NIST Special Publication 260-174 Rev. 2012 

Certification of SRM 2492:

Bingham Paste Mixture for 

Rheological Measurements

Chiara F. Ferraris

Paul E. Stutzman

William F. Guthrie

John Winpigler
NIST Special Publication 260-174 Rev. 2012 

Certification of SRM 2492:

Bingham Paste Mixture for 

Rheological Measurements

Chiara F. Ferraris

Paul E. Stutzman

John Winpigler

Materials and Construction Research Division

Engineering Laboratory

William F. Guthrie 

Statistical Engineering Division

Information Technology Laboratory

June 2012

U.S. Department of Commerce 

John E. Bryson, Secretary

National Institute of Standards and Technology 

Patrick D. Gallagher, Under Secretary of Commerce for Standards and Technology and Director
Certain commercial entities, equipment, or materials may be identified in this

document in order to describe an experimental procedure or concept adequately.

Such identification is not intended to imply recommendation or endorsement by the

National Institute of Standards and Technology, nor is it intended to imply that the

entities, materials, or equipment are necessarily the best available for the purpose.

National Institute of Standards and Technology Special Publication 260-174 Rev. 2012

Natl. Inst. Stand. Technol. Spec. Publ. 260-174 Rev. 2012, 301 pages (June 2012)

This report supersedes the previous report SP- 260-174

CODEN: NSPUE2
iv

Abstract

Rheological measurements are often performed using a rotational rheometer. In 

this type of rheometer, the tested fluid is sheared between two surfaces, one of which is

rotating [1]. Usually, the angular velocity is imposed and the response of the material is 

monitored by the measurement of the torque. The manufacturers recommend the use of a 

standard oil of known viscosity to verify that the instrument is operating correctly. 

Because these oils are expensive, however, they cannot be used for the large 

volumes employed in concrete rheometers. Therefore, a relatively inexpensive, accurate 

reference material is needed that incorporates aggregates for concrete rheometers. As 

concrete and mortar are non-Newtonian, the reference material should also be nonNewtonian. The development of this new Standard Reference Material (SRM) is based 

on a multiphase approach. This report is the description of the development and 

certification of a paste SRM. Based on this SRM, further SRMs for mortar and concrete 

will be developed in the future.

The purpose of this report is to describe the process used to certify SRM 2492, a 

“Bingham Paste Mixture for Rheological Measurements”. All measurements used for the 

development of the rheological characteristics are provided along with statistical 

analyses. 

This is report is the second edition of the report that includes the non-Newtonian 

analysis of the data collected. Thus, the following Sections were added or modified: 

2.3.2, 5.1.3, and Appendix C and D. The certificate draft was deleted from this report and 

it available only online.

This report supersedes the previous report SP-260-174
v

Acknowledgements

The authors would also like to thank some key persons at NIST without whom this 

certification could not have being completed: John Winpigler for packaging materials and 

performing the rheological tests; Max Peltz for making measurements and the packaging 

of the materials; Drs. Nicos Martys, Kenneth Snyder, Jonathan Martin (NIST) and 

Nicholas Dagalakis (NIST) for their valuable comments.

Dr. Ferraris would like to personally thank also Dr. Zhuguo Li (Yamaguchi University)

and Dr. Min-Hong Zhang (National University of Singapore) whose collaboration during 

their stay at NIST led to the basis of this SRM.
vi

Table of Contents

1 Introduction................................................................................................................. 1

2 Description of Rheological Measurements................................................................. 2

2.1 Introduction......................................................................................................... 2

2.2 Rheological parameters....................................................................................... 3

2.3 Measurements and interpretation........................................................................ 4

2.3.1 Experimental set-up ........................................................................................ 4

2.3.2 Calculation of the rheological parameters from the measurements................ 5

2.3.3 Calibration with oil ......................................................................................... 6

3 Materials ..................................................................................................................... 8

3.1 Characteristics of the Limestone and Corn Syrup .............................................. 8

3.2 Packaging.......................................................................................................... 10

3.3 Preparation of the SRM .................................................................................... 11

4 Experimental Design................................................................................................. 13

5 Statistical analysis..................................................................................................... 15

5.1.1 Introduction................................................................................................... 15

5.1.2 Newtonian Statistics...................................................................................... 15

5.1.3 Non- Newtonian Statistics............................................................................ 18

6 Summary................................................................................................................... 20

7 References................................................................................................................. 20

8 Appendix................................................................................................................... 22

Appendix A: Statistical Analysis for Newtonian calculations ...........................A-1

Appendix B: Data for Newtonian calculations ..........................................B-1

Appendix C: Statistical analysis for Non-Newtonian calculations ........................C-1

Appendix D: Data for Non-Newtonian calculations .........................................D-1
vii

List of Figures

Figure 1: Bingham model and calculation of the plastic viscosity and yield stress. .......... 4

Figure 2: Parallel plate rheometer....................................................................................... 7

Figure 3: Particle size distribution of the limestone measured in IPA ............................... 9

Figure 4: Limestone SEM pictures at various magnifications as indicated by scale bars on 

the pictures................................................................................................................ 10

List of Tables

Table 1: Physical and mineralogical properties of the limestone flour .............................. 9

Table 2: Schema for pairing the “Component 1 Corn Syrup” with the two containers of 

the “Component 2 Limestone” for CS-BX1 and BX-1 to BX-4 .............................. 12

Table 3: Pairing of the boxes of “Component 1 Corn Syrup” (CS-BXA) with the boxes 

(BX-A) of “Component 2 Limestone.”..................................................................... 13

Table 4: Set selected to be tested. BL is the corn syrup bottle (see Table 2) ................... 13

Table 5: Order of testing. CS-BXA = Corn Syrup Box A; BLA= Bottle A of corn syrup 

(from specified box); LA=Limestone bottle A (associated with specified box and 

bottle of corn syrup- see Table 2) ............................................................................. 14

Table 6: Schedule of testing. HOLIDAY and OFF are days the operator was not 

available. See Table 5 for the tests done for each A1 to F7...................................... 15

Table 7: Newtonian approximation results....................................................................... 17

Table 8: Non-Newtonian approximation results............................................................... 20
1

1 Introduction

A National Institute of Standards and Technology (NIST) Standard Reference 

Material® (SRM) meets specific certification criteria and is issued with a certificate of 

analysis that reports the results of its characterization and provides information regarding 

the appropriate use(s) of the material. An SRM is prepared and used for three main 

purposes: 1) to help develop accurate methods of analysis; 2) to calibrate measurements 

systems used to facilitate exchange of goods, institute quality control, determine 

performance characteristics, or measure a property at the state-of-art limit; and 3) to 

ensure the long-term adequacy and integrity of measurement quality assurance programs. 

The National Institute of Standards and Technology (NIST) provides over 1300 different 

SRMs to industry and academia. Every NIST SRM is provided with a certificate of 

analysis that gives the official characterization of the material’s properties. In addition, 

supplementary documentation, such as this report, describing the development, analysis, 

and use of SRMs, is also often provided to ensure effective use of these materials.

There are several SRMs related to the cement industry but none is related to the 

rheological properties of cement paste, mortar or concrete. After completing two 

international inter-laboratory studies related to rheological properties measurements of 

concrete, it was determined that the use of expensive oils was not suitable for calibration 

of concrete rheometers. Thus, a need exists for a granular reference material specifically 

designed for concrete was requested by the industry. SRM 2492, the first step for in 

concrete rheological SRM production, is a two-component fluid having Bingham 

characteristics. The operator needs to mix the two components with water in the 

proportions provided in the certificate. Once mixed the material shelf life of the mixture

is 7 d. The values given in this report were obtained through testing performed at NIST 

using a serrated parallel plate rheometer. 

The objective of this report is to describe the SRM 2492 and its rheological 

properties. A brief description of the methodology and all measurements used are 

provided along with the statistical analysis.

This is report is the second edition of the report that includes the non-Newtonian 

analysis of the data collected. Thus, the following Sections were added or modified: 

2.3.2, 5.1.3, and Appendix C and D. The certificate draft was deleted from this report and 

it available only online. 

This report supersedes the previous report SP-260-174
2

2 Description of Rheological Measurements

2.1 Introduction

Rheological measurements are commonly performed using a rotational rheometer. 

In this type of rheometer, the test fluid is sheared between two surfaces, one of which is

rotating while the other is stationary [1]. The rate of the rotating surface is precisely 

controlled by a computer, while measuring the torque resulting from the material 

response. Laboratory rheometers are mainly designed for homogeneous liquids, such as 

oils, containing no particles, such as oils. The manufacturers recommend the use of a 

standard oil of known viscosity to verify that the instrument is operating correctly. The 

kinematic viscosities are determined by reference to the water viscosity established by 

international consensus in 1953 [2], as described in ISO-3666 (International Organization 

for Standardization) [3]. In 1954, NIST [2] conducted a study to compare two rheological 

techniques, the Bingham viscometer and the Cannon Master viscometer (both based on 

capillary flow) that are still used today for determining the viscosity values of standard 

oils. 

Because these oils are expensive, it is not economically practical to use them due 

to the large volumes of oil needed in concrete rheometers. Some concrete rheometers 

have used a less expensive oil with a known viscosity to calibrate a concrete rheometer. 

For example, in 2003, a high viscosity polydimethylsiloxane fluid (with a NIST measured 

viscosity of 29.5 Pa·s ± 0.6 Pa·s at 24.4 °C ± 0.4 °C), was used in concrete rheometers 

[4] during an international round robin. It was shown that not all rheometers were able to 

measure the oil rheological properties, due to their specific shear patterns and slippage or 

lack of it on the shearing surfaces. In the case of fresh concrete, the geometry of the

rheometer needs to allow the distance between the shearing surfaces to be sufficiently

large to accommodate aggregates of at least 25 mm in diameter. The increase in size 

leads to generally unknown shear patterns and test results that cannot quantitatively 

characterized in fundamental units. Therefore, calibration of such large and non-standard 

rheometers is impossible using the traditional measurement protocols. It should be stated 

that the responses from any two concrete rheometers were found to be linearly related [4, 

5, 6]. 

Thus current research has established the need for a new reference material for 

calibrating concrete rheometers. Concrete is a non-Newtonian suspension, thus any 

reference material mixture must be a non-Newtonian suspension. Ideally such a material 

must be inexpensive, reproducible and repeatable with respect of both its physical and 

chemical properties, and readily allow the inclusion of aggregates, similar as used in 

concrete. Given the constraints, the new strategy was to develop a granular mixture 

similar to concrete. The American Concrete Institute (ACI) Committee 238 on 

“Workability of Fresh Concrete” considered this approach and recommended the use of 

an oil of known viscosity in which particles could be added. The calculation of the 

viscosity of the mixture would be a combination of experimental measurements and 

computerized modeling. Thus, spherical particles would simplify the computerized 
3

model. Moreover, the particle specific gravity should match that of the oil to avoid 

sedimentation during testing as the medium has no yield stress. Given these constraints, 

hollow plastic spheres were an excellent candidate material. Unfortunately, their cost is

prohibitive. Therefore, this idea was deemed impractical and thus, was abandoned as a 

viable strategy. Instead, a multiscale approach was considered to be the next best option.

The multiscale approach consists of developing a paste, followed by a wellcharacterized mortar and the well-characterized concrete. A mortar is produced by adding

sand to the paste, while a concrete is produced by adding coarse aggregates to this 

mortar. The rheological parameters of the mortar and concrete would be determined from 

the paste through a combination of measurements and computer simulation. The 

simulation is designed to calculate the viscosity of the suspensions (mortar or concrete) 

from the medium viscosity (cement paste) with various aggregate concentrations, 

aggregate size distribution, and particle shape. Therefore, the first step is to develop a

paste reference material. This report presents the new SRM that was produced based on a 

preliminary study [7]. 

A non-Newtonian reference material for cement paste should have the following 

characteristics: 1) no particle segregation for the duration of the test; 2) linear Bingham 

stress response to shear rates over a large range; 3) rheological and chemical properties 

unchanged over at least several days, with no chemical reactions between the medium 

and the particles; 4) a yield stress sufficient to avoid segregation of added sand and 

coarse aggregates; and 5) the linear response should be reversible, implying no structural 

breakdown or build-up, flocculation or deflocculation during the test, i.e., no hysteresis.

2.2 Rheological parameters

The primary output of rheological measurements is either a shear stress-shear rate 

plot or a plot of the rotational speed of the rotating surface versus the torque. In cases 

where the geometry of the rheometer does not permit a direct calculation of the shear 

stress and shear rate in fundamental units, the rotational speed is plotted against torque 

[8]. 

The viscosity [1] is defined as the ratio of the shear stress over the shear rate at a 

given shear rate. For a Newtonian fluid, the viscosity is the slope of a line with zero 

intercept fit to the shear stress-shear rate data. Most granular mixtures are nonNewtonian, however. Non-Newtonian mixtures exhibit a yield stress, which is the stress 

needed to initiate deformation or flow of the material. This yield stress can be measured 

in several ways. The most common method is the extrapolation from the Bingham test 

method [8, 9, 10]. 

The Bingham equation (Eq. (1)) is used in determining the plastic viscosity and 

the yield stress. This procedure implies that the plastic viscosity ηpl is defined as the slope 

of the shear stress versus shear rate curve and the yield stress τB is the intercept of the 

curve at zero shear rate. This point is generally not measured so this constitutes an 

extrapolation (Figure 1). The Bingham rheological parameters, yield stress and plastic 
4

viscosity, will characterize the flow curve within a range of shear rates, as shown in 

Figure 1and equation [1]. 

σ σ η γ = B + pl [ 1]

where σ = shear stress, σB = yield stress, ηpl = plastic viscosity, and γ = shear rate.

Figure 1: Bingham model and calculation of the plastic viscosity and yield stress.

2.3 Measurements and interpretation

2.3.1 Experimental set-up

Conventional rotational rheometers often have different geometries. Nevertheless, 

the principle always involves two surfaces shearing the material [1]. The geometry used 

in this report is serrated parallel plates as shown in Figure 2. The plates were 35 mm in 

diameter. Figure 2A shows the actual plates while Figure 2B shows a schematic of a 

parallel plate rheometer. To shear a granular material, precautions need to be taken to 

avoid slippage of the shearing surface. The device used had serrated surfaces as shown in 

Figure 2C. As this SRM contains water, precautions also need to be taken to avoid 

evaporation during the measurement. This is achieved by creating a small enclosure 

around the shearing plates as shown in Figure 2D. Finally, a wet sponge was placed in the 

enclosure to maintain a high relative humidity environment. 

The gap between the two parallel plates was 0.600 mm ± 0.001 mm. A smaller gap 

could cause the particles to jam while a larger gap might lead to the material not staying 

between the plates. The temperature of the rheometer was maintained at 23 °C ± 0.5 °C 

during all tests. A measured volume of 1.3 mL of material was placed in the rheometer 

and the gap adjusted to 0.6 mm. Then the material was nominally sheared at 0.01 s-1 for 

150 s before starting the Bingham test. The Bingham test consisted in increasing the 

nominal shear rates from 0.1 s-1 to 50 s-1 (10 points) and then decreasing shear rate from 

ηpl

σB

Shear rate

*

* *

* *

*

Shear stress

ηpl

σB

Shear rate

*

* *

* *

*

Shear stress
5

50 s-1 to 0.1 s-1 (20 points). At each point the shear rate was maintained at the desired 

value until equilibrium of the torque was reached, but for a time not to exceed 30 s.

2.3.2 Calculation of the rheological parameters from the measurements

In the rheometer used the rotational speed is controlled and the torque is measured. 

The computer software calculates automatically the shear rate and the shear stress from 

the rotational speed and the measured torque. The shear rate is calculated as follows:

n

h

R

R γ = ⋅ 2π ⋅ [ 2]

where: R γ = shear rate at the outer edge [1/s]

R = radius of shear [mm] (17.5 mm in our case)

h = gap or distance between the plates [mm] (0.600 mm ± 0.001 mm)

n = speed of rotation of the top plate, revolution/s [1/s] 

The shear stress calculation from the torque is [8]

) ln

ln (3

2 3 d R

d T

R

T

π γ

τ  + ⋅ ⋅ = [ 3]

where τ = shear stress [Pa]

T = torque at the outer edge [N.m]

R = radius of shear [mm] (17.5 mm in our case)

R γ = shear rate [1/s]

An analysis was conducted to determine the value of the factor, �3 + dlnT

dlnγ̇

R

�, using two 

different approaches, Newtonian and non-Newtonian. 

Newtonian approximation

For Newtonian liquids the factor is equal to 1. In the data collected for this project, the 

factor was estimated to be 0.84 leading to an error of about 4 % (less than the uncertainty 

due to other factors) if this material were treated as though it was Newtonian. The usage 

of the Newtonian approximation would simplify the calculations for user and the stress 

would be:

3

2

R

T

⋅

⋅ = π

τ

[ 4]

Non-Newtonian approximation

In a study conducted at NIST [7], the factor R d lnT d lnγ was found to vary with shear 

rates. If the shear rate is above 5 s-1 then the value is 0.8 ± 0.1 (one standard deviation), 

while it decreases to 0.2 for shear rates below 5 s-1. The viscosities were calculated using 
6

both Newtonian and non-Newtonian methods and it was found that the use of the simpler 

Newtonian approximation would give a plastic viscosity error of less than 3 % while the 

yield stress error would be more significant at up to 20 % [7]. 

Conclusions

Therefore, the non-Newtonian approximation was considered a better approximation of 

the factor R d lnT d lnγ and was used to calculate the certified values. Nevertheless, the 

two statistical approximations, Newtonian, and non-Newtonian will be provided in this 

report. 

2.3.3 Calibration with oil

Accurate rheological error assessment, including the correction of the zeroing of the 

plates requires a standard oil. The measurement protocol for making these assessments is 

described in Section 5.

After calculating of the shear rate and shear stress from the torque and angular 

velocity, these values were corrected for plate roughness and zeroing error (due to the 

instrument) as outlined by Ferraris et al. [9]. This correction consists of modifying the 

gap by 0.27 mm [10, 11, 12]. Further details on the uncertainty of the method can be 

found in ref. [9].

The hysteresis (Pa/s) was defined as the area between the up (increasing shear rate) 

and down (decreasing shear rates) curves of shear stress vs. shear rate.
7

A

B

C D

Figure 2: Parallel plate rheometer

Torque

gap
8

3 Materials

3.1 Characteristics of the Limestone and Corn Syrup

Preliminary tests were conducted on samples of the corn syrup from another batch 

of material used for this SRM. According to the manufacturer, the material is a pure corn 

syrup with no additives. Its density measured at NIST was 1436 kg/m3 ± 5 kg/m3 (one 

standard deviation), with a water content of 18.6 % ± 0.2 % by mass, and a composed of

100 % glucose. 

The limestone powder is referred to by the manufacturer as micro-limestone flour.

Per the manufacturer, the limestone powder is passed a #325 sieve (45 μm opening). The 

particle size distribution of the limestone is shown in Figure 3. Analyses were conducted 

on samples of the limestone powder to determine its mineralogical, chemical, and 

physical properties. 

The mineralogical analysis by X-ray powder diffraction is based upon replicate 

analyses of the bulk limestone powder. In addition, X-ray powder diffraction was also 

performed on insoluble residue of carbonate phase. The insoluble residue was obtained 

through a 10 % by volume hydrochloric acid extraction of the bulk limestone. The 

insoluble residue is typically composed of quartz, clays, and other minerals unaffected by 

the dissolution process. The residue is pipetted onto a glass slide to facilitate 

identification of the clay minerals, and the slide is analyzed after three treatments: heating 

to 110 °C to collapse any expandable clays, saturation in a 50% ethylene glycol solution 

to expand the basal spacing of any expandable clays, and then heating to 550 °C to 

collapse the layers completely and to decompose specific clay minerals. The most 

reliable numbers are the carbonates and quartz. Based upon a single measurement of 

mass loss on dissolution, the insoluble residue was estimated to comprise about 2.5 % of 

the total limestone powder. The residue also appeared deliquescent, possibly confounding 

the insoluble residue analysis. 

The limestone is composed (Table 1) of calcite, dolomite, tremolite, quartz, talc, a 

chlorite/smectite inter-stratified clay and an illite/mica. The presence of talc and tremolite 

is not uncommon in limestones exposed to some metamorphic processes. Scanning 

Electron Microscopy (SEM) pictures at various magnifications are shown in Figure 4.
9

Table 1: Physical and mineralogical properties of the limestone flour

Properties Values

Density [kg/m3] 2815 ± 5

BET surface [m2/g] 1.05 ± 0.02

Phases mass fractions

calcite 75.0 % ± 2.6 %

dolomite 20.0 % ± 2.1 %

quartz 0.8 % ± 0.7 %

tremolite 2.0 % ± 0.8 %

talc 0.8 % ± 0.2 %

chlorite 0.7 % ± 0.7 %

Figure 3: Particle size distribution of the limestone measured in IPA

0

1

2

3

4

5

0.1 1 10 100 1000

Size [μm]

Differential [%]
10

Figure 4: Limestone SEM pictures at various magnifications as indicated by scale 

bars on the pictures

3.2 Packaging

The corn syrup was purchased in 3.78 L (1 gallon) bottle and the corn syrup in each 

gallon bottle was repackaged at NIST into the smaller glass bottles containing about 500 

g of corn syrup. Each smaller bottle was numbered from 1 to 48 and placed in a box. In 

total there were 5 boxes labeled CS-BXA (A= 1 to 5). 

The limestone was ordered in a bag of 907 kg (2000 lbs). The material was then 

repackaged into plastic jars containing with about 600 g of limestone each. Each jar was 

labeled from 1 to 24 and placed in a box BX-A (A = 1 to 20). Prior to final packaging for 

shipment, the bottles were selected following the scheme shown in Table 2 for CS-BX1 

and the corresponding boxes, BX-1 to BX-4, of limestone

The packaged SRM contains enough material to make two batches of paste. It has 

one glass container labeled “Component 1 Corn Syrup” (500 g) and two plastic 
11

containers labeled “Component 2 Limestone” (each about 600 g). Each of the plastic 

containers is one batch while the glass bottle contains enough corn syrup for two batches.

3.3 Preparation of the SRM

The SRM batch must be prepared by the operator before it can be used. Once mixed, 

the shelf life of the mixture is about 7 d. Therefore, it should not be prepared too far in 

advance of its usage. To prepare the mixture, follow the instructions below.

Mixture composition

• Corn Syrup: 200 g

• Distilled water: 63.16 g

• Limestone: 458.1 g

The equipment and the method are described in ASTM C1738. Introduce the water 

and the corn syrup (in that order) into the blender, mix for 30 s and then proceed as 

described in ASTM C1738 to introduce the limestone. The water bath and the rheometer 

should be maintained at 23 °C. 

Store the mixture in a sealed plastic jar. It is recommended to use a plunger mixer to 

remix the prepared SRM before each use. Store the SRM in a sealed container, 

maintained at 23 °C ± 2 °C. 
12

Table 2: Schema for pairing the “Component 1 Corn Syrup” with the two 

containers of the “Component 2 Limestone” for CS-BX1 and BX-1 to BX-4

Corn Syrup Limestone

Box # Bottle # Box # Jar #

CS-BX1 1 BX-1 1-2

2 3-4

3 5-6

4 7-8

5 9-10

6 11-12

7 13-14

8 15-16

9 17-18

10 19-20

11 21-22

12 23-24

13 BX-2 1-2

14 3-4

15 5-6

16 7-8

17 9-10

18 11-12

19 13-14

20 15-16

21 17-18

22 19-20

23 21-22

24 23-24

25 BX-3 1-2

26 3-4

27 5-6

28 7-8

29 9-10

30 11-12

31 13-14

32 15-16

33 17-18

34 19-20

35 21-22

36 23-24

37 BX-4 1-2

38 3-4

39 5-6

40 7-8

41 9-10

42 11-12

43 13-14

44 15-16

45 17-18

46 19-20

47 21-22

48 23-24
13

Table 3: Pairing of the boxes of “Component 1 Corn Syrup” (CS-BXA) with the 

boxes (BX-A) of “Component 2 Limestone.”

Corn Syrup Limestone

CS-BX1 BX-1 to BX-4

CS-BX2 BX-5 to BX-8

CS-BX3 BX-9 to BX-12

CS-BX4 BX-13 to BX-16

CS-BX5 BX-17 to BX-20

4 Experimental Design

Twelve units of the SRM as packaged for sale were randomly selected for testing. 

Two units were tested each day. As each unit contains two batches of SRM, four tests 

were done on each day of testing. Each mixture was measured immediately after mixing 

(labeled as 1 d), and 3 d and 7 d after mixing. The order of each mixture and 

measurement was randomized as shown in Table 5 and the schedule is shown in Table 6. 

Each reported value was the average of 3 consecutive tests run back-to-back. All raw data 

are shown in Appendix B.

Table 4: Set selected to be tested. BL is the corn syrup bottle (see Table 2)

CS-BX5 BL 45

BL 12

CS-BX1 BL 23

BL 28

CS-BX3 BL 30

BL 03

CS-BX5 BL 11

BL 36

CS-BX3 BL 04

BL 41

CS-BX1 BL 33

BL 06
14

Table 5: Order of testing. CS-BXA = Corn Syrup Box A; BLA= Bottle A of corn syrup (from specified box); LA=Limestone 

bottle A (associated with specified box and bottle of corn syrup- see Table 2)

Day of mixing 3 d after mixing 7 d after mixing

CS-BX5 BL 45 L 2 A1 CS-BX5 BL 12 L 1 A3 CS-BX5 BL 12 L 2 A7

BL 12 L 2 BL 45 L 2 BL 45 L 1

BL 12 L 1 BL 45 L 1 BL 45 L 2

BL 45 L 1 BL 12 L 2 BL 12 L 1

CS-BX1 BL 23 L 2 B1 CS-BX1 BL 23 L 1 B3 CS-BX1 BL 23 L 2 B7

BL 23 L 1 BL 28 L 1 BL 23 L 1

BL 28 L 2 BL 28 L 2 BL 28 L 2

BL 28 L 1 BL 23 L 2 BL 28 L 1

CS-BX3 BL 30 L 1 C1 CS-BX3 BL 03 L 1 C3 CS-BX3 BL 03 L 1 C7

BL 03 L 1 BL 30 L 2 BL 30 L 2

BL 03 L 2 BL 03 L 2 BL 30 L 1

BL 30 L 2 BL 30 L 1 BL 03 L 2

CS-BX5 BL 11 L 2 D1 CS-BX5 BL 36 L 1 D3 CS-BX5 BL 36 L 2 D7

BL 36 L 1 BL 36 L 2 BL 11 L 1

BL 11 L 1 BL 11 L 2 BL 11 L 2

BL 36 L 2 BL 11 L 1 BL 36 L 1

CS-BX3 BL 04 L 1 E1 CS-BX3 BL 04 L 1 E3 CS-BX3 BL 41 L 2 E7

BL 41 L 2 BL 41 L 2 BL 41 L 1

BL 41 L 1 BL 04 L 2 BL 04 L 2

BL 04 L 2 BL 41 L 1 BL 04 L 1

CS-BX1 BL 33 L 1 F1 CS-BX1 BL 06 L 2 F3 CS-BX1 BL 06 L 1 F7

BL 06 L 2 BL 33 L 1 BL 06 L 2

BL 33 L 2 BL 06 L 1 BL 33 L 1

BL 06 L 1 BL 33 L 2 BL 33 L 2
15

Table 6: Schedule of testing. HOLIDAY and OFF are days the operator was not 

available. See Table 5 for the tests done for each A1 to F7.

Week 

number Day of the week

M T W T F

W1 HOLIDAY A1 A3

W2 B1 A7 B3 OFF

W3 B7 C1 C3

W4 D1 C7 D3 OFF

W5 D7 E1 E3

W6 HOLIDAY E7 OFF

W7 F1 F3

W8 F7 OFF

5 Statistical analysis

5.1.1 Introduction

The data used for the analysis of various rheological quantities for SRM 2492 were

collected using a nested design with 3 primary factors: box, day, and unit. Two replicate 

samples were prepared for each unit, each using corn syrup from the single bottle 

associated with the unit and the limestone from the two single-use bottles of limestone 

powder associated with the unit. With this design a linear model can be fit to the data to 

identify different levels of random variability associated with each of the three primary 

factors. In addition the run order of the measurements is another factor whose potential 

effect is addressed by randomization of the run order.

Results derived from the raw data were recorded for three quantities: viscosity (VS), 

yield strength (YS), and hysteresis (H) from tests carried out on the samples at three 

different ages (1 d, 3 d, and 7 d). Since age of the sample is believed to have a significant 

effect a priori, the results at each age are treated as different responses, giving 9 responses 

in all. The data used in the analysis are shown in Table 1 in Appendix A-1 for the 

Newtonian approximation and in Table 1 in Appendix C-1 for non-Newtonian 

approximation.

5.1.2 Newtonian Statistics

The first step in the analysis of the data was an exploratory data analysis. In this 

analysis plots of the data in run order, versus age, and versus each of the three primary 

factors were examined for evidence of measurement drift, outliers, factor effects, and any 

other features that might impact further analysis for certification. In addition, normal 

probability plots of each response were made to assess the normality of the data, assuming 

the effects of the other factors are not large. These plots are shown in Appendix A on pages 

A-2 through A-43 and were made using the software package R [13]. While a few outlying 

points were observed, these data were not associated with any recognized problems 

associated with sample preparation or measurement, so no data were omitted from further 

analysis. (Note, prior to this analysis, while the data were being organized, two 
16

observations that were associated with recognized issues in sample preparation or 

measurement and whose results differed significantly from what was expected and 

observed for similar cases were omitted from the analysis. One sample was omitted for all 

responses at all ages while only the measurements at an age of 1 d for the other sample 

were affected.) No large factor effects were identified from these plots either, although the 

plots suggest that small effects may be present in some cases. Assuming any factor effects 

that do exist are essentially insignificant relative to the random measurement error, all 

responses appear to follow a distribution that is approximately normal.

Next a Bayesian hierarchical model was fit to the data to quantify contributions to 

the overall variability in the data from random errors associated with the factors day and 

unit. A Bayesian model was used because after the loss of the two samples mentioned 

above, the data were no longer balanced, limiting the effectiveness of fitting the model 

using analysis of variance (ANOVA). The validity of inferences drawn using the Bayesian 

model, in contrast, is not affected by the lack of balance. In addition, the Bayesian analysis 

provides a clear statistical interpretation with no need for approximation or use of 

asymptotic results.

The factor box was not included in the model because no large box effect was seen 

in the exploratory plots and with data sampled from only three of five possible boxes, 

estimation of a variance component for this factor will be sensitive to prior assumptions. 

To avoid this situation in the future, NIST plans to sample all, or at least five, levels of the 

highest level factor in future SRM experiments. Fortunately in this case omission of 

random variation related to box does not look like it will cause any problems.

To use the Bayesian model, shown in Appendix A on page A-44, prior assessments 

of the values of each parameter in the model must be provided. The prior assessment for 

each parameter is specified as probability distribution for the parameter’s unknown value. 

Because these probability distributions are specified independently of the data (i.e. before 

the data are observed or used), these distributions are commonly called prior distributions. 

For this analysis, non-informative prior distributions were used. These distributions are 

essentially very flat and have very large variances so that they will not provide any 

quantitative information on the values of the parameters as part of the model. In this case 

uniform distributions, with ranges from -1000 to 1000 for means and ranges of 0 to 1000 

for standard deviations, were used. Fitting the model with prior distributions with larger or 

smaller ranges confirmed that the results were not sensitive to the parameters chosen for 

the prior distributions.

A probability distribution for each measurement, given with respect to the 

parameters in the model, is also specified. In this case the random errors associated with 

each factor were modeled as following a normal distribution. Then, based on the model 

and the observed data, the prior distributions for each parameter are updated using Bayes’ 

Theorem to obtain new distributions for each parameter given the information in the data. 

Finally, these new distributions, called posterior distributions, are used to obtain 

uncertainty intervals about each quantity of interest.

The Bayesian model was fit using Markov Chain Monte Carlo simulation as 

implemented in the software package WinBUGS [14, 15]. Diagnostic plots (not included 

in this report) show that the Markov Chains had converged by the 5000th iteration of the 

simulation. Then 5000 additional iterations were run for each of 5 parallel Markov chains 
17

for model validation and to estimate the parameter values. Box plots made using R for 

model validation are shown in Appendix A on pages A-45 through A-53. These plots show 

the distributions of the posterior predictive residuals from the model for each data point. 

The facts that the means of these distributions are randomly scattered around a value of 

zero and most distributions have considerable probability near zero support (but do not 

guarantee) the conclusion that this model provides a reasonable description of the data.

Assuming that the hierarchical model does provide an adequate description of the 

measurement process, proposed certified values for each of the different rheological 

quantities were determined from the predictive distribution for a randomly selected unit. 

Use of the predictive distribution was chosen for this purpose because it accounts for 

uncertainty from any potential heterogeneity among units and thus is more robust than an 

assessment that assumes under certain conditions that the material is homogenous. The 

results are presented graphically on pages A-54 through A-62 of Appendix A. The shaded

blue region under each distribution shown in blue indicates the 95 % probability intervals 

for each quantity. The corresponding values are given by the blue numbers just under the 

shaded regions.

The empirically determined posterior predictive distributions are well approximated 

by shifted and scaled Student’s t distributions with varying degrees of freedom and 

standard uncertainties. These distributions are shown as dashed red lines on each of the 

plots on Appendix A, pages A-54 through A-62. 

The corresponding numerical results, which are the values proposed for use on the 

certificate, are given in Table 7.

Table 7: Newtonian approximation results

Parameter Age

[days]

Mean 

value 

y

Standard 

Uncertainty 

u(y)

Degree 

of 

Freedom 

v

Coverage 

Factor

k

Expanded 

Uncertainty 

U

Lower 

bound

Upper 

Bound

YS 1 32.2 1.999 3.7 2.8675 5.7 26.5 38.0

YS 3 26.4 1.242 4.2 2.7251 3.4 23.0 29.7

YS 7 26.2 1.753 4.0 2.7764 4.9 21.3 31.1

VS 1 7.2 0.537 4.0 2.7764 1.5 5.7 8.6

VS 3 6.5 0.481 4.0 2.7764 1.3 5.1 7.8

VS 7 7.1 0.885 4.1 2.7499 2.4 4.7 9.5

H 1 394 106.6 4.4 2.6905 295 99 689

H 3 358 61.5 3.9 2.8047 173 185 530

H 7 432 110.5 3.6 2.9024 321 111 752
18

5.1.3 Non- Newtonian Statistics

This section describes the reanalysis of the rheological properties for SRM 2492 for 

the non-Newtonian approximation. The raw data were reduced using an improved method 

relative to the method used in Section 5.1.2. Reduction of the raw data was done prior to 

statistical analysis in both cases.

The first step in the analysis of the data was again an exploratory data analysis. In 

this analysis plots of the data in run order, versus age, and versus each of the three primary 

factors were examined for evidence of measurement drift, outliers, factor effects, and any 

other features that might impact further analysis for certification. In addition, normal 

probability plots of each response were made to assess the normality of the data, assuming 

the effects of the other factors are not large. These plots are shown in Appendix C on pages 

C-2 through C-43 and were made using the software package R [13]. While a few outlying 

points were observed in this data, these were not associated with any recognized problems 

associated with sample preparation or measurement, so no data was omitted from further 

analysis. (Note, prior to this analysis, while the data were being organized, observations 

that were associated with recognized issues in the preparation or measurement of two 

samples were omitted from the analysis. Responses from both samples were omitted for all 

ages. This differs slightly from the earlier analysis in which the results from the second 

sample were only omitted for Age=1.) No large factor effects were identified from these 

plots either, although the plots suggest that small effects may be present in some cases. 

Assuming any factor effects that do exist are essentially insignificant relative to the 

random measurement error, all responses appear to follow a distribution that is 

approximately normal.

Next a Bayesian hierarchical model was fit to the data quantify contributions to the 

overall variability in the data from random errors associated with the factors day and unit. 

A Bayesian model was used because after the loss of the two samples mentioned above, 

the data were no longer balanced, limiting the effectiveness of fitting the model using 

ANOVA. The statistical validity of inferences drawn using the Bayesian model, in 

contrast, are not affected by the lack of balance. In addition, the Bayesian analysis provides 

a clear statistical interpretation with no need for approximation or use of asymptotic 

results.

The factor box was not included in the model because no large box effect was seen 

in the exploratory plots and, with data sampled from only three of five possible boxes, 

estimation of a variance component for this factor will be sensitive to prior assumptions. 

To avoid this situation in the future, NIST plans to sample all, or at least five, levels of the 

highest level factor in subsequent experiments. Fortunately in this case omission of random 

variation related to box does not look like it will cause any problems.

In order to use the Bayesian model, shown in Appendix C on page C-44, prior 

assessments of the values of each parameter in the model must be provided. The prior 

assessment for each parameter is specified as probability distribution for the parameter’s 

unknown value. Because these probability distributions are specified independently of the 

data (i.e. before the data is observed or used), these distributions are commonly called prior 

distributions. For this analysis, non-informative prior distributions were used. These 
19

distributions are essentially very flat and have very large variances so that they will not 

provide any quantitative information on the values of the parameters as part of the model. 

In this case uniform distributions, with ranges from -1000 to 1000 for means and ranges of 

0 to 1000 for standard deviations, were used. Fitting the model with prior distributions 

with larger or smaller ranges confirmed that the results were not sensitive to the parameters 

chosen for the prior distributions.

A probability distribution for each measurement, given with respect to the 

parameters in the model, is also specified. In this case the random errors associated with 

each factor were modeled as following a normal distribution. Then, based on the model 

and the observed data, the prior distributions for each parameter are updated using Bayes’ 

Theorem to obtain new distributions for each parameter given the information in the data. 

Finally, these new distributions, called posterior distributions, are used to obtain 

uncertainty intervals about each quantity of interest.

The Bayesian model was fit using Markov Chain Monte Carlo simulation as 

implemented in the software package WinBUGS [14, 15]. Diagnostic plots (not included 

in this memo) show that the Markov Chains had converged by the 5000th iteration of the 

simulation. Then 5000 additional iterations were run for each of 5 parallel Markov chains 

for model validation and to estimate the parameter values. Box plots made using R for 

model validation are shown Appendix C on pages C-45 through C-53. These plots show 

the distributions of the posterior predictive residuals from the model for each data point. 

The facts that the means of these distributions are randomly scattered around a value of 

zero and most distributions have considerable probability near zero support (but do not 

guarantee) the conclusion that this model provides a reasonable description of the data.

Assuming that the hierarchical model does provide an adequate description of the 

measurement process, proposed certified values for each of the different rheological 

quantities were determined from the predictive distribution for a randomly selected unit. 

Use of the predictive distribution was chosen for this purpose because it accounts for 

uncertainty from any potential heterogeneity between units and thus is more robust than an 

assessment that assumes under certain conditions that the material is homogenous. The 

results are presented graphically on pages C-54 through C-62 of Appendix C. The shaded 

blue region under each distribution shown in blue indicates the 95 % probability intervals 

for each quantity. The corresponding values are given by the blue numbers just under the 

shaded regions.

The empirically determined posterior predictive distributions are well approximated 

by shifted and scaled Student’s t distributions with varying degrees of freedom and 

standard uncertainties. These distributions are shown as dashed red lines on each of the 

plots on Appendix C, pages C-54 through C-62. 

The corresponding numerical results, which are the values proposed for use on the 

certificate, are given in Table 8. 
20

Table 8: Non-Newtonian approximation results

Parameter Age

[days]

Mean 

value y

Standard 

Uncertainty 

u(y)

Degree of 

Freedom v

Coverage 

Factor

k

Expanded 

Uncertainty U

Lower 

bound

Upper 

Bound

YS 1 25.3 1.512 3.7 2.8675 4.3 21.0 29.7

YS 3 20.7 1.005 4.2 2.7251 2.7 18.0 23.4

YS 7 20.4 1.273 4.0 2.7764 3.5 16.9 24.0

VS 1 7.1 0.549 4.0 2.7764 1.5 5.6 8.6

VS 3 6.8 0.501 4.0 2.7764 1.4 5.4 8.2

VS 7 7.2 0.652 4.1 2.7499 1.8 5.4 9.0

H 1 264 77.45 4.4 2.6905 208 55 472

H 3 254 53.28 3.9 2.8047 149 104 403

H 7 345 117.97 3.6 2.9024 342 3 688

6 Summary

A new paste reference material was developed that consists of a mixture of two 

components, corn syrup and fine limestone mixed to form a suspension. The uniqueness of 

this material is that it has the texture of the cement paste with a fine powder in a liquid. 

The user needs to prepare the mixture according to the proportions defined in the 

certificate and mix it using ASTM C1738. The certified values, as shown in Table 8, were 

determined using an extensive experimental design and statistical analysis. Inter-laboratory 

tests on rheometers with different geometries would allow a better understanding of the 

usage of this material. In the future addition of fine and coarse aggregates could be used 

to develop SRM’s for characterizing the performance of mortar and concrete rheometers. 

7 References

1. Hackley V. A., Ferraris C.F, "The Use of Nomenclature in Dispersion Science and 

Technology", NIST Recommended Practice Guide, SP 960-3, (2001) 

http://www.nist.gov/public_affairs/practiceguides/SP960-3.pdf

2. Swindells J.F. , Hardy R.C., Cottington R.L., Precise Measurements with Bingham 

Viscometers and Cannon Master Viscometers, J. of Res. of the National Institute of 

Standards and Technology, 52 #3 (1954) 105-115

3. ISO/TR 3666:1998, “Viscosity of Water,” Technical report. (1998)

4. Ferraris C.F. , Brower L., editors, Comparison of Concrete Rheometers: 

International Tests at MB (Cleveland OH, USA) in May 2003, NISTIR 7154, 

(2004) (http://ciks.cbt.nist.gov/~ferraris/PDF/DraftRheo2003V11.4.pdf)

5. Brower L., Ferraris C.F., Comparison of Concrete Rheometers, Concrete 

International, Vol. 25 #8, (2003) 41-47
21

6. Ferraris C.F. , Brower L., editors, Comparison of concrete rheometers: 

International tests at LCPC (Nantes, France) in October 2000, NISTIR 6819, 

(2001) (http://fire.nist.gov/bfrlpubs/build01/PDF/b01074.pdf)

7. Ferraris, C.F., Li, Z., Zhang, M-H., Stutzman P. “Development of a Reference 

Material for the Calibration of Cement Paste Rheometers” Accepted for publication 

to ASTM-Advances in Civil Engineering Materials, June 2012

8. Collyer A.A., Clegg D.W., “Rheological Measurements”, Chapman & Hall, 

London, 1998

9. Ferraris C.F, Geiker M., Martys N. S. and Muzzatti N., “Parallel-plate Rheometer 

Calibration Using Oil and Lattice Boltzmann simulation”, J. of Advanced Concrete 

Technology, vol. 5 #3, October 2007, pp. 363-371

10. Ferraris C.F., Concrete Rheology: Knowledge and challenges, Key note speaker, 

2nd International RILEM Symposium on Advances in Concrete Through Science 

and Engineering (Quebec, Canada), (2006)

11. Davies G.A., Stokes J.R., “On the gap error in parallel plate rheometry that arises 

from the presence of air when zeroing the gap, J. of Rheology 49# 4 (2005) 919-

922

12. Sanchez-Perez J., Archer L.A., “Interfacial Slip Violations in Polymer Solutions: 

Role of Microscale Surface Roughness”, Langmuir 19 (2003) 3304-3312

13. R Development Core Team, R: A Language and Environment for Statistical 

Computing. R Foundation for Statistical Computing, Vienna, Austria, 2011,

http://www.R-project.org.

14. Lunn, D.J., Thomas, A., Best, N., and Spiegelhalter, D. (2000) “WinBUGS -- a 

Bayesian modelling framework: concepts, structure, and extensibility”, Statistics 

and Computing, Vol. 10, p. 325--337.

15. WinBUGS website, http://www.mrc-bsu.cam.ac.uk/bugs/winbugs/contents.shtml.
22

8 Appendix

Four appendixes are provided here.

Appendix A: Statistical analysis for Newtonian calculations

Provides all the graphs needed for the interpretation of the results and the extraction of the 

Newtonian values (Table 7).

Appendix B: Data for Newtonian calculations

Provides all the data for each test that was performed and that used for the Newtonian 

calculation for Section 5.1.2 and Appendix A. These data are generated using a Newtonian 

approach.

Appendix C: Statistical analysis for Non-Newtonian calculations

Provides all the graphs needed for the interpretation of the results and the extraction of the 

non-Newtonian values (Table 8).

Appendix D: Data for Non-Newtonian calculations

This appendix provides all the data for each test that was performed and that used for the 

Newtonian calculation for Section 5.1.3 and Appendix C. These data are generated using a

non-Newtonian approach.
A-1

Appendix A: Statistical analysis for 

Newtonian calculations

Provides all the graphs needed for the interpretation of the results and the extraction of the 

Newtonian values (Table 7).
Box Day Unit

Run 

Order Set Mix

Sample 

Age YS VS H

5 1 36 3 A-A SR-36A 1 24.5110045 5.1016855 146.8300575

5 1 36 2 A-B SR-36B 1 38.0401892 8.1029882 599.5369540

5 1 45 4 A-C SR-36C 1 25.8148958 5.8139769 117.0870575

1 2 6 6 B-A SR-40A 1 30.6676323 6.7706980 247.0875517

1 2 6 5 B-B SR-40B 1 31.9687011 6.2583598 225.3642414

1 2 23 8 B-C SR-40C 1 29.7526755 5.9528474 54.9344828

1 2 23 7 B-D SR-40D 1 33.6481204 6.2264754 239.7996437

3 3 3 10 C-A SR-44A 1 40.9097872 7.7255608 378.1561494

3 3 4 9 C-C SR-44C 1 31.5270166 6.5656445 293.6485057

3 3 4 12 C-D SR-44D 1 30.9301647 7.8978678 526.5810690

5 4 11 15 D-A SR-48A 1 40.9228014 9.0414858 543.5712989

5 4 11 13 D-B SR-48B 1 27.9637276 6.8837762 614.8989310

5 4 12 14 D-C SR-48C 1 36.5382341 9.0765700 717.7008966

5 4 12 16 D-D SR-48D 1 30.9553752 7.2002657 572.7330920

3 5 30 17 E-A SR-52A 1 38.3427266 8.9562687 706.4550345

3 5 30 20 E-B SR-52B 1 34.3079516 8.3760898 563.2652069

3 5 41 19 E-C SR-52C 1 34.8819674 7.7935623 587.3330805

3 5 41 18 E-D SR-52D 1 29.0200882 6.9085865 295.1170575

1 6 28 24 F-A SR-56A 1 27.4064311 6.0623746 189.5276552

1 6 28 22 F-B SR-56B 1 30.3046501 6.8273581 315.7559080

1 6 33 21 F-C SR-56C 1 30.2671011 7.1294649 424.8945402

1 6 33 23 F-D SR-56D 1 30.2593577 7.1223806 439.7840690

5 1 36 1 A-A SR-36A 3 24.1646169 5.9407810 388.6830280

5 1 36 4 A-B SR-36B 3 29.5791610 5.8758382 157.2732069

5 1 45 3 A-C SR-36C 3 31.5838727 8.5889335 849.5092414

5 1 45 2 A-D SR-36D 3 22.0854227 2.3488017 134.9444368

1 2 6 5 B-A SR-40A 3 20.8806913 6.4036422 348.7458966

1 2 6 8 B-B SR-40B 3 28.4042413 7.0300782 437.3904598

1 2 23 6 B-C SR-40C 3 21.2323524 5.0011123 174.5939540

1 2 23 7 B-D SR-40D 3 26.4431069 6.0527440 281.3226207

3 3 3 9 C-A SR-44A 3 30.2971650 6.5695726 316.7324138

3 3 4 12 C-C SR-44C 3 30.3013303 7.4190595 387.1662931

3 3 4 10 C-D SR-44D 3 25.7562635 7.3818142 384.6182529

5 4 11 16 D-A SR-48A 3 31.0566899 7.4412754 556.6608161

5 4 11 15 D-B SR-48B 3 22.3494888 5.6741953 264.2272414

5 4 12 13 D-C SR-48C 3 26.6234349 6.4669795 323.0796897

5 4 12 14 D-D SR-48D 3 22.2976615 5.4819550 390.7078161

3 5 30 17 E-A SR-52A 3 25.8318625 5.9426656 194.8256552

3 5 30 19 E-B SR-52B 3 27.5853633 7.5549883 443.8862299

3 5 41 20 E-C SR-52C 3 26.9038812 6.6001826 324.9805862

3 5 41 18 E-D SR-52D 3 23.2954879 6.7505388 226.9700690

1 6 28 23 F-A SR-56A 3 25.9154553 6.9236756 275.1048391

1 6 28 21 F-B SR-56B 3 27.2727937 6.8631364 372.4610000

1 6 33 22 F-C SR-56C 3 27.1549715 7.1699433 546.3303563

1 6 33 24 F-D SR-56D 3 27.7331164 7.1055978 427.0552299

5 1 36 4 A-A SR-36A 7 19.9051407 4.7455120 388.6830280

5 1 36 1 A-B SR-36B 7 27.4822066 6.4180012 304.4382759

5 1 45 2 A-C SR-36C 7 22.6220785 5.8523519 272.0207701

5 1 45 3 A-D SR-36D 7 22.0136765 2.1003748 124.5567241

1 2 6 6 B-A SR-40A 7 22.1736762 7.0879147 348.7458966

1 2 6 5 B-B SR-40B 7 26.8448403 6.4325844 214.5191034

1 2 23 8 B-C SR-40C 7 28.8543050 8.3980825 601.1702989

1 2 23 7 B-D SR-40D 7 30.5505157 7.5460083 455.6541207

3 3 3 9 C-A SR-44A 7 33.3086333 8.2172872 316.7324138

3 3 4 11 C-C SR-44C 7 33.2698608 9.4654822 786.6936897

3 3 4 10 C-D SR-44D 7 26.5053460 8.2890339 657.7171264

5 4 11 14 D-A SR-48A 7 28.7693956 7.1507935 556.6608161

5 4 11 15 D-B SR-48B 7 20.2730109 5.2310988 128.2817126

5 4 12 16 D-C SR-48C 7 27.9085225 8.3296071 557.1381379

5 4 12 13 D-D SR-48D 7 22.2157613 6.1402875 380.5573678

3 5 30 20 E-A SR-52A 7 25.6899137 5.8753332 194.8256552

3 5 30 19 E-B SR-52B 7 26.3105599 7.4751330 415.9729425

3 5 41 18 E-C SR-52C 7 26.1451842 7.3548969 626.8820690

3 5 41 17 E-D SR-52D 7 27.0854980 9.5732202 724.8317011

1 6 28 21 F-A SR-56A 7 25.6876456 8.6560791 275.1048391

1 6 28 22 F-B SR-56B 7 24.5331561 6.5800304 393.8614483

1 6 33 23 F-C SR-56C 7 22.8786002 5.4678895 131.3401149

1 6 33 24 F-D SR-56D 7 28.6917284 10.0329962 1034.0398391

Table 1: Data Used for Analysis of Rheological Quantities in SRM 2492

A-2
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VS versus Run Order

A-17
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VS versus Sample Age

A-18
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2345

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VS versus Box

Sample Age = 1 day

A-19
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123456

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VS versus Day

Sample Age = 1 day

A-20
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A-21
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Sample Quantiles

Normal Probability Plot of VS 

Sample Age = 1 day

A-22
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2345

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VS versus Box

Sample Age = 3 day

A-23
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123456

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Sample Age = 3 day

A-24
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A-25
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Sample Quantiles

Normal Probability Plot of VS 

Sample Age = 3 day

A-26
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VS versus Box

Sample Age = 7 day

A-27
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A-28
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A-29
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Sample Quantiles

Normal Probability Plot of VS 

Sample Age = 7 day

A-30
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A-31
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H versus Sample Age

A-32
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A-33
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A-34
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A-35
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Sample Quantiles

Normal Probability Plot of H 

Sample Age = 1 day

A-36
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A-37
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A-38
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A-39
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Sample Quantiles

Normal Probability Plot of H 

Sample Age = 3 day

A-40
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A-41
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A-42
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A-43
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Sample Quantiles

Normal Probability Plot of H 

Sample Age = 7 day

A-44
WinBUGS Implementation of Hierarchical Model for Certification of

Rheological Quantities in SRM 2492

model

{

mu~dunif(-1000,1000)

sigma.day~dunif(0,1000)

sigma.btl~dunif(0,1000)

sigma.rme~dunif(0,1000)

tau.day <- 1/(sigma.day*sigma.day)

tau.btl <- 1/(sigma.btl*sigma.btl)

tau.rme <- 1/(sigma.rme*sigma.rme)

for(i in 1:6)

{

mu.day[i]~dnorm(mu,tau.day)

}

for(i in 1:12)

{

mu.btl[i]~dnorm(mu.day[day[i]],tau.btl)

}

for(i in 1:n)

{

y[i]~dnorm(mu.btl[btl[i]],tau.rme)

pred[i]~dnorm(mu.btl[btl[i]],tau.rme)

res[i] <- y[i]-pred[i]

}

mu.nu~dnorm(mu,tau.btl)

}

A-45
−15 −10 −5 0 5 10 15

Mix

Residual

Residual Plot for Response YS at Age 1 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

A-46
−10 −5 0 5 10

Mix

Residual

Residual Plot for Response YS at Age 3 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23

A-47
−10 −5 0 5 10

Mix

Residual

Residual Plot for Response YS at Age 7 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23

A-48
−4 −2

0

2

4

Mix

Residual

Residual Plot for Response VS at Age 1 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

A-49
−6 −4 −2 0 2 4

Mix

Residual

Residual Plot for Response VS at Age 3 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23

A-50
−6 −4 −2 0 2 4 6

Mix

Residual

Residual Plot for Response VS at Age 7 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23

A-51
−600 −400 −200 0 200 400 600

Mix

Residual

Residual Plot for Response H at Age 1 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

A-52
−500

0 500

Mix

Residual

Residual Plot for Response H at Age 3 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23

A-53
−500

0 500 1000

Mix

Residual

Residual Plot for Response H at Age 7 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23

A-54
25 30 35 40

0.00 0.05 0.10 0.15 0.20

YS

Probability Density

Distribution of YS Values at Age 1 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for YS

26.57 32.25 38.15

A-55
20 22 24 26 28 30 32

0.00 0.05 0.10 0.15 0.20 0.25 0.30

YS

Probability Density

Distribution of YS Values at Age 3 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for YS

22.98 26.35 29.76

A-56
20 25 30 35

0.00 0.05 0.10 0.15 0.20

YS

Probability Density

Distribution of YS Values at Age 7 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for YS

21.35 26.21 31.24

A-57
5 6 7 8 9 10

0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7

VS

Probability Density

Distribution of VS Values at Age 1 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for VS

5.636 7.154 8.648

A-58
4 5 6 7 8 9

0.0 0.2 0.4 0.6 0.8

VS

Probability Density

Distribution of VS Values at Age 3 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for VS

5.135 6.472 7.815

A-59
4 6 8 10 12

0.0 0.1 0.2 0.3 0.4

VS

Probability Density

Distribution of VS Values at Age 7 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for VS

4.694 7.101 9.527

A-60
0 200 400 600 800

0.0000 0.0005 0.0010 0.0015 0.0020 0.0025 0.0030 0.0035

H

Probability Density

Distribution of H Values at Age 1 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for H

98.19 394.3 689.2

A-61
100 200 300 400 500 600 700

0.000 0.001 0.002 0.003 0.004 0.005 0.006

H

Probability Density

Distribution of H Values at Age 3 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for H

184.6 357.5 526.4

A-62
−200 0 200 400 600 800 1000

0.0000 0.0005 0.0010 0.0015 0.0020 0.0025 0.0030 0.0035

H

Probability Density

Distribution of H Values at Age 7 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for H

111.1 431.6 755.5

A-63
Response Age Mean Value

Standard 

Uncertainty

Degrees of 

Freedom

Coverage 

Factor

Expanded 

Uncertainty

Lower 

Bound

Upper 

Bound

y u (y ) ν k U

YS 1 32.2 1.999 3.7 2.8675 5.7 26.5 38.0

YS 3 26.4 1.242 4.2 2.7251 3.4 23.0 29.7

YS 7 26.2 1.753 4.0 2.7764 4.9 21.3 31.1

VS 1 7.2 0.537 4.0 2.7764 1.5 5.7 8.6

VS 3 6.5 0.481 4.0 2.7764 1.3 5.1 7.8

VS 7 7.1 0.885 4.1 2.7499 2.4 4.7 9.5

H 1 394 109.6 4.4 2.6905 295 99 689

H 3 358 61.5 3.9 2.8047 173 185 530

H 7 432 110.5 3.6 2.9024 321 111 752

Table 2: Certification Results for SRM 2492

A-64
B - 1

Appendix B: Data for Newtonian 

calculations

Legend of the tables

YS = yield stress

VS = plastic viscosity

SR = Shear Rate

SS = Shear Stress

R2 = r

2 calculated using a Pearson function to determine the linearity of the data

Provides all the data for each test that was performed and that used for the Newtonian 

calculation for Section 5.1.2 and Appendix A. These data are generated using a Newtonian 

approach.
B - 2

Set A1: CS-BX5 – BL45- L2 – Mixing Day – NIST code (folder SR 37-SR-36A)

SR-36A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 20.07 0.21 25.76 0.21 23.76 0.23 23.20

2.65 45.03 2.65 45.59 2.65 41.52 2.65 44.05

5.09 59.78 5.09 59.96 5.08 54.45 5.09 58.06

7.52 71.88 7.52 72.81 7.59 67.29 7.54 70.66

10.00 84.16 10.00 85.54 10.00 79.47 10.00 83.06

12.41 96.6 12.41 98.46 12.41 91.32 12.41 95.46

14.90 109.2 14.90 111 14.90 102.9 14.90 107.70

17.31 122.3 17.31 123.9 17.38 114.4 17.33 120.20

19.79 134.4 19.79 136 19.79 125.9 19.79 132.10

22.21 145.9 22.21 148.2 22.21 137.6 22.21 143.90

24.69 157.6 24.69 160.1 24.69 148.6 24.69 155.43

27.10 169.8 27.10 172 27.10 158.4 27.10 166.73

29.59 181 29.59 183.5 29.59 169.3 29.59 177.93

32.00 191.4 32.07 194.7 32.00 179.3 32.02 188.47

34.48 200.7 34.48 204.3 34.48 190.5 34.48 198.50

34.48 200.4 34.48 204.3 34.48 188.8 34.48 197.83

32.69 191 32.69 194.9 32.69 180.5 32.69 188.80

30.83 182.4 30.90 184.7 30.90 173.7 30.87 180.27

29.10 172.9 29.03 175.5 29.03 165.3 29.06 171.23

27.24 166.4 27.24 167.4 27.24 157.2 27.24 163.67

25.45 157.1 25.45 157.6 25.45 149.3 25.45 154.67

23.66 149 23.66 149.3 23.66 140.7 23.66 146.33

21.86 138.5 21.86 139.6 21.86 132.6 21.86 136.90

20.07 130.4 20.07 130.5 20.07 124.4 20.07 128.43

18.21 121 18.21 122.2 18.21 115 18.21 119.40

16.41 112.1 16.41 112.9 16.41 106.5 16.41 110.50

14.62 103 14.62 102.8 14.62 98.58 14.62 101.46

12.83 93.07 12.83 93.5 12.83 89.49 12.83 92.02

11.03 85.19 11.03 84.06 11.03 80.81 11.03 83.35

9.24 74.37 9.24 74.13 9.24 71.52 9.24 73.34

7.45 65.2 7.45 64.17 7.45 62.17 7.45 63.85

5.61 54.09 5.61 54.32 5.62 51.84 5.61 53.42

3.80 43.57 3.81 43.61 3.81 41.76 3.80 42.98

2.00 32.8 2.01 32.37 2.01 31.13 2.01 32.10

0.21 19.49 0.19 19.01 0.21 18.3 0.20 18.93

Average Stdev

YS 25.1 24.0 24.4 24.5 0.6

VS 5.2 5.3 4.9 5.1 0.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 163 219 58 147 81
B - 3

Set A1: CS-BX5 – BL12- L2 – Mixing Day – NIST code (folder SR 37-SR-36B)

SR-36B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 40.11 0.20 34.89 0.19 43.47 0.20 39.49

2.66 80.21 2.65 56.8 2.64 78.06 2.65 71.69

5.09 110.3 5.10 73.48 5.09 105.7 5.09 96.49

7.52 140.7 7.52 89.41 7.52 137.6 7.52 122.57

10.00 164.4 10.00 104.9 10.00 162.5 10.00 143.93

12.41 183.4 12.41 120.7 12.41 186.1 12.41 163.40

14.90 204 14.90 137.9 14.90 209.2 14.90 183.70

17.31 223.4 17.31 153 17.31 230.1 17.31 202.17

19.79 244 19.79 169.2 19.79 251.6 19.79 221.60

22.21 262.2 22.21 181.8 22.21 270 22.21 238.00

24.69 280 24.69 196.4 24.69 288 24.69 254.80

27.10 298 27.10 213.9 27.10 306.9 27.10 272.93

29.59 312.7 29.59 226.1 29.59 321.4 29.59 286.73

32.00 330.3 32.00 241.4 32.00 338.9 32.00 303.53

34.48 342.8 34.48 250.2 34.48 350.6 34.48 314.53

34.48 342.4 34.48 253.1 34.48 350.2 34.48 315.23

32.69 326.8 32.69 242.1 32.69 333.3 32.69 300.73

30.83 309.2 30.83 227.2 30.90 314.5 30.85 283.63

29.03 295 29.03 216.7 29.03 298.9 29.03 270.20

27.24 279.2 27.24 209.1 27.24 285.5 27.24 257.93

25.45 264.4 25.45 196.2 25.45 269 25.45 243.20

23.66 249.5 23.66 188.1 23.66 255.5 23.66 231.03

21.86 234.9 21.86 174.6 21.86 238.5 21.86 216.00

20.00 219.4 20.07 164.4 20.07 223.5 20.05 202.43

18.28 206 18.21 155.6 18.28 209.3 18.25 190.30

16.41 190.3 16.41 144.4 16.41 193.6 16.41 176.10

14.62 173.1 14.62 131 14.62 176.5 14.62 160.20

12.83 157.9 12.83 119.3 12.83 160.1 12.83 145.77

11.03 140.9 11.03 108.8 11.03 144.6 11.03 131.43

9.24 124.8 9.24 95.39 9.24 126.7 9.24 115.63

7.45 107.5 7.45 83.77 7.45 109.9 7.45 100.39

5.61 90.54 5.61 70.53 5.61 92.03 5.61 84.37

3.81 72.07 3.81 56.87 3.81 73.12 3.81 67.35

1.99 52.08 2.00 43.06 2.00 53.28 2.00 49.47

0.19 30.37 0.20 26.53 0.20 30.9 0.20 29.27

Average Stdev

YS 39.6 34.2 40.3 38.0 3.3

VS 8.9 6.4 9.0 8.1 1.5

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 753 269 777 600 287

0

50

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250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 4

Set A1: CS-BX5 – BL12- L1 – Mixing Day – NIST code (folder SR 37-SR-36C)

SR-36C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 30.05 0.20 31.97 0.19 22.11 0.20 28.04

2.64 48.71 2.65 54.09 2.66 41.36 2.65 48.05

5.10 64.62 5.09 73.06 5.09 55.64 5.09 64.44

7.52 79.09 7.52 89.66 7.59 69.47 7.54 79.41

10.00 93.23 10.00 104 10.00 83.92 10.00 93.72

12.41 107.8 12.41 118.4 12.41 98.07 12.41 108.09

14.90 122.5 14.90 132.8 14.90 111.8 14.90 122.37

17.31 136.5 17.38 147.7 17.31 126.2 17.33 136.80

19.79 150.7 19.79 161.2 19.79 139.5 19.79 150.47

22.21 164.7 22.21 176.1 22.21 153.9 22.21 164.90

24.69 178.2 24.69 189.3 24.69 166.9 24.69 178.13

27.17 190.3 27.10 199.6 27.10 177.9 27.13 189.27

29.59 203.1 29.59 212.1 29.59 191.5 29.59 202.23

32.00 214.6 32.00 221.2 32.00 202.7 32.00 212.83

34.48 227.2 34.48 234.9 34.48 216.7 34.48 226.27

34.48 224.5 34.48 229 34.48 213.9 34.48 222.47

32.69 214.1 32.69 218 32.69 204.3 32.69 212.13

30.83 205.8 30.90 210.8 30.90 196.7 30.87 204.43

29.03 195.8 29.03 199.6 29.03 187.3 29.03 194.23

27.24 185.4 27.24 189.4 27.24 176.2 27.24 183.67

25.45 176.1 25.45 180.2 25.45 168 25.45 174.77

23.66 165.7 23.66 169.1 23.66 157.1 23.66 163.97

21.86 155.7 21.86 159.2 21.86 148.7 21.86 154.53

20.07 146.4 20.07 149.5 20.07 138.6 20.07 144.83

18.21 135.2 18.21 136.8 18.21 127.7 18.21 133.23

16.41 125 16.41 126.4 16.41 117.8 16.41 123.07

14.62 115.4 14.62 118.1 14.62 108.6 14.62 114.03

12.83 104.2 12.83 106.5 12.83 98.11 12.83 102.94

11.03 94.4 11.03 96.48 11.03 87.4 11.03 92.76

9.24 82.73 9.24 84.77 9.24 77.07 9.24 81.52

7.45 72.06 7.45 74.02 7.45 65.93 7.45 70.67

5.61 59.7 5.61 60.99 5.61 54.48 5.61 58.39

3.82 47.75 3.80 49.04 3.81 42.95 3.81 46.58

2.01 35.23 2.01 36.62 2.02 30.59 2.01 34.15

0.20 21.11 0.19 22.53 0.20 16.71 0.20 20.12

Average Stdev

YS 26.9 27.9 22.6 25.8 2.9

VS 5.8 5.9 5.7 5.8 0.1

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 115 230 6 117 112

0

50

100

150

200

250

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 5

Set A1: CS-BX5 – BL45- L1 – Mixing Day – NIST code (folder SR 37-SR-36D)

SR-36D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.21 2.532 0.19 2.485 0.20 2.495 0.20 2.50

2.66 4.245 2.63 4.349 2.64 4.068 2.64 4.22

5.10 5.545 5.10 5.492 5.08 5.429 5.09 5.49

7.52 6.39 7.52 6.471 7.52 6.239 7.52 6.37

10.00 7.345 10.00 7.419 10.00 7.389 10.00 7.38

12.41 8.319 12.41 8.355 12.41 8.404 12.41 8.36

14.90 9.352 14.90 9.551 14.90 9.414 14.90 9.44

17.31 10.15 17.31 10.52 17.38 10.58 17.33 10.42

19.79 11.29 19.79 11.51 19.79 11.58 19.79 11.46

22.21 12.11 22.28 12.35 22.21 12.52 22.23 12.33

24.69 13.01 24.69 13.35 24.69 13.51 24.69 13.29

27.10 14.09 27.17 14.44 27.10 14.63 27.13 14.39

29.59 14.88 29.59 15.25 29.59 15.44 29.59 15.19

32.00 15.93 32.00 16.4 32.00 16.61 32.00 16.31

34.48 16.76 34.48 17.35 34.48 17.42 34.48 17.18

34.48 16.77 34.48 17.37 34.48 17.56 34.48 17.23

32.69 16.08 32.69 16.7 32.69 16.87 32.69 16.55

30.90 15.5 30.83 16.06 30.90 16.12 30.87 15.89

29.10 14.81 29.03 15.42 29.03 15.38 29.06 15.20

27.24 14.26 27.24 14.48 27.24 14.7 27.24 14.48

25.45 13.48 25.45 13.99 25.45 14.01 25.45 13.83

23.66 12.86 23.66 13.09 23.66 13.28 23.66 13.08

21.86 12.16 21.86 12.65 21.86 12.59 21.86 12.47

20.07 11.46 20.07 12 20.07 11.9 20.07 11.79

18.28 10.6 18.28 11.2 18.21 11.22 18.25 11.01

16.41 9.889 16.41 10.47 16.41 10.54 16.41 10.30

14.62 9.399 14.62 9.842 14.62 9.725 14.62 9.66

12.83 8.627 12.83 8.921 12.83 8.806 12.83 8.78

11.03 7.837 11.03 8.232 11.03 8.206 11.03 8.09

9.24 7.144 9.24 7.369 9.24 7.265 9.24 7.26

7.45 6.311 7.45 6.717 7.45 6.533 7.45 6.52

5.61 5.396 5.61 5.752 5.62 5.528 5.61 5.56

3.81 4.606 3.81 4.821 3.80 4.509 3.81 4.65

2.01 3.746 2.01 3.668 2.01 3.688 2.01 3.70

0.20 2.316 0.20 2.311 0.20 2.268 0.20 2.30

Average Stdev

YS 3.1 3.3 3.1 3.2 0.1

VS 0.4 0.4 0.4 0.4 0.0

R2 1.00 0.99 1.00 1.0 0.0

Hysteresis 1 6 0 2 3

Comment: Problem with mixer = material not mixed properly - a lot of sedimentation

0

2

4

6

8

10

12

14

16

18

20

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 6

Set A3: CS-BX5 – BL45- L2 – 3 day – NIST code (folder SR 38-SR-36A)

SR-36A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.22 22.31 0.22 27.19 0.22 20.25 0.22 23.25

2.86 51.26 2.86 63.29 2.86 36.73 2.86 50.43

5.53 70.43 5.51 90.65 5.53 50.01 5.52 70.36

8.22 91.68 8.22 123.3 8.15 62.63 8.20 92.54

10.84 111 10.84 144.2 10.84 74.39 10.84 109.86

13.46 128.6 13.46 159.9 13.46 86.27 13.46 124.92

16.15 147.5 16.15 174.9 16.15 98.42 16.15 140.27

18.77 164.1 18.77 191.5 18.77 110.4 18.77 155.33

21.46 181.1 21.46 205.9 21.46 122.2 21.46 169.73

24.07 195.8 24.07 223.1 24.07 133.8 24.07 184.23

26.77 210.9 26.77 237.8 26.77 145 26.77 197.90

29.38 226 29.38 248.8 29.46 156.5 29.41 210.43

32.07 239.2 32.07 264.2 32.07 166.9 32.07 223.43

34.69 252 34.69 273.6 34.69 177.6 34.69 234.40

37.38 263.6 37.38 289.4 37.38 188.1 37.38 247.03

37.38 262.3 37.38 281.3 37.38 187.4 37.38 243.67

35.44 249.7 35.44 267 35.44 178.7 35.44 231.80

33.50 236.5 33.50 256.9 33.42 170.8 33.47 221.40

31.48 224.8 31.48 243 31.48 162.4 31.48 210.07

29.53 213.2 29.53 231.2 29.53 153.7 29.53 199.37

27.59 201 27.59 218 27.59 145.9 27.59 188.30

25.64 189.6 25.64 205.2 25.64 137.1 25.64 177.30

23.70 177.6 23.70 191.5 23.70 128.8 23.70 165.97

21.76 165.4 21.76 179.1 21.76 120.6 21.76 155.03

19.74 154.2 19.74 163.9 19.81 111.7 19.76 143.27

17.79 142 17.79 151.1 17.79 103.1 17.79 132.07

15.85 129.2 15.85 139.4 15.85 94.54 15.85 121.05

13.91 117.3 13.91 125.3 13.91 85.72 13.91 109.44

11.96 104.3 11.96 112.8 11.96 77.03 11.96 98.04

10.02 91.56 10.02 98.08 10.02 67.71 10.02 85.78

8.07 78.25 8.07 84.2 8.07 58.39 8.07 73.61

6.09 64.93 6.08 68.47 6.08 48.83 6.08 60.74

4.12 50.96 4.13 53.4 4.14 39.01 4.13 47.79

2.18 35.94 2.19 37.92 2.18 28.51 2.19 34.12

0.22 18.84 0.22 19.25 0.21 16.19 0.22 18.09

Average Stdev

YS 25.3 26.2 21.0 24.2 2.8

VS 6.4 6.9 4.5 5.9 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 414 670 83 389 294

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 7

Set A3: CS-BX5 – BL12- L2 – 3 day – NIST code (folder SR 38-SR-36B)

SR-36B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 30.46 0.20 28.89 0.20 37.25 0.20 32.20

2.66 50.8 2.63 48.38 2.65 79.13 2.65 59.44

5.09 66.68 5.08 63.77 5.08 107.9 5.09 79.45

7.59 82.17 7.52 78.03 7.59 142.1 7.56 100.77

10.00 96.75 10.00 92.33 10.00 167.2 10.00 118.76

12.41 111.1 12.41 107.1 12.41 191.1 12.41 136.43

14.90 125.8 14.90 121.5 14.90 216.2 14.90 154.50

17.31 140.7 17.31 135.5 17.38 235.6 17.33 170.60

19.79 155.3 19.79 149.5 19.79 258.4 19.79 187.73

22.21 168.6 22.21 163.2 22.28 271.6 22.23 201.13

24.69 182.1 24.69 176.4 24.69 288.5 24.69 215.67

27.10 196.7 27.10 189.7 27.10 311.8 27.10 232.73

29.59 209.4 29.59 202.5 29.59 323.3 29.59 245.07

32.00 222.4 32.00 214.7 32.07 343 32.02 260.03

34.48 232.6 34.48 226.2 34.48 348.1 34.48 268.97

34.48 233.5 34.48 225.7 34.48 353.7 34.48 270.97

32.69 222.8 32.69 216 32.69 335.5 32.69 258.10

30.90 210.8 30.90 206.2 30.90 308.8 30.90 241.93

29.03 200.7 29.03 196.6 29.03 293.7 29.03 230.33

27.24 192.2 27.24 186.6 27.24 278.6 27.24 219.13

25.45 180.6 25.45 177.2 25.45 260.2 25.45 206.00

23.66 171.9 23.66 167.2 23.66 197 23.66 178.70

21.86 160.5 21.86 157.8 21.86 230 21.86 182.77

20.07 150.1 20.07 147.7 20.07 212.6 20.07 170.13

18.21 141.3 18.21 137.7 18.21 201.9 18.21 160.30

16.41 130.8 16.41 127.6 16.41 185.5 16.41 147.97

14.62 119 14.62 117.3 14.62 165 14.62 133.77

12.83 108.7 12.83 106.6 12.83 150.7 12.83 122.00

11.03 97.86 11.03 95.85 11.03 132.6 11.03 108.77

9.24 86.61 9.24 85.11 9.24 117.3 9.24 96.34

7.45 75.03 7.45 74.04 7.45 99.27 7.45 82.78

5.61 64.12 5.61 62.48 5.61 84.06 5.61 70.22

3.81 51.58 3.79 50.29 3.79 65.57 3.80 55.81

2.02 38.55 2.02 37.45 2.01 45.87 2.02 40.62

0.20 23.74 0.20 22.92 0.20 24.7 0.20 23.79

Average Stdev

YS 29.7 29.5 29.5 29.6 0.1

VS 6.0 5.8 9.1 6.9 1.9

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 214 100 1439 584 742

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 8

Set A3: CS-BX5 – BL12- L1 – 3 day – NIST code (folder SR 38-SR-36C)

SR-36C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 42.83 0.16 37.74 0.20 28.2 0.19 36.26

2.65 88.37 2.65 75.6 2.65 50.25 2.65 71.41

5.09 129.2 5.10 111.9 5.09 67.3 5.09 102.80

7.59 167.8 7.52 146.8 7.52 83.41 7.54 132.67

10.00 196 10.00 173.2 10.00 99.62 10.00 156.27

12.41 221.2 12.41 196.8 12.41 115.5 12.41 177.83

14.90 244.2 14.90 218.8 14.90 131 14.90 198.00

17.31 267 17.31 239.6 17.31 146.8 17.31 217.80

19.79 288.3 19.79 258.9 19.79 161.7 19.79 236.30

22.21 311.5 22.28 274.7 22.21 177.3 22.23 254.50

24.69 331.7 24.69 290.6 24.69 191.8 24.69 271.37

27.10 348.2 27.10 309.3 27.10 204.9 27.10 287.47

29.59 367.7 29.59 322.7 29.59 219.1 29.59 303.17

32.00 383.6 32.00 337.3 32.00 231.8 32.00 317.57

34.48 404.1 34.48 341.1 34.48 245.6 34.48 330.27

34.48 395.8 34.48 344.4 34.48 243.4 34.48 327.87

32.69 375.9 32.69 326.6 32.69 232.2 32.69 311.57

30.90 359.2 30.90 298.2 30.83 221.8 30.87 293.07

29.03 340.5 29.03 285.1 29.10 211.1 29.06 278.90

27.24 319.6 27.24 271.2 27.24 199.5 27.24 263.43

25.45 303.6 25.45 252.7 25.45 189.4 25.45 248.57

23.66 283.8 23.66 239.3 23.66 178 23.66 233.70

21.86 267 21.86 226 21.86 168.1 21.86 220.37

20.07 249.2 20.07 209.1 20.00 156.9 20.05 205.07

18.21 229 18.28 198.3 18.21 146 18.23 191.10

16.41 210.8 16.41 181.9 16.41 134.6 16.41 175.77

14.62 193.9 14.62 164.9 14.62 123.6 14.62 160.80

12.83 174.4 12.83 150.5 12.83 112 12.83 145.63

11.03 156.1 11.03 131 11.03 100.3 11.03 129.13

9.24 136.2 9.24 117.6 9.24 88.46 9.24 114.09

7.45 116.9 7.38 99.27 7.45 76.29 7.43 97.49

5.61 95.71 5.61 83.23 5.59 63.67 5.60 80.87

3.81 74.34 3.81 65.26 3.81 50.66 3.81 63.42

2.01 52.12 2.00 44.91 1.99 36.78 2.00 44.60

0.19 27.41 0.20 24.58 0.20 21.85 0.20 24.61

Average Stdev

YS 35.7 31.3 27.8 31.6 4.0

VS 10.5 8.9 6.3 8.6 2.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 963 1451 134 850 666

0

50

100

150

200

250

300

350

400

450

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 9

Set A3: CS-BX5 – BL45- L1 – 3 day – NIST code (folder SR 38-SR-36D)

SR-36D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 23.51 0.19 18.73 0.20 17.93 0.20 20.06

2.64 39.11 2.64 30.47 2.63 30.02 2.64 33.20

5.10 47.73 5.10 37.6 5.09 35.54 5.10 40.29

7.52 54.05 7.59 44.81 7.52 40.39 7.54 46.42

10.00 60.33 10.00 51.53 10.00 45.04 10.00 52.30

12.41 65.67 12.41 58.54 12.48 49.41 12.44 57.87

14.90 70.99 14.90 65.72 14.90 53.43 14.90 63.38

17.38 76.12 17.31 72.17 17.31 57.6 17.33 68.63

19.79 81.13 19.79 78.46 19.79 61.5 19.79 73.70

22.21 85.39 22.21 84.24 22.21 65.44 22.21 78.36

24.69 90.19 24.69 89.85 24.69 69.16 24.69 83.07

27.10 95.99 27.10 95.49 27.10 72.76 27.10 88.08

29.59 100.2 29.59 100.2 29.59 76.96 29.59 92.45

32.00 105.9 32.00 105.5 32.00 80.98 32.00 97.46

34.48 109.9 34.48 109.7 34.48 85.01 34.48 101.54

34.48 110.1 34.48 109.8 34.48 84.81 34.48 101.57

32.69 105.6 32.69 105.2 32.69 81.82 32.69 97.54

30.90 101.1 30.90 99.94 30.90 78.62 30.90 93.22

29.03 97.11 29.10 95.69 29.03 75.49 29.06 89.43

27.24 91.53 27.24 92.05 27.24 72.71 27.24 85.43

25.45 88.47 25.45 87.39 25.45 69.45 25.45 81.77

23.66 83.17 23.66 83.8 23.66 66.54 23.66 77.84

21.86 80.47 21.86 79.11 21.86 63.03 21.86 74.20

20.07 75.92 20.00 74.92 20.07 59.92 20.05 70.25

18.28 71.5 18.21 71.58 18.21 57.03 18.23 66.70

16.41 67.05 16.41 67.3 16.41 53.78 16.41 62.71

14.62 63.03 14.62 61.86 14.62 49.96 14.62 58.28

12.83 58.42 12.83 57.5 12.83 46.36 12.83 54.09

11.03 53.2 11.03 52.74 11.03 42.99 11.03 49.64

9.24 48.68 9.24 47.98 9.24 39.05 9.24 45.24

7.45 43.71 7.45 43.05 7.45 35.37 7.45 40.71

5.62 30.47 5.59 38.31 5.61 31.49 5.61 33.42

3.80 32.69 3.80 32.76 3.79 27.02 3.80 30.82

2.01 26.38 1.99 26.86 2.01 22.41 2.00 25.22

0.20 19.01 0.20 19.42 0.20 16.16 0.20 18.20

Average Stdev

YS 22.4 23.6 20.3 22.1 1.7

VS 2.6 2.5 1.9 2.3 0.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 238 86 80 135 89

Comment: Problem with mixer = material not mixed properly - a lot of sedimentation

0

20

40

60

80

100

120

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 10

Set A7: CS-BX5 – BL45- L2 – 7 day – NIST code (folder SR 39-SR-36A)

SR-36A

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.21 19.03 0.20 19.05 0.20 19.23 0.20 19.10

2.65 35.97 2.63 35.64 2.63 36.01 2.64 35.87

5.10 49.66 5.10 49 5.08 48.8 5.09 49.15

7.52 62.15 7.52 61.22 7.52 60.65 7.52 61.34

10.00 74.61 10.00 72.81 10.00 72.08 10.00 73.17

12.41 86.5 12.41 84.48 12.41 83.58 12.41 84.85

14.90 98.09 14.90 96.85 14.90 94.82 14.90 96.59

17.31 109.7 17.31 108.4 17.38 106.6 17.33 108.23

19.79 121.4 19.79 120.1 19.79 117.3 19.79 119.60

22.21 132.9 22.21 129.2 22.21 128.6 22.21 130.23

24.69 144.1 24.69 139.5 24.69 139 24.69 140.87

27.17 155.1 27.10 152.5 27.10 148.3 27.13 151.97

29.59 166.1 29.59 160.9 29.59 159 29.59 162.00

32.00 176.6 32.00 172.5 32.00 168 32.00 172.37

34.48 187.2 34.48 178.6 34.48 178.4 34.48 181.40

34.48 187 34.48 181.8 34.48 176.6 34.48 181.80

32.69 178.7 32.69 173.5 32.69 168.3 32.69 173.50

30.83 170.4 30.83 161.5 30.90 160.9 30.85 164.27

29.03 162.3 29.03 154.7 29.03 152.7 29.03 156.57

27.24 154.4 27.24 146.5 27.24 145.2 27.24 148.70

25.45 145.8 25.45 137.9 25.45 137.4 25.45 140.37

23.66 137.9 23.66 130.7 23.66 129.4 23.66 132.67

21.86 129.3 21.86 123.5 21.86 121.2 21.86 124.67

20.07 120.8 20.07 114.7 20.07 113.3 20.07 116.27

18.28 112.4 18.28 108.6 18.21 104.5 18.25 108.50

16.41 103.7 16.41 100 16.41 96.57 16.41 100.09

14.62 94.82 14.62 90.77 14.62 88.75 14.62 91.45

12.83 86.14 12.83 83.23 12.83 79.8 12.83 83.06

11.03 76.99 11.03 72.76 11.03 72.02 11.03 73.92

9.24 68 9.24 65.6 9.24 62.99 9.24 65.53

7.38 58.22 7.45 55.42 7.45 54.62 7.43 56.09

5.61 48.79 5.61 47.04 5.61 45.16 5.61 47.00

3.82 38.96 3.83 37.37 3.80 35.74 3.82 37.36

2.01 28.14 2.01 26.28 2.02 26.12 2.01 26.85

0.20 15.85 0.20 14.81 0.20 14.84 0.20 15.17

Average Stdev

YS 21.0 19.8 18.9 19.9 1.1

VS 4.9 4.7 4.6 4.7 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 66 261 107 145 103

0

20

40

60

80

100

120

140

160

180

200

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 11

Set A7: CS-BX5 – BL12- L2 – 7 day – NIST code (folder SR 39-SR-36B)

SR-36B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.20 25.25 0.20 27.26 0.20 33.14 0.20 28.55

2.64 46.14 2.65 47.13 2.65 62.46 2.65 51.91

5.10 62.9 5.10 62.72 5.09 87.59 5.09 71.07

7.59 79.28 7.52 77.4 7.52 112.3 7.54 89.66

10.00 95.53 10.00 91.28 10.00 133.1 10.00 106.64

12.41 110.5 12.41 105 12.41 152.1 12.41 122.53

14.90 125 14.90 119.6 14.90 171.1 14.90 138.57

17.31 138.8 17.38 133.4 17.38 189.3 17.36 153.83

19.79 151.8 19.79 147.2 19.79 206.3 19.79 168.43

22.21 164.6 22.21 158.9 22.21 222.9 22.21 182.13

24.69 176.8 24.69 171.6 24.69 238.9 24.69 195.77

27.10 187.9 27.10 186.7 27.10 254.2 27.10 209.60

29.59 199.4 29.59 198.8 29.59 269.1 29.59 222.43

32.00 211 32.07 211.7 32.07 283 32.05 235.23

34.48 224 34.48 220 34.48 297.1 34.48 247.03

34.48 222.2 34.48 222.6 34.48 293 34.48 245.93

32.69 212.4 32.69 212.4 32.62 279.1 32.67 234.63

30.90 202 30.90 199 30.90 267 30.90 222.67

29.03 193.1 29.03 189.5 29.03 253.4 29.03 212.00

27.24 181.1 27.24 181.6 27.24 240.1 27.24 200.93

25.45 172.3 20.34 170.3 25.45 227.3 23.75 189.97

23.66 161.7 23.66 162.4 23.66 213.9 23.66 179.33

21.86 153.4 21.86 151.3 21.86 200.9 21.86 168.53

20.07 142.7 20.07 141.4 20.07 187.7 20.07 157.27

18.28 133.1 18.21 133.9 18.21 173.5 18.23 146.83

16.41 123 16.41 123.9 16.41 160.1 16.41 135.67

14.62 112.8 14.62 111.5 14.62 147.1 14.62 123.80

12.83 102.7 12.83 102 12.83 133.1 12.83 112.60

11.03 72.88 11.03 91.2 11.03 119.3 11.03 94.46

9.24 81.38 9.24 80.78 9.24 104.7 9.24 88.95

7.45 69.86 7.45 69.62 7.45 90.39 7.45 76.62

5.61 59.06 5.61 59.58 5.61 75.02 5.61 64.55

3.80 47.31 3.80 47.64 3.81 59.41 3.80 51.45

2.01 34.46 2.01 34.96 2.01 42.97 2.01 37.46

0.20 20.34 0.21 20.81 0.20 24.47 0.20 21.87

Average Stdev

YS 24.1 27.0 31.3 27.5 3.6

VS 5.8 5.8 7.7 6.4 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 241 231 441 304 119

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 12

Set A7: CS-BX5 – BL12- L1 – 7 day – NIST code (folder SR 39-SR-36C)

SR-36C

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 19.76 0.20 27.17 0.21 19.76 0.20 22.23

2.64 36.73 2.65 61.63 2.66 37.35 2.65 45.24

5.08 51.02 5.10 86.46 5.10 50.3 5.10 62.59

7.59 64.19 7.52 109.4 7.52 62.91 7.54 78.83

10.00 76.36 10.00 132.3 10.00 74.69 10.00 94.45

12.41 88.47 12.48 151.6 12.41 86.52 12.44 108.86

14.90 100.9 14.90 170.2 14.90 98.79 14.90 123.30

17.38 113.2 17.38 187.7 17.31 110.4 17.36 137.10

19.79 125.2 19.79 204.6 19.79 122.2 19.79 150.67

22.21 137 22.21 220.2 22.21 132.9 22.21 163.37

24.69 148.3 24.69 235.6 24.69 144 24.69 175.97

27.10 159.5 27.10 251 27.10 155.7 27.10 188.73

29.59 170.6 29.59 264.6 29.59 166.2 29.59 200.47

32.00 181.2 32.00 278.9 32.00 176.9 32.00 212.33

34.48 192 34.48 292.1 34.48 186.1 34.48 223.40

34.48 191.3 34.48 289.6 34.48 186.5 34.48 222.47

32.62 182.8 32.69 275.1 32.69 178 32.67 211.97

30.90 174.4 30.83 260.9 30.83 168.7 30.85 201.33

29.03 166 29.03 247.3 29.03 160.5 29.03 191.27

27.24 157.9 27.24 233.6 27.24 152.9 27.24 181.47

25.45 149.4 25.45 220.6 25.45 144.1 25.45 171.37

23.66 141.1 23.66 207 23.66 136.4 23.66 161.50

21.86 132.3 21.86 194.4 21.86 127.5 21.86 151.40

20.07 123.8 20.07 181.2 20.07 119.1 20.07 141.37

18.21 115 18.21 167.7 18.21 111.2 18.21 131.30

16.41 106.3 16.41 154.3 16.41 102.6 16.41 121.07

14.62 97.25 14.62 140.8 14.62 93.43 14.62 110.49

12.83 88.1 12.83 127.4 12.83 84.81 12.83 100.10

11.03 79.14 11.03 113 11.03 76.03 11.03 89.39

9.24 69.48 9.24 99.35 9.24 66.74 9.24 78.52

7.45 60.07 7.38 84.46 7.45 57.63 7.43 67.39

5.61 50.15 5.60 69.6 5.59 48.36 5.60 56.04

3.79 39.8 3.82 54.31 3.81 38.44 3.81 44.18

2.01 28.87 2.01 37.96 1.99 27.85 2.00 31.56

0.20 16.28 0.21 19.53 0.20 15.9 0.20 17.24

Average Stdev

YS 21.7 25.7 20.5 22.6 2.7

VS 5.0 7.7 4.9 5.9 1.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 65 612 140 272 297

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 13

Set A7: CS-BX5 – BL45- L1 – 7 day – NIST code (folder SR 39-SR-36D)

SR-36D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 23.29 0.20 18.63 0.21 21 0.20 20.97

2.65 36.82 2.63 31 2.64 35.74 2.64 34.52

5.09 44.34 5.10 35.81 5.10 41.97 5.10 40.71

7.59 50.19 7.52 39.86 7.52 47.6 7.54 45.88

10.00 54.68 10.00 43.79 10.00 52.8 10.00 50.42

12.41 59.73 12.41 47.41 12.41 57.32 12.41 54.82

14.90 65.1 14.90 51.06 14.90 61.34 14.90 59.17

17.38 69.99 17.31 54.47 17.31 65.77 17.33 63.41

19.79 74.94 19.79 57.88 19.79 69.75 19.79 67.52

22.21 79.22 22.28 61.2 22.21 73.99 22.23 71.47

24.69 83.86 24.69 64.7 24.69 78.2 24.69 75.59

27.10 89.13 27.10 68.3 27.10 82.45 27.10 79.96

29.59 93.58 29.59 71.86 29.59 86.9 29.59 84.11

32.00 98.69 32.00 75.37 32.00 91.27 32.00 88.44

34.48 102.7 34.48 79.09 34.48 96.17 34.48 92.65

34.48 103.3 34.48 78.94 34.48 95.4 34.48 92.55

32.62 99.38 32.69 76.11 32.69 91.75 32.67 89.08

30.90 94.74 30.83 73.38 30.90 88.58 30.87 85.57

29.03 91.03 29.03 70.84 29.03 85.11 29.03 82.33

27.24 87.52 27.24 67.76 27.24 81.16 27.24 78.81

25.45 83.62 25.45 65.16 25.45 77.83 25.45 75.54

23.66 79.96 23.66 62.16 23.66 73.98 23.66 72.03

21.86 76.02 21.86 59.78 21.86 70.9 21.86 68.90

20.07 72.13 20.07 56.74 20.07 67.37 20.07 65.41

18.21 68.92 18.28 53.4 18.21 63.06 18.23 61.79

16.41 64.86 16.41 50.31 16.41 59.3 16.41 58.16

14.62 59.93 14.62 47.61 14.62 56.06 14.62 54.53

12.83 55.7 12.83 44.33 12.83 51.71 12.83 50.58

11.03 51.4 11.03 40.77 11.03 47.96 11.03 46.71

9.24 46.77 9.24 37.6 9.24 43.53 9.24 42.63

7.45 42.19 7.38 33.79 7.45 39.55 7.43 38.51

5.61 37.7 5.60 29.88 5.61 34.57 5.61 34.05

3.79 32.3 3.82 25.95 3.82 29.88 3.81 29.38

2.02 26.75 2.01 21.54 2.01 24.64 2.01 24.31

0.21 19.6 0.21 15.69 0.20 17.94 0.20 17.74

Average Stdev

YS 24.0 19.9 22.2 22.0 2.1

VS 2.3 1.8 2.2 2.1 0.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 155 95 123 125 30

Comment: Problem with mixer = material not mixed properly - a lot of sedimentation

0

20

40

60

80

100

120

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 14

Set B1: CS-BX1 – BL23- L2 – Mixing Day – NIST code (folder SR 41-SR-40A)

SR-40A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 24.84 0.20 28.25 0.20 32.03 0.23 28.37

2.64 53.58 2.66 48.80 2.64 68.97 2.65 57.12

5.08 70.61 5.10 64.91 5.10 95.38 5.09 76.97

7.59 86.67 7.52 79.40 7.52 124.00 7.54 96.69

10.00 101.10 10.00 94.58 10.00 149.70 10.00 115.13

12.41 115.90 12.41 109.30 12.41 172.30 12.41 132.50

14.90 131.20 14.90 124.20 14.90 193.20 14.90 149.53

17.31 146.10 17.31 139.10 17.31 209.20 17.31 164.80

19.79 160.70 19.79 153.40 19.79 224.70 19.79 179.60

22.21 174.80 22.21 167.70 22.21 240.20 22.21 194.23

24.69 188.60 24.69 181.80 24.69 255.20 24.69 208.53

27.10 202.10 27.10 195.60 27.17 267.20 27.13 221.63

29.59 215.30 29.59 209.00 29.59 280.20 29.59 234.83

32.00 228.50 32.00 222.10 32.00 292.90 32.00 247.83

34.48 240.90 34.48 234.50 34.48 311.60 34.48 262.33

34.48 241.10 34.48 234.50 34.48 301.70 34.48 259.10

32.69 230.90 32.69 224.40 32.69 286.90 32.69 247.40

30.90 220.30 30.83 214.00 30.83 278.70 30.85 237.67

29.03 210.30 29.03 204.40 29.03 265.70 29.03 226.80

27.24 200.20 27.24 194.10 27.24 246.80 27.24 213.70

25.45 190.00 25.45 183.90 25.45 237.50 25.45 203.80

23.66 179.90 23.66 173.90 23.66 220.20 23.66 191.33

21.86 169.70 21.86 163.70 21.86 211.00 21.86 181.47

20.07 159.00 20.07 153.10 20.07 197.10 20.07 169.73

18.21 148.60 18.28 142.80 18.28 179.40 18.25 156.93

16.41 137.60 16.41 132.10 16.41 165.50 16.41 145.07

14.62 126.30 14.62 121.10 14.62 154.60 14.62 134.00

12.83 114.90 12.83 110.10 12.83 139.50 12.83 121.50

11.03 103.30 11.03 98.55 11.03 124.80 11.03 108.88

9.24 91.21 9.24 87.15 9.24 109.70 9.24 96.02

7.45 79.12 7.45 75.16 7.45 94.24 7.45 82.84

5.62 66.55 5.61 62.93 5.60 76.72 5.61 68.73

3.81 52.95 3.81 50.19 3.82 60.43 3.81 54.52

2.01 38.90 1.99 36.47 2.01 43.03 2.01 39.47

0.20 22.77 0.19 21.18 0.21 23.47 0.20 22.47

Average Stdev

YS 31.2 28.5 32.3 30.7 2.0

VS 6.2 6.1 8.0 6.8 1.1

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 137 94 510 247 229

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 15

Set B1: CS-BX1 – BL23- L1 – Mixing Day – NIST code (folder SR 41-SR-40B)

SR-40B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 34.42 0.20 33.19 0.20 34.89 0.20 34.17

2.63 56.99 2.64 53.57 2.65 59.73 2.64 56.76

5.09 74.18 5.10 69.61 5.08 78.08 5.09 73.96

7.59 88.97 7.52 84.83 7.52 95.67 7.54 89.82

10.00 103.40 10.00 99.52 10.00 113.10 10.00 105.34

12.41 118.20 12.41 114.00 12.41 129.50 12.41 120.57

14.90 133.40 14.90 128.50 14.90 145.60 14.90 135.83

17.38 148.40 17.31 142.80 17.31 162.20 17.33 151.13

19.79 163.20 19.79 156.30 19.79 177.60 19.79 165.70

22.21 177.40 22.21 170.20 22.21 191.70 22.21 179.77

24.69 191.30 24.69 183.10 24.69 206.30 24.69 193.57

27.10 205.30 27.10 194.60 27.10 222.50 27.10 207.47

29.59 218.60 29.59 207.50 29.59 235.90 29.59 220.67

32.00 231.70 32.00 218.70 32.00 249.80 32.00 233.40

34.48 243.80 34.48 231.10 34.48 259.80 34.48 244.90

34.48 243.40 34.48 228.70 34.48 260.30 34.48 244.13

32.69 232.50 32.69 218.50 32.62 248.30 32.67 233.10

30.90 221.80 30.90 209.30 30.90 235.40 30.90 222.17

29.03 211.40 29.03 198.90 29.03 223.50 29.03 211.27

27.24 201.40 27.24 189.50 27.24 215.00 27.24 201.97

25.45 191.10 25.45 179.80 25.45 201.30 25.45 190.73

23.66 181.00 18.90 169.90 23.66 191.90 22.07 180.93

21.86 170.30 21.86 159.20 21.86 178.40 21.86 169.30

20.07 159.80 20.07 149.30 20.07 167.20 20.07 158.77

18.28 149.60 18.21 138.90 18.21 157.10 18.23 148.53

16.41 138.80 16.41 128.60 16.41 145.60 16.41 137.67

14.62 127.20 14.62 118.30 14.62 131.90 14.62 125.80

12.83 116.10 12.83 107.50 12.83 120.20 12.83 114.60

11.03 104.70 11.03 97.37 11.03 108.40 11.03 103.49

9.24 92.73 9.24 86.02 9.24 95.54 9.24 91.43

7.45 80.74 7.38 74.82 7.45 83.04 7.43 79.53

5.62 68.45 5.60 63.03 5.61 70.28 5.61 67.25

3.81 55.12 3.82 51.08 3.81 56.32 3.81 54.17

2.01 41.16 2.01 38.67 2.01 41.79 2.01 40.54

0.20 25.53 0.21 24.14 0.20 25.20 0.20 24.96

Average Stdev

YS 33.1 31.1 31.8 32.0 1.0

VS 6.2 5.9 6.7 6.3 0.4

R2 1.00 0.99 1.00 1.0 0.0

Hysteresis 174 137 365 225 122

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 16

Set B1: CS-BX1 – BL28- L2 – Mixing Day – NIST code (folder SR 41-SR-40C)

SR-40C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 28.24 0.19 27.00 0.19 26.25 0.19 27.16

2.66 47.24 2.65 46.90 2.65 45.98 2.65 46.71

5.10 62.69 5.11 63.54 5.09 61.24 5.10 62.49

7.52 77.32 7.52 79.70 7.59 76.80 7.54 77.94

10.00 92.55 10.00 95.45 10.00 91.03 10.00 93.01

12.41 107.10 12.41 110.50 12.41 105.10 12.41 107.57

14.90 121.50 14.90 124.50 14.90 119.70 14.90 121.90

17.31 136.40 17.31 139.90 17.38 134.30 17.33 136.87

19.79 150.60 19.79 153.70 19.79 148.40 19.79 150.90

22.21 165.40 22.21 168.90 22.21 161.50 22.21 165.27

24.69 179.40 24.69 182.90 24.69 174.80 24.69 179.03

27.10 192.40 27.10 196.10 27.10 189.20 27.10 192.57

29.59 206.10 29.59 210.60 29.59 201.80 29.59 206.17

32.00 219.10 32.00 222.80 32.00 214.90 32.00 218.93

34.48 232.60 34.48 236.40 34.48 224.60 34.48 231.20

34.48 231.70 34.48 234.50 34.48 225.60 34.48 230.60

32.69 221.90 32.69 225.00 32.69 215.60 32.69 220.83

30.83 213.00 30.90 214.50 30.90 204.80 30.87 210.77

29.03 203.60 29.03 203.50 29.03 194.40 29.03 200.50

27.24 193.10 27.24 196.10 27.24 187.40 27.24 192.20

25.45 183.80 25.45 184.70 25.45 176.70 25.45 181.73

23.66 173.60 23.66 176.00 23.66 168.10 23.66 172.57

21.86 164.10 21.86 163.70 21.86 156.30 21.86 161.37

20.00 153.50 20.07 154.00 20.07 147.20 20.05 151.57

18.28 142.80 18.28 145.10 18.21 137.60 18.25 141.83

16.41 132.30 16.41 134.40 16.41 127.50 16.41 131.40

14.62 122.20 14.62 121.90 14.62 116.20 14.62 120.10

12.83 111.20 12.83 111.00 12.83 104.90 12.83 109.03

11.03 99.96 11.03 100.60 11.03 95.77 11.03 98.78

9.24 88.71 9.24 88.24 9.24 83.39 9.24 86.78

7.45 76.76 7.38 76.65 7.45 72.96 7.43 75.46

5.61 64.56 5.60 64.88 5.61 60.78 5.61 63.41

3.81 51.96 3.82 51.87 3.80 48.22 3.81 50.68

1.99 38.22 2.01 38.10 2.01 36.10 2.00 37.47

0.20 23.08 0.20 22.43 0.20 21.27 0.20 22.26

Average Stdev

YS 30.9 30.4 28.0 29.8 1.6

VS 6.0 6.1 5.8 6.0 0.1

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 30 3 132 55 68

0

50

100

150

200

250

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 17

Set B1: CS-BX1 – BL28- L1 – Mixing Day – NIST code (folder SR 41-SR-40D)

SR-40D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.19 38.14 0.21 37.07 0.21 35.02 0.20 36.74

2.63 62.06 2.64 59.36 2.64 57.10 2.64 59.51

5.10 77.06 5.10 73.85 5.10 74.31 5.10 75.07

7.52 91.77 7.52 88.68 7.52 90.87 7.52 90.44

10.00 106.70 10.00 103.00 10.00 107.10 10.00 105.60

12.41 122.00 12.41 117.70 12.41 121.40 12.41 120.37

14.90 137.70 14.90 132.90 14.90 137.00 14.90 135.87

17.31 153.20 17.31 147.10 17.31 152.30 17.31 150.87

19.79 168.20 19.79 161.50 19.79 167.40 19.79 165.70

22.21 182.00 22.21 174.10 22.21 181.00 22.21 179.03

24.69 196.20 24.69 187.10 24.69 195.20 24.69 192.83

27.10 211.60 27.17 201.80 27.17 210.40 27.15 207.93

29.59 225.40 29.59 213.20 29.59 222.80 29.59 220.47

32.00 238.70 32.00 226.90 32.00 237.50 32.00 234.37

34.48 250.00 34.48 236.80 34.48 249.20 34.48 245.33

34.48 250.10 34.48 237.40 34.48 249.60 34.48 245.70

32.69 239.10 32.69 226.80 32.69 238.70 32.69 234.87

30.90 226.10 30.90 215.60 30.83 227.30 30.87 223.00

29.10 215.40 29.03 206.50 29.03 217.10 29.06 213.00

27.24 207.00 27.24 194.60 27.24 204.90 27.24 202.17

25.45 194.50 25.45 185.80 25.45 195.90 25.45 192.07

23.66 185.90 23.66 174.30 23.66 183.90 23.66 181.37

21.86 173.50 21.86 166.00 21.86 174.60 21.86 171.37

20.07 162.70 20.07 155.40 20.07 163.60 20.07 160.57

18.21 154.00 18.28 144.60 18.28 151.70 18.25 150.10

16.41 142.80 16.41 134.00 16.41 140.40 16.41 139.07

14.62 129.50 14.62 124.00 14.62 130.20 14.62 127.90

12.83 118.60 12.83 113.30 12.83 118.60 12.83 116.83

11.03 107.30 11.03 101.80 11.03 106.80 11.03 105.30

9.24 94.60 9.24 90.99 9.24 95.13 9.24 93.57

7.45 82.78 7.45 79.16 7.38 82.61 7.43 81.52

5.61 70.56 5.59 66.99 5.61 69.68 5.60 69.08

3.81 56.98 3.82 54.71 3.81 56.58 3.82 56.09

1.99 42.80 2.01 41.11 2.01 42.57 2.00 42.16

0.20 26.71 0.20 26.50 0.21 26.88 0.20 26.70

Average Stdev

YS 34.2 33.0 33.8 33.6 0.6

VS 6.3 6.0 6.3 6.2 0.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 241 273 206 240 33

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 18

Set B3: CS-BX1 – BL23- L2 – 4 day – NIST code (folder SR 42-SR-40A)

SR-40A

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.21 21.31 0.20 23.86 0.20 20.49 0.20 21.89

2.64 44.06 2.63 52.97 2.65 42.82 2.64 46.62

5.09 60.5 5.10 75.4 5.11 59.6 5.10 65.17

7.52 77.05 7.52 96.28 7.52 74.93 7.52 82.75

10.00 92.52 10.00 116.3 10.00 90.11 10.00 99.64

12.41 108.1 12.41 134.6 12.41 105.2 12.41 115.97

14.90 123.6 14.90 152.8 14.90 119.9 14.90 132.10

17.31 138.4 17.31 169.4 17.31 135 17.31 147.60

19.79 153.3 19.79 186.2 19.79 148.9 19.79 162.80

22.21 167.2 22.21 200.5 22.28 163.7 22.23 177.13

24.69 180.8 24.69 215 24.69 177.2 24.69 191.00

27.10 194.5 27.17 230.9 27.17 189.7 27.15 205.03

29.59 207.5 29.59 242.7 29.59 203.4 29.59 217.87

32.07 220.1 32.00 256.4 32.00 215 32.02 230.50

34.48 231.8 34.48 266.1 34.48 226.8 34.48 241.57

34.48 231.3 34.48 266.3 34.48 224.1 34.48 240.57

32.69 220.2 32.69 252.9 32.69 213.4 32.69 228.83

30.90 208.8 30.83 237.4 30.90 203.6 30.87 216.60

29.03 198 29.03 225.7 29.03 191.9 29.03 205.20

27.24 188 27.24 212.1 27.24 184.1 27.24 194.73

25.45 176.9 25.45 200.5 25.45 172.3 25.45 183.23

23.66 166.8 23.66 187.8 23.66 163.5 23.66 172.70

21.86 156.1 21.86 177.4 21.86 150.7 21.86 161.40

20.07 145.3 20.07 164.4 20.07 140.8 20.07 150.17

18.21 135.1 18.28 152.7 18.28 131.9 18.25 139.90

16.41 124.4 16.41 140.1 16.41 121.3 16.41 128.60

14.62 113 14.62 127.6 14.62 109.1 14.62 116.57

12.83 102.3 12.83 115.7 12.83 98.75 12.83 105.58

11.03 91.02 11.03 101.6 11.03 88.2 11.03 93.61

9.24 79.6 9.24 89.59 9.24 76.86 9.24 82.02

7.45 67.9 7.45 75.34 7.45 65.32 7.45 69.52

5.61 56.15 5.61 62.14 5.60 54.42 5.61 57.57

3.80 43.68 3.81 48.08 3.81 42.36 3.81 44.71

2.01 30.75 2.00 32.76 2.01 29.56 2.01 31.02

0.20 16.31 0.19 16.28 0.20 15.3 0.20 15.96

Average Stdev

YS 21.1 21.4 20.1 20.9 0.7

VS 6.1 7.1 6.0 6.4 0.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 241 624 181 349 240

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 19

Set B3: CS-BX1 – BL23- L1 – 4 day – NIST code (folder SR 42-SR-40B)

SR-40B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.23 30.32 0.21 26.19 0.20 25.58 0.21 27.36

2.63 75.51 2.65 46.92 2.64 45.09 2.64 55.84

5.10 114.3 5.09 62.89 5.10 62.02 5.10 79.74

7.52 144.6 7.59 78.55 7.52 77.08 7.54 100.08

10.00 168.1 10.00 93.19 10.00 91.58 10.00 117.62

12.41 191.9 12.41 107.9 12.41 105.9 12.41 135.23

14.90 214 14.90 123 14.90 120.6 14.90 152.53

17.31 235.7 17.38 137.3 17.31 133.9 17.33 168.97

19.79 256.5 19.79 151.5 19.79 147.9 19.79 185.30

22.28 276.9 22.21 163.1 22.21 161.1 22.23 200.37

24.69 295.5 24.69 176.4 24.69 173.7 24.69 215.20

27.17 314.8 27.10 189.4 27.10 186.3 27.13 230.17

29.59 331.6 29.59 201.1 29.59 197.1 29.59 243.27

32.00 347.9 32.07 214.3 32.00 210.3 32.02 257.50

34.48 361.5 34.48 226.2 34.48 220.9 34.48 269.53

34.48 359.4 34.48 226.4 34.48 222 34.48 269.27

32.69 342.5 32.69 216.6 32.69 212.2 32.69 257.10

30.90 322.2 30.90 204.5 30.83 199.8 30.87 242.17

29.03 305.1 29.03 195.8 29.03 191.1 29.03 230.67

27.24 292.3 27.24 184.3 27.24 181.3 27.24 219.30

25.45 272.8 25.45 174.8 25.45 170.7 25.45 206.10

23.66 259.2 23.66 164.6 23.66 162.3 23.66 195.37

21.86 240.3 21.86 156 21.86 151.8 21.86 182.70

20.07 223.9 20.00 145.2 20.00 141.6 20.02 170.23

18.21 209.6 18.21 136 18.28 134.1 18.23 159.90

16.41 193.3 16.41 125.5 16.41 123.9 16.41 147.57

14.62 174.4 14.62 114.6 14.62 111.6 14.62 133.53

12.83 158.1 12.83 104.7 12.83 101.9 12.83 121.57

11.03 140.5 11.03 92.72 11.03 91.27 11.03 108.16

9.24 123.5 9.24 82.67 9.24 80.52 9.24 95.56

7.38 105.1 7.45 70.82 7.45 69.35 7.43 81.76

5.60 87.79 5.61 59.99 5.60 58.87 5.60 68.88

3.81 68.81 3.81 47.95 3.81 46.87 3.81 54.54

2.01 48.49 2.02 34.58 2.00 34.2 2.01 39.09

0.20 26.01 0.20 20.3 0.20 20.08 0.20 22.13

Average Stdev

YS 33.2 26.3 25.8 28.4 4.2

VS 9.5 5.9 5.7 7.0 2.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 885 195 232 437 388

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 20

Set B3: CS-BX1 – BL28- L2 – 4 day – NIST code (folder SR 42-SR-40C)

SR-40C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 22.45 0.21 20.89 0.20 21.96 0.20 21.77

2.65 39.94 2.64 38.11 2.66 39.65 2.65 39.23

5.10 54.21 5.09 51.27 5.09 52.45 5.09 52.64

7.52 67.14 7.52 64.34 7.59 64.59 7.54 65.36

10.00 80.7 10.00 76.83 10.00 76.54 10.00 78.02

12.41 93.67 12.41 88.95 12.41 88.6 12.41 90.41

14.90 105.5 14.90 101 14.90 100.4 14.90 102.30

17.38 119 17.38 112.8 17.38 112.9 17.38 114.90

19.79 130.3 19.79 124.2 19.79 124.1 19.79 126.20

22.28 142.4 22.21 135.2 22.21 135.4 22.23 137.67

24.69 153.9 24.69 146.1 24.69 146.6 24.69 148.87

27.10 166 27.10 157.7 27.10 158.2 27.10 160.63

29.59 178 29.59 168.5 29.59 169.4 29.59 171.97

32.00 188.7 32.00 179.4 32.00 179.8 32.00 182.63

34.48 197.3 34.48 188.8 34.48 189.1 34.48 191.73

34.48 199.3 34.48 188.9 34.48 188.6 34.48 192.27

32.69 190.1 32.69 180.4 32.69 180 32.69 183.50

30.90 178 30.90 171.2 30.90 171.2 30.90 173.47

29.03 169.4 29.03 162.6 29.03 162.1 29.03 164.70

27.24 162.7 27.24 155.2 27.24 155.6 27.24 157.83

25.45 152.2 25.45 146.3 25.45 145.9 25.45 148.13

23.66 145.2 23.66 138.3 23.66 138.5 23.66 140.67

21.86 134.9 21.86 128.9 21.86 128.5 21.86 130.77

20.07 125.8 20.07 120.6 20.07 120.3 20.07 122.23

18.21 119.6 18.21 112.4 18.21 112.4 18.21 114.80

16.41 110.5 16.41 103.8 16.41 103.8 16.41 106.03

14.62 99.08 14.62 94.33 14.62 94.15 14.62 95.85

12.83 90.5 12.83 85.51 12.83 85.31 12.83 87.11

11.03 80.27 11.03 76.94 11.03 76.94 11.03 78.05

9.24 71.44 9.24 67.35 9.24 67.27 9.24 68.69

7.45 60.95 7.45 58.29 7.45 58.24 7.45 59.16

5.60 51.97 5.61 49.05 5.62 48.94 5.61 49.99

3.82 41.39 3.79 39.05 3.80 38.96 3.80 39.80

2.01 29.64 2.01 28.64 2.01 28.65 2.01 28.98

0.20 17.38 0.19 16.87 0.20 16.79 0.20 17.01

Average Stdev

YS 22.1 20.8 20.8 21.2 0.7

VS 5.2 4.9 4.9 5.0 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 230 150 144 175 48

0

50

100

150

200

250

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 21

Set B3: CS-BX1 – BL28- L1 – 4 day – NIST code (folder SR 42-SR-40D)

SR-40D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 27.93 2.66 49.95 0.20 26.63 1.02 34.84

2.64 47.72 5.10 66.3 2.65 48.37 3.46 54.13

5.08 63.62 7.52 81.52 5.09 69.35 5.90 71.50

7.52 78.64 10.00 97.22 7.52 83.53 8.34 86.46

10.00 93.6 12.41 112.2 10.00 99.57 10.80 101.79

12.41 108 14.90 126.7 12.41 115.8 13.24 116.83

14.90 122.1 17.31 141.4 14.90 131.8 15.70 131.77

17.31 137.2 19.79 155.3 17.31 147.8 18.14 146.77

19.79 150.5 22.21 170.4 19.79 162.8 20.60 161.23

22.21 164.2 24.69 184.2 22.21 175.7 23.03 174.70

24.69 177.3 27.10 195.8 24.69 189.4 25.49 187.50

27.10 190.3 29.59 209.1 27.10 205 27.93 201.47

29.59 203.6 32.00 221.2 29.59 217.9 30.39 214.23

32.00 215.3 34.48 235.5 32.00 230.6 32.83 227.13

34.48 225.9 34.48 232.2 34.48 240.2 34.48 232.77

34.48 225 32.69 221.7 34.48 239.3 33.89 228.67

32.62 214.6 30.83 214.1 32.69 226.7 32.05 218.47

30.90 204.2 29.10 203.7 30.90 216 30.30 207.97

29.03 193.4 27.24 191.8 29.10 204 28.46 196.40

27.24 186.3 25.45 183.2 27.24 196.5 26.64 188.67

25.45 174.8 23.66 171.2 25.45 183.8 24.85 176.60

23.66 166.5 21.86 162.8 23.66 174.9 23.06 168.07

21.86 154.4 20.00 151.9 21.86 161.3 21.24 155.87

20.07 145 18.28 140.2 20.07 151.6 19.47 145.60

18.21 135.5 16.41 129.6 18.28 139.5 17.63 134.87

16.41 125.5 14.62 120 16.41 128.7 15.82 124.73

14.62 114.3 12.83 109.2 14.62 118.5 14.02 114.00

12.83 103.4 11.03 97.37 12.83 106.2 12.23 102.32

11.03 93.7 9.24 86.57 11.03 96.77 10.44 92.35

9.24 82.02 7.45 74.57 9.24 83.63 8.64 80.07

7.45 71.53 5.60 62.72 7.45 72.84 6.83 69.03

5.61 59.9 3.80 50.54 5.61 59.5 5.01 56.65

3.80 47.67 1.99 36.9 3.80 47.18 3.20 43.92

2.02 35.37 0.20 22.38 1.99 34.93 1.40 30.89

0.20 21.1 0.00 0 0.20 20.02 0.13 13.71

Average Stdev

YS 26.7 28.1 24.5 26.4 1.8

VS 5.8 6.1 6.3 6.1 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 185 332 327 281 84

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 22

Set B7: CS-BX1 – BL23- L2 – 7 day – NIST code (folder SR 43-SR-40A)

SR-40A

Run# A Run# C Run# D Average

SR SS SR SS SR SS SR SS

0.26 16.05 0.20 27.93 0.21 21.31 0.22 21.76

2.65 43.71 2.66 68.14 2.65 44.18 2.65 52.01

5.09 61.55 5.10 94.69 5.10 62.48 5.10 72.91

7.52 77.38 7.52 120.1 7.59 80.1 7.54 92.53

10.00 93.48 10.00 142.2 10.00 96.86 10.00 110.85

12.41 109.5 12.41 163 12.41 113.8 12.41 128.77

14.90 125 14.90 184.1 14.90 130.4 14.90 146.50

17.38 141.5 17.31 203.5 17.38 147.1 17.36 164.03

19.79 156.1 19.79 221.8 19.79 163.3 19.79 180.40

22.21 171.5 22.21 238.1 22.21 178.8 22.21 196.13

24.69 186.1 24.69 254.6 24.69 194 24.69 211.57

27.10 198.2 27.10 271 27.10 209.3 27.10 226.17

29.59 213.1 29.59 286.7 29.59 224 29.59 241.27

32.00 224.5 32.00 298.9 32.00 238.1 32.00 253.83

34.48 237.8 34.48 313.6 34.48 250.4 34.48 267.27

34.48 233 34.48 308.1 34.48 250 34.48 263.70

32.62 221.4 32.69 291.9 32.62 238.3 32.64 250.53

30.90 213.9 30.90 278 30.90 226.2 30.90 239.37

29.03 201.8 29.10 262.3 29.03 214 29.06 226.03

27.24 192.2 27.24 250.2 27.24 204.8 27.24 215.73

25.45 181.6 25.45 234.8 25.45 192.8 25.45 203.07

23.66 170.3 23.66 221.6 23.66 182.4 23.66 191.43

21.86 159.1 21.86 205.4 21.86 169.4 21.86 177.97

20.07 148.9 20.07 192 20.07 158.7 20.07 166.53

18.21 134.9 18.21 175.8 18.21 147.7 18.21 152.80

16.41 124.3 16.41 161.5 16.41 136.1 16.41 140.63

14.62 115.2 14.62 148.1 14.62 123.3 14.62 128.87

12.83 102.6 12.83 132.3 12.83 110.9 12.83 115.27

11.03 92.61 11.03 118.8 11.03 99.74 11.03 103.72

9.24 79.93 9.24 102.4 9.24 86.35 9.24 89.56

7.45 68.82 7.45 87.62 7.45 74.21 7.45 76.88

5.61 54.9 5.61 70.07 5.61 60.92 5.61 61.96

3.81 42.5 3.81 53.8 3.79 46.86 3.80 47.72

2.01 30.09 1.99 36.92 2.01 32.84 2.01 33.28

0.20 15.08 0.21 17.48 0.20 16.52 0.20 16.36

Average Stdev

YS 20.1 23.4 23.0 22.2 1.8

VS 6.3 8.3 6.7 7.1 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 119 718 166 334 333

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# C

Run# D
B - 23

Set B7: CS-BX1 – BL23- L1 – 7 day – NIST code (folder SR 43-SR-40B)

SR-40B

Run# E Run# F Run# G Average

SR SS SR SS SR SS SR SS

0.21 32.16 0.20 25.65 0.19 25.21 0.20 27.67

2.65 62.97 2.83 89.02 2.64 45.33 2.71 65.77

5.09 85.78 5.08 60.62 5.11 61.51 5.09 69.30

7.52 105.6 7.52 75.08 7.52 76.82 7.52 85.83

10.00 127.1 10.00 89.4 8.00 91.75 9.33 102.75

12.41 146.5 12.34 120.5 12.41 106.5 12.39 124.50

14.90 163.8 14.90 118.7 14.90 120.8 14.90 134.43

17.31 182.3 17.38 132.8 17.31 135.8 17.33 150.30

19.79 199 19.79 147.1 19.79 149.9 19.79 165.33

22.21 219.4 22.21 160.9 22.28 163.1 22.23 181.13

24.69 235.9 24.69 174.4 24.69 175.9 24.69 195.40

27.10 245.6 27.10 188 27.10 190.2 27.10 207.93

29.59 264.5 29.59 200.9 29.59 202.4 29.59 222.60

32.00 273.6 32.07 214.5 32.00 215 32.02 234.37

34.48 295.4 34.48 226.9 34.48 223.6 34.48 248.63

34.48 282.4 34.48 226.7 34.48 225.6 34.48 244.90

32.69 269.1 32.69 216.6 32.69 214.9 32.69 233.53

30.90 265.4 30.90 206.3 30.90 200.6 30.90 224.10

29.03 251.3 29.03 196.7 29.03 191 29.03 213.00

27.24 235.2 27.24 186 27.24 183 27.24 201.40

25.45 226.1 25.45 176.5 25.45 170.9 25.45 191.17

23.66 209.8 23.66 166.3 23.66 163 23.66 179.70

21.86 199.3 21.86 156.7 21.86 152 21.86 169.33

20.07 186.8 20.07 146.5 20.07 141.3 20.07 158.20

18.21 167.6 18.21 136.2 18.28 134.4 18.23 146.07

16.41 154.7 16.41 125.7 16.41 124.1 16.41 134.83

14.62 145.8 14.62 115.2 14.62 111.1 14.62 124.03

12.83 131 12.83 104.2 12.83 101.9 12.83 112.37

11.03 118.4 11.03 93.54 11.03 89.96 11.03 100.63

9.24 103.2 9.24 82.28 9.24 80.29 9.24 88.59

7.45 89.28 7.45 71.17 7.38 68.07 7.43 76.17

5.61 72.09 5.61 59.41 5.61 58.02 5.61 63.17

3.80 56.96 3.80 47.13 3.83 46.02 3.81 50.04

2.01 41.03 2.01 34.32 2.01 32.69 2.01 36.01

0.21 22.5 0.19 20.06 0.19 18.79 0.20 20.45

Average Stdev

YS 30.6 25.9 24.1 26.8 3.3

VS 7.5 5.9 5.8 6.4 1.0

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 67 228 348 215 141

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# E

Run# F

Run# G
B - 24

Set B7: CS-BX1 – BL28- L2 – 7 day – NIST code (folder SR 43-SR-40C)

SR-40C

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 28.07 0.20 29.87 0.20 31.67 0.20 29.87

2.66 60.27 2.65 60.77 2.66 80.9 2.65 67.31

5.10 82.95 5.10 85.29 5.10 119.2 5.10 95.81

7.52 105.7 7.59 110.7 7.52 163.9 7.54 126.77

10.00 127.1 10.00 129.6 10.00 193 10.00 149.90

12.41 147.1 12.41 147.9 12.41 214.6 12.41 169.87

14.90 164.2 14.90 166 14.90 234.9 14.90 188.37

17.31 183.2 17.31 183.8 17.31 255.5 17.31 207.50

19.79 198.7 19.79 201.3 19.79 273.3 19.79 224.43

22.21 218.9 22.28 218.1 22.21 292 22.23 243.00

24.69 235.1 24.69 234.7 24.69 309 24.69 259.60

27.10 245 27.10 251.4 27.10 323.7 27.10 273.37

29.59 261.7 29.59 266.4 29.59 342.6 29.59 290.23

32.00 272.2 32.07 281.6 32.00 356.1 32.02 303.30

34.48 292.8 34.48 293.7 34.48 375.5 34.48 320.67

34.48 285.6 34.48 293.6 34.48 365.3 34.48 314.83

32.69 273.1 32.69 279.2 32.69 347.3 32.69 299.87

30.83 261.5 30.90 263.6 30.83 334.9 30.85 286.67

29.03 249.7 29.03 250.8 29.10 316.9 29.06 272.47

27.24 230.4 27.24 237.9 27.24 298.2 27.24 255.50

25.45 220.9 25.45 223.9 25.45 283.3 25.45 242.70

23.66 205 23.66 211.6 23.66 264.3 23.66 226.97

21.86 197.5 21.86 198.4 21.86 247.4 21.86 214.43

20.00 182.6 20.07 184.5 20.07 230.2 20.05 199.10

18.28 170.6 18.21 172.4 18.28 212.9 18.25 185.30

16.41 157.2 16.41 158.9 16.41 195.7 16.41 170.60

14.62 143 14.62 144.2 14.62 178.2 14.62 155.13

12.83 130.3 12.83 131 12.83 159.7 12.83 140.33

11.03 113.4 11.03 115.9 11.03 143.4 11.03 124.23

9.17 101.5 9.24 102.1 9.24 123.9 9.22 109.17

7.38 85.37 7.45 86.79 7.45 106.2 7.43 92.79

5.61 71.95 5.61 72.24 5.61 86.22 5.61 76.80

3.81 56.14 3.81 56.3 3.81 66.46 3.81 59.63

2.00 38.35 2.01 39.48 1.99 46.1 2.00 41.31

0.20 20.29 0.21 20.77 0.20 23.04 0.20 21.37

Average Stdev

YS 28.3 27.8 30.5 28.9 1.4

VS 7.6 7.7 9.9 8.4 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 293 547 964 601 339

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# H

Run# I

Run# J
B - 25

Set B7: CS-BX1 – BL28- L1 – 7 day – NIST code (folder SR 43-SR-40D)

SR-40D

Run# M Run# N Average

SR SS SR SS SR SS SR SS

0.20 27.26 0.19 39.65 0.20 33.46

2.63 47.44 2.66 77.68 2.64 62.56

5.10 63.21 5.09 107.1 5.09 85.16

7.52 78.3 7.52 136.7 7.52 107.50

10.00 93.25 10.00 158.8 10.00 126.03

12.41 107.8 12.41 180.9 12.41 144.35

14.90 122.9 14.90 203.1 14.90 163.00

17.31 137.2 17.31 222.7 17.31 179.95

19.79 151.9 19.79 243.4 19.79 197.65

22.21 165.4 22.21 260.4 22.21 212.90

24.69 179.3 24.69 278.5 24.69 228.90

27.17 193.4 27.10 298.4 27.14 245.90

29.59 205.8 29.59 313.5 29.59 259.65

32.00 219.5 32.00 330.7 32.00 275.10

34.48 231.6 34.48 342 34.48 286.80

34.48 231.8 34.48 341.8 34.48 286.80

32.69 221.6 32.69 325.5 32.69 273.55

30.83 210.9 30.90 306.4 30.86 258.65

29.03 201.6 29.03 290.9 29.03 246.25

21.79 190.3 27.24 278.1 24.52 234.20

25.45 181.2 25.45 260.9 25.45 221.05

23.66 170.2 23.66 247.6 23.66 208.90

21.86 161.4 21.86 230 21.86 195.70

20.07 150.9 20.07 215.1 20.07 183.00

18.28 140.2 18.21 200.7 18.24 170.45

16.41 129.4 16.41 184.9 16.41 157.15

14.62 119.1 14.62 168.2 14.62 143.65

12.83 107.9 12.83 151.8 12.83 129.85

11.03 96.57 11.03 136.6 11.03 116.59

9.24 85.48 9.24 119 9.24 102.24

7.45 73.58 7.45 102.6 7.45 88.09

5.59 61.56 5.61 84.46 5.60 73.01

3.82 49.06 3.81 66.18 3.81 57.62

2.01 35.41 1.99 47.26 2.00 41.34

0.21 20.69 0.20 25.66 0.20 23.18

Average Stdev

YS 27.7 33.4 30.6 4.0

VS 6.1 9.0 7.5 2.0

R2 1.0 1.0 1.0 0.0

Hysteresis 59 852 456 561

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# M

Run# N
B - 26

Set C1: CS-BX3 – BL30- L1 – Mixing Day – NIST code (folder SR 45-SR-44A)

SR-44A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.22 36.72 2.65 65.05 0.21 46.15 1.03 49.31

2.65 68.35 5.09 82.07 2.66 81.98 3.46 77.47

5.08 87.49 7.59 98.28 5.10 108.4 5.92 98.06

7.59 105.7 10.00 114.8 7.52 135.7 8.37 118.73

10.00 123.5 12.41 131.2 10.00 160.1 10.80 138.27

12.41 141.6 14.90 147.6 12.41 183.5 13.24 157.57

14.90 161.4 17.38 164.6 14.90 207.7 15.72 177.90

17.31 179.3 19.79 180.2 17.31 229.8 18.14 196.43

19.79 197.7 22.21 196.7 19.79 251.4 20.60 215.27

22.21 212.5 24.69 211.9 22.21 269.8 23.03 231.40

24.69 228.7 27.10 225.4 24.69 289 25.49 247.70

27.10 247.8 29.59 240.2 27.10 310.1 27.93 266.03

29.59 262 32.00 252.5 29.59 328.2 30.39 280.90

32.00 277.8 34.48 267.1 32.00 344.6 32.83 296.50

34.48 286.9 34.48 262.8 34.48 357.7 34.48 302.47

34.48 288.8 32.69 251.1 34.48 356 33.89 298.63

32.62 275.7 30.90 241.6 32.69 339.8 32.07 285.70

30.90 260.6 29.03 229.6 30.90 322.9 30.28 271.03

29.03 247.9 27.24 218.3 29.10 306.9 28.46 257.70

27.24 239.6 25.45 207.8 27.24 298 26.64 248.47

25.45 224.5 23.66 196 25.45 279.1 24.85 233.20

23.66 215.3 21.86 184 23.66 268.4 23.06 222.57

21.86 199.5 20.07 173.4 21.86 248 21.26 206.97

20.07 188 18.21 160.4 20.07 234.6 19.45 194.33

18.21 177.9 16.41 148.9 18.21 219.6 17.61 182.13

16.41 165.5 14.62 137.8 16.41 203.9 15.82 169.07

14.62 149.5 12.83 125 14.62 187.2 14.02 153.90

12.83 136.4 11.03 114 12.83 169.4 12.23 139.93

11.03 124 9.24 100.4 11.03 156.3 10.44 126.90

9.24 109.2 7.45 88.3 9.24 135.5 8.64 111.00

7.45 95.56 5.61 74.02 7.45 119.4 6.84 96.33

5.61 81.6 3.81 60.03 5.60 98.87 5.01 80.17

3.80 65.59 2.01 45.57 3.80 78.81 3.20 63.32

2.01 49.16 0.20 28.36 2.00 58.72 1.40 45.41

0.20 29.92 0.00 0 0.21 33.7 0.14 21.21

Average Stdev

YS 39.2 35.7 47.8 40.9 6.2

VS 7.3 6.7 9.1 7.7 1.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 367 302 466 378 83

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 27

Set C1: CS-BX3 – BL3- L1 – Mixing Day – NIST code (folder SR 45-SR-44B)

SR-44B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 6.916 0.21 5.697 0.20 6.112 0.20 6.24

2.65 9.652 2.65 8.415 2.65 9.636 2.65 9.23

5.09 11.98 5.10 10.27 5.09 11.85 5.09 11.37

7.52 13.9 7.52 11.92 7.52 13.75 7.52 13.19

10.00 15.95 10.00 13.41 10.00 15.55 10.00 14.97

12.41 17.91 12.41 15.01 12.41 17.1 12.41 16.67

14.90 19.85 14.90 16.83 14.90 18.7 14.90 18.46

17.31 21.66 17.38 18.19 17.31 20.15 17.33 20.00

19.79 23.52 19.79 19.78 19.79 21.47 19.79 21.59

22.21 25.17 22.21 21.03 22.21 22.62 22.21 22.94

24.69 26.85 24.69 22.41 24.69 23.94 24.69 24.40

27.10 28.72 27.17 23.9 27.10 25.39 27.13 26.00

29.59 30.36 29.59 24.81 29.59 26.68 29.59 27.28

32.00 32.16 32.00 25.58 32.00 28.03 32.00 28.59

34.48 33.75 34.48 26.22 34.48 29.22 34.48 29.73

34.48 33.68 34.48 25.7 34.48 29.33 34.48 29.57

32.69 32.44 32.69 24.73 32.69 28.26 32.69 28.48

30.90 31.26 30.90 24.05 30.83 27.13 30.87 27.48

29.03 30.03 29.03 23.08 29.03 26.2 29.03 26.44

27.24 29.03 27.24 22.01 27.24 25.05 27.24 25.36

25.45 27.51 25.45 21.28 25.45 23.82 25.45 24.20

23.66 26.48 23.66 20.19 23.66 22.87 23.66 23.18

21.86 25.02 21.86 19.24 21.86 21.76 21.86 22.01

20.00 23.66 20.07 18.29 20.00 20.49 20.02 20.81

18.28 22.32 18.21 17.1 18.21 19.47 18.23 19.63

16.41 20.95 16.41 16.06 16.41 18.33 16.41 18.45

14.62 19.73 14.62 15.21 14.62 17.08 14.62 17.34

12.83 18.38 12.83 14.13 12.83 16.02 12.83 16.18

11.03 17.04 11.03 13.19 11.03 14.46 11.03 14.90

9.24 15.5 9.24 11.95 9.24 13.38 9.24 13.61

7.45 13.95 7.45 10.81 7.45 11.76 7.45 12.17

5.61 12.42 5.60 9.577 5.60 10.51 5.60 10.84

3.81 10.76 3.82 8.329 3.81 9.135 3.81 9.41

2.00 9.064 2.01 7.108 1.99 7.369 2.00 7.85

0.20 6.615 0.19 5.181 0.20 5.263 0.20 5.69

Average Stdev

YS 8.0 6.3 6.6 7.0 0.9

VS 0.8 0.6 0.7 0.7 0.1

R2 1.00 1.00 0.99 1.0 0.0

Hysteresis 4 25 39 23 17

0

5

10

15

20

25

30

35

40

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 28

Set C1: CS-BX3 – BL3- L2 – Mixing Day – NIST code (folder SR 45-SR-44C)

SR-44C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 32.36 0.21 38.7 0.21 33.18 0.20 34.75

2.65 52.56 2.65 70 2.64 55.08 2.65 59.21

5.10 68 5.10 93.33 5.10 71.75 5.10 77.69

7.52 82.35 7.52 117.5 7.52 87.37 7.52 95.74

10.00 96.75 10.00 138.8 10.00 101.8 10.00 112.45

12.41 111 12.41 158.2 12.41 116.6 12.41 128.60

14.90 124.8 11.93 176.9 14.90 131.8 13.91 144.50

17.31 139.1 17.31 195.1 17.38 146.6 17.33 160.27

19.79 152.6 19.79 212.4 19.79 161.8 19.79 175.60

22.21 166.2 22.21 230.1 22.21 176.3 22.21 190.87

24.69 179.3 24.69 246.3 24.69 190.7 24.69 205.43

27.10 191.6 27.10 259.9 27.10 204.5 27.10 218.67

29.59 204.5 29.59 274.5 29.59 218.1 29.59 232.37

32.00 215.8 32.00 287.3 32.00 231.1 32.00 244.73

34.48 227.9 34.48 301.3 34.48 243.9 34.48 257.70

34.48 225.2 34.48 297.2 34.48 242 34.48 254.80

32.69 215.1 32.69 283.4 32.69 230.7 32.69 243.07

30.83 206.7 30.83 269.5 30.90 221.1 30.85 232.43

29.03 196.7 29.03 256.8 29.03 210.5 29.03 221.33

27.24 186.4 27.24 242 27.24 199.4 27.24 209.27

25.45 177.2 25.45 230 25.45 189.6 25.45 198.93

23.66 166.7 23.66 215.9 23.66 178.5 23.66 187.03

21.86 157.3 21.86 204.1 21.86 168.5 21.86 176.63

20.07 147.6 20.00 190.4 20.07 158 20.05 165.33

18.28 136.5 18.28 176.6 18.21 146.5 18.25 153.20

16.41 126.4 16.41 163.1 16.41 135.7 16.41 141.73

14.62 117.1 14.62 150.5 14.62 125.1 14.62 130.90

12.83 106.4 12.83 136.7 12.83 113.8 12.83 118.97

11.03 96.04 11.03 122.2 11.03 102.7 11.03 106.98

9.24 84.85 9.24 108.3 9.24 90.84 9.24 94.66

7.45 73.97 7.45 93.53 7.45 79.11 7.45 82.20

5.60 62 5.61 78.19 5.61 66.29 5.61 68.83

3.81 50.1 3.82 62.55 3.81 53.48 3.81 55.38

1.99 37.4 1.99 45.68 2.01 39.84 2.00 40.97

0.20 22.91 0.21 26.82 0.20 24.18 0.20 24.64

Average Stdev

YS 29.3 34.2 31.1 31.5 2.5

VS 5.8 7.7 6.2 6.6 1.0

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 142 597 142 294 262

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 29

Set C1: CS-BX3 – BL30- L2 – Mixing Day – NIST code (folder SR 45-SR-44D)

SR-44D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 34.94 0.20 33.52 0.21 37.21 0.20 35.22

2.64 70.15 2.63 63.05 2.63 82.12 2.64 71.77

5.10 94.66 5.09 88.1 5.10 114.9 5.10 99.22

7.52 119.7 7.52 112.9 7.52 148.5 7.52 127.03

10.00 141.3 10.00 133.2 10.00 173 10.00 149.17

12.41 162.6 12.41 153.2 12.41 196.6 12.41 170.80

14.90 183.3 14.90 172.8 14.90 218 14.90 191.37

17.31 202.7 17.38 190.7 17.31 239.6 17.33 211.00

19.79 221.5 19.79 208.2 19.79 257.7 19.79 229.13

22.21 239 22.21 224 22.28 275 22.23 246.00

24.69 256 24.69 239.8 24.69 291.9 24.69 262.57

27.10 272.8 27.10 254.8 27.10 309.1 27.10 278.90

29.59 288.6 29.59 268.4 29.59 324.6 29.59 293.87

32.00 302.1 32.00 280.9 32.00 339.8 32.00 307.60

34.48 316.7 34.48 293.4 34.48 349.8 34.48 319.97

34.48 310.4 34.48 289.4 34.48 347.9 34.48 315.90

32.69 295.5 32.62 275 32.69 330.3 32.67 300.27

30.90 283.7 30.90 262.2 30.90 309.1 30.90 285.00

29.03 268.7 29.03 248.1 29.03 292.4 29.03 269.73

27.24 255.5 27.24 236.6 27.24 279.1 27.24 257.07

25.45 241.6 25.45 223.1 25.45 260.9 25.45 241.87

23.66 227.5 23.66 210.6 23.66 246.7 23.66 228.27

21.86 213 21.86 196.4 21.86 230 21.86 213.13

20.07 199.5 20.07 184 20.07 214 20.07 199.17

18.28 183 18.21 170.4 18.21 201.4 18.23 184.93

16.41 168.7 16.41 157.6 16.41 185.1 16.41 170.47

14.62 156.3 14.62 143.9 14.62 166.9 14.62 155.70

12.83 141 12.83 129.7 12.83 151.8 12.83 140.83

11.03 126.4 11.03 117.1 11.03 134.1 11.03 125.87

9.24 110.9 9.24 102 9.24 118.5 9.24 110.47

7.38 95.55 7.45 88.3 7.45 100.5 7.43 94.78

5.60 78.47 5.61 73.01 5.61 84.18 5.61 78.55

3.81 62.02 3.81 57.29 3.82 65.84 3.81 61.72

2.00 44.4 2.02 41.42 2.01 45.78 2.01 43.87

0.20 23.98 0.21 22.5 0.21 24.26 0.21 23.58

Average Stdev

YS 32.3 29.6 30.9 30.9 1.4

VS 8.2 7.6 9.1 8.3 0.8

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 481 572 1184 746 382

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 30

Set C3: CS-BX3 – BL30- L1 – 3 day – NIST code (folder SR 46-SR-44A)

SR-44A

Run# K Run# M Run# N Average

SR SS SR SS SR SS SR SS

0.28 26.45 0.20 32.94 0.20 40.73 0.23 33.37

2.65 58.31 2.64 57.33 2.65 87.18 2.65 67.61

5.08 75.69 5.10 75.47 4.06 120 4.75 90.39

7.59 91.88 7.52 92.52 7.59 154.4 7.56 112.93

10.00 108.1 10.00 109.2 10.00 182.6 10.00 133.30

12.41 124 12.41 125.8 12.41 207.9 12.41 152.57

14.90 139.4 14.90 142.4 14.90 232.2 14.90 171.33

17.38 155.7 17.31 158.2 17.38 253.7 17.36 189.20

19.79 170.4 19.79 174.1 19.79 274.4 19.79 206.30

22.21 185.7 22.21 189.1 22.21 292.6 22.21 222.47

24.69 200.1 24.69 203.9 24.69 310.2 24.69 238.07

27.10 214.2 27.10 219.2 27.10 328.8 27.10 254.07

29.59 228.8 29.59 232.6 29.59 344.4 29.59 268.60

32.00 242 32.00 246.5 32.00 361.1 32.00 283.20

34.48 253.8 34.48 258.3 34.48 375.3 34.48 295.80

34.48 253.6 34.48 258.3 34.48 372.2 34.48 294.70

32.69 241.7 32.69 246.4 32.62 353.9 32.67 280.67

30.90 228.9 30.90 233.1 30.90 335.4 30.90 265.80

29.03 217.5 29.03 221.8 29.03 317.5 29.03 252.27

27.24 207.4 27.24 211.5 27.24 301.9 27.24 240.27

25.45 195.5 25.45 199.4 25.45 284.2 25.45 226.37

23.66 185.1 23.66 188.8 23.66 268.3 23.66 214.07

21.86 173.2 21.86 177.3 21.86 250.6 21.86 200.37

20.07 162.1 20.07 165.7 20.07 234.1 20.07 187.30

18.21 151.8 18.21 155.4 18.21 218.2 18.21 175.13

16.41 140.5 16.41 115.1 16.41 201.4 16.41 152.33

14.62 127.9 14.62 131.3 14.62 183 14.62 147.40

12.83 116.3 12.83 120 12.83 165.9 12.83 134.07

11.03 104.9 11.03 107.2 11.03 148.6 11.03 120.23

9.24 92.48 9.24 95.57 9.24 130.4 9.24 106.15

7.45 80.3 7.38 82.27 7.45 112.4 7.43 91.66

5.61 67.88 5.60 69.87 5.61 93.75 5.61 77.17

3.81 54.53 3.81 56.39 3.81 73.99 3.81 61.64

2.01 40.59 2.01 41.5 2.01 53.57 2.01 45.22

0.21 24.33 0.20 24.72 0.20 30.46 0.20 26.50

Average Stdev

YS 30.4 30.2 37.8 32.8 4.3

VS 6.5 6.6 9.7 7.6 1.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 295 339 1059 564 429

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# K

Run# M

Run# N
B - 31

Set C3: CS-BX3 – BL3- L1 – 3 day – NIST code (folder SR 46-SR-44B)

SR-44B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.26 11.93 0.21 18.54 0.21 16.43 0.23 15.63

2.63 23.96 2.65 32.42 2.65 27.97 2.64 28.12

5.10 28.86 5.10 39.83 5.10 33.2 5.10 33.96

7.52 33 7.52 44.58 7.52 38.11 7.52 38.56

10.00 37.5 10.00 49.25 10.00 42.2 10.00 42.98

12.41 41.62 12.41 53.83 12.41 46.07 12.41 47.17

14.90 45.43 14.90 58.5 14.90 49.98 14.90 51.30

17.31 48.93 17.31 63.33 17.31 53.51 17.31 55.26

19.79 52.38 19.79 67.84 19.79 57.45 19.79 59.22

22.21 55.65 22.21 72.19 22.21 61.16 22.21 63.00

24.69 58.93 24.69 76.6 24.69 65.04 24.69 66.86

27.17 62.06 27.10 81.1 27.10 69.02 27.13 70.73

29.59 65.31 29.59 85.39 29.59 72.75 29.59 74.48

32.00 68.63 32.00 89.66 32.00 76.8 32.00 78.36

34.48 71.89 34.48 93.77 34.48 80.78 34.48 82.15

34.48 71.83 34.48 93.58 34.48 80.47 34.48 81.96

32.69 69.2 32.69 89.76 32.69 77.43 32.69 78.80

30.83 66.46 30.83 86.01 30.83 74.61 30.83 75.69

29.03 63.71 29.03 82.51 29.10 71.77 29.06 72.66

27.24 61.38 27.24 79.19 27.24 68.8 27.24 69.79

25.45 58.69 25.45 75.61 25.45 65.81 25.45 66.70

23.66 56.23 23.66 72.3 23.66 62.95 23.66 63.83

21.86 53.35 21.86 68.73 21.86 60.01 21.86 60.70

20.07 50.87 20.07 65.22 20.07 56.96 20.07 57.68

18.21 48.37 18.21 61.84 18.28 53.78 18.23 54.66

16.41 45.64 16.41 58.26 16.41 50.7 16.41 51.53

14.62 42.51 14.62 54.39 14.62 38.29 14.62 45.06

12.83 39.8 12.83 50.59 12.83 44.62 12.83 45.00

11.03 36.99 11.03 46.89 11.03 41.25 11.03 41.71

9.24 33.82 9.24 42.77 9.17 37.84 9.22 38.14

7.45 30.64 7.45 38.71 7.38 34.08 7.43 34.48

5.60 27.66 5.60 34.18 5.59 30.28 5.60 30.71

3.82 24.11 3.81 29.5 3.81 26.31 3.81 26.64

2.01 20.08 2.00 24.54 1.99 21.93 2.00 22.18

0.21 13.56 0.20 16.65 0.21 14.85 0.20 15.02

Average Stdev

YS 18.0 21.8 19.0 19.6 1.9

VS 1.6 2.1 1.8 1.8 0.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 50 111 65 75 32.1

0

10

20

30

40

50

60

70

80

90

100

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 32

Set C3: CS-BX3 – BL3- L2 – 3 day – NIST code (folder SR 46-SR-44C)

SR-44C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 41.75 0.20 33.85 0.21 33.67 0.20 36.42

2.63 92.66 2.65 64.25 2.64 62.01 2.64 72.97

5.10 142.9 5.10 86.09 5.10 82.4 5.10 103.80

7.52 187.5 7.52 108.5 7.52 100.2 7.52 132.07

10.00 219.7 10.00 129 10.00 118.2 10.00 155.63

12.41 248.5 12.41 147.5 12.41 136.1 12.41 177.37

14.90 271.1 14.90 165.7 14.90 153.7 14.90 196.83

17.31 283.9 17.31 183.6 17.31 170.7 17.31 212.73

19.79 299 19.79 200.7 19.79 187.9 19.79 229.20

22.21 318.5 22.21 217 22.21 204 22.21 246.50

24.69 336.1 24.69 233.2 24.69 220.1 24.69 263.13

27.10 348.7 27.10 249.4 27.17 235.1 27.13 277.73

29.59 368.5 29.59 265 29.59 250.2 29.59 294.57

32.00 381.4 32.00 279.5 32.00 264.8 32.00 308.57

34.48 401.4 34.48 292.9 34.48 279.3 34.48 324.53

34.48 392 34.48 290.4 34.48 277.4 34.48 319.93

32.69 372.6 32.69 276.2 32.69 264.6 32.69 304.47

30.90 354.3 30.90 263.1 30.83 252.2 30.87 289.87

29.03 333.8 29.10 249.8 29.03 239.7 29.06 274.43

27.24 320.7 27.24 237.8 27.24 227.8 27.24 262.10

25.45 299.3 25.45 224.1 25.45 214.9 25.45 246.10

23.66 284.3 23.66 211.5 23.66 202.8 23.66 232.87

21.86 262.6 21.86 198 21.86 189.9 21.86 216.83

20.07 245.5 20.07 184.9 20.07 177.4 20.07 202.60

18.21 229.5 18.21 171.3 18.28 165.1 18.23 188.63

16.41 211.5 16.41 158.1 16.41 152.3 16.41 173.97

14.62 191.1 14.62 145 14.62 139.4 14.62 158.50

12.83 173 12.83 105.1 12.83 126.7 12.83 134.93

11.03 155.1 11.03 118 11.03 113.5 11.03 128.87

9.24 135.5 9.24 103.7 9.24 100.2 9.24 113.13

7.38 116.1 7.45 89.51 7.38 86.29 7.40 97.30

5.60 96.62 5.59 74.78 5.61 72.49 5.60 81.30

3.81 75.96 3.81 59.73 3.82 58.14 3.82 64.61

2.02 54.13 1.99 43.49 2.01 42.44 2.01 46.69

0.20 28.97 0.20 25.25 0.20 24.76 0.20 26.33

Average Stdev

YS 37.3 29.4 31.2 32.6 4.1

VS 10.3 7.6 7.2 8.4 1.7

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1349 477 297 708 563

0

50

100

150

200

250

300

350

400

450

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 33

Set C3: CS-BX3 – BL30- L2 – 3 day – NIST code (folder SR 46-SR-44D)

SR-44D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 23.22 0.20 27.58 0.19 28.18 0.20 26.33

2.64 47.56 2.65 58.5 2.64 64.12 2.64 56.73

5.10 67.39 5.08 82.8 5.08 91.87 5.09 80.69

7.52 85.44 7.52 105.8 7.52 118.2 7.52 103.15

10.00 102.6 10.00 127.5 10.00 139.4 10.00 123.17

12.41 117.7 12.41 147.6 12.41 159 12.41 141.43

14.90 132.9 14.90 166.9 14.90 177.7 14.90 159.17

17.31 147.3 17.38 185.7 17.38 195.8 17.36 176.27

19.79 162 19.79 203.6 19.79 212.9 19.79 192.83

22.21 174.3 22.21 221.4 22.21 231.2 22.21 208.97

24.69 187.9 24.69 238.2 24.69 247.6 24.69 224.57

27.17 202.8 27.10 253.5 27.10 261.4 27.13 239.23

29.59 213.4 29.59 268.6 29.59 276.8 29.59 252.93

32.00 228.2 32.07 226.9 32.00 290.1 32.02 248.40

34.48 239.4 34.48 299 34.48 306.9 34.48 281.77

34.48 239.6 34.48 295.1 34.48 300.2 34.48 278.30

32.69 228.4 32.69 280.9 32.69 285.1 32.69 264.80

30.83 215.4 30.83 266.8 30.90 274.2 30.85 252.13

29.03 206.2 29.03 253.9 29.03 259.5 29.03 239.87

27.24 192.9 27.24 237.8 27.24 244.2 27.24 224.97

25.45 183.4 25.45 224.9 25.45 232.2 25.45 213.50

23.66 171.7 23.66 210.3 23.66 216.5 23.66 199.50

21.86 163.5 21.86 198.4 21.86 204.2 21.86 188.70

20.07 151.6 20.07 184 20.07 190.5 20.07 175.37

18.28 142 18.21 169.9 18.21 174.3 18.23 162.07

16.41 130.8 16.41 156 16.41 160.2 16.41 149.00

14.62 119.3 14.62 142.9 14.62 147.9 14.62 136.70

12.83 108.6 12.83 128.7 12.83 133 12.83 123.43

11.03 95.58 11.03 113.9 11.03 119.2 11.03 109.56

9.24 85.25 9.24 100.3 9.24 103.8 9.24 96.45

7.45 72.43 7.45 85.55 7.45 89.04 7.45 82.34

5.61 60.55 5.61 70.59 5.61 72.44 5.61 67.86

3.81 47.72 3.81 55.25 3.81 56.48 3.81 53.15

2.01 33.54 2.01 38.94 2.01 39.94 2.01 37.47

0.21 18.17 0.20 20.6 0.20 20.69 0.20 19.82

Average Stdev

YS 24.5 25.5 27.3 25.8 1.4

VS 6.3 7.9 8.0 7.4 1.0

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 328 313 512 385 111

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 34

Set C7: CS-BX3 – BL30- L1 – 7 day – NIST code (folder SR 47-SR-44A)

SR-44A

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 49.15 0.19 33.64 0.21 33.31 0.20 38.70

2.64 111.9 2.64 58.53 2.65 58.15 2.64 76.19

5.08 160 5.10 76.71 5.10 78.96 5.09 105.22

7.52 206.7 7.52 93.84 7.52 96.77 7.52 132.44

10.00 237.5 10.00 111.1 10.00 113.8 10.00 154.13

12.41 266.7 12.41 128.3 12.48 131 12.44 175.33

14.90 288.6 14.90 144.8 14.90 149.4 14.90 194.27

17.31 315 17.31 161.9 17.31 166.2 17.31 214.37

19.79 333.3 19.79 177.9 19.79 183.4 19.79 231.53

22.28 357.5 22.28 193.4 22.21 196.5 22.25 249.13

24.69 376 24.69 208.4 24.69 211.3 24.69 265.23

27.10 385.8 27.10 222.7 27.17 229.9 27.13 279.47

29.59 410.1 29.59 237.1 29.59 241.5 29.59 296.23

32.00 416.8 32.00 249.1 32.00 257.5 32.00 307.80

34.48 440.2 34.48 261.1 34.48 266 34.48 322.43

34.41 415.6 34.48 257.4 34.48 269.7 34.46 314.23

32.62 393.1 32.62 244.4 32.69 258 32.64 298.50

30.90 383.5 30.90 234.5 30.83 240.3 30.87 286.10

29.10 354.7 29.03 221.3 29.03 230 29.06 268.67

27.24 346.8 27.24 212.1 27.24 217.5 27.24 258.80

25.45 318.5 25.45 199.8 25.45 204.8 25.45 241.03

23.66 307.1 23.66 189.2 23.66 194.1 23.66 230.13

21.86 276.9 21.86 175.4 21.86 183.2 21.86 211.83

20.07 261.4 20.07 165.1 20.07 170.2 20.07 198.90

18.21 243.3 18.21 152.9 18.21 162.3 18.21 186.17

16.41 225.2 16.41 141.7 16.41 149.9 16.41 172.27

14.62 202 14.62 129.6 14.62 135.1 14.62 155.57

12.83 181.1 12.83 116.8 12.83 124.7 12.83 140.87

11.03 165.9 11.03 106.7 11.03 109.7 11.03 127.43

9.24 142 9.24 92.65 9.24 98.83 9.24 111.16

7.45 123.3 7.45 81.02 7.45 84.03 7.45 96.12

5.60 102 5.61 67.38 5.60 72.17 5.60 80.52

3.79 79.64 3.81 53.54 3.82 57.99 3.81 63.72

2.01 57.57 2.01 40.3 2.01 41.66 2.01 46.51

0.20 31.12 0.21 24.09 0.20 25.08 0.20 26.76

Average Stdev

YS 38.5 29.5 31.9 33.3 4.7

VS 11.1 6.7 6.9 8.2 2.5

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1301 298 470 690 536

0

50

100

150

200

250

300

350

400

450

500

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 35

Set C7: CS-BX3 – BL3- L1 – 7 day – NIST code (folder SR 47-SR-44B)

SR-44B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 14.89 0.21 16.07 0.20 16.15 0.23 15.70

2.65 32.13 2.63 26.05 2.64 25.53 2.64 27.90

5.10 38.02 5.10 32.27 5.10 30.37 5.10 33.55

7.52 42.75 7.52 38.01 7.52 34.68 7.52 38.48

10.00 46.95 10.00 43.27 10.00 38.16 10.00 42.79

12.41 51.24 12.41 48.57 12.41 41.36 12.41 47.06

14.90 55.28 14.90 53.98 14.90 44.58 14.90 51.28

17.31 59.68 17.38 59.08 17.31 47.92 17.33 55.56

19.79 63.66 19.79 64.04 19.79 51.01 19.79 59.57

22.21 54.33 22.28 68.98 22.21 54.39 22.23 59.23

24.69 71.93 24.69 73.84 24.69 58.11 24.69 67.96

27.17 75.96 27.17 78.55 27.17 62.27 27.17 72.26

29.59 80.38 29.59 83.23 29.59 65.77 29.59 76.46

32.00 84.12 32.00 87.81 32.00 69.97 32.00 80.63

34.48 88.19 34.48 92.87 34.48 73.41 34.48 84.82

34.48 87.81 34.48 92.52 34.48 74.32 34.48 84.88

32.69 84.38 32.69 88.96 32.69 72.03 32.69 81.79

30.83 81.08 30.83 68.65 30.83 68.98 30.83 72.90

29.03 77.75 29.03 82.08 29.03 66.62 29.03 75.48

27.24 74.63 27.24 78.79 27.24 64.42 27.24 72.61

25.45 71.1 25.45 75.45 25.45 61.84 25.45 69.46

23.66 68 23.66 71.86 23.66 59.58 23.66 66.48

21.86 64.64 21.86 68.26 21.86 56.85 21.86 63.25

20.07 61.17 20.07 64.96 20.07 54.39 20.07 60.17

18.28 57.93 18.28 61.44 18.28 52.18 18.28 57.18

16.41 54.53 16.41 57.85 16.41 49.38 16.41 53.92

14.62 50.96 14.62 54.09 14.62 46.18 14.62 50.41

12.83 47.36 12.83 50.53 12.83 43.52 12.83 47.14

11.03 43.5 11.03 46.89 11.03 40.15 11.03 43.51

9.24 40.01 9.24 42.73 9.24 37.08 9.24 39.94

7.45 35.87 7.38 38.62 7.38 33.22 7.40 35.90

5.61 31.76 5.61 34.2 5.61 29.91 5.61 31.96

3.81 27.4 3.81 29.58 3.82 25.9 3.82 27.63

2.02 22.56 2.01 24.56 2.00 21.14 2.01 22.75

0.20 15.19 0.21 16.66 0.20 14.58 0.20 15.48

Average Stdev

YS 19.9 22.9 20.3 21.0 1.6

VS 2.0 2.0 1.6 1.9 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 76 3 5 28 42

0

10

20

30

40

50

60

70

80

90

100

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 36

Set C7: CS-BX3 – BL3- L2 – 7 day – NIST code (folder SR 47-SR-44C)

SR-44C

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 34.26 0.20 27.14 0.20 47.65 0.20 36.35

2.63 73.36 2.65 48.71 2.66 103.7 2.65 75.26

5.10 105.5 5.10 65.51 5.09 159.2 5.09 110.07

7.52 139.2 7.52 81.33 7.59 204.6 7.54 141.71

10.00 163.1 10.00 96.67 10.00 241.1 10.00 166.96

12.41 186.3 12.41 111.7 12.41 277.1 12.41 191.70

14.90 204.2 14.90 126 14.90 309.8 14.90 213.33

17.38 218.3 17.31 141.5 17.38 340.1 17.36 233.30

19.79 234.6 19.79 154.8 19.79 366 19.79 251.80

22.21 252.2 22.21 170.2 22.21 392 22.21 271.47

24.69 269.2 24.69 184.1 24.69 418.5 24.69 290.60

27.17 285.3 27.10 196 27.10 448.4 27.13 309.90

29.59 302.3 29.59 210.7 29.59 469.8 29.59 327.60

32.00 317.1 32.00 221.5 32.00 494.5 32.00 344.37

34.48 332.1 34.48 236.1 34.48 511.4 34.48 359.87

34.48 328.7 34.48 230.7 34.48 512.4 34.48 357.27

32.69 313 32.69 219.9 32.62 487.5 32.67 340.13

30.90 297.3 30.90 213.4 30.90 457.2 30.90 322.63

29.03 282 29.10 202.7 29.03 432.2 29.06 305.63

27.24 269.2 27.24 191.3 27.24 411 27.24 290.50

25.45 252.8 25.45 182.4 25.45 384.9 25.45 273.37

23.66 239.3 23.66 170.6 23.66 364.1 23.66 258.00

21.86 222.9 21.86 161.5 21.86 338.4 21.86 240.93

20.07 208.4 20.00 151.2 20.07 314.2 20.05 224.60

18.21 194.5 18.28 138 18.21 294.5 18.23 209.00

16.41 179.4 16.41 127.6 16.41 270.6 16.41 192.53

14.62 162.9 14.62 119.4 14.62 243.1 14.62 175.13

12.83 147.7 12.83 108 12.83 219.8 12.83 158.50

11.03 132.2 11.03 96.74 11.03 195.5 11.03 141.48

9.24 116.1 9.24 85.62 9.24 169.4 9.24 123.71

7.45 99.45 7.45 73.89 7.45 143.9 7.45 105.75

5.61 82.92 5.61 61.27 5.61 118.5 5.61 87.56

3.82 65.32 3.81 49.16 3.80 90.32 3.81 68.27

2.01 46.6 1.99 35.94 2.02 60.98 2.01 47.84

0.20 25.46 0.20 21.21 0.19 28.25 0.20 24.97

Average Stdev

YS 33.4 27.5 38.8 33.3 5.7

VS 8.6 6.0 13.7 9.5 3.9

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 772 30 1558 787 764

0

100

200

300

400

500

600

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 37

Set C7: CS-BX3 – BL30- L2 – 7 day – NIST code (folder SR 47-SR-44D)

SR-44D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 21.88 0.21 28.07 0.20 30.64 0.21 26.86

2.65 46.86 2.66 71.07 2.65 73.76 2.65 63.90

5.08 66.15 5.10 107.4 5.10 108 5.09 93.85

7.59 83.98 7.52 144.5 7.52 140.8 7.54 123.09

10.00 101.1 10.00 177.1 10.00 166.2 10.00 148.13

12.41 118.3 12.41 207 12.41 189.8 12.41 171.70

14.90 134.9 14.90 232.5 14.90 208.9 14.90 192.10

17.38 151.9 17.31 257.9 17.31 228.4 17.33 212.73

19.79 167.6 19.79 278.2 19.79 242.9 19.79 229.57

22.21 183.8 22.21 294.7 22.21 264 22.21 247.50

24.69 198.8 24.69 307.1 24.69 280.7 24.69 262.20

27.10 212 27.10 318.3 27.10 289.5 27.10 273.27

29.59 227.2 29.59 331.9 29.59 308.6 29.59 289.23

32.00 240 32.00 343.5 32.00 316.9 32.00 300.13

34.48 255.4 34.48 358 34.48 339.7 34.48 317.70

34.48 252.4 34.48 350 34.48 324.3 34.48 308.90

32.69 241 32.69 331.5 32.69 306.8 32.69 293.10

30.90 231.6 30.83 315.2 30.90 300.2 30.87 282.33

29.03 219.7 29.03 298.7 29.10 282.3 29.06 266.90

27.24 207.5 27.24 279.9 27.24 265.6 27.24 251.00

25.45 197.3 25.45 265.4 25.45 253.2 25.45 238.63

23.66 184.7 23.66 247.7 23.66 234.6 23.66 222.33

21.86 174.2 21.86 233.6 21.86 221.1 21.86 209.63

20.07 162.5 20.00 216.7 20.07 206.7 20.05 195.30

18.21 149.6 18.28 200.1 18.28 185.4 18.25 178.37

16.41 137.9 16.41 183.6 16.41 170.2 16.41 163.90

14.62 126.8 14.62 167.9 14.62 160 14.62 151.57

12.83 114.4 12.83 151.2 12.83 142.7 12.83 136.10

11.03 101.9 11.03 133.9 11.03 127.4 11.03 121.07

9.24 89.4 9.24 117 9.24 111 9.24 105.80

7.45 76.66 7.45 99.36 7.45 94.9 7.45 90.31

5.61 63.02 5.61 81.08 5.60 75.95 5.61 73.35

3.81 49.35 3.81 62.41 3.81 58.98 3.81 56.91

2.01 34.92 1.99 42.63 1.99 40.82 2.00 39.46

0.21 18.14 0.20 20.94 0.20 20.51 0.20 19.86

Average Stdev

YS 25.0 27.5 27.0 26.5 1.3

VS 6.7 9.4 8.8 8.3 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 101 1198 675 658 549

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 38

Set D1: CS-BX5 – BL11- L2 – Mixing Day – NIST code (folder SR 49-SR-48A)

SR-48A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.21 49.19 0.20 35.38 0.21 42.46 0.21 42.34

2.65 111.4 2.66 57.63 2.64 75.44 2.65 81.49

5.10 161.8 5.08 75.93 5.10 102.6 5.09 113.44

7.52 219.3 7.52 93.73 7.52 129.4 7.52 147.48

10.00 253.7 10.00 110.5 10.00 152.1 10.00 172.10

12.48 284.8 12.41 127.1 12.41 173.3 12.44 195.07

14.90 310.6 14.90 143.9 14.90 192.9 14.90 215.80

17.31 333.9 17.38 160 17.31 212.8 17.33 235.57

19.79 348.7 19.79 175.8 19.79 230.8 19.79 251.77

22.21 374.8 22.21 191 22.28 249.7 22.23 271.83

24.69 396.2 24.69 206.2 24.69 266.6 24.69 289.67

27.10 410 27.10 221.5 27.10 283.1 27.10 304.87

29.59 439.2 29.59 236 29.59 299.9 29.59 325.03

32.00 447.1 32.07 250.5 32.00 313.8 32.02 337.13

34.48 474 34.48 263.9 34.48 328 34.48 355.30

34.48 449 34.48 263.2 34.48 323.3 34.48 345.17

32.69 427 32.69 251.8 32.69 308 32.69 328.93

30.90 422.6 30.90 239.9 30.90 296.4 30.90 319.63

29.10 397.1 29.03 228.8 29.03 280.2 29.06 302.03

27.24 377.6 27.24 217.6 27.24 268.7 27.24 287.97

25.45 359.8 25.45 206.3 25.45 253.5 25.45 273.20

23.66 336.7 23.66 195.1 23.66 240.3 23.66 257.37

21.86 315.6 21.86 183.6 21.86 223.3 21.86 240.83

20.07 298 20.07 172.2 20.07 210.3 20.07 226.83

18.21 265.8 18.21 160.8 18.28 195.2 18.23 207.27

16.41 245.9 16.41 149.1 16.41 180.5 16.41 191.83

14.62 234.4 14.62 136.5 14.62 165.7 14.62 178.87

12.83 210.2 12.83 124.6 12.83 149.5 12.83 161.43

11.03 189.8 11.03 112.2 11.03 136 11.03 146.00

9.24 166 9.24 99.42 9.24 118.5 9.24 127.97

7.38 143.8 7.45 86.32 7.45 103.1 7.43 111.07

5.61 115.8 5.62 73.06 5.60 85.58 5.61 91.48

3.81 91.67 3.80 58.84 3.82 68.27 3.81 72.93

1.99 65.04 2.01 43.66 2.02 50.01 2.01 52.90

0.20 35.54 0.20 26.7 0.19 29.1 0.20 30.45

Average Stdev

YS 50.0 34.6 38.2 40.9 8.1

VS 12.0 6.7 8.4 9.0 2.7

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 946 156 529 544 395

0

50

100

150

200

250

300

350

400

450

500

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 39

Set D1: CS-BX5 – BL36- L1 – Mixing Day – NIST code (folder SR 49-SR-48B)

SR-48B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 29.36 0.20 32.12 0.19 27.99 0.20 29.82

2.63 57.83 2.64 63.62 2.63 53.53 2.64 58.33

5.10 78.62 5.10 88.3 5.10 71.41 5.10 79.44

7.52 105.6 7.52 114.8 7.52 87.86 7.52 102.75

10.00 127.7 10.00 131.7 10.00 104.3 10.00 121.23

12.41 148.9 12.41 149.4 12.48 119.3 12.44 139.20

14.90 169.1 14.90 167.5 14.90 133.4 14.90 156.67

17.31 186.9 17.31 184.5 17.31 148.5 17.31 173.30

19.79 203.5 19.79 200.8 19.79 161.9 19.79 188.73

22.21 217.3 22.28 215.8 22.28 175.5 22.25 202.87

24.69 231.4 24.69 230.8 24.69 188.6 24.69 216.93

27.17 246.3 27.10 247.4 27.10 202 27.13 231.90

29.59 256.5 29.59 260.7 29.59 215 29.59 244.07

32.00 268.8 32.00 274.3 32.00 227.2 32.00 256.77

34.48 278 34.48 282.9 34.48 236.9 34.48 265.93

34.48 276.5 34.48 284.1 34.48 236.4 34.48 265.67

32.69 262.3 32.69 270.2 32.69 225.2 32.69 252.57

30.83 245.6 30.90 252.1 30.90 212.8 30.87 236.83

29.03 234.6 29.03 240.3 29.03 202 29.03 225.63

27.24 219.4 27.24 228.5 27.24 193.2 27.24 213.70

25.45 208.1 25.45 214.6 25.45 181.4 25.45 201.37

23.66 195 23.66 203.6 23.66 172 23.66 190.20

21.86 186 21.86 190.8 21.86 160.4 21.86 179.07

20.07 172.7 20.07 177.4 20.07 150.1 20.07 166.73

18.28 161.5 18.28 167.5 18.21 141.1 18.25 156.70

16.41 149 16.41 154.5 16.41 130.4 16.41 144.63

14.62 136.6 14.62 139.8 14.62 118.1 14.62 131.50

12.83 124.2 12.83 127.6 12.83 107.4 12.83 119.73

11.03 109.3 11.03 112.7 11.03 95.84 11.03 105.95

9.24 97.99 9.24 100.5 9.24 84.92 9.24 94.47

7.38 83.36 7.45 85.53 7.38 72.89 7.40 80.59

5.61 69.92 5.60 72.23 5.61 61.54 5.60 67.90

3.81 55.4 3.82 57.08 3.82 48.94 3.82 53.81

2.01 38.99 2.01 40.19 2.01 35.02 2.01 38.07

0.20 21.58 0.19 22.29 0.20 20.12 0.20 21.33

Average Stdev

YS 28.4 29.3 26.1 28.0 1.7

VS 7.1 7.4 6.1 6.9 0.7

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 722 741 381 615 202

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 40

Set D1: CS-BX5 – BL11- L1 – Mixing Day – NIST code (folder SR 49-SR-48C)

SR-48C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 43.53 0.20 39.4 0.20 39.78 0.20 40.90

2.65 93.52 2.65 75.85 2.65 79.57 2.65 82.98

5.10 141.4 5.10 108.5 5.10 106.9 5.10 118.93

7.52 185.4 7.52 140.3 7.52 138.1 7.52 154.60

10.00 216.9 10.00 164.9 10.00 163.1 10.00 181.63

12.41 246.5 12.41 187.3 12.41 186.2 12.41 206.67

14.90 275.1 14.90 207.5 14.90 209.3 14.90 230.63

17.31 296.4 17.31 228.7 17.31 230.2 17.31 251.77

19.79 319.2 19.79 247.4 19.79 250.8 19.79 272.47

22.21 332.4 22.21 268 22.28 269 22.23 289.80

24.69 350.4 24.69 285.5 24.69 287 24.69 307.63

27.10 377.1 27.10 297.7 27.17 306.8 27.13 327.20

29.59 393.2 29.59 314.6 29.59 322.4 29.59 343.40

32.00 412.9 32.00 327.2 32.00 339.8 32.00 359.97

34.48 419.7 34.48 347.3 34.48 350.8 34.48 372.60

34.41 419.4 34.48 338.7 34.48 352 34.46 370.03

32.69 398.1 32.69 323.2 32.69 335.1 32.69 352.13

30.90 377.1 30.83 311.3 30.90 315.3 30.87 334.57

29.10 355.1 29.03 296.4 29.03 300.6 29.06 317.37

27.24 346 27.24 276.9 27.24 288.4 27.24 303.77

25.45 322.8 25.45 265.1 25.45 270.2 25.45 286.03

23.66 307.9 23.66 246.6 23.66 257.1 23.66 270.53

21.86 282.4 21.86 235.4 21.86 238.8 21.86 252.20

20.07 266.6 20.00 218.7 20.07 223.5 20.05 236.27

18.21 244.5 18.28 202 18.28 210.3 18.25 218.93

16.41 226 16.41 186.3 16.41 193.9 16.41 202.07

14.62 207.4 14.62 171.9 14.62 175.2 14.62 184.83

12.83 185.3 12.83 156 12.83 159.5 12.83 166.93

11.03 169.6 11.03 137.7 11.03 142.4 11.03 149.90

9.24 145.5 9.17 122.5 9.24 125.3 9.22 131.10

7.45 126.3 7.38 104.4 7.45 107.2 7.43 112.63

5.61 101.9 5.61 87.01 5.61 89.81 5.61 92.91

3.81 79.52 3.81 68.46 3.81 70.85 3.81 72.94

2.00 57.02 1.99 47.97 2.01 49.98 2.00 51.66

0.21 29.59 0.20 26.42 0.21 27.3 0.21 27.77

Average Stdev

YS 39.9 36.1 37.0 37.7 2.0

VS 11.1 8.9 9.2 9.8 1.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 1493 594 842 976 464

0

50

100

150

200

250

300

350

400

450

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 41

Set D1: CS-BX5 – BL36- L2 – Mixing Day – NIST code (folder SR 49-SR-48D)

SR-48D

Run# J Run# K Run# M Average

SR SS SR SS SR SS SR SS

0.20 37.07 0.19 32.35 0.21 31.87 0.20 33.76

2.64 69.64 2.65 57.1 2.63 64.66 2.64 63.80

5.10 91.97 5.10 76.69 5.10 87.66 5.10 85.44

7.52 116.5 7.59 96.97 7.52 109.7 7.54 107.72

10.00 136.6 10.00 113.9 10.00 129.1 10.00 126.53

12.41 156.2 12.41 130.4 12.41 146.8 12.41 144.47

14.90 176.8 14.90 147.2 14.90 165 14.90 163.00

17.38 193.9 17.38 162.6 17.31 181 17.36 179.17

19.79 212.6 19.79 178.1 19.79 198 19.79 196.23

22.21 226.8 22.21 190.7 22.21 211.9 22.21 209.80

24.69 242 24.69 203.9 24.69 227.3 24.69 224.40

27.17 259.7 27.10 218.9 27.17 243 27.15 240.53

29.59 272.5 29.59 230.2 29.59 255 29.59 252.57

32.00 288.6 32.00 242.9 32.00 269.7 32.00 267.07

34.48 299.1 34.48 250.9 34.48 281.9 34.48 277.30

34.48 301 34.48 251.2 34.48 280.3 34.48 277.50

32.69 286.9 32.62 238.8 32.69 266.4 32.67 264.03

30.83 270.3 30.90 224.7 30.83 255.9 30.85 250.30

29.03 258.8 29.03 213 29.03 243.7 29.03 238.50

27.24 244.3 27.24 204.9 27.24 227.2 27.24 225.47

25.45 231.5 25.45 192.1 25.45 217.7 25.45 213.77

23.66 217.8 23.66 182.8 23.66 202.4 23.66 201.00

21.86 207 21.86 169.5 21.86 192.2 21.86 189.57

20.07 193 20.07 159 20.07 179.6 20.07 177.20

18.21 180.7 18.21 149.6 18.28 164.8 18.23 165.03

16.41 166.7 16.41 138.5 16.41 151.8 16.41 152.33

14.62 153.5 14.62 125.1 14.62 140.6 14.62 139.73

12.83 139.2 12.83 113.4 12.83 126.9 12.83 126.50

11.03 124.1 11.03 102.8 11.03 113.9 11.03 113.60

9.24 110 9.24 89.83 9.24 100.1 9.24 99.98

7.38 94.92 7.45 78.16 7.38 86.45 7.40 86.51

5.61 78.92 5.61 65.61 5.60 71.44 5.61 71.99

3.81 62.69 3.81 51.98 3.82 56.89 3.81 57.19

2.01 45.03 2.01 38.5 2.01 41.19 2.01 41.57

0.21 25.59 0.20 22.4 0.20 23.26 0.20 23.75

Average Stdev

YS 34.7 28.3 29.8 31.0 3.4

VS 7.8 6.5 7.3 7.2 0.7

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 634 548 537 573 53

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# M
B - 42

Set D3: CS-BX5 – BL11- L2 – 3 day – NIST code (folder SR 50-SR-48A)

SR-48A

Run# G Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 29.44 0.21 34.11 0.20 39.4 0.20 34.32

2.63 50.18 2.65 67.47 2.64 81.05 2.64 66.23

5.10 66.09 5.10 92.42 5.09 110.3 5.10 89.60

7.52 81.5 7.52 119 7.52 144.3 7.52 114.93

10.00 95.8 10.00 140.2 10.00 164 10.00 133.33

12.41 110.3 12.41 160 12.48 183.8 12.44 151.37

14.90 125.2 14.90 179.1 14.90 203.2 14.90 169.17

17.38 139 17.31 196 17.31 222.2 17.33 185.73

19.79 153.2 19.79 213.9 19.79 239.6 19.79 202.23

22.21 165.9 22.21 229.9 22.28 258 22.23 217.93

24.69 178.5 24.69 245.3 24.69 274.7 24.69 232.83

27.17 192 27.10 260.9 27.10 291.3 27.13 248.07

29.59 203.2 29.59 273 29.59 309.2 29.59 261.80

32.00 216 32.00 288.3 32.00 321.4 32.00 275.23

34.48 226.9 34.48 298.9 34.48 336.7 34.48 287.50

34.48 227.5 34.48 298.9 34.48 328.2 34.48 284.87

32.69 217.3 32.69 284.4 32.62 311.7 32.67 271.13

30.83 205.8 30.83 266.1 30.90 301.8 30.85 257.90

29.03 196.1 29.03 253.4 29.03 284.2 29.03 244.57

27.24 186.1 27.24 240.7 27.24 271.8 27.24 232.87

25.45 176.3 25.45 225.9 25.45 256.6 25.45 219.60

23.66 166.2 23.66 213.9 23.66 241.8 23.66 207.30

21.86 156.7 21.86 199.4 17.52 224.7 20.41 193.60

20.07 146.4 20.07 185.9 20.07 211.3 20.07 181.20

18.21 136.8 18.21 175 18.21 193.3 18.21 168.37

16.41 126.3 16.41 161.3 16.41 178.6 16.41 155.40

14.62 115.7 14.62 145.4 14.62 164.8 14.62 141.97

12.83 105.6 12.83 132.1 12.83 147.6 12.83 128.43

11.03 94.26 11.03 118.1 11.03 134.3 11.03 115.55

9.24 83.93 9.24 103.5 9.24 116.2 9.24 101.21

7.38 72.21 7.45 89 7.45 101.2 7.43 87.47

5.61 60.96 5.60 74.81 5.62 82.77 5.61 72.85

3.82 49.19 3.81 59.08 3.80 65.07 3.81 57.78

2.01 36.36 1.99 42.48 2.02 47.79 2.01 42.21

0.20 21.85 0.19 24.06 0.21 26.85 0.20 24.25

Average Stdev

YS 27.7 29.7 35.8 31.1 4.2

VS 5.9 7.8 8.7 7.4 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 251 793 626 557 278

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# I

Run# J
B - 43

Set D3: CS-BX5 – BL36- L1 – 3 day – NIST code (folder SR 50-SR-48B)

SR-48B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.26 17.12 0.20 20.13 0.20 27.19 0.22 21.48

2.65 40 2.65 37.94 2.65 56.48 2.65 44.81

5.09 53.53 5.08 51.9 5.08 78.99 5.09 61.47

7.52 66.48 7.52 64.91 7.59 101.3 7.54 77.56

10.00 79.01 10.00 77.01 10.00 119.3 10.00 91.77

12.41 91.83 12.41 89.1 12.41 136.5 12.41 105.81

14.90 104.6 14.90 101.6 14.90 152.5 14.90 119.57

17.38 117.5 17.31 113.7 17.31 168.6 17.33 133.27

19.79 129.8 19.79 125.5 19.79 183.2 19.79 146.17

22.21 141.9 22.21 136.4 22.21 198.4 22.21 158.90

24.69 153.5 24.69 147.6 24.69 212.7 24.69 171.27

27.10 165.1 27.10 159.7 27.10 225.7 27.10 183.50

29.59 176.3 29.59 170.4 29.59 240.3 29.59 195.67

32.00 187.1 32.00 181.5 32.00 252 32.00 206.87

34.48 197 34.48 190.3 34.48 265.1 34.48 217.47

34.48 196.7 34.48 191.3 34.48 261.2 34.48 216.40

32.62 187.5 32.69 182.3 32.62 247.7 32.64 205.83

30.90 178.6 30.90 172.3 30.90 235.7 30.90 195.53

29.03 169.4 29.03 163.6 29.03 222.4 29.03 185.13

27.24 162 27.24 156.2 27.24 212.6 27.24 176.93

25.45 152.7 25.45 146.7 25.45 200 25.45 166.47

23.66 144.5 23.66 139.5 23.66 188.8 23.66 157.60

21.86 134.8 21.86 130.3 21.86 175.3 21.86 146.80

20.07 126.3 20.07 121.5 20.07 164.3 20.07 137.37

18.21 117.7 18.21 114.3 18.21 151.5 18.21 127.83

16.41 108.7 16.41 105.6 16.41 139.8 16.41 118.03

14.62 99.06 14.62 95.73 14.62 127.6 14.62 107.46

12.83 89.66 12.83 87.31 12.83 114.5 12.83 97.16

11.03 80.97 11.03 77.93 11.03 103.6 11.03 87.50

9.24 70.59 9.24 68.87 9.24 89.52 9.24 76.33

7.45 61.29 7.45 59.12 7.45 77.52 7.45 65.98

5.61 51.13 5.61 50.13 5.61 63.35 5.61 54.87

3.81 40.39 3.81 39.83 3.81 49.29 3.81 43.17

2.02 29.49 2.01 28.69 2.01 35.37 2.02 31.18

0.20 16.32 0.20 16.07 0.20 18.51 0.20 16.97

Average Stdev

YS 21.7 21.3 24.0 22.3 1.4

VS 5.1 5.0 6.9 5.7 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 130 175 487 264 195

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 44

Set D3: CS-BX5 – BL11- L1 – 3 day – NIST code (folder SR 50-SR-48C)

SR-48C

Run# K Run# L Run# N Average

SR SS SR SS SR SS SR SS

0.21 27.47 0.19 27.84 0.20 29.75 0.20 28.35

2.64 49.13 2.65 52.13 2.64 53.93 2.64 51.73

5.09 67.17 5.09 69.74 5.09 71.97 5.09 69.63

7.52 83.59 7.59 86.52 7.52 89.38 7.54 86.50

10.00 99.84 10.00 102.7 10.00 106.4 10.00 102.98

12.41 115.8 12.41 118.9 12.41 123.2 12.41 119.30

14.90 131.5 14.90 135.5 14.90 139.8 14.90 135.60

17.38 146.6 17.38 151.6 17.31 156.3 17.36 151.50

19.79 161.4 19.79 167.5 19.79 171.7 19.79 166.87

22.21 175.1 22.21 181.4 22.28 185.7 22.23 180.73

24.69 188.7 24.69 196 24.69 200.6 24.69 195.10

27.10 202.9 27.10 211.9 27.10 216.6 27.10 210.47

29.59 216.2 29.59 225.6 29.59 230.4 29.59 224.07

32.00 229 32.07 239.3 32.00 244.5 32.02 237.60

34.48 240.4 34.48 249.6 34.48 252.8 34.48 247.60

34.48 239.6 34.48 249.9 34.48 254.9 34.48 248.13

32.69 228.4 32.62 237.5 32.62 243.1 32.64 236.33

30.90 217 30.90 225.3 30.90 228 30.90 223.43

29.03 206 29.03 213.3 29.03 216.3 29.03 211.87

27.24 196.4 27.24 204.2 27.24 208.9 27.24 203.17

25.45 185.1 25.45 192 25.45 194.9 25.45 190.67

23.66 175.1 23.66 181.8 23.66 186.3 23.66 181.07

21.86 163.7 21.86 169 21.86 171.8 21.86 168.17

20.07 152.9 20.07 158.2 20.07 160.9 20.07 157.33

18.21 142.7 18.21 147 18.21 152 18.21 147.23

16.41 131.9 16.41 135.6 16.41 140.5 16.41 136.00

14.62 120.2 14.62 123.5 14.62 126.2 14.62 123.30

12.83 108.9 12.83 111.5 12.83 114.4 12.83 111.60

11.03 97.92 11.03 100.6 11.03 103.3 11.03 100.61

9.24 85.89 9.24 87.94 9.24 89.99 9.24 87.94

7.45 74.33 7.45 75.99 7.45 78.02 7.45 76.11

5.62 62.34 5.61 63.05 5.61 65.64 5.62 63.68

3.79 49.48 3.80 49.89 3.81 51.76 3.80 50.38

2.01 36.13 2.01 36.43 2.01 37.75 2.01 36.77

0.20 21.01 0.19 20.78 0.21 21.65 0.20 21.15

Average Stdev

YS 26.6 25.9 27.4 26.6 0.8

VS 6.2 6.5 6.6 6.5 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 245 318 407 323 81

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# K

Run# L

Run# N
B - 45

Set D3: CS-BX5 – BL36- L2 – 3 day – NIST code (folder SR 50-SR-48D)

SR-48D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 27.42 0.21 27.4 0.20 21.53 0.20 25.45

2.64 61.44 2.64 56.41 2.63 39.22 2.64 52.36

5.08 89.47 5.10 81.65 5.10 53.11 5.09 74.74

7.52 115.4 7.52 106 7.52 65.15 7.52 95.52

10.00 137.4 10.00 127.2 10.00 77.41 10.00 114.00

12.41 156.8 12.41 146.6 12.48 89.11 12.44 130.84

14.90 174.7 14.90 164.9 14.90 100.8 14.90 146.80

17.38 192.3 17.31 179.4 17.31 112.9 17.33 161.53

19.79 209.2 19.79 191 19.79 124.2 19.79 174.80

22.21 227 22.21 201.6 22.28 136.1 22.23 188.23

24.69 242.5 24.69 212.7 24.69 147.2 24.69 200.80

27.10 253.8 27.10 225.4 27.17 157.8 27.13 212.33

29.59 267.9 29.59 235.8 29.59 168.8 29.59 224.17

32.07 279.3 32.00 248.3 32.00 178.6 32.02 235.40

34.48 294.8 34.48 258.1 34.48 187.9 34.48 246.93

34.48 289.2 34.48 256.6 34.48 188.1 34.48 244.63

32.69 274.6 32.69 243.6 32.69 179.3 32.69 232.50

30.90 261.9 30.83 228.9 30.90 169.1 30.87 219.97

29.03 248.9 29.10 217.3 29.03 160.9 29.06 209.03

27.24 231.9 27.24 205.9 27.24 154 27.24 197.27

25.45 221 25.45 193.5 25.45 144.6 25.45 186.37

23.66 205.6 23.66 183.1 23.66 137.3 23.66 175.33

21.86 195.4 21.86 171 21.86 127.9 21.86 164.77

20.07 181.6 20.07 159.1 20.07 119.5 20.07 153.40

18.21 167.4 18.21 148.9 18.28 112.5 18.23 142.93

16.41 154 16.41 137.1 16.41 103.9 16.41 131.67

14.62 141.6 14.62 124.3 14.62 94.09 14.62 120.00

12.83 127.9 12.83 112.7 12.83 85.8 12.83 108.80

11.03 113.5 11.03 100.8 11.03 76.42 11.03 96.91

9.24 99.95 9.24 88.35 9.24 67.84 9.24 85.38

7.45 85.34 7.45 75.85 7.45 58.15 7.45 73.11

5.61 70.28 5.60 63.37 5.60 49.27 5.60 60.97

3.81 54.95 3.81 50.03 3.82 39.25 3.81 48.08

2.01 38.78 1.99 35.93 2.02 28.39 2.01 34.37

0.20 20.83 0.21 20.13 0.20 16.46 0.20 19.14

Average Stdev

YS 21.1 24.7 21.1 22.3 2.1

VS 4.9 6.7 4.9 5.5 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 187 798 187 391 352

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 46

Set D7: CS-BX5 – BL11- L2 – 7 day – NIST code (folder SR 51-SR-48A)

SR-48A

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.21 33.04 0.19 31.7 0.20 27.53 0.20 30.76

2.64 63.28 2.64 61.32 2.63 49.47 2.64 58.02

5.10 89.22 5.08 83 5.10 67.22 5.10 79.81

7.52 116.5 7.52 103.7 7.52 85.11 7.52 101.77

10.00 137 10.00 121.8 10.00 100.9 10.00 119.90

12.41 156.8 12.41 139.8 12.41 116 12.41 137.53

14.90 176.3 14.90 157.3 14.90 131.2 14.90 154.93

17.31 195.7 17.38 174.8 17.31 147 17.33 172.50

19.79 213.6 19.79 191.3 19.79 161.8 19.79 188.90

22.28 231.5 22.21 207.8 22.28 173.9 22.25 204.40

24.69 248.2 24.69 223.5 24.69 187.2 24.69 219.63

27.17 263.6 27.10 239.2 27.17 204.6 27.15 235.80

29.59 278.6 29.59 254.6 29.59 214.3 29.59 249.17

32.00 292 32.00 268.4 32.00 229.4 32.00 263.27

34.48 306.8 34.48 281.9 34.48 237 34.48 275.23

34.48 301.7 34.48 278.6 34.48 240.6 34.48 273.63

32.69 286.3 32.62 265.3 32.69 229 32.67 260.20

30.90 272.1 30.90 254.4 30.83 215.2 30.87 247.23

29.03 257.7 29.03 241.3 29.03 207 29.03 235.33

27.24 244.8 27.24 229.6 27.24 191.5 27.24 221.97

25.45 230.4 25.45 216.9 25.45 185.1 25.45 210.80

23.66 217.2 23.66 204.8 23.66 171.3 23.66 197.77

21.86 202.8 21.86 191.5 21.86 165.4 21.86 186.57

20.07 189.6 20.07 179.2 20.07 154.4 20.07 174.40

18.28 176.2 18.21 165.6 18.28 139.9 18.25 160.57

16.41 162.3 16.41 153.1 16.41 128.8 16.41 148.07

14.62 147.7 14.62 140.4 14.62 121.9 14.62 136.67

12.83 133.6 12.83 126.7 12.83 109.7 12.83 123.33

11.03 119.6 11.03 114.2 11.03 99.14 11.03 110.98

9.24 104.7 9.24 100.1 9.24 87 9.24 97.27

7.38 89.83 7.45 86.59 7.45 75.65 7.43 84.02

5.61 74.6 5.61 71.51 5.61 61.14 5.61 69.08

3.81 58.71 3.80 56.58 3.82 49.05 3.81 54.78

2.00 41.68 2.02 41.32 2.01 36.55 2.01 39.85

0.21 22.97 0.20 23.6 0.19 21.33 0.20 22.63

Average Stdev

YS 29.1 30.3 26.9 28.8 1.7

VS 7.9 7.3 6.2 7.2 0.9

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 546 328 406 426 110

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 47

Set D7: CS-BX5 – BL36- L1 – 7 day – NIST code (folder SR 51-SR-48B)

SR-48B

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 22.47 0.20 18.64 0.21 19 0.20 20.04

2.66 48.88 2.65 35.01 2.65 36.66 2.65 40.18

5.10 65.64 5.10 48.25 5.10 50.17 5.10 54.69

7.52 82.13 7.52 60.38 7.59 62.54 7.54 68.35

10.00 98.8 10.00 72.34 10.00 73.91 10.00 81.68

12.41 114.8 12.41 84.21 12.41 85.49 12.41 94.83

14.90 129 14.90 96.21 14.90 96.91 14.90 107.37

17.31 144.8 17.38 107.9 17.31 108.8 17.33 120.50

19.79 157.3 19.79 119.6 19.79 120 19.79 132.30

22.21 172.9 22.28 130.1 22.28 131.4 22.25 144.80

24.69 186.2 24.69 141.1 24.69 142.2 24.69 156.50

27.10 196 27.17 153.3 27.10 152.2 27.13 167.17

29.59 211.4 29.59 163.9 29.59 163.3 29.59 179.53

32.00 219.7 32.00 174.5 32.00 172.9 32.00 189.03

34.48 236 34.48 183 34.48 183.1 34.48 200.70

34.48 227.5 34.48 184.1 34.48 182.4 34.48 198.00

32.69 216.4 32.69 175.6 32.69 173.8 32.69 188.60

30.90 211.4 30.90 165.4 30.90 165.4 30.90 180.73

29.10 200.1 29.03 157.3 29.03 156.4 29.06 171.27

27.24 188.7 27.24 150.1 27.24 150.1 27.24 162.97

25.45 179.6 25.45 141.1 25.45 141.1 25.45 153.93

23.66 166.9 23.66 133.8 23.66 133.8 23.66 144.83

21.86 158.1 21.86 124.9 21.86 124.1 21.86 135.70

20.00 147.5 20.07 116.6 20.07 116.4 20.05 126.83

18.28 132.8 18.28 109.5 18.21 108.4 18.25 116.90

16.41 122.1 16.41 100.9 16.41 100 16.41 107.67

14.62 115.1 14.62 91.32 14.62 90.81 14.62 99.08

12.83 103.7 12.83 83.26 12.83 82 12.83 89.65

11.03 92.03 11.03 74.02 11.03 74.16 11.03 80.07

9.24 81.06 9.24 65.45 9.24 64.4 9.24 70.30

7.38 69.12 7.45 55.93 7.45 55.78 7.43 60.28

5.61 56.28 5.60 47.3 5.61 46.35 5.60 49.98

3.81 44.34 3.82 37.6 3.81 36.47 3.81 39.47

1.99 31.08 2.01 26.74 2.02 26.41 2.01 28.08

0.20 16.44 0.20 14.98 0.21 14.69 0.20 15.37

Average Stdev

YS 22.3 19.5 19.0 20.3 1.7

VS 6.1 4.8 4.8 5.2 0.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 100 150 134 128 26

0

50

100

150

200

250

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 48

Set D7: CS-BX5 – BL11- L1 – 7 day – NIST code (folder SR 51-SR-48C)

SR-48C

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 26.33 0.20 34.92 0.20 32.78 0.20 31.34

2.65 49.22 2.64 74.88 2.65 71.27 2.65 65.12

5.08 67.52 5.11 107.9 5.10 100.5 5.10 91.97

7.52 84.35 7.52 140.1 7.59 126.4 7.54 116.95

10.00 101 10.00 166.5 10.00 145.9 10.00 137.80

12.41 117.3 12.41 192.5 12.48 166.1 12.44 158.63

14.90 133.3 14.90 216.5 14.90 187.2 14.90 179.00

17.38 149.8 17.31 240.2 17.38 206.2 17.36 198.73

19.79 165.3 19.79 261.5 19.79 225.3 19.79 217.37

22.21 179.6 22.21 283.1 22.21 241.7 22.21 234.80

24.69 193.9 24.69 302.4 24.69 259.2 24.69 251.83

27.10 209.7 27.10 320.2 27.10 277.6 27.10 269.17

29.59 223.1 29.59 338.9 29.59 293.7 29.59 285.23

32.00 236.2 32.00 353.7 32.00 309.3 32.00 299.73

34.48 246 34.48 369.5 34.48 322.7 34.48 312.73

34.48 246 27.59 364 34.48 319.3 32.18 309.77

32.62 233.5 32.69 345.4 32.62 303.5 32.64 294.13

30.90 222.7 30.90 327.5 30.90 289 30.90 279.73

29.03 210.9 29.03 309.8 29.03 273.7 29.03 264.80

27.24 202.5 27.24 295.3 27.24 261 27.24 252.93

25.45 190.5 25.45 276.9 25.45 245.2 25.45 237.53

23.66 180.5 23.66 261.7 23.66 231.6 23.66 224.60

21.86 167.3 21.86 243.2 21.86 215.5 21.86 208.67

20.07 157.2 20.07 226.9 20.07 201.2 20.07 195.10

18.21 145.1 18.21 210.7 18.21 186.9 18.21 180.90

16.41 134.2 16.41 194 16.41 172.2 16.41 166.80

14.62 122.7 14.62 175.8 14.62 156.6 14.62 151.70

12.83 110.1 12.83 158.6 12.83 140.9 12.83 136.53

11.03 100.3 11.03 141.3 11.03 126.6 11.03 122.73

9.24 86.71 9.24 123.2 9.24 110.3 9.24 106.74

7.45 75.44 7.45 104.7 7.45 95.03 7.45 91.72

5.61 62.02 5.61 86.39 5.61 78.33 5.61 75.58

3.80 48.83 3.82 67.12 3.81 61.11 3.81 59.02

2.01 35.88 2.00 46.41 2.02 43.84 2.01 42.04

0.19 20.02 0.20 23.26 0.20 23.74 0.20 22.34

Average Stdev

YS 25.6 28.0 30.1 27.9 2.2

VS 6.5 10.1 8.5 8.3 1.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 284 750 637 557 243

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 49

Set D7: CS-BX5 – BL36- L2– 7 day – NIST code (folder SR 51-SR-48D)

SR-48D

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.19 23.89 0.20 20.32 0.20 26.22 0.20 23.48

2.65 51.08 2.65 37.21 2.64 56.84 2.65 48.38

5.10 71.81 5.10 50.52 5.10 80.3 5.10 67.54

7.52 92.49 7.52 62.32 7.52 103.9 7.52 86.24

10.00 109.9 10.00 73.83 10.00 123.9 10.00 102.54

12.41 126.1 12.41 85.17 12.41 141.9 12.41 117.72

14.90 141.6 14.90 96.28 14.90 160.3 14.90 132.73

17.38 156.7 17.38 107.9 17.38 176.1 17.38 146.90

19.79 170.6 19.79 118.5 19.79 192.8 19.79 160.63

22.21 185 22.21 129.9 22.21 207.3 22.21 174.07

24.69 198.6 24.69 140.5 24.69 221.8 24.69 186.97

27.10 211.2 27.10 150.1 27.17 237.8 27.13 199.70

29.59 224 29.59 161.1 29.59 249.7 29.59 211.60

32.07 235.4 32.00 170.7 32.00 264.6 32.02 223.57

34.48 247.2 34.48 182 34.48 275.1 34.48 234.77

34.48 243.6 34.48 179.8 34.48 274.9 34.48 232.77

32.69 230.9 32.69 171.7 32.69 261.2 32.69 221.27

30.90 220.3 30.83 165.2 30.90 245.9 30.87 210.47

29.03 208.2 29.03 157.2 29.03 233.9 29.03 199.77

27.24 197.2 27.24 148.4 27.24 219.8 27.24 188.47

25.45 186.3 25.45 141 25.45 207.7 25.45 178.33

23.66 175 23.66 132.2 23.66 194.8 23.66 167.33

21.86 163.4 21.86 124.7 21.86 183.6 21.86 157.23

20.07 152.6 20.07 116.4 20.07 170.4 20.07 146.47

18.21 140.7 18.21 107.1 18.28 158.4 18.23 135.40

16.41 129.7 16.41 98.96 16.41 145.6 16.41 124.75

14.62 118.6 14.62 91.49 14.62 132.6 14.62 114.23

12.83 106.6 12.83 82.6 12.83 120.1 12.83 103.10

11.03 95.79 11.03 73.98 11.03 106.1 11.03 91.96

9.24 83.42 9.24 65.28 9.24 93.58 9.24 80.76

7.45 71.9 7.45 56.37 7.38 79.43 7.43 69.23

5.62 59.03 5.61 46.58 5.61 66.22 5.62 57.28

3.81 46.1 3.81 37.01 3.82 52 3.81 45.04

2.01 33.42 2.01 27.15 2.01 36.22 2.01 32.26

0.19 18.12 0.21 15.46 0.20 19.28 0.20 17.62

Average Stdev

YS 22.4 20.0 24.3 22.2 2.2

VS 6.4 4.7 7.3 6.1 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 442 59 641 381 296

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 50

Set E1: CS-BX5 – BL11- L2 – Mixing Day – NIST code (folder SR 53-SR-52A)

SR-52A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.21 34.66 0.19 37.79 0.21 45.5 0.20 39.32

2.63 76.01 2.64 73.46 2.65 89.33 2.64 79.60

5.10 101.9 5.09 97 5.08 136.7 5.09 111.87

7.52 130.3 7.52 122.1 7.52 182.4 7.52 144.93

10.00 152.9 10.00 143.2 10.00 213.9 10.00 170.00

12.41 173.9 12.41 163 12.41 244 12.41 193.63

14.90 194.8 14.90 181.9 14.90 265.6 14.90 214.10

17.31 213.7 17.38 201.4 17.31 286.2 17.33 233.77

19.79 231.4 19.79 217.9 19.79 302.7 19.79 250.67

22.21 249.1 22.21 235.9 22.21 324.5 22.21 269.83

24.69 266.1 24.69 251.6 24.69 341.9 24.69 286.53

27.10 283 27.10 266.2 27.10 353 27.10 300.73

29.59 299.4 29.59 282.9 29.59 374.5 29.59 318.93

32.00 314.4 32.00 294.1 32.00 386.2 32.00 331.57

34.48 328.5 34.48 309.1 34.48 407.9 34.48 348.50

34.48 326.1 34.48 302.6 34.48 396.2 34.48 341.63

32.69 310.8 32.62 287.9 32.62 375.6 32.64 324.77

30.90 294.9 30.90 278.4 30.90 360.1 30.90 311.13

23.24 280 29.03 263 29.03 339.8 27.10 294.27

27.24 267.3 27.24 251.5 27.24 326.1 27.24 281.63

25.45 252.1 25.45 237.6 25.45 306.4 25.45 265.37

23.66 238.7 23.66 224.4 23.66 290.3 23.66 251.13

21.86 223.6 21.86 208.7 21.86 269.7 21.86 234.00

20.07 209.5 20.07 196.1 20.07 253.3 20.07 219.63

18.28 196.1 18.21 180.5 18.21 232.7 18.23 203.10

16.41 181.3 16.41 167.1 16.41 215.3 16.41 187.90

14.62 165.8 14.62 154 14.62 197.9 14.62 172.57

12.83 150.8 12.83 138.8 12.83 178 12.83 155.87

11.03 135.6 11.03 126.2 11.03 162 11.03 141.27

9.24 119.7 9.24 110.2 9.24 140.6 9.24 123.50

7.38 103.7 7.45 96.04 7.45 122 7.43 107.25

5.61 87.23 5.62 79.53 5.61 100.2 5.62 88.99

3.82 69.79 3.81 63.28 3.79 78.85 3.81 70.64

2.00 50.86 2.01 47.13 2.01 57.41 2.00 51.80

0.21 29.74 0.20 27.34 0.20 31.48 0.20 29.52

Average Stdev

YS 38.8 34.9 41.3 38.3 3.3

VS 8.6 7.9 10.4 9.0 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 520 489 1110 706 350

0

50

100

150

200

250

300

350

400

450

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 51

Set E1: CS-BX5 – BL36- L1 – Mixing Day – NIST code (folder SR 53-SR-52B)

SR-52B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 48.15 0.21 28.69 0.20 35.01 0.20 37.28

2.64 96.45 2.66 48.9 2.65 66.08 2.65 70.48

5.10 146.4 5.10 65.24 5.09 93.16 5.10 101.60

7.52 190.8 7.52 80.21 7.52 120.6 7.52 130.54

10.00 218.9 10.00 94.6 10.00 142.1 10.00 151.87

12.41 245.5 12.41 108.8 12.41 162.4 12.41 172.23

14.90 270.5 14.90 122.9 14.90 180.4 14.90 191.27

17.31 295.6 17.31 137.3 17.31 197.2 17.31 210.03

19.79 317.3 19.79 150.5 19.79 213.5 19.79 227.10

22.21 339.7 22.21 164.3 22.21 231.6 22.21 245.20

24.69 359.6 24.69 177.3 24.69 247.5 24.69 261.47

27.10 377 27.10 190.2 27.10 259.6 27.10 275.60

29.59 398.1 29.59 203.5 29.59 274.3 29.59 291.97

32.00 416.3 32.00 215 32.00 287.2 32.00 306.17

34.48 438.7 34.48 227.6 34.48 303.8 34.48 323.37

34.48 431.7 34.48 225.9 34.48 298.2 34.48 318.60

32.69 411.1 32.69 215.8 32.69 285.1 32.69 304.00

30.90 392.1 30.83 206.5 30.83 272.9 30.85 290.50

29.03 371.6 29.10 196.4 29.03 260.6 29.06 276.20

27.24 354.3 27.24 187.1 27.24 242.7 27.24 261.37

25.45 333.2 25.45 177.5 25.45 232.3 25.45 247.67

23.66 314.9 23.66 167.5 23.66 216.6 23.66 233.00

21.86 293.7 21.86 157.3 21.86 207.3 21.86 219.43

20.07 274.7 20.07 147.7 20.00 192.8 20.05 205.07

18.21 255.4 18.28 136.8 18.28 179.1 18.25 190.43

16.41 235.7 16.41 126.4 16.41 165.1 16.41 175.73

14.62 215 14.62 116.6 14.62 152 14.62 161.20

12.83 194.2 12.83 105.6 12.83 138.2 12.83 146.00

11.03 173.9 11.03 95.44 11.03 122 11.03 130.45

9.24 152 9.24 83.79 9.24 108.8 9.24 114.86

7.45 130.2 7.45 73 7.38 92.81 7.43 98.67

5.60 107.4 5.60 60.83 5.61 77.32 5.60 81.85

3.81 83.76 3.80 48.81 3.81 61.15 3.81 64.57

2.01 58.38 1.99 36.06 1.99 43.07 2.00 45.84

0.20 30.02 0.20 21.54 0.20 24 0.20 25.19

Average Stdev

YS 42.1 27.9 32.9 34.3 7.2

VS 11.4 5.8 7.8 8.4 2.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1081 119 490 563 485

0

50

100

150

200

250

300

350

400

450

500

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 52

Set E1: CS-BX5 – BL11- L1 – Mixing Day – NIST code (folder SR 53-SR-52C)

SR-52C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 33.2 0.20 42.05 0.21 41.18 0.20 38.81

2.63 54.55 2.64 73.69 2.65 81.21 2.64 69.82

5.11 71.47 5.10 104.6 5.10 110.8 5.10 95.62

7.52 87.72 7.52 133.4 7.52 142.6 7.52 121.24

10.00 103 10.00 157.6 10.00 166.8 10.00 142.47

12.41 118.2 12.41 176.3 12.41 188.3 12.41 160.93

14.90 133.2 14.90 193.5 14.90 208.8 14.90 178.50

17.31 149 17.31 211.8 17.31 228.5 17.31 196.43

19.79 163.7 19.79 228.8 19.79 248.2 19.79 213.57

22.28 177.7 22.21 245.3 22.21 267.1 22.23 230.03

24.69 191.8 24.69 260.5 24.69 284.7 24.69 245.67

27.10 207.8 27.17 275.4 27.17 300.6 27.15 261.27

29.59 221.5 29.59 285.5 29.59 316.2 29.59 274.40

32.00 234.9 32.00 298.5 32.00 331 32.00 288.13

34.48 244.3 34.48 310.1 34.48 350.7 34.48 301.70

34.48 246.5 34.48 308.4 34.48 345.2 34.48 300.03

32.69 235.8 32.69 293.4 32.69 328.9 32.69 286.03

30.83 221.7 30.83 279 30.83 317.8 30.83 272.83

29.03 212.7 29.03 266.6 29.03 302.5 29.03 260.60

27.24 201.7 27.24 249.2 27.24 284.6 27.24 245.17

25.45 191.8 25.45 238.3 25.45 271.5 25.45 233.87

23.66 180.8 23.66 222.5 23.66 254.3 23.66 219.20

21.86 172 21.86 212.6 21.86 240.3 21.86 208.30

20.07 160.6 20.07 197.5 20.07 225 20.07 194.37

18.21 151.3 18.28 184.9 18.21 206.1 18.23 180.77

16.41 140.1 16.41 170.8 16.41 190.2 16.41 167.03

14.62 128.4 14.62 157.2 14.62 176.6 14.62 154.07

12.83 117.6 12.83 142.6 12.83 127.7 12.83 129.30

11.03 104.7 11.03 126.5 11.03 143.7 11.03 124.97

9.24 93.83 9.24 112.8 9.24 126 9.24 110.88

7.38 81 7.45 96.39 7.45 108.9 7.43 95.43

5.61 68.86 5.61 81.83 5.61 89.6 5.61 80.10

3.82 55.49 3.81 65.17 3.82 71.3 3.82 63.99

2.01 40.42 2.01 46.7 2.00 51.72 2.01 46.28

0.20 24.57 0.20 26.92 0.21 28.97 0.20 26.82

Average Stdev

YS 32.9 35.7 36.0 34.9 1.7

VS 6.3 8.0 9.1 7.8 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 241 874 646 587 321

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 53

Set E1: CS-BX5 – BL36- L2 – Mixing Day – NIST code (folder SR 53-SR-52D)

SR-52D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.19 30.55 0.20 34.84 0.20 27 0.20 30.80

2.65 51.92 2.65 74.77 2.64 48.48 2.65 58.39

5.09 66.75 5.10 104 5.10 65.18 5.10 78.64

7.59 81.94 7.59 134.1 7.52 80.63 7.56 98.89

10.00 96.82 10.00 158 10.00 95.57 10.00 116.80

12.41 111.3 12.41 179.7 12.41 110.5 12.41 133.83

14.90 125.1 14.90 199.6 14.90 125.7 14.90 150.13

17.31 139 17.31 219.3 17.31 140.2 17.31 166.17

19.79 152.4 19.79 237.3 19.79 155 19.79 181.57

22.21 167.1 22.21 257.3 22.21 168.1 22.21 197.50

24.69 180.4 24.69 274.6 24.69 181.8 24.69 212.27

27.10 190.9 27.10 287.9 27.17 196.5 27.13 225.10

29.59 204.5 29.59 305 29.59 208.9 29.59 239.47

32.00 214.8 32.00 318.4 32.00 222.5 32.00 251.90

34.48 229.5 34.48 337.2 34.48 233.1 34.48 266.60

34.48 224.9 34.48 329.9 34.48 234.2 34.48 263.00

32.69 214.6 32.69 314 32.69 223.7 32.69 250.77

30.90 208.2 30.90 302.2 30.83 211.7 30.87 240.70

29.03 197.9 29.03 287.1 29.03 202.4 29.03 229.13

27.24 186.9 27.24 269.3 27.24 191.6 27.24 215.93

25.45 178.3 25.45 256.7 25.45 181.3 25.45 205.43

23.66 167 23.66 239.3 23.66 171.1 23.66 192.47

21.86 158.3 21.86 227.3 21.86 162 21.86 182.53

20.07 148.1 20.07 212 20.07 151 20.07 170.37

18.21 135.8 18.28 195.4 18.28 141.1 18.25 157.43

16.48 125.5 16.41 180.2 16.41 130.2 16.44 145.30

14.62 117.2 14.62 166 14.62 119.3 14.62 134.17

12.83 106.1 12.83 149.9 12.83 108.5 12.83 121.50

11.03 95.1 11.03 133.5 11.03 96.23 11.03 108.28

9.24 84.31 9.24 117.5 9.24 85.54 9.24 95.78

7.45 72.89 7.45 100.6 7.38 73.14 7.43 82.21

5.61 60.3 5.61 82.56 5.61 61.18 5.61 68.01

3.81 48.23 3.81 64.27 3.81 48.56 3.81 53.69

2.01 35.43 2.01 45.08 2.01 34.54 2.01 38.35

0.20 20.8 0.19 23.97 0.20 19.6 0.20 21.46

Average Stdev

YS 27.5 33.0 26.5 29.0 3.5

VS 5.9 8.8 6.1 6.9 1.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 83 588 215 295 262

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 54

Set E3: CS-BX5 – BL11- L2 – 3 day – NIST code (folder SR 54-SR-52A)

SR-52A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 21.07 0.20 26.63 0.20 26.3 0.23 24.67

2.64 48.35 2.65 50.84 2.65 47.78 2.65 48.99

5.10 65.33 5.09 67.35 5.10 64.06 5.09 65.58

7.52 80.42 7.59 81.93 7.52 79.27 7.54 80.54

10.00 94.88 10.00 97.16 10.00 93.23 10.00 95.09

12.41 108.8 12.41 112.7 12.41 107.6 12.41 109.70

14.90 122.8 14.90 127.7 14.90 121.6 14.90 124.03

17.31 137.5 17.38 143.2 17.31 135.8 17.33 138.83

19.79 151.1 19.79 157.9 19.79 149.3 19.79 152.77

22.21 165.2 22.21 172.7 22.21 162.6 22.21 166.83

24.69 178 24.69 186.9 24.69 175.4 24.69 180.10

27.10 191.3 27.10 200.2 27.10 187.9 27.10 193.13

29.59 204 29.59 214.4 29.59 200.6 29.59 206.33

32.00 216 32.00 227.3 32.00 211.9 32.00 218.40

34.48 226.7 34.48 240.3 34.48 223.2 34.48 230.07

34.48 225.7 34.48 239.2 34.48 220.9 34.48 228.60

32.69 215 32.69 227.8 32.62 210.2 32.67 217.67

30.83 204.7 30.90 216.2 30.90 201.9 30.87 207.60

29.03 193.7 29.03 205.3 29.03 191.4 29.03 196.80

27.24 185.6 27.24 195.7 27.24 182.4 27.24 187.90

25.45 174.7 25.45 184.4 25.45 172.5 25.45 177.20

23.66 165.5 23.66 174.2 23.66 162.8 23.66 167.50

21.86 153.9 21.86 162.6 21.86 152.1 21.86 156.20

20.07 144.7 20.07 152.1 20.07 142.8 20.07 146.53

18.21 134.8 18.21 141.6 18.21 131.6 18.21 136.00

16.41 124.6 16.48 130.8 16.41 121.9 16.44 125.77

14.62 113.5 14.62 119.1 14.62 112.2 14.62 114.93

12.83 102.6 12.83 107.9 12.83 101 12.83 103.83

11.03 93.21 11.03 96.95 11.03 91.88 11.03 94.01

9.24 81.34 9.24 85.09 9.24 80.14 9.24 82.19

7.45 70.76 7.45 73.65 7.45 70.06 7.45 71.49

5.61 59.46 5.61 61.92 5.61 57.88 5.61 59.75

3.82 47.51 3.81 49.49 3.80 46.14 3.81 47.71

2.01 35.08 2.01 36.26 2.01 34.57 2.01 35.30

0.19 20.29 0.20 20.79 0.21 20.22 0.20 20.43

Average Stdev

YS 25.9 26.1 25.5 25.8 0.3

VS 5.9 6.2 5.8 5.9 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 212 193 179 195 17

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 55

Set E3: CS-BX5 – BL36- L1 – 3 day – NIST code (folder SR 54-SR-52B)

SR-52B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 27.78 0.20 26.71 0.21 30.46 0.20 28.32

2.65 58.25 2.65 55.21 2.65 65.3 2.65 59.59

5.08 83.22 5.10 78.11 5.09 89.65 5.09 83.66

7.59 105.5 7.52 101.8 7.52 114 7.54 107.10

10.00 124.6 10.00 120.5 10.00 137.3 10.00 127.47

12.41 143.3 12.41 137.9 12.41 158.4 12.41 146.53

14.90 161.4 14.90 154.7 14.90 177.9 14.90 164.67

17.31 178.8 17.31 171.4 17.38 197.3 17.33 182.50

19.79 195.6 19.79 187.5 19.79 214.5 19.79 199.20

22.21 211.4 22.21 203.4 22.21 233.6 22.21 216.13

24.69 225.8 24.69 218.7 24.69 250.5 24.69 231.67

27.10 240.6 27.10 233 27.10 265.5 27.10 246.37

29.59 254.9 29.59 247.6 29.59 282.8 29.59 261.77

32.00 268.6 32.00 260.3 32.00 296.8 32.00 275.23

34.48 279.7 34.48 274.1 34.48 313.2 34.48 289.00

34.48 278.1 34.48 270.1 34.48 307 34.48 285.07

32.62 264.4 32.69 257 32.62 292.3 32.64 271.23

30.90 250.8 30.90 245.9 30.90 281 30.90 259.23

29.03 237.3 29.03 233.4 29.03 266.5 29.03 245.73

27.24 226.4 27.24 220.8 27.24 252.1 27.24 233.10

25.45 212.7 25.45 209.1 25.45 238.5 25.45 220.10

23.66 201 23.66 196.5 23.66 224 23.66 207.17

21.86 186.6 21.86 184.6 21.86 210.1 21.86 193.77

20.07 174.4 20.07 172.6 20.07 196.1 20.07 181.03

18.21 162.1 18.21 159.2 18.21 180 18.21 167.10

16.41 149.4 16.41 146.8 16.41 165.8 16.41 154.00

14.62 135.6 14.62 135.2 14.62 152.7 14.62 141.17

12.83 122.3 12.83 122.1 12.83 137.3 12.83 127.23

11.03 110 11.03 109.1 11.03 122.9 11.03 114.00

9.24 95.7 9.24 95.81 9.24 107.4 9.24 99.64

7.45 82.57 7.45 82.25 7.45 92.09 7.45 85.64

5.61 68.52 5.59 67.6 5.62 75.11 5.61 70.41

3.80 53.69 3.81 53.31 3.81 58.67 3.81 55.22

2.01 38.77 1.99 38.05 2.01 41.57 2.00 39.46

0.20 21.13 0.20 20.61 0.20 21.47 0.20 21.07

Average Stdev

YS 26.4 27.4 28.9 27.6 1.3

VS 7.3 7.1 8.2 7.6 0.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 564 359 409 444 107

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# F
B - 56

Set E3: CS-BX5 – BL11- L1 – 3 day – NIST code (folder SR 54-SR-52C)

SR-52C

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 28.26 0.20 28.06 0.20 25.04 0.20 27.12

2.63 55.12 2.65 54.07 2.66 48.43 2.64 52.54

5.10 76.25 5.09 73.92 5.08 69.55 5.09 73.24

7.52 96.6 7.59 93.3 7.59 90.67 7.56 93.52

10.00 115.4 10.00 110.4 10.00 109.1 10.00 111.63

12.41 132.6 12.41 127.1 12.41 125.5 12.41 128.40

14.90 149.7 14.90 142.7 14.90 141 14.90 144.47

17.31 165.5 17.31 159.3 17.38 156 17.33 160.27

19.79 181.1 19.79 174.1 19.79 170.9 19.79 175.37

22.21 195.8 22.21 189.8 22.21 186 22.21 190.53

24.69 210 24.69 203.9 24.69 200.1 24.69 204.67

27.17 223.1 27.10 216.2 27.10 212.3 27.13 217.20

29.59 236.5 29.59 230.8 29.59 225.6 29.59 230.97

32.00 248.8 32.00 241.5 32.07 237.7 32.02 242.67

34.48 262.5 34.48 253.3 34.48 252.1 34.48 255.97

34.48 258.5 34.48 250 34.48 248.3 34.48 252.27

32.69 246 32.69 237.9 32.69 236.7 32.69 240.20

30.83 234.5 30.90 227 30.90 226.8 30.87 229.43

29.03 223 29.03 214.7 29.03 215.6 29.03 217.77

27.24 209.9 27.24 205.5 27.24 202.3 27.24 205.90

25.45 199.4 25.45 193.3 25.45 192.6 25.45 195.10

23.66 186.8 23.66 182.8 23.66 180.1 23.66 183.23

21.86 175.8 21.86 170 21.86 170.5 21.86 172.10

20.07 164.5 20.07 159.3 20.07 159.1 20.07 160.97

18.21 151.7 18.21 147.5 18.21 146.7 18.21 148.63

16.41 139.8 16.41 136.3 16.41 135.4 16.41 137.17

14.62 128.6 14.62 124.4 14.62 124.9 14.62 125.97

12.83 116.3 12.83 112.4 12.83 112.9 12.83 113.87

11.03 104.4 11.03 101.6 11.03 101 11.03 102.33

9.24 91.55 9.24 88.54 9.24 89.05 9.24 89.71

7.45 79.07 7.45 76.81 7.45 76.95 7.45 77.61

5.61 65.52 5.61 63.97 5.61 63.95 5.61 64.48

3.81 52.17 3.81 50.77 3.81 50.78 3.81 51.24

2.00 37.8 2.01 37.37 2.01 37.05 2.00 37.41

0.20 21.65 0.20 21.39 0.19 21.27 0.20 21.44

Average Stdev

YS 27.1 26.7 27.0 26.9 0.2

VS 6.8 6.5 6.5 6.6 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 371 361 243 325 71

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# J

Run# K

Run# L
B - 57

Set E3: CS-BX5 – BL36- L2 – 3 day – NIST code (folder SR 54-SR-52D)

SR-52D

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.19 22.96 0.21 21.46 0.20 26.65 0.20 23.69

2.64 46.35 2.65 42.96 2.64 58.13 2.64 49.15

5.08 64.35 5.10 60.7 5.08 80.92 5.09 68.66

7.52 80.49 7.52 76.37 7.52 95.16 7.52 84.01

10.00 96.16 10.00 91.42 10.00 126.2 10.00 104.59

12.41 111.2 12.41 106.1 12.41 152.6 12.41 123.30

14.90 125.7 14.90 119.9 14.90 172.7 14.90 139.43

17.31 140.4 17.31 134.3 17.38 193.2 17.33 155.97

19.79 154.3 19.79 147.7 19.79 212.5 19.79 171.50

22.21 168.6 22.21 161.5 22.21 232.7 22.21 187.60

24.69 181.9 24.69 174.2 24.69 251 24.69 202.37

27.10 194.2 27.10 186.6 27.10 266.9 27.10 215.90

29.59 207.9 29.59 199.5 29.59 284.8 29.59 230.73

32.00 219.6 32.00 210.3 32.00 299.5 32.00 243.13

34.48 232.2 34.48 222.8 34.48 316.5 34.48 257.17

34.48 229.3 34.48 219.1 34.48 311.1 34.48 253.17

32.62 218.2 32.69 208.5 32.62 295.8 32.64 240.83

30.90 208.9 30.90 200 30.90 282.5 30.90 230.47

29.03 197.8 29.10 189.3 29.03 267.2 29.06 218.10

27.24 187.7 27.24 179.8 27.24 254.2 27.24 207.23

25.45 177.7 25.45 170 25.45 239 25.45 195.57

23.66 167 23.66 159.7 23.66 225.3 23.66 184.00

21.86 156.6 21.86 149.3 21.86 209.5 21.86 171.80

20.07 146.3 20.07 139.8 20.07 195.4 20.07 160.50

18.21 134.7 18.21 128.3 18.21 180.4 18.21 147.80

16.41 124.3 16.41 118.2 16.41 166 16.41 136.17

14.62 114 14.62 108.9 14.62 151.2 14.62 124.70

12.83 102.4 12.83 97.81 12.83 135.9 12.83 112.04

11.03 92.16 11.03 88.21 11.03 121.6 11.03 100.66

9.24 80.3 9.24 76.64 9.24 105.3 9.24 87.41

7.45 69.36 7.45 66.3 7.45 90.14 7.45 75.27

5.61 56.9 5.61 53.94 5.61 73.72 5.61 61.52

3.81 44.48 3.81 42.38 3.81 56.71 3.81 47.86

2.02 32.16 1.99 30.57 2.01 39.3 2.01 34.01

0.21 17.48 0.20 16.72 0.20 18.92 0.20 17.71

Average Stdev

YS 22.6 21.4 25.9 23.3 2.3

VS 6.1 5.8 8.4 6.8 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 208 168 304 227 70

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# G

Run# H

Run# I
B - 58

Set E7: CS-BX5 – BL11- L2 – 7 day – NIST code (folder SR 55-SR-52A)

SR-52A

Run# L Run# M Run# N Average

SR SS SR SS SR SS SR SS

0.21 25.67 0.20 25.35 0.20 25.05 0.20 25.36

2.65 47.05 2.65 45.51 2.65 45.3 2.65 45.95

5.10 63.92 5.10 61.21 5.10 61.96 5.10 62.36

7.52 79.83 7.52 75.21 7.52 77.07 7.52 77.37

10.00 95.18 10.00 88.82 10.00 91.36 10.00 91.79

12.41 109.9 12.41 102.6 12.41 105.7 12.41 106.07

14.90 124.5 14.90 117.1 14.90 120.4 14.90 120.67

17.31 138.8 17.38 131.1 17.31 134.7 17.33 134.87

19.79 153 19.79 144.6 19.79 149 19.79 148.87

22.21 167.1 22.21 156.5 22.21 162.9 22.21 162.17

24.69 180.7 24.69 169 24.69 176.5 24.69 175.40

27.17 193.5 27.17 183.7 27.10 189.9 27.15 189.03

29.59 206.5 29.59 195 29.59 202.8 29.59 201.43

32.00 218.9 32.00 208.3 32.00 215.5 32.00 214.23

34.48 232.8 34.48 216.8 34.48 227.9 34.48 225.83

34.48 230.5 34.48 219 34.48 226.5 34.48 225.33

32.69 220.2 32.69 209 32.69 216.3 32.69 215.17

30.83 211.4 30.83 196.9 30.83 206.8 30.83 205.03

29.03 201.4 29.03 188.5 29.03 196.9 29.03 195.60

27.24 189.8 27.24 177.8 27.24 187.1 27.24 184.90

25.45 180.6 25.45 168.7 25.45 177.2 25.45 175.50

23.66 169.2 23.66 158.6 23.66 167.1 23.66 164.97

21.86 159.9 21.86 150.5 21.86 157 21.86 155.80

20.07 149.6 20.07 140.2 20.07 146.8 20.07 145.53

18.28 137.5 18.21 130.6 18.21 135.8 18.23 134.63

16.41 127 16.41 120.5 16.41 125.4 16.41 124.30

14.62 117.4 14.62 110.7 14.62 115.6 14.62 114.57

12.83 105.9 12.83 100.9 12.83 104.7 12.83 103.83

11.03 95.48 11.03 89.27 11.03 94.04 11.03 92.93

9.24 83.85 9.24 79.74 9.24 82.79 9.24 82.13

7.45 72.58 7.38 68.47 7.45 71.51 7.43 70.85

5.60 59.85 5.61 57.03 5.60 59.34 5.60 58.74

3.82 47.73 3.81 45.64 3.81 47.39 3.81 46.92

2.01 35.15 2.01 33.08 2.00 34.56 2.01 34.26

0.20 20.37 0.20 19.37 0.20 20.12 0.20 19.95

Average Stdev

YS 26.0 25.0 26.1 25.7 0.6

VS 6.0 5.7 5.9 5.9 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 101 249 86 145 90

0

50

100

150

200

250

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# L

Run# M

Run# N
B - 59

Set E7: CS-BX5 – BL36- L1 – 7 day – NIST code (folder SR 55-SR-52B)

SR-52B

Run# A Run# B Run# D Average

SR SS SR SS SR SS SR SS

0.20 28.46 0.21 26.61 0.26 16.57 0.22 23.88

2.65 69.06 2.65 59.3 2.63 40.53 2.64 56.30

5.09 102.6 5.10 87.05 5.09 57.15 5.09 82.27

7.52 133 7.52 118.1 7.52 72.38 7.52 107.83

10.00 157.3 10.00 141.2 10.00 86.84 10.00 128.45

12.41 177.8 12.41 165.3 12.41 100.9 12.41 148.00

14.90 197.5 14.90 182.4 14.90 114.1 14.90 164.67

17.31 218.1 17.31 195.8 17.31 127.3 17.31 180.40

19.79 236.9 19.79 211.8 19.79 139.6 19.79 196.10

22.21 256.7 22.21 229.6 22.21 152.9 22.21 213.07

24.69 274.4 24.69 246.3 24.69 164.9 24.69 228.53

27.10 289.4 27.10 261.2 27.10 174.8 27.10 241.80

29.59 306.8 29.59 278 29.59 187.2 29.59 257.33

32.00 321 32.00 290.5 32.00 197.9 32.00 269.80

34.48 338.5 34.48 307 34.48 211.2 34.48 285.57

34.48 332.7 34.48 300.7 34.48 207.8 34.48 280.40

32.69 316.6 32.69 285.9 32.69 198 32.69 266.83

30.90 303.3 30.83 274 30.90 191.2 30.87 256.17

29.03 287.7 29.10 259.5 29.03 181.4 29.06 242.87

27.24 272 27.24 244.6 27.24 171.4 27.24 229.33

25.45 257.5 25.45 231.7 25.45 162.9 25.45 217.37

23.66 241.4 23.66 216.6 23.66 152.7 23.66 203.57

21.86 226.7 21.86 204 21.86 143.5 21.86 191.40

20.07 211.2 20.07 190 20.07 134.3 20.07 178.50

18.21 194.5 18.21 174.8 18.21 122.8 18.21 164.03

16.41 179.1 16.41 160.8 16.41 113.3 16.41 151.07

14.62 164.2 14.62 147.7 14.62 104.9 14.62 138.93

12.83 147.6 12.83 133.2 12.83 94.49 12.83 125.10

11.03 131.9 11.03 118.5 11.03 85.08 11.03 111.83

9.24 114.8 9.24 103.8 9.24 74.25 9.24 97.62

7.45 98.23 7.45 88.69 7.45 64.24 7.45 83.72

5.61 80.18 5.61 72.94 5.61 52.63 5.61 68.58

3.80 62.03 3.81 57.1 3.79 41.58 3.80 53.57

2.01 43.42 1.99 39.92 2.02 30.22 2.01 37.85

0.20 21.73 0.20 21.13 0.20 16.53 0.20 19.80

Average Stdev

YS 29.8 27.4 21.8 26.3 4.1

VS 8.9 8.0 5.5 7.5 1.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 630 523 95 416 283

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# D
B - 60

Set E7: CS-BX5 – BL11- L1 – 7 day – NIST code (folder SR 55-SR-52C)

SR-52C

Run# E Run# F Run# G Average

SR SS SR SS SR SS SR SS

0.20 41.41 0.21 24.42 0.20 23.81 0.20 29.88

2.65 89.56 2.63 43.76 2.65 43.13 2.64 58.82

5.08 128.1 5.10 59.57 5.09 59.16 5.09 82.28

7.52 180.5 7.52 74.19 7.59 73.1 7.54 109.26

10.00 213.7 10.00 88.43 10.00 87.19 10.00 129.77

12.41 244.4 12.41 102.3 12.41 101.3 12.41 149.33

14.90 268.9 14.90 115.9 14.90 114.8 14.90 166.53

17.31 291.5 17.31 129.4 17.31 128.3 17.31 183.07

19.79 311.3 19.79 142.7 19.79 141.3 19.79 198.43

22.21 331.6 22.28 155.2 22.21 155.4 22.23 214.07

24.69 348.5 24.69 167.4 24.69 168.1 24.69 228.00

27.10 363 27.10 180.6 27.10 178.8 27.10 240.80

29.59 378.2 29.59 192.4 29.59 191.2 29.59 253.93

32.00 395.3 32.00 204.2 32.07 202.3 32.02 267.27

34.48 413.4 34.48 213.2 34.48 215.5 34.48 280.70

34.48 409.2 34.48 213.8 34.48 213.4 34.48 278.80

32.69 388.4 32.69 203.6 32.69 204 32.69 265.33

30.83 365.3 30.90 192 30.83 195 30.85 250.77

29.03 347.2 29.03 182 29.03 186 29.03 238.40

27.24 325.5 27.24 175 27.24 174.2 27.24 224.90

25.45 306.5 25.45 163.9 25.45 166.5 25.45 212.30

23.66 287.7 23.66 155.9 23.66 155.6 23.66 199.73

21.86 269.9 21.86 144.4 21.86 148.2 21.86 187.50

20.00 249.8 20.07 135.2 20.07 137.9 20.05 174.30

18.21 234.5 18.28 127.3 18.21 128.1 18.23 163.30

16.41 215.3 16.41 117.4 16.41 118 16.41 150.23

14.62 193.3 14.62 105.8 14.62 108.7 14.62 135.93

12.83 174.8 12.83 96.35 12.83 98.66 12.83 123.27

11.03 154.6 11.03 86.28 11.03 87.53 11.03 109.47

9.24 135 9.24 75.95 9.24 77.89 9.24 96.28

7.45 114.3 7.45 65.18 7.45 66.74 7.45 82.07

5.59 94.82 5.60 55.31 5.61 55.83 5.60 68.65

3.81 72.65 3.81 44 3.81 44.43 3.81 53.69

1.99 49.25 2.01 31.84 2.02 31.96 2.01 37.68

0.20 24.22 0.21 18.55 0.20 18.41 0.20 20.39

Average Stdev

YS 31.2 23.2 24.1 26.1 4.4

VS 10.9 5.6 5.6 7.4 3.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1521 266 94 627 779

0

50

100

150

200

250

300

350

400

450

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# E

Run# F

Run# G
B - 61

Set E7: CS-BX5 – BL36- L2– 7 day – NIST code (folder SR 55-SR-52D)

SR-52D

Run# I Run# J Run# K Average

SR SS SR SS SR SS SR SS

0.19 46.02 0.21 20.42 0.20 27.35 0.20 31.26

2.64 132.1 2.65 40.45 2.65 66.73 2.65 79.76

5.10 200.1 5.08 55.92 5.10 93.11 5.10 116.38

7.52 264.8 7.59 70.01 7.52 119.5 7.54 151.44

10.00 314.1 10.00 84.32 10.00 141 10.00 179.81

12.41 353.6 12.41 98.21 12.41 161.6 12.41 204.47

14.90 377.9 14.90 110.9 14.90 183 14.90 223.93

17.31 416.2 17.31 125.1 17.31 202.1 17.31 247.80

19.79 432.6 19.79 137.2 19.79 221.3 19.79 263.70

22.28 476.9 22.21 151.7 22.28 237.8 22.25 288.80

24.69 500.9 24.69 164 24.69 254.7 24.69 306.53

27.10 502.7 27.10 173.2 27.10 272.1 27.10 316.00

29.59 541.6 29.59 186.8 29.59 286.6 29.59 338.33

31.93 546.2 32.00 195.6 32.00 300.5 31.98 347.43

34.48 583.7 34.48 210.4 34.48 312.7 34.48 368.93

34.41 536.4 34.48 204.2 34.48 310.8 34.46 350.47

32.62 505.9 32.69 194.4 32.69 294.9 32.67 331.73

30.90 508.4 30.90 189.8 30.90 278.4 30.90 325.53

29.10 464.7 29.03 179.8 29.03 263.5 29.06 302.67

27.24 453.9 27.24 168.8 27.24 251.5 27.24 291.40

25.52 421.3 25.45 161 25.45 235.8 25.47 272.70

23.66 400.1 23.66 150.2 23.66 222.9 23.66 257.73

21.86 359.5 21.86 141.8 21.86 207 21.86 236.10

20.07 341 20.07 132.6 20.07 193.4 20.07 222.33

18.21 305.2 18.21 119.7 18.28 180.1 18.23 201.67

16.41 281 16.41 110.3 16.41 165.6 16.41 185.63

14.62 259.4 14.62 103.3 14.62 149.8 14.62 170.83

12.83 226.4 12.83 92.76 12.83 135.4 12.83 151.52

11.03 210.7 11.03 83.05 11.03 120.7 11.03 138.15

9.24 174.1 9.24 72.79 9.24 104.9 9.24 117.26

7.45 151.6 7.45 62.54 7.45 89.43 7.45 101.19

5.61 118.2 5.61 50.46 5.61 73.64 5.61 80.77

3.81 88.91 3.81 39.7 3.82 57.05 3.81 61.89

2.01 60.5 2.01 28.62 2.01 39.21 2.01 42.78

0.20 23.81 0.19 15.45 0.20 19.53 0.20 19.60

Average Stdev

YS 34.8 20.3 26.2 27.1 7.3

VS 15.0 5.5 8.3 9.6 4.9

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1410 17 748 725 697

0

100

200

300

400

500

600

700

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# I

Run# J

Run# K
B - 62

Set F1: CS-BX1 – BL33- L1 – Mixing Day – NIST code (folder SR 57-SR-56A)

SR-56A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.24 25.02 0.20 26.72 0.21 25.21 0.22 25.65

2.63 58.61 2.65 46.35 2.64 44.67 2.64 49.88

5.10 79.75 5.10 61.56 5.08 60.55 5.09 67.29

7.52 99.07 7.52 75.38 7.52 74.84 7.52 83.10

10.00 116.6 10.00 89.47 10.00 88.78 10.00 98.28

12.41 133.8 12.41 103.2 12.41 102.5 12.41 113.17

14.90 151.4 14.90 117 14.90 115.6 14.90 128.00

17.31 166.5 17.31 130.9 17.38 128.9 17.33 142.10

19.79 182.7 19.79 144.4 19.79 141.4 19.79 156.17

22.21 197.1 22.21 157 22.21 155.3 22.21 169.80

24.69 211.9 24.69 169.8 24.69 167.8 24.69 183.17

27.17 227.7 27.10 182.9 27.10 178.6 27.13 196.40

29.59 241.3 29.59 194.7 29.59 192 29.59 209.33

32.00 255.8 32.00 207.3 32.00 202.4 32.00 221.83

34.48 268.4 34.48 218.4 34.48 215.4 34.48 234.07

34.48 268.6 34.48 218.6 34.48 212.5 34.48 233.23

32.69 256.6 32.69 209 32.69 202.8 32.69 222.80

30.83 243.2 30.90 198.8 30.90 194.9 30.87 212.30

29.03 232.2 29.03 189.7 29.03 184.8 29.03 202.23

27.24 219.7 27.24 180.7 27.24 176.3 27.24 192.23

25.45 207.8 25.45 171.1 25.45 166.9 25.45 181.93

23.66 195.6 23.66 161.8 23.66 157.8 23.66 171.73

21.86 184.5 21.86 152.1 21.86 147.5 21.86 161.37

20.07 171.9 20.07 142.4 20.07 138.5 20.07 150.93

18.28 159.9 18.28 133.1 18.28 127.9 18.28 140.30

16.41 147.7 16.41 123.1 16.41 118.4 16.41 129.73

14.62 135.3 14.62 112.6 14.62 109 14.62 118.97

12.83 123.1 12.83 102.9 12.83 98.76 12.83 108.25

11.03 109.6 11.03 91.99 11.03 89.31 11.03 96.97

9.24 97.21 9.24 81.7 9.24 78.2 9.24 85.70

7.38 83.28 7.38 70.26 7.45 67.96 7.40 73.83

5.61 69.57 5.60 59.2 5.61 56.6 5.61 61.79

3.82 55.43 3.83 47.64 3.80 45.23 3.82 49.43

2.02 40.05 2.00 34.83 2.01 33.47 2.01 36.12

0.21 22.55 0.20 20.31 0.21 19.36 0.21 20.74

Average Stdev

YS 29.6 27.2 25.4 27.4 2.1

VS 7.0 5.6 5.5 6.1 0.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 369 124 76 190 157

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
B - 63

Set F1: CS-BX1 – BL6- L2 – Mixing Day – NIST code (folder SR 57-SR-56B)

SR-56B

Run# D Run# E Run# G Average

SR SS SR SS SR SS SR SS

0.19 28.77 0.21 35.43 0.20 32.33 0.20 32.18

2.65 46.8 2.65 65.97 2.65 58.15 2.65 56.97

5.09 61.53 5.10 92.14 5.10 80.68 5.09 78.12

7.52 74.96 7.52 117.9 7.52 102.2 7.52 98.35

10.00 88.17 10.00 138.3 10.00 120.6 10.00 115.69

12.41 101.6 12.41 158.5 12.41 137.8 12.41 132.63

14.90 114.9 14.90 178.1 14.90 154.5 14.90 149.17

17.31 128.2 17.31 196.3 17.31 170.9 17.31 165.13

19.79 141 19.79 214.6 19.79 187.3 19.79 180.97

22.21 153.9 22.21 232.9 22.21 202.2 22.21 196.33

24.69 166.1 24.69 249.8 24.69 216.9 24.69 210.93

27.10 177.7 27.10 265.2 27.10 232.4 27.10 225.10

29.59 189.7 29.59 281.3 29.59 246.3 29.59 239.10

32.00 200.9 32.00 294.9 32.00 260.3 32.00 252.03

34.48 212.3 34.48 310.7 34.48 272.7 34.48 265.23

34.48 211 34.48 305.5 34.48 271.7 34.48 262.73

32.69 201.6 32.69 290.7 32.69 258.8 32.69 250.37

30.90 193.3 30.83 278.6 30.90 245.6 30.87 239.17

29.03 183.7 29.03 264.4 29.03 233.3 29.03 227.13

27.24 175.2 27.24 250.4 27.24 222.4 27.24 216.00

25.45 166.1 25.45 237.2 25.45 209.5 25.45 204.27

23.66 157.1 23.66 222.7 23.66 198.2 23.66 192.67

21.86 147.3 21.86 209.4 21.86 185.3 21.86 180.67

20.07 138.6 20.00 195.7 20.07 173.5 20.05 169.27

18.21 129.2 18.28 180.3 18.21 161.3 18.23 156.93

16.41 119.7 16.41 166.3 16.41 149 16.41 145.00

14.62 110 14.62 153.4 14.62 136.4 14.62 133.27

12.83 99.79 12.83 138.3 12.83 123.6 12.83 120.56

11.03 90.62 11.03 124.3 11.03 111.4 11.03 108.77

9.24 79.83 9.24 109.1 9.24 97.83 9.24 95.59

7.45 69.99 7.45 94.24 7.45 84.81 7.45 83.01

5.61 58.68 5.59 77.69 5.61 70.48 5.60 68.95

3.80 47.21 3.81 61.46 3.81 56.27 3.80 54.98

2.01 35.8 1.99 44.5 1.99 41.24 2.00 40.51

0.20 21.98 0.20 24.96 0.20 23.92 0.20 23.62

Average Stdev

YS 28.2 32.3 30.5 30.3 2.1

VS 5.4 8.0 7.1 6.8 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 95 442 410 316 192

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# G
B - 64

Set F1: CS-BX1 – BL33- L2 – Mixing Day – NIST code (folder SR 57-SR-56C)

SR-56C

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.19 32.11 0.20 28.81 0.20 33.45 0.20 31.46

2.65 58.7 2.64 53.48 2.64 67.66 2.64 59.95

5.10 79.32 5.10 73.04 5.08 93.37 5.09 81.91

7.52 99.52 7.52 91.18 7.52 118.9 7.52 103.20

10.00 117.6 10.00 107 10.00 138.8 10.00 121.13

12.41 135 12.41 123.3 12.41 157.8 12.41 138.70

14.90 153.3 14.90 138.8 14.90 177.3 14.90 156.47

17.31 169.8 17.31 154 17.38 195.4 17.33 173.07

19.79 186.7 19.79 168.9 19.79 212.9 19.79 189.50

22.21 201.1 22.21 183.8 22.21 228.5 22.21 204.47

24.69 216.2 24.69 198.1 24.69 244.8 24.69 219.70

27.10 232.4 27.10 211.3 27.10 262.1 27.10 235.27

29.59 245.7 29.59 225.5 29.59 277.3 29.59 249.50

32.00 260.4 32.00 237.9 32.00 292.4 32.00 263.57

34.48 270.3 34.48 251.3 34.48 304.3 34.48 275.30

34.48 270.8 34.48 247.6 34.48 303.5 34.48 273.97

32.69 258.1 32.69 235.9 32.62 288.7 32.67 260.90

30.83 243.3 30.83 227 30.90 272.9 30.85 247.73

29.03 231.4 29.10 215.7 29.03 258.8 29.06 235.30

27.24 220.7 27.24 204.4 27.24 247.4 27.24 224.17

25.45 207.7 25.45 194.1 25.45 232.6 25.45 211.47

23.66 196.7 23.66 182.2 23.66 220.3 23.66 199.73

21.86 183.7 21.86 171.9 21.86 205.1 21.86 186.90

20.00 171.6 20.00 160.8 20.07 192 20.02 174.80

18.21 160.8 18.28 147.9 18.21 179.1 18.23 162.60

16.41 148.5 16.41 136.6 16.41 165.6 16.41 150.23

14.62 135.1 14.62 126.7 14.62 150.6 14.62 137.47

12.83 122.7 12.83 114.9 12.83 136 12.83 124.53

11.03 110.1 11.03 102.9 11.03 122.8 11.03 111.93

9.24 96.93 9.24 91.04 9.24 107.2 9.24 98.39

7.45 83.62 7.45 78.62 7.45 92.93 7.45 85.06

5.61 70.08 5.61 65.39 5.61 77.41 5.61 70.96

3.81 55.9 3.81 52.39 3.80 60.93 3.81 56.41

2.00 40.79 1.99 38.46 2.01 44.33 2.00 41.19

0.19 23.46 0.21 22.48 0.21 24.76 0.20 23.57

Average Stdev

YS 29.9 29.0 31.9 30.3 1.5

VS 7.0 6.4 7.9 7.1 0.7

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 461 193 620 425 216

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# H

Run# I

Run# J
B - 65

Set F1: CS-BX1 – BL6- L1 – Mixing Day – NIST code (folder SR 57-SR-56D)

SR-56D

Run# k Run# L Run# M Average

SR SS SR SS SR SS SR SS

0.19 33.46 0.19 32.25 0.20 31.53 0.20 32.41

2.64 62.22 2.64 60.28 2.64 55.92 2.64 59.47

5.08 85.29 5.10 83.44 5.10 77.81 5.09 82.18

7.52 108 7.52 105.3 7.52 98.84 7.52 104.05

10.00 126.6 10.00 124 10.00 116.6 10.00 122.40

12.41 144.6 12.41 141.4 12.41 133.1 12.41 139.70

14.90 162.3 14.90 158.7 14.90 149.3 14.90 156.77

17.38 179.8 17.31 175.3 17.31 165.4 17.33 173.50

19.79 196.1 19.79 191.4 19.79 180.7 19.79 189.40

22.21 211.9 22.21 206.6 22.21 194.8 22.21 204.43

24.69 227.6 24.69 221.5 24.69 209 24.69 219.37

27.10 243.6 27.17 236.9 27.17 224.9 27.15 235.13

29.59 258.8 29.59 250.3 29.59 237.8 29.59 248.97

32.00 272.9 32.00 264.3 32.00 251.9 32.00 263.03

34.48 285.2 34.48 276.9 34.48 262.7 34.48 274.93

34.48 283.2 34.48 275 34.48 263.1 34.48 273.77

32.62 269.5 32.69 262.1 32.69 250.7 32.67 260.77

30.90 256.8 30.83 249 30.90 236.8 30.87 247.53

29.03 243.3 29.03 236.8 29.03 224.8 29.03 234.97

27.24 232.7 27.24 224.1 27.24 214.3 27.24 223.70

25.45 219.2 25.45 212.5 25.45 201.9 25.45 211.20

23.66 207.5 23.66 200.1 23.66 190.6 23.66 199.40

21.86 193.3 21.86 188.2 21.86 178.5 21.86 186.67

20.07 181.1 20.07 175.9 20.07 167 20.07 174.67

18.21 168.8 18.28 163.9 18.28 156.5 18.25 163.07

16.41 156.1 16.41 151.2 16.41 144.4 16.41 150.57

14.62 142.4 14.62 138.3 14.62 131.1 14.62 137.27

12.83 128.8 12.83 125.8 12.83 119.3 12.83 124.63

11.03 116.6 11.03 112.4 11.03 106.7 11.03 111.90

9.24 101.9 9.24 99.37 9.24 94.08 9.24 98.45

7.45 88.62 7.45 85.13 7.38 80.88 7.43 84.88

5.61 73.54 5.61 71.22 5.61 68.16 5.61 70.97

3.81 58.16 3.82 56.62 3.81 54.24 3.81 56.34

2.01 42.96 2.01 40.75 2.01 39.05 2.01 40.92

0.20 24.45 0.20 23.07 0.19 22.68 0.20 23.40

Average Stdev

YS 31.6 30.3 28.9 30.3 1.4

VS 7.4 7.2 6.8 7.1 0.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 428 440 451 440 12

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# k

Run# L

Run# M
B - 66

Set F3: CS-BX1 – BL33- L1 – 3 day – NIST code (folder SR 58-SR-56A)

SR-56A

Run# E Run# F Run# G Average

SR SS SR SS SR SS SR SS

0.20 27.68 0.20 29.37 0.20 21.24 0.20 26.10

2.63 55.17 2.65 61.98 2.65 39.63 2.64 52.26

5.10 79.2 5.08 87.81 5.10 54.73 5.09 73.91

7.52 102.1 7.59 112.5 7.59 68.7 7.56 94.43

10.00 119.1 10.00 134.4 10.00 82.35 10.00 111.95

12.41 136 12.41 154.9 12.41 95.44 12.41 128.78

14.90 153.3 14.90 174.1 14.90 108.7 14.90 145.37

17.31 169 17.31 193.7 17.38 121.9 17.33 161.53

19.79 185.2 19.79 211.7 19.79 135 19.79 177.30

22.21 200.4 22.21 230.6 22.21 147.1 22.21 192.70

24.69 215.7 24.69 248.3 24.69 159.7 24.69 207.90

27.17 230.4 27.10 264.4 27.10 171.5 27.13 222.10

29.59 244 29.59 282.5 29.59 183.3 29.59 236.60

32.00 257.8 32.00 297 32.00 194.5 32.00 249.77

34.48 273.3 34.48 312.4 34.48 205.6 34.48 263.77

34.48 269.4 34.48 308.7 34.48 204.8 34.48 260.97

32.69 256.6 32.62 293.6 32.69 195.5 32.67 248.57

30.83 246.9 30.90 280.3 30.90 186.7 30.87 237.97

29.03 234 29.03 265 29.03 177.4 29.03 225.47

27.24 222.1 27.24 253.1 27.24 168.7 27.24 214.63

25.45 209.5 25.45 238.3 25.45 159.5 25.45 202.43

23.66 198 23.66 225 23.66 150.7 23.66 191.23

21.86 184.3 21.86 209 21.86 141.5 21.86 178.27

20.07 172.4 20.07 195.8 20.00 132 20.05 166.73

18.28 159.9 18.21 180.9 18.21 123.2 18.23 154.67

16.41 147.7 16.41 166.9 16.41 113.8 16.41 142.80

14.62 134.6 14.62 151.6 14.62 103.8 14.62 130.00

12.83 121.4 12.83 136.3 12.83 94.23 12.83 117.31

11.03 109.2 11.03 123 11.03 84.1 11.03 105.43

9.24 95.14 9.24 106.2 9.24 74.23 9.24 91.86

7.45 81.87 7.45 91.6 7.45 63.65 7.45 79.04

5.60 67.63 5.61 75.13 5.61 53.1 5.61 65.29

3.81 52.99 3.79 58.22 3.80 41.92 3.80 51.04

2.01 37.65 2.01 41.13 2.01 30.11 2.01 36.30

0.20 19.93 0.20 20.73 0.19 16.57 0.20 19.08

Average Stdev

YS 26.9 28.2 22.6 25.9 3.0

VS 7.2 8.2 5.4 6.9 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 303 425 97 275 166

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# E

Run# F

Run# G
B - 67

Set F3: CS-BX1 – BL6- L2 – 3 day – NIST code (folder SR 58-SR-56B)

SR-56B

Run# A Run# C Run# D Average

SR SS SR SS SR SS SR SS

0.26 20.61 0.20 27.79 0.20 26.4 0.22 24.93

2.65 53.74 2.64 56.62 2.63 52.06 2.64 54.14

5.10 73.72 5.10 77.13 5.09 72.68 5.10 74.51

7.52 96.08 7.52 98.18 7.52 92.88 7.52 95.71

10.00 113 10.00 116.5 10.00 110.3 10.00 113.27

12.41 129.9 12.41 133.4 12.41 126.6 12.41 129.97

14.90 146.9 14.90 150.8 14.90 143.2 14.90 146.97

17.31 162.3 17.31 166.9 17.31 158.9 17.31 162.70

19.79 177.8 19.79 183.3 19.79 174.3 19.79 178.47

22.21 191.9 22.21 197.9 22.21 188.6 22.21 192.80

24.69 206.2 24.69 212.9 24.69 203 24.69 207.37

27.10 220.8 27.17 229.3 27.10 218.2 27.13 222.77

29.59 233.8 29.59 242.7 29.59 231.2 29.59 235.90

32.00 247 32.00 257.7 32.07 245.7 32.02 250.13

34.48 258.7 34.48 269.7 34.48 257.5 34.48 261.97

34.48 257.4 34.48 270.5 34.48 257.1 34.48 261.67

32.69 245.2 32.69 257.8 32.69 245.4 32.69 249.47

30.83 232.6 30.90 243.7 30.83 233.4 30.85 236.57

29.03 220.7 29.03 231.5 29.03 222.3 29.03 224.83

27.24 210.3 27.24 220.3 27.24 209.6 27.24 213.40

25.45 198.2 25.45 207.7 25.45 199.4 25.45 201.77

23.66 187.1 23.66 196.2 23.66 187.1 23.66 190.13

21.86 174.5 21.86 184 21.86 176.7 21.86 178.40

20.07 163.2 20.07 171.9 20.07 165 20.07 166.70

18.21 151.6 18.28 160.9 18.21 152.4 18.23 154.97

16.41 139.6 16.41 148.3 16.41 140.5 16.41 142.80

14.62 127.5 14.62 134.9 14.62 129.2 14.62 130.53

12.83 115.1 12.83 122.8 12.83 116.9 12.83 118.27

11.03 103.4 11.03 109.5 11.03 104.6 11.03 105.83

9.24 90.33 9.24 96.43 9.24 91.79 9.24 92.85

7.45 78.05 7.38 82.51 7.45 78.85 7.43 79.80

5.61 64.14 5.61 69.29 5.61 65.07 5.61 66.17

3.81 50.5 3.83 54.64 3.05 51.1 3.56 52.08

1.99 36.24 2.01 38.65 2.01 36.56 2.01 37.15

0.20 19.69 0.19 21.12 0.20 19.82 0.20 20.21

Average Stdev

YS 25.7 28.6 27.6 27.3 1.4

VS 6.8 7.1 6.7 6.9 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 403 401 313 372 52

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# C

Run# D
B - 68

Set F3: CS-BX1 – BL33- L2 – 3 day – NIST code (folder SR 58-SR-56C)

SR-56C

Run# K Run# L Run# M Average

SR SS SR SS SR SS SR SS

0.21 28.42 0.20 33.57 0.20 23.35 0.20 28.45

2.65 58.79 2.64 77.55 2.65 42.11 2.65 59.48

5.10 80.44 5.10 111.2 5.10 56.62 5.10 82.75

7.52 99.87 7.52 147.1 7.52 69.93 7.52 105.63

10.00 118.5 10.00 170.5 10.00 83.74 10.00 124.25

12.41 136.3 12.41 191 12.41 97.04 12.41 141.45

14.90 153.7 14.90 211.1 14.90 110 14.90 158.27

17.31 170.6 17.31 229.7 17.38 122.8 17.33 174.37

19.79 185.9 19.79 248.3 19.79 135.4 19.79 189.87

22.28 200.9 22.21 267 22.21 147 22.23 204.97

24.69 215.2 24.69 284.9 24.69 158.7 24.69 219.60

27.10 230.7 27.10 302.2 27.10 170.8 27.10 234.57

29.59 244.8 29.59 318.6 29.59 182 29.59 248.47

32.00 258.4 32.00 334.6 32.00 193.4 32.00 262.13

34.48 269 34.48 350.1 34.48 202.7 34.48 273.93

34.48 270 34.48 346.6 34.48 203 34.48 273.20

32.69 257.1 32.69 329.3 32.62 193.7 32.67 260.03

30.90 241.9 30.90 312.2 30.90 182.9 30.90 245.67

29.03 230 29.03 296.1 29.03 173.8 29.03 233.30

27.24 219.4 27.24 280.8 27.24 166.4 27.24 222.20

25.45 205.5 25.45 264.3 25.45 156.3 25.45 208.70

23.66 195.1 23.66 249 23.66 148.5 23.66 197.53

21.86 182.1 21.86 232.6 21.86 138.4 21.86 184.37

20.07 169.5 20.07 216.9 20.07 129.2 20.07 171.87

18.28 159.4 18.28 201.2 18.21 121.5 18.25 160.70

16.41 146.9 16.41 185.2 16.41 112.2 16.41 148.10

14.62 132.9 14.62 168.8 14.62 101.5 14.62 134.40

12.83 120.8 12.83 152.4 12.83 92.53 12.83 121.91

11.03 107.2 11.03 135.8 11.03 82.87 11.03 108.62

9.24 94.85 9.24 118.9 9.24 72.97 9.24 95.57

7.45 80.89 7.38 101.6 7.45 62.94 7.43 81.81

5.61 67.96 5.61 83.92 5.61 53.24 5.61 68.37

3.82 53.65 3.81 65.62 3.79 42.4 3.81 53.89

2.01 38.02 2.01 46.16 2.02 30.74 2.01 38.31

0.20 21.05 0.19 24.33 0.20 18.04 0.20 21.14

Average Stdev

YS 27.2 31.4 22.9 27.2 4.3

VS 7.1 9.2 5.3 7.2 2.0

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 535 894 210 546 342

0

50

100

150

200

250

300

350

400

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# K

Run# L

Run# M
B - 69

Set F3: CS-BX1 – BL6- L1 – 3 day – NIST code (folder SR 58-SR-56D)

SR-56D

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 31.37 0.19 30.4 0.20 23.54 0.20 28.44

2.65 67.72 2.66 64.05 2.63 42.71 2.64 58.16

5.10 96 5.09 85.09 5.10 60.03 5.10 80.37

7.52 123.4 7.52 106 7.52 75.19 7.52 101.53

10.00 144.8 10.00 125.3 10.00 88.59 10.00 119.56

12.41 165.3 12.41 143.4 12.41 101.8 12.41 136.83

14.90 185.3 14.90 161.5 14.90 115.8 14.90 154.20

17.31 203.1 17.38 179.3 17.31 129 17.33 170.47

19.79 221.1 19.79 195.3 19.79 142.5 19.79 186.30

22.21 237.5 22.28 211.2 22.21 155.2 22.23 201.30

24.69 253.8 24.69 227.1 24.69 167.7 24.69 216.20

27.10 270.1 27.10 242.7 27.10 180.5 27.10 231.10

29.59 285.2 29.59 258 29.59 192.2 29.59 245.13

32.00 300.3 32.00 272.6 32.00 204.3 32.00 259.07

34.48 314.1 34.48 284.7 34.48 215.8 34.48 271.53

34.48 310.7 34.48 284.4 34.48 215.4 34.48 270.17

32.69 295.8 32.62 270.6 32.69 205.6 32.67 257.33

30.90 281.7 30.90 255.8 30.90 195.8 30.90 244.43

29.03 267.5 29.03 242.5 29.03 186.4 29.03 232.13

27.24 253.9 27.24 232.4 27.24 176.4 27.24 220.90

25.45 239.8 25.45 218.4 25.45 167.4 25.45 208.53

23.66 225.8 23.66 207.2 23.66 157.5 23.66 196.83

21.86 211.5 21.86 192.7 21.86 148.5 21.86 184.23

20.07 197.3 20.07 180.2 20.07 138.7 20.07 172.07

18.21 182.8 18.21 168.6 18.21 128.7 18.21 160.03

16.41 168.3 16.41 155.6 16.41 118.8 16.41 147.57

14.62 154.1 14.62 140.8 14.62 109 14.62 134.63

12.83 139.1 12.83 127.5 12.83 98.97 12.83 121.86

11.03 124.2 11.03 114.5 11.03 88.54 11.03 109.08

9.24 108.7 9.24 99.96 9.24 78.18 9.24 95.61

7.45 93.09 7.45 86.18 7.45 67.29 7.45 82.19

5.61 76.49 5.61 71.71 5.61 56.01 5.61 68.07

3.81 59.9 3.81 56.23 3.82 44.74 3.81 53.62

1.99 42.34 2.01 40.1 2.01 32.6 2.01 38.35

0.21 22.62 0.20 21.69 0.21 18.95 0.20 21.09

Average Stdev

YS 30.0 28.9 24.3 27.7 3.0

VS 8.2 7.5 5.6 7.1 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 626 499 156 427 243

0

50

100

150

200

250

300

350

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# H

Run# I

Run# J
B - 70

Set F7: CS-BX1 – BL33- L1 – 7 day – NIST code (folder SR 59-SR-56A)

SR-56A

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 39.64 0.20 20.4 0.20 25.97 0.20 28.67

2.64 101.2 2.64 38.22 2.65 58.06 2.64 65.83

5.10 153.2 5.09 52.12 5.09 80.16 5.09 95.16

7.52 207.2 7.59 64.83 7.59 102.8 7.56 124.94

10.00 244.5 10.00 77.08 10.00 123.6 10.00 148.39

12.41 279.5 12.41 89.28 12.41 142.1 12.41 170.29

14.90 308.2 14.90 101.7 14.90 160.5 14.90 190.13

17.31 341.6 17.38 113.4 17.31 178 17.33 211.00

19.79 365 19.79 125.4 19.79 195.2 19.79 228.53

22.21 398.4 22.21 136.5 22.21 210.9 22.21 248.60

24.69 423.9 24.69 147.6 24.69 227.1 24.69 266.20

27.10 440.2 27.10 159.3 27.10 243.4 27.10 280.97

29.59 469.9 29.59 169.9 29.59 258.3 29.59 299.37

32.00 486 32.07 180.7 32.00 273 32.02 313.23

34.48 507.6 34.48 190.1 34.48 285.3 34.48 327.67

34.48 498.6 34.48 190.4 34.48 284.1 34.48 324.37

32.62 473.4 32.69 181.6 32.62 270.1 32.64 308.37

30.90 439.7 30.90 171.9 30.90 255.5 30.90 289.03

29.03 413.8 29.03 163.2 29.03 242.1 29.03 273.03

27.24 400.2 27.24 155.5 27.24 229.1 27.24 261.60

25.45 369.4 25.45 146.4 25.45 215.9 25.45 243.90

23.66 353.1 23.66 138.4 23.66 203.2 23.66 231.57

21.86 323 21.86 129.1 21.86 189.9 21.86 214.00

20.07 300.8 20.07 120.6 20.07 176.8 20.07 199.40

18.21 285.2 18.21 112.6 18.21 164.4 18.21 187.40

16.41 262.2 16.41 103.8 16.41 151.2 16.41 172.40

14.62 231.6 14.62 94.23 14.62 136.8 14.62 154.21

12.83 208.9 12.83 85.23 12.83 123.7 12.83 139.28

11.03 185.1 11.03 76.44 11.03 110 11.03 123.85

9.24 160.1 9.24 66.89 9.24 96.22 9.24 107.74

7.38 135 7.45 57.67 7.45 81.92 7.43 91.53

5.60 111.3 5.60 48.3 5.61 68.05 5.60 75.88

3.82 83.84 3.79 38.06 3.79 52.88 3.80 58.26

2.01 54.99 2.02 27.52 2.01 36.9 2.01 39.80

0.20 23 0.20 15.69 0.21 19.02 0.20 19.24

Average Stdev

YS 33.0 19.6 24.4 25.7 6.8

VS 13.4 5.0 7.6 8.7 4.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1574 187 523 761 724

0

100

200

300

400

500

600

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# H

Run# I

Run# J
B - 71

Set F7: CS-BX1 – BL6- L2 – 7 day – NIST code (folder SR 59-SR-56B)

SR-56B

Run# D Run# E Run# G Average

SR SS SR SS SR SS SR SS

0.19 28.04 0.21 22.52 0.20 27.98 0.20 26.18

2.65 56.67 2.65 41.75 2.64 59.57 2.65 52.66

5.10 78.14 5.10 56.82 5.10 85.73 5.10 73.56

7.52 98.19 7.52 70.5 7.52 113.6 7.52 94.10

10.00 116.6 10.00 83.43 10.00 132.9 10.00 110.98

12.41 134.2 12.41 96.3 12.41 150.8 12.41 127.10

14.90 151.7 14.90 109.5 14.90 167.4 14.90 142.87

17.38 167.9 17.38 121.5 17.31 184.5 17.36 157.97

19.79 184.1 19.79 134.8 19.79 199.7 19.79 172.87

22.21 199.3 22.21 147 22.21 216.5 22.21 187.60

24.69 214.1 24.69 159.1 24.69 231.1 24.69 201.43

27.17 229.3 27.10 170.9 27.10 244 27.13 214.73

29.59 243.2 29.59 181.6 29.59 259 29.59 227.93

32.00 256.3 32.07 193.4 32.00 270 32.02 239.90

34.48 268.4 34.48 205.4 34.48 283.6 34.48 252.47

34.48 265.7 34.48 204.6 34.48 278.9 34.48 249.73

32.69 252.6 32.69 195.4 32.69 265.1 32.69 237.70

30.90 240.3 30.83 186.4 30.90 250.8 30.87 225.83

29.03 227.3 29.03 177.7 29.03 237.4 29.03 214.13

27.24 216.7 27.24 166.5 27.24 227.4 27.24 203.53

25.45 203.7 25.45 158.7 25.45 212.4 25.45 191.60

23.66 192.3 23.66 148.4 23.66 201.4 23.66 180.70

21.86 179 21.86 141.1 21.86 186.4 21.86 168.83

20.07 167.4 20.07 131.4 20.07 174 20.07 157.60

18.28 155.7 18.28 122.2 18.21 162.7 18.25 146.87

16.41 143.5 16.41 112.7 16.41 149.8 16.41 135.33

14.62 130.4 14.62 103.4 14.62 135.2 14.62 123.00

12.83 117.6 12.83 93.84 12.83 122.1 12.83 111.18

11.03 105.8 11.03 83.54 11.03 109 11.03 99.45

9.24 92.19 9.24 73.94 9.24 95.34 9.24 87.16

7.45 79.19 7.45 63.62 7.38 81.4 7.43 74.74

5.60 65.88 5.61 53.14 5.60 67.76 5.60 62.26

3.83 51.76 3.79 42.03 3.81 52.94 3.81 48.91

2.01 36.86 2.01 30.41 2.01 37.25 2.01 34.84

0.20 20.07 0.20 17.48 0.20 20.11 0.20 19.22

Average Stdev

YS 25.6 22.6 25.4 24.5 1.7

VS 7.0 5.3 7.4 6.6 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 432 126 624 394 251

0

50

100

150

200

250

300

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# D

Run# E

Run# G
B - 72

Set F7: CS-BX1 – BL33- L2 – 7 day – NIST code (folder SR 59-SR-56C)

SR-56C

Run# K Run# L Run# M Average

SR SS SR SS SR SS SR SS

0.20 22.65 0.20 22.66 0.21 22.81 0.20 22.71

2.65 40.94 2.65 41.46 2.65 43 2.65 41.80

5.10 56.34 5.09 57 5.09 58.94 5.09 57.43

7.52 70.07 7.52 71.2 7.52 73.77 7.52 71.68

10.00 82.93 10.00 84.9 10.00 88.09 10.00 85.31

12.41 95.84 12.41 98.73 12.41 101.9 12.41 98.82

14.90 108.9 14.90 113 14.90 115.1 14.90 112.33

17.31 121.5 17.38 126.4 17.38 129.1 17.36 125.67

19.79 134.2 19.79 140.2 19.79 142.1 19.79 138.83

22.21 146.8 22.21 152.5 22.21 155.5 22.21 151.60

24.69 158.8 24.69 165 24.69 168 24.69 163.93

27.10 170.2 27.10 177.3 27.10 179.6 27.10 175.70

29.59 181.8 29.59 188.7 29.59 192.1 29.59 187.53

32.00 193 32.07 200.7 32.00 202.9 32.02 198.87

34.48 204.6 34.48 212.3 34.48 214.9 34.48 210.60

34.48 203.1 34.48 210.9 34.48 213.1 34.48 209.03

32.69 193.6 32.69 201.2 32.69 203.1 32.69 199.30

30.83 185 30.90 192.3 30.90 193.6 30.87 190.30

29.03 176.1 29.03 182.9 29.03 183.8 29.03 180.93

27.24 166.2 27.24 172.4 27.24 175 27.24 171.20

25.45 157.7 25.45 164 25.45 164.9 25.45 162.20

23.66 148.1 23.66 153.9 23.66 156.1 23.66 152.70

21.86 139.7 21.86 145.2 21.86 145.8 21.86 143.57

20.00 130.3 20.07 135.5 20.07 136.3 20.05 134.03

18.28 121.1 18.21 125.3 18.21 126.5 18.23 124.30

16.41 111.6 16.41 115.5 16.41 116.9 16.41 114.67

14.62 102.3 14.62 106.2 14.62 106.8 14.62 105.10

12.83 92.81 12.83 96.35 12.83 96.84 12.83 95.33

11.03 82.75 11.03 86.15 11.03 86.94 11.03 85.28

9.24 73.13 9.24 75.89 9.24 76.35 9.24 75.12

7.45 62.9 7.45 65.33 7.45 65.78 7.45 64.67

5.60 52.43 5.61 54.5 5.61 54.91 5.61 53.95

3.81 41.78 3.81 43.29 3.81 43.64 3.81 42.90

2.01 30.24 2.01 31.51 2.02 31.82 2.01 31.19

0.20 17.65 0.21 17.99 0.21 18.28 0.20 17.97

Average Stdev

YS 22.3 23.1 23.2 22.9 0.5

VS 5.3 5.5 5.6 5.5 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 120 118 155 131 21

0

50

100

150

200

250

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# K

Run# L

Run# M
B - 73

Set F7: CS-BX1 – BL6- L1 – 7 day – NIST code (folder SR 59-SR-56D)

SR-56D

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 16.67 0.20 52.37 0.19 20.63 0.22 29.89

2.63 40.2 2.66 153.1 2.65 38.28 2.65 77.19

5.10 55.69 5.10 226.6 5.10 52.63 5.10 111.64

7.52 69.86 7.59 320.8 7.52 65.48 7.54 152.05

10.00 83.46 10.00 368.8 10.00 78.2 10.00 176.82

12.41 96.94 12.41 420.7 12.41 90.57 12.41 202.74

14.90 110.4 14.90 468.1 14.90 102.4 14.90 226.97

17.31 123.8 17.31 512.1 17.31 115 17.31 250.30

19.79 136.6 19.79 551.6 19.79 126.5 19.79 271.57

22.21 148.8 22.21 581.7 22.21 139 22.21 289.83

24.69 160.6 24.69 614.1 24.69 150.4 24.69 308.37

27.10 172.3 27.10 653.6 27.10 160.9 27.10 328.93

29.59 183.5 29.59 684.7 29.59 172.5 29.59 346.90

32.00 194.9 32.00 711 32.00 182.9 32.00 362.93

34.48 206.2 34.48 733.6 34.48 194.2 34.48 378.00

34.48 205 34.48 725.7 34.48 193.3 34.48 374.67

32.69 195.6 32.62 685.5 32.69 184.7 32.67 355.27

30.83 186.7 30.90 640.8 30.90 175 30.87 334.17

29.03 177.7 29.10 604.5 29.03 166.3 29.06 316.17

27.24 168.1 27.24 579.8 27.24 159.1 27.24 302.33

25.45 159.2 25.45 538.2 25.45 149.4 25.45 282.27

23.66 149.6 23.66 510.7 23.66 141.8 23.66 267.37

21.86 140.7 21.86 469.5 21.86 132 21.86 247.40

20.07 131.3 20.07 437.4 20.07 123.5 20.07 230.73

18.28 121.5 18.21 407.9 18.21 115.5 18.23 214.97

16.41 111.9 16.41 373.8 16.41 106.6 16.41 197.43

14.62 102.7 14.62 335.6 14.62 96.7 14.62 178.33

12.83 92.71 12.83 300.1 12.83 87.79 12.83 160.20

11.03 83.12 11.03 268.4 11.03 78.78 11.03 143.43

9.24 73.04 9.24 230.5 9.24 69.16 9.24 124.23

7.45 62.89 7.45 195.9 7.45 59.21 7.45 106.00

5.61 52.09 5.59 157.2 5.61 49.69 5.60 86.33

3.82 41.41 3.81 117.6 3.82 39.37 3.82 66.13

2.01 29.9 2.01 77 2.01 28.46 2.01 45.12

0.20 16.84 0.21 29.48 0.19 16 0.20 20.77

Average Stdev

YS 21.5 43.7 20.8 28.7 13.0

VS 5.4 19.6 5.1 10.0 8.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 139 2849 114 1034 1571

0

100

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400

500

600

700

800

0.00 10.00 20.00 30.00 40.00

Shear rate

Shear Stress

Run# A

Run# B

Run# C
C - 1

Appendix C: Statistical analysis for NonNewtonian calculations 

Provides all the graphs needed for the interpretation of the results and the extraction of the nonNewtonian values (Table 8).
Box Day Unit

Run 

Order Set Mix

Sample 

Age YS VS H

5 1 36 3 A-A SR-36A 1 19.3064199 4.9975396 91.5480028

5 1 36 2 A-B SR-36B 1 29.1662483 8.0212475 280.2616425

5 1 45 4 A-C SR-36C 1 20.6727873 5.6778243 153.2836974

1 2 6 6 B-A SR-40A 1 25.0966409 6.5626316 203.7850420

1 2 6 5 B-B SR-40B 1 25.0481254 6.1495963 122.2930032

1 2 23 8 B-C SR-40C 1 24.2140165 5.7646911 31.9522212

1 2 23 7 B-D SR-40D 1 26.0465144 6.1368060 104.5553066

3 3 3 10 C-A SR-44A 1 32.4249565 7.5430304 200.1295053

3 3 4 9 C-C SR-44C 1 24.5803305 6.4623221 200.5767660

3 3 4 12 C-D SR-44D 1 23.3224192 8.2778063 472.7525037

5 4 11 15 D-A SR-48A 1 33.4651166 8.7658072 528.2914642

5 4 11 13 D-B SR-48B 1 20.2635688 6.9259024 307.7473006

5 4 12 14 D-C SR-48C 1 29.2572367 9.6299466 556.7189354

5 4 12 16 D-D SR-48D 1 23.5995673 7.1397625 281.9765655

3 5 30 17 E-A SR-52A 1 29.7893455 8.8359725 509.3005499

3 5 30 20 E-B SR-52B 1 27.5356258 8.1859882 405.1682756

3 5 41 19 E-C SR-52C 1 27.2523805 7.6746132 330.4198266

3 5 41 18 E-D SR-52D 1 23.3495891 6.7447280 237.8220784

1 6 28 24 F-A SR-56A 1 21.8544397 5.9304506 112.6469520

1 6 28 22 F-B SR-56B 1 23.6524221 6.7265001 221.5057333

1 6 33 21 F-C SR-56C 1 23.5187875 7.0357733 249.1711148

1 6 33 23 F-D SR-56D 1 23.5977287 7.0174218 250.8748781

5 1 36 1 A-A SR-36A 3 18.6890537 5.8773721 283.1595794

5 1 36 4 A-B SR-36B 3 21.4386488 7.0448216 220.9322999

5 1 45 3 A-C SR-36C 3 22.9017911 8.6331887 482.9083653

5 1 45 2 A-D SR-36D 3 17.1488751 2.2883394 65.1217671

1 2 6 5 B-A SR-40A 3 15.7096706 6.3836834 195.6812180

1 2 6 8 B-B SR-40B 3 21.6862982 6.9743657 220.6756558

1 2 23 6 B-C SR-40C 3 16.1741501 4.9636549 70.2085966

1 2 23 7 B-D SR-40D 3 22.8365409 5.7745906 119.2855205

3 3 3 9 C-A SR-44A 3 24.8232588 7.5790606 310.9187905

3 3 4 12 C-C SR-44C 3 24.9741271 8.3294252 469.2950691

3 3 4 10 C-D SR-44D 3 19.6503882 7.3297032 276.2035683

5 4 11 16 D-A SR-48A 3 23.9800112 7.3683777 331.9426032

5 4 11 15 D-B SR-48B 3 17.0345993 5.6325033 153.8899520

5 4 12 13 D-C SR-48C 3 20.2483012 6.4242668 143.4271823

5 4 12 14 D-D SR-48D 3 18.0357110 6.3945586 326.6226030

3 5 30 17 E-A SR-52A 3 20.1247702 5.8589626 133.9268194

3 5 30 19 E-B SR-52B 3 21.9814558 7.4209182 324.2353297

3 5 41 20 E-C SR-52C 3 20.7897916 6.5279639 253.5568971

3 5 41 18 E-D SR-52D 3 18.6348805 6.6284021 213.2981225

1 6 28 23 F-A SR-56A 3 20.8439344 6.7789771 206.2433202

1 6 28 21 F-B SR-56B 3 21.0483733 6.7876283 194.9406918

1 6 33 22 F-C SR-56C 3 20.4308499 7.1445562 289.7368003

1 6 33 24 F-D SR-56D 3 21.7570672 7.0029645 246.5515718

5 1 36 4 A-A SR-36A 7 15.5361239 4.6775444 59.3795843

5 1 36 1 A-B SR-36B 7 21.4029677 6.3342544 168.0009222

5 1 45 2 A-C SR-36C 7 17.6003594 5.7803670 159.0549592

5 1 45 3 A-D SR-36D 7 17.2876817 2.0217890 63.8531682

1 2 6 6 B-A SR-40A 7 17.9185800 6.9589998 258.0594469

1 2 6 5 B-B SR-40B 7 21.3495931 6.3069751 199.2255447

1 2 23 8 B-C SR-40C 7 22.8562218 8.2655517 444.4045981

1 2 23 7 B-D SR-40D 7 23.6039568 7.4161522 235.8165445

3 3 3 9 C-A SR-44A 7 25.3134951 8.1673146 560.6808423

3 3 4 11 C-C SR-44C 7 25.5922443 9.3827809 455.6381540

3 3 4 10 C-D SR-44D 7 20.8883642 8.1792238 906.2229008

5 4 11 14 D-A SR-48A 7 21.6203608 7.1263480 247.5195673

5 4 11 15 D-B SR-48B 7 15.8771034 5.1574202 129.6630455

5 4 12 16 D-C SR-48C 7 22.1501211 8.1390299 364.3580627

5 4 12 13 D-D SR-48D 7 17.0126234 6.0910298 242.2908669

3 5 30 20 E-A SR-52A 7 20.3873427 5.7598697 85.1299548

3 5 30 19 E-B SR-52B 7 21.1317456 7.3303978 338.5755449

3 5 41 18 E-C SR-52C 7 19.6244611 7.3328384 402.6905175

3 5 41 17 E-D SR-52D 7 22.3475634 9.3734880 884.4920402

1 6 28 21 F-A SR-56A 7 18.7562898 8.6796266 461.3903596

1 6 28 22 F-B SR-56B 7 18.7114924 6.5360503 264.3368318

1 6 33 23 F-C SR-56C 7 18.2019711 5.3596391 106.9575936

1 6 33 24 F-D SR-56D 7 20.5929528 10.0893716 597.8741723

Table 1: Data Used for Analysis of Rheological Quantities in SRM 2492

C-2
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5 10 15 20

15 20 25 30

Run Order

YS

YS versus Run Order

C-3
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15 20 25 30

(Sample Age)/day

YS

YS versus Sample Age

C-4
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2345

20 22 24 26 28 30 32 34

Box

YS

YS versus Box

Sample Age = 1 day

C-5
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123456

20 22 24 26 28 30 32 34

Day

YS

YS versus Day

Sample Age = 1 day

C-6
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20 22 24 26 28 30 32 34

Unit

YS

YS versus Unit

Sample Age = 1 day

C-7
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20 22 24 26 28 30 32 34

Theoretical Quantiles

Sample Quantiles

Normal Probability Plot of YS 

Sample Age = 1 day

C-8
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2345

16 18 20 22 24

Box

YS

YS versus Box

Sample Age = 3 day

C-9
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123456

16 18 20 22 24

Day

YS

YS versus Day

Sample Age = 3 day

C-10
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16 18 20 22 24

Unit

YS

YS versus Unit

Sample Age = 3 day

C-11
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Theoretical Quantiles

Sample Quantiles

Normal Probability Plot of YS 

Sample Age = 3 day

C-12
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2345

16 18 20 22 24

Box

YS

YS versus Box

Sample Age = 7 day

C-13
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16 18 20 22 24

Day

YS

YS versus Day

Sample Age = 7 day

C-14
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Unit

YS

YS versus Unit

Sample Age = 7 day

C-15
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Theoretical Quantiles

Sample Quantiles

Normal Probability Plot of YS 

Sample Age = 7 day

C-16
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Run Order

VS

VS versus Run Order

C-17
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(Sample Age)/day

VS

VS versus Sample Age

C-18
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2345

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Box

VS

VS versus Box

Sample Age = 1 day

C-19
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Day

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VS versus Day

Sample Age = 1 day

C-20
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Unit

VS

VS versus Unit

Sample Age = 1 day

C-21
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Theoretical Quantiles

Sample Quantiles

Normal Probability Plot of VS 

Sample Age = 1 day

C-22
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VS versus Box

Sample Age = 3 day

C-23
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VS versus Day

Sample Age = 3 day

C-24
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VS versus Unit

Sample Age = 3 day

C-25
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Theoretical Quantiles

Sample Quantiles

Normal Probability Plot of VS 

Sample Age = 3 day

C-26
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VS

VS versus Box

Sample Age = 7 day

C-27
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Day

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VS versus Day

Sample Age = 7 day

C-28
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Sample Age = 7 day

C-29
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Theoretical Quantiles

Sample Quantiles

Normal Probability Plot of VS 

Sample Age = 7 day

C-30
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Run Order

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H versus Run Order

C-31
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C-33
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C-34
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Sample Age = 1 day

C-36
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C-40
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C-43
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Sample Age = 7 day

C-44
WinBUGS Implementation of Hierarchical Model for Certification of

Rheological Quantities in SRM 2492

model

{

mu~dunif(-1000,1000)

sigma.day~dunif(0,1000)

sigma.btl~dunif(0,1000)

sigma.rme~dunif(0,1000)

tau.day <- 1/(sigma.day*sigma.day)

tau.btl <- 1/(sigma.btl*sigma.btl)

tau.rme <- 1/(sigma.rme*sigma.rme)

for(i in 1:6)

{

mu.day[i]~dnorm(mu,tau.day)

}

for(i in 1:12)

{

mu.btl[i]~dnorm(mu.day[day[i]],tau.btl)

}

for(i in 1:n)

{

y[i]~dnorm(mu.btl[btl[i]],tau.rme)

pred[i]~dnorm(mu.btl[btl[i]],tau.rme)

res[i] <- y[i]-pred[i]

}

mu.nu~dnorm(mu,tau.btl)

}

C-45
−15 −10 −5 0 5 10 15

Mix

Residual

Residual Plot for Response YS at Age 1 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-46
−10 −5

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5 10

Mix

Residual

Residual Plot for Response YS at Age 3 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-47
−10 −5

0

5 10

Mix

Residual

Residual Plot for Response YS at Age 7 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-48
−4 −2

0

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4

Mix

Residual

Residual Plot for Response VS at Age 1 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-49
−3 −2 −1 0 1 2 3

Mix

Residual

Residual Plot for Response VS at Age 3 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-50
−4 −2 0 2 4 6

Mix

Residual

Residual Plot for Response VS at Age 7 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-51
−400 −200

0 200 400

Mix

Residual

Residual Plot for Response H at Age 1 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-52
−300 −200 −100 0 100 200 300 400

Mix

Residual

Residual Plot for Response H at Age 3 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-53
−500

0 500

Mix

Residual

Residual Plot for Response H at Age 7 day(s)

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22

C-54
20 25 30

0.00 0.05 0.10 0.15 0.20 0.25

YS

Probability Density

Distribution of YS Values at Age 1 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for YS

20.96 25.34 29.68

C-55
16 18 20 22 24 26

0.0 0.1 0.2 0.3

YS

Probability Density

Distribution of YS Values at Age 3 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for YS

17.9 20.7 23.61

C-56
14 16 18 20 22 24 26

0.00 0.05 0.10 0.15 0.20 0.25 0.30

YS

Probability Density

Distribution of YS Values at Age 7 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for YS

16.94 20.44 24.07

C-57
4 5 6 7 8 9 10

0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7

VS

Probability Density

Distribution of VS Values at Age 1 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for VS

5.597 7.094 8.648

C-58
5 6 7 8 9

0.0 0.2 0.4 0.6 0.8

VS

Probability Density

Distribution of VS Values at Age 3 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for VS

5.433 6.829 8.265

C-59
4 5 6 7 8 9 10

0.0 0.1 0.2 0.3 0.4 0.5 0.6

VS

Probability Density

Distribution of VS Values at Age 7 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for VS

5.356 7.198 9.069

C-60
0 200 400 600

0.000 0.001 0.002 0.003 0.004 0.005

H

Probability Density

Distribution of H Values at Age 1 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for H

50.68 263.8 474.2

C-61
0 100 200 300 400 500

0.000 0.002 0.004 0.006

H

Probability Density

Distribution of H Values at Age 3 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for H

102.4 253.9 410.7

C-62
−200 0 200 400 600 800 1000

0.0000 0.0005 0.0010 0.0015 0.0020 0.0025 0.0030

H

Probability Density

Distribution of H Values at Age 7 for a New Unit of SRM 2492

Shaded Area Gives a 95% Uncertainty Interval for H

12.6 345.3 681.3

C-63
Response Age Mean Value

Standard 

Uncertainty

Degrees of 

Freedom

Coverage 

Factor

Expanded 

Uncertainty Lower Bound Upper Bound

y u (y ) ν k U

YS 1 25.3 1.512 3.7 2.8675 4.3 21.0 29.7

YS 3 20.7 1.005 4.2 2.7251 2.7 18.0 23.4

YS 7 20.4 1.273 4.0 2.7764 3.5 16.9 24.0

VS 1 7.1 0.549 4.0 2.7764 1.5 5.6 8.6

VS 3 6.8 0.501 4.0 2.7764 1.4 5.4 8.2

VS 7 7.2 0.652 4.1 2.7499 1.8 5.4 9.0

H 1 264 77.45 4.4 2.6905 208 55 472

H 3 254 53.28 3.9 2.8047 149 104 403

H 7 345 117.97 3.6 2.9024 342 3 688

Table 2: Certification Results for SRM 2492

C-64
D - 1

Appendix D: Data for Non-Newtonian 

calculations

Legend of the tables

YS = yield stress

VS = plastic viscosity

SR = Shear Rate

SS = Shear Stress

R2 = r2 calculated using a Pearson function to determine the linearity of the data

This appendix provides all the data for each test that was performed and that used for the Newtonian 

calculation for Section 5.1.3 and Appendix C. These data are generated using a non-Newtonian 

approach. 
D - 2

Set A1: CS-BX5 – BL45- L2 – Mixing Day – NIST code (folder SR 37-SR-36A)

SR-36A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 16.87 0.21 21.66 0.21 19.11 0.23 19.21

2.65 37.96 2.65 38.47 2.65 33.66 2.65 36.70

5.09 51.49 5.09 51.69 5.08 47.00 5.09 50.06

7.52 62.96 7.52 63.79 7.59 59.80 7.54 62.18

10.00 75.42 10.00 76.70 10.00 71.95 10.00 74.69

12.41 88.22 12.41 89.96 12.41 83.36 12.41 87.18

14.90 101.25 14.90 103.02 14.90 94.45 14.90 99.57

17.31 114.03 17.31 115.13 17.38 105.99 17.33 111.72

19.79 124.56 19.79 125.66 19.79 118.32 19.79 122.85

22.21 136.51 22.21 138.73 22.21 129.06 22.21 134.76

24.69 148.34 24.69 150.57 24.69 136.86 24.69 145.25

27.10 158.76 27.10 160.98 27.10 146.31 27.10 155.35

29.59 167.63 29.59 169.83 29.59 158.72 29.59 165.39

32.00 176.55 32.07 179.84 32.00 169.47 32.02 175.29

34.48 183.13 34.48 186.38 34.48 179.36 34.48 182.96

34.48 196.14 34.48 199.62 34.48 181.46 34.48 192.41

32.69 185.86 32.69 189.32 32.69 170.45 32.69 181.88

30.83 174.55 30.90 176.83 30.90 162.79 30.87 171.39

29.10 161.11 29.03 163.32 29.03 156.88 29.06 160.44

27.24 155.98 27.24 157.09 27.24 146.77 27.24 153.28

25.45 149.04 25.45 150.17 25.45 142.02 25.45 147.08

23.66 140.86 23.66 141.99 23.66 132.25 23.66 138.37

21.86 131.22 21.86 132.34 21.86 123.42 21.86 128.99

20.07 122.51 20.07 122.51 20.07 118.43 20.07 121.15

18.21 114.07 18.21 115.19 18.21 108.90 18.21 112.72

16.41 104.75 16.41 105.53 16.41 98.46 16.41 102.91

14.62 96.67 14.62 96.45 14.62 91.35 14.62 94.82

12.83 85.40 12.83 85.84 12.83 82.91 12.83 84.71

11.03 78.46 11.03 77.48 11.03 74.37 11.03 76.77

9.24 68.35 9.24 68.13 9.24 65.56 9.24 67.35

7.45 59.34 7.45 58.37 7.45 56.67 7.45 58.12

5.61 48.58 5.61 48.80 5.62 46.45 5.61 47.94

3.80 37.94 3.81 37.94 3.81 36.49 3.80 37.46

2.00 26.76 2.01 26.37 2.01 25.45 2.01 26.19

0.21 15.73 0.19 15.34 0.21 14.79 0.20 15.29

Average Stdev

YS 19.6 18.5 19.8 19.3 0.7

VS 5.1 5.2 4.7 5.0 0.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 86 123 65 92 30
D - 3

Set A1: CS-BX5 – BL12- L2 – Mixing Day – NIST code (folder SR 37-SR-36B)

SR-36B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 32.87 0.20 27.83 0.19 35.04 0.20 31.91

2.66 66.28 2.65 45.68 2.64 63.56 2.65 58.51

5.09 97.44 5.10 62.97 5.09 93.43 5.09 84.61

7.52 125.71 7.52 78.90 7.52 125.43 7.52 110.01

10.00 144.74 10.00 94.47 10.00 146.56 10.00 128.59

12.41 162.41 12.41 111.59 12.41 169.18 12.41 147.73

14.90 183.89 14.90 127.67 14.90 190.04 14.90 167.20

17.31 201.94 17.31 142.18 17.31 210.55 17.31 184.89

19.79 222.15 19.79 155.43 19.79 228.63 19.79 202.07

22.21 238.71 22.21 167.14 22.21 242.59 22.21 216.15

24.69 254.99 24.69 186.85 24.69 261.70 24.69 234.51

27.10 268.29 27.10 202.13 27.10 277.83 27.10 249.42

29.59 282.23 29.59 210.01 29.59 289.60 29.59 260.61

32.00 298.55 32.00 222.20 32.00 300.86 32.00 273.87

34.48 302.04 34.48 220.39 34.48 303.25 34.48 275.23

34.48 330.55 34.48 240.90 34.48 342.58 34.48 304.68

32.69 319.60 32.69 240.83 32.69 331.89 32.69 297.44

30.83 298.90 30.83 224.72 30.90 308.23 30.85 277.28

29.03 281.17 29.03 197.81 29.03 283.40 29.03 254.12

27.24 265.58 27.24 195.79 27.24 272.73 27.24 244.70

25.45 251.46 25.45 184.35 25.45 253.57 25.45 229.79

23.66 235.88 23.66 176.54 23.66 240.89 23.66 217.77

21.86 220.81 21.86 166.85 21.86 227.76 21.86 205.14

20.00 206.20 20.07 148.67 20.07 208.84 20.05 187.90

18.28 191.86 18.21 140.58 18.28 193.90 18.25 175.45

16.41 178.69 16.41 137.61 16.41 181.36 16.41 165.89

14.62 162.54 14.62 124.29 14.62 166.56 14.62 151.13

12.83 147.20 12.83 108.36 12.83 148.71 12.83 134.76

11.03 131.48 11.03 99.87 11.03 134.40 11.03 121.92

9.24 115.26 9.24 87.37 9.24 117.67 9.24 106.77

7.45 97.82 7.45 75.44 7.45 100.11 7.45 91.12

5.61 81.38 5.61 63.09 5.61 83.07 5.61 75.84

3.81 63.67 3.81 49.44 3.81 64.38 3.81 59.16

1.99 42.58 2.00 34.90 2.00 43.70 2.00 40.39

0.19 24.56 0.20 21.26 0.20 25.00 0.20 23.60

Average Stdev

YS 30.8 26.4 30.3 29.2 2.4

VS 8.7 6.3 9.0 8.0 1.5

R2 1.00 0.99 1.00 1.0 0.0

Hysteresis 389 62 390 280 189
D - 4

Set A1: CS-BX5 – BL12- L1 – Mixing Day – NIST code (folder SR 37-SR-36C)

SR-36C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 23.95 0.20 25.59 0.19 17.89 0.20 22.48

