InstructionsforfillingFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheetForexample:"ASTMInstructionsforfillingFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).IftheunitsofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.ProvidetheSampleNumberandSampleDateontheFuelsSampleResultsworksheet.Youmustprovideaminimumof3compositesamplesconsistingof3combinedgrabsampleseach,butyouarenotlimitedtothatnumberifyouhavecollectedmore.7.Providetheresultsoftheanalysesforeachconstituentrequested.Usethedrop‐downboxestofillintheunitsofmeasure.EIA Facility CodeFacility Name Boiler ID Test Date Fuel Type 11073 Prairie Creek 4 4/7/2010 subbituminousFuel Type 2 Fuel Type 3 Other Fuel Descriptionsubbituminous subbituminousEIA Facility Code Facility Name Boiler ID Basis AnalyteAnalysis Method for each Analyte(example: ASTM D5865-04)1073 Prairie Creek 4 As Received Higher Heating Value ASTM D58651073 Prairie Creek 4 As Received % Moisture ASTM D33021073 Prairie Creek 4 As Received % Ash ASTM D31741073 Prairie Creek 4 As Received % Sulfur ASTM D42391073 Prairie Creek 4 Dry basis Higher Heating Value ASTM D58651073 Prairie Creek 4 Dry basis % Moisture1073 Prairie Creek 4 Dry basis % Ash ASTM D31741073 Prairie Creek 4 Dry basis % Sulfur ASTM D42391073 Prairie Creek 4 Dry basis Antimony1073 Prairie Creek 4 Dry basis Arsenic1073 Prairie Creek 4 Dry basis Beryllium1073 Prairie Creek 4 Dry basis Cadmium1073 Prairie Creek 4 Dry basis Chlorine ASTM D67211073 Prairie Creek 4 Dry basis Chromium1073 Prairie Creek 4 Dry basis Cobalt1073 Prairie Creek 4 Dry basis Fluorine1073 Prairie Creek 4 Dry basis Lead1073 Prairie Creek 4 Dry basis Manganese1073 Prairie Creek 4 Dry basis Mercury1073 Prairie Creek 4 Dry basis Nickel1073 Prairie Creek 4 Dry basis Selenium

# EIA Facility Code Facility Name Boiler ID 

# E m i ss i ons t es t me th o d( s )

conducted at time of fuel

sample collection (e.g., M30B,

M26A, M0031 with SW-846

M6260B)

1073 Prairie Creek 4 Method 23

Sample Number

(minimum of 3

composite

samples) Sample Date

(MM/DD/YYYY) Higher

Heating

Value (HHV)

(as

received) HHV Units % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received)



# Sample 006 4/7/2010 8273.00 Btu/lb 30.26 5.44 0.27 Fuel Testing Results

# Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units A rsenic (Dry

Basis)



# 11863 Btu/lb 7.8 0.39 <10 ppm

# Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis)

# Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

# EIA Facility Code Facility Name Boiler ID 

# E m i ss i ons test met h o d( s ) con d ucte d at

time of fuel sample collection (e.g.,

M30B, M26A, M0031 with SW-846

M6260B)

1073 Prairie Creek 4 Method 23

Sample Number

(minimum of 3

composite

samples) Sample Date

(MM/DD/YYYY) Higher

Heating

Value

(HHV)

(as

received) HHV Units % Moisture

(as

received) % Ash

(as

received)



# Sample 009 4/8/2010 8346.00 Btu/lb 29.71 5.38 Fuel Testing Results

# % Sulfur

(as

received) Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units



# 0.26 11874 Btu/lb 7.65 0.37 <10 ppm

# Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units

# Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

# EIA Facility Code Facility Name Boiler ID 

# Emissions test method(s)

conducted at time of fuel

sample collection (e.g.,

M30B, M26A, M0031 with

SW-846 M6260B)

1073 Prairie Creek 4 Method 23

Sample Number

(minimum of 3

composite

samples) Sample Date

(MM/DD/YYYY) Higher

Heating

Value

(HHV)

(as

received) HHV Units % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received)



# Sample 012 4/9/2010 8340.00 Btu/lb 30.03 5.11 0.27 Fuel Testing Results

# Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units A rsenic (Dry

Basis)



# 11920 Btu/lb 7.31 0.38 <10 ppm

# Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis)

# Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

# EIA Facility Code Facility Name Boiler ID 

# E m i ss i ons t es t me th o d( s )

conducted at time of fuel

sample collection (e.g.,

M30B, M26A, M0031 with

SW-846 M6260B)

1073 Prairie Creek 4

Sample Number

(minimum of 3

composite

samples) Sample Date

(MM/DD/YYYY) Higher

Heating

Value

(HHV)

(as

received) HHV Units % Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) 

# Fuel Testing Results

# Higher

Heating

Value (HHV)

(Dry Basis) HHV Units % Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units A rsenic (Dry

Basis)

# Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis)

# Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to theorangehightlighted cell, if necessary.Fuel Units of Measure - HHV Units of Measure - Cl, Flanthracite Btu/lb %bituminous Btu/gallon ppmsubbituminouslignitecoal refuse (culm or gob)No.2 Fuel Oil (distillate)No.6 Fuel Oil (residual or bunker C)Units of Measure - Metalssynfuel mg/gpetroleum cokeμg/gothermg/Kg