BOBBY JINDAL 

GOVERNOR 

~tate of JI..ouisiana 

DEPARTMENT OF ENVIRONMENTAL QUALITY 

ENVIRONMENTAL SERVICES 

Certified Mail No.: 7005 1820 0002 2092 4244 

Mr. Charles Cost 

Plant Manager 

Caluniet Lubricants Company, L.P. 

P.O. Box 97 

Cotton Valley, LA 71018 

PEGGY M. HATCH 

SECRETARY. 

Agency Interest No.: 312 

Activity No.: PER20!20002 

RE: Operating permit modification, Calumet Cotton Valley, Calumet Lubricants Company L.P., 

Cotton Valley, Webster Parish, Louisiana 

Dear Mr. Charles Cost: 

This is to inform you that the permit modification for the above referenced facility has been approved under LAC 

33:III.501. The permit is both a state preconstruction and Part 70 Operating Penni!. The submittal was approved on the 

basis of the emissions reported and the approval in no way guarantees the design scheme presented will be capable of 

controlling the emissions as to the types and quantities stated. A new application must be submitted if the reported 

emissions are exceeded after operations begin. The synopsis, data sheets and conditions are attached herewith. 

It will be considered a violation of the permit if all proposed control measures and/or equipment are not installed and 

properly operated and maintained as specified in the application. 

Operation of this facility is hereby authorized under the terms and conditions of this permit. This authorization shall 

expire at midnight on the ~ of January , 2015, unless a timely and complete renewal application has 

been submitted six months prior to expiration. Terms and conditions of this permit shall remain in effect until such 

time as the permitting authority takes final action on the application for permit renewal. The permit number and 

agency interest number cited above should be referenced in future correspondence regarding this facility. 

Please be advised that pursuant to provisions of the Environmental.Quality Act and the Administrative Procedure 

Act, the Department may initiate review of a· permit during its term. However, before it takes any action to 

modify, suspend or revoke a permit, the Department shall, in accordance with applicable statutes and regulations, 

notify the permittee by mail of the facts or operational conduct that warrant the intended action and provide the 

permittee with the opportunity to demonstrate compliance with all lawful requirements for the retention of the 

effective permit. 

Done this__j_2__day o$~ 

PerrnitNo.: 3080-00010-V6 

::J?t~ Sam L. Philhps 

Assistant Secretary 

SLP:fjh 

c: EPA Region VI 

'2012. 

PoSt Office Box 4313 • Baton Roug~. Louisiana 70821-4313 • Phone 225-219-3181 • Fax 225-219-3309 

WW\\'.deq.louislana.gov 
AIR PERMIT BRIEFING SHEET 

PERMITS DIVISION 

LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

I. BACKGROUND 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company,L.P. 

Cotton Valley, Webster Parish, Louisiana 

' 

Calumet Cotton Valley Facility has been in operation prior to 1969. The facility Permit 

No. 3080-00010-VS was issued January 8, 2010. The site is located at 1756 Old Highway 

7 in Cotton Valley, Louisiana. 

II. ORIGIN 

A permit application and Emission Inventory Questionnaire (EIQ) dated July 27, 2012, 

were received requesting a Part 70 Operating Permit Modification. 

III. DESCRIPTION 

Calumet Cotton Valley Facility is a small refinery which uses atmospheric distillation 

and hydrotreating to refine "sweet" local crude oil into various petroleum products, 

including but not limited to aliphatic and hydrotreated low aromatic solvents, light 

straight run, and diesel. The facility is primarily dedicated to manufacturing aliphatic 

solvents. The product range of the aliphatic solvents includes hydrotreating low aromatic 

solvents as well as conventionally refined products. These specialty solvents find 

applications in a wide variety of markets including paints and coating, inks, extraction, 

and mining. 

The proposed modifications of the facility are as follows: 

I. Address and satisfy Condition 62 of the Consent Decree [SA-MM-1 0-0090], 

effective January 31, 2012; 

2. Revise S02 emissions for the heaters that are now subject to 40 CFR 60 Subpart J in 

accordance with the Consent Decree [SA-MM-1 0-0090]; and 

3. Incorporate the case-by-case dated December II, 2012 into the permit; Increase the 

loading throughput of the existing product known as 50 Fuel. 

2 
IV. 

AIR PERMIT BRIEFING SHEET 

PERMITS DIVISION 

LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

Estimated emissions in tons per year are as follows: 

Pollutant Before After 

PM1o 25.98 25.98 

so2 31.43 42.02 

NOx 127.58 127.58 

co 139.07 139.07 

voc. 428.53 428.95 

•voc LAC 33:111 Chapter 51 Toxic Air Pollutants (TAPs): 

Pollutant Before After 

Benzene 6.17 6.17 

Cumene <0.01 <0.01. 

Ethyl benzene 1.23 1.23 

Lead Compounds <0.01 <0.01 

Methyl Isobutyl Ketone <0.01 <0.01 

Naphthalene <0.01 <0.01 

Toluene 5.44 5.44 

Xylene (mixed Isomers) 6.85 6.97 

n-Hexane 4.72 4.72 

Total 24.45 24.57 

TYPE OF REVIEW 

Change 

+I 0.59 

+0.42 

Change 

+0.12 

+0.12 

This application was reviewed for compliance with the Louisiana Part 70 operating 

permit program, Louisiana Air Quality Regulations, NSPS, and NESHAP. Prevention of 

Significant Deterioration does not apply. 

The refinery is a minor source of toxic air pollutants. 

3 
AIR PERMIT BRIEFING SHEET. 

PERMITS DIVISION 

LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

V. Credible Evidence 

Notwithstanding any other provisions of any applicable rule or regulation or requirement 

of this permit that state specific 'methods that may be used to assess compliance with 

applicable requirements, pursuant to 40 CFR Part 70 and EPA's Credible Evidence Rule, 

62 Fed. Reg. 8314 (Feb .. 24, 1997), any credible evidence or information relevant to 

whether a source would have been in compliance with applicable requirements if the 

appropriate performance or compliance test or procedure had been performed shall be 

considered for purposes of Title V compliance certifications. Furthermore, for purposes 

of establishing whether or not a person has violated or is in violation of any emissions 

limitation or standard or permit condition, nothing in this permit shall preclude the use, 

including the exclusive use, by any person of any such credible evidence or information. 

VI. Public Notice 

Public notice is not required for minor modification to a Part 70 operating permit. 

VII. General Condition XVII Activities: 

Activity Frequency 

I 

VOC Emissions 

TPY 

Sample Collection 150/day 2.11 

Tank Gauging/Sampling 45 tanks/month 1.30 

Equipment Startup/Shutdown 200 times/yr 1.46 

Pump Maintenance 400 times/yr 0.29 

Changing Fi hers 200 times/yr 2.92 

Pump Evacuation/Priming 16,425 times/yr 4.80 

Misc. Equipment Maintenance & Preparation 150 times/yr 0.44 

4 
AIR PERMIT BRIEFING SHEET 

PERMITS DIVISION 

LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

IX. Insignificant Activities: 

IDNo.: Description Capacity 

Totes Portable Totes (number varies) <250 gals 

Tank Process Treatment Chemical 1,000 gals 

Tank Process Treatment Chemical 1,000 gals 

Tank Process Treatment Chemical 1,000 gals 

Tank Process Treatment Chemical 1,000 gals 

Tank Process Treatment Chemical 1,350 gals 

Tank Process Treatment Chemical 1,350 gals 

Tank Diesel Storage Tank 1,000 gals 

Tank Diesel Storage Tank 1,000 gals 

Tank Diesel Storage Tank 9,000 gals 

Tank Diesel Storage Tank 500 gals 

Laboratory Equipment NA 

Truck Loading Dock Sump NA 

North Separator 11,340 gals 

Citation 

LAC 33:111.501.8.5.A.2 

LAC 33:111.501.8.5.A.3 

LAC 33:111.501.8.5.A.3 

LAC 33:111.501.B.5.A.3 

LAC 33:111.501.8.5.A.3 

LAC 33:111.501.8.5.A.3 

LAC 33:111.501B.5.A.3 

LAC 33:111.501.B.5.A.3 

LAC 33:111.5018.5.A.3 

LAC 33:111.501B.5.A.3 

LAC 33:111.501.8.5.A.3 

LAC 33:111.5018.5.A.6 

LAC 33:111.5018.5.0 

LAC 33:111.501.8.5.0 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

X. Applicable Louisiana and Federal Air Quality Requirements 

LAC 33:111 Chapter 

IDNo. Description 5 .. 9 II 13 IS 2103 2107 2109 2111 2113 2115 2121 

UNFOOOI Entire Facility I I I I I 3 

EQTOI9 HFR Storage Tank 

EQT020 10 • 500 BBL HFR Storage Tank 3 

IO_QT021 II - 500 BBL HFR Storage Tank 3 

EQT022 14 • 2,000 BBL VFR Storage Tank' 3 

EQT023 15-2,000 BBL VFR Storage Tank 3 

EQT024 16- 2,000 BBL VFR Storage Tank 3 

EQT025 17- 2,000 BBL VFR Storage Tank 3 

EQT026 18- 2,000 BBL VFR Storage Tank 3 

IO_QT027 19 • 2,000 BBL VFR Storage Tank 3 

EQT028 - 500 BBL HFR Storage Tank 3 

EQT029 0- 2,000 BBL VFR Storage Tank 3 

EQT030 I - 2,000 BBL VFR Storage Tank 3 

EQT031 2- 5,000 BBL VFR Storage Tank 3 

EQT032 3 - 5,000 BBL VFR Storage Tank 3 

EQT033 4 • 5,000 BBL VFR Storage Tank 3 

EQT034 5 - 5,000 BBL VFR Storage Tank 3 

EQT035 6- 5,000 BBL VFR Storage Tank 3 

EQT036 7- 5,000 BBL VFR Storage Tank 3, 

EQT037 8- 6,000 BBL VFR Storage Tank 3 

EQT038 9- 50,000 BBL IFR Storage Tank I 

EQT039 • 500 BBL HFR Storage Tank 3 ·-

6 

2147 29* 51* 56 59* 

I I I 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Colton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Colton Valley, Webster Parish, Louisiana 

pc Applicable Louisiana and Federal Air Quality Requirements 

LAC 33:111 Chapter 

ID !'"o. Dcscriplion s• 9 II 13 15 ltOJ 2107 2109 2111 2113 2115 2121 

'QT040 0 • 6.500 BBL VFR Storage Tank 3 

lf:QT041 I • 6,500 BBL VFR Storage Tank 3 

~QT042 2 • 20.000 BBL VfR Storage Tank 3 

~QT043 3 - 20.000 BBL IFR Storage Tank I 

~QT044 4- 10,000 BBL VFR Storage Tank 3 

lf:QT045 5- 10.000 BBL VFR Storage Tank 3 

IEQT046 - 500 BBL HFR Storage Tank 3 

EQT047 7- 80,000 BBL IFR Storage Tank I 

IEOT048 • 500 BBL HFR Storage Tank 3 

~QT049 4 - I 0.000 BBL IFR sw·rage Tank I 

lf:QT050 5- I 0,000 BBL IFR Storage Tank I 

"'QT051 6- 10,000 BBL IFR Storage Tank I 

~QT052 7- 80.000 BflL VFR Storage Tank 3 

IEOT053 8 • 500 BBL llfR Storage Tank 3 

IEOT054 • 500 BilL HfR Storage Tank 3 

fsQT055 0 • 5,000 BBL IFR Storage Tank I 

IEOT056 6 • I 0.000 BBL VFR Storage Tank 3 

f.QT057 7- 10,000 BBL VFR Storage Tank 3 

~QT058 9-700 BBL HFR Storage Tank 3 

);QT059 • 500 BBL HFR Storage Tank 3 

EQT060 I -900 BBL HFR Storage Tank 3 

.QT061 t72- 5.500 BBL VFR Storage Tank 3 ----

7 

2147 29· sJ• S6 59• 

- - --
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

IX· Applicable Louisiana and Federal Air Quality Requirements 

LAC 33:111 Chapter 

IDNo. loescription s'" 9 II 13 IS 2103 2107 2109 2111 2113 

~QT062 ~3 • 5,000 BBL VFR Storage Tank 3 

~QT063 ~6 • 10,000 BBL VFR Storage Tank 3 

~QT064 ~9 • 5,500 BBL VFR Storage Tank 3 

~QT065 8 • 500 BBL HFR Storage Tank , 3 

~QT066 r · 500 BBL HFR Storage Tank 3 

~QT067 ~-1401 ·No. I Boiler I I I 

~QT068 ~-1402 ·No.2 Boiler I I I 

~QT069 ~D ·Blue Drum 

~QT070 ~T- Cooling Tower 

~QT071 FL2 ·Flare - I I I 

~QT072 fp - Emergency Firewater Pumps 

~QT073 pEN- Backup Generator I I I 

~QT074 ~-101- 100 Crude Unit Process Heater I I I 

~QT075 ~-201A- 1100 Crude Unit Process Heater I I I 

~QT076 )i-202 - Hot Oil Process Heater No. I I I I 

~QT077 H-203 -Hot Oil Process Heater No. 2 I I I 

~QT078 H-204- Solvents Unit Heater I I I 

EQT079 H.:.zos - Hydrotreater Heater I I I 

EQT080 H-30 I -No. I Hydrotreater Heater I I I 

EQT081 H-601 -Solvent Train Process Heater I I I 

/'QT082 l"f-602/1 000- Utility Fractionator Process 

~eater I I I 

8 

2115 2121 

3 

3 

3 

3 

3 

3 

3 

3 

3 

3 

3 

2147 29* st• 56 59* 

--
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

~- Applicable Louisiana and Federal Air Quality Requirements 

I.AC JJ:IIJ Chapter 

IDNo. !Description s• 9 II 13 IS 2103 2107 2109 2111 2113 2115 2121 

~QT083 IJ-i-701 -700 Unit Process Heater I I I 3 

~QT084 lfi-90 I -Hydrogen Plant Reformer I I I 3 

FQT085 f.-0 - Loading Operations I I 

f'QT086 ~~~-Air Dryer (OOS) I I I 3 

EQT087 fww- Wastewater Emissions · 2 

)'UG002 tFE ·Fugitive Emissions I I 

FUGOOJ rt-JR- Unpaved Road Emissions 

£QT088 I A -Pressurized Storage Tank I 

EQT089 ~7 -Pressurized Storage Tank I 

EQT090 ~8 -Pressurized Storage Tank I 

EQT091 ~9 -Pressurized Storage Tank I 

FQT092 ~0 -Pressuri7...cd Storage Tank I 

"'QT093 ~I -Pressurized Storage Tank I 

~QT094 ~4 -Pressurized Storage Tank I 

~QT095 ~6 -Pressuril..Cd Stora.ge Tank I 

EQT096 170 -Pressurized Storage Tank I 

EQT097 12 -Pressurized Storage Tank I 

.QT098 2 -Pressurized Storage Tank I 

~QT099 43 -Pressuri7.cd Storage Tank I 

-QTtOO 5 -Pressuri7.ed Storage Tank I 

EQTIOI 9 -Pressurized Storage Tank I 

EQTJ02 62 -Pressurized Storage Tank I 

9 

2147 29· SJ• 56 59• 
LOillSIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana · 

IX· Applicable Louisiana and Federal Air Quality Requirements 

LAC 33:III Chapter 

IDNo. Descriotion s• 9 II 13 15 2103 2107 2109 2111 2113 

EQT103 3 -Pressurized Storage Tank I 

cQTI04 4 -Pressurized Storage Tank I. 

EQTIOS 5 -Pressurized Storage Tank I 

1:.QTI06 8 -Pressurized Storage Tank I 

~;,QTI07 OPE- Dual Phase Extraction System 

EQT108 OPE OWS Dual Phase Extraction System 2 Oil/Water Separator 

• The regulations indicated aboye are State Only regulations. 

2115 2121 2147 29* 51* 56 59* 

• All I.;AC 33:III Chapter 5 citations are federally enforceable including LAC 33:111.50l.C.6 citations, except when the requirement found in the "Specific Requireme~t~" 

report specifically states that the regulation is State Only. 

KEY TO MATRIX 

-The regulations have applicable requirements which apply to this particular emission source. 

-The emission source·may have an exemptiOn from control stated in the regulation. The emission source rimy not have to be coiltrolled but may have monitoring, 

recordkeeping, or reporting requirements. ' , 

2 -The regulations have applicable requirements which apply to this particular emission source but the source is currently exempt from these requirements due to 

meeting a specific criteria, such as it has not been constructed, modified or reconstructed since the regulations have been in place. If the specific criteria changes 

the source will have to comply at a future date. 

3 -The regulations apply to this general type of emission source (i.e. vents, furnaces, towers, and fugitives) but do not apply to thiS particular emission source. 

Blank- The regulations clearly do not app!Y_!Q_1t_lis type of emission source. 

10 
-------------------.------------------

LOUISIANA DEPARTMEJ\'T OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

X. Applicable Louisiana and Federal Air Quality Requirements 

:'iSPS 40 CFR 60 

1D No. Description A ll lla llb llc K Ka Kb J GGG 

UNFOOOI :ntire Facility I I 

EQT019 HFR Storage Tank 

IEQT020 10- 500 flBL HFR Storage Tank 3 3 3 

IEQT021 II - 500 BBL HFR Storage Tank 3 3 3 

!EOT022 14- 2,000 BBL VFR Storage Tank 3 3 3 

IEQT023 15 - 2,000 BBL VFR Storage Tank 3 3 3 

'QT024 16-2.000 BilL VFR Storage Tank 3 3 3 

IEQT025 17- 2,000 BBL VFR Storage Tank 3 J 3 

"'QT026 18- 2,000 BBL VFR Storage Tank 3 3 3 

i"QT027 19- 2,000 BBL VFR Storage Tank 3 3 3 

IEQT028 ~- 500 BBL HFR Storage Tank 3 3 3 

IEQT029 ~0- 2,000 BBL VFR Storage Tank 3 3 3 

IEQT030 ~I - 2,000 BBL VFR Storage Tank 3 3 3 

IEQT031 ~2- 5,000 BBL VFR Storage Tank 3 3 3 

IEQT032 123 - 5,000 BRL VFR Storage Tank 3 3 3 

lr,QT033 124- 5,000 BBL VFR Storage Tank 3 3 3 

i"QT034 ~5 - 5,000 BBL VFR Storage Tank 3 3 3 

IEQT035 ~6- 5.000 BRL VFR Storage Tank 3 3 3 

IEQT036 ~7- 5,000 BRL VFR Storage Tank 3 3 3 

"'QT037 128 ~ 6,000 BBL VFR Storage Tank 3 I 

11 

/ 

St:SHAP 

40CFR61 

000 A ~t FF 

I I I 

. 

St:SHAP 40 40 40 CFR 63 

i"GG O'R CFR 

A cc 0 lc;c; 64 82 

2 3 

I 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

~- Applicable Louisiana and Federal Air Quality Requirements 

NSPS 40 CFR 60 

IDNo. lnescription A D Da Db De K Ka Kb J GGG 

!EQT038 ~9- 50,000 BBL IFR Storage Tank I 

!EOT039 p - 500 BBL HFR Storage Tank 3 3 '3 

!EQT040 ~0- 6,500 BBL VFR Storage Tank 3 I 

IEQT041 ~I - 6,500 BBL VFR Storage Tank 3 3 3 

!EQT042 ~2- 20,000 BBL VFR Storage Tank t 

IEQT043 ~3 - 20,000 BBL IFR Storage Tank t 

IEQT044 ~4- 10,000 BBL VFR Storage Tank 3 3 3 

!EOT045 p5- 10,000 BBL VFR Storage Tank 3 3 3 

IEQT046 ~- 500 BBL HFR Storage Tank 3 3 3 

IEQT047 ~7- 80,000 BBL IFR Storage Tank t 

!EQT048 ~ - 500 BBL HFR Storage Tank 3 3 3 

!J'QT049 ~4- 10,000 BBL IFR Storage Tank I 

IEQT050 ~5- 10,000 BBL IFR Storage Tank I 

EQT051 ~6- I 0,000 BBL IFR Storage T-ank I 

[EQT052 ~7- 80,000 BBL VFR Storage Tank 3 3 3 

!EQT053 ~8- 500 BBL HFR Storage Tank 3 3 3 

IEQT054 ~- 500 BBL HFR Storage Tank 3 3 3 

IEQT055 ~0- 5,000 BBL IFR Storage Tank I 

[EQT056 ~6- 10,000 BBL VFR Storage Tank 3 I 

[EQT057 . ~7- 10,000 BBL \fF~Storage Tank ~3 I ----

12 

NESHAP 

40 CFR 61 

looo A M FF 

-

NESHAP 

40 CFR63 

~GG 

A cc 0 k;G 

40 40 

CFR CFR 

64 82 

. 
•· 

LOUISIAl"JA DEPART;\1ENT OF ENVIRONI\1ENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parisb, Louisiana 

X. Applicable Louisiana and Federal Air Quality Requirements 

NESIIAP 

:-;sps 40 CFR 60 40 CFR 61 

ID No. Description A ll Da Db De K Ka Kb J CGG looo A ~I FF 

EQT058 69 • 700 BBL HFR Storage Tank 3 3 3 

'QT059 • 500 BBL HFR Storage Tank 3 3 3 

.QT060 71 • 900 BBL HFR Storage Tank 3 3 3 

.QT061 172 • 5,500 BBl. VFR Storage Tank 3 I 

cQT062 ~3 • 5,000 BilL Vf'R Storage Tank 3 I 

iQT063 76 • 10,000 IIBL VFR Storage Tank 3 I 

~QT064 79 • 5,500 BBL VFR Storage Tank 3 I 

EQT065 8 • 500 BBL HFR Storage Tank 3 3 3 

'QT066 9 • 500 BilL HFR Storage Tank 3 3 3 

cQT067 1!-1401 ·No. I Boiler 3 3 3 3 I 

'0T068 B-1402. No.2 Boiler 3 3 3 3 I 

EQT069 RD -Blue Drum 3 I 

£QT070 CT- Cooling Tower 

oQT07I FL2- Flare I 

·QT072 FP- Emergency Firewater Pumps 

EQT073 GEN- Backup Generator 

·QT074 1·10 I • I 00 Crude Unit Process Heater 3 3 3 3 I 

iQT075 H-201A- 1100 Crude L:nit Process Heater I 

'QT076 H-202- Hot Oil Process Heater ~o. 1 3 3 I 3 3 I 

EQT077 H-203 -Hot Oil Process Heater No.2 I I I 

13 

NESIIAP 40 40 400"R63 

GGG CFR CFR 

A cc Q GG 64 82 

3 

2 
LOillSIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

IX· Applicable Louisiana and Federal Air Quality Requirements 

NSPS 40 CFR 60 

ID No. Description A D Da Db De K Ka Kb J GGG 

EQT078 IH-204 - Solvents Unit Heater 3 3 3 3 . I 

EQT079 IH-205 - Hydrotreater Heater 3 3 3 3 I 

EQT080 IJ-I-301- No. 1 Hydrotreater Heater 3 3 3 3 I 

loQTOSI H-60 I -Solvent Train Process Heater I 

EQT082 H-602/1000- Utility Fractionator Process 3 3 3 3 I Heater- -

EQT083 H-701 -700 Unil Process Heater 3 3 3 3 I 

EQT084 H-90 I -Hydrogen Plant Reformer 3 3 3 3 I 

EQT085 LO - Loading Operations 

EQT086 H-Air Dryer (OOS) 3 3 3 3 3 

EQT087 WW- Wastewater Emissions · 

FUG002 E - Fugitive Emissions I 

FUG003 UR- Unpaved Road Emissions 

~QT088 lA -Pressurized Storage Tank 

EQT089 7 -Pressurized Storage Tank 

EQT090 8 -Pressurized Storage Tank . 

EQT091 9 -Pressurized Storage Tank 

EQT092 0 -Pressurized Storage Tank 

IoQT093 1 -Pressurized Storage Tank 

EQT094 4 -Pressurized Storage Tank 

14 

NESHAP 

40 CFR 61 

IQQQ A M FF 

3 I 

NESHAP 40 40 40 CFR63 

Q ~gG CFR CFR 

A cc 64 82 

. 

. 

2 2 I 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

pc Applicable Louisiana and Federal Air Quality Requirements 

~SPS 40 CFR 60 

ID No. Dtscription ·A D Da Db De K Ka Kb J GGG 

IEQT095 6 -Pressurized Storage Tank 

~QT096 0 -Pressurized Storage Tank 

IEQT097 12 -Pressurized Storage Tank 

IEOT098 2 -Pressurized Storage Tank 

I"QT099 ~3 -Pressurized StoragC Tank 

lr.QTIOO ~5 -Pressurized Storage Tank · 

ii;QTIOI ~9 -Pressurized Stomge Tank 

~QTI02 ~2 -Pressurized Storage Tank 

lEOTI OJ p3 -Pressurized Storage Tank 

~QT104 ts4 -Pressurized Storage Tank 

i"QT105 ~5 -Pressurized Storage Tank 

!EOTI06 ~8 -Pressurized Storage Tank 

IEOT 107 loPE - Dual Phase Extraction System 

IEOT 108 fDPE OWS- Dual Phase Extraction System 

Oil/Water Separator 

15 

NESIIAP 

40 CFR 61 

QQQ A M FF 

3 I 

NESHAP 40 40 40 CFR 63 

.GG CFR CFR 

A cc Q lr;c; 64 82 

I 

3 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

KEY TO MATRIX 

Calumet Cotton Valley 

Agency Interest No,: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

-The regulations have applicable requirements which apply to this particular emission source. 

-The emission source may have an exemption from control stated in the regulation. The emission source may not have to be controlled but may have monitoring, 

recordkeeping, or reporting requirements. 

2 -The regulations have applicable requirements which apply to this particular emission source but the source is currently exempt from these requirements due to 

meeting a specific criteria, such as it has not been constructed, modified or reconstructed since the regulations have been in place. If the specific criteria changes the 

source wi II have to comply at a future date. 

3 -The reg~Jations apply to this general type of emission source (i.e. vents, furnaces, towers. and fugitives) but do not appl)t to this particular emission source. 

Blank- The ~ulations clearly do not apply to this type of emission source. 

16 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

XI. Explanation for Exemption Status or Non-Applicability of a Source 

DNo: Requirement Notes 

ftnlire Facility Lontrol of Emissions of Carbon Monoxide· DOES NOT APPLY. Does not have catalyst regeneration 

~FOOOI ,etroleum Refinery Emissions 

LAC 33:111.1705] 

jWaste Gas Disposal .OXEMPT. VOC in the waste gas less than 30,000 ppm. 

LAC 33:111.2115] 

r'ESIIAP, Subpart CC- NESIIAPs for 

~efincrics 

DOES NOT APPLY. Not a major source of HAPs. 

40 CFR 63.640] 

EQT028. EQT039, EQT046, EQT048, EQT054, EQT059, ~to rage of Volatile Organic Compounds lOES NOT APPLY. Vapor Pressure <1.5 psia. 

oQT065. EQT066. EQT020, EQT021, EQT053, EQT058, LAC 33:111.2103] 

jEQT060 

FR Storage Tanks) r-:sPS Subpart K, Ka, Kb li>r Storage Tanks ilJOES l'OT APPL. Y. All tanks except 58, 69, 70, 71 were 

40CFR60.110, I lOa, I lOb] ·onstructed prior to 1973; Tanks 58, 69, 70, and 71- vapor 

~ressure <I SkPa. 

EQT022. EQT023, EQT024, EQT025, EQT026, EQT027, ~to rage of Volatile Organic Compounds poES NOT APPLY. Vapor Pressure <1.5 pSia. 

1'QT029. EQT030, EQT031, EQT032, EQT033, EQT034, I.AC 33:111.2103] 

EQTOJS. EQT036, EQT041' EQT044, EQT045, EQT052 P'SPS Subpart K. Ka, Kb for Storage Tanks !DOES :-<OT APPLY. Constructed prior <o 1973. 

(FR S<orage Tanks) 40CFR60.110, I lOa, !lOb] 

17 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 · 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

~1. Explanation for Exemption Status or Non-Applicability of a Source 

liD No: Requirement Notes 

fEQT037, EQT040, EQT042, EQT056, EQT057.EQT061, 

poQT062, EQT063, EQT064 

~torage of Volatile Organic Compounds DOES NOT APPLY. Vapor Pressure <1.5 psia. 

[LAC 33:IIl.2103] 

FR Storage Tanks) NSPS Subpart K for Storage Tanks DOES NOT APPLY. Constructed prior to 1973. 

[40CFR60.110, I lOa, I lOb] 

fEQT067, EQT068 NSPS Subpart D for Boilers DOES NOT APPLY. Maximum heat input rate <250 MM 

Boilers) 40 CFR 60.40] BTU/hr. 

"SPS Subpart Da for Boilers DOES NOT APPLY. Not Electric Utility Steam Generating 

40 CFR 60.40a] Units. 

~SPS Subpart Db for Boilers DOES NOT APPLY. Maximum heat input rate <100 MM 

40 CFR 60.40b] BTU/hr. 

~SPS Subpart De for Boilers DOES NOT APPLY. Constructed prior to 1989. 

40 CFR 60.40c] 

lWaste Gas Disposal pOES NOT APPLY. Do not bum a waste gas stream 

[LAC 33:IIl.2115] ~ontaining VOCs. 

EQT074, EQT075, EQT076, EQT077, EQT078, · 1'/SPS Subpart D, Da, Db, De for Boilers pOES NOT APPLY. Constructed prior to applicable dates, 

EQT081 EQT086 [40 CFR 60.40,40a,40b, 40c] ~nd/or 

Heaters, Air Dryer) <100 MM BTU/hr, 3nd are not steam generating units 

"SPS Subpart J Standards of Performance for 

!Petroleum Refineries 

pOES NOT APPLY. Constructed prior to 1973 or do not burn 

~el gas. 

40 CFR 60. 100] 

jWaste Gas Disposal poES NOT APPLY. Do not bum a waste gas stream 

[LAC 33:1ll.2115] ontaining VOCs. 

18 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

!XI. Explanation for Exemption Status or Non-Applicability of a Source 

DNo: Requirement Notes 

EQT079, EQT080. EQT083 

NSPS Subpart D. Da. Db. De for Boilers !DOES NOT APPLY. These are no steam generating units. 

Heaters) 

40 CFR 60.40, 40a. 40b, 40c] 

Waste Gas Disposal pOES l'OT APPLY. Do not bum a waste gas stream 

LAC 33:111.2115] Fontaining VOCs. 

cQT084 NSPS Subpart D, Da, Db, De lor Boilers poES NOT APPLY. These are not steam generating units. 

Hydrogen Reformer) 40 CFR 60.40, 40a, 40b, 40c] 

Waste Gas Disposal poES NOT APPLY. Does not bum a waste gas stream 

LAC 33:111.2115] ontaining VOCs. 

~tandards of Performance for Petroleum ~XEMPT. Fuel gas stream is inherently low in sulfur content 

Refineries 

40 CFR 60. 105(a)(4)(iv)(C)] 

~QT070 NESHAP, Subpart Q- Chromium emissions poES NOT APPLY. Facility is not a major source of HAPs 

Cooling Tower) rom Industrial Process Cooling Towers pnd 

40 CFR 63.402] hromium-based treatment chemicals are not used. 

t:QT069 NSPS, Subpart • QQQ VOC Standards for )QES NOT APPLY. Facility was not constructed, 

Blue Drum) Petroleum Refinery Wastewater Syst~ms econstructed. or modified after May 4, 1987. 

40 CFR 60.690] 

NESHAP, Subpart FF- Benzene Waste !Shall comply with the requirements of 40 CFR 61.343. 

Opera~ions 

40 CFR 61.340] 

19 

I 
~-------------------------------------------------------------------------------------------------------------------------------------------------------------------------------~ ----~ 

LOUISIANA DEPARTMENT OF ENVffiONMENT AL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

~1. Explanation for Exemption Status or Non-Applicability of a Source 

DNo: !Requirement Notes 

~QT087 ~SPS, Subpart - QQQ VOC Standards for pOES NOT APPLY. Facility was not constructed, 

Wastewater Emissions) !Petroleum Refinery Wastewater Systerns econstructed. or modified after May 4, 1987. 

40 CFR 60.690] 

pii!Water ·Separation fEXEMPT. Emits <100 tons per year regulated hydrocarbons. 

LAC 33:111.2109] 

~QT071 r-ompliance Assurance Monitoring ~XEMPT. Subject to NSPS Subpart A. 

Flare) 40 CFR 64] 

!Waste Gas Disposal poES NOT APPLY. This regulation is not applicable to 

LAC 33:111.2115] jwaste gas stfeams which must comply with a control device 

equirement as stated in LAC 33:111.2115. 

~QT107 !National Emissions Standards for Hazardous facility is not a major source of HAP's. 

loPE- Dual Phase Extraction System ~ir Pollutants: Site Remediation- Subpart 

jGGGGG · 

40CFR6U . 

jEQTJ08 . ' ~tandards for Petroleum Refinery Wastewater his equipment does not come·in contact with or store oily 

joPE OWS- Dual Phase Extraction System- Oil/Water ~ystems- Subpart QQQ vastewater. 

Separator [40 CFR 60.690] 

' 

pii/Water Separation 

jrLAC 33:111.2109] 

jEXEMT. Emits <lOO tons per year regulated hydrogen 

Farbons. 

---- -----------~ -

20 
LOUISIANA DEPARTMENT OF ENVIRONMENTAL QUALITY 

Calumet Cotton Valley 

Agency Interest No.: 312 

Calumet Lubricants Company, L.P. 

Cotton Valley, Webster Parish, Louisiana 

jx:I. Explanation for Exemption Status or Non-Applicability of a Source 

ID No: !Requirement Notes 

EQT082/ll60211 000 NSPS Subpart D. Da. Db. De for Boilers )QES NOT APPLY. These arc no steam generating units. 

F ractionator Process Heater) 40 CFR 60.40. 40a. 40b. 40c) 

[Waste Gas Disposal )OES NOT APPLY. Do not bum a waste gas stream 

LAC 33:111.2115) ontain.ing VOCs. 

~SPS Subpart J Standards of Performance for pOES NOT APPLY. Heater converted from ercfinery fuel gas 

Petroleum Refineries o natural gas. 

40 CFR 60.1 00) 

21 
Also Known As: ID 

2211900010 

3080-00010 

7205811 

73-0974954 

LAD000225805 

LAD000225805 

LA0005312 

WP0400 

General Information 

AJID: 312 Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VG 

Air- Title V Regular Permit Minor Mod 

Name User GroUp 

AFS (EPA Air Facility Syslem) AFS (EPA Air Facility Syslem) 

CDS Number COS Number 

EPA EIS Facility Site ID EPA EIS Facility Site 10 

Kerr McGee Refining Corp Federal Tax 10 

Calumet Cotton Valley. Hazardous Waste Notification 

Site 10 # Inactive & Abandoned Sites 

LPDES Permit # LPDES Permit # 

WPC State Permit Number LWDPS Permit# · 

Priority 1 Emergency Site . Priority 1 Emergency Site 

Start Date 

01-01-2000 

08-05-2002 

01-01-2008 

11-21-1999 

04-11-2000 

06-09-1981 

05-22-2003 

06-25-2003 

07-18-2006 

7295 X-Ray Registration Number Radiation X-ray Registration Number 11-21-1999 

1000005936 Cotton Valley Refinery Risk Management Plan EPA ID 

GD-119-1791 Solid Waste Facility No. Solid Waste Facility No. 

P-0196 Standard Permit Solid Waste Permitting 

36528 Kerr McGee Refining Corp TEMPO Merge 

47229 Kerr McGee Corp Cotton Valley Ref TEMPO Merge 

71018KRRMCLA7SO TRI# Toxic Release Inventory 

Physical Location: 1756 Old Hwy 7 

Cotton Valley. LA 71018 

Mailing Address: PO Box 97 

Cotton Valley, LA 710180097 

Location of Front Gate: 32.7972671atitude, -93.4146891ongitude, Coordinate Method: l,.at.\Long.- OMS, Coordinate Datum: NA083 

Related People: Name 

Larry Allen· 

Charles Cost 

Charles Cost 

Fred Holt 

Fritz Howes 

Jeff Lang 

R Murray 

Lynn Shearer . 

Meridith Sheets 

K~p Southerland 

· Mailing Address 

PO Box 97 Cotton Valley, LA 710180097 

PO Box 97 Cotton Valley, LA 710180097 

PO Box 3099 Shreveport, LA 71 ~333099 

2780 Waterfront Pkwy E Sle 200 lndianaplois, IN 46214 

PO Box 97 Cotton Valley, LA 71018 

PO Box 97 Cotton Valley, LA 710180097 

Page 1 of 2 

Phone (Type) 

3188324236 (WP) 

3188324236 (WP) 

charles.cost@calurn 

3188324236 (WP) 

3186324103 (WP) 

3188324236 (WP) 

3188324236 (WP) 

3188324236 (WP) 

01-01-2001 

08-21-2001 

03-01-1989 

06-09-2002 

10-02-2001 

07-09-2004 

Main Phone: 3188324236 

Relationship 

Employed by 

Responsible Official for 

Responsible Official for 

Employed by 

Accident Prevention Billing Party for 

Accident Prevention Contact for 

Water Billing Party for 

Radiation·contact For 

Employed by 

Emission Inventory Facility Contact for 

TPOR0148 
Rel~ted People: Name 

Kep Southertand 

General Information 

AIID: 312 Calumet Lubricants Co. Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080..00010-V& 

Air· Title V Regular Permit Minor Mod 

Mailing Address Phone (Type) 

PO Box 97 Cotton Valley, LA 710180097 kep.souther1and@ca 

Relationship 

Ennsion Inventory FaC:ility Contact for 

Related Organlutlona: Name Addresa Phone (Type) Relationship 

NAJC Codu: 

Calumet Lubricants Co 

Calumet Lubricants Co 

Calumet lubricants Co LP 

G.llumet Lubricants Co LP 

Calumet Lubricants Co LP 

Calumet lubricants Co LP 

Calumet Lubricants Co LP 

Calumet Lubricants Co LP 

Kerr-McGee Refining Corp 

32411, Petroleum Refineries 

324110, Petroleum R8finerles 

PO Box 97 Cotton Valley, LA 710180097 

PO Box 97 Cotton Valley. LA 710180097 

2780 Waterfront Pkwy Ste 200 lnd•anapolis, IN 46214 

2780 Waterfront Pk'Ny Ste 200 Indianapolis, IN 46214 

2780 Waterfront Pkwy Ste 200 Indianapolis. IN 46214 

2780 Waterfront Pkwy Sle 200 Indianapolis. IN 48214 

2780 Waterfront Pkvly Ste 200 Indianapolis. IN 46214 

2780 Waterfront Pkvly Ste 200 Indianapolis. IN 46214 

PO Box 25861 Oklahoma C•ty. OK 73125 

3188324236 (WP) 

3188324236 (WP) 

kep.southertand@ca 

3188324236 (WP) 

kep.southertand@CG 

3188324236 (WP) 

kep.souther1and@c:G 

3188324236 (WP) 

4052702071 (WP) 

Air Billing Party for 

Radiation Registration Billing Party for 

Sohd Waste Billing Party for 

Sol•d Waste Billing Party for 

Ef'nlssion Inventory Billing Party 

Owns 

Owns 

Emission Inventory B•lling Party 

Agent of Service for 

Note: This report entJUed "General Information" contains a summary of facility-level Information contained In LDEQ'a TEMPO database for this facility and Is not considered a part of the permit. 

Please review the Information contained In this document for accuracy and completeness. If any changes are required or if you have questions re93rding this document, you may email your 

ch•nges to facupdate@la.gov. 

Page 2 of 2 TPOR01"4 
Subject Item Inventory: 

10 Description 

Entire Facility 

EQT 0019 HFR- HFR Storage Tank 

EQT 0020 10 - 500 BBL HFR Storage Tank 

EQT 0021 11 - 500 BBL HFR Storage Tank 

EQT 0022 14- 2,000 BBL VFR Storage Tank 

EQT 0023 15-2,000 BBL VFR Storage Tank 

EQT 0024 16-2,000 BBL VFR Storage Tank 

EQT 0025 17- 2,000 BBL VFR Storage Tank 

EQT 0026 18-2,000 BBL VFR Storage Tank -- EQT 0027 19-2,000 BBL VFR Storage Tank 

EQT 0028 2- 500 BBL HFR Storage Tank 

EQT 0029 20-2.000 BBL VFR Storage Tank 

EQT 0030 21 -2,000 BBL VFR Storage Tank 

EQT 0031 22-5,000 BBL VFR Storage Tank 

EQT 0032 23 - 5,000 BBL VFR Storage Tank - EQT 0033 24-5,000 BBL VFR Storage Tank 

EOT 0034 25 - 5,000 BBL VFR Storage Tank 

EQT 0035 26 - 5,000 BBL VFR Storage Tank 

EQT 0036 27 - 5,000 BBL VFR Storage Tank 

EQT 0037 28 - 6,000 BBL VFR Storage Tank 

EQT 0038 29- 50,000 BBL IFR Storage Tank 

EaT 0039 3- 500 BBL HFR Storage Tank 

EQT 0040 30- 6,500 BBL VFR Storage Tank 

EQT0041 31 -6,500 BBL VFR Storage Tank 

EQT 0042 32-20.000 BBL VFR Storage Tank 

EQT 0043 33 - 20,000 BBL IFR Storage Tank 

EQT 0044 34- 10,000 BBL VFR Storage Tank 

EQT 0045 35- 10,000 BBL VFR Storage Tank 

EQT 0046 4 - 500 BBL HFR Storage Tank 

EQT 0047 47- 80,000 BBL IFR Storage Tank 

EQT0048 5- 500 BBL HFR Storage Tank 

EQT0049 54- 10,000 BBL IFR Storage Tank 

EQT 0050 55- 10,000 BBL IFR Storage )"ank 

EQT 0051 56- 10,000 BBL IFR Storage Tank 

EQT 0052 57-80,000 BBL VFR Storage Tank 

EQT 0053 58-500 BBL HFR Slorage Tank 

EQT 0054 6- 500 BBL HFR Storage Tank 

EQT 0055 60 - 5,000 BBL IFR Storage Tank 

EOT 0056 [66- 10,000 BBL VFR Storage Tank 

EQT 0057 167- 10,000 BBL VFR Storage Tank 

INVENTORIES 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air. Title V Regular Permit Minor Mod 

Tank Volume Max. Operating Rate Nonnal Operating Rate 

21000 gallons 

21000 gallons 

84000 gallons 

84000 gallons 

84000 gallons 

84000 gallons 

_J 84000 gallons 

I 84000 gallons 

21000 gallons I 

84000 gallons r--

84000 gallons 

I 210000 ga11ons L_ 

~=-----~ 210000 gallons 

210000 ga11ons 

--·------ 210000 gallons 

210000 ga11ons 

'210000 gallons 

252000 gallons ---- 50000 bbl 

21000 gallons 

273000 ga11ons 

273000 ga11ons 

1 840000 ga11ons 

840000 gallons 40000 bbl/yr 40000 bbl/yr - 420000 ga11ons 

420000 ga11ons - 21000 gallons 

80000 bbl 

., 21000 gallons 

420000 gallons 

420000 ga11ons 

420000 ga11ons 

80000 bbl 

21000 ga11ons 

T2'fooo ga11ons 

I [ 210000 gallons 

420000 gallons 

_______ _j_ 420000 gallons 

Page 1 of a 

Contents 

I 

Operating Time -~ 

8760 hrlyr 1 

8760 hrlyr 

8760 hrlyr ~ 8760 hrlyr I 

8760 hrlyr =.=] 

8760 hrlyr 1 

8760 hrlyr 1 

8760 hrlyr j 

8760 hrlyr i 8760 hrlyr _J 

I 8760 hrlyr i 

8760 hrlyr 1 

8760 hrlyr 

j -· 8760 hrlyr 

8760 hr/yr -· 8760 hr/yr ~ - - 8760 hrlyr i 

8760 hrlyr I --- 8760 hrlyr 1 --- 8760 hrlyr 

8760 hrlyr --j 

8760 hr/yr 1 

8760 hr/yr _____ j ---- 8760 hrlyr __ 

1 

8760 hr/yr 

8760 hr/yr , 

8760 hrlyr I 

8760 hrlyr I 

I --- 8760 hrlyr 

8760 hrlyr 

8760 hrlyr 

8760 hrlyr 

8760 hrlyr 

8760 hrlyr 

~-- 8760 hr/yr --

8760 hrlyr 

8760 hrlyr 

8760 hrlyr 

8760 hrlyr _j 

TPOR0149 
Subject Item Inventory: 

.10 -·· DB&ciiPilon 

INVENTORIES 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air· Title V Regular Permit Minor Mod 

1 Tank V01lime · M~::~~~-~~tihg Rate I Normal Operating Ra~e r Contents ___ Lperatlng nme "1 

-------j 294oO gall?~'--:_ -. ---- .. )- -~ _ 876oi>,;y;--~~ 

tHE; :9~:~: l=-= ----- ---~-~-:- ~-t_--_];~6 

1 Entire Facility 

lEar 0058 69 · 700 BBL HFR Storage Tank - ---

f"EOT 0059 7- 500 BBL HFR Storage Tank ··-- ;·Ear·aoso 71 -900 BBL HFR Storage Tank 

IEar·oasT 72- 5,500 BBL VFR Storage Tank -· ·-

----- 210000 gallons : 1 8760 hrfyr i 

420000 gallons r-·--·· -·-. ·-· ·-·-·· --------------1 --8760hr;yf"' i 

223111 gallons ·r-··---- --·- ···- ····· ·· ·· ---- -------· ----·-- 8760 hrlyr - --, 

l

21DOO_gallons ! -__ -_ --- ~=~----- 1 ·a_?GOhiiyi ~ 

- ~-~=a~l:~~ -~~~ _3~:48 MMBTtlhir--f-3:t48MM BTUfllr ·-- -----~----.-~==·JJ :;: ~;~; -l 

i 16.74 MM BTU/hr 16.74 MM BTU/hr 8760 t-·"-

1 EOT 0069 lBO - Blue Drum _ . l 30 gallons/min 30 gallons/min 1 B!_6E_! 

J EOT 0070 ICT- Cooling Tower ··-· _ _ I __ _; ___ 1500 gallonslmm __ l 1500 gallons/min -·--·- .. _ ···-·· J_ __ 8760 hrtyr ·I [EO~ 0071 .FL2- Flare _ __ -·· I 15.9 MM ft"3ty~ ---=r------r5.9 MM ft"3tyr ___ .. _________ L __ 8_760 ~r!fr __ _ 

l E~! -~~?3__!FP · Emergen~ Fir~t.I!~-~~!'"Ps ......... _ _ :... __ 5_:3_5_ -~~~~power 1 535 horsepower 

1 

____________ ... ____ !._ __ --~2 hrlyr 1 

1 EOT 0073 IGEN - Backup Generator · 241 horsepower i 241 horsepower j 500 hrlyr j 

j EOT 0074 IH- 101 · 100 Crude Umt Process Heater .. 1 ··----1~2-MM BTUth_r ___ ··1 30.52 MM BTU/hr I Natural Gas· ---· · -.-. ,----·-·8760 hr,Yr ~ 

EOT 0075 !H-201A- t 10~ Crude Umt Process Heater __ _ ______ j 10.18 MM B~~~~--1_ ____ 1_~~!.. MM BTU/hr 1 Fuel Gas ____ . ··----L 8760 h~"f!. ___ l

02: OO?~.!H-202- Hot Od Proces~ ~~a_ter No 1 __ __:. . 37 ~M ~TU/hr ! 37 MM BTU/h~--! Natural Gas-----·- .. ____ 1 _____ 8760 hr/'yr -··- . . ! 

OT 0077 IH-203- Hot 01l Process Heater No 2 ! 26.56 MM BTUihr i 26.56 MM BTU/hr I Fuel Gas i 8760 hrtyr : 

I E:Qf 00i8.1H-204- Solvents UM Heater --- ··: ·---18. MMBTUthi-"--i- 18 MM-BH}/hr Natural Gas -- -· .. • -· r-·- ... 8760 hrfyr . ; 

i EOT 0079H-205 · Hydro"'ir8Bi8r Healer - - ---)- 35.7-M·M-BTUihi ···-i 35.7 MM BTUihr Natural Gas &"FUen;as --1 ---8i60 hrryr·--! 

I EOT 0080 H-301- No.1 Hydrotreater Heater · -- -- · · -i --13 32 MM BTU/hr ! t3 32 MM BTU/hr I Fuel Gas -- · 1 8760 hr/yr ---~ 

:ecn 0081 H-601 ·Solvent Train Pr~~.!". Heater --·- ·-· . -·L---8---~~ 8Tlflhr····-·-·i- 8 MM B!U!tu Fuel Gas ______ ~--·~~~~~-= _J ~-hr,Yi ---1 

: EOT 0082 H-602f1000_:_~Iillty Fractionator P~~~ Heater 1 .. __ _ 1 .. __ 9 MM ~~~-~r .. _____ !..... 9 MM BTU!hr Natural Gas --· ··--·- 1 8760 -~rty~__j 

EOT 0083 IH-701- 700 Uml Process Heater I I 18.49 MM BTU/hr j 18.49 MM BTU/hr Fuel gas I 8760 hr/yr 1 

~EaT 0064 IH-901 - HydfOgen·Piant Reformer --------·- 1 ··-- - 33-. 7~EH-Lilh-r -r--33.74--MM BTU!hr Natural & Waste G-a·s ----·---~----8760 ht,yr--1 

:-Ear 0085 iLO- Loading Operations 1 ··· · · · ··~6807 "t)bl;y;.--·---·i---- ---·- ----··-j·---·-8766 hrlyr j 

rEQT 0086 :~H ·Air Dryer (OOS) _ _ _____ ! -·-· ~--~=-= 8 ~~ BTi.Jihf··----, 8 MM BTU!hr Natural Gas --~ ~ ·:~~-~L-~.: lfi6o n.~~~--~· 

LE9_ !..~~'!!_.ww- Wastewater Em1ssions ..• . ... ___ 2_1~ ~a_llonsl~ ___ l 1 ~0 gallonsln\ln ·-·-· .... __ [ 876~ hr/yr II l EOT 0088 lA- Pressunzed Storage Tank • 36750 gallons J i · 8760 hrtyr 

1 

EQT"i:i089 ·37- Pressunzod Storage Tank --· ·-·· 28266 gallons ,-- -------i ·- ------ ·---~ ·- ··--8-iSO"hi/Yr 

0090 38- Pressunzed Storage Tar\k---·--·---- "28266. Q811onS ..... -----~- ----···----·. -j-- 8760 hr/yr 

I EOT 0091 ,39. Pressurized Storage tank ____ - ---- 398874--gallons ·1··- ··----··-·---··--1 ---- ·· ·· -·-.. -··-r·· -·-·arso hr/yr · 

[Eat oos2 73- 5.000 BBL VFR Storage Tank ·-··-

LE~T 00~3 76. 10.000 BBLVFR Stor.tgerank f EQT 0064 79- 5.500 BBL VFR Storage Tank 

ea'roos5 8-500 BBL HFR Storage"Tank 

[EQT 0086 9 - 500 BBL HFFfStorage Tank ·-··-- I EQT 0067 B-1401- No.1 Boiler 

i"i~ar ooss B-1402- No.2 Boiler 

[-EOT-Oi592- 40- Pressurized Storag0"i'80k ... -·- .398496 gallons r··. --- -·----· --- ·-·-· .. ---; 8760 hrtyr--

. EOT 0093 41 -Pressurized Storage Tank __________ -·-- 398748 gallons : ··· ··-··-·--···---·--- -·- ···- ---· ··- · · ·· · 8760 hr/yr ··· 

----· ---- ···--· --····----·-· ··-- -· -----·-··----------··---·· ----· .50T 0094 44- Pre~~-unzod Storage !_ank __j_~_0084_2 ___ g~l!~.':~--~----·-· ---·----· ---··· --··-·-· 8760 h_r_~~----- EOT 0095 46- Pressunzed Storage Tank : 116634 gallons 8760 hrlyr 

~?!6_j70-PressurizedStorageTank ______ ---~------j 26334 gallons : ··--··-- __ ····-·----8-~60hrlyr ! 

Page 2 of 8 TPOROt•t 
Subject Item Inventory: 

10 Description 

Entire Facility 

EQT 0097 12- Pressurized Storage Tank 

EQT 0098 42 • Pressurized Storage Tank 

EOT 0099 43- Pressurized Storage Tank 

EQT 0100 45- Pressurized Storage Tank 

EOT 0101 59 - Pressurized Storage Tank 

EQT 0102 62 - Pressurized Storage Tank 

EOT 0103 63- Pressurized Storage Tank 

EQT 0104 64 - Pressurized Storage Tank 

EQT 0105 65 - Pressurized StOrage Tank 

EOT 0106 68- Pressurized Storage Tank 

EQT 0107 OPE- Dual Phase Extraction System 

INVENTORIES 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080..()001 O·V6 

Air· Title V Regular Permit Minor Mod 

Tank Volume Max. Operating Rate I Normal Operating Rate 

21672 gallons r--

190512 gallons --l 191016 gallons 

116676 gallons -=± 

22008 gallons __ ___j __ ~-

21084 gallons ' 

21084 gallons ' - 23436 gallons I 

23436 gallons I 

23436 gallons -r --- 1600 ft"3/min r- 1600 ft"3/min 

EQT 0108 OPE OWS - Dual PhasB Extraction System- Oil/Water - 50 gallons/miri -

! 50 gallons/min 

Separator j___ 

FE- Fugitive Emissions- - ; FUG 0002 I I - FUG 0003 UR- Unpaved Road Emissions I _ _j ___ 

Stack Information· 

10 Description Velocity Flow Rate Diameter 

(fUsee) (cubic fUmin-actual) (feet) 

Entire Facility 

EQT 0019 HFR • HFR Storage Tank 

EQT 0020 10-500 BBL HFR Storage Tank 1 6 .3 -- EQT 0021 11 • 500 BBL HFR Storage Tank 1 6 .3 

EQT 0022 14-2,000 BBL VFR Storage Tank 1 6 _3 

EQT 0023 15 • 2,QOO BBL VFR Storage Tank 1 6 .3 

EQT 0024 16 • 2,000 BBL VFR Stoiage Tank 1 6 .3 

-~------- EOT 0025 17 • 2,000 BBL VFR Storage Tank 1 6 .3 

EQT 0026 18 • 2,000 BBL VFR StoraQe Tank 1 6 .3 

EQT 0027 19 • 2,000 BBL VFR Storage Tank 1 6 .3 

EQT 0028 2 • 500 BBL HFR Storage Tank 1 6 .3 

EQT 0029 20 • 2,000 BBL VFR Storage Tank 1 6 .3 

EQT 0030 21 • 2,000 BBL VFR Storage Tank 0 .. 01 .3 

EQT 0031 22- 5,000 BBL VFR Storage Tank 1 6 .3 

EQT 0032 23 • 5,000 BBL VFR Storage Tank 1 6 .3 

EQT 0033 24 • 5,000 BBL VFR Storage Tank 1 6 .3 

Page 3 of 8 

Contents Operating Time 

8760 hr/yr 

8760 hr/yr -- 8760 hr/yr 

8760 hr/yr 

8760 hr/yr 

8760 hr/yr 

8760 hr/yr 

8760 hr/yr 

· 8760 hr/yr 

8760 hr/yr 

8760 hr/yr I 

8760 hr/yr 

-~·-

8760 hr/yr 

8760 hr/yr _J 

Discharge Area Height Temperature 

(square feet) (feet) (oF) 

-- -- 40 

40 77 

40 77 _j 

24 77 i 

24 77 ~ 24 77 I 

24 77 j 

24 77 I 

24 77 I 

40 77 

24 77 I 

24 77 I 

30 77 __, I 30 77 --1 30 77 __j 

TPOR0149 
Stack Information: c:=--- Oeacrlptlon 

: Entire Facility 

INVENTORIES -

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

Velocity 

(f11sec) 

Flow Rate 

(cub1c fUmin-actual) 

Diameter 

(feel) 

Discharge Area 

(square feet) 

---

Height 

(feet) 

Temperature 

(oF) 

i EQT 0034 25-5.000 BBL VFR .. Si0r_a.Q8 Tank ----,- ------6··--·-·-·----.3 --.-- -------- ... 30 --- __ 7_7 ___ _ 

-EQ'f003526': s.oaa·ssL VF·R-StOrage ra-nk _____ ·-- 1 s ··-- · .3 · -- Jo 11 

I EOT 0036 27- 's.OOO-BBL VFR s!oiage-tank - 1 --- -s·=~:~. -~y- 30 ,,-~: :=~-j 

1 EOT 0037 26-6,000 BBL VFR Slmage Tank 1 6 .3 25 77 ! 

I EQT 0038 29 :·'S'Q.Ooo BBLIFR Storage Tank i 6 3 -- 40 77 

. EQT 0039 3-500 BBL HFR Storage Tank . --------------· 1 -- --·-·e-···---- .3 ----40 . -----77----- -i 

EQT 0040 30 - 6.500 BBI'VFR Storage Tank 1 --- s--------- .3 25 77 ~ 

1 EOT0041 31-s:sOOeslVF-RStoiiQeT~------- ..... 1 6 -·· ---~3-- -----------25 

EQT 0042 32-20.000 BBL-VFR Storage Tank ,-- --·-- ... if··-···--·--- .3 36 ------- -;;----~~~--~1 EOT0043 33-20.000BBCLFRStoraQeTank ,-- --· .. ·····s··*--------- 3 36.5 77 I 

i EQT 0044 34- 10.000 BBL vFR Storage Tank 1-- ----- ---~ _ .:~-~-~~---~~:- ... --~3- __ _ 30 ~----· 

EQT 0045 35 · 10,000 BBL VFR Storage Tank 77 

EQT 0046 4 - 500 BBL HF-R Storage Tank 

EQT 0047 4'f- 80,000 BBl.IFfnii0fiQ8filiik"" _____ --

- EQT 0048 5- 500 BBL HFR Storage Tank 

EOT 0049 54- 10,000 ~sCi FR. Storage Tank 

-E-6T 0050 55. 10.000 BEfL I FR. si0i-8ge Tank 

ear 0051 56- 10.0-tio·e:eL··IFR SiOrage Tank 

EQT 0052 57- 80.000 .BBL VFR SlOrage Tank 

EOT 0053 Sa-~ ·saO ·aBL H.FFfStorage Tank ---- --

~T oos4- 6 ·: Soo eBCHFR storage T3nk 

EOT 0055 60-5,000 BBLIFR Storage Tank 

EOT 0056 66- HJ.oo(fsel VFR Storage Tank -- -.. -· 

EOT 0057 67- 10.000 BBL VFR Storage Tank 

~cn----·----· -- . -----·-----· ------ EOT 0058 69- 700 BBL HFR Storage Tank 

' 

1 -- . 0 

0 

1 

---- ... -

1 

- 1 

1 

-------------------,-. 

. ------------- 1 

--- 1 

1 

1 

6 .3 30 --· ... -6·- ... ------- ...... 'j --- --40 

--m··--------~------------------ -- 40 

.01------------ --·-j·- ---- --·· 40 

6 .3 42 

----6-- . -- ----- .3 42 

.If-- ---···· ·- ..... -· 3- ---------- ·42 

--6·------------j- ----------------- 40 

-- -.---------- .. 6 .3 40 

77 

-fr---

77 

77 

77 

~ 

__ , 

- ---- 'ii ______ _ 

-·· 77 _______ _ 

------__ 6 _____________ 3 ------- 40 77 _ __, 

------ -6" -·-- ---- - - :3 30- -·---,7-·---

6 .3 18 , ,] 

6 .3 18 77 i 

. ----- -----,----------------- -·----·---- -- ------- ------- --------1 6 .3 18 77 I 

ear-oos·g-=,-: 5(i6 ' ·saL HFR siorage Tank ____ ------- ·-- --- ---.,-- -----6-------·-- --·----. -:3 ----- -------- 40 ·-----77----~ 

EOT 0060 71 - 900 BBL HFR Storage Tank 1 ---6------- -- "T"'' ---,8 77 ---i 

Ear oosf· 72- s.ScXfBBL VFR Storag8T~----- . -------------1·---- -----6-----------.-3-·------ ----- ------- -32 ----77 i 

EOT 0062 73 · 5.000 BBL VFR Storage Tank ---- ---- 1 - -- - ----6----·----- y- -- j2 77 ! 

EOT 0063 76- 10.000 BBL VFR Storage Tank . --- ------ 1 -s-···- ------ · .3 1a 77-----; 

f-gar 0064 -·:;g-.-5.500 BBL VFffStorage tanr-------·· -- ---·- 1 --s··---------- ·----:3· ---,8 -----~----· 

• ---

[ EOT 0065 ~~-~ ~~~-H~~-~~orage Tank -·--··-- __ _ --. ·--6-- ·-- ----- - 3 40 77 ------------------

Page 4 of 8 TPORD 148 
INVENTORIES 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080..00010-VS 

Air· Title V Regular Permit Minor Mod 

Stack Information· 

10 Description Velocity Flow Rate Diameter 

(fUsee) (cubic tumi_n·actual) (feet) 

Entire Facility 

EQT 0066 9-500 BBL HFR Storage Tank 1 6 .3 

EOT 0067 B-1401- NO.1 BoiTiif ___ 51.7 12882 2.3 

EQT 0068 B-1402- No.2 Boi19r 68.3 12870 2 

EOT 0069 BD - Blue Drum-··· - .2 

EQT 0070 CT- Cooling Tower 

EOT 0071 FL2 - Flare 197 20880 1.5 

EQT 0072 FP- Emergency Firewater Pumps 339.1 1440 .3 

EQT 0073 GEN- Backup Generator 190 2238 .5 

EQT 0074 H-101- 100 Crude Unit Process Heater 15.1 14400 4.5 

.• 

EQT 0075 H-201A- 1100 Crude Unit Process Heater 61.5 18102 2.5 

EOT 0076 H-202 - Hot Oii-Pra·ce·ss Heciter No. 1 17 12810 4 

EQT 0077 H-203 - Hot Oil ProceSs Heater No. 2 48.8 14364 - 2.5 

EOT 0076 H-204- Solvents Unit Heater 48.8 26568 3.4 

EQT u079 H-205 - Hydrotreater Heater 12.9 12306 . ---------u 

EQT 0080 H-301 -No.1 Hydrotreater Heater 46.26 19621 3 

EQT 0081 H-601- Solvent Train Process Heater 25 18840 4 

EQT 0082 H-602/1000- Utility Fractionator Process Heater 19.3 14544 4 

EQT 0083 H-701 - 700 Unit Prociss Heater 42.5 12510 2.5 

EQT 0084 H-901 - Hydrogen Plant Refo~mer 24.7 7272 2.5 

EQT 0085 LO- Loading Operations 

EQT 0086 SH -Air Dryer (OOS) 21.06 15875 4 

EQT 0087 WW- Wastewater Emissions 

EOT 0107 OPE- Dual Phase EXtraction System 1 

FUG 0002 FE- Fugitive Emissions 

FUG 0003 UR- Unpaved Road Emissions 

GRP 0010 Crude-Cap- Crude Cap (Capped Tank 47) 80.000 BBL IFR STORAGE 

TANK 

GRP 0011 HEAVY CAP-1 • Heavy VOL Cap-1 (Capped Tank 57) 80,000 BBL VFR 

STORAGE TANK 

GRP 0012 HEAVY CAP-2 ·Heavy VOL Cap-2 (Capped Tank 57) 80,000 BBL VFR 

STORAGE TANK 

GRP 0013 UH VOL IFR CAP· UH VOL tFR Cap (Capped Tank 54) 10,000 BBL tFR 

STORAGE TANK - GRP 0014 VFR/HFR CAP· LighUHeavy VOL VFRIHFR Cap (Capped Tank 16) 2,000 

BBL VFR STORAGE TANK 

Page 5 of 8 

Discharge Area 

(square feet) 

Height Temperature 

(feet) (oF) 

40 77 

19.6 400 

19.6 400 

13 120 

20 

60 1100 

10 840 

15 854 

40 500 

-- 25 750 

88 380 

40 500 

57.2 500 

106.5 500 . I 

29.5 850 ·-· l 

60 800 

60 800 ----~ 37 350 •--'-

65 300 

20 

60 600 

20 

20 70 

20 

-- 20 

40 I 

40 I 

40 I 

36.5 I 

I 

24 

__ __] TPOR01o49 
Stack Information: 

.INVENTORIES 

AIID: 312- Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air· Title V Regular Permit Minor Mod 

[ io '-""==---------;;:D.,-oa'"c:-:crlpti~~------ _ ·- y;,~~~tY·-··· ... - "flo~ Rate Diameter Discharge Area Height ---T-e~Peratur~--l 

(N~_c_l ____ (cub•c N~n-a~ual) (feel) (square feel) _':;~) -~~~~~-~oF) ~j .Entire Facility 

l.~RP 001 ~---""~"'~"P~""~""b ~~~~:_s_P_s_K_B_F_R--C~P (CA~.~~~-·r_AN_K_7~:.1~.-6~~---a_· B_L _____ _ 

Relationships: 

Subject Item Groups: 

~-- iii- --,-1 --=---------,Group Typo 

~-CRG 0001· .. ,CQmn;QrlR&qliiremeniSGfOU·p 

-------,--- - - · ··------- ·· ···- Group Description ---- ------·•·· 

~--: CQiiSeniOicre·e~e~~~~=nO'Isr:f;:o:;;r -;Bc;oi'Cie0r

0

ann«dnHceca;;-le0r<s "'"""""'"'=..,-----------· 

--, 

! 

