Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

3845 TransAlta Centralia Generation LLC BW22 subbituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

3845 TransAlta Centralia Generation LLC BW22 As Received Higher Heating Value

3845 TransAlta Centralia Generation LLC BW22 As Received % Moisture

3845 TransAlta Centralia Generation LLC BW22 As Received % Ash

3845 TransAlta Centralia Generation LLC BW22 As Received % Sulfur

3845 TransAlta Centralia Generation LLC BW22 Dry basis Higher Heating Value

3845 TransAlta Centralia Generation LLC BW22 Dry basis % Ash

3845 TransAlta Centralia Generation LLC BW22 Dry basis % Sulfur

3845 TransAlta Centralia Generation LLC BW22 Dry basis Antimony

3845 TransAlta Centralia Generation LLC BW22 Dry basis Arsenic

3845 TransAlta Centralia Generation LLC BW22 Dry basis Beryllium

3845 TransAlta Centralia Generation LLC BW22 Dry basis Cadmium

3845 TransAlta Centralia Generation LLC BW22 Dry basis Chlorine

3845 TransAlta Centralia Generation LLC BW22 Dry basis Chromium

3845 TransAlta Centralia Generation LLC BW22 Dry basis Cobalt

3845 TransAlta Centralia Generation LLC BW22 Dry basis Fluorine

3845 TransAlta Centralia Generation LLC BW22 Dry basis Lead

3845 TransAlta Centralia Generation LLC BW22 Dry basis Manganese

3845 TransAlta Centralia Generation LLC BW22 Dry basis Mercury

3845 TransAlta Centralia Generation LLC BW22 Dry basis Nickel

3845 TransAlta Centralia Generation LLC BW22 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D 5865

ASTM D 3302

ASTM D 3174/5142

ASTM D 4239

ASTM D 5865

ASTM D 3174/5142

ASTM D 4239

ASTM D 6357

ASTM D 6357

ASTM D 6357

ASTM D 6357

ASTM D 6721

ASTM D 6357

ASTM D 6357

ASTM D 3761

ASTM D 6357

ASTM D 6357

ASTM D 6722

ASTM D 6357

SW7740
EIA Facility Code Facility Name Boiler ID

HAPs 

Test 

Group

3845 TransAlta Centralia Generation LLC BW22 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples)

Test Start 

Date

(MM/DD/YYY

Y)

Test Stop 

Date

(MM/DD/YYY

Y)

Higher 

Heatin

g 

Value 

(HHV)

(as 

receiv

HHV 

Units

% 

Moistur

e

(as 

received

)

% Ash

(as 

received

)

1-0600-032310-U2-TEMA (1-fuel-2) 3/22/2010 3/23/2010 8062 Btu/lb 28.14 9.67

2-2045-032310-U2-TEMA (2-fuel-2) 3/23/2010 3/23/2010 7990 Btu/lb 31.51 6.4

3-0530-032410-U2-TEMA (3-fuel-1) * see note on analysis sheet 3/23/2010 3/24/2010 8130 Btu/lb 30.37 7

 Fuel Testing Results


 non-mercury metalic HAPs

% 

Sulfur

(as 

receive

d)

Higher 

Heating 

Value 

(HHV)

(Dry

Basis) HHV Units

% Ash

(Dry

Basis)

% 

Sulfur

(Dry

Basis)

Chlo

rine

(Dry

Basi

s)

Chlori

ne 

Units

Mercu

ry (Dry

Basis)

Mercu

ry

Units

Anti

mo

ny

(Dr

y 

Bas

is)

Antim

ony

Units

Ars

eni

c 

(Dr

y 

Ba

sis

Arseni

c 

Units

Bery

llium 

(Dry

Basi

s)

Beryll

ium 

Units

Cad

miu

m 

(Dry

Basi

s)

Cadm

ium 

Units

Chr

omi

um 

(Dry

Bas

is)

Chrom

ium 

Units

0.34 11219 Btu/lb 13.45 0.47 63 ppm 0.06 μg/g 2 μg/g 2 μg/g 0.4 μg/g 0.4 μg/g 12 μg/g

0.34 11667 Btu/lb 9.34 0.49 35 ppm 0.07 μg/g 2 μg/g 2 μg/g 0.3 μg/g 0.4 μg/g 7 μg/g

0.39 11676 Btu/lb 10.05 0.57 53 ppm 0.08 μg/g 2 μg/g 3 μg/g 0.3 μg/g 0.4 μg/g 8 μg/g


Note the Proximate/Ultimate data below should be r

Le

ad 

(Dr

y 

Ba

sis

)

Lead 

Units

Man

gane

se 

(Dry

Basi

s)

Mang

anese 

Units

Nick

el 

(Dry

Basi

s)

Nickel 

Units

Sel

eni

um 

(Dry

Bas

is)

Seleni

um 

Units

Fluor

ine 

(Dry

Basi

s)

Fluori

ne 

Units

Co

balt 

(Dr

y 

Bas

is)

Cobal

t 

UnitsTotal Moisture Volatiles AshFixed CarbonCarbonHydrogenNitrogen

4 μg/g 82 μg/g 10 μg/g 1 μg/g 77 ppm 2 μg/g 28.14 40.6 13.45 46 64.3 4.62 0.92

4 μg/g 35 μg/g 7 μg/g 1 μg/g 68 ppm 1 μg/g 31.51 43.2 9.34 47.5 67.3 4.75 0.98

4 μg/g 41 μg/g 8 μg/g 1 μg/g 58 ppm 2 μg/g 30.37 42.9 10.05 47.1 66.9 4.76 0.95

Proximate Analyses, % by wt Ultimate Analyses, % by wt


te data below should be recorded on a dry basis (including ash).

Total SulfurOxygen

0.47 16.24

0.49 17.17

0.57 16.74

mate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID

3845 TransAlta Centralia Generation LLCBW22

Sample Number (minimum of 3 composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received)

2-2045-032310-U2-TEMA (2-fuel-2) 3/23/2010 3/23/2010 7990

3-0530-032410-U2-TEMA (3-fuel-1) * see note on analysis sheet 3/23/2010 3/24/2010 8130

 Fuel Testing Results


HAPs Test Group

Acid gas HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 31.51 6.4 0.34 11667

Btu/lb 30.37 7 0.39 11676


HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Btu/lb 9.34 0.49 35 ppm 0.07 μg/g

Btu/lb 10.05 0.57 53 ppm 0.08 μg/g


Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

2 μg/g 2 μg/g 0.3 μg/g 0.4 μg/g 7

2 μg/g 3 μg/g 0.3 μg/g 0.4 μg/g 8


Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

μg/g 4 μg/g 35 μg/g 7 μg/g 1 μg/g

μg/g 4 μg/g 41 μg/g 8 μg/g 1 μg/g


Note the Proximate/Ultimate data below should be 

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

68 ppm 1 μg/g 31.51 43.2 9.34 47.46

58 ppm 2 μg/g 30.37 42.9 10.05 47.08

Proximate Analyses, % by wt


ltimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

67.27 4.75 0.98 0.49 17.17

66.93 4.76 0.95 0.57 16.74

Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

3845 TransAlta Centralia Generation LLC BW22

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

Proximate Analyses, 


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Proximate Analyses, % by wt Ultimate Analyses, % by wt


EIA Facility Code Facility Name Boiler ID HAPs Test Group

3845 TransAlta Centralia Generation LLCBW22

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)


Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)


Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units


Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units Total Moisture

Proximate Analys


Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Proximate Analyses, % by wt Ultimate Analyses, % by wt


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm