Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.EIA

Facility Code Facility Name Boiler ID Fuel Type 1

4129 Piney

Creek Power Project

BRBR1 bituminousFuel Type 2 Fuel Type 3 Other Fuel Description

synfuelEIA

Facility Code Facility Name Boiler ID Basis An alyte

4129 Piney Creek Power Project BRBR1 As Received Higher Heating Value 4129 Piney Creek Power Project BRBR1 As Received % Moisture 4129 Piney Creek Power Project BRBR1 As Received % Ash 4129 Piney Creek Power Project BRBR1 As Received % Sulfur 4129 Piney Creek Power Project BRBR1 Dry

basis Higher Heating Value 4129 Piney Creek Power Project BRBR1 Dry

basis % Ash 4129 Piney Creek Power Project BRBR1 Dry

basis % Sulfur 4129 Piney Creek Power Project BRBR1 Dry

basis Antim ony 4129 Piney Creek Power Project BRBR1 Dry

basis Arsenic 4129 Piney Creek Power Project BRBR1 Dry

basis Beryllium 4129 Piney Creek Power Project BRBR1 Dry

basis Cadmium 4129 Piney Creek Power Project BRBR1 Dry

basis Chlorine 4129 Piney Creek Power Project BRBR1 Dry

basis Chromium 4129 Piney Creek Power Project BRBR1 Dry

basis Cobalt 4129 Piney Creek Power Project BRBR1 Dry

basis Fluorine 4129 Piney Creek Power Project BRBR1 Dry

basis Lead 4129 Piney Creek Power Project BRBR1 Dry

basis Manganese 4129 Piney Creek Power Project BRBR1 Dry

basis Mercury 4129 Piney Creek Power Project BRBR1 Dry

basis Nickel 4129 Piney Creek Power Project BRBR1 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04)

ASTMD5865 ASTM D3172 ASTM D3172 ASTM D4239-02 ASTMD5865 ASTM D3172 ASTM D4239-02 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D4208-02 ASTM D6357

ASTM D3761-02 ASTM D6357 ASTM D6357 ASTM 6722-01 ASTM D6357 ASTM D4606/D6357EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 4129 Piney Creek Power Project BRBR1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units M5/29 1 6/1/2010 6/1/2010 7254.00 Btu/lb M5/29 2 6/2/2010 6/2/2010 7250.00 Btu/lb M5/29 3 6/3/2010 6/3/2010 7579.00 Btu/lb M30B 1 6/1/2010 6/1/2010 7115.00 Btu/lb M30B 2 6/2/2010 6/2/2010 7458.00 Btu/lb M30B 3 6/3/2010 6/3/2010 7448.00 Btu/lb OTM27/28 1 6/1/2010 6/1/2010 7212.00 Btu/lb OTM27/28 2 6/2/2010 6/2/2010 7264.00 Btu/lb OTM27/28 3 6/3/2010 6/3/2010 7371.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 7.96 40.48 2.97 7881 Btu/lb 43.98 3.23 8.77 38.96 3.38 7947 Btu/lb 42.71 3.7 8.33 37.1 3.37 8268 Btu/lb 40.47 3.67 7.87 40.83 3.09 7723 Btu/lb 44.32 3.35 8.22 39.26 3.41 8126 Btu/lb 42.77 3.71 8.94 40.05 3.26 8179 Btu/lb 43.98 3.58 8.08 40.28 3.01 7846 Btu/lb 43.82 3.28 8.25 39.92 3.54 7918 Btu/lb 43.84 3.85 9.89 36.96 3.52 8180 Btu/lb 41.02 3.9Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 475 mg/kg 0.507 mg/Kg 1.52 mg/Kg 33.4 mg/Kg 2.29 426 mg/kg 0.641 mg/Kg 1.56 mg/Kg 39.6 mg/Kg 2.23 496 mg/kg 0.551 mg/Kg 1.25 mg/Kg 33.3 mg/Kg 2.07 439 mg/kg 0.487 mg/Kg 1.85 mg/Kg 34.2 mg/Kg 2.31 433 mg/kg 0.631 mg/Kg 1.77 mg/Kg 39 mg/Kg 2.07 501 mg/kg 0.516 mg/Kg 1.86 mg/Kg 33.7 mg/Kg 2.09Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg 0.17 mg/Kg 53.9 mg/Kg 25.1 mg/Kg 180 mg/Kg mg/Kg 0.15 mg/Kg 52.9 mg/Kg 26.5 mg/Kg 185 mg/Kg mg/Kg 0.16 mg/Kg 48.6 mg/Kg 23.9 mg/Kg 155 mg/Kg mg/Kg 0.25 mg/Kg 55.8 mg/Kg 25.9 mg/Kg 207 mg/Kg mg/Kg 0.19 mg/Kg 49.9 mg/Kg 25.1 mg/Kg 205 mg/Kg mg/Kg 0.29 mg/Kg 47.7 mg/Kg 23.8 mg/Kg 167 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 32.7 mg/Kg 5.55 mg/Kg 203 mg/kg 7.96 33.5 mg/Kg 5.35 mg/Kg 197 mg/kg 8.77 26.6 mg/Kg 5.46 mg/Kg 168 mg/kg 8.33 33.3 mg/Kg 4.83 mg/Kg 183 mg/kg 7.87 31.3 mg/Kg 6.87 mg/Kg 200 mg/kg 8.22 26.8 mg/Kg 6.33 mg/Kg 174 mg/kg 8.94 8.08 8.25 9.89 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 20.99 43.98 35.03 44.24 2.84 0.92 3.23 21.02 42.71 36.27 44.69 2.8 0.86 3.7 21.77 40.47 37.76 45.69 2.84 0.91 3.67 21.25 44.32 34.43 43.68 2.79 0.87 3.35 21.36 42.77 35.87 45.18 2.81 0.89 3.71 20.89 43.98 35.13 45.61 2.7 0.88 3.58 20.75 43.82 35.43 43.51 2.77 0.91 3.28 20.9 43.5 35.6 43.84 2.62 0.85 3.85 21.58 41.02 37.4 45.24 2.96 0.93 3.9 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

