 11 2 10 9 1.7 0 38 3 0.2 0 0.447 2 6 3 5 9 2.0 0 36 7 0.1 6 0.400 0 6 9 6 6 1.6 0 37 4 a 6 0.1 5 0.387 3 11 4 10 9 1.6 0 38 3 0.1 8 0.424 3 6 3 5 9 1.8 0 36 7 0.1 7 0.412 3 6 9 6 6 1.7 0 37 3 a 7 0.1 5 0.387 3 11 4 11 1 1.6 0 38 2 0.1 4 0.374 2 6 0 5 9 1.40 36 7 0.1 6 0.400 0 6 7 6 7 1.6 0 37 2 a6 0.1 3 0.360 6 11 5 11 2 1.4 0 38 3 0.1 6 0.400 0 6 1 5 9 1.6 0 36 7 0.1 7 0.412 3 7 1 6 7 1.7 0 37 2 a9 0.1 4 0.374 2 11 7 11 2 1.5 0 38 3 0.1 7 0.412 3 6 1 5 9 1.7 0 36 6 0.1 6 0.400 0 7 3 6 9 1.6 0 37 2 a1 0 0.1 5 0.387 3 11 8 11 0 1.6 0 37 8 0.1 7 0.412 3 6 2 5 9 1.7 0 36 6 0.1 6 0.400 0 7 7 7 2 1.6 0 37 2 a1 1 0.1 5 0.387 3 11 3 10 9 1.6 0 38 1 0.1 6 0.400 0 6 3 6 0 1.6 0 36 6 0.1 2 0.346 4 8 0 7 5 1.2 0 37 1 a1 2 0.1 3 0.360 6 10 9 10 7 1.4 0 38 0 0.1 6 0.400 0 6 2 6 0 1.6 0 36 5 0.1 5 0.387 3 8 1 7 8 1.5 0 37 1 AV G 0.15 0.385 7 108. 7 1.5

9 38

2 0.17 0.416

8 60. 3 1.7

4 36

7 0.16 0.394

2 69.5 1.5 6 37

2E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T



### iJ Samplin g Trai n Ru n Numbe r

### i

>.2 -

### C. t - /H^i,' Clk 

### " ! 

### rb^yx Facilit yLocallo n ^Sc t

### tf-ff P / 

### 'J-£~ Sourc e Dal e Operato r SlackDia . - iu . StartTime Sto p Tim e Ilarometrl c treasur e ^ 2 7 < C

j 0 Stati c Pressure (+/-

) ••/• ' ,/f Probe/Pilo tNumbe r.yCf,fS^-/~ Pito l Coefficien tQ . g"-/ Filte rBo *No . - ft* Mete rB OJ

INo . LEA KCHECK S i n "H g INITIA L VAC . 

### IS" In . CF M 

### t<JjS MIDVAC . <~ " III. , CF M — - "in . CF M 

### '0 0 7 FINA L VAC . /

V INIT . PITO T FINA L PITOT 3 9 ^ /0'iCO / il . SA M P I I POIN I CLOC K VELOCIT Y UEA D Ddi-iP , In. « ORIFIC E

M lJF KVO L Drilt Hi nIY C Orinc e Coefliclen t(Y ) (VQff/t- / Deli a I I @ ,.3.,OS9Q Nozzl e Size/No . , i/J Q XA D Thermocoupl e ID : Im p Outle tTC . U) : FILTE R DAT A NUMBER

S 

### mum IMI'INO I R \ OL" > INIT, 

### o 7 C o _S2
_ FlrtA L 

### 7 W ^ 7 2

SILIC A GE L
tlASMUM t YDI.UM 1 

### W
. TEMPERATUR E READINGS
. ° F /t
. 7
MAC K IKOIl l OVE N OIIUAM C MODUL E IM P iin jl^METEft i||i ; '"IN" " ) " '

wr ' Orsa t CO Z p i

)>.> •

Fina lP H POM P VACUU M '"H D lHI'.linM'.M'Wl CUMMFNT S 

### •U- Z Z 

### 2 2 1 4 ^ - 

### 4 a 

### -L2L UL 22L -L

.•••> XJ-iC 

### LL. •a. ^ 4 - 

### i t ^.i 7 3 (3.0

7 5 0 

### 277
. & 4 - 

### S 2 L 

### •Hop 

# UK 7 l-" L Ml. 5% M l ILL. d L . 

### iM. &1L2. J L Z
. 

### MSL 6 / 1 2 . 3 Vy . ^ 4 ^ - i£JL 

### (JL I L 

### LA. i l l &.V6' 

### £*± Slop Z L



### 2JL lk. L L ikii . 

### 1^0E F AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n ,,CQ3 SA Ru n Numbe r Clien t Facilit yLocatio n Sourc e Dat e Operato r//2« I Barometri c Pressure Stati c Pressure (+/-

) -j-t? , 3, 0 

### o,ayy. Probe/Pito tNu m be r^ C-. Pilo tCoefficien ttf, 'cf< / Filte rBoxNo . A// ? - fr* Mete rBoxNo . ft,V£x,2. LEA KCHECK S I n "H g INITIA L VAC . j

In .

111. , III . M P VAC . _ J FINA L VAC . CFM
_ C F M ,0 0 /

INIT . PITO T FINA L PIT O X>^ ~ StackDIa. - Slar tTim e in . i!i

,:i ' 0 //V-\L L Orific e Coefficien t(Y ) ^ B . 757 ' V Delt aI I @^.<^5 "fei > Nozil e Slie/No . 0:^/^0 FILTE RDAT A J NOMBER S STAKE S lMPINCUUO I " 3 jam . 

### /CO 

### o FINA L RINS M Orsa t toi l

/ Im p Outle tT C ID : C.JC - Z^T [ 1 Fina l P H ^

, , .l^ ^ SAMPL E POIN I CLOC K

TIM E VELOCIT Y

HEA D llrUll ' 'IM' C ORIFIC E

M " ru tM M ')el l il l l u T C <}ASM I IH t 

### TEMPERATUR E RE A DlNGS.^Ff e 7 VACUU M ln-Ht ; COMMENT S SAMPL E POIN I CLOC K

TIM E VELOCIT Y

HEA D llrUll ' 'IM' C ORIFIC E

M " ru tM M ')el l il l l u T C un.i'M r / S I \ (IC PttQB E OVE N OHiMNI C MOflliL F ,igA $.P.E5CE R VACUU M

ln-Ht ; COMMENT S SAMPL E POIN I CLOC K

TIM E VELOCIT Y

HEA D llrUll ' 'IM' C ORIFIC E

M " ru tM M ')el l il l l u T C un.i'M r / S I \ (IC PttQB E OVE N OHiMNI C MOflliL F IM P I N 0 0

### r VACUU M ln-Ht ; COMMENT S 

### ft 1 ,/< / 

### X</ 1 li,n / . r , / V 'IP..! , < ? 

### JSV r r 

# vi /.,'" > 

### 11,0

. / v 0 iA S 

### •pil any 

## '/,< r h$ </- 0 1
. 7 . c r 

### (J W. o 

## i t o

## 0 V/,x
. 0 &?> (

### i .r« v -?. r 

### ! ; -

/ ' I ; 

### 4'< i 1 ' f i ,*.rt > 

### )3.. T • ? o 

### 4i/.9 i 1 . f\f r 

## 0 ."ll iiL '0,3
. . . ... . 

### fa ^ 

## > ;A, r 

### j. ; V n i 

## 7 1- 7 Y / 

## 3 .1 0 7 3 vii i l o v 

### 4.S " /
. L ? ' / 1 , /
. S '•i 

## }r9 k j ..r o 

### 7 c? - 

## '/, 0 ' ; T ) . a . 

### 47/
. L S o 

### 7

## 5 " li-0 

## 7, > 1 — 

### W o , 

## V MX r W r 

### Si'OOE P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n _ Ri m Numbe r Clien t -U?.?. A Barometri c Presmr e 

## <p %sS Stati c Pressure (+/-

) •/ • Facilit yLocatio n Squc,ef , T C Sourc e Dal e Operato r SUc k Dia . 

# j^Ag s l 

# ° p T 

# " n 

# ' j^trO/Ttn/mifr) Probe/Pilo tNumbe r j/ Cf,C->'P Plto tCoemden tQ.fr't ' Filte rBoxNo . 

### A/R-£rh<3' Mete rBo xNo . 

### $f@t]i0^f4&CA.mT. PITO T Orific e Coefficien t(Y ) Q.^sy ^ Delt a H @

### J.CXTf^ NozileSlie/No . Q,y.?< S LEA KCHECK S I n "H g INITIA L VAC . /,f~~In . MI D VAC . 111 . FINA L VAC . /2 * S In . CFM
_ C F M FINA L PIT O

XA D Thermocoupl e ID i 

### XjLD

JlZ" Im p Outle tT C ID : FILTE R DAT A IMPlNGKI l VOL'S . INIT . 

### /OO /ao M N A X , 

# 222 1 

# 32JL 232*

SlUCACE L Fina l Purg e Rate
_ Fina l P H RINSE * Orja t; j 

### mm mm

a i

1Uni t2

MULT I METAL S FIEL D DAT A

S:\SfACKUOB\2003\onyxRP\repoilMlysheels.cloc Novembe r200 3

### Metho d 2 9 Metal s Samplin g Parameter s UNI T2 

### Ru n No
. Ru n 1 Ru n 2 Ru n 3 Date 18-Sep-0 3 19-Sep-0 3 19-Sep-0 3 Star tTim e Unit s 144 5 83 0 125 0 Sto p Tim e 181 0 111 2 153 1 AVG S Nozzl e Diamete r inche s 0.43 1 0.43 1 0.43 1 0.43 1 Barometri cPressur e in
. H g 29.5 5 29.6 0 29.6 0 29.5 8 NetSamplin g Tim e min
. 120. 0 120. 0 120. 0 120. 0 Volum e Metere d dc f 85.39 1 84.76 3 82.28 8 84.14 7 Avg
. DG M Temp
. ° F 98. 3 60. 0 67. 2 75. 2 Av g Delt aH i n H 2 

### 0 1.7 4 1.78 1.67 1.73 Av g Delt aH in
. H g 0.128 1 0.131 1 0.122 5 0.127 2 DG M Calibratio n Facto r 

# - 0.975 3 0.975 3 0.975 3 0.975 3 Ga s Sampl e Volum e dsc f 78.12 0 83.40 5 79.85 2 80.45 9 Tota l Wate rCollecte d m L 1326. 0 1304. 4 1298. 0 1309. 5 Volum e o fWate rVapo r sc f 62.52 1 61.50 2 61.20 1 61.74 1 Moisture (measured ) % v/ v 44. 5 42. 4 43. 4 43. 4 Moisture ( @ saturation ) %v/ v 101. 1 101. 1 101. 0 101. 1 Dr yMol e Fraction , 100-%r i 0.555 5 0.575 6 0.566 1 0.565 7 C 0 2

### atStac k %dty 6.7 0 6.7 0 6.7 0 6.7 0 0 2

### a tStac k %-dr y 12.1 0 12.1 0 11.5 0 11.9 0 C O + N 2 

### %dr y 81.2 0 81.2 0 81.8 0 81.4 0 Dr yMolecula rWeigh t Ib/lb-mol e 29.5 6 29.5 6 29.5 3 29.5 5 WetMolecula rWeigh t Ib/lb-mol e 24.4 2 24.6 5 24.5 3 24.5 3 Exces s Ai ra

tStac k % 

### 129. 6 129. 6 113. 9 124. 4 Stac k Diameter
. inche s 39. 0 39. 0 39. 0 39. 0 Stac k Are a sq . in
. 1194. 6 1194. 6 1194. 6 1194. 6 Stati cPressur e i n H 2 

### 0 0.4 5 0.1 1 0.2 0 0.2 5 Stac k Pressur e in
. H g 29.5 8 29.6 1 29.6 1 29.6 0 Avg
. Stac k

Temp
. 381. 7
. ; 367. 8 372. 3 373. 9 Avg
. Sqroo to

fDelt aP


# - 0.404 7 0.422 2 0.408 0 0.411 6 SD E Averag e 

# - 11.74 2 12.14 7 11.76 9 11.88 6 PitotCoefficien t ~ 

### 0.8 4 0.8 4 0.8 4 0.8 4 Stac k Ga s Velocity afp m 1,883 1,938 1,882 1,90 1 Stac k Flowrat e we tacf m 15,61 7 16,07 4 15,61 1 15,76 7 Stac k Flowrat e we tscf m 9,68 7 10,14 6 9,80 2 9,87 8 Stac k Flowrat e dscf m 5,38 1 5,84 0 5,54 9 5,59 0 Isokinetic s % 

### 9 9 9 7 9 8 9 8 Mete rBo xNo
. 

# - 8060 4 8060 4 8060 4 — 

### DeltaH @ i n H 2 

### 0 2.004 7 2.004 7 2.004 7 Fiel d QAYq c . 

### 1.005 1 0.988 0 0.991 1 0.994 7 [Deviation ] Pre- Y % 

### 3.06 % 1.30 % 1.62 % 1.99 % S:\STACK\JOB\2003\onyxRPWciata\Sep ! 03\[Metal s Blan k Correctio n Uni t2.xls]RU N 1

### Uni t2 RU N1 AVG S - - METAL S RU N2 AVG S - METAL S RU N3 AVG S - - METAL S P T Deli a P SQR T Deli a P DG M

I N DG M

OU T Delt a H STAC K TEM P Deli a P SQR T Delt a P DG M

I N DG M

OU T Delta H STAC K TEM P Delt a P SQR T Delt a P DG M

I N DG M

OU T Delt a H STAC K TEM P a 1 0.1 9 0.435 9 9 6 9 6 2.0 0 37 6 0.1 9 0.435 9 5 9 5 9 1.9 0 37 0 0.1 5 0.387 3 6 3 6 3 1.5 0 37 0 a 2 0.1 5 0.387 3 9 7 9 5 1.6 0 38 1 0.1 9 0.435 9 6 3 5 9 1.9 0 37 0 0.1 7 0.412 3 6 6 6 4 1.7 0 37 3 a 3 0.1 7 0.412 3 9 4 9 4 1.8 0 38 0 0.1 8 0.424 3 6 1 5 9 1.8 0 36 9 0.1 7 0.412 3 6 6 6 4 1.7 0 37 4 a 4 0.1 8 0.424 3 9 7 9 6 1.9 0 38 3 0.1 7 0.412 3 6 0 5 8 1.7 0 36 8 0.1 7 0.412 3 6 6 6 4 1.7 0 37 6 a 5 0.1 5 0.387 3 9 9 9 7 1.6 0 38 3 0.1 7 0.412 3 6 0 5 8 1.7 0 36 8 0.1 8 0.424 3 6 7 6 5 1.8 0 37 5 a 6 0.1 4 0.374 2 10 1 9 8 1.5 0 38 3 0.1 8 0.424 3 6 1 5 9 1.8 0 36 7 0.1 8 0.424 3 6 8 6 5 1.8 0 37 5 a7 0.1 6 0.400 0 10 2 10 2 1.7 0 38 1 0.1 7 0.412 3 6 1 6 0 1.7 0 36 7 0.1 7 0.412 3 6 6 6 6 1.7 0 37 0 a 8 0.1 7 0.412 3 10 1 10 1 1.8 0 38 1 0.1 8 0.424 3 6 1 5 9 1.8 0 36 7 0.1 7 0.412 3 6 9 6 7 1.7 0 37 1 a 9 0.1 9 0.435 9 10 0 9 9 2.0 0 38 4 0.1 7 0.412 3 6 1 5 9 1.7 0 36 7 0.1 8 0.424 3 7 0 6 7 1.8 0 37 2 a1 0 0.1 6 0.400 0 10 2 10 0 1.7 0 38 6 0.1 8 0.424 3 6 2 5 9 1.8 0 36 7 0.1 7 0.412 3 7 2 6 9 1.7 0 37 3 a1 1 0.1 5 0.387 3 10 0 9 9 1.6 0 38 3 0.1 8 0.424 3 6 2 5 9 1.8 0 36 7 0.1 5 0.387 3 7 3 7 0 1.5 0 37 1 a1 2 0.1 6 0.400 0 9 7 9 7 1.7 0 37 9 0.1 8 0.424 3 6 2 6 0 1.8 0 36 6 0.1 4 0.374 2 7 2 7 0 1.4 0 36 8 b1 0.000 0 0.000 0 0.000 0 b 2 0.000 0 0.000 0 0.000 0 b 3 0.000 0 0.000 0 0.000 0 b4 0.000 0 0.000 0 0.000 0 b 5 0.000 0 0.000 0 0.000 0 b 6 0.000 0 0.000 0 0.000 0 b 7 0.000 0 0.000 0 0.000 0 b 8 0.000 0 0.000 0 0.000 0 b 9 0.000 0 0.000 0 0.000 0 b1 0 0.000 0 0.000 0 0.000 0 b l 1 0.000 0 0.000 0 0.000 0

. b1 2 0.000 0 0.000 0 0.000 0

• 

### AV G 0.1 6 0.4047 98.3 1.7 4 38 2 0.1 8 0.422

2 60.0 1.7 8 368 0.1 7 0.4080 67.2 1.6 7 372E P AISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n Ru n Numbe r Clien t Facilit yLocatio n Sourc e Dat e Operato r Stac k Dia.-In . StartTim e Slo p Tim e SialicPressur e(+/- ) + Barometri c Pressure Probe/Flto tNumbe r Pilo tCoemden t Filte rBoxNo . ~ Mete rBoxNo . LEA KCHECK S I n "H g INITIA L VAC . /

5 MI D VAC . _ FINA L VAC . C F M

INIT . PITO T Orinc e Coemden t(Y ) Q.9yj\ J Delt a H ( Nozzl e Size/No . 

### fe CFM0<30 |
FINA L VlTOTtyC FILTE RDAT A NUMBE R TAR E

• — — <Vu.i)vl"7* - lMl'JNOKttVOX'S. ;



### /OO FlNA

t

/ OA

SILIC A GE L Fina l Purg eR«te
_ Fina l P H' Orsa t 

### mm 

### 67 

# £>7 1T&
TEMPERATUR E READINGS
. " F

j ORGANI C OVK N I MOIHIL F 

# 22 £ IM P VACUO M COMMENT S



### S t yJ5K

Ah7F 

# S I

3 ZE P A-ISOKINETI C SAMPLIN G - FIEL D DAT ASHEE T Samplin g Trai n Ru n Numbe r Clltn l Facilit yLocatio n Sourc e Dal e Operato r Slac k Dia . StartTim e Sto p Tim e llaroiuetrl c Pressure Stati c Pressure {+/-

) -f" Q ,-\ I Probe/Pito tNumbe r

### yC\

fZ-A"' 2. Plto tCoelTlcleu tQ. % Filte rBoxNo . Mete rBoxNo . LEA KCHECK S I n "H g INITIA L VAC . / 4 In . MI D YAC . In. . III . lMPlNtUKVOI'S .

FINA L VAC . ? 

### C F MO.cVaj ] CFM
_ CFM " 

### 1)

•iu .

SAMPL E POlN I 

### rr-- .

CLOC K TIM K VELOCIT Y

II I 

### Wl 0*1 1 il'.ii l w

t OIMF1C E 

### MIlfKNO I ttcllnfl I n ire Oriric e Coetnclen t(Y ) £ > 9 7^ 3

Delt a II ® Nozzl e Size/No . Q ..L / 3 I XA D Thermocoupl e ID ; Im p Outle tT C ID : 8'CVx»<V / 1N1T.PIT0T
_ •FINA L PIT0«n- O FTLTERDAT A

liASM T IER v o n Mr . ft ' SNUMBEIV : INIT.
yc>c> FINAL, . 

# WL 7

- SILICA PE L 

### TEMPERATUR E READINGS
. ° F ? I * I ; i^rftiiSif! l!!'W; i .RlNSgjj


### ,/if O Orsa t



### LP

IP-. I Fina l Purg e Rale
_ Fina l P H

STAC K PROB E OVE N OIU3V .M C MODUL E IM P CA S METE R I N Otl T VACUU M t n H g COMMENT ^ 

### B 1 

### a 7LJ 7 T5 

### ZSLL 

# EK t 5 ~



# I 10 SUT 2 i l 

## I T
± Z 2 ISO 

## u n f t 

### HO u i T \

## . ' i 

### 5 2 1 S o £ 2
_ £ 2 0 •f T O T 

### J o
. 

### 5. m . ZkHL " E E 

## ML ^ 7 0 

# 'tea. ISO 2 ^ jte — o

•n S t O H ' 3 k
_

## EP A ISOKINETI C SAMPLIN G- FIEL D DAT A SHEE T Samplin g Trai n Ru n Numbe r Clien t Facilit yLocatio n Sourc e Date Optrnlo r Slac kDia . - In. StartTime Sto p Tim e (7J--CJ ^A*: ?

" 3 ? 

### XJ 1 

### YlSO Unromefrl tPressure •21 , UO Stati c Pressure (+/-

) -j- d '

2. Q Probe/Pito tNumbe r

### ^j/l^S"' <Z L PltotCoerncieu tO •g Fille rBoxNo . ^ Mete rBoxNo . /fo^/i ? <r»< 7 Orinc e Coefficien t(Y ) 7^7" ? Delt a H @

### e?.Q*V? Nonlf . Slie/No . LEA KCHECK S I n "H g INITIA L VAC . / 5 In . CBbld'OC'l MI D VAC . 1 lu . CF M FINA LVAC . ~ 7 In . cniQtQO)
INIT . PITO T FINA L PITO T

FILTE R DAT A
\Sb\ XA D Thermocoupl e ID ; 

### ^e/ySi Im p Outle tT C ID : 

### C^T-^l •NUMBy u I TAKE ; lMlljiGlRVO l S

•INIT , I. FINAL. . /G>0 

### TTT TTo~ J.

SIL1CAGE L RlNSE .



### 4- Orsa t


# G-S i // . S I SOi i



### IL Fina l Purg e Rat e Fina l P H r SAMPL E POIN T r*r r J1M K VELOCIT Y HEA D Old ] 

### 11 1 1f t ORIFIC E MUHUO l Drlli'l , I n >

T C KiWi

M n i I t ,(JL!'M r w KTAC K TEMPERATUR E READINGS . ° F PROS E OVE N OK I WU MODUL E IM P I N POM P VACUU M ..ill * COMMENT S 

### O y 

### ~T7o 1p} 7 . 0/?.? - J7U 

## W T MA. <7T L a . 

### Q7YT -c r I T 

### ML 

## 30. 

# QTT 7 4 

### Hi. 

# 5H X S 3
. 

### 9 III
. I L 

### Ml LL. r; 0 L MS 

### ILL M l
u o 

### 2
. 10 s2

_ 

## lob"?'

" TT T ZL X<5 ft 5L, 0 - > y 

## s : ZLLL 10 

## I f

j t •1 5 

## 4 1 TTT T )0 & 1* 0 

# -14

- LL



## z n

### APPENDI XB WAST E FEE D AN D OPERATIN G CONDITION S

C:\Documents an

d Seffingstatoo!Me\MyDocuments\Onyx\090 3 teslingranpc 090

3 dauAAppendixCoveis.do c January2004

### Ony xEnvironmenta l Service s - Sauget , I L Uni t2 an d Uni t4 Proces s Operatin g Dat a l l Unit4 

### •

/ \l . „ Unit2 Sept . 2003 -" ' T p ^ 

# >° ^ Sept . 2003 1 Units R1C 1 R2C 1 R3C 1 Averag e R1C 2 R2C 2 R3C 2 Averag e R 1 R2 R 3 Averag e Pumpabl e Waste Ibs/h r 4,25 9 4,270 4,256 4,262 4,245 4,05 1 4,269 4,188 3,865 3,823 3,838 3,842 Tota l Waste Ibs/h r 14,675 15,553 14,17 9 14,802 14,46 4 14,90

2 14,68

7 14,68

4 4,662 4,787 4,860 4,770 Stackflo w 

### XI

aV m 43. 4 43. 9 44. 3 43. 9 43. 2 43. 4 43. 6 43. 4 15.4 15. 6 15. 6 15. 5 PC C Tem p De g F 1,51 7 1,49 7 1,50

6 1,50

7 1,51 6 1,51 5 1,49 7 1.50

9 1,66 8 1,65

9 1,64

9 1,65

9 SC C Tem p - De g F 1,887 - 1,88 3 1,88

9 1,88

6 1,891 1,89 2 1,88

5 1,88

9 1,851 1,84 9 1,87

2 1,85

7 42 5 B.H . tnletTem p De g F 434 43 9 432 435 436 43 9 436 437 42 5 42 5 42 5 42 5 LV M Ibs/h r 48 49 4 8 4

8 4 4 4

7 49 4 7 4 4 41 48 4 4 67" " SV M Ibs/h r 11 1 11 1 12 8 11 7 11 8 12 8 11 6 12JU- . 6 1 70 7 1 67" "

— — Mercur y Ibs/h r 0.056 0.054 0.054 f 0.055 , ) 0.173 0.193 0.19 2 { 0.186 ^ 0.00035 0.00026 0.00043(' 0.00035 Chlorin e Ibs/h r 27 2 28 1 269 27 4 272 283 287 28 1 255 275 282 271 As h Ibs/h r 8,21 9 6,768 7,69 1 7,559 8,208 7,97 4 9,324 8,50 2 1,301 1,76 3 1,76

6 1,61 0

## OnyxEnvironmenta l Service s - Sauget , I L Uni t2 Fee d Data Uni t# 2 Ru n # 1 Date : 09/18/0 3 Tes tTime : 14:4 5 t o 18:4 9 P P M P P M P P M P P M P P M P P M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1337 0 0.5 4 14. 7 0.22 8 9.9 6 0.8 6 33. 6 0.02 5 3.1 3 82 2 P C C Lo wBt u 50 0 0. 5 1 0 0.031 6 0. 4 0.26 8 0.76 6 0.0 1 0.31 2 180 6 (Chromiu m Spike ) 50 0 0. 5 75. 2 0.0 8 2 0 1 35 8 0. 5 19900 0 22 2 P C C S p Fd r 50 0 0. 5 56. 5 0.004 2 0. 4 0.03 8 0.2 5 0.0 1 0.42 5 46 8 (Chlorin e Spike ) 50 0 83. 5 0.0 5 0.00 9 8.1 1 0.1 7 2.1 2 0.0 8 0.8 5 17 9 P C C Soli d Charge s 50 0 0. 5 96. 7 0.16 2 38. 3 1.3 6 28. 3 0.0 9 11. 4 51 9 P C C Labpac k

Charge s 17 2 (Lea d Spike ) 50 0 0. 5 65. 6 0.00 9 63900 0 13. 3 4.3 1 0.1 7 9 6 (Chlorin e Spike ) 50 0 89. 8 2. 7 0.0 1 7.6 9 0.3 8 4.8 1 0.1 9 1.9 2 9 4 S C C Hig h Bt u 1337 0 0.5 4 0. 5 0.00 4 1 0.0 5 0.62 5 0.02 5 0.2 5 23 4
Total s

