## Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of
measure.

## Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units of

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

3845 TransAlta Centralia Generation LLC BW 22 

## subbituminous

### Fuel Type 2 Fuel Type 3 Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte



## 3845 TransAlta Centralia Generation LLC BW22 As Received Higher Heating Value 

## 3845 TransAlta Centralia Generation LLC BW22 As Received % Moisture 

## 3845 TransAlta Centralia Generation LLC BW22 As Received % Ash 

## 3845 TransAlta Centralia Generation LLC BW22 As Received % Sulfur 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Higher Heating Value 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis % Ash 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis % Sulfur 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Antim ony 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Arsenic 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Bery llium 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Cadmium 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Chlorine 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Chromium 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Cobalt 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Fluorine 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Lead 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Manganese 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Mercury 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Nickel 

## 3845 TransAlta Centralia Generation LLC BW22 Dry

basis Selenium

### An alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

## ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6357 ASTM D 6721 ASTM D 6357 ASTM D 6357 ASTM D 3761 ASTM D 6357 ASTM D 6357 ASTM D 6722 ASTM D 6357 SW7740EIA Facility Code Facility Name Boiler ID 

### HA Ps Test Group 

## 3845 TransAlta Centralia Generation LLC BW22 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYY Y) Test Stop

Date (MM/DD/YYY Y) Higher

Heatin g Value (HHV) (as receiv HHV

Units % Moistur
e (as received ) % A

sh (as received ) 

## 1-0600-032310-U2-TEMA (1-fuel-2) 3/22/2010 3/23/2010 8062 Btu/lb 28.14 9.67 2-2045-032310-U2-TEMA (2-fuel-2) 3/23/2010 3/23/2010 7990 Btu/lb 31.51 6.4 3-0530-032410-U2-TEMA (3-fuel-1) * see note on analysis sheet 3/23/2010 3/24/2010 8130 Btu/lb 30.37 7 Fuel Testing Results

## Mercury and non-mercury metalic HAPs

% Sulfur (as receive d) Higher Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur (Dry Basis) Chlo rine (Dry Basi s) Chlori
ne Units Mercu ry (Dry Basis) Mercu

ry Units An ti
mo ny (Dr y Bas is) An tim ony Units Ars eni
c (Dr y Ba sis Arseni
c Units Bery llium (Dry Basi s) Bery ll ium Units Cad miu
m (Dry Basi s) Cadm ium Units Chr omi
um (Dry Bas is) Chrom ium Units 

## 0.34 11219 Btu/lb 13.45 0.47 63 ppm 0.06 μg/g 2 μg/g 2 μg/g 0.4 μg/g 0.4 μg/g 12 μg/g 0.34 11667 Btu/lb 9.34 0.49 35 ppm 0.07 μg/g 2 μg/g 2 μg/g 0.3 μg/g 0.4 μg/g 7 μg/g 0.39 11676 Btu/lb 10.05 0.57 53 ppm 0.08 μg/g 2 μg/g 3 μg/g 0.3 μg/g 0.4 μg/g 8 μg/g

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Le ad (Dr y Ba sis ) Lead Units Man gane se (Dry Basi s) Mang
anese Units Nick el (Dry Basi s) Nickel Units Sel eni
um (Dry Bas is) Seleni
um Units Fluor ine (Dry Basi s) Fluori
ne Units Co balt (Dr y Bas is) Cobal t Units Total Moisture

Volatiles As h

Fixed Carbon

Carbon Hydrogen Nitrogen 

## 4 μg/g 82 μg/g 10 μg/g 1 μg/g 77 ppm 2 μg/g 28.14 40.6 13.45 46 64.3 4.62 0.92 4 μg/g 35 μg/g 7 μg/g 1 μg/g 68 ppm 1 μg/g 31.51 43.2 9.34 47.5 67.3 4.75 0.98 4 μg/g 41 μg/g 8 μg/g 1 μg/g 58 ppm 2 μg/g 30.37 42.9 10.05 47.1 66.9 4.76 0.95 Proximate A naly

ses, % by

wt Ultimate Analy ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Sulfur

Oxygen 

## 0.47 16.24 0.49 17.17 0.57 16.74 Ultimate A naly

ses, % by

wtEIA Facility Code Facility Name Boiler ID 

## 3845 TransAlta Centralia Generation LLC BW22

Sample Number (minimum of 3 composite

samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) 

## 2-2045-032310-U2-TEMA (2-fuel-2) 3/23/2010 3/23/2010 7990 3-0530-032410-U2-TEMA (3-fuel-1) * see note on analysis sheet 3/23/2010 3/24/2010 8130 Fuel Testing Results

### HA Ps Test Group



## Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

## Btu/lb 31.51 6.4 0.34 11667 Btu/lb 30.37 7 0.39 11676HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

## Btu/lb 9.34 0.49 35 ppm 0.07 μg/g Btu/lb 10.05 0.57 53 ppm 0.08 μg/gAn timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis) Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

## 2 μg/g 2 μg/g 0.3 μg/g 0.4 μg/g 7 2 μg/g 3 μg/g 0.3 μg/g 0.4 μg/g 8Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

## μg/g 4 μg/g 35 μg/g 7 μg/g 1 μg/g μg/g 4 μg/g 41 μg/g 8 μg/g 1 μg/g

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

## 68 ppm 1 μg/g 31.51 43.2 9.34 47.46 58 ppm 2 μg/g 30.37 42.9 10.05 47.08 Proximate A naly

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

## 67.27 4.75 0.98 0.49 17.17 66.93 4.76 0.95 0.57 16.74

Ultimate Analy

ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3845 TransAlta Centralia Generation LLC BW22

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate A naly

ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate A naly

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 

## 3845 TransAlta Centralia Generation LLC BW22

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Bery llium

(Dry Basis)Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate A naly ses, % by

wt

### Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate A naly

ses, % by

wt Ultimate Analy ses, % by

wt

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orange hightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm