### Name: Patricia Q. West

Title: Manager, Environmental, Energy Supp Company: Progress Energy Florida, Inc. Sign Date: 9/3/2010 Name: Michael Sussman, P.E. Title: Project Manager Company: Kleinfelder Southeast, Inc. Sign Date: 9/3/2010 Permitted Facility Representative / Date Testing Company Representative / Date



## Progress Energy Florida Suwannee River Power Plant Unit 2 Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Thursday, February 17, 2011 Page 1 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Facility Information: Progress Energy Florida, Inc. Suwannee Riv
4037 River Road

Live Oak FL 32060 Contact: Cary W. Hamilton Phone: Fax: Email: cary.hamilton@pgnmail.com Testing Company:
Kleinfleder Southeast Inc. 6200 Harris Technology Blvd.

Charlotte NC 28269 Contact: W. Quentin Best Phone: 704-598-1049 Fax: 704-598-1050 Email: qbest@kleinfelder.com

Air Permit Number: 1210003-007-AV Permitted Source ID/Name: Fossil Fuel Fired Steam Generator Unit No. 2 Suw Unit 2 Permitted Maximum Process Rate: Max. Normal Operation Process Rate: Target Process Test Rate Industry/SCC/NAIS 221121 AFS #: 1212100003 FRS #: 110000909214

SCC / Description 10100501 External Combustion Boilers - Electric Generation - Distillate Oil - Grades 1 and 2 Oil

The following state and federal regulations that apply to the proposed testing:

Regulation Description Compound Limit Unit ICR % H2O 0 percent(%) ICR 1,2,3,4,6,7,8-HpCDD 0 ng/dscm corrected ICR 1,2,3,4,6,7,8-HpCDD 0 lb/million BTU using O2 ICR 1,2,3,4,6,7,8-HpCDF 0 ng/dscm corrected ICR 1,2,3,4,6,7,8-HpCDF 0 lb/million BTU using O2 ICR 1,2,3,4,7,8,9-HpCDF 0 ng/dscm corrected ICR 1,2,3,4,7,8,9-HpCDF 0 lb/million BTU using O2 ICR 1,2,3,4,7,8-HxCDD 0 ng/dscm corrected ICR 1,2,3,4,7,8-HxCDD 0 lb/million BTU using O2 ICR 1,2,3,4,7,8-HxCDF 0 ng/dscm corrected ICR 1,2,3,4,7,8-HxCDF 0 lb/million BTU using O2 ICR 1,2,3,6,7,8-HxCDD 0 ng/dscm corrected ICR 1,2,3,6,7,8-HxCDD 0 lb/million BTU using O2 ICR 1,2,3,6,7,8-HxCDF 0 ng/dscm corrected ICR 1,2,3,6,7,8-HxCDF 0 lb/million BTU using O2 ICR 1,2,3,7,8,9-HxCDD 0 ng/dscm corrected



### Thursday, February 17, 2011 Page 2 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
ICR 1,2,3,7,8,9-HxCDD 0 lb/million BTU using O2 ICR 1,2,3,4,6,7,8-HpCDF 0 ng/dscm corrected ICR 1,2,3,7,8,9-HxCDF 0 lb/million BTU using O2 ICR 1,2,3,7,8-PeCDD 0 ng/dscm corrected ICR 1,2,3,7,8-PeCDD 0 lb/million BTU using O2 ICR 1,2,3,7,8-PeCDF 0 ng/dscm corrected ICR 1,2,3,7,8-PeCDF 0 lb/million BTU using O2 ICR 2,3,3',4,4',5,5'-HpCB (PCB189) 0 ng/dscm corrected

ICR 2,3,3',4,4',5,5'-HpCB (PCB189) 0 lb/million BTU using O2 ICR 2,3,3',4,4',5/2,3,3',4,4',5'- HxCB (PCBs156/157) 0 ng/dscm corrected

ICR 2,3,3',4,4',5/2,3,3',4,4',5'- HxCB (PCBs156/157) 0 lb/million BTU using O2 ICR 2,3,3',4,4'-PeCB (PCB105) 0 ng/dscm corrected ICR 2,3,3',4,4'-PeCB (PCB105) 0 lb/million BTU using O2 ICR 2,3',4,4',5,5'-HxCB (PCB167) 0 ng/dscm corrected

ICR 2,3',4,4',5,5'-HxCB (PCB167) 0 lb/million BTU using O2 ICR 2,3,4,4',5-PeCB (PCB114) 0 ng/dscm corrected ICR 2,3,4,4',5-PeCB (PCB114) 0 lb/million BTU using O2 ICR 2,3',4,4',5-PeCB (PCB118) 0 ng/dscm corrected ICR 2,3',4,4',5-PeCB (PCB118) 0 lb/million BTU using O2 ICR 2',3,4,4',5-PeCB (PCB123) 0 ng/dscm corrected ICR 2',3,4,4',5-PeCB (PCB123) 0 lb/million BTU using O2 ICR 2,3,4,6,7,8-HxCDF 0 ng/dscm corrected ICR 2,3,4,6,7,8-HxCDF 0 lb/million BTU using O2 ICR 2,3,4,7,8-PeCDF 0 ng/dscm corrected ICR 2,3,4,7,8-PeCDF 0 lb/million BTU using O2 ICR 2,3,7,8-TCDD 0 ng/dscm corrected ICR 2,3,7,8-TCDD 0 lb/million BTU using O2 ICR 2,3,7,8-TCDF 0 ng/dscm corrected ICR 2,3,7,8-TCDF 0 lb/million BTU using O2 ICR 2-Methylnaphthalene 0 ng/dscm corrected ICR 2-Methylnaphthalene 0 lb/million BTU using O2 ICR 3,3',4,4',5,5'-HxCB (PCB169) 0 ng/dscm corrected