4.79 5.24 6.42 4.99 4.64 3.25 5.71 5.34 5.95EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 4129 Piney Creek Power Project BRBR1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 6c/7E 1 6/3/2010 6/3/2010 7094.00 Btu/lb 6c/7E 2 6/3/2010 6/3/2010 7412.00 Btu/lb 6c/7E 3 6/3/2010 6/3/2010 7431.00 Btu/lb HCN 1 6/4/2010 6/4/2010 7398.00 Btu/lb HCN 2 6/4/2010 6/4/2010 6931.00 Btu/lb HCN 3 6/4/2010 6/4/2010 7199.00 Btu/lb 26 1 6/3/2010 6/3/2010 7613.00 Btu/lb 26 2 6/3/2010 6/3/2010 7406.00 Btu/lb 26 3 6/4/2010 6/4/2010 6944.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 10.09 39.05 3.12 7891 Btu/lb 43.44 3.47 10.38 37.19 2.92 8270 Btu/lb 41.49 3.26 8.54 38.8 3.43 8124 Btu/lb 42.42 3.75 9.62 39.6 3.19 8185 Btu/lb 43.82 3.53 9.34 40.53 2.95 7654 Btu/lb 44.7 3.25 9.3 37.59 2.8 7937 Btu/lb 41.44 3.08 9.43 36.84 3.16 8406 Btu/lb 40.67 3.49 9.83 35.61 3.36 8213 Btu/lb 39.49 3.73 9.64 37.07 2.66 7685 Btu/lb 41.03 2.94Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 461 mg/kg 473 mg/kg 479 mg/kg 394 mg/kg 410 mg/kg 466 mg/kg 520 mg/kg 506 mg/kg 420 mg/kgBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 162 mg/kg 121 mg/kg 170 mg/kg 164 mg/kg 154 mg/kg 129 mg/kg 145 mg/kg 163 mg/kg 171 mg/kgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

10.09 21.07 43.44 35.49 43.94 2.76 0.91 3.47 10.38 22.15 41.49 36.36 46.61 2.97 0.91 3.26 8.54 21.33 42.42 36.25 45.3 2.88 0.87 3.75 9.62 21.2 43.82 34.98 45.09 2.88 0.9 3.53 9.34 20.34 44.7 34.96 42.47 2.74 0.81 3.25 9.3 21.96 41.44 36.6 44.81 2.71 0.91 3.08 9.43 22.45 40.67 36.88 47.05 2.99 0.95 3.49 9.83 21.34 39.49 39.17 45.78 2.81 0.89 3.73 9.64 21.96 41.03 37.01 44.22 2.86 0.91 2.94 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 5.48 4.76 4.78 3.78 6.03 7.05 4.85 7.3 8.04EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 4129 Piney Creek Power Project BRBR1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 6c/10 1 6/3/2010 6/3/2010 7094.00 Btu/lb 6c/10 2 6/3/2010 6/3/2010 7412.00 Btu/lb 6c/10 3 6/3/2010 6/3/2010 7431.00 Btu/lb 25a/320 1 6/4/2010 6/4/2010 7398.00 Btu/lb 25a/320 2 6/4/2010 6/4/2010 6931.00 Btu/lb 25a/320 3 6/4/2010 6/4/2010 7199.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 10.09 39.05 3.12 7891 Btu/lb 43.44 3.47 10.38 37.19 2.92 8270 Btu/lb 41.49 3.26 8.54 38.8 3.43 8124 Btu/lb 42.42 3.75 9.62 39.6 3.19 8185 Btu/lb 43.82 3.53 9.34 40.53 2.95 7654 Btu/lb 44.7 3.25 9.3 37.59 2.8 7937 Btu/lb 41.44 3.08Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 461 mg/kg 473 mg/kg 479 mg/kg 394 mg/kg 410 mg/kg 466 mg/kgBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 162 mg/kg 10.09 121 mg/kg 10.38 170 mg/kg 8.54 164 mg/kg 9.62 154 mg/kg 9.34 129 mg/kg 9.3 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 21.07 43.44 35.49 43.94 2.76 0.91 3.47 5.48 22.15 41.49 36.36 46.61 2.97 0.91 3.26 4.76 21.33 42.42 36.25 45.3 2.88 0.87 3.75 4.78 21.2 43.82 34.98 45.09 2.88 0.9 3.53 3.78 20.34 44.7 34.96 42.47 2.74 0.81 3.25 6.03 21.96 41.44 36.6 44.81 2.71 0.91 3.08 7.05 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 4129 Piney Creek Power Project BRBR1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm