P.1 

RCRA Box 321 

Prepped by Ryan Dugan 

Document Number: 

236) OGRC-S0029 

Docket Number: 

F-93-OGRC-FFFFF 

Printed 5/8/2007 3:36:33 PM Sheet 236 of 259 
P.2 

KANSAS HEALTH AND ENVIRONMENTAL LABORATORY 

Department of Health and Environment 

Biochemical Analysis Laboratory 

Bldg. 740, Forbes Field, Topeka, KS 66620-8420 

(913) 296-1657 

OCrRtz.SOOdic\ 

RESULTS OF LABORATORY ANALYSES 

Report To: 

Address: 

TOM GROSS-fl&Wtt Lab Number: 101675PT 

Lab Acct Code: WM 

Env Acct Code: HD 

Locality: ARNOLD BRINE (WALLACE ENERGY INC ARNOLD NESS CO) 

Collected By: KAREN SCHMIDT Time: 1130 

Site ID: Matrix: Water 

Comments: #5 

Depth: 

Date Collected: 

Date Received: 

Date Reported: 

1-15-91 

1-17-91 

1-31-91 

Results Expressed In Milligrams/Liter 

Total Hard. 

(CaC03) 

Calcium 

Magnesium 

8999 

2783 

500 

Sodium 17430 

Potassium 

Total Alk. 

(CaC03) 

Chloride 

Sulfate 

Nitrate (N) 

Nitrite 

Fluoride 

Cyanide 

Oil/Grease 

Phenols 

TDP 

Sulfide 

Total Coliform 

Fecal Coliform 

Fecal Strep 

Chemist: FD 

000 

139 

000 

382.26 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

pH (Units) 

Turbidity (NTU) 

Spec. Conductance 

(micromhos/cm) 

T. Dissolved Solids 

Total Phosphorus (P) 

Silica (Si02) 

Boron 

Dissolved Oxygen 

BOD 

COD 

CBOD 

Ammonia (N) 

T. Sus. Solids 

Corrosivity (LI) 

Kjeldahl Nitrogen 

Chromium (+6) 

Tin 

MBAS 

Flash Pt (Celsius) 

NA - Not Analyzed 

NA 

NA 

NA 

NA 

NA 

20.959 

10.565 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

NA 

Aluminum 

Antimony 

Arsenic 

Barium 

Beryllium 

Cadmium 

Chromium 

Cobalt 

Copper 

Iron 

Lead 

Manganese 

Mercury 

Molybdenum 

Nickel 

Selenium 

Silver 

Thallium 

Vanadium 

Zinc 

LT -

LT 

LT 

LT 

LT 

LT 

LT 

LT 

LT 

.-

Less 

0.35 

0.02 

0.100 

0.222 

0.001 

0.003 

0.009 

0.004 

0.014 

12.214 

0.100 

1.267 

NA 

0.001 

0.016 

0.120 

0.004 

0.015 

0.003 

0.104 

Than 

Copy To: File 

KAREN SCHMIDT-NWD-HAYS 

RON SMITH-BAWM 

DECEIVED 

BUREAU OF 

m 0 4 1991 

AIR and WASTE 

.MANAGEMENT 
P.3 

KANSAS IPARTMENT OF HEALTH AND EF "RONMENT 

Kansas Health & Environmental Laboratory 

Organic Chemistry Laboratory 

Topeka, Kansas 66620 

GC/MS ANALYSIS REPORT 

Report To: 

Address: 

TOM GROSS-BAWM 

FORBES BLDG. 740, TOPEKA, KS 66620 

SAMPLE COLLECTION INFORMATION 

Lab Number: 

Report Date: 

101788OC 

1-25-91 

Site ID No.: SAMPLE#6 Program Code: HD Sample Type: WATER 

Collection Site: ARNOLD BRINE-WALLACE ENERGY INC, ARNOLD, NESS CO. 

Collected By: BAWM-SCHMIDT, KAREN Date: 1-15-91 Time: 

' RESULTS OF ANALYSIS 

1130 

PURGABLE ORGANICS 

CHLOROMETHANE 

BROMOMETHANE 

VINYL CHLORIDE 

CHLOROETHANE 

DICHLOROMETHANE 

1,1-DICHLOROETHYLENE 

1,1-DICHLOROETHANE 

TRANS &/OR CIS 1,2-DICHLOROETHYLENE 

TRICHLOROMETHANE (THM) 

1,2-DICHLOROETHANE 

1,1,1-TRICHLOROETHANE 

TETRACHLOROMETHANE 

BROMODICHLOROMETHANE (THM) 

1,2-DICHLOROPROPANE 

TRANS 1,3-DICHLOROPROPENE 

TRICHLOROETHYLENE 

BENZENE 

DIBROMOCHLOROMETHANE (THM) 

CIS 1,3-DICHLOROPROPENE 

1,1,2-TRICHLOROETHANE 

BROMOFORM (THM) 

1,1,2,2-TETRACHLOROETHANE 

TETRACHLOROETHYLENE 

TOLUENE 

CHLOROBENZENE 

ETHYLBENZENE 

META-XYLENE 

ORTHO &/OR PARA-XYLENE 

1,3-DICHLOROBENZENE 

1,2-DICHLOROBENZENE 

1,4-DICHLOROBENZENE 

Comment: MANY PETROLEUM TYPE HYDROCARBON COMPOUNDS WERE INDICATED. 

Concentration 

(UG/L) 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

39.9 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED . 

NOT DETECTED 

136 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

285 

NOT DETECTED 

26.4 

136 

139 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

Reporting Limit 

(UG/L) 

100 

24.0 

16.0 

74.0 

18.0 

12.0 

10.0 

10.0 

10.0. 

12.0 

14.0 

14.0 

10.0 

10.0 

16.0 

12.0 

10.0 

14.0 

18.0 

12.0 

30.0 

12.0 

22.0 

10.0 

10.0 

14.0 

12.0 

12.0 

20.0 

20.0 

20.0 

Analyst: FRANK ZHANG P 

Copy To: KAREN SCHMIDT-NWD HAYS 

RON SMITH-BAWM 

Roger H. Carlson, Ph.D., Director 

;; RECEIVED" 

BUREAU OF 

JAN 3 1 1991 

AIR and WASTE 

MANAGEMENT 
P.4 

KANSAS APARTMENT OF HEALTH AND EF RONMENT 

Kansas Health & Environmental Laboratory 

Organic Chemistry Laboratory 

Topeka, Kansas 66620 

ANALYTICAL REPORT 

Report To: 

Address: 

TOM GROSS-BAWM 

FORBES BLDG. 740, TOPEKA, KS 66620 

SAMPLE COLLECTION INFORMATION 

Lab Number: 

Report Date: 

101789OC 

1-22-91 

Site ID No.: SAMPLE#6 Program Code: HD Sample Type: 

Collection Site: ARNOLD BRINE-WALLACE ENERGY INC, ARNOLD, NESS CO. 

Collected By: BAWM-SCHMIDT, KAREN 

COMPOUND 

ORTHO-CRESOL 

PARA-CRESOL 

2,4-DINITROTOLUENE 

HEXACHLOROBENZ ENE 

HEXACHLOROBUTADIENE 

HEXACHLOROETHANE 

NITROBENZENE 

PENTACHLOROPHENOL 

2,4,6-TRICHLOROPHENOL 

2,4,5-TRICHLOROPHENOL 

Analyst: DENNIS L. DOBSON , A 

Copy To: KAREN SCHMIDT-NWD HAYS 

RON SMITH-BAWM 

WATER 

Date: 1-

ANALYSIS 

Concentration 

(MG/L) 

0.087 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

Roger H. 

-15-•91 

Carlson, 

Time: 1130 

Reporting Limit 

(MG/L) 

— 

0.050 

0.050 

0.050 

0.050 

0.050 

0.050 

0.250 

0.050 

0.050 

Ph.D., Director 

RECEIVED 

BUREAU OF 

JM 2 fl 1991 

AIR and WASTE 

MANAGEMENT 
P.5 

KANSAS PARTMENT OF HEALTH AND ENVIRONMENT 

Kansas Health & Environmental La*, ratory 

Organic Chemistry Laboratory 

Topeka, Kansas 66620 

•riC ' l 

ANALYTICAL REPORT 

Report To: 

Address: 

TOM GROSS-BAWM 

FORBES BLDG. 7 40, TOPEKA, KS. 66620 

SAMPLE COLLECTION INFORMATION 

Lab Number: 

Report Date: 

101708OC 

1-10-91 

Site ID No.: Program Code: HD Sample Type: OIL 

Collection Site: ARNOLD BS, WALLACE ENERGY, INC., ARNOLD 

Collected By: Date: 1- 3-91 Time: 1200 

COMPOUND 

HEXACHLOROETHANE 

NITROBENZENE 

HEXACHLOROBUTADIENE 

2,4-DINITROTOLUENE 

HEXACHLOROBENZENE 

2,4,6-TRICHLOROPHENOL 

PENTACHLOROPHENOL 

ORTHO-CRESOL 

PARA-CRESOL 

2,4,5-TRICHLOROPHENOL 

RESULTS OF ANALYSIS 

Concentration 

(MG/KG) 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

Analyst: DENNIS L. DOBSO^ r 

Copy To: KAREN SCHMIDT-NWD-HAYS 

Reporting Limit 

(MG/KG) 

1.5 

0.8 

0.8 

1.5 

0.8 

1.5 

3.8 

0.8 

1.5 

1.5 

Roger H. Carlson, Ph.D., Director 

iRECEIV" : 

\ BUREAU Cr 

JAN 1 5 1991 

A!fM:-VM-
P.6 

KANSAS PARTMENT OF HEALTH AND EN" "RONMENT 

Kansas Health & Environmental La., oratory 

Organic Chemistry Laboratory 

Topeka, Kansas 66620 

ANALYTICAL REPORT 

Report To: TOM GROSS-BAWM 

Address: FORBES BLDG. 740, TOPEKA, KS 66620 

SAMPLE COLLECTION INFORMATION 

Lab Number: 

Report Date: 

101707OC 

1-10-91 

Site ID No.: 

Collection Site: 

Collected By: 

Program Code: HD 

ARNOLD WASTE, WALLACE ENERGY, INC 

Date: 

'RESULTS OF ANALYSIS 

Sample Type: OIL 

, ARNOLD 

1- 3-91 Time: 1200 

COMPOUND 

HEXACHLOROETHANE 

NITROBENZENE 

HEXACHLOROBUTADIENE 

2,4-DINITROTOLUENE 

HEXACHLOROBENZENE 

2,4,6-TRICHLOROPHENOL 

PENTACHLOROPHENOL 

ORTHO-CRESOL 

PARA-CRESOL 

2,4,5-TRICHL0ROPHEN0L 

Analyst: DENNIS L. DOBSON ^ 

Copy To: KAREN SCHMIDT-NWD-HAYS 

Concentration 

(MG/KG) 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

Reporting Limit 

(.MG/KG) 

1 

0 

0 

1 

0 

1 

4 

0 

1 

.1 

Roger H. Carlson, Ph.D., Director 

BUriAU OG 

JAN 1 5 1991 

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ANALYST: FRAN< ZHANG T* ?0'3ER H . CARLSON/ PH.D. / 3IRECT0 R 
P.9 

TCLP REPORT 

EPA Method 1311 

Federal Register, Vol. 55, No. 126 

Friday, June 29, 1990 

Sample Collected By: Client (Karen Schmidt) 

Date Collected: 1/3/91 

Received In Lab: 1/11/91 

Date Reported: 1/22/91 

Sample 

Lab No. 91 71 

Client: Ks. Dept. of Health & Environment 

Bureau of Air and Waste Management 

Forbes Field 

Topeka, Kansas 66620-7202 

Description: Solid Waste 

Sample #3 - Arnold Waste 

Wallace Energy. Inc., Arnold, Ks. (Ness Co.) 

ANALYTES 

Benzene 

Carbon Tetrachloride 

Chlorobenzene 

Chloroform 

1,4-Dichlorobenzene 

1,2-Dichloroethane 

1,1-Dichloroethylene 

Methyl Ethyl Ketone 

Tetrachloroethylene 

Trichloroethylene 

Vinyl Chloride 

Hexachloro-1,3-Butadiene 

Hexachloroethane 

Nitrobenzene 

Pyridine 

Chlordane 

2,4-Dinitrotoluene 

Endrin 

Heptachlor 

Heptachlor Epoxide 

Hexachlorobenzene 

Lindane 

Methoxychlor 

Toxaphene 

2.4-D 

2.4,5-TP (Silvex) 

o-Cresol 

m-Cresol 

p-Cresol 

Cresol (Total) 

Pentachlorophenol 

2,4,5-Trichlorophenol 

2,4.6-Trichlorophenol 

RESULTS 

mg/l 

0.33 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

DETECTION 

LIMIT 

mg/l 

0.05 

0.05 

0.05 

0.05 

0.05 

0.05 

0.05 

0.50 

0.05 

0.05 

0.05 

TCLP LIMIT 

mg/l 

0.5 

0.5 

100.0 

6.0 

7.5 

0.5 

0.7 

200.0 

0.7 

0.5 

0.2 

0.5 

3.0 

2.0 

5.0 

0.03 

0.13 

0.02 

0.008 

0.008 

0.13 

0.4 

10.0 

0.5 

10.0 

1.0 

200.0 

200.0 

200.0 

200.0 

100.0 

400.0 

2.0 

EXTRACT ANALYSIS 

METHOD 

EPA SW-846 / Method 8240 

EPA SW-846 7 Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 7 Method 8240 

EPA SW-846, / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8240 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8080 

EPA SW-846 / Method 8150 

EPA SW-846 / Method 8150 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8270 

EPA SW-846 / Method 8270 

COMMENT: Sample was collected in an inappropriate plastic sample container and sample quantity was barely 

sufficient to perform analyses requested. 

* Not requested by client. 

Analysis By: J^to^^Ap A 

Susan J. Snyber/Kimoeriv 

1. Approved By: 

Snyewr/Kimberly Brokmann Michael A. Dalrymple, P.E 

President 

M.D. Chemical and Testing Co., Inc., P.O. Box 67094, Topeka, Kansas 66667 
P.10 

M.D. Chemical and Testing Co., Inc. 

P.O. Box 67094, Forbes Field, Bldg 281, Topeka, Kansas 66667 

(913)-862-3500 

FAX(913)-862-5132 

•CERTIFICATE OF ANALYSIS *»***»*•*»*•• 

Name & Address of Client: Ks. Dept. of Health & Environment 

Bureau of Air & Waste Management 

Forbes Field 

Topeka, Ks. 66620-7202 

Exact Sampling Point: Wallace Waste 

Sample Type: Representative 

Sample Collected by: Client 

Sample preserved by: Client 

Sampled: 

Rec'd in Lab: 

Date Reported: 

Date Analyzed: 

DATE TIME 

see below 

1/14/91 

1/23/91 

see below 

1:45 PM 

1/22/91 

Sample date: 

Sample time: 

Lab# 

Sample Description 

TEST PARAMETER 

Arsenic 

Barium 

Cadmium 

Chromium 

Lead 

Selenium 

Silver 

Mercury 

1/2/91 

1530 

9169 

Smpl.#1 

(mg/L) 

]• 

1.054 

63.9 

0.36 

2.43 

8.84 

0.072 

0.22 

ND(0.002) 

1/2/91 

1530 

9170 

Smpl.#2 

(mq/kq) 

0.450 

9.31 

1.03 

3.43 

11.3 

ND (0.05) 

ND (0.5) 

ND(0.1) 

1/3/91 

1200 

9171 

Smpl.#3 

(mq/kq) 

0.129 

ND (2.0) 

0.68 

2.04 

3.88 

ND (0.05) 

ND (0.5) 

ND(0.1) 

1/3/91 

1200 

9172 

Smpl.#4 

(mq/kq) 

0.087 

ND (2.0) 

0.63 

1.99 

4.86 

ND (0.05) 

ND (0.5) 

ND(0.1) 

1/2/91 

1530 

EPA 

TCLP 

LIMIT 

mq/kq 

100 

2000 

20 

100 

100 

20 

100 

4.0 

TEST 

METHOD' 

3050/7060 

3050/7080 

3050/7130 

3050/7190 

3050/7420 

3050/7740 

3050/7760 

3050/7470 

ANALYST 

HK 

HK 

HK 

HK 

HK 

HK 

HK 

HK 

NA = Not Available 

ND (), where noted, indicates none detected with the detection limit in parentheses 

* Test Methos for Evaluating Solid Waste, EPA Publication SW-846,3rd Ed., Nov., 1986. 

Total Metal Analyses were requested on these samples. 

The results of total analyses are reported because the TCLP method states that if a total analysis demonstrate 

that the analytes of interest are present in a waste but below the regulatory level, the TCLP Extraction need 

not be run. Since the ratio between sample and liquid is 20:1 in all TCLP fractions, a leachate concentration 

may be obtained by dividing all results by 20 and assigning the concentration unit of "mg/l" to each result. 

The TCLP Limits are given relative to the extract and to the sample for your information. 

Approved by: 

Michael A. Dalrymple, P.E. 

President 

OOJ^y^t^ 
P.11 

TCLP EXTRACT ANALYSIS - METALS 

Sample Collected By: Client 

Date Collected: 1/3/91 @ 12:00 pm 

Received In Lab: 1/14/91 @ 1:45 pm 

Date Analyzed: 1/22/91 

Date .Reported: 1/23/91 

Lab No. 

Client: 

Sample Description: 

9171 

Ks. Dept Health & Environ. 

Bureau of Air/Waste Mgmt. 

Forbes Held 

Topeka, Ks. 66620-7202 

Sample #3 

Wallace Waste 

Wallace Energy Inc. 

Plainville (Rooks Co.) 

Oil Sample 

ANALYTES 

Arsenic 

Barium 

Cadmium 

Chromium 

Lead 

Mercury 

Selenium 

Silver 

TCLP EXTRACT 

RESULTS 

mg/l 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

Not Detected 

DETECTION 

LIMIT 

mg/l 

0.005 

0.20 

0.07 

0.05 

0.07 

0.02 

0.05 

0.05 

EPA 

TCLP LIMIT 

mg/l 

5.0 

100 

1.0 

5.0 

5.0 

0.2 

1.0 

5.0 

EPA SW-846 

METHOD 

1311 /7060 

1311 /7080 

1311 / 7130 

1311 /7190 

1311 /7420 

1311 /7470 

1311 /7740 

1311 /7760 

COMMENT: 

1. Test Procedures as per EPA TCLP regulations in 40 CFR 261, Appendix II, as amended. 

2. This sample does not exhibit EPA TCLP Metal Toxicity. 

3. mg/1 (milligram per liter) = part per million 

Analysis BvV:/^/A : //*. f'/>* ^^j 1 / 

Hal Kennedy, Jr.

 / Y 

Approved By: 

Michael A. Dalrymple.P.E. 

President 

M.D. Chemical and Testing Co., Inc., P.O. Box 67094, Topeka, Kansas 66667 
P.12 

KANSAS APARTMENT OF HEALTH AND ENT "RONMENT 

Kansas Health & Environmental La-^ratory 

Organic Chemistry Laboratory 

Topeka, Kansas 66620 

ANALYTICAL REPORT 

Report To: 

Address: 

TOM GROSS-BAWM 

FORBES BLDG. 740, TOPEKA, KS. 66620 

Lab Number: 

Report Date: 

101706OC 

1-10-91 

SAMPLE COLLECTION INFORMATION 

Site ID No.: Program Code: HD 

Collection Site: WALLACE OIL BS, WALLACE OIL INC 

Collected By: BAWM-SCHMIDT, KAREN Date: 

Sample Type: OIL 

PLAINVILLE 

1- 2-91 Time; 1530 

RESULTS OF ANALYSIS 

COMPOUND 

HEXACHLOROETHANE 

NITROBENZENE 

HEXACHLOROBUTADIENE 

2,4-DINITROTOLUENE 

HEXACHLOROBENZENE 

2,4,6-TRICHLOROPHENOL 

PENTACHLOROPHENOL 

ORTHO-CRESOL 

PARA-CRESOL 

2,4,5-TRICHLOROPHENOL 

Concentration 

(MG/KG) 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

Reporting Limit 

(MG/KG) 

1.5 

0.8 

0.8 

1.5 

0.8 

1.5 

3.8 

0.8 

1.5 

1.5 

Analyst: DENNIS L. DOBSON 

rX 

Copy To: KAREN SCHMIDT-NWD-HAYS 

Roger H. Carlson, Ph.D., Director 

"•i £Z."*~^*—~ •' •' 

jj" ' BUREAU O. 

1 JAN 1 5 199I 

i. I 

'i 
P.13 

Report To: 

Address: 

KANSAS iPARTMENT OF HEALTH AND EN- RONMENT 

Kansas Health & Environmental Laboratory 

Organic Chemistry Laboratory 

Topeka, Kansas 66620 

ANALYTICAL REPORT 

TOM GROSS-BAWM 

FORBES BLDG. 7 40, TOPEKA, KS 66620 

SAMPLE COLLECTION INFORMATION 

Lab Number: 

Report Date: 

101705OC 

1-10-91 

Site ID No.: Program Code: HD Sample Type: OIL 

Collection Site: WALLACE WASTE, WALLACE ENERGY INC., PLAINVILLE 

Collected By: BAWM-SCHMIDT, KAREN Date: 1- 2-91 Time 

RESULTS OF ANALYSIS 

1530 

COMPOUND 

HEXACHLOROETHANE. 

NITROBENZENE 

HEXACHLOROBUTADIENE 

2,4-DINITROTOLUENE 

HEXACHLOROBENZENE 

2,4,6-TRICHLOROPHENOL 

PENTACHLOROPHENOL 

ORTHO-CRESOL 

PARA-CRESOL 

2,4,5-TRICHLOROPHENOL 

Analyst: DENNIS L. DOBSON~ r 

Copy To: KAREN SCHMIDT-NwD-HAYS 

Concentration 

(MG/KG) 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

NOT DETECTED 

Reporting Limit 

(MG/KG) 

1.7 

0.8 

0.8 

1.7 

0.8 

1 .7 

4 .2 

0.8 

1.7 • 

1.7 

Roger H. Carlson, Ph.D., Director 

~ G„.*, . . •- .7...-J \ 

JAN 1 5 1991 

iviAJ-JACE.-.'eNT 
P.M 

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