### Thursday, February 17, 2011 Page 3 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
ICR 3,3',4,4',5,5'-HxCB (PCB169) 0 lb/million BTU using O2 ICR 3,3',4,4',5-PeCB (PCB126) 0 ng/dscm corrected ICR 3,3',4,4',5-PeCB (PCB126) 0 lb/million BTU using O2 ICR 3,3',4,4'-TCB (PCB77) 0 ng/dscm corrected ICR 3,3',4,4'-TCB (PCB77) 0 lb/million BTU using O2 ICR 3,4,4',5-TCB (PCB81) 0 ng/dscm corrected ICR 3,4,4',5-TCB (PCB81) 0 lb/million BTU using O2 ICR Acenaphthene** 0 ug/dscm corrected ICR Acenaphthene** 0 lb/million BTU using O2 ICR Acenaphthylene** 0 ug/dscm corrected ICR Acenaphthylene** 0 lb/million BTU using O2 ICR Anthracene** 0 ug/dscm corrected ICR Anthracene** 0 lb/million BTU using O2 ICR Antimony 0 lb/million BTU using O2 ICR Arsenic 0 lb/million BTU using O2 ICR Barium 0 lb/million BTU using O2 ICR Benzo(a)Anthracene* 0 ug/dscm corrected ICR Benzo(a)Anthracene* 0 lb/million BTU using O2 ICR Benzo(a)Pyrene* 0 ug/dscm corrected ICR Benzo(a)Pyrene* 0 lb/million BTU using O2 ICR Benzo(b)Fluoranthene* 0 ug/dscm corrected ICR Benzo(b)Fluoranthene* 0 lb/million BTU using O2 ICR Benzo(e)Pyrene 0 ug/dscm corrected ICR Benzo(e)Pyrene 0 lb/million BTU using O2 ICR Benzo(ghi)Perylene** 0 ug/dscm corrected ICR Benzo(ghi)Perylene** 0 lb/million BTU using O2 ICR Benzo(k)Fluoranthene* 0 ug/dscm corrected ICR Benzo(k)Fluoranthene* 0 lb/million BTU using O2 ICR Beryllium 0 lb/million BTU using O2 ICR Bromine 0 lb/million BTU using O2 ICR Cadmium 0 lb/million BTU using O2 ICR Carbon Monoxide 0 ppm corrected ICR Carbon Monoxide 0 lb/million BTU using O2


### Thursday, February 17, 2011 Page 4 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
ICR Chromium 0 lb/million BTU using O2 ICR Chrysene* 0 ug/dscm corrected ICR Chrysene* 0 lb/million BTU using O2 ICR Co2 0 percent(%) ICR Cobalt 0 lb/million BTU using O2 ICR Copper 0 lb/million BTU using O2 ICR Dibenzo(a,h)Anthracene* 0 ng/dscm corrected ICR Dibenzo(a,h)Anthracene* 0 lb/million BTU using O2 ICR Filterable Particulate 0 lb/million BTU using O2 ICR Filterable PM2.5 0 lb/million BTU using O2 ICR Fluoranthene** 0 ug/dscm corrected ICR Fluoranthene** 0 lb/million BTU using O2 ICR Fluorene** 0 ug/dscm corrected ICR Fluorene** 0 lb/million BTU using O2 ICR Formaldehyde 0 ppm corrected ICR Formaldehyde 0 lb/million BTU using O2 ICR Hydrogen Chloride 0 lb/million BTU using O2 ICR Hydrogen Fluoride 0 lb/million BTU using O2 ICR Indeno(1,2,3-cd)Pyrene* 0 ug/dscm corrected ICR Indeno(1,2,3-cd)Pyrene* 0 lb/million BTU using O2 ICR Inorganic (Aqueous) Condensible Part. 0 lb/million BTU using O2 ICR Lead 0 lb/million BTU using O2 ICR Magnesium 0 lb/million BTU using O2 ICR Manganese 0 lb/million BTU using O2 ICR Mercury 0 lb/million BTU using O2 ICR Naphthalene** 0 ug/dscm corrected ICR Naphthalene** 0 lb/million BTU using O2 ICR Nickel 0 lb/million BTU using O2 ICR Nitrogen oxides (NOx) 0 ppm corrected ICR Nitrogen oxides (NOx) 0 lb/million BTU using O2 ICR O2 0 percent(%) ICR OCDD 0 ng/dscm corrected



### Thursday, February 17, 2011 Page 5 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
ICR OCDD 0 lb/million BTU using O2 ICR OCDF 0 ng/dscm corrected ICR OCDF 0 lb/million BTU using O2 ICR Organic Condensible Particulate 0 lb/million BTU using O2 ICR Other Di-CBs 0 ng/dscm corrected ICR Other Di-CBs 0 lb/million BTU using O2 ICR Other Hepta-CBs 0 ng/dscm corrected ICR Other Hepta-CBs 0 lb/million BTU using O2 ICR Other Hexa-CBs 0 ng/dscm corrected ICR Other Hexa-CBs 0 lb/million BTU using O2 ICR Other HpCDD 0 ng/dscm corrected ICR Other HpCDD 0 lb/million BTU using O2 ICR Other HpCDF 0 ng/dscm corrected ICR Other HpCDF 0 lb/million BTU using O2 ICR Other HxCDD 0 ng/dscm corrected ICR Other HxCDD 0 lb/million BTU using O2 ICR Other HxCDF 0 ng/dscm corrected ICR Other HxCDF 0 lb/million BTU using O2 ICR Other Mono-CBs 0 ug/dscm corrected ICR Other Mono-CBs 0 lb/million BTU using O2 ICR Other Nona-CBs 0 ng/dscm corrected ICR Other Nona-CBs 0 lb/million BTU using O2 ICR Other Octa-CBs 0 ng/dscm corrected ICR Other Octa-CBs 0 lb/million BTU using O2 ICR Other PeCDD 0 ng/dscm corrected ICR Other PeCDD 0 lb/million BTU using O2 ICR Other PeCDF 0 ng/dscm corrected ICR Other PeCDF 0 lb/million BTU using O2 ICR Other Penta-CBs 0 ng/dscm corrected ICR Other Penta-CBs 0 lb/million BTU using O2 ICR Other TCDD 0 ng/dscm corrected ICR Other TCDD 0 lb/million BTU using O2 ICR Other TCDF 0 ng/dscm corrected ICR Other TCDF 0 lb/million BTU using O2


### Thursday, February 17, 2011 Page 6 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
ICR Other Tetra-CBs 0 ng/dscm corrected ICR Other Tetra-CBs 0 lb/million BTU using O2 ICR Other Tri-CBs 0 ng/dscm corrected ICR Other Tri-CBs 0 lb/million BTU using O2 ICR Perylene 0 ug/dscm corrected ICR Perylene 0 lb/million BTU using O2 ICR Phenanthrene** 0 ug/dscm corrected ICR Phenanthrene** 0 lb/million BTU using O2 ICR Phosphorus (yellow or white) 0 lb/million BTU using O2 ICR Pyrene** 0 ug/dscm corrected ICR Pyrene** 0 lb/million BTU using O2 ICR Selenium 0 lb/million BTU using O2 ICR Silver 0 lb/million BTU using O2 ICR Sulfur Dioxide 0 ppm corrected ICR Sulfur Dioxide 0 lb/million BTU using O2 ICR Thallium 0 lb/million BTU using O2 ICR Total 16*/**PAH 0 ug/dscm corrected ICR Total 16*/**PAH 0 lb/million BTU using O2 ICR Total 7*PAH 0 ug/dscm corrected ICR Total 7*PAH 0 lb/million BTU using O2 ICR Total Dioxins 0 ng/dscm corrected ICR Total Dioxins 0 lb/million BTU using O2 ICR Total Furans 0 ng/dscm corrected ICR Total Furans 0 lb/million BTU using O2 ICR Total organic compounds (TOC) as Propane 0 ppm corrected

ICR Total organic compounds (TOC) as Propane 0 lb/million BTU using O2 ICR Total PCBs 0 ng/dscm corrected ICR Total PCBs 0 lb/million BTU using O2 ICR Total PM2.5 0 lb/million BTU using O2 ICR Total TEQ 0 ng/dscm corrected ICR Total TEQ 0 lb/million BTU using O2 ICR Zinc 0 lb/million BTU using O2 ICR Methane 0 ppm corrected



### Thursday, February 17, 2011 Page 7 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Boiler No. 2 (E.U. ID No. -002) is a nominal 34.0 megawatt electric steam generator. The boiler is allowed to fireNo.2 fuel oil, No.6 fuel oil, “on specification” used oil, natural gas and a blend of fuel oil and natural gas. The “onspecification used oil is generally fired as blended fuel oil with either the No.2 fuel oil or No. 6 fuel oil. The boiler drives a turbine generator for electrical power and vents to its own stack. There is no air pollution equipment control devices associated with the boiler.
Sampling Location Information:

Test Parameter Information: Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width Stack Exit 84 900 216 2 0 24 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location Carbon Monoxide Method 10 3 120 0 Stack Exit Formaldehyde Method 0011 3 120 0 Stack Exit 2,3,7,8-TCDD Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDD Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,7,8,9-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,4,6,7,8-HpCDD Method 23 3 480 0 Stack Exit OCDD Method 23 3 480 0 Stack Exit 2,3,7,8-TCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDF Method 23 3 480 0 Stack Exit 2,3,4,7,8-PeCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 2,3,4,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8,9-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,4,6,7,8-HpCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8,9-HpCDF Method 23 3 480 0 Stack Exit OCDF Method 23 3 480 0 Stack Exit Other TCDD Method 23 3 480 0 Stack Exit Other PeCDD Method 23 3 480 0 Stack Exit Other HxCDD Method 23 3 480 0 Stack Exit Other HpCDD Method 23 3 480 0 Stack Exit Other TCDF Method 23 3 480 0 Stack Exit Other PeCDF Method 23 3 480 0 Stack Exit Other HxCDF Method 23 3 480 0 Stack Exit Other HpCDF Method 23 3 480 0 Stack Exit Total Dioxins Method 23 3 480 0 Stack Exit ICR Methane 0 lb/million BTU using O2 ICR Hydrogen Cyanide 0 lb/million BTU using O2



### Thursday, February 17, 2011 Page 8 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.

Total Furans Method 23 3 480 0 Stack Exit 3,3',4,4'-TCB (PCB77) Method 23 3 480 0 Stack Exit 3,4,4',5-TCB (PCB81) Method 23 3 480 0 Stack Exit 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 0 Stack Exit 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 0 Stack Exit 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 0 Stack Exit 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 0 Stack Exit 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 0 Stack Exit 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 0 Stack Exit

2,3',4,4',5,5'-HxCB (PCB167) Method 23 3 480 0 Stack Exit 3,3',4,4',5,5'-HxCB (PCB169) Method 23 3 480 0 Stack Exit 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 0 Stack Exit

Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Stack Exit

Hydrogen Fluoride Method 26A 3 180 0 Stack Exit Hydrogen Chloride Method 26A 3 180 0 Stack Exit Organic Condensible

Particulate OTM - 27/28 3 360 0 Stack Exit

Total PM2.5 OTM - 27/28 3 360 0 Stack Exit Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 360 0 Stack Exit

Filterable Particulate OTM - 27/28 0 Stack Exit Total Particulate OTM - 27/28 0 Stack Exit Filterable PM2.5 OTM - 27/28 3 360 0 Stack Exit Arsenic Method 29 3 240 0 Stack Exit Cadmium Method 29 3 240 0 Stack Exit Thallium Method 29 3 240 0 Stack Exit Beryllium Method 29 3 240 0 Stack Exit Chromium Method 29 3 240 0 Stack Exit Lead Method 29 3 240 0 Stack Exit Copper Method 29 3 240 0 Stack Exit Silver Method 29 3 240 0 Stack Exit Zinc Method 29 3 240 0 Stack Exit Filterable Particulate Method 29 3 240 0 Stack Exit Antimony Method 29 3 240 0 Stack Exit Cobalt Method 29 3 240 0 Stack Exit Barium Method 29 3 240 0 Stack Exit Manganese Method 29 3 240 0 Stack Exit Nickel Method 29 3 240 0 Stack Exit Selenium Method 29 3 240 0 Stack Exit O2 Method 3A O2 3 120 0 Stack Exit Co2 Method 3A CO2 3 120 0 Stack Exit Mercury Method 30B 6 120 0 Stack Exit Sulfur Dioxide Method 6C 3 180 0 Stack Exit Nitrogen oxides (NOx) Method 7E 3 180 0 Stack Exit



### Thursday, February 17, 2011 Page 9 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010

Thursday, February 17, 2011 Page 10 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Sampling / Stack Data Results Summary



### Location Stack Exit - Method 0011 Average Run Number 1 2 3
Test Date 2/27/2010 2/28/2010 2/28/2010 Run Start Time 12:55:00 PM 8:58:00 AM 12:55:00 PM

Run Finish Time 3:13:00 PM 11:15:00 AM 3:13:00 PM

Net Run Time, minutes 120 120 120 Dry Gas Meter Volume Sampled, dscf 87.443 86.808 91.373 88.541 Moisture Content of Stack Gas, % 7.43 6.41 5.13 6.323 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 10.31 10.19 10.09 10.197 Oxygen, % 8.04 8.19 8.24 8.157 Average Stack Gas Temperature, °F 332.58 329.33 336.04 332.650 Dry Volumetric Flow Rate, dry scfm 104,043.1 104,141.1 109,696.9 105,960.367 Actual Wet Volumetric Flue Gas Flow Rate, acfm 169,280.1 166,070.5 174,036.9 169,795.833 Percent Isokinetic of Sampling Rate, % 99.4 98.6 98.5 98.833 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Location Stack Exit - Method 10 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Thursday, February 17, 2011 Page 11 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 23 Average Run Number
Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2
Fw
Fc



### Location Stack Exit - Method 25A Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Thursday, February 17, 2011 Page 12 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 26A Average Run Number
Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2
Fw
Fc



### Location Stack Exit - Method 29 Average Run Number
Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2
Fw
Fc



### Thursday, February 17, 2011 Page 13 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 6C Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Location Stack Exit - Method 7E Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Fuel Type
Fw
Fc



### Thursday, February 17, 2011 Page 14 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - OTM - 27/28 Average Run Number
Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2
Fw
Fc



### Thursday, February 17, 2011 Page 15 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Emissions Summary



### Location: Stack Exit - Method 0011 Compound: Formaldehyde Average RunNumber 1 2 3 Mass_mg 0.00414 0.00245 0.00248 0.003 Elb/hr 6.52E-04 3.89E-04 3.94E-04 0.000 gr/dscf 7.31E-07 4.36E-07 4.19E-07 0.000 lb/mmBtuO2 1.56E-06 9.40E-07 9.08E-07 0.000 mg/dscm 1.67E-03 9.97E-04 9.59E-04 0.001 ppm 1.34E-03 7.98E-04 7.68E-04 0.001 ppm@7%O2 1.45E-03 8.73E-04 8.43E-04 0.001



### Location: Stack Exit - Method 10 Compound: Carbon Monoxide Average Run 1 2 3 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.00E+00 0.000 ppm 0.00E+00 0.00E+00 0.00E+00 0.000 ppm@7%O2 0.00E+00 0.00E+00 0.00E+00 0.000



### Location: Stack Exit - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber 1 2 3 Mass_mg 0.00000000552 0.00000000361 0.00000000474 0.000 Elb/hr 2.05E-10 1.31E-10 1.71E-10 0.000 lb/mmBtuO2 5.06E-13 3.22E-13 4.43E-13 0.000 ng/dscm 5.66E-04 3.53E-04 4.71E-04 0.000 ng/dscm@7%O2 5.87E-04 3.73E-04 5.13E-04 0.000 

### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber 1 2 3 Mass_mg 0.00000000325 0.0000000063 0.0000000129 0.000 Elb/hr 1.20E-10 2.28E-10 4.67E-10 0.000 lb/mmBtuO2 2.98E-13 5.61E-13 1.20E-12 0.000 ng/dscm 3.33E-04 6.16E-04 1.28E-03 0.001 ng/dscm@7%O2 3.45E-04 6.51E-04 1.39E-03 0.001 

### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber 1 2 3 Mass_mg 0.00000000479 0.00000000305 0.00000000353 0.000 Elb/hr 1.78E-10 1.10E-10 1.28E-10 0.000 lb/mmBtuO2 4.39E-13 2.72E-13 3.30E-13 0.000 ng/dscm 4.91E-04 2.98E-04 3.51E-04 0.000 ng/dscm@7%O2 5.09E-04 3.15E-04 3.82E-04 0.000



### Thursday, February 17, 2011 Page 16 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Compound: 1,2,3,4,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.00000000451 0.00000000256 0.00000000352 0.000 Elb/hr 1.67E-10 9.27E-11 1.27E-10 0.000 lb/mmBtuO2 4.13E-13 2.28E-13 3.29E-13 0.000 ng/dscm 4.62E-04 2.50E-04 3.50E-04 0.000 ng/dscm@7%O2 4.79E-04 2.64E-04 3.81E-04 0.000 

### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.00000000313 0.00000000228 0.00000000257 0.000 Elb/hr 1.16E-10 8.26E-11 9.30E-11 0.000 lb/mmBtuO2 2.87E-13 2.03E-13 2.40E-13 0.000 ng/dscm 3.21E-04 2.23E-04 2.55E-04 0.000 ng/dscm@7%O2 3.33E-04 2.36E-04 2.78E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.00000000429 0.00000000265 0.00000000324 0.000 Elb/hr 1.59E-10 9.60E-11 1.17E-10 0.000 lb/mmBtuO2 3.93E-13 2.36E-13 3.03E-13 0.000 ng/dscm 4.40E-04 2.59E-04 3.22E-04 0.000 ng/dscm@7%O2 4.56E-04 2.74E-04 3.51E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.00000000278 0.00000000197 0.00000000235 0.000 Elb/hr 1.03E-10 7.13E-11 8.50E-11 0.000 lb/mmBtuO2 2.55E-13 1.76E-13 2.20E-13 0.000 ng/dscm 2.85E-04 1.93E-04 2.34E-04 0.000 ng/dscm@7%O2 2.95E-04 2.04E-04 2.55E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000046 0.00000000322 0.000000004 0.000 Elb/hr 1.71E-10 1.17E-10 1.45E-10 0.000 lb/mmBtuO2 4.21E-13 2.87E-13 3.74E-13 0.000 ng/dscm 4.71E-04 3.15E-04 3.98E-04 0.000 ng/dscm@7%O2 4.88E-04 3.33E-04 4.34E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber 1 2 3 Mass_mg 0.00000000367 0.00000000303 0.00000000355 0.000 Elb/hr 1.36E-10 1.10E-10 1.28E-10 0.000 lb/mmBtuO2 3.36E-13 2.70E-13 3.32E-13 0.000 ng/dscm 3.76E-04 2.96E-04 3.53E-04 0.000 ng/dscm@7%O2 3.90E-04 3.13E-04 3.85E-04 0.000