_I ~5'RP 0010 I Equipment Group 

l?R~ ~~2._1 _ _jEquipment Group 

~-~p 0012 _ .J~~~i~~~-Gr~u~ 

~~~-0?.~~--JEaurpment Group 

I 

Crude-Cap· Crude Cap (Capped Tank 47) 80.000 BBL IFR STORAGE TANK 

---------+"'HEAVY CAP-1 - He~~~LCap-1 (Capi>e_d_ Tank_:;7J 80.000 ~Bl VFR_ST""O"'RA'"""G"'E'"T'-AN""K,----- ~ 

I HEAVY CAP-2- Heavy VOL Cap-2(Cappcd Tank 57) 80.000 BBL VFR STORAGE TANK : 

.. ---. ·-· ----p.iH v"(:}C-iF_~ ~~ -. uH VOL I~R Cap (Capped Tank 54) 10.000 BBL IFR STORAGE T A_NK -------- j RP 00.14 ___ :_Equipment Group 

GRP 0015 Equrpment Group 

GRP-0017- 'eauroment Group 

j VFRIHFR CAP- LrghVHea~ VOL VFRIHF~ Cap (C~_P_Ped Ta~~-~~_:~~~~L VFR ~~?~~~ !~----- __ j 

i. N~PS_ l<_b CAP- NSPS KB FR CAP (CAPPED TANK 76) ~~~~~0 BBL STORAGE TANK --·----- ·-· -1 

1 PST - Pressunzed Slorttge Tanks 

~-0~~~~~ or Facility Wide ____ j EF- E~~~ Facll1ty ------.. .. .. ·--·- ] 

Group Membership: 

~~-oo~o · --.. --htr-·sao sBLHFRSiO'raQe ;~~~~-~~~ .. --~~-crip.tlon -~_:·~~- ==--~----~--- - GRPoooodOOo11 MemberotGrOUps ------- -.--

:Ear o02f ___ "j""1T:s·aa BBL HFR Storage l'irik ___ -- ----· ---- -GRF,-OOoOOOoO;l-------

1 EQT 0022 I 14- 2,000 BBL VFR Storag8-Tci·n·k ·---------- . - .•. _ .. __ GRP0000000011 

EOT 0023 115-2.000 BBL VFR Storage Tci.ik .. ________ ·· ·- ·--------· ·e;:OR~P"o:;,o;;oo;:o"o"oo;c.o;c.1;;1-------------------···---··-·- ----

EbT 0024 ---;Ts: 2.ooo·aBL vFffStC:ir3Qe·rank____ ·- · ---------- · ·-·- GRP·ooaooo"o"'o'"1'4 _____ _ 

EQT 0025 j17 · 2,000 BBL VFR Storage Tank______ ·-- GRP0000000011 

! EQT 0026 i 18-2,000 BBL VFR Storage Taii"k ··--- ·---· I GRPOOoQjjo:C.0;;0;-.1-.4 ______ -----

:·E6T.002i ···---·r--;g-:-2.000 a·BIVFRSiOrage· Tel~---·-· . -· . -··-·· ··---·· : GRPOOoooooo11 

: EQT ooi8 ____ 2-500 BBL HFR Storage Tank GRPOOOOO·i<o-<ooic1;-;1;----

:-EQT 0029 20-2,000 BBL VFR Storoige Tank-- . -·- GRPOOOOOOoi<o<1<1 -----

~-E-ar oojQ---·:F-2.000 BBlVFR Sto·raQe Tcin_k______ ... ·-------------.- .. -·; GRP0000000011 

/'i:ar 00j1---; 22-5.000 BBL VFR SiOr.age rank· ·-------·. --j-GRPooOOOOOOff______ --·----·--·- -· ------ ··---·--··--: 

~~;_;~~~~~-=I.~-~-~~-:~~:~~~~i~~-~:-~-:~---· ..... ~--~~~=~-----------~~~~~~~~ ·-· -. ·- --------- -- -~-j ~ EOT 0034 I 25- 5,000 BBL VFR Storage Tank GRP0000000011 i 

-----! .. _ _J 

··eat oOJs·---~000 BBL VFR Storage T3nk ·------·- ----- GRP0000000011 --··--i 

-EQT 0036 : 27 · S.060"esL VFR Storage~ Tank GRP0000000011 

"EQTQ()37 I 28 - 6.060 BBL VFR Stor£i9~ !_.in_~_ ·-·-·----·· -----· -+G;;R"'-P"ooooo""'""'o"oo;c1"5;_ _________ -_------..... ·------=~j 

Page 6 of 8 TPOR01~g 

" 
Group Membership: 

10 

EQT 0038 29 - 50,000 BBL IFR Storaga Tank 

EQT 0039 3 - 500 BBL HFR Storage Tank 

EQT 0040 30 • 6,500 BBL VFR Storage Tank 

EQT 0041 31 - 6,500 BBL VFR Storage Tank 

EQT 0042 32- 20,000 BBL VFR Storage Tank 

EQT 0044 34- 10,000 BBL VFR Storage Tank 

EQT 0045 35- 10,000 BBL VFR Storage Tank 

EQT 0046 4 - 500 BBL HFR Storage Tank 

EQT 0047 47 - 80,000 BBL IFR Storage Tank 

EaT 0048 5- 500 BBL HFR Storage Tank 

EQT 0049 54- 10,000 BBL IFR Storage Tank 

EaT 0050 55- 10,000 BBL IFR Storags Tank 

EQT 0052 57- 60,000 BBL VFR Storage Tank 

EQT 0053 58 - 500 BBL HFR Storage Tank 

EQT 0054 6 - 500 BBL HFR Storage Tank 

EQT 0055 60- 5,000 BBL IFR Storage Tank 

EQT 0056 66- 10,000 BBL VFR Storage Tank 

EQT 0057 67- 10,000 BBL VFR Storage Tank 

EQT 0058 - 69- 700 BBL HFR Storage Tank 

EQT 0059 7- 500 BBL HFR Storage Tank 

EQT 0062 73- 5,000 BBL VFR Storage Tank 

EQT 0063 76- 10,000 BBL VFR Storage Tank 

EQT 0064 79 - 5,500 BBL VFR Storage Tank 

I EOT 0065 8-500 BBL HFR Storage Tank 

iEOT0066 9 - 500 BBL HFR Storage Tank 

I EQT 0067 B-1401 -No.1 Boiler 

EQT 0068 B-1402- No.2 Boiler 

EQT 0074 H-101 -100 Crude Unit Process Heater 

EQT 0075 H-201A-1100 Crude Unit Process Heater 

EQT 0076 H-202 - Hot Oil Process Heater No. 1 

EQT 0077 H-203- Hot Oil Process Heater No. 2 

EQT 0078 H-204- Solvents Unit Heater 

EQT 0079 H-205 - Hydrotreater Heater 

EQT0080 H-301 -No. 1 Hydrotreater Heater 

EQT 0081 H-601- Solvent Train Process Heater 

INVENTORIES 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permil Number: 3080-00010-VS, 

Air. Tille V Regular Permit Minor Mod 

Description 

GRPOOOOOOOO 1 0 

:.GRP0000000011. 

: ,. '", GRP0000000015 

GRP0000000011 

GRP0000000011 

GRPOOOOOOOO 11 

GRP0000000011 

GRP0000000011 

GRPOOOOOOOO 10 

GRPOOOOOOOO 11 

GRP0000000013 

GRP0000000013 

Member of Groups 

--

--

·-

- GRPOOOOOOOO 11 , GRPOOOOOOOO 12 ----·---~·- GRPOOOOOOOO 11 

GRP0000000011 - - GRPOOOOOOOO 13 

GRP0000000015 ---- GRPOOOOOOOO 15 

GRPOOOOOOOO 11 ----- GRP0000000014 - GRP0000000015 

GRP0000000015 

GRP0000000015 

GRP0000000011 - ----- GRP0000000011 

CRGOOOOOOOOO 1 

CRGOOOOOOOOO 1 ·----- CRGOOOOOOOOO 1 

CRG0000000001 

CRG0000000001 

CRG0000000001 

CRG0000000001 

CRG0000000001 

CRG0000000001 

.. CRG0000000001 

EQT 0082 H-602/1000- Utility Fractionator Process Heater CRG0000000001 

EQT 0083 H-701 - 700 Unit Process Heater CRG0000000001 

EQT 0084 H-901 -Hydrogen Plant Reformer - CRG0000000001 

EQT 0088. 1A- Pressurized Storage Tank '• GRP0000000017 

EQT 0089 37- Pressurized Storage Tank GRP0000000017 

EQT 0090 38- Pressuriz~~ _§_!~~age Tank GRP0000000017 ----- ---- -- --

Page 7 ofB 

,·. --

--

I 

TPOR0149 
Group Members~lp: 

INVENTORIES 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080.()001 O-V6 

Air- Title V Regular Permit Minor Mod 

------ "l 

I 

I EOT 00 ~1 ! 39"- Pressurized Storage Tank' -· O.scr1ptiOrl ___ - ...... ·-- li GRPOOOO~~~~;··-·-· Member of Groups 

i~~ ~~ ---~--1 ~: ~=:~~~~ ~:::~ ~=~:- ------ ----- -~- -- --- --- ------ ~:::~~~~~~-~- ------------ ·- ·------- . -· ···-··- ·----1 

----1 

EOT 0095 ·-·-- - i"46 · Pressunzed Storage Tank --------------· ·-- ---- I GRP0000000017 ·- -------- -·-·····i 

1 EQT 0096 ~7"0·--Pressurized Storage Tank ____ ·· · · ·- :--~------- GRP000000001!. __ ----- _____ -··-· ---···- __ _j 

· EQT 0097 ! 12- Pressurized Storage Tank 1 GRP0000000017 

-~-~!!___ _ -~~---PressurizedStorageTaiik___ ----- --··-- __ i GRPOOOO_~~~~?. --·---- --- -· _______ ] 

~~~- :r::~L~~~E~-- ~:~-- ___ ~-------:~:::=~~:---=~~=- __ ---~--- ~-:~~-~~:j I EQT 0102 ·--·-· 62 ~Pressurized Storag!_Ta~~-------- ____ GR~0000017_____ _ ______ _J 

EQT 0103 63- Pressurized Storage Tank GRP0000000017 : 

-ear 0104 ___ · 64. -·Pressurized Storage-Tank. - -----· GRP0000000017 ··· ··-------

EOT0'10s -··· 65"- Pressurized Storage Tank ·--- . ·-· GRP0000000017 ----···· 

EQT 010~ 68- Pressurized Srorage Tank -·--· G~~~~~~~~~!~_--__ ----------------- - -~~ _:-=-:J 

NOTE: The UNF group relationship Is not printed in this table. Every subject item is a member of the UNF group 

Annual Maintenance FH: 

I FHNU.Tiber· I ··-AJr c~~~aminant Source c-·--~_ultiPrier·~ Units~ Measure "l 

0720 10720 Petroleum Refimng (~-~t~~-CapaCJty) 12 I M bblfd~¥. i 

-- SIC Codes: 

[ --rPetrOioum refin-;-ri"g---·-· --·-·-·- -----: AI 312 J ---==[ ~~r~leum re~nl'2_~-- --~ ~=~~~ -=·~--~F 001 ________ _:: 

Page 8 of 8 TPQR01•9 
co 

Subject Item Avg lb/hr Max lb/hr 

Entire F.aclllty 

EQT 0020 

\0 

EQT 0021 , 

EQT 0022 14 

EQT 0023 15 

EQT 0024 16 

EQT 0025 

~F 17 

EQT 0026 

18 

EQT 0027 18 

EQT 0028 2 

EQT 0029 

20 . EQT 0030 1--

21 

EQT 0031 22 

EQT 0032 23 

EQT 0033 24 

EQT 0034 25 

EQT 0035 

26 

EQT 0036 27 

EQT 0037 28 . 

EQT 0038 ' 29 

EQT 0039 J 

EQT 0040 

JO 

. EQT 0041 

__ =± " EQT 0042 J2 

.EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-V6 

Air -Title v Regular Permit Minor Mod 

·-·-- NOx PM10. 502 

Tons/Year Avg lb/hr Max lb/hr Tons/Year Avg lb/hr Max lb/hr Tons/Year Avg lb/hr 

- - I 

·-----

-

~=----~~-· c__-

I 

I ----~ I 

\ --- ;----- . I I .-----T ·-----r-----

---j I ---1-- r [ ___ 1 

I i 

--- ___j 

I 

i 

T 

I 

---[------

I 

----!-------- ri --~--------

------- . L ___ 

Page 1 of 8 

--

Max lb/hr Tons/Year 

-

-

I 

TPOR0145 
EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Penni! Number: 3080~0010-VG 

Air· Tille V Regular Penni! Minor Mod 

I Subloct ttom ~~~=/hr Max lblhr i ;.~~:.~ ·· Av~~~- .. ·-·.. -~- M~~~blh: ~- ~~~::::-1 - __ _J 

; Entire Facility : j t j I ~,or oo2o ·-- 1 2_0 \"" -~ 1 

EOr0021- ! 

2

_

9 

- --· -: i l I 11 I I i I 

f--;::~ :::: -----· :495 --- -------1 F~ 

[ ~.or 0024 I 28.7 ---- -T I -- -i ---- ... - -- -- --------------- ... __ I 

I EOr 0025 I 14 5 I' I I' 1 11 1 · 

I -1 ··- ----- ·-· j ~.or oo2s , 28_7 i I I ~or 002f--1--- -- 0.97 ---r- ---1 ------- 1 ----1 -· ~or 0028 l 19 -- - I l I --l 

! ~OT 0029 •. -------

0

_9f --- ----~------·. - -- ~-----! 

'I Eor 0030 14.5 I . . 'I ---+- i" ------ -1 21 I I I 

:· EOr 0031 I .~;-- I i. -- I --· I ----1 ~ zz · , ! I --~aT 0032 ------- ··r--~- -- -- : _ -- 1 

-----

1-------·1 

;·-;,o_r_o_o_J_J ----1 - ·- 14_

5 

; --·-' ____ l____ • -- -- -----' 

L . __ !_____ ·-· -- ··-· ·---··-·· 

I ~:~ ::: i -+--;:: I -- ;· I - -- 1--- --i 

, ~:: :: F=__j ::: - ---~- ~-- ----=1==----J 

;·i'ar-oa38 ----H*- ---- ------ ! · ----+----- ~-~,-:: ::: --· -~ ::8 I --___ ~--~~------~~------- -_ r-----

. ; ----- ·- I ---- --------------'----- -- EOT 004+1 I . 148 i 31 ' . . 

or 0042 ----~ 14 5 j · --------; __ _[ ----------· 

Page 2 of 8 TPQR01•S 
co 

Subject Item Avg lb/hr Max lb/hr 

Entire Facility 

r EQT 0043 33 

EQT 0044 

" EQT 0045 35 

EQT 0046 4 

EQT 0047 

" 

I EQT 0048 5 

EQT 0049 

~ 54 

EQT 0050 55 

EQT 0051 56 

EQT 0052 

57 

EQT 0053 58 

EQT 0054 6 

EQT 0055 60 

EQT 0056 66 

EOT 0057 67 

EQT 0058 

" EQT 0059 7 

EQT 0060 71 

EQT 0062 73 

EQT 0063 76 

EQT 0064 

79 

EQT 0065 B 

EQT 0066 9 

EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312 -Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

NOx PM10 502 

Tons/Year Avg lblhr Max Jb/hr Tons/Year Avg lb/hr Max lb/hr Tons/Year Avg lblhr 

---

-

- I - _j_ 

' 

I 

I --

i I 

-T -·--

I -

----j 

I 

I 

rI _I __ Page 3 of 8 

Max lb/hr Tons/Year 

j 

I 

I I 

I 

I 

TPOR0145 
i--voc 

EMISSION-RATES FOR CRITERIA POLLUTANTS-AND C02e 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

Lead ------ · - -l 

f -SubjKt"""itii"in ___ j-Aviibihr-~Bx lblhr __ , 

' Entire FacUlty : 1 i ! 

Tona/Ye~~A_V~-~b/hr I. Max lblhr ~- "ToOiiY~ 

l-_ ~,ar~ao;;~~r----;; ;~ -ro-.-a -, 0.43 ___ i___ j --- _}~ _ ---1 

ear 0044 I • 14 5 

(~~f:~::~-:_l_~~----·-~~ 5 ___ . ---- --~-. ---·--~+---~~ r- E.CJr~~----~--- 0.62 1 ---+ f--iar 0048 1 3 2 , 

i iar 004~----- _r_-- 0.22 I r-- . -_ _J_ 

EOT 0050 i 0.16 ! i __ _ 

S5 I . . ... 'j -·· --- J 

~ar o~5:~~~L~---f-~~~-- (___:! ____ , ______ ,____ _: ____ ----! 

EQT 0052 . 10 7 I . • 

iar oos3 ____ :----- --- o9~-T-- ------~--- ----_ i ~:~-~~-: --=C __ _j 

~ar- 0054 -··-- · --- - --r 2 ;--- 1 ---r---=--1 __ _!_ ________ I 

~QT 0055 --i--- I 0 ,. ___ I ___ _L ____ j___ --1---- ---1 ~:~-::::-- --- . ~ ~-----~;~:: --1----L --=--=:L=:~- _]_-=~----- -~ EQT 0058 --! ! 2 4 ! i ! 

.!~QT 0059··----: ---- -·-;0-- ) ___ --'-----i------~---==·~ , L ! I I ----- = ---- ·-iEar oo6o I 0_35 : 24.8 , 1.5 : _ _ ___ J 

------, 

,. . ------ I ... ,. ... --ass [____ _ _ 2 9 I_ ______ !_ _ __ . _____ ___ _ _ __ 

1 ~0066 --'---------- 19 _]_ _t-__ _ 

Page 4 of 8 TPQR()I~S 
co 

Subject Item Avg lb/hr Max lb/hr 

Entire Facility 

EQT 0067 2.80 2.80 B-1401 

EQT 0068 1.40 1.40 8·1402 

EQT 0069 

80 

EQT 0070 

CT f---iat 0071 0.15 0.15 FL2 

EQT 0072 FP 3.57 3.57 

~QT 0073 1.61 1.61 GEN -· 

EQT 0074 H-101 2.50 2.50 

EQT 0075 0.84 0.84 l:l·201A 

EOT 0076 3.05 3.05 H-202 

EQT 0077 H-203 2.20 2.20 

EQT 0078 1.50 1.50 H-20< 

EOT 0079 2.94 2.94 H-205 

EOT 0080 1.10 1.10 H-301 

EQT 0081 H-601 0.66 0.66 

EQT 0082 H-602/1000 0.69 0.69 

EQT 0083 H-701 1.50 1.50 

EQT 0084 9.60 9.60 H-901 

EQT 0085 LO 

EQT 0086 SH 0.66 0.66 

EQT 0087 

ww 

EQT 0107 

OPE 

. EQT 0108 OPE OWS 

EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312 -Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-0001 O-V6 

Air- Title V Regular Permit Minor Mod 

- NOx PM10 

Tons/Year Avg lb/hr Max lb/hr Tons/Year Avg lb/hr Max lb/hr Tons/Year 

12.07 3.30 3.30 14.37 ! 0.25 0.25 1.09 

6.04 1.60 1.60 7.19 --t-o~-- 0.12 0.55 

~ I 

T 1.70 1.70 7.49 I ' 

0.67 _j 0.18 0.18 0.80 ·r 0.01 0.01 0.06 

I 

__ i _____ 

0.54 0.18 i 16.59 16.59 2.49 ______ )._ ___ 1.18 1.18 

j 

0.40 i 7.47 '7.47 1.87 I 0.53 I 0.53 0.13 

' 

I 11.01 3.00 3.00 13.1, ' I 0.23 0.23 1.00 

-; r 3.67 1.00 1.00 4.37 0.08 0.08 0.33 i 

13.35 3.63 3.63 15.89 :-· 0.28 0.28 1.21 -I 9.58 2.60 2.60 11.41 I 0.20 0.20 0.87 

- L 

' 6.49 1.80 1.80 ·7.73 I 0.13 0.13 0.59 ' 

12.88 I 3.50 3.50 15.33 L 0.27 0.27 1.17 

4.60 1.30 1.30 5.72 _l 0.10 0.10 0.43 --

2.89 0.78 0.78 3.44 I 0.06 0.06 0.26 , __ 

3.01 0.82 0.82 3.58 0.06 0.06 0.27 

-

6.67 1.80 1.80 7.94 I 0.14 0.14 0.60 

42.11 2.00 2.00 8.90 1 ·: o.s7 • 0.87 3.81 

·r--- - ! L 0.78 i 2.89 0.78 3.44 ! 0.06 0.06 0.26 

J I 

I ' 

! r I i 

T 

PageS of~ 

502 

Avg lb/hr Max lb/hr Tons/Year 

0.82 0.82 3.58 

-----·-· 

0.41 0.41 1.79 

_J 

I 

_j 

0.001 0.001 0.01 I 

- : ::----1 1.10 1.10 

0.49 0.49 

3~:.:.---1 0.80 0.80 - ---

0.25 0.29 1.09 

0.98 0.98 4.27. I 

I --~-, 

0.65 0.65 2.84 j 

0.47 0.47 2.08 I 

0.87 0.87 3.82 1 

~ 0.33 0.33 1.43 

0.20 0.20 0.86 -j 0.22 0.22 0.96 

0.45 0.45 1.98 I 

3.10 3.10 13.48 -! ---~ 

I 

0.01 0.01 0.02 J 

I 

I 

I 

' I TPOR0145 
---------- -----·------------------------- -----------· --· --- -

-Eatoon , 0.14 

1-(.JI)J •. i --.-------- EQT 0078 I 0. '" 

EQT -~~ H-701 

EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Pennit Number: 3080-00010-VS 

Air· Title V Regular Permit Minor Mod 

I ;--

. <0.01 

.. ~ 

___ J 

! 

' 

-! 

<0.001 <0.0 

<0.01 <0 0 

Page 6 of 8 TPQI=t014S 
I 

[ 

Subject Item 1 

Entire Facility _J__ 

FUG 0002 ' FE ' ' 

EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

ron NOx PM10 I 502 .... _,_ --.. ----- wv 

Avg lb/hr Max lb/hr TonsfYear Avg lb/hr I Max lblhr I Tons/Year I Avg lblhr I Max lblhr I Tons/Year I Avg lb/hr Max lb/hr jTOOsiYW 

' I - ----·--1------

FUG 0003 ------

UR 

GRP 0010 

Crude-Gap 

GRP 0011 I HEAVYCAP-1 -~1 GRP 0012 I ~~; ~~~-~ -- - . 

----t--r= i --- 1 1 I =1 _F __ -, I I I I ~-!--_== - ---,-

I 

__ , ' 5.30 

I c 

I 1.so I 5.68 

_j_ 

L_._l I . _I tJH VOLIFR CAP j GRP 0014·· ----

VFRIHFR CAP ' GRP -0015 ______ 

NSPS Kb CAP __ [ 

____ i i ____ ----

---t---l----+---+---+-----+----l----+---1----lc--- ]---~~~-=1 

Page 7 of 8 TPOR0145 
EMISSION RATES FOR CRITERIA POLLUTANTS AND C02e 

AIID: 312- Calumet lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

-·-voc· ~---- Lead 

Subject Item ·j-AV9riilhf. r· ·.;fait lblhr To~a/Year j --.A:::v:::g-,lb"'lh=r-ri--.:M.-:a::x;-;l;.,blhr· -~ono/Yoar I 

EnUre Facility ' , I 1 

-~EUG_0_00_2----~--;-6_8_1 ___ t·· 26_~-~-- 117.45 -f r ---~ FUG 0003 ·---~ .. ·····. -·-·····r-- -- . -·i UR : I 

~' I 3.52 I GRP 0010 ··-!·--~--~~-- ----~------

~~~~-~ _L_~~~~~;i~----~L. ______ """" __ _ GRP 0012 I 9 54 I • 

15929 r··· - 1 ... 1 I 

41.77 ·r I _ ·-, -4 

1.96 , ______ 1 _ ---~=1 

HE.\VV CAP-2 . I 

t~~~~~k_ ---r~~~-~~~L-~-~ 

[},;~~---~--~~----\-- .. 

~~ ~~ ... J ·---~~~~--

,,. I_- _J - [ 35.91 1 --- . . ! . , .. . ··-··· --- ! --~ I ------ ... i 

Note: Emlsalon rates in bold ara from altern•te &cenarios and are not Included In pennitted totals unless otherwise noted in a footnote. 

Page 8 of 8 TPQR0\•5 
Emission Pl 

I 

EQT 0020 

10 

EOT 0021 

1\ 

EOT 0022 

14 

EQT 0023 

15 

EQT 0024 

EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod· 

Pollutant 

I 

Avg lb/hr I Max lblhr 

Ethyl benzene 

~ 0.01 

Toluene O.Q1 

Xylene (mixed isomers) 0.02 

n-Hexane 0.01 

Ethyl benzene 0.01 

Toluene O.Q1 

Xylene (mixed isomers) 0.03 

n-Hexane 0.02 

Ethyl benzene O.Q1 

Toluene O.Q1 

Xylene (mixed isomers) O.Q3 

n-Hexane 0.02 

Ethyl benzene O.Q3 

Toluene 0.02 

Xylene (mixed isomers) 0.15 

n-Hexane 0.09 

Ethyl benzene 0.06 

TonsNear ! 

_____ j 

I 

I 

I I" ----------·t---------1 -- _ _.J 

~---------------! ___ ~ _ _j __ o_.o_4 ___ -+------------J 

' 

1 I I xytene (mixed isomers) [ ___ 0.29 

In-Hexane 

---

0.76 

EQT 0025 Ethyl benzene 0.03 17 

Toluene 0.02 

Xylene (mixed isomers) 0.14 

n-Hexane 0.09 

EOT 0026 Ethyl benzene 0.06 16 

Toluene I _j_ 0.04 

-------l 

I l I Xylene (mixed isomers) 0.29 

n-Hexane I 0.76 I 

EOT 0027 Ethyl benzene I 0.01 19 

Toluene 0.01 

Xylene (rruxed 1somers) 0.01 L ·- 0.01 . ----------------------+----- I ~QT 0028 IEthyl"benzene 0.01 J 

Page 1 of 8 • TPOR0146 
EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080.()001 O-V6 

Air - Title V Regular Permit Min or Mod 

----,---------··-

Pollutant : Emlsolon Pt. I 

I EOT 00~---· ----+-----'----

Avg lb/hr Max lb/hr TonsNear 

! 2 I Toluene ·----· 

1Xy1ene (rrixed isomers_)---

jn-Hexane 

0.01 

002 I 

I 

. -·=i-.. ---_-_ -_-__ -, -0-.0-1 --+-1 ___ _____, ·- ·---- EOT 0029 

,. 

··--·-· EQT 0030 

,, 

L._ __ ----·-----. 

I ;,01 0031 

' I 

I 

1 EQT 0032 ---- " 

EOT 0033 ,. 

I 

EOT 003ot 

" 

1-EOT 0035 .,. 

]Ethyl benzene I 001 I 

___ t=·----- --~~-~:~---± ---~11 I a.a1 ------~- · -------

----1" -----~--- o.o3 1 _____ __J 

---,-·-··-- II 0.02 ~-----1 

------ -. Toluene 

jxy1ene (rrix~ iso:~-~ _____ __ 

r;-Hexane 

; Ethyl benzene 

Jh;~eno ---

' ------r·------- i --~;,- I ·n--He_xa_n~--------- -- -----.. ~ 0.09 

--~~~-benzene ___ ---:~~~--------!,_ ----- --~--__ -;0~--- __ .. _-_-_T

1

f-----_· _---~~~---------1 ·Toluene 1 I 0.02 

~ ----

!Xylene (rrixod isomers) 

i 0.14 1 

----- T--0-.09---+i ____ __, 

·---r-·-_- ____________ -o_o-3_-_ -_ -_--r_-_------~~-=-____, 

------------+-------,--o._o2 -~- _ 

.

1

'Xylene (rrjxed isomer~>_______ ! 0.14 =1 

n-Hexane __ , ____________ o.og -----=1~. 

Xylene (rrixod isomers) 

---

jn-Hoxano 

' 1 Elh)i benzene 

-----

.Toluene 

: E1hyt bcnzen_o_____ _ ________ o_.o_3 ____ i J 

jTolucn~ ---,-------- -----j' o.o2 L I 

[~~-~no (mxod tsomerS) _____ 0_1•_ ----~-- .. ----- _: 

!n-Hexano 1 0 09 L 

::~.'-~-~-is-ome-rs-) -- -1 ~ .. -!-:;;u-. ------~-fl-.·_· ---------------1 

jn-Hexano ----- 1 J 0.09 [ j 

. ---~£~~~~~-.. -__ -~-------:~~~:--.. _______ _!__ . - -- ~-------~-!'.---~~~ , Toluene ., 

-·----t- .. 

Toluene ··--t-.. . --- ,. 

Pago 2 of 8 

0.09 

0.03 

0.02 

I I --·-r- --·---1 

TPOR0146 
Emission Pt. 

EOT 0036 

27 

EQT 0037 

" 

- EOT 0038 

"' 

EOT 0039 

' 

' 

EOT 0040 

"' 

EQT 0041 

" . 

EOT 0042 

" 

I 

EOT 0043 

" 

EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

Pollutant Avg lb/hr Max lb/hr 

Xylene (mixed isomers) 0.14 

n·Hexane 0.09 

Ethyt benzene 0.03 

Toluene 0.02 

Xylene (mixed isomers) 0.15 

n-Hexane 0.09 

!Benzene 0.01 

lcumene <0.001 

Ethyl benzene 0.001 

Naphthalene <0.001 

Toluene 0.01 

Xylene {mixed isomers) 0.01 

n-Hexane c 0.01 

. .. Ethyl benzene 0.01 

Toluene 0.01 

Xylene (mixed isomers) 0.02 

n-Hexane !_ ___ 0.01 

Ethyl benzene I 0.03 -~ --· Toluene I 0.02 I 

I . .. ----

Xylene (mixed isomers) I 0.15 

n-Hexane 0.09 

Ethyl benzene 0.03 

Toluene 0.02 

Xylene (mixed isomers} 0.14 

n-Hexane 0.09 

Ethyl benzene O.D3 

.-------

i Toluene I 0.02 

I Xylene (mixed isomers) ' 0.14 I 

I l n-Hexane 0.09 

Benzene ' 0.002 0.002 

Toluene <0.001 <0.001 

Xylene (mixed isomers) <0.001 <0.001 

n-Hexane 0.001 0.001 

Page 3 of 8 

Tons/Year 

! 

! ·---j 

J 

i 

______ j 

i 

~ 

' I 

' 

0.01 

<0.01 

<0.01 

<0.01' 

TPOR0146 
EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

~~:, ::~-~ion Pt_ --·--· ·\E;~~ be_n.z_e_n_o _____ :•_'~~·~~- ____ [__ __ ~·~-~~~'.. : ::: lblhr _ -'L·----~ ; ,. ;r~u-e-ne _____________ -------;---0-.0-2 ____ [_ ·-· -.·. _· ---~ 

[_____ :::::~~xed iso~rs) ::: I ... ·- - _

1 

EOT 0045 Ethyt benzene 

" 0.03 

Toluene I 0.02 I 

I-X_y1_e_no_(_mr_·x_ed_iso_mcr_s_l _______ +-------·--:_j1_-_--_··_o_.1_4 ____ .!_ __ _ 

i"·~exane ____ [_______ 0.09 j I EOT """"i)()46--------. . """i ..... --- --------i ; 4 !Ethyt benzeno ~ i 0.01 

! !~~;~;~-~-------------- ---------! --------------- -- _1, 

' ' 

0 01 ' ···-·-· ---- t•••• 

I ........... _. -··--·---------~--- ··---·-----,--.......... ·--. i f~~~n-e (rrixed isomers) __________ i_____ ___ __ . 0.02 ________ _j ______ ---i 

I l

n-Hoxane 1·. I 0.01 I ~~~~~,~~~,~----~1-Bc-"-,-.-".------------+~-------.. r·-- a_o, 

t-------------+-------+-------11----· ··-- Cumene 1 <0001 

Ethyt bonzono 1 o.oo1 

__ ___! 

I-N_•_P"_tha_'"-""-----------+------~~--_-LI __ <_o_:oo_1 ____ !__ ~-~ ______ ·: -·.-- Toluene ! 0.01 

=c==·-·---·- ---~~~;;~~~~50~~·~~-:====:1-~~--~:~- ---·- ---·-- ~~: -. .... .. -! . --·-----. 

EOT 0048 IEthyt benzene ! 0.01 

!:~~=~::~~~~~)-- --·---·--:-- -----· --~-~~~--~~- ------------------1 

k f:::;::~ene ~------ ~----_- ___ -:-:-2-1----i~---1-------1 I ;:.·· -~- :roluone 0.001 j ----·-··----

1 j;y1ene (n>xed is=ers) [ __ -=[-~~~~-----~~~~~c--------1 1 r>-Hexane I 0 01 J 

I

. ECT 0050 

" Elhyt benzene 

[Tolu~-""----- r0.001 

·-'---

0.001 

:xytene (rnxod isomors) I 0.01 ~ 

'"in--H-e_xa_n_o--------------1 l 0.004 -- --~ 

~c;;a:;-T-;;005='--~----+~n---H-exa_n_e ________ -_-_-_-_-_-_-_-_-_-_-_-_-t-~~~~<~0~.00=~01 ___ - i

1

_· _<_o_.ooo __ 1___ 

1 

__ <_o_.~~- -----· 

EOT 0052 jethyt benzene 0.02 " ----'--

Page 4 of 8 
Emission Pt. 

EQT 0052 

57 

I 

EQT 0053 

58 

EOT 0054 

• 

' 

EQT 0055 

60 

EQT 0056 

" 

EOT 0057 

67 

I 

'--- I EQT 0058 

I" 

EQT 0059 

7 

EQT 0060 

71 

EMISSION RATES FOR'TAP/HAP & OTHER POLLUTANTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 . . 

Permit Number: 3080-0001 O-V6 

Air- Title V Regular Permil Minor Mod 

Pollutant Avg lb/hr Max lb/hr 

Toluene I 0.01 

1

xyrene (mixed isomers) I 0.11 

n·Hexane 0.06 

Ethyl benzene 0.01 

Toluene 0.01 

Xylene (mixed isomers) 0.01 

n-Hexane O.Q1 

Ethyl benzene 0.01 

Toluene I 0:01 _......L_ 

Xylene {mixed isomers) I 0.02 

n-Hexane . 0.01 

Ethyl benzene 0.001 

Toluene 0.001 

Xylene (mixed isomers) O.Q1 

n-Hexane 0.01 

Ethyl benzene ' 0.03 

Toluene 0.02 

Xylene (mixed isomers) 0.15 

n-Hexane I 0.09 

Ethyl benzene I 0.03 

Toluene i 0.02 

' !Xylene (mixed isomers) i 0.15 

n-Hexane ! 0.09 

Ethyl benzene 0.01 

Toluene 0.01 

Xylene (mixed isomers) · 0.02 

n-Hexane O.Q1 

Ethyl benzene I 0.01 

Toluene 0.01 

Xylene (mixed isomers) . 0.02 

. 

n-Hexane 0.05 

Benzene 0.001 O.Q7 

-------------

Ethyl benzene 0.0002 0.02 

Page 5 of 8 

Tons/Year 

! I 

i 

' 

r----------------' 

I 

] 

' 

I --

I 

-; 

I 

___j 

I 

I 

0.004 

0.001 

TPOR0146 
EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AI 10: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-0001 O-V6 

Air- Title V Regular Permit Minor Mod 

i Emisslo_n ~-- _ -- :·· ~~~~~----p~~~~~~;~~~-~-~=~----=-_A•g lb~'-~_: ___ -~~--~-·-~~; __ ... J... 

~~,ar··oooo iToluene_____________________________ --~~-~~--- o 11 i 

Tons/Year 

0.01 

' 

r=-=---0062 

jXytene (mixed isomers) 0.002 011 

073 

I 

I 

0.01 

1 0.05 ----- i----- ... . ··----,-

- --"------------ ---- ~n-He)lane . _______ j ____ 0.01 _______ l ~Ethyl benzene___ I 0 03 

I ~1:-:-:-::-·-(~-.-ed-.~--.. -)-------;---------+_--~~~:-:-:-_-__ -_ ~----1 I 

I"Ei:H 0063 . 

I" 

I 

EOT CICl6A 

" 

EOT 0065 

EOT 0066 

9 

jn-Hexane 0.09 .. ···:· 

~:~c:"~"-""------------;-- ----- -----1-----------t----------1 

!

Xylene __ (nlx_e_d_ isomers) -----;-··----------- j --

003 

0.02 

0 15 

-------------'---------- I 

n-Hoxano 0.09 ]--~· O.oJ J ---- I 

----~-E~th~yl~bc~~n-z_e~ne~~~~~~~~~~-=---------_-___,i,_·~-=-----_ -_ -_ -_ -_-_-_-,-_ -----

! I Toluene 

Xylene (rrlxod isomers) 

n-Hexane 

~yt benzene 

' :Toluene 

~----

!xytcno (mxod isomers) 

'n-Hoxano 

;Ethyl bcnzono 

0.02 I 

0.15 i 

' 0.09 ' I 

0.01 

---1 I 

-------·--·--------t---------! 

1 001 ----·------· -·---- __ T __________ J _______ -

1 0.03 : ---- -- ----- --- -- i . -002 . . 

0.01 , __ ---------------------

Toluene 0.01 

1-----------+------------·------------------1 

Xylene (rrlxod isomors) 0.02 

n-Hoxano 0.01 I 

~i 006-

9

--------~~f-~~th~:~:~~nz~o~n~o~~~~~~~~~~~~~~~~~~~~:~~~~:-:_: ________ ------.~~~~-:--:-~-----------+~--:-.-=---_-_ -----1 

IToiueno 0.49 I ----oo-.~

6 ____ . I 7------~ 

EOT 0071 

"' 

ixyleno (mixod isomors) 0.16 

-------~--- ----------

t.~~~~------ 0.01 I 0 01 I 0 02 I 

~~E-1h_Y'_bc_n_zc_n_• _______ ~~-----~~~~--------l-~----_-:,_~_-_oo_-1-_--_--_-__ +j

1

-_-_<_0_oo_1 ___ __,·f--<-O._o_1_ ---l--

·INaphthaleno <0.001 I <0.001 <0.01 

~~T_ol_u_e_ne------------+--<0 ___ 00_1 ____ fj-- <0.001 -i· <001 ------~ 

lxytcno (rrlxod i~rs) <0 001 <0.001 I 

.. _ ------·· jLJ,n_·H_o_xa_n_• ____________ , __ o_o7___ --! -0-~7 r 

<0.01 I 

-J 

I 0.32 

Page 6 of 8 TPOR0146 
Emission Pt. 

EQT 0085 

LO 

EOT 0087 

ww 

EQT 0107 

OPE 

EOT 0108 

OPE OWS 

FUG 0002 

FE 

EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AI ID: 312 - Calumel Lubricants Co - Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-0001 O·V6 

Air· Title V Regular Permit Minor Mod 

Pollutant Avg lb/hr Max lblhr 

Benzene 0.004 0.004 

Ethyl benzene 0.01 0.01 

Toluene 0.03 0.03 

Xylene (mixed isomers) . 0.08 0.08 

n-Hexane O.Q1 0.01 

Benzene 0.92 0.92 

Ethyl benzene 0.03 0.03 

0.31 

Xylene (mixed isomers) 0.24 0.24 

Benzene 0.06 0.06 

Ethyl benzene 0.001 0.001 

Toluene 0.01 0.01 

Xylene (mixed isomers) 0.01 0.01 

n-Hexane 0.02 0.02 

Benzene 0.002 0.002 

Ethyl benzene <0.001 <0.001 

Toluene I <0.001 <0.001 

Xylene (mixed isomers) l <0.001 <0.001 

n-Hexane 0.001 0.001 

Benzene 0.07 0.07 

Cumene <0.001 <0.001 

Ethyl benzene 0.02 0.02 

Methyl isobutyl ketone <0.001 <0.001 

Tons/Year 

0.02 

0.05 

0.12 

0.35 

0.04 

4.03 

0.13 

--

1.36 

1.04 I 

0.25 

<0.01 

0.06 

0.02 

0.09 

0.01 

<0.01 i <0.01 I 

<0.01 I 

<0.01 

0.30 

<0.01 

0.07 

<0.01 

Naphthalene j <0.001 j

1 <0.001 <0.01 

f---------------·---- -------··- -----------~-------------1 

Xylene (mixed isomers) 

Toluene :._!1 ____ 

0

0 .. 1

1

5

7 

_______ 

1

1 __ 

0

0 .. 1

17

5 __ 

11

! __ 0o .. 

74~ _ ---~~· 

f-;;;;;;-=.-------·~ln_-H_e_x_a_n• _____ ------------. 0.56 ·r 0.56 r.. 2.47 I 

GRP 0010 Benzene Crud&-Cao 

GRP 0011 HEAVYCAP·1 

Cumene 

Ethyl benzene 

Ethyl benzene 

Toluene 

f---------------

Xylene (mixed isomers) 

Page 7 of 8 

0.02 0.08 

<0.001 <0.01 

<0.001 <0.01 

0.09 0.40 

0.05 0.20 

0.37 1.60 

TPOR0146 
EMISSION RATES FOR TAP/HAP & OTHER POLLUTANTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-V& 

Air- Title V Regular Permit Minor Mod 

 

1

- ---· ---------------· 

Emission Pt. 

1---

Pollutant 

···-----·-·· 

I 

., Avg lb/hr Max lb/hr Tons/Year 

I

GRP 0011 . HEAWCAP-1 

I GAP 0012 I HE.A\IY CAP·2 

i 

n-Hexano 

,Benzene 

[~thy1_ benzene 

iToluene 

0 23 

0.03 

0.05 

016 

i 1.00 . __ _j ______ ·-··-···-· _; 

010 

o;o __ __J . !·---------: 

I --------

o.1o 1 

I 

I 

r

0013 

!Xylene (ll"¥xed isomers) 

:n-Hexane 

! Ethyl benzene 

__ -_-----i_ - _-- ::: __ ~o~:-_-----+1 __ :_:_o_ 

----1- _ 0.001 1 <0.01 

! . 

iTolucnc <0.01 ' ""'"CAl' 

i 

!----------·----·--

!Xylene (mixed isomers) 

1-------· 

! o 001 1 --=---,-- 0004 __ +l_--_-- 0.02 

' 

GAP 0014 

VfRJHFR CloP 

GAP 0015 I NSPS K.b CAP 

I 

I 

I 

In-Hexane 

Elhy1 benzene 

Toluene 

Xylene (mixed 1somers) 

n-Hexane 

Bonze no 

Ethyl benzene 

IT~~cno 

I ·----

!Xylene (ll"¥xcd isomers) 

r :n-Hexane 

' ------;_;,_--nz_-~-.--_--_--__ _ 

Cumcnc 

------ -------

1 Elhy1 benzene 

--- Methyl isobutyt ketone 

-------------

\~~~~~~~~~--

!Toluene , I 

[~~~~ne ~~~~rs) 

[ ________ __ji_n_-_H_e_xane __ ---'-----

j_ 

I 

0 02 1 005 

0 01 O.Q2 

0003 001 

0 10 . ------1 

-·----__j, 

o 30 I 

002 

006 

.. ---------! 

0005 0 02 

-------. 0 02 0 11 

0 03 ; 

----! 

0 15 __ , 

0 13 i 060 

0.05 020 

6.17 

<0.01 

1.23 

-- --"j 

I <0.01 j 

---+----- -·- I 

1 <0 01 1 

r- 544 ___ j ___ _i_ -------· 

I I 6.s_ 5--=---1 -------j---

J ' -----~1 __ 4_.7_2 . 

Nole: Emission rates In bok:t are from attemate scenarios and are not Included In piNmltted totals unless otherwise noted in a footnote. Emission rates 

attributed to the UNF reflect the sum of the TAP/HAP limits of the lndlvldualemlaaioo p<Mnts (or ca.ps) under this permit, but do not constitute an 

emission cap. 

Page 8 of 8 Tf'CR014& 
EQT 0037 28 - 6,000 BBL VFR Storage Tank 

SPECIFIC REQUIREMENTS 

AI 10: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

I [40 CFR 60.116b(b)] Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the· life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)] . 

EQT 0038 29 - 50,000 BBL IFR Storage Tank 

2 [40. CFR 60.112b(a)(l )(i)) Equip with a fixed roof in combination with an internal floating roof. The internal floating roof shall rest or float on the liquid surface (but not 

necessarily in complete contact with it) inside a storage vessel that has a fixed roof. The internal floating roof shall be floating on the liquid 

surface at all times, except during initial fill and during those intervals when t~e storage vessel is completely.emptied or subsequentlY emptied 

and refilled. When the roof is resting on the leg suppo1:1s, the process of filling, emptying, or refilling shall be continuous and shall be 

accomplished as rapidly as possible. Subpart Kb. [40 CFR 60.112b(a)(l )(i)] 

3 [40 CFR 60.112b(a)(l)(ii)(A)] Equip internal floating roof with a liquid mounted seaLconsisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circumference of the tank. Subpart Kb. [ 40 CFR 60. I 12b(a)( I )(ii)(A)J 

4 [40 CFR 60.112b(a)(l )(ii)(B)] Equip internal floating roof with two seals mounted secondary above the primary so that each fonns a continuous closure that completely covers 

the space between the wall of the storage vessel and the edge of the internal floating roo[ The primary seal may be vapor-mounted, but both 

must be continuous. Subpart Kb. [40 CFR 60.1 I 2b(a)(l)(ii)(B)] 

5 [40 CFR 60.112b(a)(l)] Each opening in a noncontact internal floating roof except for automatic bleeder vents (vacuum breaker vents) and the rim space vents is to 

provide a projection below the liquid surface. Equip each opening in the internal floating roof except for leg sleeves, automatic bleeder vents, . 

rim space vents, column wells, ladder wells, sample wells, and slub drains with a cover or lid and maintain in a closed position at all times (i.e .• 

rio visible gap) except when the device is in actual use. Equip the cover or lid with a gasket. Bolt covers on each access hatch and automatic 

gauge float well except when they are in use. Equip automatic bleeder vents with a gasket and close at all times when the roof is floating except 

when the roof is being floated off or is being landed on the roof leg supports. Equip rim space vents with a gasket and set to open only when the 

internal floating roof is not floating or at the manufacturer's recommended setting. Each penetration of the internal floating roof for the purpose 

of sampling shall be a sample well. The sample well shall have a slit fabric cover that covers at least 90 percent of the opening. Each 

penetration of the internal floating roof that allows for passage of a column supporting the fixed roof shall have a flexible fabric sleeve seal or a 

gasketed sliding cover. Each penetration of the internal floating roof that allows for passage of a ladder shall have a gasketed sliding cover. 

Subpart.Kb. [40 CFR 60.112b(a)(l)] 

6 [40 CFR 60.113b(a)(l)] Tank roof and seals monitored by visual inspection/detennination at the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, and the secondary seal (if one is in service), prior to filling the storage vessel with VOL If there are holes, tears, or other openings 

in the primary seal, the secondary seal, or the_ seal fabric or defects in the internal floating roof, or both, repair the items before filling the storage 

vessel. Subpart Kb. [40 CFR 60.1 I 3b(a)(l )] 

Which Months: All Year Statistical Basis: None specified 

Page 1 of 49 TPOR0147 
-SPECIFIC-REQUIREMENTS -

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0038 29 - 50,000 BBL IFR Storage Tank 

7 [40CFR60.11Jb(a)(2)) 

8 [40 CFR 60.113b(a)(2)) 

9 [40 CFR 60.11Jb(a)(J)(i)) 

10 [40 CFR 60.11Jb(a)(3)(11)) 

II [40 CFR 60.11 lb(a)(4)) 

12 [40CFR60.11Jb(a)(4)J 

13 [40CFR60.11Jb(a)(5)) 

14 [40CFR60.115b(a)(l)) 

If the internal floating roof is not resting on the surface oft he VOL inside the storage vessel, or there is liquid accumulated on the roof, or the 

seal is detached, or there arc holes or tears in the seal fabric, repair the items or empty and remove the storage vessel from service within 45 days. 

If a failure that is detected during inspections required in this paragraph cannot be repaired within 45 days and.if the vessel cannot be emptied 

within 45 days, request a 30-day extension from DEQ m the inspection report required in 40 CFR 60.115b(a)(3). Document in the request for 

extension that alternate storage capacity is Wlavailable and specify a schedule of actions the company will take that will asswc that the control 

equipment will be repaired or lhe vessel will he emplied as soon as possible. Subpart Kb. (40 CFR 60.113b{a)(2)) 

Tank roof and seals monitored by visual inspcctionldctcnnination annually. Inspect the internal floating roof and the primary seal or the 

secondary seal (1f one is in service) through manholes and roof hatches on the fixed roof at least once every 12 months after initial filL If a 

failure is detected during inspections required in th1s parat.rraph initiate repair provisions. Subpart Kb. [40 CFR 60.113b(a)(2)] 

Which Months: All Year Statistical Rasis: l\"one spec1fled 

Tank roof and seals monilored by visual inspectlon/dctermmalion once every five years as specified in 40 CFR 60.113b(a)(4). Subpart Kb. (40 

CFR 60.113b(a)(3)(t)] 

Which Months: All Year Statistical Rasis: None specified 

Tank roof and seals mom lured by vtsual mspeclionidclerminalion annually as specified in 40 CFR 60.113b(a)(2) Subpart Kb. (40 CFR 

60.11 Jb(a)(J)(ti)) 

Which Months: All Y car Statistical Basis: None specified 

If the internal noating roof has defects. the primary seal has holes, tears, or other openings in the seal or the seal fabric. or the secondary seal has 

holes. tears, or other openings in the seal or the seal fabric. or the gaskets no longer close ofl the liquid swfaces from the atmosphere, or the 

sloned membrane has more than I 0 percent open area, repair the items as necessary So that none of the conditions specified in this paragr~ph 

exist before refilling the storage vessel with VOL In no event shall inspections conducted in accordance with this provision occw at intervals 

greater than 10 years in the case of vessels conductmg the annual visual inspection as specified in 40 CFR 60. 113b(a)(2) and (a)(3)(ii) and at 

intervals no greater than 5 years in lhe case of vessels spCCJiied in paragraph 40 CFR 60. I I lb(a)( J )( i) of this secuon. Subpart Kb. [40 CfR 

60.113b(a)(4)] 

Tank roof and seals monitored by visual inspcctionldctennination at the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, the secondary seal (if one is in service), gaskets, slotted membranes and sleeve seals (if any) each time the storage vessel is emptied 

and degassed. If a failure is detected dwing inspections required in this paragraph initiate repair provisions. Subpart Kb. [40 CFR 

60.113b(a)(4)) 

Which Months: All Y car Statistical Basis: None specified 

Submit notification in writing: Due at least 30 days pnor to the filling or refilling of each storage vessel for which an inspection is required by 

40 CFR 60.113b(a)(l) and (a)(4) to afford DEQ an opportunily lo have an observer presenl. lflhe inspcelion required by parab'Taph 40 CFR 

60.11 3b(a)(4) is not planned and the owner or operator could not have knOwn about the inspection 30 days in advance or refilling the tank, notify 

DEQ at least 7 days prior to the refilling of the storage vessel. Notify by telephone immediately followed by \loTitten documentation 

demonstrating why the mspcction wa.-. unplanned. Alternatively, submit notification in writing including the written documentation and send by 

express mail so that 11 is received by DEQ at leas! 7 days pnor to the refilling. Subpart Kb. (40 CFR 60.lllb(a)(5)) 

Submil a report: Due lo DEQ as an allachmenllo lhe notificalion required by 40 CFR 60.7(a)(3). Th1s report shall describe the control 

equipment and certify thallhe conlroi equtpment meets the specificalions of 40 CFR 60.112b(a)( I) and 60.11 Jb(a)( I). Keep coptes of all reports 

for at leas! two years. Subpart Kb. (40 CFR 60.115b(a)( I)) 

Page 2 ol49 TPQR01.c7 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-o0010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0038 29 - 50,000 BBL IFR Storage Tank 

15 [40CFR60.l15b(a)(2)) 

16 [40CFR60.115b(a)(3)) 

17 [40 CFR 60.115b(a)(4)] 

18 [40CFR60.116b(b)] 

!9 [40CFR60.116b(c)) 

20 [40 CFR 60.116b(d)] 

21 [LAC 33:I!L2103.B] 

22 [LAC 33:l!T.2103.C.I.a] 

23 [LAC 33:I!L2103.C] 

24 [LAC 33:l!T.2103.E.l] 

25 [LAC 33:1!1.2103.H.3] 

26 [LAC 33:l!T.2103.1] 

Inspection records recordkeeping by electronic or hard copy upon each occurrence of inspection, per 40 CFR 60.!!3b(a)(l) through (4). Each 

record shall identify the storage vessel on which the inspection was performed and shall contain the date the vessel was inspected and the 

observed condition of each component of the control equipment (seals, internal floating roof, and fittings). Keep copies of all records for at least 

two years. Subpart Kb. (40 CFR 60.115b(a)(2)] 

Submit a report: Due to DEQ within 30 days of the annual visual inspection required by 40 CFR 60.!13b(a)(2) that detects any of the conditions 

described in 4o CFR 60.113b(a)(2). Each report shall identify the storage vessel, the nature of the defects, and the date the storage vessel was 

emptied or the nature of and date the repair was made. Keep copies of all reports for at least two years. Subpart Kb. (40 CFR 60.115b(a)(3)] 

Submit a report: Due to DEQ within 30 days of each inspection required by 40 CFR 60.!13b(a)(3) that finds 

holes or tears in the seal or seal fabric, or defects in the internal floating roof, or other control equipment defects listed in 40 CFR 

60.113b(a)(3)(ii). The report shall identify the storage vessel and the reason it did not meet the specifications of 40 CFR 61.112b(a)(l) or 40 

CFR. 60.!13b(a)(3) and list each repair made. Keep copies of all reports for at least two years. Subpart Kb. (40 CFR 60.115b(a)(4)] 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an aflalysis showing' the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)] 

VOL storage data reCordkeeping by electronic or hard copy at the approved frequency. Records consist of the VOL stored,.the period of storage, 

and the maximum true vapor pressure of that VOL during'the respective storage period. Keep.copies of all records for at least two years ... 

Subpart Kb. (40 CFR 60.116b(c)] 

Submit notification: Due within 30 days when the maximum true vapor pressure of the liquid exceeds the respective maximum true vapor 

pressure values for each volume range. Subpart Kb. [40 CFR 60.116b(d)] 

Equip with a submerged fill pipe. 

Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

Wall of the storage vessel and the floating roof continuously around the circumference of the tank 

Equip with an internal floating roof consisting of a pontoon type roof, double deck roof, or internal floating cover which will rest or float on the 

surface of the liquid c~ntents and is equipped with a closure seal to close the space between the roof edge and tank wall'. All t~nk gauging and 

sampling devices will be gas-tight except when gauging or sampling is taking place. 

VOC, Total>= 95% control efficiency using a vapor loss control system. This limitation does not apply during periods of planned rqutine 

maintenance which may not exceed 240 hours per year. 

Which Months: All Year Statistical Basis: None specified 

Determine VOC maximum true vapor pressure using the methods in LAC 33:1!1.21 03.H.3.a-e. 

Equiprilent/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency. Keep records of the information 

specified in LAC 33:111.2103.1.1 - 7, as applicable. · 

EQT 0040 30 - 6,500 BBL VFR Storage Tank 

27 [40CFR60.116b(b)] Equipment/operational data recordkeeping by electronic or har~ copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.!!6b(a). Subpart Kb. (40 CFR 60.116b(b)] 

Page 3 of 49 TPOR0147 
·- SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-{)0010-V& 

Alr- Title V Regular Permit Minor Mod 

EQT 0042 32 - 20,000 BBL VFR Storage Tank 

28 [40 CFR 60.116b(b)j Equipment/operational data rccordkeeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpan Kb. [40 CFR 60.116b(b)] 

EQT 0043 33 - 20,000 BBL IFR Storage Tank 

29 [40 CFR 60.112a(a)(2)} 

30 [40CFR60.115aj 

31 [LAC 33:111.2103.!!} 

32 [LAC lliii.2103.BI 

33 [LACJ31112103CJ 

34 [LAC lliii2103.E I} 

35 [LAC ll:III.2103.H.3 J 

36 [LAC 33:111.21031} 

Equip with a fixed roof and an internal floating type cover having a continuous Closwe device between the tank wall and the cover edge. The 

cover is to be floating at all times, (i.e., ofT the leg supports) except during initial fill and when the tank is completely emptied and subsequently 

refilled. The process of emptying and refilling when the cover is resting on the leg supports shall be continuous and shall be accomplished as 

rapidly as possible. Each opening in the cover except for automatic bleeder vents and the rim space vents is to provide a proJection below the 

.liquid surface. Equip each opening in the cover except for automatic bleeder vents, rim space vents, stub drains and leg sleeves wtth a cover, 

seal, or lid and maintain in a closed position at all times (i.e., no visible gap) except when the device is in actual usc. Close automatic bleeder 

vents at all times when the cover is floating except when the cover is being floated ofT or is being landed on the leg support.;;. Set rim vents to 

open only when the cover is being floated ofT the leg supports or at the manufacturer's recommended setting. Subpart K.a. (40 CFR 

60.112a(a)(2)] 

Petroleum liquid storage data recordkeeping by electronic or hard copy at the approved frequency. Maintain a record of the petroleum liquid 

stored, the period of storage, and the maximum true vapor pressure of that liquid during the respective storage period,' except as provided m 40 

CFR 60.1 IS a( d). Subpan Ka. 

Equip with a submerged fill pipe. 

Maintain working pressures sufficient at all times under normal operating conditions to prevent vapor or gas loss to the atmosphere. 

Equip with an internal floating roof consisting of a pontoon type roof, double deck roof, or internal floating cover which will rest or float on the 

surface of the liquid contents and is equipped with a closure seal to close the space between the roof edge and tank wall_ All tank gauging and 

sampling devices will be gas-tight except when gauging or sampling is taking place. 

VOC. Total > .. 95 %control efftctency using a vapor loss control system. This limitation docs not apply during periods of planned routine 

maintenance which may not exceed 240 hours per year. 

Which Months: All Year Statistical Basis: None specified 

Determine VOC maximum true vapor pressure using the methods iO LAC 33:1li.2103.H.3.a-e. 

Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency. Keep records of the information 

specified in LAC 33:111.21 03.l.i - 7. as applicable. 

EQT 0047 47 - 80,000 BBL IFR Storage Tank 

37 [40 CfR 60 112b(a)(l)(i)j Equip with a fixed roof in combination with an internal noating roof. The internal floating roof shall rest or float on the liquid surface (but not 

necessarily in complete contact with it) inside a storage vessel that has a fixed roof. The internal floating roof shall be floating on the liquid 

~urface al all times, except during iniual fill and during those intervals when the storage vessclts completely emptied or subsequently emptied 

and refilled. When the roof is resting on the leg suppons, the process of filling, emptying, or refilling shall be continuous and shall be 

accomphshed as rapidly as possible. Subpan Kb. [40 CFR 60.il2b(a)(l)(i)] 

Page 4 of 49 TPOR0141 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 • 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0047 47- 80,000 BBL IFR Storage Tank 

38 [40 CFR 60.112b(a)(J)(ii)(A)) Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circumference of the tank. Subpart Kb. [40 CFR 60.112b(a)(l )(ii)(A)] 

39 [40 CFR 60.112b(a)(l )(ii)(B)) Equip internal floating roof with two seals mounted secondary above the primary so that each forms a continuous closure that completely covers 

the space between the wall of the storage vessel and the edge of the internal floating roof. The primary seal may be vapor-mounted, but both 

must be continuous. Subpart Kb. [40 CFR 60.112b(a)(I)(ii)(B)] 

40 [40 CFR 60.112b(a)(l )] Each opening in a noncontact internal floating roof except for automatic bleeder vents (vacuum breaker vents) and the rim space vents is to 

provide a projection below the liquid surface. Equip each opening in the internal floating roof except for leg sleeves, automatic bleeder vents, 

rim space vents, colU11U1 wells, ladder wells, sample' wells, and stub drains with a cover or lid and maintain in a closed posit~on at all tim~s (i.e., 

no visible gap) except when the device is in actual use. Equip the cover or lid with a gasket. Bolt covers on each access hatch and automatic 

gauge float well except when they are in use. Equip automatic bleeder vents with a gasket and close at all times when the roof is floating except 

when the roof is being floated off or is being landed on the roof leg supports .. Equip rim space vents with a gasket and set to open only when the 

internal floating roof is not floating or at the manufacturer's recorrunended setting. Each penetration of the internal floating roof for the purpose 

of sampling shall be a sample well. The sample well shall have a slit fabric cover that covers at least 90 percent of the opening. Each 

penetration of the internal floating roof that allows for passage of a column supporting the fixed roof shall have a flexible fabric sleeve seal or a 

gasketed sliding cover. Each penetration of the internal floating roof that allows for passage of a ladder shall have a gasketed sliding cover. 

Subpart Kb. [40 CFR 60.112b(a)(I )] 

41 [40 CFR 60.113b(a)(l}] Tank roof and seals monitored by visual inspection/determination at the regulation's specified frequency. Inspect the internal floating roof. the 

primary seal, and the secondary se31 (if one is in service), prior to filling the storage vessel with VOL. If there are holes, tears, or other openings 

in the primary seal, the secondary seal, or the seal fabric or defects in the internal floating roof, or both, repair the items before filling the storage 

vessel. Subpart Kb. [40 CFR 60.113b(a)(l)] 

Which Months: All Year ·Statistical Basis: None specified 

42 [40 CFR 60.113b(a)(2)] ·If the internal floating roof is not resting on the surface of the VOL inside the storage vessel, or there is liquid accumulated on the roof, or the 

seal is detached, or there are holes or tears in the seal fabric, repair the items or empty and remove the storage vessel from service within 45 days. 

If a failure that is detected during inspections required in this paragraph cannot be repaired within 45 dayS and if the vessel cannot be emptied 

within 45 days, request a 30-day extension from DEQ in the inspection report required in 40 CFR 60.115b(a)(3). Document in the request for 

extension that alternate storage capacity is unavailable and specify a schedule of actions the company will take that will assure that the control 

equipment" will be repaired or the vessel will be emptied as soon as possible. Subpart Kb. [40 CFR 60.113b(a)(2)] 

43 [40 CFR 60.113b(a)(2)) Tank roof and seals monitored by visual inspection/determination annually. Inspect the internal floating roof and the primary seal or the 

secondary seal (if one is in service) through manholes and roof hatches on the fixed roof at least once every 12 months after initial fill. If a 

failure is detected during inspections required in this. paragraph initiate repair provisions. Subpart Kb. [40 CFR 60.113b(a)(2)] 

Which Months: All Year Statistical Basis: None specified · 

44 [40 CFR 60.113b(a)(3)(i)) Tank roof and seals monitored by visual inspection/determination once every five years as speCified in 40 CFR 60.113b(a)(4). Subpart Kb. [40 

CFR 60.113b(a)(3)(i)] 

Which Mo.nths: All Year . Statistical Basis: None specified. 

45 [40 CFR 60.113b(a)(3)(ii)) Tank roof and seals monitored by visual inspection/determination annually as specified in 40 CFR 60.113b(a)(2). Subpart Kb. [40 CFR 

60.113b(a)(3)(ii)] 

Which Months: All Year Statistical Basis: None specified 

Page 5 of 49 TPOR0147 

' 

/ 
SPECIFIC REQUIREMENTS 

AIID: 312 -Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air- Title V Regular Permit Minor Mod 

 

EQT 0047 47 - 80,000 BBL IFR Storage Tank 

46 (40 CFR 60.lllb(a)(4)] 

47 (40 CFR 60.lllb(a)(4)] 

48 [40 CFR 60.11 lb(a)(S)] 

49 [40 CFR 60.115b(a)( I)] 

50 [40 CFR 60.115b(a)(2)] 

51 (40 CFR 60.115b(a)(l)] 

52 [40 CFR 60.115b(a)(4)] 

53 [40 CFR 60.116b(b)] 

If the internal floating roof has defects, the primary seal has holes, tears, or other openings in the seal or the seal Iabrie, or the secondary seal has 

holes, tears, or other openings in the seal or the seal fabric, or the gaskets no longer close ofT the liquid surfaces from the atmosphere, or the 

stoned membrane has more than I 0 percent open area, repair the items as necessary so that none of the conditions specifted in this paragraph 

exist before refilling the storage vessel with VOL In no event shall mspections conducted in accordance with this provision occur at intervals 

greater !han 10 years in lhe case of vessels conducting lhe annual visual inspection as specified in 40 CFR 60.113b(a)(2) and (a)(3)(ii) and al 

intervals no greater !ban 5 years m lhe case of vesselsspecified in paragraph 40 CFR 60.113b(a)(3)(i) of this section. Subpart Kb. [40 CFR 

60.113b(a)(4)] 

Tank roof and seals monitored by visual inspection/determination at the regulation's specified frequency. Inspect the internal lloating roof, the 

primary seal, the secondary seal (if one is in service), gaskets, slotted membranes and sleeve seals (if any) each time the storage vessel is emptied 

and degassed. I fa failure is detected during inspections required in this paragraph initiate repair prov1sions. Subpart Kb. !40 CFR 

60.113b(a)(4)] 

Which Months: All Year Statistical Basis: None specif1ed 

Submit notification in writing: Due at least 30 days prior to the fill.ing or refilling of each storage vessel for which an inspection is required by 

40 CFR 60.113b(a)(l) and (a)(4) lo afford DEQ an opportunity 10 have an observer present lflhe inspection required by paragraph 40 CFR 

60.113b(a)(4) is not planned and the owner or operator could not have known about the inspection 30 days in advance or refilling the tank, notify 

DEQ at least 7 days prior to the refillmg of the storage vessel. ~oufy by telephone immediately followed by wrincn documentation 

demonstrating why the inspection was unplanned. Alternatively, submit notification in writing including the written dOcumentation and send by 

express mali so lhal il is received by DEQ alleasl 7 days prior 10 the refilling. Subpart Kb. [40 CFR 60.113b(a)(5)] 

Submit a report: Due to DEQ as an anachment to the notification reqmred by 40 CFR 60.7(a)(3). This report shall describe the control 

eqmpmenl and certify lhallhe control equipment meels lhe spcc1fical!Ons of 40 CFR 60.112b(a)( I) and 60.113b(a)( I). Keep copies of all reporl.< 

for al leasllWo years. Subpart Kb. [40 CFR 60.115b(a)( I)] 

Inspection records recordkecping by electronic or hard copy upon each occurrence of inspection, per 40 CFR 60.1 I 3b(a)( 1) through (4): Each 

record shall identify the storage vessel on which the inspection was performed and shall contain the date the vCssel was inspected and the 

observed condition of each component of the control equipment (seals, internal noating roof. and fittings). Keep copies of all records for at least 

two years. Subpart Kb. [40 CFR 60.115b(a)(2)] 

Submit a report: Due lo DEQ wnhin 30 days oflhe annual visual inspection reqUired by 40 CFR 60.113b(a)(2) !hal deleciS any oflhe condillons 

described in 40 CFR 60.113h(a)(2). Each report shall identify the storage vessel, the nature of the defects, and the dale the storage vessel was 

emptied or lhe nature of and dale lhe repair was made. Keep copies of all reports for al leas! lwo years. Subpart Kb. [40 CFR 60.115b(a)(3)] 

Submit a report: Due lo DEQ within 30 days of each inspection required by 40 CFR 60.113b(a)(3) lhal finds 

holes or tears in the seal or seal fabric, or defects in the internal floating roof, or other control equipment dCfects listed in 40 CFR 

60.113b(a)(3)(ii). The report shall identify lhe storage vessel and the reason 11 did nol meel lhe specifications of 40 CFR 61.112b(a)( I) or 40 

CFR. 60.113b(a)(3) and list each repair made. Keep copies of all reports fo~ al leas! lwo years. Subpart Kb. [40 CFR 60.115b(a)(4)] 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vesseL Keep copies of all records for the life of the so wee as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)] 

Page 6 C?f 49 TPQA01 .. 7 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 • 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0047 47- 80,000 BBL IFR Storage Tank 

54 [40 CFR 60.116b(c)] 

55 [ 40 CFR 60.116b(d)] 

56 [LAC 33:111.2103.8] 

57 [LAC 33:111.21 03.C.I.a] 

58 [LAC 33:111.2103.CJ 

59 [LAC 33:lii.2103.E.I] 

60 [LAC 33:lii.2103.H.3] 

61 [LAC 33:111.21 03.1] 

VOL storage data recordkeeping by electronic or hard copy at the approved frequency. Records consist of the VOL stored, the period of storage, 

and the maximum true vapor pressure of that VOL during ·the respective storage period. Keep copies of all records for at least two years. 

Subpart Kb. [40 CFR 60.116b(c)] 

Submit notification: Due within 30 days when the maximum true vapor pressure of the liquid exceeds the respective maximum true vapor 

pressure values for each volume range. Subpart Kb. [40 CFR 60.116b(d)] 

Equip with a submerged fill pipe. 

Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wan of the storage vessel and the floating roof continuously arowtd the circumference of the tank. 

·Equip with a~ internal floating roof consisting of a pontoon 'type ·roof, 'dOuble deck roof, or internal floating cover which will rest or float on the 

surface of the liquid contents and is equipped with a closure.seal to close the space between the roof edge and tank wall. All tank gauging and 

sampling devices will be gas-tight except when gauging or sampling is taking place. ..... 

VOC, Total>= 95% control efficiency using a vapor loss control system. This limitation does not apply during periods of planned routine 

maintenance which may not exceed 240 hours per year. 

Which Months: All Year Statistical Basis: None specified . 

Determine VOC maxirnu~ true vapor pr~ssure using the methodS in LAC 33:III.2103.H.3.a-e. 

Equipment/operational data recordkeeping by electronic or h_ard copy at the regulation's specified frequency. Keep records ofthc information 

. specified in LAC 33:III.2103.1.1 -7, as applicable. 

"'· J,, 

EQT 0049 54- 10,000 BBL IFR Storage Tank 

62 [40 CFR 60.112b(a)( I )(i)] Equip with a fixed roo fin combination with an internal floating roof. The internal floating roof shall rest or float on the liquid surface (but not 

necessarily in complete contact with it} inside a storage vessel that has a fixed roof. The internal flOating roof shall be floating on the liquid 

surface at all times, except during initial fill and during· those intervals when the storage vessel is completely emptied or subsequently emptied 

and refilled. When the roof is resting on the leg supports, the process of filling, emptying, or refilling shall be continuous and shall be 

accomplished as rapidly as possible. Subpart Kb. [40 CFR 60.112b(a)(l)(i)] 

63 [40 CFR 60.112b(a)(l)(ii)(A)] Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circumference of the tank. Subpart Kb. [40 CFR 60. I I 2b(a)(l )(ii)(A)] 

64 [40 CFR 60.112b(a)(l)(ii)(B)J Equip internal floating roof with tWo se~ls mounted secondary above the primary so that each forms a continuous closure that completely covers 

the space between the wall of the storage vessel and the edge of the internal floating roof. The primary seal may be vapor-molfnted. but both 

must be continuous. Subpart Kb. [40 CFR 60.112b(a)(l )(ii)(B)] 

Page 7 of 49 TPOR0147 
- -SPECIFIC .REQUIREMENTSAIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0049 54- 10,000 BBL IFR Storage Tank 

65 (40 CFR 60.112b(a)(I)J 

66 (40 CFR 60.11lb(a)(I)J 

67 [40CFR 60.11lb(a)(2)J 

68 (40 CfR 60 lllb(a)(2)) 

69 (40 CfR 60.113b(a)(3)(1)) 

70 [40 CFR 6U.IIlb(aXJXii)J 

Each opening in a noncontact internal floating roof except for automatic bleeder vent.:; (vacuwn breaker vents) and the urn space vents is to 

provide a projection below the liquid surface. Equip each opening in the mtcmal floating roof except for leg sleeves, automatic bleeder vents, 

nm space vents, column wells, ladder wells, sample wells, and stub drains with a cover or lid and maintain in a closed position at all times (i.e., 

no visible gap) except when the device is in acrual use. Equip the cover or lid with a gasket. Bolt covers on each access hatch and automatic 

gauge float well except when they are in usc. Equip automatic bleeder vents with a gasket and close at all times when the roof is floating except 

when the roof is being floated off or is being landed on the roof leg supports. Equip rim space vents with a gasket and set to open only when the 

internal floatmg roof is not floating or at the manufacturer's recommended setting_ Each penetration of the internal floating roof for the purpose 

of Sampling shall be a sample welL The sample well shall have a slit fabric cover that covers at least 90 percent of the opening_ Each 

penetration of the internal floatmg roof that allows for passage of a column supporting the fixed roof shall have a flex1ble fabric sleeve seal or a 

gasketed sliding cover. Each penetration of the internal floating roof that allows for passage of a ladder shall have a gaskcted shding cover 

Subpart Kb. (40 CFR 60.!!2b(a)(! )) 

Tank roof and seals monitored by visual inspection/determination at the_ regulation's specified frequency. Inspect the mtcrnal floatmg roof, the 

prima:ry seal, and the secondary seal {if one is in service). prior to filling the storage vessel with VOL. If there arc holes, tears. or other openings 

in the primary seal, the secondary seal, or the seal fabric or defects in the intemal floating roof, or both, repair the items before filhng the storage 

vessel. Subpart Kb. [40 CFR 60.!!3b(a)(l )) 

Which Months: All Year Statistical Basis: None specified 

If the internal floating roof is not resting on the surface of the VOL inside the storage vessel. or there is liquid accumulated on the roof. or the 

scal1s detached, or there are holes or tears in the seal fabric, repair the items or emply and remove the storage vessel from scrv1cc within 45 days. 

If a failure that IS detected during mspections required in this paragraph cannot be repaued within 45 days and 1f the vessel cannot be empt1ed 

wlthm 45 days. request a 30·day extension from DEQ in the mspection report required 10 40 CFR 60. I I 5b(a)(3). Document m the request for 

extension that alternate storage capacity is unavailable a:nd specify a schedule of actions the company will take that will assure that the control 

eqlllpmenl Will be repaired or the vessel will be emplicd as soon as pomble. Subpart Kb (40 CFR 60.1!3b(a)(2)] 

Tank roof and seals monitored by visual inspectionldctennination annually. Inspect the internal floating roof and the primary seal or the 

secondary seal (if one is in service) through manholes and roof hatches on the fixed roof at least once every I 2 months after initial fill · If a 

failure is detected during inspections required in this paragraph imtiate repair provisions. Subpan Kb. [40 C.FR 60.11 Jb(a)(2) J 

Which Months: All Year Statisucal Basis: None specified 

Tank roof and seals monitored by v1sual inspccllon/dclcrminalion once every five years as specified in 40 CFR 60.!13b(a)(4). Subpart Kb. (40 

CFR 60.113b(a)(3)(i)] 

Which Months: All Year Statistical Basis: !\:one specified 

Tank roof and seals moni10red by visual inspecllon/delermination annually as specified in 40 CFR 60.!!3b(a)(2). Subpart Kb. (40 CFR 

60.113b(a)(3)(ii)] 

Which Months: All Y car Statistical Bas1s: None specified 

Page 8 of 49 TPOA0147 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

' Activity Number: PER20120002 

Permit Number: 3080-Q0010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0049 54- 10,000 BBL IFR Storage Tank 

71 [40 CFR 60.113b(a)(4)) 

72 [40 CFR 60.113b(a)(4)) 

73 [40 CFR 60.11Jb(a)(5)) 

74 [40 CFR 60.115b(a)(l)) 

75 [ 40 CFR 60.115b(a)(2)) 

76 [40 CFR 60.115b(a)(J)) 

77 [40 CFR 60.115b(a)(4)) 

78 [40 CFR 60.116b(b)) 

If the internal floating roof has defects, the primary seal has holes, tears, or other openings in the seal or the seal fabric, or the secondary seal has 

holes, tears, or other openings in the seal or the seal fabric, or the gaskets no longer close offthe.liquid surfaces from the atmosphere, or the 

slotted membrane has more than I 0 percent open area, repair the items as necessary so that none of the conditions specified in this paiagraph 

exist before refilling the storage vessel with VOL. In no event shall inspections .conducted in accordance with this provision occur at intervals 

greater than 10 years in the case of vessels conducting the annual visual inspection as specified in 40 CFR 60.!13b(a)(2) and (a)(3)(ii) and at 

intervals no greater than 5 years in the case of vessels specified in paragraph 40 CFR 60.113b(a)(J)(i) of this section. Subpart Kb. [40 CFR 

60.113b(a)(4)] 

Tank roof and seals monitored by visual inspectionldetennination at the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, the secondary seal (if one is in service), gaskets, slotted membranes and sleeve seals (if any) each time the storage vessel is emptied 

and degassed. If a failure is detec~ed during inspections required in this pa~agraph initiate repair provisions. Subpart Kb. [40 CFR 

60.!!3b(a)(4)] 

Which Months: All Year Statistical Basis: None specified . . 

Submit notification in writing: Due at least 30 days prior to the filling'or refilling of each storage vessel for which an inspection is required by 

40 CFR 60.113b(a)( I) and (a)( 4) to afford DEQ an opportunity to have an observer present. If the inspection required by paragraph 40 CFR 

60.1!3b(a)(4) is not planned and the owner or operator could not have known about the inspection 30 days in advance or refilling the tank, notifY 

bEQ at least 7 days prior to the refilling of the storage vessel. 1'J'otify by telephone immediately followed by written documentation 

demonstrating why the inspection was unplanned. Alternatively, submit notification in writing including the written documentation and send by 

express mail so that it is received by DEQ at least 7 days prior to the refilling. Subpart Kb. [40 CFR 60.!!3b(a)(5)] 

Submit a report: Due to DEQ as an attachment to the notification required by 40 CFR 60.7(a)(3). This report shall describe the control 

equipment and certifY that the control equipment meets the specifications of 40 CFR 60.!!2b(a)(l) and 60.113b(a)(l ). Keep copies of all reports 

for at least two years. Subpart Kb. [40 CFR 60.115b(a)(!)] '· 

Inspection records recordkeeping by electronic or hard copy upon each occurrence of inspection, per 40 CFR 60.113b(a)(l) through (4). Each 

record shall identify the storage vessel on which the inspection .was performed and shall contain the date the vessel was inspected and the 

observed condition of each component of the control equipment (seals, internal floating roof, and fittings). Keep copies of all records for at least 

two years. Subpart Kb. [40 CFR 60.115b(a)(2)] · 

Submit a report: Due to DEQ within 30 days of the annual visual inspection required by 40 CFR 60.113b(a)(2) that detects any of the conditions 

described in 40 CFR 60.113b(a)(2). Each report shall identifY the storage vessel, the nature of the defects, and the date the slorage vessel was 

emptied or the nature of and date the repair was made. Keep copies of all reports for at least two years. Subpart Kb. [40 CFR 60.115b(a)(3)] 

Submit a report: Due to DEQ within 30 days of each inspection required by 40 CFR 60.113b(a)(3) that finds 

holes or teafs in the seal o,r seal fabric, or defects in the internal floating roof, or other control equipment defects listed in 40 CFR 

60.113b(a)(3)(ii). The report shall identifY the storage vessel and the reason it did not meet the specifications of 40 CFR 6!.!12b(a)( I) or 40 

CFR. 60.113b(a)(3) and list each repair made. Keep copies of all reports for at least two years. Subpart Kb. [40 CFR 60.115b(a)(4)] 

Equipment/operational data recordke~ping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all recordS for the life of the source as 

specified by 40 CFR 60.!!6b(a). Subpart Kb. [40 CFR 60.116b(b)] 

Page 9 of 49 TPOR0147 
SPECIFIC REQUIREMENTS 

AIID: 312 -Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-V& 

Air- Title V Regular Permit Minor Mod 

EQT 0049 54- 10,000 BBL IFR Storage Tank 

79 [40 CFR 60.116b(c)] 

80 [40 CFR 60.116b(d)] 

81 [LAC 33:111.2103.8] 

82 (LAC 33:111.2103.C.J.a] 

83 (LAC Jl"lll2103 C] 

84 (LAC 33:111.2103.£ 1 I 

85 [LAC 33:111.2!03.H.3] 

86 [LAC 33111.21031] 

VOL storage data rccordkecping by electronic or hard copy at the approved frequency. Records consist of the VOL stored, the period of storage, 

and the maximum true vapor pressure of that VOL during the respective storage period. Keep copies of all records for at least two years. 

Subpart Kb.(40 CFR 60.116b(c)] 

Submit notification: Due within 30 days when the f!ta:<imum true vapor pressure of the liquid exceeds the respective maximum hUe vapor 

pressure values for each volume range. Subpart Kb. [40 CFR 60.1 16b(d)] 

Equip with a submerged fill pipe. · 

Equip internal noating roof with a liqmd mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circumference of the tank. 

Equip with an internal floatmg roof consisting of a pontoon type roof, double deck roof, or internal floating cover which will rest or float on the 

surface of the hquid contents and is equipped with a closure seal to close the space bctv.·ecn the roof edge and tank wall. All tank gaugmg and 

sampling devices will be gas-tight except when gauging or sampling JS taking place. 

VOC, Total >= 95 %control efficiency using a vapor loss control system. This limitation docs not apply during periods of planned routine 

maintenance which may not exceed 240 hours per year. 

Which Months: All Year Statistical Basis: ~one specified 

Determine VOC maximum true vapor pressure using. the methods in LAC 33:ll1.2103.11.3.a-e. 

Equipment/operational data recordkeeping by electronic_ or hard copy at the regulation's specified frequency. Keep records of the information 

speCified in LAC 33:111.2103.1.1 - 7. as applicable. 

EQT 0050 55- 10,000 BBL IFR Storage Tank 

87 [40 CFR 60.112b(a)( I )(i)] Equip with a fixed roof in combination with an internal floating roof. The internal floating roof shall rest or float on the liquid surface (but not 

necessarily in complete contact with it) inside a storage vessel that has a fixed roof. The internal floating roof shall be floating on the liquid 

surface at all times, except during initial fill and during those intervals when the storage vessel is completely emptied or subsequently emptied 

and refilled. When the roof is resting on the leg supports, the process of filling, emptying, or refilling shall be continuous and shall be 

. accomplished as rapidly a.• pombie. Subpart Kb. [40 CFR 60. I 12b(a)( I )(i)] 

88 [40 CFR 60.112b(a)(l)(•i)(A)] Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in conlact with the liquid between the 

wail of the storage vessel and the floaling roof continuously around !he circumference oflhe lank. Subpart Kb. [40 CFR 60. I 12b(a)(l )(ii)(A)] 

89 [40 CFR 60.112b(n)( l)(ii)(B)) Equip intcm_al floating roof with two seals mounted secondary above the primary so that each forms a continuous closure that completely covers 

the space between the wall of the storage vessel and the edge of the internal floating roof. The primary seal may be vapor-mounted, but both 

musl be conlinuous. Subpart Kb. [40 CFR 60.1 12b(a)( l)(ii)(B)] 

Page 10 of 49 rPQR01~1 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS. 

Air- Title V Regular Permit Mi.nor Mo~ 

EQT 0050 55- 10,000 BBL IFR Storage Tank 

90 [40 CFR 60.112b(a)(ll] 

91 [40CFR60.113b(a)(l)] 

92. [40 CFR 60.113b(a)(2)] 

93 [40 CFR 60.113b(a)(2)] 

94 [40 CFR 60.113b(a)(3)(i)] 

95 . · [40 CFR 60.113b(a)(3)(ii)] 

Each opening in a noncontact internal floating roof except for automatic' bleeder vents (vacuum breaker ven~s) and the rim space vents is to 

provide a projection below the liquid surface. Equip each opening in the internal floating roof except for leg sleeves, automatic bleeder vents, 

rim space vents, column wells, ladder wells, sample wells, and stub drains with a cover or lid and maintain in a closed position at all times (i.e., 

no visible gap) except when the device is in actual use. Equip the cover or lid with a gasket. Bolt covers on each access hatch and automatic 

gauge float well except when they are in.use. Equip automatic bleeder vents with a gasket and close at all times when the roof is floating except 

when the roof is being floated off or is being landed on the roof leg suppOrts. Equip rim space vents with a gasket and set to open only When the 

internal floating roof is .not floating or at the manufacturer's recommended setting. Each penetration of the internal floating roof for the purpose 

of sampling shall be a sample well. The sample well shall have a slit fabric cover that covers at least 90 percent of the opening. Each 

penetration of the internal floating roof that allows for passage of a column supporting the fixed roof shall have a flexible fabric sleeve seal or a 

gasketed sliding cover. Each penetration of the internal floating roof that allows for passage of a ladder shall have a gasketed sliding cover. 

Subpart Kb. [40 CFR 60.112b(a)(l)] 

Tank roof and seals monitored by visual inspection/determination at the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, and the secondary seal (if one is in service), prior to filling the storage vessel with VOL. If there are holes, tears, or other openings 

in the primary seal, the secondary seal, or the seal fabric or defects in the internal floating roof, or both, repair the items before filling the storage 

vessel. Subpart Kb. [40 CFR 60.113b(a)(l)] 

Which Months: All Year Statistical Basis: None specified 

If the internal floating roof is not resting on the surface of the VOL inside the storage vessel, or there is liquid accumulated on the roof, or the 

seal is detached, or there are holes or tears in the seal fabric, repair the items or empty and remove the storage vessel from service within 45 days. 

If a failure that is detected during inspections required in this paragraph cannot be repaired within 45 days and if the vessel cannot be emptied 

within 45 days, request a 30-day extension from DEQ in the inspection report required in 40 CFR 60.115b(a)(3). Document in the request for 

extension that alternate storage capacity is unavailable and specify a schedule of actions the company will take that will assure that the control 

equipment will be repaired or the vessel will be emptied ~s soon as possible. Subpart Kb. [40 CFR 60.113b(a)(2)] 

Tank roof and seals monitored by visual inspection/determination annually. Inspect the internal floating roof and the primary seal or the 

secondary seal (if one is in service) through manholes and roof hatches on the fixed roof at least once every 12 months after initial fill. If a 

failure is detected during inspections required in this paragraph initiate repair provisions. Subpart Kb. [40 CFR 60.113b(a)(2)] 

Which Months: All Year Statistical Basis: None specified 

Tank roof and seals monitored by visuaUnspectionidetermination once every five years as specified in 40 CFR 60.113b(a)(4). Subpart Kb. [40 

CFR 60.113b(a)(3)(i)] . 

Which Months: All Year Statistical Basis: None specified 

Tank roof and seals monitored by visual inspection/determination annually as specified in 40 CFR 60.113b(a)(2). Subpart Kb. [40 CFR 

60.113b(a)(3)(ii)] 

Which Months: All Year Statistical Basis: None specified , 

Page 11 of49 TPOR0147 
SPECIFIC REQUIREMENTS 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002· 

Permit Number: 3080-00010·V6 

Air· Title V Regular Permit Minor Mod 

EQT 0050 55 ·10,000 BBL IFR Storage Tank 

96 (40CFR60,11lb(a)(4)] 

97 (40 CFR 60 113b(a)(4)] 

98 (40 CFR 60.113b(a)(5)] 

99 (40CFR60.115b(a)(l)] 

100 [40CFR60.11Sb(a)(2)] 

101 (40 CFR 60.11Sb(aX3)] 

102 (40CFR60.11Sb(a)(4)] 

103 [40CFR60.116b(b)] 

If the internal floatmg roof has defects, the primary seal has holes, tears, or other openings in the seal or the seal fabric, or the secondary seal ha<> 

holes, tears, or other openings in the seal or the seal fabric, or the gaskets no longer close ofT the liquid surfaces from the atmosphere, or the 

slotted membrane has more than I 0 percent open area, repair the items as necessary so that none of the conditions specified in this paragraph 

exist before refilling the storage vessel with VOL In no event shall inspections conducted in accordance with this provision occur at intervals 

greater than 10 years in the case of vessels conductmg the annual visual inspection as spec1fied m 40 CFR 60.1 i3b(a)(2) and (a)())(li) and at 

intervals no greater than 5 years in the case of vessels specified in paragraph 40 CFR 60.113b(a)(3)(i) of this section. Subpart Kb. (40 CFR 

60.113b(a)(4)J 

Tank roof and seals monitored by visual inspection/determination at the regulation's specified frequency. lrL'ipect the internal floating roof, the 

primary seal, the secondary seal (if one is in service), gaskets, slorted membranes and sleeve seals (if any) each time the storage vessel is emptJcd 

and degassed. If a failure is detected during inspections required in this paragraph initiate repair provisions. Subpart Kb. [40 CFR 

60.113b(a)(4)) 

Which Months: All Year Statistical Basis: None specified 

Submit notification in writing: Due at least 30 days prior to the filling or refilling of each storage vessel for which an inspection is required by 

40 CFR 60.113b(a)( I) and (a)(4) to afford DEQ an opporrunity to have an observer present. If the mspection reqmred by paragraph 40 CFR 

60. I 13b(a)(4) is not planned and the owner or operator could nOt h3vc known about the inspection 30 days in advance or refilling the tank. notifY 

DEQ at least 7 days prior to the refilling of the storage vesseL !':otify by telephone immediately followed by wrinen documentation 

demonstrating why the inspection VIaS unplanned. Alternatively. submit notification in writing including the wrinen documentation and send by 

express mail so that it is received by DEQ alleast 7 days prior to the refilling. Subpart Kb. (40 CFR 60.113b(a)(5)) 

Submit a report: Due to DEQ as an anachment to the notification required by 40 CfR 60.7(a)(3). This report shall describe the control 

equipment and certify that the control equipment meet< the specificallons of 40 CFR 60.112b(a)( I) and 60.113b(a)( I). Keep cop1es of all reports 

for at leas I lwo years. Subpart Kb. (40 CFR 60.115b(a)( I)) 

Inspection records recordkeeping by electronic or hard copy upon each occurrence of inspection, per 40 CFR 60.113b(a)( I) through (4)_ Each 

record shall identify the storage vessel on which the inspection was performed and shall contain the date the vessel was inspected and the 

ob~erved condition of each component of the control equipment (seals, internal floating roof. and fittings). Keep copies of all records for at least 

two years. Subpart Kb. (40 CFR 60.115b(a)(2)) 

Submit a report: Due to DEQ Within 30 days of the annual visual mspect1on reqmred by 40 CFR 60.113b(a)(2) that delect< any of the cond1t1ons 

described in 40 CFR 60.113b(a)(2). Each report shall1dentify the storage vessel. the narure of the defects, and the date the storage vessel was 

emptied or the narure of and date the repair was made. Keep copies of aH reports for at least two years. Subpart Kb. [ 40 CFR 60.115h(a)(3) I 

Submit a report: Due to DEQ within 30 days of each inspection required by 40 CFR 60.113b(a)(3) thai finds 

holes or tears in the seal or seal fabric, or defects in the internal floating roof, or other control equipment defects listed m 40 CFR 

60.113b(a)(3)(1i). The report shall identify the storage vessel and the reason It did not meet the spec1ficalions of 40 CFR 61.112b(a)( I) or 40 

ct"R. 60.113b(a)(3) and list each repa!T made. Keep copies of all reports for at least two years. Subpart Kb. (40 CFR 60.115b(a)(4)) 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. (40 CFR 60.116b(b)) 

Page 12 of 49 TPOA0147 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cottori Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-o001 0-VG 

Air- Title V Regular Permit Minor Mod 

EQT 0050 55- 10,000 BBL IFR Storage Tank 

104 [40 CFR 60.116b(c)] 

I OS [40 CFR 60.116b(d)] 

I 06 [LAC 33:11!.2 103.8] 

107 [LAC33:11!.2103.C.I.a] 

108 [LAC 33:111.2103.C] 

109 [LAC 33:11!.2103.E.I] 

I 10 [LAC 33:11!.2103.H.3] 

Ill [LAC 33:lll.2103.1] 

VOL storage data recordkeeping by electronic or hard copy at the approved frequency. Records consist of the VOL stored, the period of storage, 

and. the maximum true vapor pressure of that VOL during the respective ·storage period. Keep copies of all records for at least two years. 

Subpart Kb. [40 CFR 60.116b(c)] 

Submit notification: Due within 30 days when the maximum true vapor pressure of the liquid exceeds the respective maximum true vapor 

pressure values for each volume range. Subpart Kb. [ 40 CFR 60.!16b(d)] 

Equip with a submerged fill pipe. · 

Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roofcontinuoll:~ly ar~und the circumference o(the tank. . 

Equip with ail internal floating roof consisting of a poritoon type roof, Oouble deck roof, or internal floating cover which will rest or float on the 

surface of the liquid contents arid is equipped with a closure seal to close the space between the roof edge and tank wall. All tank gauging and 

sampling devices will be gas-tight except when gauging or sampling is taking place. 

VOC, Total>= 95% control efficiency using a vapor loss control system. This limitation does not apply during periods of planned routine 

maintenance which may not exceed 240 hours per year.· 

Which Months: All Year Statistical Basis: None specified 

Determine VOC maximum true vapor pressure using the methods in LAC 33:JII.2103.H.3.a-e. 

Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency. Keep records of the infonnation 

specified in LAC 33:111.2103.1.1 -7, as applicable. 

EQT 0051 56- 10,000 BBL IFR Storage Tank 

112 [40 CFR 60.1 12b(a)(l)(i)] Equip with a fixed roof in combination with an internal floating roof. The internal floating roof shall rest or float on the liquid surface (but not 

necessarily in complete contact with it) inside a storage vessel that has a fixed roof. The internal floating roof shall be floating on the liquid 

surface at all times, except during initial fill and during those inte~als when the storage vessel.is completely emptied or subsequently emptied 

and refilled. When the roof is resting on the leg supports, the process of fil1ing, emptying, or refilling shall be continuous and shall be 

accomplished as rapidly as possible. Subpart Kb. [ 40 CFR 60.112b(a)(J )(i)] 

113 [40 CFR 60.112b(a)( I )(ii)(A)] Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circumference of the tank. Subpart Kb. [40 CFR 60.112b(a)(l )(ii)(A)] 

114 [40 CFR 60.112b(a)(l)(ii)(B)] Equip internal floating roof with two seals mounted secondary above the primary so th~t each forms a continuous closure that completely covers 

th~ space between the wall of the storage vessel" and the edge of the internal floating roof. The primary seal may be vapor-mounted, but both 

must be continuous. Subpart Kb. [40 CFR 60.112b(a)(I)(ii)(B)) · 

Page 13 of 49 TPOR0147 
SPECIFIC REQUIREMENTS . -

AliD: 312- Calume1 Lubrlcan1s Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0051 56 -10,000 BBL IFR Storage Tank 

115 [40CFR60.112b(a)(l)l 

116 (40CFR60.11Jb(a)(l)) 

117 [40 CFR 60.113b(a)(2)) 

118 (40 CFR 60.113b(aX2l) 

119 (40 CFR 60 113b(a)(J)(o)] 

120 (40CFR60.11Jb(a)(J)(ii)] 

Each opening in a noncontact internal floating roof except for automatic bleeder vents (vacuum breaker vents) and the rim space vents is to 

provide a projection below the liquid surface. Equip each opening in the internal floating roof except for leg sleeves, automatic bleeder vents, 

rim space vents, column wells, ladder wells. sample wells, and stub drains with a cover or lid and maintain in a closed position at all times (i.e., 

no visible gap) except when the device is in actual usc. Equip the cover or lid with a gasket. Bolt covers on each access hatch and automatic 

gauge float well except when they are in use. Equip'automatic bleeder vents with a gasket and close at all times when the roof is floating except 

when the roof is being floated ofT or is being landed on the roof leg supports. Equip rim space vents with a gasket and set to open only when the 

internal floating roof is not floating or at the manufacturer's recomffiended setting. Each penetration of the mternal floating roof fOr the purpose 

of sampling shall be a sample welL The sample well shall have a slit fabric cover that covers at least 90 percent of the opening. Each 

penetration of the internal floating roof that allows for pac;sage of a column supporting the fixed roof shall have a flexible f3bric sleeve seal or a 

gac;keted sliding cover. Each penetration of the internal floating roof that allows for passage of a ladder shall have a gasketed sliding cover. 

Subpan Kb. [40 CFR 60.112b(a)(l)) 

Tank roof and seals monitored by visual inspection/determination at the regulation's specified frequency. Inspect the internal floating roof. the 

primary seal, and the secondary seal (if one is in service), prior to filling the storage vessel with VOL If there are holes. tears, or other openings 

in the primary seal, the secondary seal, or the seal fabric or defects in the internal floating roof, or both, repair the items before filling the storage 

vessel. Subpan Kb. [40 CFR 60.113b(a)(l)) 

Which Months: All Year Statistic,al Basis· None specified 

If the internal floating roof is not resting on the swface of the VOL inside the storage vessel, or there is liquid accumulated on the roof. or the 

seal is detached, or there are holes or tears in the seal fabric, repair the items or empty and remove the storage vessel from serv1ce within 45 days. 

If a failure that is detected during inspections required in th1s paragraph cannot be repaired w1thin 45 days and if the vessel cannot be emptied 

within 45 days. request a 30-day extension from DEQ in the inspection report required in 40 CFR 60.11 Sh(a)(3). Document in the request for 

extension that alternate storage capacity is unavailable and specify a schedule of actions the company will rake that will assure that the control 

equipment Wlll be repaired or the vessel will be empllcd as soon as possible: Sub pan Kb. [40 CFR 60.113b(a)(2)] 

Tank roof and seals monitored by visual inspection/determination annually. Inspect the internal floating roof and the primary seal or the 

secondary seal (if one is in service) through manholes and roof hatches on the fixed roof at least once every 12 months after initial filL If a 

failure is detected during inspections required on this paragraph onitiate repaor provisions. Subpan Kb. [40 CFR 60.113b(a)(2)] 

Which Months: All Year Statistical Basis: None specified 

Tank roof and seals monitored by visual inspecllonidctcmunation once every five years as specified in 40 CFR 60.113b(a)(4). Sub pan Kb. [40 

CFR 60.113b(a)(3)(i)] 

Which Months: All Year Statistical Ba.c;is: None specified 

Tank roof and seals monitored by visual inspectoon/determination annually._, specified on 40 CFR 60.113b(a)(2). Subpart Kb. [40 CFR 

60.113b(a)(3)(ii)] 

Which Months: All Year Statistical Basis: None specified 

Page 14 of 49 TPOR0\•7 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 -

Permit Number: 3080-00010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0051 56 - 10,000 BBL IFR Storage Tank 

121 [40 CFR 60.113b(a)(4)] 

122 [40CFR60.113b(a)(4)] 

123 [40 CFR 60.113b(a)(S)] 

124 [40 CFR 60.115b(a)(l)] 

125 [40 CFR 60.115b(a)(2)] 

126 [40 CFR 60.115b(a)(3)] 

127 [40CFR60.115b(a)(4)] 

128 [40CFR60.116b(b)J 

If the internal floating roof has defects, the primary seal has holes, tears, or other openings in the seal or the seal fabric, or the secondary seal has 

holes, tears, or other openings in the seal or the seal fabric, or the gaskets no longer close off the liquid surfaces from the atmosphere, or the 

slotted membrane has more than I 0 percent open area, repair the items as necessary so that none of the conditions specified in this paragraph 

exist before refilling the storage vessel with VOL. In no event shall inspections conducted in accordance with this provision occur at intervals 

greater than 10 years in the case of vessels conducting the annual visual inspection as specified in 40 CFR 60.113b(a)(2) and (a)(3)(ii) and at 

intervals no greater than 5 years in the case of vessels specified in paragraph 40 CFR 60.113b(a)(3)(i) of this section. Subpart Kb. [40 CFR 

60.1!3b(a)(4)] 

Tank roof and seals monitored by visual inspection/determinatlon at the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, the secondary seal (if one is in service), gaskets, slott~d membranes and sleeve seals (if any) each time 'ihe storage vessel is emptied 

and degassed. If a failure is detected during inspections required in this paragraph initiate repair provisions. Subpart Kb. [40 CFR 

60.113b(a)(4)] 

Which Months: All Year Statistical Basis: None specified 

Submit notification in writing: Due at least 30 days prior to the filling or refilling of each storage vessel for which an inspection is required by 

40 CFR 60.113b(a)(l) and (a)(4) to afford DEQ an opportunity to have an observer present. If the inspection required by paragraph 40 CFR 

60.113b(a)(4) is not planned and the owner or operator Could not have known about the inspection 30 days in advance or refil1ing the tank, notify 

DEQ at least 7 days prior to the refilling of the storage vessel. Notify by telephone immediately followed by written documentation 

demonstrating why the inspection was unplanned. Alternatively, submit" notification in writing including the written documentation and send by 

express mail so that it is received by DEQ at least 7 days prior to tjle refilling. Subpart Kb. [40 CFR 60.113b(a)(S)] 

Submit a report: Due to DEQ as an attachment to the notification required by 40 CFR 60.7(a)(3). This report shall describe the control· 

equipment and certify that the control equipment meets th~ specifications of 40 CFR 60.1!2b(a)(l) and ·60.113b(a)(l ). Keep copies of all reports 

for at least two years. Subpart Kb. [40 CFR 60.11 Sb(a)(l)] 

Inspection records recordkeeping by electronic or hard copy upon each occurrence of inspection, per 40 CFR 60.113b(a)(l) through (4). Each 

record shall identify the storage vessel on which the inspection was_ performed and shall contain the date the vessel was inspected and the 

·observed condition of each component Of the control equipment (s~als, internal floating roof, and fittings). Keep copies of all records for at least 

two years. Subpart Kb. [40 CFR 60.!1 Sb(a)(2)] 

Submit a report: Due to DEQ within 30 days of the annual visual inspection required by 40 CFR 60.1!3b(a)(2) that detects any of the conditions 

described in 40 CFR 60.113b(a)(2). Each report shall identify the storage vessel, the nature of the defects, and the date the storage vessel was 

emptied or the nature of and date the repair was ma~e. Keep copies of all reports for at least two years. Subpart Kb. [ 40 CFR 60.11 Sb(a)(3)] 

Submit a report: Due to DEQ within 30 days of each inspection required by 40 CFR 60.113b(a)(3) that finds 

holes or tears in the seal or seal fabric, or defects in the internal floating roof, or other control equipment defects listed in 40 CFR 

60.113b(a)(3 )(ii). The report shall identify the storage vessel and the reason it did not meet the specifications of 40 CFR 6l.ll2b(a)( I) or 40 

CFR. 60.113b(a)(3) and list each repair made. Keep copies of all reports for at least two years. Subpart Kb. [40 CFR 60.11 Sb(a)(4)] 

Equipment/ope~ational data recordkeeping by electronic or ha~d copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the cap_acity of the storage vessel. Keep copi-es of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)] 

Page 15 of 49 TPQR0147 
SPECIFIC REQUIREMENTS 

AIIO: 312- Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0051 56- 10,000 BBL IFR Storage Tank 

129 (40CFR 60.116b(c)l 

130 (40 CFR 60.116b(d)] 

131 (LAC 33:1111103.8] 

132 (LAC 33:1111103.C.I.a] 

133 (LAC JJ 111.210J.C] 

134 (LAC ll IIUIOJ.E.I] 

135 (LAC J1111210J.IU] 

136 [LAC JJIII110J I) 

VOL storage data recordkeeping by electronic or hard copy at the approved frequency. Records consist of the VOL stored, the period of storage, 

and the maximum true vapor pressure of that VOL dunng the respective storage period. Keep copies of all records for at least two years. 

Subpart Kb. (40 CFR 60.116b(c)) 

Submit notification: Due within 30 days when the maximum true vapor pressure of the liquid exceeds the respective maximum true vapor 

pressure values for each volume range. Subpart Kb. (40 CrR 60.116b(d)) 

Equip wilh a submerged fill pipe. 

Equip internal noating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circwnference of the tank. 

Equip with an internal floating roof consisting of a pontoon typ~ roof, double deck roof, or internal floating cover which will rest or float on the 

surface of the liquid contents and is equipped with a closure seal to close the space between the roof edge and lank waiL All tank gauging and 

sampling devices wlll be gas-tight except when gauging or sampling is taking place. 

VOC, Total>= 95% cnnlrol efficiency using a vapor loss control system. This limitation does not apply during periods of planned routine 

maintenance which may not exceed 240 hours per year. 

Which Months: All Year Stat.islical Basis: None specified 

Detennine VOC maximum true vapor pressure using the methods in LAC 33:111.2103.H.3.a-e. 

Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency. Keep records of the infonnation 

spec1fied in LAC 33:!11.21 03.1. I - 7, as applicable. · 

EQT 0055 60 - 5,000 BBL IFR Storage Tank 

I 3 7 (40 CFR 60.112b(a)( I )(i)] Equip with a fixed roof in combination with an internal floatmg roof. The internal lloating roof shall rest or float on the liquid surface (but not 

nccessanly in complete contact with it) mstde a storage vessel that has a fixed roof. The internal floating roof shall be floating on the liquid 

surface at all times. except during initial fill and during those mtervals when the storage vessel is completely emptted or subsequently emptied 

and refilled. \\'hen the roof is resting on the leg supports, the process of filling, emptying, or refilling shall be continuous and shall be 

accomplished as rapidly as possible. Subpart Kb. (40 CFR 60.112b(a)( l)(1)) 

138 (40 CFR 60. 112b(a)( l)(il)(A)) Equip internal noating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of1he Slorage vessel and !he floa<ing rnof cnnlinuously around !he circumference of !he lank. Subpart Kb. [40 CFR 60.112b(a)( I )(ii)(A)) 

I 39 [40 CFR 60. 112b(a)( l)(i1)(B)) EquiP internal floating roof with two seals mount~d secondary above the primary so that each forms a continuous closure that completely covers 

the space between the wall of the storage vessel and rhe edge oft~e internal floating roof. The primary seal may be vapor-mounted, but both 

mus< be con<inuous. Subpart Kb. [40 CFR 60.1!2b(a)(l)(ii)(B)] 

Page t6 of 49 TPOR01•7 
--------------------------------------------------------------------------------------------------------------------------------------------------------

· SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080..00010-VS 

Air- Title V Regular Permit Minor Mod 

•·. 

EQT 0055 60 - 5,000 BBL IFR Storage Tank 

140 [40CFR60.112b(a)(l)] 

141 [40 CFR 60.113b(a)(l)] 

142 [40 CFR 60.113b(a)(2)] 

143 [40 CFR 60.113b(a)(2)] 

144 [40CFR60.113b(a)(3)(i)] 

145 [40CFR60.113b(a)(3)(ii)] 

Each opening in a noncontact internal floating roof except for automatic bleeder vents (vacuum breaker vents) and the rim space vents is to 

provide a projection below the liquid surface. Equip each opening in the internal floating roof except for leg sleeves, automatic bleeder vents, 

rim space vents, column wells, ladder wells, sample wells, <ind stub drains with a cover or lid and maintain in a closed position at all times (i.e., 

no visible gap) except when the device is in actual use. Equip the cover or lid with a gasket. Bolt covers on each access hatch and automatic 

gauge float well except when they are in use. Equip automatic bleeder vents with a gasket and close at all times when the roof is floating except 

when the roof is being floated off or is being landed on the roof leg supports. Equip rim space vents with a gasket and set to open only when the 

internal floating roof is not floating or at the manufacturer's' recominendC:d' setting. Each penetration of the internal floating roof for the purpose 

of sampling shall be a sample well. The sample well sh'all have a slit fatiric cover that cove"rs at least 90 percent of the opening. Each· 

penetration of the internal floating roof that ~illows for passage of a column supporting the fixed roof shall have a flexible fabric sleeve seal or a 

gasketed sliding cover. Each penetration of the internal floating roof that allows for passage of a ladder shall have a gasketed sliding cover. 

Subpart Kb. [40 CFR 60.112b(a)(l)] . . ., .. , 

Tank roof and seals monitoied by visual inspection/determination ~t the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, and the secondary seal (if one is in service), prior to filling the storage vessel with VOL. If there a~e holes, tears, or other openings 

in the primary seal, the secondary seal, or the seal fabric or defects in the internal floating roof, or both, repair the items before filling the storage 

vessel. Subpart Kb. [ 40 CFR 60.113b(a)( I)] 

Which Months: All Year Statistical Ba.o;;is: None specified 

If the internal floating roof is not resting on the surface of the VOL inside the storage vessel, or there is liquid accumulated on the roof, or the.· 

seal is dC:tached, or there are holes or tears in the seal fabric, repair the items or empty and remove the storage vessel from service within 45 days. 

If a failure that is detected during inspections required in this paragraph cannot be repaired within 45 days and if the vessel cannot be emptied 

within 45 days. request a 30-day extension from DEQ in the inspection r~port required in 40 CFR 60.115b(a)(3). Document in the request for 

extension that alternate storage capacity is unavailable and sPecify a schedule of actions the company will take that will assure that the control 

equipment will be repaired or the vessel will be emptied as soon as possible. Subpart Kb. [40 CFR 60.113b(a)(2)] 

Tank roof and 'seals monitored by visual inspection/determination annually. Inspect the internal floating roof and the primary seal or the 

secondary seal (if one is in service) through manholes and roof hatches on the fixed roof at least once every 12 months after initial f.ill. If a 

failure is detected during inspections required in this paragraph initiate repair provisions. Subpart Kb. [40 CFR 60.113b(a)(2)] 

Which Months: All Year Statistical Basis: None specified 

Tank roof and seals monitored by visual inspection/determination once every five years as specified in 40 CFR 60.113b(a)(4). Subpart Kb. [40 

CFR 60.113b(a)(3)(i)] . . . . 

Which Months: All Year Statistical Basis: None specified 

Tank roof and seals monitored by visual inspection/determination annually as specified in 40 CFR 60.113b(a)(2). Subpart Kb. [40 CFR 

60.113b(a)(3)(ii)] · 

Which Months: All Year Statistical Basis: None specified 

Page 17 of 49 TPOR0147 
SPECIFIC.REQUIREMENTSAIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-V& 

Air- Title V Regular Permit Minor Mod 

EQT 0055 60 - 5,000 BBL IFR Storage Tank 

146 (40CFR60.113b(o)(4)) 

147 (40CFR 60.113b(a)(4)] 

148 )40 CFR 60.113b(a)(5)) 

149 (40 CFR 60.115b(a)(l)) 

I 50 [40 CFR 60.115b(a)(2)] 

151 (40CFR60.115b(a)(3)) 

152 (40 CFR 60 115b(a)(4)] 

153 [40 CFR 60.116b(b)) 

If the internal floating roof h.as defects, the primary seal has holes, tears, or other openings in the seal or the seal fabric, or the secondary seal has 

holes, tears, or other openings in the seal or the seal fabric, or the gasket<; no longer close off the liquid surfaces from the atmosphere, or the 

stoned membrane has more than 10 percent open area, repair the Items as necessary so that none of the conditions specified in this paragraph 

exist before refilling the storage vessel wlth VOL. In no event shall inspections conducted in accordance with this provision occur at intervals 

grealer !han 10 years in !he case of vessels conductmg !he armuai visual inspection as specified in 40 CFR 60. I 13b(a)(2) and (a)(3)(ii) and at 

inlervais no greater !han 5 years in !he case of vessels spec1fied in paragraph 40 CFR 60. I 13b(a)(3)(i) ofth1s section. Subpan Kb. (40 CFR 

60.1 13b(a)(4)] · 

Tank roof and seals monitored by visual inspection/determination at the regulation's specified frequency. Inspect the internal floating roof, the 

primary seal, the secondary seal (if one is in service), gaskets, sloned membranes and sleeve seals (if any) each time the storage vessel is emptied 

and degassed. If a failure is detected during inspections required in this paragraph initiate repair provisions Subpart Kh. (40 CFR 

60.1 13b(a)(4)) 

Which Months: All Year Statis!lcal Basis: None specified 

Submit notification in writing: Due at least 30 days prior to the filling or refilling of each storage vessel for which an inspection IS required by 

40 CFR 60.1 I 3b(a)( I) and (a)(4) to afford DEQ an opportunity to have an observer present. if !he inspeclion reqUired by paragraph 40 CFR 

60. I 13b(a)(4) is not planned and the owner or operator could not have known about the inspection 30 days in advance or refilling the tank. notify 

DEQ at least 7 days prior to the refilling of the storage vessel. !'Jotify by telephone immediately followed by written documentation 

demonstrating why the inspection \\'aS unplanned. Allematively, submit notification in writing including the written documentation and send by 

express mali so !hat 11 IS rece1ved by DEQ at least 7 days prior to the refilling. Subpan Kb. (40 CFR 60.113b(a)(S)) 

Submit a report: Due to DEQ as an attachment to the notification reqwrcd by 40 CFR 60.7(a){3). This report shall describe the control 

equipment and cenify that the control equipment meets the specifications of 40 CFR 60.112b(a)( I) and 60.113b(a)( I). Keep cop1es of ail repons 

for at least two years. Sub pan Kb [40 CFR 60. I I Sb(a)(l )) 

Inspection records recordkeeping by electronic or hard copy upon each occunence of inspection, per 40 CFR 60.1 I 3b(a)( I) through (4). Each 

record shall identify the storage vessel on which the inspection was performed and shall contain the date the vessel was inspected and the 

observed condition of each component of the control e"'uiprnent (seals. internal floating roof, and fittings). Keep copies of all records for at least 

two years. Subpan Kb. [ 40 CFR 60.1 I 5b(a)(2)] ' 

Submit a rcpon: Due to DEQ 10.ithin 30 days of the annual viSual mspection required by 40 CFR 60. I 13b(a)(2) that detects any of the conditions 

described in 40 CFR 60.1 I 3b(a)(2). Each report shall identify the storage vessel. the nature of the defects, and the date the storage vessel was 

emptied or !he nature of and date !he repair was made. Keep copies of ail reports for at least two years. Subpan Kb. (40 CFR 60.11 Sb(a)(3)) 

Submit a repon: Due to DEQ within 30 days of each inspection required by 40 CFR 60.1 13b(a)(3) that finds 

holes or tears in the seal or seal fabric, or defects in the internal floating roof, or other control equipment defects listed in 40 CFR 

60. I I 3b(a)(3)(ii). The repon shall identify the storage vessel and the reason it did not meet the specifications of 40 CFR 61.112b(a)( I) or 40 

CFR. 60. I I 3b(a)(3) and hst each repair made. Keep cop1es of ali rcpons for at least two years. Sub pan Kb. [ 40 CFR 60.115b(a)(4)] 

Equiprnent/opemtional dala recordkeeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vesseL Keep copies of all records for the life of the source as 

spec1fied by40 CFR 60 I 16b(a). Subpan Kb. (40 CFR 60. 116b(b)) 

Page 18 of 49 TPOROI.-1 
--------------------------------------------------------------------------------------------------------------------------------------------------------------------------- -------

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

ActivitY Number: PER20120002 

Permit Number: 3080-00010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0055 60 - 5,000 BBL IFR Storage Tank 

IS4 [40 CFR 60.116b(c)] 

ISS [40 CFR 60.116b(d)] 

IS6 [LAC 33:111.2103.8] 

IS7 [LAC 33:111.2103.C.I.a] 

ISS [LAC 33:111.2103.C] 

IS9 [LAC 33:111.2103.E.1] 

160 [LAC 33:111.2103.11.3] 

161 [LAC 33:111.2103.1] 

VOL stOrage data recordkeeping by electronic or hard copy at the approved frequency. Records consist of the VOL stored, the period of storage, 

and the maximum true vapor pressure of that VOL during the respective storage period. Keep copies of all records for at least two years. 

Subpart Kb. [40 CFR 60.116b(c)] 

Submit notification: Due within 30 days when the rnaximum.tr':Ie.~apor pressure of the liquid exceeds the respective maximum true vapor 

pressure values for each volume range. Subpart Kb: [40 CFR 60.116b(d)] 

Equip with a submerged fill pipe. · 

Equip internal floating roof with a liquid mounted seal consisting of a foam- or liquid-filled seal mounted in contact with the liquid between the 

wall of the storage vessel and the floating roof continuously around the circumference of the tank. 

Equip with an internal floating roof consisting of a pontoon type roof, double deck roof, or internal floating cover which will rest or float on the 

surface of the liquid contetits and is equipped with a closure seal to close the space between the roof edge and tank wall. All tank gauging and 

sampling devices will be gas-tight exCept when gauging or sampling is taking place. 

VOC, Total>= 95% control efficiency using a vapor loss control system. This limitation does not apply during periods of planned routine 

maintenance which may not exceed 240 hours per year. . . 

Which Months: All Year Statistical Basis: None sPecified 

Determine VOC maximum true vapor pressure using the methods in LAC 33:111.2103.H.3.a-e. 

Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency. Keep records of the information 

specified in LAC 33:111.2103.1.1 -7, as applicable. 

EQT 0056 66- 10,000 BBL VFR Storage Tank 

162 [40CFR60.116b(b)] Equipment/Operational data recordkeeping by electronic or ha~d copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis Showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [ 40 CFR 60.116b(b )] 

EQT 0057 67- 10,000 BBL VFR Storage Tank 

163 [40 CFR 60.116b(b)] Equipment/operational data recordkeeping by electronic or hard copy at the-approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [ 40 CFR 60.116b(b )] 

EQT 0061 72 - 5,500 BBL VFR Storage Tank 

164 [40 CFR60.116b(b)j Equipment/operational data recordkeeping b)relectronic or hard copy at the approved frequency. Keep readily accessible; records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)] 

EQT 0062 73 - 5,000 BBL VFR Storage Tank .. ·,. · · · 

Page ,9 of 49 TPOR0147 

~ 
SPECIFIC REQUIREMENTS 

AIIO: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-40010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0062 73 • 5,000 BBL VFR Storage Tank 

165 (40 CFR 60.116b(b)] Equipment/operational data rccordkceping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. (40 CFR 60.116b(b)). 

EQT 0063 76 • 10,000 BBL VFR Storage Tank 

166 (40CFR60.116b(b)] Equipment/operational data record.keeping by electronic or hard copy at the approved frequency. Keep readily accessible records showing the 

dimension of the storage vessel and an analysis showing the capacity of the storage vesseL Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)) 

EQT 0064 79 • 5,500 BBL VFR Storage Tank 

167 (40CFR60.116b(b)) 

EQT 0067 B-1401 ·No. 1 Boiler 

t6R (40CFR 60.104(o)(l)] 

169 (40 CFR 60.105(a)(3)(11)] 

170 (40 CFR 60.105(a)(3)] 

171 (40 CFR 60.105(a)(4)) 

172 (40 CFR 60.106(a)] 

173 140 CFR 60.106] 

174 (LAC 33111.1101.8] 

175 (LAC 33:111.1313 C) 

Equipment/operational data rccordkeepmg by electronic or hard copy at the approved frequency. Keep readily acccssJblc records showmg the 

dimension of the storage vessel and an analysis showing the capacity of the storage vessel. Keep copies of all records for the life of the source as 

specified by 40 CFR 60.116b(a). Subpart Kb. [40 CFR 60.116b(b)] 

Fuel gas: Hydrogen sulfide<= 0.1 gridscf (230 mg/dscm). Sub pari J. [40 CFR 60.1 04(a)( I)) 

Which Months: All Year Statistical Basis: Three~hour rolling average 

Fuel gas: Sulfur dioxide<= 20 ppm dry basis, 0% excess air. Subpart J. [40 CFR 60.105(a)(3)(ii)] 

Which Months: All Year Statistical Basis: Three·hour rolling average 

Sulfur dioxide monitored by continuous emission monitor (CEM) continuously Include an oxygen monitor for correctmg the data for excess air 

Subpart J. [40 CFR 60.105(a)(J)j 

Which Months: All Year Statistical Basis: None spec1fied 

Hydrogen sulfide monitored by continuous emission monitor (CEM) continuously. Monitor Lhe H2S in fuel gases be~orc being burned in any 

fuel gas combustion device. Subpart J. [40 CFR 60.105(a)(4)) 

Which Months: All Year Statistical Rasis: None specified 

Usc as reference methods and procedures the test methods in 40 CFR 60 appendix A or other methods and procedures as specified in 40 CFR 

60.106, except as provided in 40 CFR 60 8(b), in conductmg the performance tests required in 40 CFR 60.8. Subpart J. [40 CFR 60.106(a)] 

Detennme compliance with standards using the test methods and procedures specified in 40 CFR 60.1 06(a) through (k). Subpart J. 

Opacity<= 20 percent, except during the cleaning of a fire box or building of a new f1re, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitator.;, which may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 lb/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified 

Page 20 of 49 TPQR01•7 
EQT 0067 B-1401 ·No. 1 Boiler 

176 [LAC 33:1Il.l513] 

EQT 0068 B-1402 -No.2 Boller 

177 [40 CFR 60.104(a)(l)] 

178 [40 CFR 60.105(a)(3)(ii)] 

179 [40 CFR 60.105(a)(3)] 

180 [40 CFR 60.105(a)(4)] 

181 [40 CFR 60.106(a)]" 

182 [40 CFR 60.106] 

183 [LAC33:l!T.II 0 I :B] 

184 [LAC33:111.1313.CJ 

185 [LAC33:l!T.1513] 

EQT 0069 BD • Blue Drum 

186 [40CFR61.355] 

187 [40CFR61.356] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet lubricants Co- Cotton Valley Refinery 

Activity Number: ·PER20120002 

Permit Number: 3080-0001 O-V6 

Air- Title V Regular Permit Minor Mod 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:III.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to? re~resentative of DEQ or the U.S. EPA on request. 

Fuel gas: Hydrogen sulfide<= 0.1 gr/dscf (230 mg/dscm). Subpart J. (40 CFR 60.1 04(a)(l )] 

Which Months: All Year Statistical Basis: Three-hour rolling average 

Fuel gas: Sulfur dioxide<= 20 ppm dry basis. 0% excess air. Subpart J. [40 CFR 60.105(a)(3)(ii)] 

Which Months: All Year Statistical Basis: Three-hour rolling average 

Sulfur dioxide monitored by continuous emission monitor (CEM) continuously. Include an oxygen monitor for correcting the data for excess air. 

Subpart J. [40 CFR 60.105(a)(3)] 

Which Months: All Yea:r Statistical Basis: None specified 

Hydrogen sulfide monitored by continuous emission monitor (CEM) continuously. Monitor the H2S in fuel gases before being burned in any 

fuel gas combustion device. Subpart J. [40 CFR 60.105(a)(4)] · 

Which Months: All Year Statistical Basis: None specified 

Use as reference methods and procedures the test methods in 40 CFR 60 appendix A or other methods and procedures as specified in 40 CFR 

60.106, excepl as provided in 40 CFR 60.8(b), in conducting the performance tests required in 40 CFR 60.8. Subpart J. [40 CFR 60.106(a)] 

Determine ~ompliance with standards using the test methods and procedures specified in 40 CFR 60.106(a) through (k). Subpart J. 

Opacity<~ 20 percent, except during the cleaning of a fire box or building of a new fue, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 lb/MMBTU of heal input. 

Which Months: All Year Statistical Basis: None specified 

EqUipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:1II.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

Determine compliance with 40 CFR 61 Subpart FF using the test methods and procedures specified in 40 CFR 61.355(a) through (i). as 

applicable. Subpart FF. 

Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency Maintain records as specified in 40 

CFR 61.356(a) through (n), as applicable. Maintain each record in a readily accessible location at the facilily site for a period not less lhan two 

years from the date the inforination is recorded unless otherwise sp,ecified. Subpart FF. 

Page 21 of 49 TPOR0147 
EQT 0071 Fl2 • Flare 

188 [40 CFR 60.104(a)(l)] 

189 [40 CFR 60.106(a)] 

190 [40CFR60.1J(i)] 

191 (40 CFR 60.18(c)( I)] 

192 [40 CFR 60.18(c)(2)] 

193 [40 CFR 60.18(c)(J)(ii)) 

194 [40 CFR 60.18(c)(5)) 

195 [40 CFR 60.18(d)) 

196 [40 CFR 60.18(e)) 

197 [40 CFR 60.18(1)(2)) 

198 [40 CFR 60.18] 

199 [LAC JJ:III.IIOS] 

200 [LAC JJ:IIL 1105] 

201 [LAC JJ:Illl J II CJ 

202 [LAC JHILISIJ] 

SPECIFIC REQUIREMENTS 

AIID: 312. Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air. Title V Regular Permit Minor Mod 

Fuel gas: Hydrogen sulfide<= 0.1 gr/dscf(230 mgldscm). Subpan J. (40 CFR 60. i04(a)(i )] 

Which Months: All Year Statistical Basis: Three-hour rolling average 

Use ao; reference methods and procedures the test methods in 40 CFR 60 appendix A or other methods and procedures as specified in 40 CFR 

60.106, except as provided in 40 CFR 60.8(b), m conductmg the perfonnance tests reqUired m 40 CFR 60.8. Subpan J. (40 CFR 60 i06(a)] 

Calwnct's alternative method uses ASTM D 4952-02, "Standard Test Method for Qualitative Analysis for Active Sulfur Spcc1es in Fuels and 

Solvents (Doctor's Test)". A Doctor's Test is performed once per day ifLSR loading has occurred durmg the day. An additional Doctor's Test is 

performed on a daily ba.-.is on the combined product stream that leaves the hydrotreater. Results of each test, the associated QAJQC data, and the 

product being loaded during sampling are recorded and retained onsite for a minimum of 3 years. Calumet will submit reports indicating 

instances of failed Doctor's Tests as pan of Cotton Valley's semiannual repon. (40 CFR 60. I 3(i)] 

Design and operate for no visible emissions, as determined by the methods specified in 40 CFR 60.18(f), except for periods not to exceed a total 

of 5 mmutes dunng any two consecu!lve hours. Subpan A. [40 CFR 60 I 8(c)(1 )] 

Operate with a flame present at ali times, as dctcrmmed by the methods specified in 40 CFR 60.18(1)(2). Subpan A. (40 CFR 60. I 8(c)(2)] 

Heat content>= 300 BTU/scf ( 11.2 MJ/scm). Determine the net heating value of the ga.o; being com busted by the methods specified in 40 CFR 

60. i 8(1)(3). Subpan A. (40 CFR 60. i 8(c)(3)(ii)] 

Which Months: All Year Statistical Basis: None specttied 

Exll VelocJty < 194 ftlsec (Vmax). Determine Vmax using the method spec1fied m 40 CFR 60.18(1)(6) Subpart A (40 CFR 60.18(c)(5)] 

Which Months: All Year Statistical Basis: None specified 

Monitor flares to ensure that they are operated and maintained in conformance with their designs. Applicable subparts will provide provisions 

statmg how to monitor flares. Subpart A. (40 CFR 60.18(d)] 

Operate at ali t1mes when emisstons may be vented to the flare. Subpan A. (40 CFR 60.18(e)] 

Presence of a flame monitored by flame monitor continuously. Use a thermocouple or any other equivalent device to detect the presence of a 

flare pilot flame. Subpan A. (40 CFR 60.18(1)(2)] 

Which Months: All Year Statistical Basis: None specified 

Permittee shall comply with ali applicable provistons of 40 CFR 60. I 8. 

Opacity<= 20 percent, except for a combined total of six hours in any 10 consecutive day period, for burning in connection with pressure valve 

releases for control over process upsets. 

Which Months: All Year Statistical Basis: None specified 

Submit notification: Due to the Office of Environmental Compliarlce, Emergency and Radiological Services Division. Single Point of Contact 

(SPOC). as soon as possible after the start of burning of pi"essure valve releases for control over process upsets. Notify in accordance with LAC 

33:1.3923. Notification is required only if the upset cannot be controlled in six hows. 

Opacity<= 20 percent; except emissions may have an average opacity in excess of 20 percent for not more than one six-minute period in any 60 

consecutive minutes. 

Which Months: All Year Statistical Basis: Six-minute average 

Equipment/operational data rccordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data reguired to demonstrate exemption from the provisions of LAC 33:111.Chaptcr 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

Page 22 of 49 TPOR01•7 
EQT 0071 FL2 -Flare 

203 [LAC JJ:Ili.501.C.6] 

204 [LAC JJ:III.501.C.6] 

205 [LAC JJ:III.501.C.6] 

206 [LAC JJ:III.501.C.6] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

Compiiance with the Emission Limit at 40 C.F.R. § 60.104(a)(l ). 

a. Continuous or Intermittent, Routinely-Generated Refinery Fuel Gases. For continuous or intermittent, routinely-generated refinery fuel gases 

that are combusted in any of the Flaring Devices identified in Appendix A, Calwnet shall either take the Flaring Device that is associated with 

such a gas stream out of service or shall comply with the emission limit at 40 C.F.R. § 60.1 04(a)(l) by the dates specified in Appendix A in the 

Consent Decree [SA-MM-10-0090] 

b. Non-Routinely Generated Gases. The combustion of gases generated by the startup, shutdown, or Malfunction of a refinery process unit or 

released to a Flaring Device as a result of relief valve leakage caused by excessive pressure build-up or other emergency Malfunction shall be 

exempt from the requirement to comply with 40 C.F.R. § 60.1 04(a)(l) [SA-MM-10-0090]. 

Good Air Pollution Control Practices. . 

For all Flaring Devices identified in Appendix A in the Conseitt Decree, Calumet shall comply with the NSPS obligation to imp]eme~t good air 

pollution control practices as required by 40 C.F.R. § 60.ll(d) to minimize HC and AG Flaring Incidents. [SA-MM-10-0090]. 

Identification of and NSPS Applicability for Flaring Devices. 

Calumet owns and operates the Flaring Devices identified iri.Apperidix A of the Consent Decree. Consistent with the terms of this Section V.D 

in the Consent Decree and the schedule in Appendix A, the Flaring Devices in Appendix A in the COnsent Decree shall be affected facilities, as 

that term is used in NSPS, 40 C.F.R. Part 60, and shall be subject to and comply with the requirements of 40 C.F.R. Part 60, Subparts A and J for 

fuel gas combustion devices [SA-MM-1 0-0090]. · 

Monitoring the Flaring Devices and Reporting. 

By no later than the dates identified in Appendix A of the Consent Decree, all Flaring Devices identified in Appendix A that Calumet keeps in 

service to combust continuous or intennittent, routinely-generated refinery. fuel gases, shall either (a) be equipped with a CEMS as required by 

40 C.F.R. § 60.105(a)(4); (b) have submitted to or comply with an alternative monitoring plan approved by EPA under 40 C.F.R. § 60.13(i); or 

(c) demonstrate that the fuel gas streams combusted in the fuel gas combustion device are inherently low in sulfur content in accordance with 40 

C.F.R. § 60.105(a)(4)(iv) or 40 C.F.R. § 60.105(b). Use of a properly-sized and operated flare gas recovery system on a flare may obviate the 

need to continuously monitor the emissions as otherwise required by 40 C.F.R. 60.105(a)(4) and 40 C.F.R. 60.7. Calumet shall comply with the 

applicable reporting requirements of 40 C.F.R. Part 60 Subpart J for all such flaring devices [SA-MM-10-0090]. · 

EQT 0073 GEN - Backup Generator 

207 [LAC 33:IIT.llOI.B] Opacity<= 20 percent, except during the _cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which.may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

208 [LAC 33:JII.1305] Prevent particulate matter from becoming airborne by taking.all reasonable precautions. These precautions shall include, but not be limited to, 

those specified in LAC 33:111.1305.A.I-7. 

209 [LAC 33:III.13ll.C] Opacity <= 20 percent; except emissions may have an average opacity in excess of 20 percent for not more than one six-minute period in any 60 

consecutive minutes (Complies by using sweet natural gas as fuel). · 

Which Months: All Year Statistical Basis: Six-minute average 

Page 23 of 49 TPQR0147 
-SPECIFIC REQUIREMENTS --

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0073 GEN -Backup Generator 

210 [LAC 33:TII1313 C[ 

211 [LAC 33:111.151 3] 

Tolal suspended particulate<= 0.6 lb/MMBTU of heat inpul. 

Which Months: All Year Statistical Basis: None spccifit:d 

Equipmcnllopcrational ~ala recordkccping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:III.Chaptcr 15. Record all emissions data in the units of the standard 

using the av~raging time of the standard. Make records avaJiablc to a representative ofDEQ or the lj_S, EPA on request. 

EQT 0074 H-101 -100 Crude Unit Proces~ Heater 

212 [LAC3.1:TIIIIOI Bl 

213 [LAC 33:1111305] 

214 [LACJ31111313CI 

215 [LAC 331111513] 

Opacity<= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incmerator. 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of 20 percent for not more than one s1x-minute 

period in any 60 consecutive minutes 

Which Months: All Year Statistical Basis: l'o:one specified 

Prevent particulate matter from becoming airborne by taking all reasonable precautions These precautions shall include, but not be limited to. 

those specified in LAC 33:111.1 305.A.i-7. 

Total suspended particulate<= 0.6 lb/MMBTU of heat input 

Which Months: All Year Statistical Basis: None specified 

Equipmenlloperational data recordkeepmg by electronic or hard copy at the approved frequency Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:Ili.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative of DEQ or the lJ.S. EPA on request. 

EQT 0075 H-201A- 1100 Crude Unit Process Heater 

216 [LAC lllll 1101.8] 

217 [LAC 33 llii313.C] 

218 [LAC 33:1l11Sil] 

Opacity<= 20 percent, except during the cleaning of a fire box or building of a new fue, soot blowmg or lancmg, charging of an mcinerator, 

equipment changes, ash removal or rapping of precipitators, y,:hich may have an opacity in excess of 20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: 'f\:one specified 

Total suspended particulate<= 0.6 lb/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exempllon from the provisions of LAC 33:111.Chapter IS. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available.to a reprcsentallvc ofDEQ or the U.S. EPA on request. 

EgT 0076 H-202 - Hot 011 Process Heater No. 1 

219 [LAC 33:111.11011l] Opacity<= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an mcmerator. 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specif1ed 

Page 24 of 49 TPQR01A7 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0076 H-202 - Hot Oil Process Heater No. 1 

220 [LAC33:ii1.1313.CJ 

221 [LAC33:iii.t513] 

Total suspended particulate<= 0.6 ib/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:1JI.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

EQT 0077 H-203 - Hot Oil Process Heater No. 2 

2i2 [LAC 33:1ii.IIOI.B] 

223 [LAC 33:111.1313.C] 

224 [LAC33:1ll.l513] 

Opacity <= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of 20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 ib/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:1U.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

EQT 0078 H-204 - Solvents Unit Heater 

225 [LAC 33:1li.IIOI.B] 

226 [LAC33:111.1313.CJ 

227 [LAC 33:111.1513] 

Opacity <,;, 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of 20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 lb/MMBTU ofheat·input. 

Which Months: All Year Statistical Basis: None sPecified' 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:III.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available tO a representative of DEQ or the U.S. EPA on request. 

EQT 0079 H-205 - Hydrotreater Heater 

228 (40CFR60.t04(a)(l)] Fuel gas: Hydrogensuifide<=O.i gr/dscf(230mgldscm). SubpartJ. [40CFR60.104(a)(i)] 

Which Months: All Year Statistical Basis: Three-hour rolling average 

229 [40 CFR 60.105(a)(3)(ii)] Fuel gas: Sulfur dioxide<= 20 ppm dry basis, 0% excess air. Subpart 1. [40 CFR 60. 105(a)(3)(ii)] 

Which Months: All Year Statistical Basis: Three-hour rolling average 

Page 25 of 49 TPOR0147 
EQT 0079 H-205 - Hydrotreater Heater 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080.()0010-VS 

Air- Title V Regular Permit Minor Mod 

230 (40 CFR 60. JOS(a)(J)] Sulfur dioxide monitored by continuous emission monitor (CEM) continuously. Include an oxygen monitor for correcting the data for excess air. 

Subpart J. [40 CFR 60.105(a)(3)] 

Which Months: All Year Statistical Basis: None specified 

231 (40 CFR 60.105(a)(4)) Hydrogen sulfide monitored by continuous emission monitor (CEM) continuously. Mon.itor the H2S in fuel gases before being burned many 

fuel gas combustion device. Subpart J. [40 CFR 60.105(a)(4)] 

Which Months: All Year Statistical Basis. None specified 

232 [40 CFR 60.106(a)] Use as reference methods and procedures the test methods in 40 CFR 60 appendix A or other methods and procedures as specified in 40 CFR 

60.106, except as provided in 40 CFR 60.8(b), m conductmg the performance tests rcqmrcd in 40 CFR 60.8. Subpart J. [40 CrR 60.106(a)] 

233 [40 CFR 60 106] Determine compliance with standards using the test methods and procedures specified m 40 CFR 60.106(a) through (k). Subpart J 

234 [LAC JJ:IIIt tOI.B) Opacity<"" 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator. 

equipment changes, ash removal or rapping of precipitators, which may have an opacuy in excess of 20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

235 (LAC JJ:III.t3t3.C) 

Which Months: All Year Statistical Basis: None spcc1ficd 

Total suspended paniculate <= 0.6 lb/M~BTU of heat input. 

Which Months: All Year Statistical Basis_ None specified 

236 [LAC JJ:III.tStl) Equipment/operational data recordkecping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:1II.Chaptcr 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative of DEQ or the U.S. EPA on request. 

EQT 0080 H-301 - No. 1 Hydrotreater Heater 

237 [40 CFR 60. t04(a)(l )J Fuel gas: Hydrogen sulfide<= 0.1 gridscf (230 mg/dscm). Subpart J. [40 CFR 60.104(a)( I)] 

Which Months: All Year Statistical Basis: Three-hour rolling average 

238 [40 CFR 60.tOS(a)(lX1i)) Fuel gas: Sulfur dioxide<= 20 ppm dry bas1s, 0% excess air. Subpart J. [40 CFR 60.105(a)(3)(u)] 

Which Months: All Year Statistical Basis: Three-how rolling average 

239 (40 CFR 60.105(a)(3)] Sulfur dioxide monitored by continuous emission monitor (CEM) continuously. Include an oxygen monitor for correcting the data for excess a1r. 

Subpart J. [40 CrR 60.105(a)(3)] 

Which Months: All Year Statistical Baliis: None specified 

240 (40 CFR 60. J05(aX4)) Hydrogen sulfide'monitored by continuous emission monitor (CEM) continuously. Monitor the H2S in fuel gases before being burned in any 

fuel gas combustion device. Subpart J. [40 CFR 60.105(a)(4)] · 

Which Months: All Y car Statistical Basis: None specified 

241 [40 CFR 60. 106(a)) Use as reference methods and procedures the test methods in 40 CFR 60 appendix A or other methods and procedures as specified m 40 CFR 

60.106, except as prov1ded in 40 CFR 60.8(b), in conducting the performance tests required in 40 CFR 60.8. Subpart J. [40 CFR 60.1 06(a)] 

242 [40 CFR 60.t06) Detennine compliance with standards using the test methods and procedures specified in 40 CFR 60.106(a) through (k). Subpart J. 

Page 26 of 49 TPORCP•7 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-Q0010-V6 

Air- Title V Regular Permit Minor Mod 

EQT 0080 H-301 -No. 1 Hydrotreater Heater 

243 [LAC 33:111.1101.8] 

244 [LAC 33:lli.I313.C] 

245 [LAC33:llLI513] 

Opacity<= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 lb/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specifie~ 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33 :Ill. Chapter 15. Record all emissions data in the unitS of the standard 

using the averaging time of the standard. Make records available to a representative of DEQ or the U.S. EPA on request. 

EQT 0081 H-601 -Solvent Train Process Heater 

246 [LAC 33:Ill.IIOI.B] 

247 [LAC 33:11!.1313.C] 

248 [LAC 33:lll.l513] 

Opacity <= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of 20 percent for not more than one six-minute 

period in any 60 consecutive minutes. · '' · 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.61b/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified · 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:Ili.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

EQT 0082 H-60211 000 - Utility Fractionator Process Heater 

249 [LAC 33:III.1101.B] Opacity<= 20 percent, except during the cleaning of a fire box' or building of a new frre, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of20 percent fOr not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis:.None specified 

250 [LAC 33:lll.l313.C] Total suspended particulate<= 0.61b/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified 

251 [LAC 33:111.15131 Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:lll.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

EQT 0083 H-701 - 700 Unit Process Heater 

252 [40 CFR 60.!04(a)(I)] Fuel gas: Hydrogen sulfide<= 0.1 gr/dscf (230 mg!dscm). Subpart J. [40 CFR 60.1 04(a)(l )) 

Which Months: All Year Statistical Basis: Three-houf rolling average 

Page 27 of 49 

. •:' 

TPOR0147 
------------------- -- - ------- ----- ·---·-----

. SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-V& 

Air- Title V Regular Permit Minor Mod 

EQT 0083 H-701 • 700 Unit Process Heater 

253 (40 CFR 60.105(a)(l)(II)J 

254 (40 CFR 60.105(a)(l)J 

255 [40 CFR 60.105(a)(4)) 

256 (40 CFR 60.106(a)) 

257 (40 CFR 60.106] 

258 [LAC 33:111 110\.B) 

25Q [LAC JJ:III.J J I J CJ 

260 [LAC JJ.\11.1513) 

Fuel gas: Sulfur dioxide<= 20 ppm dry basis, 0% excess air_ Subpart J. [40 CFR 60.105(a)(J)(ii)] 

~ich Months: All Year Statistical Basis: Three-hour rolling average 

Sulfur dioxide monitored by continuous em1ssion rnoni10r (CEM) continuously. Include an oxygen monitor for corrcctmg the data for excess air 

Subpart J. [40 CFR 60.105(a)(J)] 

Which Months: All Year Statistical Basis: None specified 

Hydrogen sulfide monitored by continuous emission monitor (CEM) continuously. Monitor the H2S in fuel gases before being burned in any 

fuel gas combustion device. Subpart J. (40 CFR 60.105(a)(4)] 

Which Months: All Year Statistical Basis: None specified 

Use as reference methods and procedures the test methods in 40 CFR 60 appendix A or other methods and procedures as specified in 40 CFR 

60.106, except as prov1ded in 40 CFR 60.8(b), m conducting the performance tests required m 40 CFR 60.8 Subpart J. (40 CFR 60.106(a)] 