1 o f2

## OnyxEnvironmenta l Service s - Sauget , I L Uni t2 Fee d Data Uni t# 2 Run# 1 Date : 09/18/0 3 Tes tTime : 14:4 5 t o 18:4 9 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 10.9 9 4.4 4 120.8 3 0.00018 7 0.0 1 0.0 0 0.0 3 0.0 0 0.0 0 P C C Lo wBt u 0.9 0 9.0 3 180.6 0 0.00005 7 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 1 .166.9 4 0.00001 8 0.0 0 0.0 0 0.0 8 0.0 0 44.1 8 P C C S p Fd r 0.2 3 2.3 4 264.4 2 0.00000 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chlorin e Spike ) 0.0 9 149.4 7 0.0 9 0.00000 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.2 6 2.6 0 501.8 7 0.00008 4 0.0 2 0.0 0 0.0 1 0.0 0 0.0 1 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 5 0.4 8 62.9 8 0.00000 1 61.3 4 0.0 0 0.0 0 0.0 0 0.0 0 (Chlorin e Spike ) 0.0 5 84.4 1 2.5 4 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 3.1 3 1.2 6 1.1 7 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 15.8 1 255.1 3 1301.4 4 0.00035 3 61.3 8 0.0 0 0.1 2 0.0 0 44.1 9

2 o f2

## OnyxEnvironmenta l Service s - SaugetI L Uni t2 Fee d Data Uni t#2 Ru n #2 Date : 09/19/0 3 Tes tTime : 08:3 0 t o 11:4 2 P P M P P M P P M P P M P P M P P M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1087 0 1. 2 9. 8 0.071 6 1.7 5 0.46 3 5.6 5 0.02 5 0.73 2 87 0 P C C Lo wBt u 50 0 0. 5 2 3 0.055 6 0. 4 0.75 5 7.1 8 0.0 1 0.10 2 182 4 (Chromiu m Spike ) 50 0 0. 5 7 5 0.01 6 1 5 0.2 9 26 2 0.1 6 18200 0 22 3 P C C S p Fd r 50 0 0. 5 7 4 0.001 6 0. 4 0.0 5 0.2 5 0.0 1 0.52 7 42 6 (Chlorin e Spike ) 50 0 83. 5 0.0 5 0.0 1 3.3 9 0.1 7 2.1 2 0.0 8 0.8 5 18 1 P C C Soli d Charge s 50 0 0. 5 95. 7 0.13 7 43. 6 1. 1 22. 4 0. 1 8.9 9 62 9 P C C Labpac k

Charge s (Lea d Spike ) 50 0 0. 5 65. 8 0.0 1 63900 0 7.4 4 5 0. 2 2 11 0 (Chlorin e Spike ) 50 0 89. 8 88. 5 0.0 1 8. 7 0.4 3 5.4 3 0.2 2 2.1 7 10 7 22 2 S C C Hig h Bt u 1337 0 0.5 4 3. 1 0.0 1 3.5 7 0.1 8 2.2 3 0.0 9 0.8 9
Total s

1 o f2

## OnyxEnvironmenta l Service s - Sauge tI L Uni t2 Fee d Data Uni t#2 Ru n #2 Date : 09/19/0 3 Tes tTime : 08:3 0 t o 11:4 2 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 9.4 6 10.4 4 85.2 6 0.00006 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Lo wBt u 0.9 1 9.1 2 419.5 2 0.00010 1 0.0 0 0.0 0 0.0 1 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 2 167.2 5 0.00000 4 0.0 0 0.0 0 0.0 6 0.0 0 40.5 9 P C C S p Fd r 0.2 1 2.1 3 315.2 4 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chlorin e Spike ) 0.0 9 151.1 4 0.0 9 0.00000 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.3 1 3.1 5 601.9 5 0.00008 6 0.0 3 0.0 0 0.0 1 0.0 0 0.0 1 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 6 0.5 5 72.3 8 0.00000 1 70.2 9 0.0 0 0.0 0 0.0 0 0.0 0 (Chlorin e Spike ) 0.0 5 96.0 9 94.7 0 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 2.9 7 1.2 0 6.8 8 0.00000 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 14.1 8 274.9 2 1763.2 7 0.00026 0 70.3 3 0.0 0 0.0 9 0.0 0 40.5 9

2 o f2

## Ony xEnvironmenta l Service s - Sauget , I L

Unit2 Fee d Dat

a Uni t#2 Ru n #3 Date : 09/19/0 3 Tes tTime : 12:5 0 t o 16:0 1 PP M PP M PP M PP M PP M PP M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr ) PC C Hig h Bt u 1087 0 1. 2 7. 4 0.0 5 3.7 7 0.4 4 2.3 6 0.09 0.9 4 99 0 PC C Lo wBt u 50 0 0. 5 2 0 0.10 1 3. 7 0. 8 4. 2 0.0 9 0.9 3 172 2 (Chromiu m Spike ) 50 0 0. 5 75 0.01 6 1 5 0. 3 29 9 0.1 7 21300 0 22 4 PC C S p Fd r 50 0 0. 5 78. 4 0.001 6 0. 4 0.0 2 0.2 5 0.0 1 1.3 9 43 8 (Chlorin e Spike ) 50 0 83. 5 0.0 5 0.0 1 3.5 7 0.1 8 2.2 3 0.0 9 0.89 18 1 PC C Soli d Charge s 50 0 0. 5 94. 8 0.27 5 41. 8 1.8 5 63. 4 0. 1 12. 1 71 9 PC C Labpac k

Charge s (Lea d Spike ) 50 0 0. 5 66. 5 0.00 9 60800 0 9.9 9 3.8 3 0. 1 1 11 6 (Chlorin e Spike ) 50 0 89. 8 67. 2 0.0 1 8 0. 4 5 0. 2 2 11 3 SC C Hig h Bt u 1337 0 0.5 4 1. 5 0.0 1 4 0. 2 2. 5 0. 1 1 18 0
Total s

1 of2

## Ony xEnvironmenta l Service s -Sauget , I L

Unit2 Fee d Dat

a Uni t# 2 Ru n #3 Date : 09/19/0 3 Tes tTime : 12:5 0 t o 16:0 1 Therma l Chlorin e As h Mercury Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g " (lb/hr) ' " Wast e Typ e (MMBtu/hr ) (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) Loadin g " (lb/hr) ' " PC C Hig h Bt u 10.7 6 11.8 8 73.2 6 0.00005 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 PC C Lo wBt u 0.8 6 8.6 1 344.4 0 0.00017 4 0.0 1 0.0 0 0.0 1 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 2 168.0 0 0.00000 4 0.0 0 0.0 0 0.0 7 0.0 0 47.7 1 PC C S p Fd r 0.2 2 2.1 9 343.3 9 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chlorin e Spike ) o.o s 151.1 4 0.0 9 0.00000 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 PC C Soli d Charge s 0.3 6 3.6 0 681.6 1 0.00019 8 0.0 3 0.0 0 0.0 5 0.0 0 0.0 1 PC C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 6 0.5 8 77.1 4 0.00000 1 70.5 3 0.0 0 0.0 0 0.0 0 0.0 0 (Chlorin e Spike ) 0.0 6 101.4 7 75.9 4 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 SC C Hig h Bt u 2.4 1 0.9 7 2.7 0 0.00000 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 14.9 2 261.5 6 1766.5 3 0.00043 1 , 70.5 7 0.0 0 0.1 2 0.0 0 47.7 2