### Thursday, February 17, 2011 Page 17 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Compound: 1,2,3,7,8-PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000037 0.00000000204 0.00000000283 0.000 Elb/hr 1.37E-10 7.39E-11 1.02E-10 0.000 lb/mmBtuO2 3.39E-13 1.82E-13 2.64E-13 0.000 ng/dscm 3.79E-04 1.99E-04 2.81E-04 0.000 ng/dscm@7%O2 3.93E-04 2.10E-04 3.06E-04 0.000 

### Compound: 1,2,3,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.00000000243 0.00000000185 0.00000000211 0.000 Elb/hr 9.01E-11 6.70E-11 7.63E-11 0.000 lb/mmBtuO2 2.23E-13 1.65E-13 1.97E-13 0.000 ng/dscm 2.49E-04 1.81E-04 2.10E-04 0.000 ng/dscm@7%O2 2.58E-04 1.91E-04 2.29E-04 0.000 

### Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber 1 2 3 Mass_mg 0.00000000239 0.00000000487 0.00000000432 0.000 Elb/hr 8.86E-11 1.76E-10 1.56E-10 0.000 lb/mmBtuO2 2.19E-13 4.34E-13 4.04E-13 0.000 ng/dscm 2.45E-04 4.76E-04 4.29E-04 0.000 ng/dscm@7%O2 2.54E-04 5.03E-04 4.67E-04 0.000 

### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber 1 2 3 Mass_mg 0.0000000531 0.0000000327 0.0000000225 0.000 Elb/hr 1.97E-09 1.18E-09 8.14E-10 0.000 lb/mmBtuO2 4.86E-12 2.91E-12 2.10E-12 0.000 ng/dscm 5.44E-03 3.20E-03 2.24E-03 0.004 ng/dscm@7%O2 5.64E-03 3.38E-03 2.44E-03 0.004 

### Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber 1 2 3 Mass_mg 0.000000187 0.000000126 0.0000000672 0.000 Elb/hr 6.93E-09 4.56E-09 2.43E-09 0.000 lb/mmBtuO2 1.71E-11 1.12E-11 6.28E-12 0.000 ng/dscm 1.92E-02 1.23E-02 6.68E-03 0.013 ng/dscm@7%O2 1.99E-02 1.30E-02 7.28E-03 0.013 

### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber 1 2 3 Mass_mg 0.00000002 0.0000000147 0.00000000812 0.000 Elb/hr 7.41E-10 5.32E-10 2.94E-10 0.000 lb/mmBtuO2 1.83E-12 1.31E-12 7.58E-13 0.000 ng/dscm 2.05E-03 1.44E-03 8.07E-04 0.001 ng/dscm@7%O2 2.12E-03 1.52E-03 8.79E-04 0.002



### Thursday, February 17, 2011 Page 18 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber 1 2 3 Mass_mg 0.0000000125 0.00000000851 0.00000000628 0.000 Elb/hr 4.63E-10 3.08E-10 2.27E-10 0.000 lb/mmBtuO2 1.15E-12 7.58E-13 5.87E-13 0.000 ng/dscm 1.28E-03 8.32E-04 6.24E-04 0.001 ng/dscm@7%O2 1.33E-03 8.79E-04 6.80E-04 0.001 

### Compound: 2,3',4,4',5-PeCB (PCB118) Average RunNumber 1 2 3 Mass_mg 0.000000518 0.000000338 0.000000182 0.000 Elb/hr 1.92E-08 1.22E-08 6.58E-09 0.000 lb/mmBtuO2 4.74E-11 3.01E-11 1.70E-11 0.000 ng/dscm 5.31E-02 3.30E-02 1.81E-02 0.035 ng/dscm@7%O2 5.50E-02 3.49E-02 1.97E-02 0.037 

### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber 1 2 3 Mass_mg 0.00000000976 0.00000000475 0.00000000413 0.000 Elb/hr 3.62E-10 1.72E-10 1.49E-10 0.000 lb/mmBtuO2 8.94E-13 4.23E-13 3.86E-13 0.000 ng/dscm 1.00E-03 4.64E-04 4.11E-04 0.001 ng/dscm@7%O2 1.04E-03 4.90E-04 4.48E-04 0.001 

### Compound: 2,3,4,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.00000000274 0.00000000201 0.00000000229 0.000 Elb/hr 1.02E-10 7.28E-11 8.28E-11 0.000 lb/mmBtuO2 2.51E-13 1.79E-13 2.14E-13 0.000 ng/dscm 2.81E-04 1.96E-04 2.28E-04 0.000 ng/dscm@7%O2 2.91E-04 2.07E-04 2.48E-04 0.000 

### Compound: 2,3,4,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.00000000238 0.00000000175 0.00000000193 0.000 Elb/hr 8.82E-11 6.34E-11 6.98E-11 0.000 lb/mmBtuO2 2.18E-13 1.56E-13 1.80E-13 0.000 ng/dscm 2.44E-04 1.71E-04 1.92E-04 0.000 ng/dscm@7%O2 2.53E-04 1.81E-04 2.09E-04 0.000 

### Compound: 2,3,7,8-TCDD Average RunNumber 1 2 3 Mass_mg 0.00000000347 0.00000000293 0.00000000304 0.000 Elb/hr 1.29E-10 1.06E-10 1.10E-10 0.000 lb/mmBtuO2 3.18E-13 2.61E-13 2.84E-13 0.000 ng/dscm 3.56E-04 2.86E-04 3.02E-04 0.000 ng/dscm@7%O2 3.69E-04 3.02E-04 3.29E-04 0.000



### Thursday, February 17, 2011 Page 19 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Compound: 2,3,7,8-TCDF Average RunNumber 1 2 3 Mass_mg 0.00000000579 0.00000000484 0.00000000152 0.000 Elb/hr 2.15E-10 1.75E-10 5.50E-11 0.000 lb/mmBtuO2 5.30E-13 4.31E-13 1.42E-13 0.000 ng/dscm 5.93E-04 4.73E-04 1.51E-04 0.000 ng/dscm@7%O2 6.15E-04 5.00E-04 1.64E-04 0.000 

### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber 1 2 3 Mass_mg 0.00000000501 0.00000000458 0.00000000662 0.000 Elb/hr 1.86E-10 1.66E-10 2.39E-10 0.000 lb/mmBtuO2 4.59E-13 4.08E-13 6.18E-13 0.000 ng/dscm 5.13E-04 4.48E-04 6.58E-04 0.001 ng/dscm@7%O2 5.32E-04 4.74E-04 7.17E-04 0.001 

### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber 1 2 3 Mass_mg 0.00000000344 0.00000000629 0.00000000396 0.000 Elb/hr 1.28E-10 2.28E-10 1.43E-10 0.000 lb/mmBtuO2 3.15E-13 5.60E-13 3.70E-13 0.000 ng/dscm 3.52E-04 6.15E-04 3.94E-04 0.000 ng/dscm@7%O2 3.65E-04 6.50E-04 4.29E-04 0.000 

### Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber 1 2 3 Mass_mg 0.0000000289 0.0000000323 0.0000000236 0.000 Elb/hr 1.07E-09 1.17E-09 8.54E-10 0.000 lb/mmBtuO2 2.65E-12 2.88E-12 2.20E-12 0.000 ng/dscm 2.96E-03 3.16E-03 2.35E-03 0.003 ng/dscm@7%O2 3.07E-03 3.34E-03 2.56E-03 0.003 

### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber 1 2 3 Mass_mg 0.00000000555 0.00000000807 0.0000000082 0.000 Elb/hr 2.06E-10 2.92E-10 2.97E-10 0.000 lb/mmBtuO2 5.08E-13 7.19E-13 7.66E-13 0.000 ng/dscm 5.69E-04 7.89E-04 8.15E-04 0.001 ng/dscm@7%O2 5.90E-04 8.34E-04 8.88E-04 0.001 

### Compound: OCDD Average RunNumber 1 2 3 Mass_mg 0.0000000141 0.000000017 0.0000000139 0.000 Elb/hr 5.23E-10 6.16E-10 5.03E-10 0.000 lb/mmBtuO2 1.29E-12 1.51E-12 1.30E-12 0.000 ng/dscm 1.44E-03 1.66E-03 1.38E-03 0.001 ng/dscm@7%O2 1.49E-03 1.75E-03 1.50E-03 0.002



### Thursday, February 17, 2011 Page 20 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Compound: OCDF Average RunNumber 1 2 3 Mass_mg 0.00000000867 0.000000113 0.0000000771 0.000 Elb/hr 3.21E-10 4.09E-09 2.79E-09 0.000 lb/mmBtuO2 7.94E-13 1.01E-11 7.20E-12 0.000 ng/dscm 8.88E-04 1.10E-02 7.66E-03 0.007 ng/dscm@7%O2 9.20E-04 1.16E-02 8.34E-03 0.007 

### Compound: Other HpCDD Average RunNumber 1 2 3 Mass_mg 0.00000000552 0.00000000361 0.00000000474 0.000 Elb/hr 2.05E-10 1.31E-10 1.71E-10 0.000 lb/mmBtuO2 5.06E-13 3.22E-13 4.43E-13 0.000 ng/dscm 5.66E-04 3.53E-04 4.71E-04 0.000 ng/dscm@7%O2 5.87E-04 3.73E-04 5.13E-04 0.000 

### Compound: Other HpCDF Average RunNumber 1 2 3 Mass_mg 0.00000000393 0.0000000111 0.0000000129 0.000 Elb/hr 1.46E-10 4.02E-10 4.67E-10 0.000 lb/mmBtuO2 3.60E-13 9.89E-13 1.20E-12 0.000 ng/dscm 4.03E-04 1.08E-03 1.28E-03 0.001 ng/dscm@7%O2 4.18E-04 1.14E-03 1.39E-03 0.001 

### Compound: Other HxCDD Average RunNumber 1 2 3 Mass_mg 0.00000000445 0.00000000279 0.00000000357 0.000 Elb/hr 1.65E-10 1.01E-10 1.29E-10 0.000 lb/mmBtuO2 4.08E-13 2.49E-13 3.33E-13 0.000 ng/dscm 4.56E-04 2.73E-04 3.55E-04 0.000 ng/dscm@7%O2 4.73E-04 2.89E-04 3.87E-04 0.000 

### Compound: Other HxCDF Average RunNumber 1 2 3 Mass_mg 0.00000000304 0.00000000227 0.0000000026 0.000 Elb/hr 1.13E-10 8.22E-11 9.41E-11 0.000 lb/mmBtuO2 2.78E-13 2.02E-13 2.43E-13 0.000 ng/dscm 3.11E-04 2.22E-04 2.58E-04 0.000 ng/dscm@7%O2 3.22E-04 2.35E-04 2.81E-04 0.000 

### Compound: Other PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000037 0.00000000204 0.00000000283 0.000 Elb/hr 1.37E-10 7.39E-11 1.02E-10 0.000 lb/mmBtuO2 3.39E-13 1.82E-13 2.64E-13 0.000 ng/dscm 3.79E-04 1.99E-04 2.81E-04 0.000 ng/dscm@7%O2 3.93E-04 2.10E-04 3.06E-04 0.000



### Thursday, February 17, 2011 Page 21 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Compound: Other PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000373 0.0000000084 0.00000000202 0.000 Elb/hr 1.38E-09 3.04E-10 7.31E-11 0.000 lb/mmBtuO2 3.42E-12 7.48E-13 1.89E-13 0.000 ng/dscm 3.82E-03 8.21E-04 2.01E-04 0.002 ng/dscm@7%O2 3.96E-03 8.68E-04 2.19E-04 0.002 

### Compound: Other TCDD Average RunNumber 1 2 3 Mass_mg 0.00000000533 0.00000000353 0.00000000423 0.000 Elb/hr 1.98E-10 1.28E-10 1.53E-10 0.000 lb/mmBtuO2 4.88E-13 3.15E-13 3.95E-13 0.000 ng/dscm 5.46E-04 3.45E-04 4.21E-04 0.000 ng/dscm@7%O2 5.66E-04 3.65E-04 4.59E-04 0.000 