Determine compliance with standards using the test methods and procedures specified m 40 CfR 60.106(a) through (k). Subpart J_ 

Opaciry <= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opaciry in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0 6 lh/MMRTU ofhea! input. 

Which Months: All Year Statistical Bas1s: None specified 

Equipmenu'operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least rwo years 

the data required to demonstrate: exemption from the provisions of LAC 33:111.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

EQT 0084 H-901 • Hydrogen Plant Reformer 

261 [LAC JJ:\11 t toLB) 

262 [LAC JJ.I\\.1 J I J.C) 

263 [LAC JJ:\11.1513) 

Opaciry <= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 lb/MMBTU of heat input 

Which Months: All Year Statistical Rasis: None specified 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 3 3 :III.Chapter 15. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available to a representative ofDEQ or the U.S. EPA on request. 

EQT 0085 LO • Loading Operations 

264 (40 CFR 64.3(b)(3)] Specific QA/QC Procedures: Calibrate, operate, and mamtain instrumentation using procedures that take into account manufacturer's 

specifications_ (40 CFR 64.3(b)(3)] 

Page 28 of 49 Tl'QROI•7 
SPECIFIC REQUIREMENTS 

AI 10: 312 -Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-{)0010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0085 LO - Loading Operations 

265 [40 CFR 64.4(e)) 

266 [40 CFR 64.6(c)(l)] 

267 [40 CFR 64.6(c)(2)] 

268 [40 CFR 64.6(c)(2)] 

269 [40 CFR 64.6(c)(4)] 

270 [40 CFR 64.6(d)] 

271 [40CFR64.7(a)] 

272 [40 CFR 64.7(b)] 

273 [40 CFR 64.7(c)] 

274 [40 CFR 64.7(d)(l)] 

275 [40 CFR 64.7(e)] 

276 [40 CFR 64.8(a)] 

Comply with. the submitted implementation plan and schedule for i~stalling, testing and pefforrning any other appropriate activities prior to use 

of the monitoring, if any of the approved monitoring in this pennit requires installation, testing, or other necessary activities prior to use of the 

monitoring for purpOses of 40 CFR 64. Implement monitoring as expeditiously as practicable after approval of the monitoring pursuant to 40 

CFR 64.6, but in no .case shall the period for completing installation and beginning operation of the monitoring exceed 180 days after approval of 

the pennit. (40 CFR 64.4(e)] 

Equipment/operational data monitored by technically sound method continuously Monitor the temperature at the flare tip which will detennine 

the continuous presense of a flame in the flare and maintain records Ofteinperature at the flare tip. [40 CFR 64.6(c){l )] 

Which Months: All Year Statistical Basis: None specified 

An excursion or exceedance is defined as the absence of a flame. (40 CFR 64.6(c)(2)] 

Submjt Notification: Due at the DEQ upon the establisliment or reesb.bti~hment of any exceedance or excursion level, fOr purposes of responding 

to and reporting exceedances or excursions under 40 CFR 64.7 and 64.8. (40 CFR 64.6(c)(2)] 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. (40 CFR 64.6(c)(4)] 

Schedule for installation, testing or final verification• of operational status: (40 CFR 64.6(d)] 

Conduct the monitoring required under 40 CPR 64 upon issuance of a part 70 or 71 permit that includes such monitoring, or by such later date 

specified in the pennit pursuant to 40 CFR 64.6(d). (40 CFR 64. 7(a)] 

Maintain the monitoring required under 40 CFR 64 at all tiines,. including but not limited to maintaining necessary parts for routine repairs of the 

monitoring equipment [40 CFR 64.7(b)] 

Conduct all monitoring required under 40 CPR 64 in continuous operation (or collect data at all required intervals) at all times that the pollutantspecific emissions unit is operating, except for, as applicable, monitoring malfunctions, associated repairs, and required quality assurance or 

control activities (including, as applicable, calibration checks and required zero and span adjustments). Do not use data recorded during 

monitoring malfunctions, associated repairs, and required quality assurance or control activities for purposes of 40 CFR 64, including data 

averages and calcul<itions. or for fulfilling a minimum data availability requirement, if applicable. Use all the data collected during all other 

periods in assessing the operation of the control device and associated control system. (40 CFR 64.7(c)] 

Restore operation of the pollutant-specific emissions unit (including the control device and associated capture system) to its normal or usual 

manner of operation as expeditiously as practicable upon detecting an excursion or exceci:dance, in accordance with good air pollution control 

practices for minimizing en:issions. Minimize the period of any startup, shutdown or malfunction, and take any necessary corrective actions to 

restore normal operation and prevent the likely recurrence of the c"ause of an excursion or exceedance (other than those caused by excused 

startup or shutdown conditions). [40 CFR 64. 7(d)(l)] 

Submit written notification: Due to the Office of Environmental Compliance within 72 hours upon identifying a failu_re to achieve compliance 

with the " emission limitation or the " standard for which, after approval of monitoring under 40 CFR 64, the approved monitoring did not 

provide an indication of an excursion or exceedance while providing valid data, or the results of coinpliance or performance testing document a 

need to modify the existing indicator ranges or designated conditions. If necessary, submit a proposed modification to the part 70 or 71 pennit to 

address the necessary monitoring changes. [40 CFR 64. 7(e)] '. 

An absence of a flame at the flare, as indicated when the temperature at the flare tip drops below 550 degrees F, occurring 6 times in any 12-

month periods is the threshold limit of excursions o~ exceedances at ~hich implementation of a QIP is required. [40 CFR 64.8(a)] 

Page 29 of 49 TPOR0147 
SPECIFIC REQUIREMENTS -

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-40010-VS 

Air- Title V Regular Permit Minor Mod 

EQT 0085 LO -Loading Operations 

277 (40 CFR 64.8(b)] 

278 [40 CFR 64.8(c)] 

279 [40 CFR 64.8(c)] 

280 (40 CFR 64.8(d)] 

281 (40 CfR 64.9(a)] 

282 [40 CFR 64.9(b)(J)] 

283 (40 CrR 64.9(b)(J)] 

284 (40 CrR 64.9(b)(l)] 

285 [LAC 33:111.2107 B] 

286 [LAC 33:111.2107.0] 

287 [LAC JJ:IIL2107.E] 

288 [LAC J3:11L50LC.6] 

289 [LAC J3:IIL50LC.6] 

290 [LAC J3:IIL50LC.6] 

291 [LAC JJ:IIL50LC.6] 

Maintain a written Quality Improvement Plan (QIP) and have it available for inspection. Include initially in the plan procedures for evaluating 

the control performance problems and, bao;cd on the results of the evaluation procedwes, modify the plan to mcludc procedures for conducting 

one or more of the acuons specified in 40 CFR 64.8(b)(2)(i) through (b)(2)(v), as appropnale_ [40 CFR 64.8(b)] 

Develop and implemenl a QualiJy Improvement Plan (QIP) as expcduiously as practicable [40 CFR 64.8(c)) 

Submit notification: Noufy the DEQ if the period for completing the Improvements contained in the Quality Improvement Plan (QJP) exceeds 

180 days from the dale on which the need 10 Implement the QIP was determined. [40 CFR 64.8(c)) 

Make reasonable changes to the Quality Improvement Plan (QJP) as the DEQ requires, upon any determination pursuant to 40 CFR 64. 7(d)(2) 

subsequent lo implementalion. [40 CFR 64.8(d)) 

Submit report: Due on and after the date specified in 40 CFR 64. 7(a) by which the owner or operator must use monitoring that meets the 

requirements of40 CFR 64. Submit momtoring repons to the: DEQ in accordance 'Nlth 40 CFR 70.6(a)(3)(iil). Include in a report for 

monitoring under 40 CFR 64, at a minimum, the infonnation required under 40 CFR 70.6(a)(3)(iii) and the information specified in 40 CFR 

64.9(a)(2)(1) through (a)(2)(1il), as applicable_ [40 CFR 64.9(a)] 

Comply wuh the recordkeepmg reqUirements spec1fied in 40 CFR 70.6(a)(3)(ii).[40 CfR 64.9(h)(l)) 

Equipment/operational data recordkeeprng by electronic or hard copy at the approved frequency. Maintain records of monitor performance data, 

corrective actions taken, any Mitten quality improvement plan required pursuant to 40 CFR 64.8 and any activities undertaken to implement a 

quality improvement plan, and other supporting information required to be maintained under 40 CFR 64 (such as data used to document the 

adequacy of monitoring, or records of monitoring maintenance or corrective actions). Maintain these records for a period of at least five years 

[40 CFR 64.9(b)(l)) 

Monitoring data recordkccping by electronic or hard copy at the approved frequency. ~aintam these records for a period of at least five years 

[40 CFR 64.9(b)(l )) 

VOC, Total >• 90 % DRE. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data record.Jceeping by electronic or hard copy at the regvlation's specified frequency. Keep records of the information 

specified in LAC 33:11L2107.D.3-4. 

Delennine compliance with LAC 33:11L2107.B using the methods in LAC 33:111.21 07.E. I through 5, as appropriate. 

EquiP.menlloperational data<= 6.05 MM bbVyr. Noncompliance with this limitation is a reportable violation of the permit. Notify the Office of 

Environmental Compliance, EnfOrcement Division if throughput exceeds the maximum listed in this specific condition for any twelve 

consecutive month period. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data monitored by technically sound method continuously. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data recordkeeping by electronic or hard copy monihly. Keep records of the Jype of products and quantily (throughput) 

through the loading faciliJy each month, as well as the total Jype of products and quanlily (throughput) through the loadmg facility for the last 

twelve months. Make records av~ilable for inspection by DEQ personneL 

Submit report: Due annually, by the 3 I st of March. Report the type of product and total throughput for the preceding calendar year to the Office 

of Environmental Compliance, Enforcement Division 

Page 30 of 49 TPQR01<H 
' 

EQT 0086 SH -Air Dryer (005) 

292 [LAC 33:lli.IIOI.B] 

293 [LAC 33:lll.l 3 I 3.C] 

294 [LAC 33:lll.l513] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-Q0010-V6 

Air- Title V Reguiar Permit Minor Mod 

Opacity<= 20 percent, except during the cleaning of a fire box or building of a new fire, soot blowing or lancing, charging of an incinerator, 

equipment changes, ash removal or rapping of precipitators, which may have an opacity in excess of20 percent for not more than one six-minute 

period in any 60 consecutive minutes. . 

Which Months: All Year Statistical Basis: None specified 

Total suspended particulate<= 0.6 lb/MMBTU of heat input. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data recordkeeping by electronic or hard copy at the approved frequency. Record and keep on site for at least two years 

the data required to demonstrate exemption from the provisions of LAC 33:lii.Chapter 15 .. Record all emissions data in the units of the standard 

using the averaging time of the standard. Make records available tO a representative ofDEQ or the U.S. EPA on request. 

' 

EQT 0087 WW - Wastewater Emissions 

295 (40 CFR 61.355] 

296 [40 CFR 61.356] 

Detennine compliance with 40 CFR 61 Subpart FF using the test methods and procedures specified in 40 CFR 61.355(a) through (i). as 

applicable. Subpart FF. 

Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency Maintain records as specified in 40 

CFR.61.356(a) through (n), as applicable. Maintain each record in a readily accessible location at the facility site for a period not less than two 

years from the date the information is recorded unless otherwise specified. SUbpart FF. 

EQT 0108 OPE OWS- Dual Phase Extraction System- Oil/Water Separator 

297 (40 CFR 61.355] Detennine compliance with 40 CFR 61 Subpart FF using the test methods and procedures specified in 40 CFR 61.355(a) through (i), as 

applicable. Subpart FF. 

298 [40 CFR 61.356] Equipment/operational data recordkeeping by electronic or hard copy at the regulation's specified frequency Maintain records as specified in 40 

CFR 61.356(a) through (n), as applicable. Maintain each record in a readily accessible location at the facility site for a period not less than two 

years from the date the information is recorded WIIess otherwise specified. Subpart FF. 

FUG 0002 FE - Fugitive Emissions 

299 (40 CFR 60.592(a)] 

300 [40 CFR li0.592(d)] 

301 (40 CFR 60.592(e)] 

302 [LAC 33:111.2111] 

303 [LAC 33:111.2121.8.1] 

Comply with the requirements of 40 CFR 60.482- I to 482- I 0 as soon as practicable, but no later than I 80 days after initial startup. Subpart 

GGG. (40 CFR 60.592(a)] 

Comply with the provisions of 40 CFR 60.485 except as provided in 40 CFR 60.593. Subpart GGG. [40 CFR 60.592(d)] 

Comply with the provisions of 40 CFR 60.486 and 60.487. Subpart GGG. (40 CFR 60.592(e)] 

Equip all rotary pumps and compressors handling volatile organic compounds having a true vapor pressure of I .5 psia or greater at handling 

conditions with mechanical seals or other equivalent equipment. · 

Repair according to LAC 33:Ill.212i.B.3 any regulated component observed leaking by sight, sound, or smell, regardless of the leak's 

concentration. 

Page 31 of 49 TPOR0147 

~· 
----,------

SPECIFIC REQUIREMENTS 

AIID: 312 ·Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-V& 

Air- Title V Regular Permit Minor Mod 

FUG 0002 FE -Fugitive Emissions 

304 [LAC JJJIL2121.B.2] 

305 [LAC 33:111.2121.B.J] 

306 (LAC JJ:IIL2121.C l.a.1] 

307 [LAC ll:IIL2121.CI a.uJ 

308 [LAC JJ:III.2121.C I ajii] 

309 (LAC]] 111.2121.C.I.b.IJ 

310 [LAC 33:111.2121.C l.b.1i] 

311 [LAC JJJIL2121.CJ.bjii] 

312 [LACJJ:lii.2121.C.IcJ 

313 [LAC Jl:IIL2121.Cl.aJ 

314 [LAC JJJIL2121CJ.b] 

315 [LAC JJ:III.2121.C.4.c] 

Do not locate any valve, except safety pressure relief valves, valves on sample lines, valves on drain lines and valves that can be removed and 

replaced without a shutdown, at the end of a pipe or line containing VOC unless the end of such line is sealed with a second valve, a blind flange, 

a plug, or a cap. Remove such scaling dcv1ces only when the line is in use, for example, when a sample is bcmg taken. When the line has been 

used and is subsequently resealed. close the upstream valve first, followed by the scaling device. 

Make every reasonable effort to repair a leaking component, as described in LAC 33:111.2121.8, within 15 days, except as provided. 

Pump seals: VOC, Total monitored by 40 CFR 60, Appendix A, ~ethod 21 annually (one time per year). If a readmg of 10,000 ppmv or 

greater is recorded, a leak is detected. If a leak is detected, initiate repair provisions specified in LAC 33:111.2121.8.3 

Which Months: All Year Statistical Basis: None specified 

Valves m hqUJd service: VOC, Total momtored by 40 CFR 60, Appendix A, Method 21 annually (one ume per year) !fa readmg of 10,000 

ppmv or greater is recorded, a leak is detected. If a leak is detected. initiate repair provisions specified m LAC 33:111.2121_8.3 

Which Months: All Year Statistical Basis: None specified 

Process drains: VOC, Total monitored by 40 CFR 60, Appendix A, Method 21 annually (one time per year). If a readmg of I 0,000 ppmv or 

b"TCatcr is recorded, a leak is detected. If a leak is detected, initiate repair provisions specified in LAC 33:111.2121.8.3 

Which Months: All Year Statistical Basis· }.;one specified 

Compressor seals: VOC, Total monitored by 40 CFR 60, Appendix A, Method 21 quancrly (four times per year). If a readmg of I 0,000 ppmv 

or greater is recorded, a leak is detected_ If a leak is detected, initiate repair provisions specified in LAC 33:111.2121.8.3. 

Which Months: All Year Statistical Bao;is: None specified 

Valves in gas service: VOC, Total monitored by 40 CFR 60, Appendix A, Method 21 quarterly (four times per year). If a reading of I 0,000 

ppmv or greater is recorded, a leak is detected. If a leak is detected, initiate repair provisions specified in LAC 33:111.2121.8.3. Permittee may 

elect to comply with the alternate standards for valves in LAC 33:111.2121.0 (skip period prov1s1ons). 

Which Months: All Year Statistical Basis: None spec1f1ed 

Presswe relief valves in gas service: VOC, Total monitored by 40 CFR 60, Appendix A. Method 21 quarterly (four times per year) If a reading 

of 10,000 ppmv or greater is recorded, a leak is detected. If a leak is detected, initiate repair provisions specified in LAC 33:111.2121.8.3 

Which Months: All Y car Statistical Basis: None specified 

Pwnps: Seal or closure mechanism monitored by visual inspection/determination weekly (52 times per year). 

Which Months: All Year Statistical Basis: None specified 

Pressure relief valves: VOC, Total monitored by 40 CFR 60, Appendix A, Method 21 within 24 hours after venting to the atmosphere. If a 

reading of I 0,000 ppmv or greater is recorded, a leak is detected. If a leak is detected, initiate repair provisions specified in LAC 

33:111.2121.8.3. 

Which Months: All Year Statistical Basis: None specified 

All components: VOC, Total monitored by 40 CFR 60, Appendix A, Method 21 upon each occurrence of a leak detected by sight, smell, or 

sound, u~less electing to implement actions as specif1ed in LAC 33:III.2121 .. B.3. 

Which Months: All Year Statistical Basis: None specified 

Inaccessible valves: VOC, Total monitored by 40 CFR 60, Appendix A, Method 21 annually (at a minimum). 

Which Months: All Year Statistical Basis: None specified 

Page 32 of 49 rPOJ{01H 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: .PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Mln.or Mod 

FUG 0002 FE -Fugitive Emissions 

316 (LAC 33:Ill.2121.C.4.c] 

317 (LAC 33:l!L2121.E.l] 

318 (LAC33:!!1.2121.E] 

319 (LAC 33:l!L212I.F] 

320 ·(LAC 33:l!LSOI.C.6] 

321 (LAC 33:l!LSOI.C.6] 

322 (LAC 33:l!LSOI.C.6] 

Unsafe-to-monitor valves: VOC, Total monitored by 40 CFR 60, Appendix~ Method 21 upon each occurrence. of conditions allowing these 

valves to be monitored safely. 

Which Months: All Year Statistical Basis: None specified 

When a leak that caimot be repaired on-line and in-place is located, affix to the leaking component a weatherproof and readily visible tag bearing 

an identification number and the date the leak is located. Date and remove the tag after the leak is repaired. 

Equipf11ent/operational data recordkeeping by survey log upon each occurrence of a leak. Include the leaking component information specified 

in LAC 33:111.2121.E.2. Retain the survey log for two years after the latter date specified in LAC 33:111.2121.E.2 and make said log available to 

DEQ upon request. 

Submit report: Due semiannually, by the 31st of January and July, to the Office of Environmental Assessment, Air Quality Assessment Division. 

Include the information specified in LAC 33 :lll.212l.F.I through 4 for each calendar quarter during the reporting period. · 

Adding New Valves and Pumps. . 

By no later than one hundred and twenty ( 120) days from the Effective Date of the Consent Decree, Calumet shall establish a tracking program 

for maintenance records (e.g., a Management of Change program) to ensure that valves and pumps added to the Refinery during maintenance and 

construction are integrated into the LDAR program.[SA-MM-1 0-0090]. 

Calibration/Calibration Drift Assessment. 

a. Calibration. Calumet shall conduct all calibrations of LDAR monitoring equipment using methane as the calibration gas, in accordance with 

40 C.F.R. Part 60, EPA Reference Test Method 21. 

b. Calibration Drift Assessment. Beginning no later than the Effe~tive Date of the Consent Decree, Calumet shall conduct calibration drift ·. · 

assessments ofLDAR monitoring equipment at the end of each monitoring shift, at a minimum. Calumet shall conduct the calibration drift 

assessment using, at a minimum, a 500 ppm calibration gas. If any calibration drift assessment after the initial calibration shows a negative drift 

of more than I 0% from the previous calibration, Calumet shall remonitor al1 valves that were monitored since the last calibration that had a 

reading greater than 100 ppm and shall remonitor all pumps that were monitored since tht last calibration that had a reading greater than 500 

ppm.[SA-MM-1 0-0090]. 

Delay of Repair. 

Beginning no later than the Effective Date of the Consent Decree, for any equipment for which Calumet is allo:wed, under the applicable 

regulations, to place on the "delay ofrepair" list for repair: 

a. For all equipment, Calumet shall: 

i. Require sign off by the unit supervisor/lead opera.tor.that the piece of equipment is technically infeasible to repair without a process nnit 

shutdown, before the component is eligible for inclusion on the "delay of repair" list; and 

ii. Include equipment that is placed on the "delay of repair" list in Caiumet(.S regular LDAR monitoring.[SA-MM-10-0090]. 

Page 33 of49 TPOR0147 

' 
--SPECIFIC REQUIREMENTS 

AJ 10: 312 -Calumet Lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-V& 

Alr- Title V Regular Permit Minor Mod 

FUG 0002 FE - Fugitive Emissions 

323 (LAC 33 III.SOI.C6) 

324 (LAC 33:111.SOI.C6) 

325 (LAC 33:iii.SOI.C6) 

326 (LAC 33JII.SOI.C6) 

Electronic Monitoring, Storing, and Reporting of LDAR DaHl. 

a. Electronic Storing and Reporting of LDAR Data. Calumet ha.o:; and will continue to maintain an electronic database for storing and reporting 

LDAR data. By no later than six months after the EfTcctivc Date of the consent Decree, the electronic database shall include data identifying the 

date and time of the monitored event, and the operator and instrument used in the monitored event. 

b. Electronic Data Collection During LDAR Monitoring and Transfer Thereafter. By no later than 180 days after the Effective Date of the 

Consent Decree, Calumet shall submit to the LDEQ operational specifications for the data logger, software, and monitoring equipment. By no 

later than the Effective Date of the Consent Decree, Calumet shall use dataloggers and/or electronic data collection devices during alll..DAR 

monitoring. Calumet, or its designated contractor, shall use its/their best efforts to transfer, on a daily basis, electronic data from electronic 

data logging devices to the electronic database of Paragraph 55.o of the Consent Decree. For all monitoring events in which an electronic data 

collection device is used, the collected monitoring data shall include a time and date stamp. Calumet may usc paper logs where necessary or 

more feasible (e.g., small rounds, rcmonitoring, or when dataloggers are not available or broken). and shall record, at a minimum. the 

identification of the t_echnician undertaking the monitoring, the date, and the identification of the monitoring equipment Calumet shall use 1ts 

best efforts to transfer any manually recorded monitoring data to the electronic databac;e of Paragraph 55.a of the Consent Decree within seven 

days ofmoniloring.[SA-MM- 10-0090). 

LDAR Aud1ts. 

Commencing upon the Effective Date of the Consent Decree. Calumet shall implement at the Refinery wlde audits set forth in Paragraph 50 of 

the Consent Decree, to enswe theRefinery's compliance wnh all applicable LDAR regulations. The LDAR audits shall include but not be limited 

to, comparative monitoring, records review, tagging, data management, and observation of the LDAR technicians(. calibration and monitoring 

lechniques [SA-MM-10-0090]1. 

LDAR Personnel 

By no later than 30 days after the Effective Date of the Consent pecree, Calumet shall establish a program that will hold LDAR personnel 

accountable for LDAR performance. Calumet shall maintain a position within the Refinery responsible for LDAR management with the 

aulhority to implement improvements.[SA-M~-1 0-0090). 

Leak Detection and Repair (LDAR) Program Enhancements. 

In order to minimize or eliminate fugitive emissions ofvolat1le organic compounds (VOCs). benzene, volatile hazardous air pollutants (VHAPs). 

and organic hazardous air pollutants (HAPs) from equipment i1_1light liquid and/or in gas/vapor service, Calumet shall undertake the 

enhancements in this Section J to the Refinery's LDAR program under Title 40 of the Code of Federal Regulations, Part 60, Subparts VV and 

GGG; Part 61, Subparts J and V; Part 63, Subpart CC: and applicable LDEQ LDAR regulations. The terms "equipmcnl," "m i•ghlliqUld 

service" and "in gas/vapor service" shall have the definitions set fonh in the applicable provisions of Title 40 of the Code of Federal Regulations. 

Part 60, Subparts VV and GGG; Part 61. Subparts J and V; Part 63, Subpart CC; and applicable LDEQ LDAR reguialions. Nolhing in lhis 

Section J shall be construed to require Calumet to include in the enhancCd program described herein any equipment or units not otherwise subject 

10 any applicable federal or slale LDAR regula lion [SA-MM- I 0-0090). 

Page 34 of 49 rPQR01C7 
FUG 0002 FE - Fugitive Emissions 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-D0010-V6 

Air- Title V Regular Permit Minor Mod 

327 [LAC 33:111.501.C.6] QNQC ofLDAR Data. 

By no later than ninety (90) days after the Effective Date of the Consent Decree, Calumet, or a third party contractor retained by Calumet, shall 

develop and implement a procedure to ensure a quality assurance/quality control (QA/QC) review of all data generated by LDAR monitoring 

technicians. Calumet shall ensure that monitoring data provided to Calumet by its contractors is reviewed for QA/QC before the contractor 

submits the data to Calumet. At least once per calendar quarter, Calwnet shall perform QAJQC of the contractor's monitoring data which shall 

include, but not be limited to: number of components monitored per teclmician, time between monitoring events, and abnormal data patterns. 

[SA-MM- I 0-0090]. 

Page 35 of 49 TPOR0147 
SPECIFIC REQUIREMENTS 

AJID: 312- Calumet Lubricants Co- Conori Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air- Title V Regular Permit Minor Mod 

FUG 0002 FE - Fugitive Emissions 

328 [LAC JJIIISOJC.6] Rccordkccping and Reporting Requirements. 

a. Wrincn Refinery-Wide LDAR Program No later than I 80 days after the Effective Date of the Consent Decree. Calumet shall submit a copy 

to LDEQ oftheRefincry's LDAR Program developed pursuant to Paragraph 47 in the Consent Decree. 

b. Submission of Operational Specifications for Electronic Data Collection during LDAR Monitoring and Certification of Usc of Electronic 

Data Collection during LDAR Monitonng. By no later than 180 days after the Effective Date of the consent Decree, Calumet shall submit to 

LDEQ operational specifications designed to minimize the use of any form of data collection and data transfer during and after LDAR 

monitoring other than electronic data collection and transfer 

c. As Part of Either the Reports Required under the Refinery's applicable LnAR program or the Semi-annual Progress Report Procedures of 

Section IX (Recordkeeping and Reporting) of the Consent Decree. Consistent with the requirements of Section IX (Recordkeeping and 

Reponing) of Consent Decree, Calumet shall include the following information, at the following times, in its semi-annual progress reports: 

L First Semi-annual Progress Report Due unde the Consent Decree. At the later of: the first semi-annual progress report due under the Consent 

Decree or the first semi-annual progress report for which the requirement becomes due, Calumet shall include the following: 

( 1) A certification of the implementation of QNQC procedures for review of data generated by LDAR technicians as required by Paragraph 56 

in the Consent Decree; 

(2) An identification of the mdividual at each Refinery responsible for LDAR perfonnance as required by Paragraph 57 in the Consent Decree; 

(3) A certification of the development of a tracking program for new valves and pumps added during maintenance and construction as required 

by Para1:,"Taph 58 in the Consent Decree; 

(4) A certification of the implementation of the calibration drift assessment procedures of Paragraph 59 in the Consent Decree; 

(5) A certification of the implementation of the "delay of repair" procedures of Paragraph 60 in the Consent Decree, and 

. (6) Information identifying the training measures that Calumet toOk to comply with the provisions of Paragraph 48 in the Consent Decree. 

ii. Semi-annual Progress Report for the First Semi-Annual Reporting Period. Until termination of the Consent Decree, in the semi-annual 

progress report that Calwnet submits pursuant to Section IX of the Consent Decree for the first semi-annual reporting period of each year, 

Calumet shall include an identification of each audit that was conducted pursuant to the requirements of Paragraph 50 in the Consent Decree tn 

the previous calendar year including, for the Covered Refinery, an identification of the auditors, a summary of the audit results, and a summary 

of the actions that Calumet took or intends to take to correct all deficiencies identified in the audits. 

iii. ln Each Report due under the Refinery's Applicable LDAR Program. ln each report due under the Refinery's applicable LDAR program, 

Calumet shall include: ' 

Monitoring. The following information on LDAR monitoring: 

(a) a list of the process units monitored during the quarter; 

(b) the number of valves and pumps monitored in each process unit; 

(c) the number of valves and pumps found leaking; 

(d) the number of "difficult to monitor' pieces of equipment monitored; 

(e) the projected month of the next monitoring event for that unit; and (I) a list of all equipment currently on the "delay of repair" list and the date 

each component wa• placed on the list. [SA-MM-1 0-0090). 

Page 36 of 49 TPQA01•7 
SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-Q0010-V6 

Air- Title V Regular Permit Minor Mod 

FUG 0002 FE· Fugitive Emissions 

329 (LAC 33:111.501.C.6] 

330 [LAC 33:111.501.C.6] 

Reporting, Recording, Tracking, Repairing and Remonitoring Leaks ~rYalves and Pumps Based on the Internal Leak Definitions. 

a. Reporting. For regulatory reporting purposes, Calumet may continue to report leak rates in valves and pumps against the applicable 

regulatory leak definition, or may use the lower, internal leak definitions specified in Paragraph 52 of the Consent Decree. 

b. Recording, Tracking, Repairing and Remonitoring Leaks. Calumet shall record, track, repair and remonitor all leaks in excess of the internal 

leak definitions of Paragraph 52 of the Consent Decree at such time as !hose definitions become applicable, in accordance with the applicable 

LDAR program for the Refinery. [SA-MM-10-0090]. 

Written Refinery-Wide LDAR Program. 

By no later than 120 days after the Effective Date of the Consent Decree; Calumet shall develop and maintain a written facility wide program for 

compliance with all applicable federal and state LDAR regulations. Until termination of the Consent Decree, Calumet shall implement this 

program on a Refinery wide basis, and Calumet shall update the Refinery's program as necessary to ensure continuing compliance. The Facilitywide program shall include at a minimum: 

a. An overall. Refmery-wide leak rate goal that will be a target for achievement on a process unit-by-process unit basis; 

b. An identification of all equipment in light liquid and/or in gas/vapor service that has the potential to leak VOCs, HAPs, VHAPs, and benzene 

within process units that are owned and main~ined by the Refinery; 

c. Procedures for identifying leaking equipment within process units that are oWned and maintained by the Refinery; 

d. Procedures for repairing and keeping track of leaking equipment; 

e. Procedures for identifying and including in the LDAR program new equipment; and 

f. A process for evaluating new and replacement equipment to promote consideration ~nd installation Of equipment that will minimize leaks 

and/or eliminate chronic leakers.[SA-MM-10-0090]. · 

GRP 0010 Crude-Cap· Crude Cap (Capped Tank 47) 80,000 BBL IFR STORAGE TANK 

Group Members: EQT 0038 EQT 0047 

331 [LAC 33:Ill.501.C.6] 

332 [LAC 33:111.50J.C.6] 

333 [LAC 33:111.50l.C.6] 

334 [LAC 33:Ill.50J.C.6] 

Equipment/operational data<= 8.76 MM bbVyr. Noncompliance with this limitation is a reportable violation of the permit. Notify the Office of 

Environmental Compliance, Enforcement Division if the throughput exceeds the maximum listed in this specific condition for any twelve 

consecutive month Period. .. 

Which Months: All Year Statistical Basis: None specified · 

Equipment/operational data monitored by technically sound method continuously. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data recordkeeping.by electronic or hard copy monthly. Keep records of the throughput ~ach month, aS well as the total 

throughput for the last twelve months. Make records available for inspection by DEQ personnel. 

Submit report: Due annually. by the 31st of March. Report the throughput for the preceding calendar year to the Office of Environmental 

Compliance, Enforcement Division. · 

GRP 0011 HEAVY CAP-1- Heavy VOL Cap-1 (Capped Tank 57) 80,000 BBL VFR S,TORAGE TANK 

Group Members: EQT 0020 EQT 0021 EQT 0022 EQT 0023 EQT 0025 EQT 0027 EQT 0028 EQT 0029 EQT 0030 EQT 0031 E,QT 0032 EQT 0033 EQT 0034 EQT 0035 EQT 0036 EQT 0039 EQT 0041 EQT 0042 , • I ,• ' 

Page 37 of 49 TP0R0147 
SPECIFIC REQUIREMENTS 

AIIO: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-40010-VS 

Air- Title V Regular Permit Minor Mod 

GRP 0011 HEAVY CAP-1- Heavy VOL Cap-1 (Capped Tank 57) 80,000 BBL VFR STORAGE TANK 

~~E~~~~~~E~~~~~~~~~~~~ 

335 [LAC 33:1li.501.C.6] Equipment/operational data<= 5.60 MM bbl/yr. Noncompliance with th1s limitation is a reportable violation of the pcrmtt Notify the Office of 

Environmental Compliance, Enforcement Division if the throughpUt exceeds the maximum listed in th1s specific condition for any twelve 

consecutive month period. 

Which Months: All Year Statistical Basis: None specified 

336 [LAC JJ:III.SOI_C.6] Equipment/operational data monitored by technically sound method continuously. 

Which Months: All Year Statistical Basis: None specified 

337 [LAC 33:1I1.50l.C.6] Equipmcnlloperational data rccordkecping by electronic or hard copy monthly. Keep records of the throughput each month, as well as the total 

throughput for the last twelve months. Make recordc; ava1lablc for inspection by DEQ personneL 

338 [LAC 33:111.501.C.6] Submit report: Due annually, by the 3 I st of March. Report the throughput for the preceding calendar year to the Office of Environmental 

Compliance, Enforcement Division 

GRP 0012 HEAVY CAP-2- Heavy VOL Cap-2 (Capped Tank 57) 80,000 BBL VFR STORAGE TANK 

Group !\1rmbcrs: F.QT 0052 

339 (LAC 33:111.SOJ.C.6) . 

340 (LAC 33:IILSOI.C.6) 

34i (LAC 33:111.SOJ.C.61 

Equipment/operational data<== 720000 MM bbUyr. Noncompliance with this limitation is a reportable violation of the permit. Notify the Office 

of Environmental Compliance. Enforcement Division if the throughput exceeds the maximum listed in this specific condition for any twelve 

consecutive month period. · 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data monitored by technically sound method continuously. 

Which Months: All Year Statistical Basis: None specified 

Submit report: Due annually, by the 31st of March. Report the throughput for the preceding calendar year to the Office of Environmental 

Compliance, Enforcement Division. 

GRP 0013 UH VOL IFR CAP- UH VOL IFR Cap (Capped Tank 54) 10,000 BBL IFR STORAGE TANK 

Group Mrmbrrs: EQT 0049EQT 0050EQT OOSS 

342 (LAC ll:IILSOI.C.6} 

343 (LAC 33:11LSOJ.C.6) 

344 (LAC 33 IILSOJ.C.6) 

EqUJpmenl/operational data<= 1.14 MM bbUyr. Noncompliance with this limitation is a reportable violation of the permit. Notify the Office of 

Environmental Compliance, Enforcement Division if the throughput exceeds the maximum listed in this specific condition for any twelve 

consecutive month period. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data monitored by technically sound method continuously. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data rccordkccping by electronic or hard copy monthly. Keep records of the throughput each month, as well as the total 

throughput for the last twelve months. Make records available for-inspection by DEQ personnel. 

Page 38 of 49 TPQR0\•7 
SPECIFIC REQUIREMENTS 

AIID: 312 ·Calumet Lubricants Co· Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~001 O·V6 

Air· Title V Regular Permit Minor Mod 

GRP 0013 UH VOL IFR CAP· UH VOL IFR Cap (Capped Tank 54) 10,000 BBL IFR STORAGE TANK 

345 '[LAC JJ:II!.501.C.6] Submit report: Due annually, by the 31st of March. Report the throughput for the preceding calendar year to the Office of Environmental 

Compliance. Enforcement Division. 

GRP 0014 VFR/HFR CAP· Light/Heavy VOL VFR/HFR Cap (Capped Tank 16) 2,000 BBL VFR STORAGE TANK 

Gr~p Members: EQT 0024EQT 0026EQT OOS9 

346 (LAC J3:lll.501.C.6] 

347 (LAC 33:lll.501.C.6] 

348 (LAC 33:1I!.501.C.6] 

349 [LAC 33:111.501.C.6] 

Equipment/operational data<= 354120 bbVyr. Non~ompliru;c·e With thi~ limitation is a reportable violation of the permit. Notify the Office of 

Environmental Compliance, Enforcement Division if the throughput exceeds the maximum listed in this specific condition for any twelve 

consecutive month period. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data monitored by technically sound method continuously. 

Which Months: All Year Statistical Basis: None specified , ... 

Equipment/operational data recordkeeping by electronic or har~ copy monthly. Keep records of the throughput each month, as well as the total 

throughput for the last twelve months. Make records available "for inspection by DEQ personnel. 

Submit report: Due annually, by the 31st of March. Report the throughput for the preceding calendar year to the Office of Environmental 

Compliance. Enforcement Division. · · 

GRP 0015 NSPS Kb CAP· NSPS KB FR CAP (CAPPED TANK 76) 10,000 BBL STORAGE TANK 

Group Members: EQT 0003 EQT 003 7 EQT 0040 EQT 0056 EQT 0057 EQT 0062 EQT 0063 EQT 0064 