2 of2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Data Uni t#4 Run# 1 Conditio n #1 Date : 09/16/0 3 Tes tTime : 09:5 6 t o 13:5 3 P P M P P M P P M P P M P P M P P M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1203 0 2.1 4 10. 3 0.05 2 2.1 8 0.82 5 2.7 6 0.02 5 0.2 5 111 0 P C C Lo wBt u 50 0 0. 5 21. 3 0.00 6 1.0 3 2.7 4 0.52 4 0.00 5 0.36 2 170 5 (Chromiu m Spike ) 50 0 0. 5 75. 3 0.01 6 15 0.3 3 31 6 0.2 1 21200 0 22 6 P C C Chlorin e Spik e (X-10 ) 200 0 83. 5 0.0 5 0.0 1 3.9 2 0. 2 2.4 5 0. 1 0.9 8 13 6 P C C Soli d Charge s 50 0 0. 5 93. 9 1.1 9 19. 7 1. 4 16. 7 0. 1 8.6 8 145 6 P C C Labpac k

Charge s 500 0 0. 5 (Mercur ySpik e - Mod e 1 ) 50 0 0. 5 2. 9 2980 0 0. 2 0.0 1 0.12 5 0.00 5 0.44 2 1.6 4 (Mercur ySpik e - Mod e 2 ) (Lea d Spike ) 50 0 0. 5 66. 1 0.00 9 62900 0 40 1 5 0. 2 2 17 6 P C C Bul k

Solid s (w/hex ) 150 0 1. 5 87. 3 0.72 1 15. 7 1.1 3 37. 9 0. 1 5. 4 694 8 (Chlorin e Spike ) S C C Hig h Bt u 866 0 1.2 9 2. 2 0.082 2 1.4 3 0.0 5 2.0 9 0.02 5 0.2 5 100 3
Total s

1 o f2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Data Uni t#4 Run# 1 Conditio n #1 Date : 09/16/0 3 Tes tTime : 09:5 6 t o 13:5 3 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 13.3 5 23.7 5 114.3 3 0.00005 8 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Lo wBt u 0.8 5 8.5 3 363.1 7 0.00001 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 3 170.1 8 0.00000 4 0.0 0 0.0 0 0.0 7 0.0 0 47.9 1 P C C Chlorin e Spik e (X-10 ) 0.2 7 113.5 6 0.0 7 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.7 3 7.2 8 1367.1 8 0.00173 3 0.0 3 0.0 0 0.0 2 0.0 0 0.0 1 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 1 ) 0.0 0 0.0 1 0.0 5 0.04887 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 2 ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 9 0.8 8 116.3 4 0.00000 2 110.7 0 0.0 7 0.0 0 0.0 0 0,0 0 P C C Bul k

Solid s (w/hex ) 10.4 2 104.2 2 6065.6 0 0.00501 0 0.1 1 0.0 1 0.2 6 0.0 0 0.0 4 (Chlorin e Spike ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 8.6 9 12.9 4 22.0 7 0.00008 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 34.5 2 272.3 0 8218.9 8 0.05577 1 110.8 5 0.0 9 0.3 7 0.0 0 47.9 6 tota l SV M 110.9 4 48.3 3 tota l LV M

2 o f2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Data Uni t#4 Ru n # 2 Conditio n #1 Date : 09/16/0 3 Tes tTime : 16:4 5 t o 19:5 3 P P M P P M P P M P P M P P M P P M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1203 0 2.1 4 8. 1 0.079 2 2.0 4 0.80 5 3.1 6 0.02 5 2.1 1 111 0 P C C Lo wBt u 50 0 0. 5 29. 4 0.005 2 0.94 6 2.5 3 0.5 2 0.00 5 0.8 1 171 0 (Chromiu m Spike ) 50 0 0. 5 74. 1 0.01 6 1 5 0.2 6 31 0 0.1 8 21600 0 22 7 P C C Chlorin e Spik e (X-10 ) 200 0 83. 5 0.0 5 0.00 9 4 0. 2 2. 5 0. 1 1 14 4 P C C Soli d Charge s 50 0 0. 5 95. 9 0.06 6 15. 6 0.6 1 2.6 6 0. 1 7.0 7 150 1 P C C Labpac k

Charge s 500 0 0. 5 (Mercur ySpik e - Mod e 1 ) 50 0 0. 5 1. 8 2950 0 0.40 3 0.0 1 0.12 5 0.00 5 0.49 2 1.6 6 (Mercur ySpik e - Mod e 2 ) (Lea d Spike ) 50 0 0. 5 65. 4 0.0 1 62100 0 6.3 5 4.8 1 0.1 9 1.9 2 17 9 P C C Bul k

Solid s (w/hex ) 150 0 1. 5 62. 6 0.71 9 10. 6 0.6 7 16. 8 0. 1 8.9 4 706 2 (Chlorin e Spike ) S C C Hig h Bt u 866 0 1.2 9 3 0.06 8 1.1 8 0.0 5 1.7 1 0.02 5 0.2 5 100 4
Total s

1 o f2

## OnyxEnvironmenta l Service s - Sauget , I L Uni t4 Fee d Data Uni t#4 Ru n # 2 Conditio n # 1 Date : 09/16/0 3 Tes tTime : 16:4 5 t o 19:5 3 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (lb/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 13.3 5 23.7 5 89.9 1 0.00008 8 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Lo wBt u 0.8 6 8.5 5 502.7 4 0.00000 9 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 4 168.2 1 0.00000 4 0.0 0 0.0 0 0.0 7 0.0 0 49.0 3 P C C Chlorin e Spik e (X-10 ) 0.2 9 120.2 4 0.0 7 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.7 5 7.5 1 1439.4 6 0.00009 9 0.0 2 0.0 0 0.0 0 0.0 0 0.0 1 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 1 ) 0.0 0 0.0 1 0.0 3 0.04897 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 2 ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 9 0.9 0 117.0 7 0.00000 2 111.1 6 0.0 0 0.0 0 0.0 0 0.0 0 P C C Bul k

Solid s (w/hex ) 10.5 9 105.9 3 4420.8 1 0.00507 8 0.0 7 0.0 0 0.1 2 0.0 0 0.0 6 (Chlorin e Spike ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 8.6 9 12.9 5 30.1 2 ,0.00006 8 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 34.7 4 280.9 7 6768.4 2 0.05431 8 111.2 7 0.0 1 0.2 0 0.0 0 49.1 1 111.2 8 49.3 1

2 o f2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Data Uni t#4 Ru n # 3 Conditio n #1 Date : 09/17/0 3 Tes tTime : 08:0 0 t o 11:0 9

.. . P P M P P M P P M P P M P P M P P M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1203 0 2.1 4 5. 9 0.078 6 1 0.74 2 0.62 5 0.02 5 0.2 5 111 0 P C C Lo wBt u 50 0 0. 5 27. 1 0.013 8 1.4 4 2.7 1 0.88 2 0.00 5 0.0 5 171 0 (Chromiu m Spike ) 50 0 0. 5 74. 4 0.01 6 15 0.3 5 30 7 0.2 5 21700 0 22 2 P C C Chlorin e Spik e (X-10 ) 200 0 83. 5 0.0 5 0.02 3 3.8 5 0.1 9 2. 4 0. 1 0.9 6 13 5 P C C Soli d Charge s 50 0 0. 5 95. 9 0.05 8 15. 2 0.6 2 15. 5 0.0 9 4.1 8 155 5 P C C Labpac k

Charge s 500 0 0. 5 (Mercur ySpik e - Mod e 1 ) 50 0 0. 5 0. 3 2920 0 1 7 0.0 1 0.12 5 0.00 5 0.0 5 1.7 2 (Mercur ySpik e - Mod e 2 ) (Lea d Spike ) 50 0 0. 5 65. 9 0.0 1 66800 0 7.2 2 4.6 3 0.1 9 1.8 5 18 5 P C C Bul k

Solid s (w/hex ) 150 0 1. 5 78. 4 0.52 5 66 8 0.9 6 36. 6 0. 1 8.3 1 675 6 (Chlorin e Spike ) S C C Hig h Bt u 866 0 1.2 9 8. 7 0.093 4 1.3 8 0.06 5 2.0 9 0.02 5 0.2 5 100 3
Total s

1 o f2

## OnyxEnvironmenta l Service s - Sauget , I L Uni t4 Fee d Data Uni t#4 Ru n # 3 Conditio n # 1 Date : 09/17/0 3 Tes tTime : 08:0 0 t o 11:0 9 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 13.3 5 23.7 5 65.4 9 0.00008 7 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Lo wBt u 0.8 6 8.5 5 463.4 1 0.00002 4 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 1 165.1 7 0.00000 4 0.0 0 0.0 0 0.0 7 0.0 0 48.1 7 P C C Chlorin e Spik e (X-10 ) 0.2 7 112.7 3 0.0 7 0.00000 3 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.7 8 7.7 8 1491.2 5 0.00009 0 0.0 2 0.0 0 0.0 2 0.0 0 0.0 1 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 1 ) 0.0 0 0.0 1 0.0 1 0.05022 4 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 2 ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 9 0.9 3 121.9 2 0.00000 2 123.5 8 0.0 0 0.0 0 0.0 0 0.0 0 P C C Bul k

Solid s (w/hex ) 10.1 3 101.3 4 5296.7 0 0.00354 7 4.5 1 0.0 1 0.2 5 0.0 0 0.0 6 (Chlorin e Spike ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 8.6 9 12.9 4 87.2 6 0.00009 4 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 34.2 8 269.1 3 7691.2 7 0.05407 4 128.1 3 0.0 1 0.3 5 0.0 0 48.2 4 128.1 4 48.5 8

2 o f2

## Ony xEnvironmenta l Service s -Sauget , I L

Unit4 Feed Dat

a Uni t# 4 Run# 1 Conditio n # 2 Date : 09/17/0 3 Tes tTime : 11:4 5 t o 15:0 4

- ••••• PP M PP M PP M PP M PP M PP M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercury Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr ) PC C Hig h Bt u 1203 0 2.1 4 5. 5 0.068 8 1 0. 7 1.4 1 0.02 5 0.2 5 110 8 PC C Lo wBt u 50 0 0. 5 3 1 0.00 5 0.81 4 2.4 2 0.41 7 0.00 5 0.6 3 170 9 (Chromiu m Spike ) 50 0 0. 5 75 0.01 6 4 0.5 2 36 9 0.1 5 20500 0 21 3 PC C Chlorin e Spik e (X-10 ) 200 0 83. 5 0.0 5 0.0 1 4 0. 2 2. 5 0. 1 1 13 8 PC C Soli d Charge s 50 0 0. 5 96. 4 0.0 9 17. 7 0.7 9 10. 3 0. 1 6.2 7 154 0 PC C Labpac k

Charge s 500 0 0. 5 (MercurySpik e - Mod e 1 ) (MercurySpik e - Mod e 2 ) 50 0 0. 5 1 3000 0 0. 2 0.0 1 0.12 5 0.00 5 0.57 4 5.6 5 (Lea d Spike ) 50 0 0. 5 65. 9 0.0 1 66400 0 7. 8 5 0. 2 2 17 6 PC C Bul k

Solid s (w/hex ) 150 0 1. 5 86. 2 0.41 6 12 5 1.8 5 53. 6 0. 1 10. 6 678 6 (Chlorin e Spike ) S C C Hig h Bt u 866 0 1.2 9 0. 7 0.063 8 1 0.0 5 1.42 0.02 5 0.2 5 100 3
Total s

1 of2

## Ony xEnvironmenta l Service s - Sauget , I L

Unit4 Fee d Dat

a Uni t# 4 Run #1 Conditio n # 2 Date : 09/17/0 3 Tes tTime : 11:4 5 t o 15:0 4 Therma l Chlorin e As h Mercury Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr ) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib/hr

) (Ib

/hr ) PC C Hig h Bt u 13.3 3 23.7 1 60.9 4 0.00007 6 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 PC C Lo wBt u 0.8 5 8.5 5 529.7 9 0.00000 9 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.07 159.7 5 0.00000 3 0.0 0 0.0 0 0.0 8 0.0 0 43.6 7 PC C Chlorin e Spik e (X-10 ) 0.2 8 115.2 3 0.0 7 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 PC C Soli d Charge s 0.7 7 7.7 0 1484.5 6 0.00013 9 0.0 3 0.0 0 0.0 2 0.0 0 0.0 1 PC C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (MercurySpik e - Mod e 1 ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (MercurySpik e - Mod e 2 ) 0.0 0 0.0 3 0.0 6 0.16950 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 9 0.8 8 115.9 8 0.00000 2 116.8 6 0.0 0 0.0 0 0.0 0 0.0 0 PC C Bul k

Solid s (w/hex ) 10.1 8 101.7 9 5849.5 3 0.00282 3 0.8 5 0.0 1 0.3 6 0.0 0 0.0 7 (Chlorin e Spike ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 SC C Hig h Bt u 8.6 9 12.9 4 7.0 2 0.00006 4 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 34.2 9 271.8 9 8207.7 0 0.17261 7 117.7 4 0.0 2 0.4 6 0.0 0 43.7 5 117.7 6 44.2 1

2 o f2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Data Uni t#4 Ru n # 2 Conditio n #2 Date : 09/17/0 3 Tes tTime : 15:4 0 t o 18:4 9 P P M P P M P P M P P M P P M PPM ' Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1203 0 2.1 4 5. 5 0.051 4 1 0.7 1 0.91 2 0.02 5 0.2 5 88 0 P C C Lo wBt u 50 0 0. 5 26. 6 0.0 1 0.68 5 1.9 9 0.44 6 0.00 5 0.43 2 170 8 (Chromiu m Spike ) 50 0 0. 5 74. 3 0.01 6 4 0.5 1 37 2 0. 1 21100 0 22 3 P C C Chlorin e Spik e (X-10 ) 200 0 83. 5 0.0 5 0.0 1 4 0. 2 2. 5 0. 1 1 14 4 P C C Soli d Charge s 50 0 0. 5 95. 7 0.17 1 45. 1 1.7 5 42. 1 0.0 9 12. 7 152 0 P C C Labpac k

Charge s 500 0 0. 5 (Mercur ySpik e - Mod e 1 ) (Mercur ySpik e - Mod e 2 ) 50 0 0. 5 2. 6 3090 0 0. 2 0.0 1 0.12 5 0.00 5 0.59 8 6.1 1 (Lea d Spike ) 50 0 0. 5 6 6 0.01 1 66600 0 6. 7 6.2 5 0.2 5 2. 5 19 0 P C C Bul k

Solid s (w/hex ) 150 0 1. 5 76. 2 0.5 4 17 5 4. 4 21 8 0. 1 23. 1 750 6 (Chlorin e Spike ) S C C Hig h Bt u 866 0 1.2 9 0. 6 0.063 4 1 0.05 2 1.0 9 0.02 5 0.2 5 100 1
Total s

1 o f2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Data Uni t#4 Ru n #2 Conditio n #2 Date : 09/17/0 3 Tes tTime : 15:4 0 t o 18:4 9 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 10.5 9 18.8 3 48.4 0 0.00004 5 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Lo wBt u 0.8 5 8.5 4 454.3 3 0.00001 7 0.0 0 0.0 0 0.0 0
. 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 2 165.6 9 0.00000 4 0.0 0 0.0 0 0.0 8 0.0 0 47.0 5 P C C Chlorin e Spik e (X-10 ) 0.2 9 120.2 4 0.0 7 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.7 6 7.6 0 1454.6 4 0.00026 0 0.0 7 0.0 0 0.0 6 0.0 0 0.0 2 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 1 ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 2 ) 0.0 0 0.0 3 0.1 6 0.18879 9 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.1 0 0.9 5 125.4 0 0.00000 2 126.5 4 0.0 0 0.0 0 0.0 0 0.0 0 P C C Bul k

Solid s (w/hex ) 11.2 6 112.5 9 5719.5 7 0.00405 3 1.3 1 0.0 3 1.6 4 0.0 0 0.1 7 (Chlorin e Spike ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 8.6 7 12.9 1 6.0 1 0.00006 3 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 32.6 3 282.8 1 7974.2 7 0.19324 5 127.9 3 0.0 4 1.7 9 0.0 0 47.2 5 127.9 7 49.0 4

2 o f2

## OnyxEnvironmenta l Service s -Sauget , SL Uni t4 Fee d Data Uni t#4 Ru n #3 Conditio n # 2 Date : 09/18/0 3 Tes tTime : 08:1 0 t o 11:1 8 P P M P P M P P M P P M P P M P P M Feedrat e Wast e Typ e Btu/l b %Chlorin e %As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m (Ib/hr) P C C Hig h Bt u 1203 0 2.1 4 16. 9 0.19 5 1 1.0 6 0.62 5 0.02 5 0.6 5 110 9

• P C C Lo wBt u 50 0 0. 5 27. 2 0.036 3 0.9 7 2. 3 0.82 6 0.00 5 0.97 8 171 1 (Chromiu m Spike ) 50 0 0. 5 74. 1 0.16 7 15 0.5 1 32 5 0. 1 21600 0 22 6 P C C Chlorin e Spik e (X-10 ) 200 0 83. 5 0.0 5 0.00 9 3.3 9 0.1 7 2.1 2 0.0 8 0.8 5 13 9 P C C Soli d Charge s 50 0 0. 5 93. 8 0.26 1 56. 2 2.0 6 42. 5 0.0 9 10. 6 154 6 P C C Labpac k

Charge s 500 0 0. 5 154 6 (Mercur ySpik e - Mod e 1 ) (Mercur ySpik e - Mod e 2 ) 50 0 0. 5 0.0 5 3100 0 0. 2 0.0 1 0.12 5 0.00 5 0.55 5 6.0 5 (Lea d Spike ) 50 0 0. 5 66. 8 0.02 6 61700 0 0.4 5 5.6 8 0.2 3 2.2 7 18 8 P C C Bul k

Solid s (w/hex ) 150 0 1. 5 88. 7 0.52 9 56. 1 1. 1 64. 3 0.0 9 10. 8 772 2 (Chlorin e Spike ) S C C Hig h Bt u 866 0 1.2 9 7. 8 0.07 9 1.2 9 0.07 8 1.8 5 0.02 5 0.3 7 100 3
Total s

1 o f2

## OnyxEnvironmenta l Service s -Sauget , I L Uni t4 Fee d Dat a Uni t#4 Ru n # 3 Conditio n #2 Date : 09/18/0 3 Tes tTime : 08:1 0 t o 11:1 8 Therma l Chlorin e As h Mercur y Lea d Cadmiu m Arseni c Berylliu m Chromiu m Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Loadin g Wast e Typ e (MMBtu/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (lb/hr ) (Ib/hr) (Ib/hr) (Ib/hr) (Ib/hr) P C C Hig h Bt u 13.3 4 23.7 3 187.4 2 0.00021 6 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Lo wBt u 0.8 6 8.5 6 465.3 9 0.00006 2 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Chromiu m Spike ) 0.1 1 1.1 3 167.4 7 0.00003 8 0.0 0 0.0 0 0.0 7 0.0 0 48.8 2 P C C Chlorin e Spik e (X-10 ) 0.2 8 116.0 7 0.0 7 0.00000 1 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 P C C Soli d Charge s 0.7 7 7.7 3 1450.1 5 0.00040 4 0.0 9 0.0 0 0.0 7 0.0 0 0.0 2 P C C Labpac k

Charge s 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 1 ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Mercur ySpik e - Mod e 2 ) 0.0 0 0.0 3 0.0 0 0.18755 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 (Lea d Spike ) 0.0 9 0.9 4 125.5 8 0.00000 5 116.0 0 0.0 0 0.0 0 0.0 0 0,0 0 P C C Bul k

Solid s (w/hex ) 11.5 8 115.8 3 6849.4 1 0.00408 5 0.4 3 0.0 1 0.5 0 0.0 0 0.0 8 (Chlorin e Spike ) 0.0 0 0.0 0 0.0 0 0.00000 0 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0 S C C Hig h Bt u 8.6 9 12.9 4 78.2 3 0.00007 9 0.0 0 0.0 0 0.0 0 0.0 0 0.0 0
Total s 35.7 3 286.9 5 9323.7 3 0.19244 0 116.5 2 0.0 2 0.6 4 0.0 0 48.9 2 | 116.5 4 49.5 6

2 o f2

### APPENDIXC FIEL D EQUIPMENTCALIBRATIO N FORM S

### ANALYTICA LDAT AREPORTS

C:\Doamrents an d SeoingsVM i W W * r i * ^ 090 3 datauppe * Covers.tJo c January200 4

## V