### Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL for Existing Sources

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Test**  **Method Sample** 

**Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  **3x RDL**

**( μg/dscm)**  **F d** **Factor**

**(dscf/MMBtu) 3x RDL** 

**( lb/MMBtu)**  ALBoiseWhitePaperJackson 102-0001-Z013 Solid 1 8/5/2009 26A 120 2.00 9.00E+01 9,780 ALBoiseWhitePaperJackson 102-0001-Z013 Solid 2 8/5/2009 26A 120 2.00 9.00E+01 9,780 ALBoiseWhitePaperJackson 102-0001-Z013 Solid 3 8/5/2009 26A 120 2.00 9.00E+01 9,780 ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #1 7/7/2009 26A 120 2.00 9.00E+01 9,780 ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #2 7/7/2009 26A 120 2.00 9.00E+01 9,780 ALIPCourtland No. 3 Combination Boier / 11Cu301 Solid Sample #3 7/8/2009 26A 120 2.00 9.00E+01 9,780 ARAnthonyForestProducts SN-12 Solid Sample #19/1/2009 26 120 2.00 1.25E+02 9,780 ARAnthonyForestProducts SN-12 Solid Sample #2 9/1/2009 26 120 2.00 1.25E+02 9,780 ARAnthonyForestProducts SN-12 Solid Sample #3 9/2/2009 26 120 2.00 1.25E+02 9,780 ARPotlatchForestWarren Wellons Boiler Solid Sample #18/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 ARPotlatchForestWarren Wellons Boiler Solid Sample #2 8/8/2006 26A 60 1.00 15.5 1.80E+02 9,780 4.23E-04 ARPotlatchForestWarren Wellons Boiler Solid Sample #3 9/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 ARPotlatchForestWarren Wellons Boiler Solid 1 9/8/2009 26A 60 1.00 4.22 1.80E+02 9,780 1.38E-04 ARPotlatchForestWarren Wellons Boiler Solid 2 9/8/2009 26A 60 1.00 4.9 1.80E+02 9,780 1.43E-04 ARPotlatchForestWarren Wellons Boiler Solid 3 9/8/2009 26A 60 1.00 4.39 1.80E+02 9,780 1.39E-04 AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #13/24/2006 26A 60 1.00 1.80E+02 9,780 AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #23/24/2006 26A 60 1.00 1.80E+02 9,780 AZCatalystPaperSnowflake Power Boiler #2 Coal Solid Sample #33/24/2006 26A 60 1.00 1.80E+02 9,780 FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #112/16/2002 9,780 FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #212/16/2002 9,780 FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #312/16/2002 9,780 FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #11/19/2005 9,780 FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #21/19/2005 9,780 FLSugarCaneGrowersCoop Boiler No. 8 Solid Sample #31/19/2005 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #112/10/2002 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #212/10/2002 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #312/10/2002 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #112/1/2006 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #112/1/2006 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #212/1/2006 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #212/1/2006 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #312/1/2006 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 4 Solid Sample #312/1/2006 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #112/31/2002 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #212/31/2002 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #312/31/2002 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #1 1/2/2003 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #2 1/2/2003 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #3 1/2/2003 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #11/25/2007 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #21/25/2007 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #31/25/2007 26A 50 0.83 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #15/15/2007 26A 60 1.00 1.80E+02 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #25/15/2007 9,780 FLUSSugarCorp Boiler No. 7 Solid Sample #35/16/2007 9,780 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #18/13/2009 26 240 4.00 6.25E+01 9,780 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #28/13/2009 26 240 4.00 6.25E+01 9,780 GAGPMadisonPly 800 Wood Waste Boiler Solid Sample #38/14/2009 26 240 4.00 6.25E+01 9,780 GARayonierJesupMill PB01 Solid Sample #15/11/2004 9,780 GARayonierJesupMill PB01 Solid Sample #25/11/2004 9,780 GARayonierJesupMill PB01 Solid Sample #35/12/2004 9,780 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #18/24/2009 FTIR 240 4.00 9,780 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #28/24/2009 FTIR 240 4.00 9,780 IAArchersDanielsMidlandDesMoines Asea Boiler #1 Solid Sample #38/25/2009 FTIR 240 4.00 9,780 IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 1 6/2/2009 26A 120 2.00 9.00E+01 9,780 IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 2 6/2/2009 26A 120 2.00 9.00E+01 9,780 IARoquetteAmerica Circulating Fluidized Bed Boiler (121) Solid 3 6/3/2009 26A 120 2.00 9.00E+01 9,780 IDMoyieSprings Lumber420 HFB1 Solid Sample #19/12/2003 9,780 IDMoyieSprings Lumber420 HFB1 Solid Sample #29/12/2003 9,780 IDMoyieSprings Lumber420 HFB1 Solid Sample #39/12/2003 9,780 IDPotlatch PB-1 CE Solid Sample #17/28/2009 26 60 1.00 13.2 2.50E+02 9,780 4.13E-04 IDPotlatch PB-1 CE Solid Sample #27/28/2009 26 60 1.00 13.8 2.50E+02 9,780 4.47E-04 IDPotlatch PB-1 CE Solid Sample #37/28/2009 26 60 1.00 13 2.50E+02 9,780 4.02E-04 IDTASCOPaul Babcock and Wilcox (B&W) Boiler Solid Sample #1 6/1/2006 26A 64 1.07 1.80E+02 9,780 IDTASCOPaul Erie City Boiler Solid Sample #16/20/2006 26A 64 1.07 1.80E+02 9,780 IDTASCOPaul Erie City Boiler Solid Sample #26/20/2006 26A 64 1.07 1.80E+02 9,780 IDTASCOPaul Erie City Boiler Solid Sample #36/21/2006 26A 64 1.07 1.80E+02 9,780 INAlcoaWarrick Unit #3 Solid M26A-1 8/17/2009 9,780 INAlcoaWarrick Unit #3 Solid M26A-2 8/17/2009 9,780 INAlcoaWarrick Unit #3 Solid M26A-3 8/17/2009 9,780 LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #18/14/2007 26A 60 1.00 1.80E+02 9,780 LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #28/14/2007 26A 60 1.00 1.80E+02 9,780 LAGPPortHudson EQT0109 - No. 6 CFB Boiler Solid Sample #38/14/2007 26A 60 1.00 1.80E+02 9,780 MEBoralexStratton Boiler #1 Solid Sample #110/21/2009 26A 60 1.00 6.3 1.80E+02 9,780 1.57E-04 MEBoralexStratton Boiler #1 Solid Sample #210/21/2009 26A 60 1.00 5.9 1.80E+02 9,780 1.53E-04 MEBoralexStratton Boiler #1 Solid Sample #310/21/2009 26A 60 1.00 5.9 1.80E+02 9,780 1.53E-04 MICityofEscanaba EUBOILER#1 Solid Sample #110/27/2004 26A 60 1.00 1.80E+02 9,780 MICityofEscanaba EUBOILER#1 Solid Sample #210/27/2004 26A 60 1.00 1.80E+02 9,780 MICityofEscanaba EUBOILER#1 Solid Sample #310/27/2004 26A 60 1.00 1.80E+02 9,780 MSBowaterSouth Bark Boiler Solid Sample #11/23/2007 9,780 MSBowaterSouth Bark Boiler Solid Sample #21/23/2007 9,780 MSBowaterSouth Bark Boiler Solid Sample #31/23/2007 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #17/12/2006 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #27/12/2006 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #37/12/2006 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #19/22/2010 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #29/23/2010 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #39/23/2010 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #19/28/2010 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #29/29/2010 9,780 MSGPNewAugusta AA-015 Power Boiler Solid Sample #39/30/2010 9,780 MSHankinsLumber Boiler #1 (AA-001) Solid Sample #21/10/2005 9,780 MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #110/14/2003 26A 60 1.00 1.80E+02 9,780 MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #210/14/2003 26A 60 1.00 1.80E+02 9,780

Page 1 of 3

### Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL for Existing Sources

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Test**  **Method Sample** 

**Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  **3x RDL**

**( μg/dscm)**  **F d** **Factor**

**(dscf/MMBtu) 3x RDL** 

**( lb/MMBtu)**  MSHoodWaynesboro AA-001 (Wood-Fired Boiler) Solid Sample #310/14/2003 26A 60 1.00 1.80E+02 9,780 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #18/6/2009 26A 120 2.00 8.06 9.00E+01 9,780 8.93E-05 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #2 8/6/2009 26A 120 2.00 7.25 9.00E+01 9,780 8.40E-05 MSWeyerhaeuserBruce AA-002 No. 2 Boiler Solid Sample #3 8/6/2009 26A 120 2.00 7.63 9.00E+01 9,780 8.64E-05 NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #17/14/2004 26A 60 1.00 1.80E+02 9,780 NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #27/14/2004 26A 120 2.00 9.00E+01 9,780 NCGPRoxboro ES-1 Wood fired Boiler Solid Sample #37/14/2004 26A 120 2.00 9.00E+01 9,780 NCLPRoaringRiver Boiler #2 Solid Sample #110/13/2004 9,780 NCLPRoaringRiver Boiler #2 Solid Sample #210/14/2004 9,780 NCLPRoaringRiver Boiler #2 Solid Sample #310/14/2004 9,780 NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 1 8/25/2009 26A 120 2.00 9.00E+01 9,780 NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 2 8/25/2009 26A 120 2.00 9.00E+01 9,780 NDCargillWestFargo Foster Wheeler Boiler (EU43) Solid 3 8/25/2009 26A 120 2.00 9.00E+01 9,780 NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #110/26/2006 26A 60 1.00 1.80E+02 9,780 NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #210/26/2006 26A 60 1.00 1.80E+02 9,780 NDMinnDakFarmers Babcock and Wilcox Boiler #5 Solid Sample #310/26/2006 26A 60 1.00 1.80E+02 9,780 ORRoseburgCoquille Boiler 1 Solid Sample #110/14/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgCoquille Boiler 1 Solid Sample #110/14/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgCoquille Boiler 1 Solid Sample #110/14/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgCoquille Boiler 1 Solid Sample #210/14/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgCoquille Boiler 1 Solid Sample #210/14/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgCoquille Boiler 1 Solid Sample #210/14/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgRiddle2 Boiler #2 Solid Sample #110/11/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgRiddle2 Boiler #2 Solid Sample #210/11/2004 26A 60 1.00 1.80E+02 9,780 ORRoseburgRiddle2 Boiler #2 Solid Sample #310/11/2004 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #81 Coal Boiler Solid Sample #37/17/2007 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #81 Coal Boiler Solid Sample #17/18/2007 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #81 Coal Boiler Solid Sample #27/18/2007 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #81 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #82 Coal Boiler Solid Sample #37/17/2007 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #82 Coal Boiler Solid Sample #17/18/2007 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #82 Coal Boiler Solid Sample #27/18/2007 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780 PADomtarJohnsonburg #82 Coal Boiler Solid 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #111/25/2003 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #211/25/2003 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #311/25/2003 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #111/3/2005 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #211/3/2005 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #311/3/2005 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #111/7/2007 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #211/7/2007 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #311/7/2007 26A 60 1.00 1.80E+02 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #18/18/2009 26A 240 4.00 4.50E+01 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #28/18/2009 26A 240 4.00 4.50E+01 9,780 SCCogenSouth B001 - Main Boiler Solid Sample #38/19/2009 26A 240 4.00 4.50E+01 9,780 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #17/14/2009 26A 180 3.00 9.74 6.00E+01 9,780 6.85E-05 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #27/14/2009 26A 180 3.00 9.38 6.00E+01 9,780 6.63E-05 SCMarlboroPaper Hogged Fuel Boiler Solid Sample #37/14/2009 26A 180 3.00 9.11 6.00E+01 9,780 6.48E-05 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #110/6/2005 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #210/6/2005 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #310/6/2005 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #110/7/2005 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #210/7/2005 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #310/7/2005 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #18/4/2009 26A 120 2.00 9.00E+01 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #2 8/4/2009 26A 120 2.00 9.00E+01 9,780 TNBowaterNewsprint Bubbling Fluidized Bed Boiler Solid Sample #3 8/5/2009 26A 120 2.00 9.00E+01 9,780 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #18/26/2009 26A 120 2.00 9.00E+01 9,780 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #28/27/2009 26A 120 2.00 9.00E+01 9,780 TNEastman_NO_CBIDATA Boiler 30 Solid Sample #38/27/2009 26A 120 2.00 9.00E+01 9,780 TXDibollTemple-Inland PB-44 Solid Sample #16/29/2007 26A 60 1.00 1.80E+02 9,780 TXDibollTemple-Inland PB-44 Solid Sample #26/29/2007 26A 60 1.00 1.80E+02 9,780 TXDibollTemple-Inland PB-44 Solid Sample #36/29/2007 26A 60 1.00 1.80E+02 9,780 VASmurfitStoneWestpt PB08 Solid Sample #111/8/2004 9,780 VASmurfitStoneWestpt PB08 Solid Sample #211/8/2004 26A 60 1.00 1.80E+02 9,780 VASmurfitStoneWestpt PB08 Solid Sample #311/8/2004 26A 60 1.00 1.80E+02 9,780 VASmurfitStoneWestpt PB08 Solid Sample #19/26/2009 26A 120 2.00 9.00E+01 9,780 VASmurfitStoneWestpt PB08 Solid Sample #29/26/2009 26A 120 2.00 9.00E+01 9,780 VASmurfitStoneWestpt PB08 Solid Sample #39/26/2009 26A 120 2.00 9.00E+01 9,780 VAUniversityofVirginia 7103-1-01R Solid M26A-1 9/15/2009 26A 120 2.00 9.00E+01 9,780 VAUniversityofVirginia 7103-1-01R Solid M26A-2 9/16/2009 26A 120 2.00 9.00E+01 9,780 VAUniversityofVirginia 7103-1-01R Solid M26A-3 9/17/2009 26A 120 2.00 9.00E+01 9,780 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #16/22/2006 26 60 1.00 2.50E+02 9,780 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #26/22/2006 26 60 1.00 2.50E+02 9,780 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #36/22/2006 26 60 1.00 2.50E+02 9,780 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #18/14/2009 26 60 1.00 2.50E+02 9,780 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #28/14/2009 26 60 1.00 2.50E+02 9,780 WAGraysHarborPaper No. 6 Boiler (EU2) Solid Sample #38/14/2009 26 60 1.00 2.50E+02 9,780 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #18/11/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #28/11/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05 WAWeyerhaeuser_Raymond Hog Fuel Boiler EU1 Solid Sample #38/12/2009 26 240 4.00 7 6.25E+01 9,780 5.73E-05 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #110/27/1992 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #210/27/1992 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #310/27/1992 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #18/10/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #28/10/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #38/11/2004 26A 60 1.00 6 1.80E+02 9,780 1.54E-04 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #17/19/2005 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #27/19/2005 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #37/19/2005 26A 60 1.00 1.80E+02 9,780

Page 2 of 3

### Appendix D-1: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL for Existing Sources

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Test**  **Method Sample** 

**Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  **3x RDL**

**( μg/dscm)**  **F d** **Factor**

**(dscf/MMBtu) 3x RDL** 

**( lb/MMBtu)**  WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #18/21/2006 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #28/21/2006 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid Sample #38/21/2006 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780 WIGPGreenBay2818 B29 - Fluidized Bed Boiler #9 Solid 26A 60 1.00 1.80E+02 9,780 WINewPageBiron B24 Solid Sample #19/12/2007 26A 60 1.00 1.80E+02 9,780 WINewPageBiron B24 Solid Sample #29/12/2007 26A 60 1.00 1.80E+02 9,780 WINewPageBiron B24 Solid Sample #39/12/2007 26A 60 1.00 1.80E+02 9,780 WINewPageBiron B24 Solid 1 8/25/2009 26A 120 2.00 9.00E+01 9,780 WINewPageBiron B24 Solid 2 9/22/2009 26A 120 2.00 9.00E+01 9,780 WINewPageBiron B24 Solid 3 9/22/2009 26A 120 2.00 9.00E+01 9,780 WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #112/14/2005 26A 60 1.00 1.80E+02 9,780 WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #212/15/2005 26A 60 1.00 1.80E+02 9,780 WINewPage-WisconsinRapids Power Boiler 1 - B21 Solid Sample #312/15/2005 26A 60 1.00 1.80E+02 9,780 CTElectric Boat EMU 17 Liquid 1 8/17/2009 9,190 CTElectric Boat EMU 17 Liquid 2 8/17/2009 9,190 CTElectric Boat EMU 17 Liquid 3 8/17/2009 9,190 PABoeingRidleyPark 033 Liquid Sample #19/22/2009 9,190 PABoeingRidleyPark 033 Liquid Sample #29/23/2009 9,190 PABoeingRidleyPark 033 Liquid Sample #39/24/2009 9,190 SCMilliken-Dewey D30 Liquid Sample #18/13/2009 26A 120 2.00 3.83 9.00E+01 9,190 6.32E-05 SCMilliken-Dewey D30 Liquid Sample #28/13/2009 26A 120 2.00 4.02 9.00E+01 9,190 6.39E-05 SCMilliken-Dewey D30 Liquid Sample #38/13/2009 26A 120 2.00 3.96 9.00E+01 9,190 6.37E-05 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #18/31/2006 26A 60 1.00 10 1.80E+02 9,190 1.98E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #28/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #38/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #17/29/2009 26A 60 1.00 7.4 1.80E+02 9,190 1.60E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #27/30/2009 26A 60 1.00 6.4 1.80E+02 9,190 1.49E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #37/30/2009 26A 60 1.00 6.8 1.80E+02 9,190 1.53E-04 WVMountainStateCarbonFollansbee S1 Process Gas Sample #110/22/2009 26A 120 2.00 4.5 9.00E+01 8,710 6.23E-05 WVMountainStateCarbonFollansbee S1 Process Gas Sample #210/22/2009 26A 120 2.00 4.7 9.00E+01 8,710 6.31E-05 WVMountainStateCarbonFollansbee S1 Process Gas Sample #310/23/2009 26A 120 2.00 4.8 9.00E+01 8,710 6.35E-05

Page 3 of 3

### Appendix D-2: Sample Times and Oxygen Percentages Used to Estimate HCl 3x RDL for New Sources

**Facility ID Combusor ID**  **Fuel Category Test ID**  **Test Date Test**  **Method Sample** 

**Time (min)**  **Sample Time (hrs)** **Stack Oxygen**

**Concentration (%)**  **3x RDL**

**( μg/dscm)**  **F d** **Factor**

**(dscf/MMBtu) 3x RDL** 

**( lb/MMBtu)**  ARPotlatchForestWarren Wellons Boiler Solid Sample #18/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 ARPotlatchForestWarren Wellons Boiler Solid Sample #2 8/8/2006 26A 60 1.00 15.5 1.80E+02 9,780 4.23E-04 ARPotlatchForestWarren Wellons Boiler Solid Sample #3 9/8/2006 26A 60 1.00 16 1.80E+02 9,780 4.65E-04 ARPotlatchForestWarren Wellons Boiler Solid 1 9/8/2009 26A 60 1.00 4.22 1.80E+02 9,780 1.38E-04 ARPotlatchForestWarren Wellons Boiler Solid 2 9/8/2009 26A 60 1.00 4.9 1.80E+02 9,780 1.43E-04 ARPotlatchForestWarren Wellons Boiler Solid 3 9/8/2009 26A 60 1.00 4.39 1.80E+02 9,780 1.39E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #18/31/2006 26A 60 1.00 10 1.80E+02 9,190 1.98E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #28/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #38/31/2006 26A 60 1.00 9.9 1.80E+02 9,190 1.96E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #17/29/2009 26A 60 1.00 7.4 1.80E+02 9,190 1.60E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #27/30/2009 26A 60 1.00 6.4 1.80E+02 9,190 1.49E-04 TNInvistaChattanooga EU003 - Vaporizer #2 Liquid Sample #37/30/2009 26A 60 1.00 6.8 1.80E+02 9,190 1.53E-04 WVMountainStateCarbonFollansbee S1 Process Gas Sample #110/22/2009 26A 120 2.00 4.5 9.00E+01 8,710 6.23E-05 WVMountainStateCarbonFollansbee S1 Process Gas Sample #210/22/2009 26A 120 2.00 4.7 9.00E+01 8,710 6.31E-05 WVMountainStateCarbonFollansbee S1 Process Gas Sample #310/23/2009 26A 120 2.00 4.8 9.00E+01 8,710 6.35E-05

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# Appendix D-3a: Summary of HCl 3x RDL for Existing Sources

**Fuel Category Average Sample Volume (dscm)**  **or Sample Time (hrs) 3x RDL**  **( μg/dscm)**  **F d** 

# Factor for Subcategory

**(dscf/MMBtu) Average Stack Oxygen** 

**Concentration (%) 3x RDL**  **( lb/MMBtu)**  Solid 2 1.52E+02 9,780 8.72 **1.91E-04** Liquid 1 1.50E+02 9,190 6.91 **1.38E-04** Process Gas 2 9.00E+01 8,710 4.67 **6.30E-05**



# Appendix D-3b: Summary of HCl 3x RDL for New Sources

**Fuel Category Average Sample Volume (dscm)**  **or Sample Time (hrs) 3x RDL**  **( μg/dscm)**  **F d** 

# Factor for Subcategory

**(dscf/MMBtu) Average Stack Oxygen** 

**Concentration (%) 3x RDL**  **( lb/MMBtu)**  Solid 1 1.80E+02 9,780 10.17 **2.96E-04** Liquid 1 1.80E+02 9,190 8.40 **1.75E-04** Process Gas 2 9.00E+01 8,710 4.67 **6.30E-05**

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