350 (LAC 33:lll.50l.C.6] 

351 [LAC 33:111.501.C.6] 

352 (LAC 33:111.501.C.6] 

353 (LAC 33:111.501.C.6] 

Equipment/operational data<= 1.53 MM bbl/yr. Noncompliance with this limitation is a reportable violation of the pennit. Notify the Office of 

Environmental Compliance, Enforcement Division if the throughput exceeds the maximum listed in this specific condition for any twelve 

consecUtive month period. 

Which Months: All Year Statistical Basis: None specified 

Equipment/operational data monitored by technically sound metho'd continuously. 

Which Months: All Year Statistical Basis: None specified - . · 

Equipment/operational data recordkeeping by electronic or hard copy monthly. Keep records of the throughput each month, as well as the total 

throughput for the last twelve months. Make records available for inspection by DEQ personnel. 

Submit report: Due annually, by the 31st of March. Report the throughput for the preceding calendar year to the Office of Environmental 

Compliance, Enforcement Division. 

GRP 0017 PST- Pressurized Storage Tanks 

G'oop Momb"" EQT 0088EQT 0089EQT 0090EQT 009t EQT 0092EQT 0093EQT 0094EQT 009SEQT 0096EQT 0097EQT 0098EQT 0099EQT OIOOEQT Otot EQT Ot02EQT Ot03EQT Ot04EQT OtOS 

EQTOI06 

354 [LAC JJ:lll.2103.B] Maintain working pressur~s sufficient at all times under no~al operating conditions to prevent vapor or gas loss to the atmosphere. 

Page 39 of.4~ TPOR0147 

---1 
· SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-V& 

Air- Title V Regular Permit Minor Mod 

CRG 0001 CD -Consent Decree Requlrments for Boiler and Heaters 

Group Members: EQT 0067F.QT 0068F.QT 0074EQT 007SEQT 0076EQT 0071t:QT 0078EQT 0079EQT 0080f.QT 0081 EQT 0082Jo:Q·r 008JEQT 0084 

355 [LAC 33.11LSOI.C.6] 

356 [LAC ll:lll 50LC.6] 

357 [LAC 33 111.50LC.6] 

UNF 0001 EF- Entire Facility 

358 [40 CFR 60.] 

359 (40 CFR 61.] 

360 [40CFR68.12(b)(l)) 

361 (40 CFR 68.12(b)(2)) 

362 [ 40 CFR 68.12(b)(3 )) 

363 (40 CFR 68.12(bX4l) 

Calumet shall undertake measures to reduce 502 emissions from refinery heaters and boile_rs by restricting 1125 in refinery fuel gas and by 

agreeing not 10 conhnuc and/or commence the burning of fuel oil except under the provisions set forth herein [SA-~M- I 0-0090]. 

Elimination of Fuel Oil Burning 

From the Effective Date of the Consent Decreet through termination, Calumet shall continue not to bum Fuel Oil in any existing heater or boiler, 

. except dunng natural gas curtailment.(SA-MM-1 0-0090). 

NSPS Applicability of lleaters and Boilers. 

a. L"pon the Effective Date of the Consent Dccn:c, the existing heaters and boilers at the facility, as that term is used in 40 C F.R Pan 60, 

Subparts A and J. and shall bc subject to and comply with the requirements ofNSPS Subparts A and J. Unless exempted by regulation, by no 

later than the Effective Date Of the Consent Decree, Cal~met shall install, ccnify, calibrate, maintain and operate a fuel gas CEMS at the Covered 

Refmcrics in accordance with the rcqUI_rements of 40 C.F.R. §§ 60.11, 60.13 and Part 60 Append1x A, and the applicable JXrformance 

specification test of 40 C.F.R. Part 60 Appcnd1ces R and F. These CEMS will be used to demonstrate compliance with emission limits. 

b. Compliance with the Consent Decree constitutes compliance with certain NSPS Subpart A requirements. for each fuel gas combustion 

device that becomes an "affected facility." as that term is used in 40 CF_R. Part 60, Subparts A and J, pursuant to this Paragraph 15 of the 

Consent Decree. compliance with the relevant monitoring requirements of this Consent Decree for such fuel gas combustion devices will satisfy 

the notice requirements of 40 C.F.R. 60.7(a) and the initial performance test requiremenLc; of 40 C.F.R. 60.8(a). 

c. If, prior to the tc:nnination of the Consent Decree, any heater, boiler or other fuel gas combustion device becomes subject to NSPS Subpart Ja 

for a particular pollutant due to a ''modification" (ac; that term is defined in the final Subpart Ja rule). the modified affected facility shall be 

subject to and comply with I'SPS Subpart Ja 10 lieu ofNSPS. Subpart 1 for that regulated pollutant Io wh1ch a standard applies as a result of the 

modification. 

d. If, prior to the termination of the Consent Decree, any heater, boiler or other fuel gas combll'ition device becomes subject to NSPS Subpart Ja 

due to a "reconstruction" (as that term is defined in the final Subpart Ja rule), the r~constructed facility shall be subject to and comply with NSPS 

Subpart Ja for all pollutants in lieu of Subpart J.[SA-MM-10-0090] 

All affected facilities shall comply Wlth all applicable provisions in 40 CFR 60 Subpart A. 

All affected facilities shall comply with all applicable provisions in 40 CFR 61 Subpart A. 

Equipment/operational data recordkeeping by electronic or hard copy continuoLtc;ly. Document that the nearest public receptor is beyond the 

distance to a toxic or flammable endpoint defined in 68.22. (40 CFR 68.12(b)(l)) 

Complete the five-year accident history for the process as provided in 68.42. (40 CFR 68.12(b)(2)] 

Ensure that response actions have been coordinated with local emergency planning and response agencies. (40 CFR 68.12(b)(3)] 

Include in the RMP the certification specified 10 68.12(b)(4). (40 CFR 68.12(h)(4)] 

Page 40 of 49 T'P()A01U 
UNF 0001 EF - Entire Facility 

364 [40 CFR 68.150] 

365 [40 CFR 68.155] 

366 [40CFR68.160] 

367 [40 CFR 68.165] 

368 [40 CFR 68.168] 

369 [40 CFR 68.180] 

370 [40 CFR 68.190(c)] 

371 [40CFR68.190] 

372 [40 CFR 68.200] 

373 [40 CFR 68.22] 

374 [40 CFR 68.25] 

375 [40 CFR 68.28] 

376 [40 CFR 68.30] 

377 [40 CFR 68.33] 

378 [40 CFR 68.36(b)] 

379 [40 CFR 68.36] 

380 [40 CFR 68.39] 

381 · [40 CFR 68.42] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 ., 

Permit Number: 3080.00010-VS 

Air- Title V Regular Permit Minor. Mod 

Submit Risk Management Plan (RMP): Due no later than June 21, 1999, or three years after the date on which a regulated substance is first 

Jisted under 68.130, or the date on which a regulated substance is first present above a threshold quailtity in'.\ process. Submit in a method and 

format to a central point as specified by EPA prior to JW1e 21, 1999. 

Provide .in the RMP an executive sununary that includes a brief description of the elements listed in 68.155(a) through (g). 

Complete a single registration form and include in the RMP. Covel- all regulated substances handled in covered processes. lnclude in the 

registration the information specified in 68.160(b)(1) through (13 ). 

Submit in the RMP information one worst-case release scenario for each Program 1 process. Include the data specified in 68.165(b)(l) through 

( 13). 

Submit in the RMP the information provided in 68.42(b) on each accident covered by 68.42(a). 

Provide in the RMP the emergency response information listed in 68.180(a) through (c). 

Submit revised registration to EPA: Due within six months after a stationary source is no longer subject to 40 CFR 68. Indicate that the 

stationary source is no longer covered. [40 CFR 68.190(c)] · 

Review and update the RMP as specified in 68.190(b) and submit it in a method and format to a central point specified by EPA prior to Jun·e 21, 

1999. . 

Maintairi records supporting the implementation of 40 CFR 68 for five years unless otherwise provided. 

Use the endpoints specified in 68.22(a) through (g) for analyses of offsite consequences. 

Analyze the release scenarios in 68.25, as specified in 68.25(a) through (h). 

Identify and analyze at least one alternative release scenario for each regulated toxic substance held in a covered process(es} and at least one 

alternative release scenario to represent all flammable substances held in covered processes, as specified in 68.28(b} through (e). 

Estimate in the RMP the population within a cifcle with its center ~t the point of the release and a radius determined by the distance to the 

endpoint defined in 68.22(a). · 

List in the RMP environmental receptors within a circle' with its center at the point of the release and a radius detennined by the distance to the 

endpoint defined in 68.22(a). 

Submit revised RMP: Due within six months after changes in processes, quantities stored or harldled. or any other aspect of the stationary source 

increase or decrease the distance to the endpoint by a factor of two or more. [40 CFR 68.36(b)] 

Review and update the offsite consequence analyses at least once evyry five years. COmplete a revised analysis Within six months if.changes in 

processes, quantities stored or handled, or any other aspect of the stationary source might reasonably be expected to increase or decrease the 

distance to the endpoint by a factor of two or more. · 

Equipment/operational data recordkeeping by electronic or hard copy continuously. Maintain the records specified in 68.39(a) through (e) on the 

offsite consequence analyses. · . 

lnclude in the five-year accident history all accidental releases from covered processes that resulted in deaths, injuries, or significant property 

damage on site, or known offsite deaths, injuries, evacuations, sheltering in place, property damage, or environmental damage. Include the 

information specified in 68.42(b )(I) through (I 0) for each accidental release .. 

Page41of49, TPOR0147 
UNF 0001 EF - Entire Facility 

3R2 (LAC 33:1111103) 

3X3 (LAC 331111303.8) 

384 (LAC 33:1112113 A) 

385 (LAC 33:111219] 

386 (LAC 33:111.2901.0) 

387 (LAC 33 IIL2901.F) 

388 (LAC 33:111501.841 

389 (LAC 33:111SOI.C.1 I 

390 (LAC 33:111.501.C6] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cot1on Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-()0010-VS 

Air- Title V Regular Permit Minor Mod 

Emissions of smoke which pass onto or across a public road and create a traffic hazard by Impairment of visibility as defined in' LAC 33:IIL Ill 

or intensify an extsting traffic hazard condition are prohibited. 

Emissions of particulate matter which pass onto or across a public road and create a traflic hazard by impairment of visibility or intensify an 

existing traffic hazard condition are prohibited. 

Maintain best practical housekeeping and maintenance practices at the h1ghcst possJble standards to reduce the quantity of organic compounds 

emissions. Good housekeeping shall include, but not be. limited to, the practices listed in LAC 33:111.2113.A.I-5. 

Failure to pay the prescribed application fee or annual fee as provided herein, within 90 days after the due date, will constitute a violation of 

these regulations and shall subject the person to applicable enforcement actions under the Louisiana Environmental Quality Act including. but 

not limited to, revocation or suspension of the applicable permit, license, registration. or variance. 

Discharges of odorous substances at or beyond property lines which cause a perceived odor intensity of six or greater on the specified eight point 

bulanol scale as dc1cnnmcd by Mc1hod 41 of LAC 33:111.2901.G arc prohibllcd. 

Jf requested to monitor for odor intensity, take and transport samples in a manner wh1ch minimizes alteration of the samples either hy 

contamination or loss of material. Evaluate all samples as soon after collection as possible in accordance with the procedures set forth in LAC 

33:111.290i.G. 

The owner or operator of any sowcc which IS not a major sowce rn.ay apply for an cxcmphon from the penrunmg requirements of this Chapter 

provided each of the following criteria arc met i. the source emits and has the potential to emit no more than 5 tons per year of any regulated air 

pollutant; ii. the source emits and has the potential to emit less than the minimum emission rate listed in LAC 33:111.51 I 2, Table 5 1.1, for each 

Louisiana toxic air pollutant; iii. no enforceable pcnnit conditions are necessary to ensure compliance with any applicable requirement; and IV. 

no public notice is required for any permitting or other activity at the source. Any source to which an exemption is granted under this Paragraph 

shall be operated in accordance with any terms stated in the exemption and upon which the decision to grant the exemption was based. Failure to 

operate the source in accordance with the tenns of the exemption may tenninate such exemption and shall constitute a violation of the general 

duty to operate under a pennit established pwsuant to Subsection C of this Section. 

Submit permit application: Due prior to construction, reconstruction or modification unless otherwise provided in LAC 33:11J.Chapter 5. 

Submit a timely and complete penn it application to the Office of Environmental Services, Air Penn its Division, as required in accordance with 

the procedures in LAC 33:111.Chaptcr 5. 

Annual Program. 

By no later than 180 days after the Effective Date of the Consent Decree, Calumet shall establish an annual program of reviewing process 

information for the facility, incl~ding but not limited to construction projects, to enswe that all new benzene waste streams arc included in the 

facility's waste stream inventory (SA-MM-10-0090) 

Page 42 of 49 TPQR01C7 
UNF 0001 EF -Entire Facility 

391 [LAC 33:111.501.C.6] 

392 [LAC 33:111.50i.C.6] 

393 [LAC 33:111.50i.C.6] 

394 [LAC 33:111.50i.C.6] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-0001 O-V6 

Air- Title V Regular Permit Minor Mod 

At Variable Times. 

As soon as practicable, but in no event later than 180 days after the effective date or establishment of any surviving emission limits, standards 

and schedules under Section V of the Consent Decree, Calumet shall submit appliCations to LDEQ to incorporate those emission limitations, 

standards, and/or schedules into the Title V permit of the Covered Refinery. Following submission of the permit applications, Calumet shall 

cooperate with LDEQ by promptly submitting to LDEQ all information that LDEQ seeks following its receipt of the permit applications.[SAMM-1 0-0090]. 

Benzene Spills. . 

For each spill at the facility after the Effective Date of of the Consent Decree, Calumet ·shall review such spills to delermine if benzene waste was 

generated. Calumet shall include benzene generated by such spills in the TAB for for the facility. [SA-MM-1 0-0090].' · 

Benzene Waste NESHAP Program Enhancements. 

In addition to continuing to comply with all applicable ;equirements of40 C.F.R. Part 61, Subpart FF (Benzene Waste, NESHAP, or Subpart 

FF), Calumet agrees to undertake the measures set forth in Paragraphs 33 through 45 of the Consent Decree to ensure continuing compliance _ 

with Subpart FF and to minimize or eliminate fugitiVe benzene.waste emissions.[SA-MM-10-0090]. 

cOmmercial Unavailability of Control Equipment. 

Calumet shall be solely responsible for compliance With anY deadline or the performance of any work described in Sections V and VI of the 

Consent Decree that requires the acquisition and installation of control equipment. If it appears that the conunercial unavailability of any control 

equipment may delay Calumet£,S performance of work according. to an applicable implementation schedule, Calumet shall notify LDEQ of any 

such delays as soon as Calumet reasonably concludes that the delay could affect its ability to comply wlth the implementation schedule set forth 

in the Consent Decree. Calumet shall propose for approval by LDEQ a modification to the applicable schedule of implementation. Prior to the 

notice required by this Paragraph VII in the Consent Decree, Cal~et must have contacted a reasonable number of vendors of sUch equipment or 

additive and obtained a written representation (or equivalent communication to LDEQ) from the vendor that the equipment is commercially 

unavailable. In the notice, Calumet shall reference this Paragraph VIII of the Consent Decree, identify the milestone date(s) it contends it will 

not be able to meet, provide LDEQ with written correspondence to the vendor identifying efforts made to secure the Cot:~trol equipment, and 

describe the specific efforts Calumet has taken and will continue to take to find such equipment. Calumet may propose a modified schedule or 

modification of other requirements of the Consent Decree to address such commercial unavailability. Section XV of the Cons~nt Decree 

("Dispute Resolution") shall govern the resolution of any claim of commercial unavailability. LDEQ shall not unreasonably withhold its consent 

to requests for modifications of schedules of implementation if the requirements of this Paragraph are met. All modifications to any dates 

initially set forth in the Consent Decree or in any approved schedule of implementation shall be signed in writing by LDEQ and Calwnet. 

Stipulated penalties shall not accrue nor be due and owing during any period between an originally-scheduled implementation date and an 

approved modification to such date; provided however, that LDEQ shall retain the right tO seek stipulated penalties if LDEQ does not approve a 

modification to a date or dates. The failure by Calumet to secure control equipment shall not constitute a force majeure event triggering the 

requirements of Section XIV of the Consent Decree; this Paragraph shall apply. [SA-MM-10-0090]. 

Page 43 of 49 TPOR0147 

." i •. • _" ~ I 
UNF 0001 EF -Entire Facility 

395 [LAC 33JII.501.C6) 

396 [LAC 331JL501.C6) 

397 [LAC 331JL501.C6) 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080~0010-VS 

Air- Title V Regul~r Pen\iii Minor''!'lod 

Current Compliance Status and Refinery Compliance Slarus Changes 

As of the Effective Date of the Consent Decree Calumet believes that the facility has a Total Annual Benzene (TAB) of less than 10 Mglyr. 

Calwnet will review and verify the TABs at the facilityis consistent with the requirements of Paragraph 35 of the Consent Decree. If al any time 

from the Effective Date of the Consent Decreet through its termination is determined to have a TAB equal to or greater than 10 Mg/yr, Calumet 

shall comply with the compliance option set forth at 40 C.F.R. § 61.342(e) (heremafter referred to a< the "6 BQ compliance option") [SA-MM1 0-0090) 

Exception to General Prohibition. 

a. Conditions Precedent to Utilization of the Exception to the General Prohibition against the Use or Generation of the Consent Decree 

Emissions Reductions. Utilization of the exception set forth in Paragraph 72.b in the Consent Decree to the general prohibition against the 

generation or utilization of the Consent Decree Emissions Reductions set forth in Paragraph 72 in the Consent Decree is subject to the followlng 

conditions: 

i. Under no circumstances shall Calumet use the Consent Decree ~missions Reductions for netting and/or offsets prior to the time that acrual the 

Consent Decree Emissions Reductions have occUITed; 

ii. Consent Decree Emissions Reductions may be used only at the Covered Refinery that generated them; 

iii. The Consent Decree Emissions Reductions provisions of this Consent Decree are for pw-poses of this Consent Decree only and neither 

Calumet, nor any other entity may use t~e Consent Decree Em1ssions Reductions for any purpose, including in any subsequent permitting or 

enforcement proccedmg, except as provided herein; and 

iv. Calumet still shall be subject to all federal an.d state regulations applicable to the PSD, major non-attainment and/or minor NSR pennining 

process. 

b. Exception to General Prohibition. Notwithstanding the general prohibition set forth in Paragraph 71 in the Consent Decree Calumet may use 

20 tons per year ofNOx and I 0 tons per year of VOCs from the Consent Decree Emissions Reductions as credits or offsets in any PSD, major 

non-attainment and! or minor NSR permit or permit proceeding occurring after the Effective Date of the Consent Decree, provided that the new 

or modified emissions unit is being constructed or nlodified for purposes of compliance with Tier II gasoline or low sulfur diesel requirements; 

and already has emissions limits at the time of permitting as follows: 

i. For heaters and boilers. a limit of0.020 lbs NOx per million BTU or less on a 3-hour rolling average basis; 

ii. For heaters and boilers, a limit ofO.IO grams of hydrogen sulfide per dry standard cubic foot of fuel gas or 20 ppmvd S02 corrected to 0% 02 

both on a 3-hour rolling average: · :·- _ · '· : . · •1 

iii. For heaters and boilers, no liquid or solid fuel fuing ~-~pabiiities! and i 

iv. For SRPs, NSPS Subpart J emission limits.[SA-MM-10-0090). 

General Prohibition. 

Calum~t shall not generate or use any NOx, S02, PM, VOC. or CO emissions reductions that result from any projects conducted or controls 

required pursuant to the Consent Decree as nening reductions or emissions offsets in any PSD, major non-anainment anc.Vor minor New Sowce 

Review (NSR) pennit or pennit proceeding.[SA-MM-10-0090). 

Page 44 of 49 T~DI•7 
UNF 0001 EF -Entire Facility 

398 [LAC 33:111.501.C.6] 

399 [LAC 33:111.501.C.6] 

400 [LAC 33:111.501.C.6] 

SPECIFIC REQUIREMENTS 

AI 10: 312 - Calumet lubricants Co -Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-Q0010-V6 

Air- Title V Regular Permit Minor Mod 

Outside the Scope of the General Prohibition. 

Nothing in the Section VII in the Consent Decree is intended to prohibit Calumet from seeking to: ( 1) utilize or generate emissions credits or 

reductions from refinery units that are covered bythe consent Decree to the extent that the proposed credits or reductions represent the difference 

between the emissions limitations set forth in the COnsent Decree for these refinery units and the more stringent emissions limitations that 

Calumet may elect to accept for these refinery units in a permitting process; or (2) utilize or generate emissions credits or reductions on refinery 

~}nits that are not covered by the Consent Decree.[SA-MM-1 0-0090). 

Securing Permits. 

For any work under Sections V or VI of the Consent Decree that requires a federal, state and/or local permit or approval, Calumet shall be 

responsible for submitting in a timely fashion applications for federal, state and local pennits and approvals for work and activities required so 

that permit or approval decisions can be made in a timely fashion. Calumet shall use its best efforts to: (I) submit permit applications (i.e., 

applications for permits to construct, operate, or their equivalent) that comply with all applicable requirements; and (2) secure approval of 

permits after filing the applications, including timely supplying additional information, if requested. If it appears that the failure of a 

governmental entity to act upon a timely-submitted permit application may delay Calumet[.s performance of work according to an applicable 

implementation schedule, Calumet shall notifY LDEQ of any such delays as soon as Calumet reasonably concludes that the delay could affect its 

ability to comply with the implementation schedule set forth in the Consent Decree. Calumet shall propose for approval by LDEQ a modification 

to the applicable schedule of implementation. LDEQ shall not unreasonably withhold its consent to requests for modifications of schedules of 

implementation if the requirements of this Paragraph are met. All modifications to any dates initially set forth in this Settlement or in any 

approved schedule of implementation shall be signed in writing by LDEQ and Calumet. Stipulated penalties shall not accrue nor be due and 

owing during any period between an originally-scheduled impl.ementation date and an approved modification to such date; provided however, 

that LDEQ shall retain the right to seek stipulated penalties if LDEQ does not approve a modification to a date or dates. The failure of a 

governmental entity to act upon a timely-submitted permit or approval application shall not constitute a force majeure event triggering the 

requirements of Section XIV of the Consent Decree; this Paragraph shall apply.[SA-MM-10-0090]. 

Tail Gas Incidents: 

a. Investigation, Reporting, Corrective Action and Stipulated Penalties. The Cotton Valley Refinery does not have Tail Gas Treatment Units; 

therefore, the Cotton Valley has not had any Tail Gas Incidents. The provisions of this Paragraph 30 of the Consent Decree are not applicable to 

the Cotton Valley unless the facility adds a Tilil Gas Treatment Unit. For Tail Gas Incidents shall follow the same investigative, reporting, 

corrective action and assessment of stipulated· penalty procedures as those outlined in Paragraphs 26 - 28 of the Consent Decree for Acid Gas 

Flaring Incidents. Those procedures shall be applied to TGTU shutdowns, bypasses of a TGTU, unscheduled shutdowns of a Sulfur Recovery 

Plant, or other miscellaneous unscheduled Sulfur Recovery Plant events which result in a Tail Gas Incident (SA-MM-1 0-0090] . 

Page 45 of 49 TPOR0147 
UNF 0001 EF • Entire Facility 

401 [LAC ll:IILIOI.C.6} 

402 [LAC JJ:IIL501.C.6J 

403 (LAC Jl:lll 507.A.I.a} 

404 (LAC 33 IIL507.A.I.b} 

405 [LAC 33:111.507.A.I.c) 

406 [LAC 3311L507.A.I.d} 

Training 

-SPECIFIC REQUIREMENTS 

AI 10: 312 ·Calumet Lubricants Co ·Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080.00010·V6 

Air· Title V Regular Permit Minor Mod 

a. Calumet currently has one employee who draws benzene waste samples for BenZene Waste r\ESHAP ptuposcs at the facility. By no later 

than I 80 days after the Effective Date of the Consent Decree, Calumet shall develop and begin implementation of annual (i.e.: once each 

calcnd~ year) "refresher" training for that employee. Calumet shall also provide annual training to all other employees who draw beru:cne waste 

samples for Benzene Waste NESHAP purposes. 

b_ If and when the facility's TAB reaches 10 Mg!yr or more, Calumet shall complete the development of standard operating procedures for all 

control equipment used to comply with the Benzene Waste NESHAP. Calumet shall complete an initial training program regarding these 

procedwes for all operators assigned to this equipment. Comparable trainiJlg shall be provided to any persons who subsequently become 

operators, prior to their assumption of this dury. "Refresher" training shall b~ perfonned on a periodic basis. Calumet shall propose a schedule 

for the initial and refresher training at the same time that Calumet proposes a plan, pursuant to either Paragraph 36.b ot the Consent Decree, or 

Paragraph 4J.d of the Consent Decree, that identifieS the compliance strategy and schedule that Calumet will implement to come into compliance 

with the 6 BQ compliance option. 

c. As part of Calumet's training program, it must ensure that the employees of any contractors htred to perfOrm the requirements of this 

Paragraph are properly tratned to implement all provisions ofthas Paragraph at the facility_ [SA-MM-1 0--0090]. 

Within 180 Days After the Effective Date of the Consent Decree. As soon as practicable followmg the Effective Date of the Consept Decreet. 

but in no event later than 180 days followmg the Effective Date of the Consent Decree, Calumet shall submit applications to LDEQ to 

incorporate the surviving emission lim1ts, standards, and/or schedules required by the Consent Decree: that are effective as of the Effective Date 

of the Consent Decree mto the Title V permit of the Covere.d Refinery. Following submission of the pennit applications, Calumet shall · 

cooperate with LDEQ by promptly submitting to LDEQ all information that LDEQ S<eks following ats receipt of the permit applications.[SA· 

MM·l 0-0090]_ 

Any maJor sowce as defined in LAC 33:111.502 is designated a Part 70 sowce and is required to obtain a permit which will meet the 

requirements of LAC 33:111.507. 

Any nonmajor (area) source of hazardous air pollu~nts required to obtain an operating permit pursuant to regulations promulgated under section 

112 of the federal Clean Air Act is designated a Part 70 source and is required to obtain a permit which will meet the requirements of LAC 

33:111.507. 

Any nopmajor sowce required to obtain an operating pennit pursuant to regulations promulgated under section I ,II of the federal Clean Air Act 

is designated a Part 70 source and is requtred Ia obtain a permit which will meet the requirements of LAC 33:111.507. 

Any affected source, as defined in LAC 33:111.502, pursuant to the acid rain provisions of title IV of the federal Clean Air Act is designated a 

Part 70 source and is required to obtain a permit which will meet the requirements of LAC 33:111.507. 

Page 46 of 49 Tl'QROI<H 
UNF 0001 EF- Entire Facility 

407 [LAC 33:111.507.8.2] 

408 [LAC 33:lll.507.C.I] 

409 [LAC 33:111.507.C.3] 

410 [LAC 33:111.507.E.4] 

411 [LAC 33:111.511] 

412 [LAC 33:111.517.A.1] 

413 [LAC 33:111.517.A.2] 

414 [LAC33:111.517.B.I] 

SPECIFIC REQUIREMENTS 

AIID: 312- Calumet lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080-00010-VS 

Air- Title V Regular Permit Minor Mod 

No Part 70 source may operate after the time that the owner or operator of such source is required to submit a permit application under 

Subsection C of this Section, unless an application has been submitted by the submittal deadline and such application provides information 

addressing all applicable sections of the application form and has been certified as complete in accordance with LAC 33 :Ill.517 .8.1. No Part 70 

source may operate after the deadline provided for supplying additional information requested by the permitting authority under LAC 33:111.519, 

unless such additional informatio!l has been submitted within the time specified by the permitting authority. Permits issued to the Part 70 source 

under this Section shall include the elements required by 40 CFR 70.6. The Louisiana Department of Environmental Quality hereby adopts and 

incorporates by reference the provisions of 40 CFR 70.6(a), as in effect on July 21, 1992. Upon issuance of the permit, the Part 70 source shall 

be operated in compliance with all terms and conditions of the perriut~ Noncompliance with any federally applicable term or condition of the 

permit shall constitute a violation of the Clean Air Act and shall be 'grounds for enforcement action; for permit termination, revocation and 

reissuance, or revision; or for denial of a Permit rene'wal application. 

Any Part 70 source for which construction or operation has begun prior to the effective date of LAC 33:III.507 shall submit an application for an 

_initial Part 70 permit. Permit applications shall be prepared in accordance with LAC 33:111.517 and with forms and guidance provided by DEQ. 

and shall be submitted no later than one year after the. effective date of the Louisiana Part 70 program. 

Any source that becomes subject to the requirements of LAC 33 :lll.507 after the effective date of the Louisiana Part 70 program due to 

regulations promulgated by the Environmental Protection Agency or by the Department of Environmental Quality shall submit an application to 

the Office of Environmental Services, Air Permits Division, in accofdance with the requirements established by the applicable regulation. In flO 

case shall the required application be submitted later than one year from the date on which the source first becomes subject to LAC 33:Ill.507. 

Any permit application to renew an existing pennit shall be submitted at least six months prior to the date of permit expiration, or at such earlier 

time as may be required by the existing permit or approved by the permitting authority. In no event shall the appliCation for permit renewal be 

submitted more than 18 months before the date of permit expiration. 

Submit notification: Due to the permitting authority prior to the initiation of any project which will result in emission reductions. Include in the 

notification a description of the proposed action, a location map, a description of the composition of air contaminants involved, the rate and 

temperature of the emissions, the identity of the sources involved and the change in emissions. Make any appropriate permit revision reflecting 

the emission reduction no later than 180 days after commericement of operation and in accordance with the procedures of LAC 33:JII.Chapter 5. 

Submit permit application: Due prior to commencement of construction, reconstruction, or modification of the source, for new or modified 

sources. Do not commence construction, reconstruction, or modification of any source required to be permitted under LAC 33:III.Chapter 5 prior 

to approval by the permitting authority. ' 

Submit permit application: Due by the date established for' submittal in accordance with LAC 33:lll.507.C. The permit application is for an 

initial permit to be issued in accordance with LAC 33: IIi.507. Provide a copy of each permit application pertaining to a major Part 70 source to 

EPA at the time of application submittal to the permitting authority. 

Any application form, report, or compliance certification submitted under this Chapter-shall contain certification by a responsible official of 

truth, accuracy, and completeness. The certification shall state that, based on information and belief formed after reasonable inquiry, the 

statements and information contained in the application are true, accurate, and complete. 

Page 47 of 49 TPOR0147 
UNF 0001 EF - Entire Facility 

415 [LAC 33:111517.CJ 

416 (LAC 33:111.517.0] 

417 (LAC Jl:111.517.E] 

418 (LAC JJ:111517.GJ 

419 (LAC 33 111535] 

420 (LAC 33 111.5609AI.b] 

421 (LAC 33 111 5609 A 2 b) 

422 (LAC 33:1115609.A.3.b] 

423 [LAC 33:111.5609.A) 

424 (LAC 33:111.5611.A) 

425 [LAC 33:1115611.B) 

426 [LAC 33:111.5901.A] 

427 (LAC 33:111.5907] 

428 [LAC 33:111.5911.A) 

429 [LAC 33:111.5911.C] 

430 [LAC 33:111.919] 

431 (LAC 33:111.927] 

 

SPECIFIC REQUIREMENTSAIID: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120002 

Permit Number: 3080.00010-VS 

Air- Title V Regular Permit Minor Mod 

Suhmit supplementary facts or corrected information: Due promptly upon becoming aware of f3ilurc to submit or incorrect submittal regarding 

permit applications. In add1tion, provide information as necessary to address any requirements that become applicable to the source after the 

date of tiling a complete application but prior to release of a proposed permit 

Submit applications for perrrUts in accordance with forms and guidance provided by the DEQ. At a mmimum, each permit application submitted 

under LAC 33:iii.Chaplcr 5 shall contain lhe mformalion spccJficd in LAC 33:111.517.D, subparagraphs 1-18. 

In addition to those elements listed under LAC 33:1Il.S17.D, include in each application pertaining to a Pan 70 source the information specified 

in LAC 33:111.517 E. Subparagraphs I -8. 

Submit change ofovroership notification in accordance with LAC 33:l.Chaptcr 19. 

Comply with the Part 70 General Conditions as set forth in LAC 33:111.535 and the Louisiana General Conditions as set forth in LAC 33:111.537 

[LAC 33 iii535. LAC 33 iii537] 

Activate the preplanned abatement strategy listed in LAC 33:111.5611.Table 5 when the administrative authority declares a~ Air Pollution Alert. 

Activate the preplanncd strategy listed in LAC 33:111.5611 Table 6 when the administrative authority declares an Air Pollution Warning 

Activate the preplanned abatement strategy listed in LAC 33:111.5611 .Table 7 when the administrative authority declares an Air Pollution 

Emergency. 

Prepare standby plans fOr the reduction of emissions during periods of Air Pollution Alert, Air Pollution Warning and Air Pollution Emergency 

Design standby plans to reduce or eliminate emissions in accordance with the objectives as set forth m LAC 33:111.56JI.Tables 5, 6, and 7. 

. Submit standby plan for the reduction or elimination of emissions during an Air Pollution Alert. Air Pollution Warning, or Air Pollution 

Emergency: Due within 30 days after requested by the administrative authority. 

During an Air Pollution Alert, Air Pollution Warning or Air Pollution Emergency, make the standby plan available on the premises to any person 

authorized by the department to enforce these regulations. 

Comply with the provisions m 40 CFR 68, except as specified in LAC 33:111.5901. 

Identify hv.ards !hal may result from accidental releases oft he substances listed in 40 CFR 68. I 30, Table 59.0 of LAC 33:iii.5907, or Table. 

59. I of LAC 33:111.59 I 3 using appropriate hazard assessment techniques, design and maintain a safe facility, and minimize the ofT-site 

consequences of acctdental releases of such substances that do occur. 

Submit regtstration: Due January 31, 1998, or within 60 days after the source becomes subject to LAC 33:111.Chaptc:r 59, whichever is later. 

Include the informallon listed in LAC 33:111.59JI.B, and submit to the Department of Environmental Compliance 

Submit amended registration: Due to the Office of Environmental Compliance within 60 days after the information in the sub mined registration 

is no longer accurate. 

Submit Emission Inventory (El)/Annual Emissions Statement: Due annually, by the 30th of April to the Office of Environmental Services, for the 

reponing period of the previous calendar year that coincides with period of ownership or operatorship, unless otherwise: directed by DEQ. 

Submit bo~ an emissions inventory and the certification statement required by LAC 33:111.919.F.I.c, separately for each AI, in a format 

specified by DEQ. include the information specified in LAC 33:111.919.F.1.a through F. I .d. 

Report the unauthorized discharge of any air pollutant into the atmosphere in accordance with LAC 33:1.Chapter 39, Notification Regulations 

and Procedures for Unauthorized Discharges. Submit written reports to the department pursuant to LAC 33:1.3925 Submit timely and 

appropriate follow-up reports detailing methods and procedures to be used to prevent similar atmospheric releases. 

Page :48 ol49 TPOA01•7 
SPECIFIC REQUIREMENTS 

AI 10: 312- Calumet Lubricants Co- Cotton Valley Refinery 

Activity Number: PER20120.002· 

Permit Number: 3080-0001 O-V6 

Air- Title V Regular Permit Minor Mdd 

:. 

iii 

t '• ~ 

Pag~e 49 of. 49 

,'I ~, 

TPOR0147