### Compound: Other TCDF Average RunNumber 1 2 3 Mass_mg 0.0000000201 0.0000000125 0.00000000122 0.000 Elb/hr 7.45E-10 4.53E-10 4.41E-11 0.000 lb/mmBtuO2 1.84E-12 1.11E-12 1.14E-13 0.000 ng/dscm 2.06E-03 1.22E-03 1.21E-04 0.001 ng/dscm@7%O2 2.14E-03 1.29E-03 1.32E-04 0.001 

### Compound: Total Dioxins Average RunNumber 1 2 3 Mass_mg 0.0000000591 0.00000004245 0.00000003527 0.000 Elb/hr 2.19E-09 1.54E-09 1.28E-09 0.000 lb/mmBtuO2 5.41E-12 3.78E-12 3.29E-12 0.000 ng/dscm 6.06E-03 4.15E-03 3.51E-03 0.005 ng/dscm@7%O2 6.28E-03 4.39E-03 3.82E-03 0.005 

### Compound: Total Furans Average RunNumber 1 2 3 Mass_mg 0.000000104 0.00000017435 0.00000012397 0.000 Elb/hr 3.86E-09 6.31E-09 4.48E-09 0.000 lb/mmBtuO2 9.53E-12 1.55E-11 1.16E-11 0.000 ng/dscm 1.07E-02 1.70E-02 1.23E-02 0.013 ng/dscm@7%O2 1.11E-02 1.80E-02 1.34E-02 0.014



### Location: Stack Exit - Method 25A Compound: Total organic compounds (TOC) as Average Run 1 2 3 Elb/hr 3.12E-01 3.17E-01 2.98E-01 0.309 lb/mmBtuO2 7.85E-04 7.84E-04 7.28E-04 0.001 ppm 4.59E-01 4.53E-01 4.19E-01 0.444 ppm@7%O2 4.96E-01 4.95E-01 4.60E-01 0.484



### Thursday, February 17, 2011 Page 22 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010

Location: Stack Exit - Method 26A Compound: Hydrogen Chloride Average RunNumber 1 2 3 Mass_mg 2.82 2.85 2.76 2.810 lb/mmBtuO2 7.40E-04 7.36E-04 7.30E-04 0.001 

### Compound: Hydrogen Fluoride Average RunNumber 1 2 3 Mass_mg 0.368 0.388 0.318 0.358 lb/mmBtuO2 9.66E-05 1.00E-04 8.41E-05 0.000



### Location: Stack Exit - Method 29 Compound: Antimony Average RunNumber 1 2 3 Mass_mg 0.16005 0.16803 0.183 0.170 lb/mmBtuO2 2.90E-05 2.99E-05 3.35E-05 0.000 

### Compound: Arsenic Average RunNumber 1 3 2 Mass_mg 0.0086 0.0087 0.00857 0.009 lb/mmBtuO2 1.56E-06 1.59E-06 1.52E-06 0.000 

### Compound: Barium Average RunNumber 1 3 2 Mass_mg 0.12922 0.15011 0.12807 0.136 lb/mmBtuO2 2.34E-05 2.75E-05 2.28E-05 0.000 

### Compound: Beryllium Average RunNumber 1 3 2 Mass_mg 0.00023 0.000243 0.000224 0.000 lb/mmBtuO2 4.17E-08 4.45E-08 3.98E-08 0.000 

### Compound: Cadmium Average RunNumber 3 1 2 Mass_mg 0.000859 0.00079 0.001009 0.001 lb/mmBtuO2 1.57E-07 1.43E-07 1.79E-07 0.000 

### Compound: Chromium Average RunNumber 1 3 2 Mass_mg 0.01321 0.01271 0.01431 0.013 lb/mmBtuO2 2.39E-06 2.33E-06 2.54E-06 0.000 

### Compound: Cobalt Average


### Thursday, February 17, 2011 Page 23 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
RunNumber 1 3 2 Mass_mg 0.0268 0.02789 0.02664 0.027 lb/mmBtuO2 4.85E-06 5.11E-06 4.74E-06 0.000 

### Compound: Copper Average RunNumber 1 3 2 Mass_mg 0.06393 0.07713 0.06563 0.069 lb/mmBtuO2 1.16E-05 1.41E-05 1.17E-05 0.000 

### Compound: Filterable Particulate Average RunNumber 1 3 2 Mass_mg 89.1 96.6 91 92.233 lb/mmBtuO2 1.61E-02 1.77E-02 1.62E-02 0.017 

### Compound: Lead Average RunNumber 1 2 3 Mass_mg 0.16391 0.16901 0.17061 0.168 lb/mmBtuO2 2.97E-05 3.01E-05 3.13E-05 0.000 

### Compound: Manganese Average RunNumber 1 2 3 Mass_mg 0.16289 0.16488 0.1718 0.167 lb/mmBtuO2 2.95E-05 2.93E-05 3.15E-05 0.000 

### Compound: Nickel Average RunNumber 1 2 3 Mass_mg 0.05119 0.52909 0.52449 0.368 lb/mmBtuO2 9.27E-06 9.41E-05 9.62E-05 0.000 

### Compound: Selenium Average RunNumber 1 2 3 Mass_mg 0.0067 0.0062 0.0071 0.007 lb/mmBtuO2 1.21E-06 1.10E-06 1.30E-06 0.000 

### Compound: Silver Average RunNumber 1 3 2 Mass_mg 0.0007 0.00047 0.001217 0.001 lb/mmBtuO2 1.27E-07 8.62E-08 2.16E-07 0.000 

### Compound: Thallium Average RunNumber 3 1 2 Mass_mg 0.00026 0.00024 0.000249 0.000 lb/mmBtuO2 4.77E-08 4.35E-08 4.43E-08 0.000 

### Compound: Zinc Average


### Thursday, February 17, 2011 Page 24 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
RunNumber 1 3 2 Mass_mg 0.9302 1.0489 0.9573 0.979 lb/mmBtuO2 1.68E-04 1.92E-04 1.70E-04 0.000



### Location: Stack Exit - Method 6C 

### Compound: Sulfur Dioxide Average Run 1 2 3 Elb/hr 3.88E+02 3.99E+02 3.86E+02 391.000 lb/mmBtuO2 9.90E-01 9.94E-01 9.73E-01 0.986 ppm 3.96E+02 3.93E+02 3.81E+02 390.000 ppm@7%O2 4.31E+02 4.33E+02 4.23E+02 429.000



### Location: Stack Exit - Method 7E 

### Compound: Nitrogen oxides (NOx) Average Run 1 2 3 Elb/hr 1.07E+02 1.11E+02 1.10E+02 109.333 lb/mmBtuO2 2.74E-01 2.77E-01 2.76E-01 0.276 ppm 1.53E+02 1.53E+02 1.51E+02 152.333 ppm@7%O2 1.67E+02 1.69E+02 1.68E+02 168.000



### Location: Stack Exit - OTM - 27/28 Compound: Filterable Particulate Average RunNumber 1 2 3 Mass_mg 82.6 49.2 149.2 93.667 lb/mmBtuO2 2.26E-02 1.22E-02 3.66E-02 0.024 

### Compound: Filterable PM2.5 Average RunNumber 1 2 3 Mass_mg 74 40.2 124.8 79.667 lb/mmBtuO2 2.03E-02 1.00E-02 3.06E-02 0.020 

### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber 1 2 3 Mass_mg 31.3 19.6 47.5 32.800 lb/mmBtuO2 8.58E-03 4.87E-03 1.17E-02 0.008 

### Compound: Organic Condensible Particulate Average RunNumber 1 2 3 Mass_mg 32.7 6 3.7 14.133 lb/mmBtuO2 8.96E-03 1.49E-03 9.09E-04 0.004 

### Compound: Total Particulate Average RunNumber 1 2 3 Mass_mg 146.6 74.8 200.4 140.600 lb/mmBtuO2 4.02E-02 1.86E-02 4.92E-02 0.036



### Thursday, February 17, 2011 Page 25 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010

Process Run Data Compound: Total PM2.5 Average RunNumber 1 2 3 Mass_mg 138 65.8 176 126.600 lb/mmBtuO2 3.78E-02 1.64E-02 4.32E-02 0.032



### Thursday, February 17, 2011 Page 26 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Process Run Data

APCD Run Data

Process Lab Run Data 

### Run Name Value UOM Comments Target Value 1 Distillate Oil (No. 1 & 2) Burned 0 1000 Gallons 0


### 1 Average Heat Inpt 0 Million Btu/hr 0
1 Average Steam Output 0 1000 lb steam/hr 0



### Run Name Value UOM Comments Target Value 1 NA 0 0

Run Name Value UOM Comments 

### 1 Ash Content 0 Percent 1 Sulfur Content 0 Percent 1 BTU Content 0 BTU 

### 1 Carbon Content 0 Percent 1 Hyrdrogen Content 0 Precent 1 Nitrogen Content 0 Present



### Thursday, February 17, 2011 Page 27 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010 Sampling / Stack Data Results Detail



### Location Stack Exit - Method 0011 Average Run Number 1 2 3 Test Date 2/27/2010 2/28/2010 2/28/2010 Run Start Time 12:55:00 PM 8:58:00 AM 12:55:00 PM Run Finish Time 3:13:00 PM 11:15:00 AM 3:13:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 120 120 120 Nozzle Diameter, inches 0.223 0.223 0.223 0.223 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.006 1.006 1.006 1.006 Barometric Pressure, inches of Mercury 29.74 29.88 29.88 29.833 Average Orifice Meter Differential, inches H2O 2.01 1.93 2.13 2.023 Dry Gas Meter Volume Sampled, cubic feet 88.114 87.097 92.110 89.107 Average Dry Gas Meter Temperature, °F 74.67 74.75 77.54 75.653 Dry Gas Meter Volume Sampled, dscf 87.443 86.808 91.373 88.541 Total Moisture Liquid collected, g 149.2 126.4 105 126.867 Volume of Water Vapor, standard cubic feet 7.02 5.95 4.94 5.970 Moisture Content of Stack Gas, % 7.43 6.41 5.13 6.323 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9257 0.9359 0.9487 0.937 Carbon Dioxide, % 10.31 10.19 10.09 10.197 Oxygen, % 8.04 8.19 8.24 8.157 Carbon Monoxide & Nitrogen, % 81.65 81.62 81.67 81.647 Fuel Factor 1.25 1.25 1.25 Dry Molecular Weight, lb/lb-Mole 29.97 29.96 29.94 29.957 Wet Molecular weight, lb/lb-Mole 29.08 29.19 29.33 29.200 Flue Gas Static Pressure, inches of H2O 1.1 1.2 1.2 1.167 Absolute Flue Gas Pressure, inches of Mercury 29.82 29.97 29.97 29.920 Average Stack Gas Temperature, °F 332.58 329.33 336.04 332.650 Average Velocity Head, inches of H2O 1.1400944386 824 1.111590864

48537 1.216356144

536 1.156

Average Stack Gas Velocity, feet/second 73.31 71.92 75.37 73.533 Stack Cross-Sectional Area, square feet 38.485 38.485 38.485 38.485 Dry Volumetric Flow Rate, dry scfm 104,043.1 104,141.1 109,696.9 105,960.367 Actual Wet Volumetric Flue Gas Flow Rate, acfm 169,280.1 166,070.5 174,036.9 169,795.833 Percent Isokinetic of Sampling Rate, % 99.4 98.6 98.5 98.833 Percent Excess Air, % 59.5 61.3 61.9 60.900 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Round Duct Diameter, inches 84 84 84 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 10320 10,320.000 Fc 1420 1420 1420 1,420.000



### Thursday, February 17, 2011 Page 28 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 10 Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 29 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 23 Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Thursday, February 17, 2011 Page 30 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 25A Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 31 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 26A Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Thursday, February 17, 2011 Page 32 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 29 Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Thursday, February 17, 2011 Page 33 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 6C Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 34 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - Method 7E Average Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type Fw Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 35 of 36

### Progress Energy Florida Suwannee River Power Plant Unit 2

9/3/2010
Location Stack Exit - OTM - 27/28 Average Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Thursday, February 17, 2011 Page 36 of 36