2.64 39.24 2.65 43.79 2.66 33.79 2.65 38.94

5.10 55.90 5.09 63.61 5.09 48.52 5.09 56.01

7.52 70.09 7.52 78.97 7.59 62.63 7.54 70.57

10.00 84.29 10.00 92.31 10.00 77.52 10.00 84.70

12.41 99.26 12.41 107.15 12.41 91.16 12.41 99.19

14.90 113.48 14.90 121.33 14.90 104.87 14.90 113.22

17.31 127.62 17.38 135.60 17.31 118.58 17.33 127.27

19.79 141.82 19.79 150.30 19.79 132.62 19.79 141.58

22.21 154.94 22.21 162.94 22.21 148.44 22.21 155.44

24.69 164.71 24.69 171.73 24.69 155.73 24.69 164.06

27.17 176.90 27.10 182.31 27.10 166.26 27.13 175.16

29.59 190.66 29.59 192.16 29.59 181.17 29.59 188.00

32.00 200.07 32.00 202.01 32.00 192.98 32.00 198.36

34.48 210.98 34.48 225.59 34.48 207.24 34.48 214.60

34.48 219.66 34.48 229.05 34.48 205.87 34.48 218.19

32.69 202.46 32.69 205.76 32.69 190.84 32.69 199.69

30.83 191.84 30.90 195.71 30.90 183.25 30.87 190.26

29.03 188.00 29.03 192.17 29.03 183.56 29.03 187.91

27.24 177.16 27.24 177.45 27.24 169.73 27.24 174.78

25.45 165.54 25.45 171.65 25.45 159.60 25.45 165.60

23.66 158.14 23.66 161.45 23.66 148.63 23.66 156.07

21.86 147.31 21.86 148.31 21.86 138.62 21.86 144.75

20.07 137.35 20.07 143.61 20.07 133.82 20.07 138.26

18.21 128.21 18.21 131.79 18.21 121.54 18.21 127.18

16.41 116.32 16.41 115.29 16.41 109.42 16.41 113.68

14.62 107.59 14.62 108.75 14.62 101.50 14.62 105.95

12.83 96.60 12.83 98.90 12.83 92.47 12.83 95.99

11.03 87.50 11.03 89.06 11.03 81.63 11.03 86.06

9.24 76.16 9.24 77.87 9.24 71.66 9.24 75.23

7.45 65.83 7.45 67.80 7.45 60.88 7.45 64.84

5.61 54.00 5.61 54.96 5.61 49.55 5.61 52.84

3.82 41.90 3.80 42.83 3.81 38.32 3.81 41.02

2.01 28.77 2.01 29.69 2.02 25.21 2.01 27.89

0.20 17.03 0.19 18.09 0.20 13.65 0.20 16.26

Average Stdev

YS 21.5 21.8 18.7 20.7 1.7

VS 5.7 5.8 5.5 5.7 0.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 124 266 70 153 102
D - 5

Set A1: CS-BX5 – BL45- L1 – Mixing Day – NIST code (folder SR 37-SR-36D)

SR-36D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.21 2.03 0.19 2.00 0.20 1.99 0.20 2.00

2.66 3.43 2.63 3.52 2.64 3.28 2.64 3.41

5.10 4.71 5.10 4.63 5.08 4.63 5.09 4.66

7.52 5.45 7.52 5.58 7.52 5.38 7.52 5.47

10.00 6.47 10.00 6.50 10.00 6.64 10.00 6.53

12.41 7.50 12.41 7.59 12.41 7.57 12.41 7.55

14.90 8.42 14.90 8.82 14.90 8.67 14.90 8.64

17.31 9.29 17.31 9.61 17.38 9.88 17.33 9.59

19.79 10.47 19.79 10.48 19.79 10.63 19.79 10.52

22.21 10.97 22.28 11.28 22.21 11.56 22.23 11.27

24.69 12.20 24.69 12.65 24.69 12.84 24.69 12.56

27.10 13.28 27.17 13.55 27.10 13.61 27.13 13.48

29.59 13.78 29.59 14.26 29.59 14.58 29.59 14.21

32.00 15.07 32.00 15.82 32.00 15.81 32.00 15.57

34.48 15.42 34.48 16.28 34.48 15.95 34.48 15.88

34.48 15.97 34.48 15.84 34.48 16.59 34.48 16.13

32.69 14.99 32.69 15.49 32.69 15.90 32.69 15.46

30.90 14.14 30.83 14.77 30.90 15.39 30.87 14.77

29.10 13.49 29.03 14.75 29.03 14.30 29.06 14.18

27.24 13.37 27.24 13.52 27.24 13.54 27.24 13.48

25.45 12.57 25.45 13.09 25.45 13.04 25.45 12.90

23.66 11.79 23.66 12.10 23.66 12.33 23.66 12.07

21.86 11.16 21.86 11.08 21.86 11.61 21.86 11.28

20.07 10.75 20.07 10.96 20.07 10.79 20.07 10.83

18.28 9.89 18.28 10.30 18.21 10.07 18.25 10.09

16.41 8.74 16.41 9.37 16.41 9.62 16.41 9.24

14.62 8.35 14.62 8.97 14.62 9.08 14.62 8.80

12.83 7.85 12.83 8.10 12.83 7.92 12.83 7.96

11.03 7.01 11.03 7.38 11.03 7.36 11.03 7.25

9.24 6.34 9.24 6.47 9.24 6.50 9.24 6.44

7.45 5.62 7.45 5.87 7.45 5.81 7.45 5.76

5.61 4.67 5.61 5.02 5.62 4.90 5.61 4.86

3.81 3.86 3.81 4.14 3.80 3.82 3.81 3.94

2.01 3.02 2.01 2.97 2.01 2.97 2.01 2.99

0.20 1.86 0.20 1.84 0.20 1.82 0.20 1.84

Average Stdev

YS 2.5 2.6 2.4 2.5 0.1

VS 0.4 0.4 0.4 0.4 0.0

R2 1.00 0.99 1.00 1.0 0.0

Hysteresis 1 4 4 3 2

Comment: Problem with mixer = material not mixed properly - a lot of sedimentation
D - 6

Set A3: CS-BX5 – BL45- L2 – 3 day – NIST code (folder SR 38-SR-36A)

SR-36A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.22 18.54 0.22 22.66 0.22 16.31 0.22 19.17

2.86 42.82 2.86 53.24 2.86 29.97 2.86 42.01

5.53 62.44 5.51 82.14 5.53 43.83 5.52 62.81

8.22 84.25 8.22 113.90 8.15 56.17 8.20 84.77

10.84 102.24 10.84 126.86 10.84 67.61 10.84 98.90

13.46 118.90 13.46 139.87 13.46 79.80 13.46 112.85

16.15 137.64 16.15 153.99 16.15 91.98 16.15 127.87

18.77 152.30 18.77 170.86 18.77 103.95 18.77 142.37

21.46 167.80 21.46 185.98 21.46 115.80 21.46 156.53

24.07 182.00 24.07 204.17 24.07 126.39 24.07 170.85

26.77 196.01 26.77 209.81 26.77 136.56 26.77 180.80

29.38 207.19 29.38 221.93 29.46 147.47 29.41 192.19

32.07 218.43 32.07 235.93 32.07 157.17 32.07 203.84

34.69 229.74 34.69 246.95 34.69 168.85 34.69 215.18

37.38 238.44 37.38 274.68 37.38 173.39 37.38 228.84

37.38 259.63 37.38 279.62 37.38 186.42 37.38 241.89

35.44 246.64 35.44 256.83 35.44 170.42 35.44 224.63

33.50 229.74 33.50 242.85 33.42 160.99 33.47 211.20

31.48 215.60 31.48 232.08 31.48 158.26 31.48 201.98

29.53 204.57 29.53 223.64 29.53 146.20 29.53 191.47

27.59 190.43 27.59 209.07 27.59 139.36 27.59 179.62

25.64 181.99 25.64 197.49 25.64 131.67 25.64 170.38

23.70 170.58 23.70 182.93 23.70 119.59 23.70 157.70

21.76 154.56 21.76 172.39 21.76 114.39 21.76 147.11

19.74 144.06 19.74 158.20 19.81 106.11 19.76 136.12

17.79 135.55 17.79 141.49 17.79 96.54 17.79 124.53

15.85 122.74 15.85 131.09 15.85 88.57 15.85 114.13

13.91 110.47 13.91 116.68 13.91 79.99 13.91 102.38

11.96 97.84 11.96 105.21 11.96 71.60 11.96 91.55

10.02 85.40 10.02 91.75 10.02 62.63 10.02 79.93

8.07 72.19 8.07 78.36 8.07 53.38 8.07 67.98

6.09 59.08 6.08 62.86 6.08 44.02 6.08 55.32

4.12 45.52 4.13 47.78 4.14 34.30 4.13 42.53

2.18 29.89 2.19 31.61 2.18 23.38 2.19 28.29

0.22 15.48 0.22 15.86 0.21 13.09 0.22 14.81

Average Stdev

YS 19.2 20.7 16.2 18.7 2.3

VS 6.4 6.8 4.5 5.9 1.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 238 557 54 283 255
D - 7

Set A3: CS-BX5 – BL12- L2 – 3 day – NIST code (folder SR 38-SR-36B)

SR-36B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 24.32 0.20 23.09 0.20 30.69 0.20 26.03

2.66 41.05 2.63 39.07 2.65 65.62 2.65 48.58

5.09 57.54 5.08 55.07 5.08 95.76 5.09 69.45

7.59 72.94 7.52 69.15 7.59 130.20 7.56 90.76

10.00 87.27 10.00 83.75 10.00 150.58 10.00 107.20

12.41 101.68 12.41 98.65 12.41 174.02 12.41 124.78

14.90 116.45 14.90 112.17 14.90 195.47 14.90 141.36

17.31 131.21 17.31 126.73 17.38 212.66 17.33 156.87

19.79 145.66 19.79 139.87 19.79 231.21 19.79 172.25

22.21 156.12 22.21 151.67 22.28 238.74 22.23 182.18

24.69 171.83 24.69 166.03 24.69 265.88 24.69 201.25

27.10 186.10 27.10 178.97 27.10 282.05 27.10 215.71

29.59 194.24 29.59 188.89 29.59 289.23 29.59 224.12

32.00 205.66 32.00 200.32 32.07 299.56 32.02 235.18

34.48 211.23 34.48 205.91 34.48 277.51 34.48 231.55

34.48 226.74 34.48 214.72 34.48 356.94 34.48 266.13

32.69 221.96 32.69 205.44 32.69 355.42 32.69 260.94

30.90 204.78 30.90 197.77 30.90 317.54 30.90 240.03

29.03 185.85 29.03 187.00 29.03 278.94 29.03 217.26

27.24 183.08 27.24 175.94 27.24 273.15 27.24 210.72

25.45 170.79 25.45 166.43 25.45 250.99 25.45 196.07

23.66 162.87 23.66 156.93 21.86 221.42 #REF! 180.41

21.86 154.49 21.86 149.38 20.07 197.61 21.86 167.16

20.07 137.97 20.07 137.94 18.21 186.06 20.07 153.99

18.21 129.92 18.21 128.63 16.41 181.57 18.21 146.70

16.41 123.92 16.41 118.70 14.62 158.14 16.41 133.59

14.62 111.23 14.62 108.91 12.83 142.15 14.62 120.76

12.83 100.21 12.83 98.96 11.03 125.30 12.83 108.16

11.03 90.37 11.03 88.36 9.24 109.77 11.03 96.16

9.24 79.55 9.24 77.78 7.45 90.88 9.24 82.74

7.45 67.56 7.45 66.93 5.61 76.04 7.45 70.18

5.61 57.09 5.61 55.81 3.79 58.81 5.61 57.24

3.81 45.06 3.79 43.95 2.01 38.00 3.80 42.33

2.02 31.25 2.02 30.42 0.20 20.19 2.02 27.29

0.20 19.06 0.20 18.41 0.20 18.73

Average Stdev

YS 22.4 23.5 18.4 21.4 2.7

VS 5.9 5.6 9.6 7.0 2.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 78 55 529 221 267
D - 8

Set A3: CS-BX5 – BL12- L1 – 3 day – NIST code (folder SR 38-SR-36C)

SR-36C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 35.16 0.16 30.66 0.20 22.69 0.19 29.50

2.65 73.44 2.65 62.19 2.65 40.90 2.65 58.85

5.09 116.70 5.10 101.70 5.09 58.52 5.09 92.31

7.59 151.41 7.52 134.58 7.52 74.65 7.54 120.22

10.00 174.57 10.00 155.26 10.00 90.88 10.00 140.24

12.41 196.46 12.41 176.52 12.41 106.21 12.41 159.73

14.90 218.52 14.90 196.13 14.90 121.86 14.90 178.84

17.31 239.30 17.31 215.78 17.31 138.00 17.31 197.69

19.79 260.52 19.79 228.70 19.79 150.89 19.79 213.37

22.21 282.07 22.28 241.97 22.21 166.54 22.23 230.19

24.69 295.12 24.69 262.10 24.69 177.89 24.69 245.03

27.10 311.65 27.10 276.30 27.10 190.92 27.10 259.62

29.59 330.31 29.59 285.24 29.59 205.23 29.59 273.60

32.00 345.55 32.00 282.71 32.00 218.25 32.00 282.17

34.48 372.21 34.48 267.67 34.48 233.54 34.48 291.14

34.48 393.71 34.48 344.01 34.48 239.65 34.48 325.79

32.69 364.95 32.69 352.64 32.69 221.12 32.69 312.90

30.90 341.87 30.90 308.65 30.83 210.18 30.87 286.90

29.03 334.05 29.03 268.23 29.10 204.39 29.06 268.89

27.24 308.79 27.24 264.49 27.24 191.62 27.24 254.97

25.45 291.85 25.45 246.17 25.45 179.56 25.45 239.19

23.66 273.16 23.66 223.94 23.66 168.86 23.66 221.99

21.86 253.04 21.86 214.92 21.86 157.49 21.86 208.48

20.07 239.42 20.07 194.31 20.00 146.86 20.05 193.53

18.21 220.67 18.28 183.47 18.21 138.33 18.23 180.82

16.41 198.11 16.41 173.68 16.41 126.31 16.41 166.03

14.62 181.72 14.62 154.96 14.62 115.33 14.62 150.67

12.83 164.85 12.83 144.62 12.83 104.79 12.83 138.09

11.03 145.82 11.03 122.65 11.03 93.20 11.03 120.55

9.24 127.31 9.24 108.34 9.24 81.77 9.24 105.81

7.45 108.44 7.38 91.58 7.45 69.67 7.43 89.90

5.61 87.91 5.61 75.71 5.59 57.49 5.60 73.70

3.81 66.69 3.81 58.64 3.81 44.61 3.81 56.65

2.01 43.26 2.00 37.18 1.99 30.10 2.00 36.85

0.19 22.46 0.20 20.05 0.20 17.63 0.20 20.05

Average Stdev

YS 27.3 19.7 21.7 22.9 3.9

VS 10.4 9.2 6.2 8.6 2.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 692 636 121 483 315
D - 9

Set A3: CS-BX5 – BL45- L1 – 3 day – NIST code (folder SR 38-SR-36D)

SR-36D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 18.80 0.19 14.94 0.20 14.35 0.20 16.03

2.64 31.39 2.64 24.36 2.63 24.10 2.64 26.62

5.10 39.51 5.10 31.65 5.09 29.11 5.10 33.43

7.52 45.20 7.59 38.79 7.52 33.82 7.54 39.27

10.00 51.12 10.00 45.66 10.00 38.23 10.00 45.01

12.41 55.98 12.41 52.81 12.48 42.38 12.44 50.39

14.90 61.06 14.90 59.54 14.90 46.35 14.90 55.65

17.38 66.00 17.31 65.30 17.31 50.34 17.33 60.54

19.79 70.36 19.79 71.02 19.79 54.02 19.79 65.13

22.21 74.24 22.21 76.10 22.21 57.71 22.21 69.35

24.69 80.78 24.69 81.51 24.69 60.95 24.69 74.41

27.10 86.08 27.10 86.17 27.10 65.30 27.10 79.19

29.59 89.90 29.59 90.17 29.59 70.28 29.59 83.45

32.00 95.23 32.00 94.53 32.00 73.96 32.00 87.91

34.48 96.17 34.48 96.41 34.48 77.63 34.48 90.07

34.48 104.16 34.48 103.90 34.48 77.76 34.48 95.27

32.69 99.76 32.69 101.50 32.69 75.48 32.69 92.25

30.90 93.79 30.90 95.51 30.90 72.50 30.90 87.27

29.03 92.07 29.10 87.20 29.03 68.33 29.06 82.54

27.24 84.54 27.24 84.42 27.24 65.84 27.24 78.27

25.45 81.36 25.45 80.21 25.45 63.04 25.45 74.87

23.66 75.41 23.66 76.60 23.66 60.50 23.66 70.84

21.86 71.50 21.86 72.38 21.86 57.41 21.86 67.09

20.07 69.36 20.00 66.55 20.07 53.14 20.05 63.02

18.28 64.73 18.21 63.48 18.21 50.33 18.23 59.51

16.41 59.66 16.41 61.52 16.41 48.41 16.41 56.53

14.62 56.05 14.62 56.21 14.62 45.09 14.62 52.45

12.83 52.66 12.83 51.29 12.83 40.95 12.83 48.30

11.03 47.29 11.03 46.81 11.03 37.83 11.03 43.98

9.24 42.62 9.24 42.22 9.24 34.13 9.24 39.66

7.45 43.32 7.45 37.08 7.45 30.38 7.45 36.93

5.62 25.80 5.59 32.54 5.61 26.78 5.61 28.37

3.80 25.79 3.80 27.36 3.79 22.42 3.80 25.19

2.01 20.92 1.99 21.27 2.01 17.77 2.00 19.98

0.20 14.93 0.20 15.21 0.20 12.69 0.20 14.28

Average Stdev

YS 17.5 17.9 16.1 17.1 1.0

VS 2.5 2.5 1.8 2.3 0.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 112 39 45 65 40

Comment: Problem with mixer = material not mixed properly - a lot of sedimentation
D - 10

Set A7: CS-BX5 – BL45- L2 – 7 day – NIST code (folder SR 39-SR-36A)

SR-36A

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.21 15.44 0.20 15.41 0.20 15.60 0.20 15.49

2.65 29.57 2.63 29.21 2.63 29.47 2.64 29.41

5.10 43.69 5.10 42.97 5.08 42.64 5.09 43.10

7.52 55.95 7.52 54.88 7.52 54.14 7.52 54.99

10.00 68.23 10.00 66.29 10.00 65.63 10.00 66.71

12.41 79.72 12.41 78.41 12.41 77.07 12.41 78.40

14.90 91.16 14.90 90.81 14.90 88.13 14.90 90.03

17.31 102.69 17.31 101.80 17.38 99.94 17.33 101.48

19.79 114.24 19.79 111.35 19.79 110.23 19.79 111.94

22.21 125.50 22.21 118.64 22.21 120.75 22.21 121.63

24.69 135.67 24.69 132.14 24.69 129.74 24.69 132.52

27.17 148.09 27.10 144.17 27.10 139.18 27.13 143.81

29.59 157.45 29.59 150.26 29.59 148.29 29.59 152.00

32.00 167.69 32.00 158.88 32.00 156.42 32.00 161.00

34.48 177.59 34.48 153.84 34.48 170.52 34.48 167.32

34.48 179.69 34.48 176.15 34.48 172.62 34.48 176.15

32.69 170.75 32.69 175.76 32.69 164.40 32.69 170.30

30.83 159.86 30.83 160.66 30.90 152.68 30.85 157.73

29.03 153.43 29.03 147.20 29.03 145.74 29.03 148.79

27.24 147.38 27.24 141.15 27.24 137.85 27.24 142.13

25.45 139.06 25.45 130.58 25.45 130.86 25.45 133.50

23.66 130.75 23.66 121.48 23.66 124.51 23.66 125.58

21.86 122.43 21.86 117.09 21.86 115.41 21.86 118.31

20.07 114.83 20.07 106.68 20.07 108.05 20.07 109.85

18.28 106.01 18.28 100.03 18.21 99.06 18.25 101.70

16.41 97.55 16.41 95.11 16.41 90.33 16.41 94.33

14.62 88.94 14.62 84.89 14.62 83.71 14.62 85.85

12.83 80.52 12.83 78.92 12.83 74.67 12.83 78.04

11.03 71.63 11.03 67.69 11.03 67.03 11.03 68.78

9.24 62.75 9.24 60.51 9.24 58.23 9.24 60.50

7.38 53.29 7.45 50.79 7.45 50.08 7.43 51.39

5.61 44.04 5.61 42.24 5.61 40.94 5.61 42.41

3.82 34.42 3.83 33.35 3.80 31.57 3.82 33.11

2.01 23.16 2.01 21.63 2.02 21.45 2.01 22.08

0.20 12.84 0.20 12.05 0.20 12.04 0.20 12.31

Average Stdev

YS 17.2 14.7 14.8 15.5 1.4

VS 4.8 4.7 4.6 4.7 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 46 41 91 59 28
D - 11

Set A7: CS-BX5 – BL12- L2 – 7 day – NIST code (folder SR 39-SR-36B)

SR-36B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.20 20.45 0.20 21.8 0.20 26.89 0.20 23.06

2.64 37.65 2.65 38.3 2.65 51.31 2.65 42.40

5.10 55.13 5.10 54.4 5.09 77.85 5.09 62.47

7.59 71.67 7.52 68.8 7.52 101.61 7.54 80.71

10.00 87.74 10.00 82.2 10.00 119.88 10.00 96.62

12.41 101.35 12.41 96.8 12.41 137.99 12.41 112.04

14.90 115.05 14.90 111.1 14.90 155.85 14.90 127.33

17.31 128.47 17.38 123.7 17.38 173.06 17.36 141.75

19.79 140.31 19.79 137.5 19.79 190.34 19.79 156.03

22.21 152.22 22.21 146.3 22.21 203.94 22.21 167.48

24.69 161.21 24.69 162.2 24.69 217.85 24.69 180.41

27.10 171.87 27.10 178.1 27.10 233.38 27.10 194.45

29.59 185.46 29.59 185.8 29.59 244.87 29.59 205.36

32.00 199.22 32.07 194.0 32.07 256.52 32.05 216.59

34.48 213.42 34.48 194.0 34.48 273.05 34.48 226.83

34.48 212.07 34.48 212.1 34.48 285.86 34.48 236.66

32.69 205.63 32.69 211.4 32.62 268.66 32.67 228.57

30.90 191.22 30.90 196.7 30.90 256.91 30.90 214.96

29.03 188.29 29.03 177.8 29.03 243.93 29.03 203.35

27.24 175.38 27.24 175.1 27.24 229.56 27.24 193.35

25.45 163.16 25.45 160.5 25.45 216.49 25.45 180.06

23.66 152.20 23.66 153.9 23.66 203.42 23.66 169.85

21.86 144.14 21.86 145.4 21.86 190.35 21.86 159.96

20.07 134.99 20.07 128.5 20.07 178.29 20.07 147.26

18.28 123.44 18.21 123.2 18.21 163.98 18.23 136.88

16.41 115.46 16.41 118.7 16.41 150.11 16.41 128.10

14.62 105.70 14.62 105.4 14.62 138.39 14.62 116.48

12.83 117.52 12.83 94.7 12.83 125.19 12.83 112.46

11.03 66.85 11.03 84.6 11.03 110.81 11.03 87.41

9.24 63.62 9.24 74.5 9.24 96.65 9.24 78.25

7.45 63.58 7.45 62.7 7.45 82.92 7.45 69.74

5.61 52.83 5.61 53.1 5.61 67.91 5.61 57.96

3.80 41.62 3.80 41.9 3.81 52.51 3.80 45.34

2.01 28.17 2.01 28.5 2.01 35.32 2.01 30.68

0.20 16.40 0.21 16.8 0.20 19.85 0.20 17.67

Average Stdev

YS 19.1 20.6 24.5 21.4 2.7

VS 5.7 5.7 7.6 6.3 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 168 17 319 168 151

Note: Run #B show shear rates in the down curve that are not equally spaced, e.g. 2 points at about 20 1/s not consecutive. 
D - 12

Set A7: CS-BX5 – BL12- L1 – 7 day – NIST code (folder SR 39-SR-36C)

SR-36C

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 15.98 0.20 22.56 0.21 16.02 0.20 18.18

2.64 30.08 2.65 51.56 2.66 30.58 2.65 37.41

5.08 44.93 5.10 76.67 5.10 43.94 5.10 55.18

7.59 57.67 7.52 99.17 7.52 56.49 7.54 71.11

10.00 69.74 10.00 120.29 10.00 67.83 10.00 85.95

12.41 81.79 12.48 138.21 12.41 80.01 12.44 100.00

14.90 94.08 14.90 154.41 14.90 92.24 14.90 113.57

17.38 106.06 17.38 171.24 17.31 103.48 17.36 126.93

19.79 117.43 19.79 186.12 19.79 114.74 19.79 139.43

22.21 129.39 22.21 199.80 22.21 124.01 22.21 151.07

24.69 139.86 24.69 215.18 24.69 136.01 24.69 163.68

27.10 150.49 27.10 229.18 27.10 148.09 27.10 175.92

29.59 162.45 29.59 241.60 29.59 156.94 29.59 187.00

32.00 171.25 32.00 254.11 32.00 165.87 32.00 197.08

34.48 181.12 34.48 263.88 34.48 172.50 34.48 205.84

34.48 181.72 34.48 285.81 34.48 179.69 34.48 215.74

32.62 175.08 32.69 270.33 32.69 173.58 32.67 206.33

30.90 166.65 30.83 256.17 30.83 163.97 30.85 195.60

29.03 157.78 29.03 240.43 29.03 151.37 29.03 183.19

27.24 150.05 27.24 225.11 27.24 146.79 27.24 173.98

25.45 141.73 25.45 214.31 25.45 136.99 25.45 164.35

23.66 135.53 23.66 197.79 23.66 130.15 23.66 154.49

21.86 125.88 21.86 186.20 21.86 122.31 21.86 144.79

20.07 115.75 20.07 172.64 20.07 110.77 20.07 133.06

18.21 107.87 18.21 158.18 18.21 103.77 18.21 123.28

16.41 99.87 16.41 145.66 16.41 97.30 16.41 114.28

14.62 91.35 14.62 133.94 14.62 87.95 14.62 104.42

12.83 82.29 12.83 120.63 12.83 79.09 12.83 94.00

11.03 73.68 11.03 105.96 11.03 70.89 11.03 83.51

9.24 64.25 9.24 92.42 9.24 61.83 9.24 72.83

7.45 54.92 7.38 78.31 7.45 52.44 7.43 61.89

5.61 45.24 5.60 63.87 5.59 43.52 5.60 50.87

3.79 35.15 3.82 48.69 3.81 33.99 3.81 39.28

2.01 23.73 2.01 31.70 1.99 22.82 2.00 26.09

0.20 13.22 0.21 16.04 0.20 12.90 0.20 14.05

Average Stdev

YS 17.6 19.2 16.0 17.6 1.6

VS 4.9 7.7 4.8 5.8 1.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 52 363 62 159 177
D - 13

Set A7: CS-BX5 – BL45- L1 – 7 day – NIST code (folder SR 39-SR-36D)

SR-36D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 18.51 0.20 14.91 0.21 16.86 0.20 16.76

2.65 29.41 2.63 24.80 2.64 28.72 2.64 27.65

5.09 36.47 5.10 28.95 5.10 34.29 5.10 33.23

7.59 41.48 7.52 32.94 7.52 39.78 7.54 38.07

10.00 45.82 10.00 36.62 10.00 44.44 10.00 42.29

12.41 51.36 12.41 40.09 12.41 48.44 12.41 46.63

14.90 56.46 14.90 43.60 14.90 52.26 14.90 50.77

17.38 61.14 17.31 46.76 17.31 56.82 17.33 54.91

19.79 65.73 19.79 50.11 19.79 60.49 19.79 58.78

22.21 69.48 22.28 53.65 22.21 65.06 22.23 62.73

24.69 75.21 24.69 57.64 24.69 69.19 24.69 67.35

27.10 80.35 27.10 61.08 27.10 73.96 27.10 71.80

29.59 84.63 29.59 64.46 29.59 78.47 29.59 75.86

32.00 88.89 32.00 68.29 32.00 83.31 32.00 80.16

34.48 90.35 34.48 72.37 34.48 88.80 34.48 83.84

34.48 95.50 34.48 72.17 34.48 89.12 34.48 85.60

32.62 94.11 32.69 69.30 32.69 84.13 32.67 82.51

30.90 89.07 30.83 66.32 30.90 80.54 30.87 78.64

29.03 82.61 29.03 64.68 29.03 78.69 29.03 75.33

27.24 79.68 27.24 61.55 27.24 74.53 27.24 71.92

25.45 76.17 25.45 58.75 25.45 71.03 25.45 68.65

23.66 72.50 23.66 55.34 23.66 66.78 23.66 64.87

21.86 68.95 21.86 53.00 21.86 63.35 21.86 61.76

20.07 63.75 20.07 51.59 20.07 61.31 20.07 58.88

18.21 60.76 18.28 47.93 18.21 57.32 18.23 55.34

16.41 59.04 16.41 44.15 16.41 52.40 16.41 51.86

14.62 54.11 14.62 41.92 14.62 49.88 14.62 48.64

12.83 49.29 12.83 39.38 12.83 45.88 12.83 44.85

11.03 45.41 11.03 35.70 11.03 42.32 11.03 41.14

9.24 41.00 9.24 32.56 9.24 37.93 9.24 37.16

7.45 36.21 7.38 29.11 7.45 34.22 7.43 33.18

5.61 31.95 5.60 25.45 5.61 29.56 5.61 28.99

3.79 26.92 3.82 21.49 3.82 24.81 3.81 24.41

2.02 21.13 2.01 17.00 2.01 19.44 2.01 19.19

0.21 15.37 0.21 12.30 0.20 14.07 0.20 13.91

Average Stdev

YS 18.6 15.8 17.4 17.3 1.4

VS 2.3 1.7 2.1 2.0 0.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 60 52 80 64 15

Comment: Problem with mixer = material not mixed properly - a lot of sedimentation
D - 14

Set B1: CS-BX1 – BL23- L2 – Mixing Day – NIST code (folder SR 41-SR-40A)

SR-40A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 20.7 0.20 22.70 0.20 26.4 0.23 23.29

2.64 44.9 2.66 39.59 2.64 57.4 2.65 47.29

5.08 60.9 5.10 56.16 5.10 84.6 5.09 67.24

7.59 76.5 7.52 70.56 7.52 113.3 7.54 86.81

10.00 90.7 10.00 85.97 10.00 137.1 10.00 104.57

12.41 105.6 12.41 100.93 12.41 157.0 12.41 121.18

14.90 120.7 14.90 116.09 14.90 173.5 14.90 136.76

17.31 135.9 17.31 129.40 17.31 184.0 17.31 149.77

19.79 148.9 19.79 143.60 19.79 199.4 19.79 163.98

22.21 163.3 22.21 157.94 22.21 214.9 22.21 178.72

24.69 176.1 24.69 172.13 24.69 225.7 24.69 191.32

27.10 187.6 27.10 184.94 27.17 234.8 27.13 202.46

29.59 200.6 29.59 196.17 29.59 250.2 29.59 215.67

32.00 213.8 32.00 207.49 32.00 270.0 32.00 230.43

34.48 225.8 34.48 216.29 34.48 294.8 34.48 245.63

34.48 232.0 34.48 220.92 34.48 294.6 34.48 249.21

32.69 221.5 32.69 213.61 32.69 265.2 32.69 233.46

30.90 207.2 30.83 202.84 30.83 254.9 30.85 221.66

29.03 195.5 29.03 194.23 29.03 265.3 29.03 218.34

27.24 189.0 27.24 183.40 27.24 238.2 27.24 203.54

25.45 180.4 25.45 174.03 25.45 227.7 25.45 194.04

23.66 167.7 23.66 163.20 23.66 206.8 23.66 179.21

21.86 158.3 21.86 153.82 21.86 193.5 21.86 168.54

20.07 148.6 20.07 144.80 20.07 193.2 20.07 162.22

18.21 138.0 18.28 133.53 18.28 174.0 18.25 148.51

16.41 129.3 16.41 122.90 16.41 151.5 16.41 134.55

14.62 117.6 14.62 113.01 14.62 142.9 14.62 124.51

12.83 106.4 12.83 102.75 12.83 130.6 12.83 113.25

11.03 95.5 11.03 91.48 11.03 116.0 11.03 101.01

9.24 83.8 9.24 80.42 9.24 101.9 9.24 88.72

7.45 71.9 7.45 68.62 7.45 87.5 7.45 75.99

5.62 59.8 5.61 56.71 5.60 70.3 5.61 62.26

3.81 46.6 3.81 44.17 3.82 53.9 3.81 48.22

2.01 31.8 1.99 29.85 2.01 35.6 2.01 32.39

0.20 18.4 0.19 17.09 0.21 19.2 0.20 18.24

Average Stdev

YS 25.3 23.4 26.6 25.1 1.6

VS 6.0 5.9 7.8 6.6 1.0

R2 1.00 1.00 0.99 1.0 0.0

Hysteresis 63 45 503 204 259
D - 15

Set B1: CS-BX1 – BL23- L1 – Mixing Day – NIST code (folder SR 41-SR-40B)

SR-40B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 27.5 0.20 26.40 0.20 28.0 0.20 27.32

2.63 46.0 2.64 43.09 2.65 48.4 2.64 45.82

5.09 63.3 5.10 59.77 5.08 67.2 5.09 63.45

7.59 77.6 7.52 74.86 7.52 84.8 7.54 79.08

10.00 92.4 10.00 89.31 10.00 101.9 10.00 94.52

12.41 107.4 12.41 103.67 12.41 117.9 12.41 109.64

14.90 122.3 14.90 117.71 14.90 134.7 14.90 124.89

17.38 137.7 17.31 132.07 17.31 149.5 17.33 139.76

19.79 151.2 19.79 145.20 19.79 161.4 19.79 152.60

22.21 165.1 22.21 157.01 22.21 177.0 22.21 166.34

24.69 179.2 24.69 168.66 24.69 193.8 24.69 180.57

27.10 192.1 27.10 180.50 27.10 207.8 27.10 193.46

29.59 203.3 29.59 191.96 29.59 218.6 29.59 204.61

32.00 214.6 32.00 202.50 32.00 226.1 32.00 214.41

34.48 223.4 34.48 218.72 34.48 231.6 34.48 224.58

34.48 233.8 34.48 223.20 34.48 249.9 34.48 235.62

32.69 223.3 32.69 209.78 32.62 243.2 32.67 225.42

30.90 211.7 30.90 199.55 30.90 229.8 30.90 213.67

29.03 198.6 29.03 186.30 29.03 207.3 29.03 197.38

27.24 189.9 27.24 178.89 27.24 204.8 27.24 191.20

25.45 181.3 25.45 170.24 25.45 192.1 25.45 181.22

23.66 170.6 23.66 160.81 23.66 181.0 23.66 170.83

21.86 160.0 21.86 149.95 21.86 169.5 21.86 159.81

20.07 147.5 20.07 140.02 20.07 154.9 20.07 147.44

18.28 137.5 18.21 130.88 18.21 144.2 18.23 137.54

16.41 129.7 16.41 119.74 16.41 138.5 16.41 129.31

14.62 118.5 14.62 109.95 14.62 125.2 14.62 117.89

12.83 107.1 12.83 99.17 12.83 110.9 12.83 105.72

11.03 96.4 11.03 89.64 11.03 100.1 11.03 95.36

9.24 84.8 9.24 78.55 9.24 87.8 9.24 83.72

7.45 72.9 7.38 67.71 7.45 75.0 7.43 71.86

5.62 61.0 5.60 56.43 5.61 62.9 5.61 60.13

3.81 48.1 3.82 44.32 3.81 49.3 3.81 47.26

2.01 33.4 2.01 31.41 2.01 34.1 2.01 32.94

0.20 20.5 0.21 19.34 0.20 20.3 0.20 20.03

Average Stdev

YS 26.1 24.4 24.6 25.0 0.9

VS 6.1 5.8 6.6 6.1 0.4

R2 1.00 0.99 1.00 1.0 0.0

Hysteresis 90 104 173 122 45
D - 16

Set B1: CS-BX1 – BL28- L2 – Mixing Day – NIST code (folder SR 41-SR-40C)

SR-40C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 22.6 0.19 21.6 0.19 21.1 0.19 21.78

2.66 38.2 2.65 38.1 2.65 37.3 2.65 37.86

5.10 54.4 5.11 55.7 5.09 53.4 5.10 54.47

7.52 69.1 7.52 71.8 7.59 68.9 7.54 69.93

10.00 84.4 10.00 87.0 10.00 82.7 10.00 84.69

12.41 98.4 12.41 101.4 12.41 97.1 12.41 98.95

14.90 113.0 14.90 115.8 14.90 111.8 14.90 113.54

17.31 128.8 17.31 130.5 17.38 125.8 17.33 128.39

19.79 141.8 19.79 143.3 19.79 139.4 19.79 141.52

22.21 156.2 22.21 160.3 22.21 150.8 22.21 155.75

24.69 169.0 24.69 171.7 24.69 165.1 24.69 168.60

27.10 182.0 27.10 184.7 27.10 179.6 27.10 182.10

29.59 194.7 29.59 199.0 29.59 190.8 29.59 194.84

32.00 206.4 32.00 210.2 32.00 198.5 32.00 205.02

34.48 223.8 34.48 222.3 34.48 200.9 34.48 215.65

34.48 219.2 34.48 220.9 34.48 220.5 34.48 220.21

32.69 209.0 32.69 211.7 32.69 210.0 32.69 210.22

30.83 199.6 30.90 206.7 30.90 195.7 30.87 200.64

29.03 190.8 29.03 189.6 29.03 178.9 29.03 186.45

27.24 181.3 27.24 183.6 27.24 175.0 27.24 179.95

25.45 174.0 25.45 173.5 25.45 166.2 25.45 171.22

23.66 163.2 23.66 165.5 23.66 160.2 23.66 162.98

21.86 153.2 21.86 155.2 21.86 149.9 21.86 152.76

20.00 144.8 20.07 142.4 20.07 136.5 20.05 141.21

18.28 134.0 18.28 134.0 18.21 128.6 18.25 132.18

16.41 121.4 16.41 126.1 16.41 120.0 16.41 122.54

14.62 112.9 14.62 115.4 14.62 109.8 14.62 112.70

12.83 103.4 12.83 102.6 12.83 96.6 12.83 100.87

11.03 92.1 11.03 92.9 11.03 88.6 11.03 91.21

9.24 81.4 9.24 81.0 9.24 76.9 9.24 79.80

7.45 69.8 7.38 69.2 7.45 66.3 7.43 68.42

5.61 57.8 5.60 58.2 5.61 54.9 5.61 56.98

3.81 45.4 3.82 45.6 3.80 42.2 3.81 44.43

1.99 31.2 2.01 31.2 2.01 29.5 2.00 30.61

0.20 18.6 0.20 18.1 0.20 17.2 0.20 17.95

Average Stdev

YS 25.5 25.0 22.1 24.2 1.8

VS 5.8 5.8 5.7 5.8 0.1

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 9 52 35 32 22
D - 17

Set B1: CS-BX1 – BL28- L1 – Mixing Day – NIST code (folder SR 41-SR-40D)

SR-40D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.19 30.4 0.21 29.5 0.21 27.96 0.20 29.28

2.63 49.7 2.64 47.6 2.64 46.03 2.64 47.79

5.10 64.9 5.10 62.4 5.10 63.83 5.10 63.72

7.52 79.8 7.52 77.5 7.52 80.45 7.52 79.23

10.00 95.3 10.00 91.7 10.00 95.61 10.00 94.19

12.41 111.4 12.41 107.2 12.41 109.38 12.41 109.32

14.90 126.6 14.90 122.2 14.90 125.74 14.90 124.86

17.31 142.2 17.31 135.6 17.31 141.29 17.31 139.70

19.79 155.4 19.79 148.8 19.79 154.54 19.79 152.91

22.21 167.1 22.21 160.6 22.21 166.25 22.21 164.66

24.69 184.2 24.69 174.5 24.69 182.82 24.69 180.50

27.10 199.8 27.17 187.9 27.17 197.41 27.15 195.03

29.59 210.6 29.59 198.4 29.59 209.17 29.59 206.05

32.00 218.1 32.00 207.4 32.00 221.13 32.00 215.54

34.48 223.6 34.48 209.7 34.48 227.81 34.48 220.40

34.48 245.0 34.48 229.4 34.48 238.24 34.48 237.53

32.69 236.1 32.69 218.9 32.69 229.61 32.69 228.19

30.90 220.1 30.90 204.6 30.83 215.02 30.87 213.24

29.10 198.7 29.03 197.8 29.03 206.58 29.06 201.02

27.24 193.0 27.24 186.4 27.24 194.42 27.24 191.28

25.45 183.7 25.45 174.9 25.45 185.18 25.45 181.28

23.66 174.5 23.66 162.0 23.66 173.04 23.66 169.84

21.86 164.3 21.86 153.9 21.86 161.83 21.86 160.01

20.07 147.8 20.07 146.6 20.07 154.62 20.07 149.66

18.21 141.3 18.28 135.3 18.28 143.62 18.25 140.07

16.41 135.5 16.41 124.7 16.41 128.89 16.41 129.71

14.62 121.3 14.62 113.8 14.62 120.11 14.62 118.40

12.83 108.7 12.83 104.5 12.83 110.26 12.83 107.83

11.03 99.0 11.03 93.4 11.03 98.06 11.03 96.79

9.24 86.5 9.24 82.8 9.24 86.57 9.24 85.29

7.45 74.2 7.45 71.4 7.38 74.75 7.43 73.44

5.61 62.7 5.59 59.5 5.61 62.26 5.60 61.49

3.81 49.6 3.82 47.6 3.81 49.16 3.82 48.77

1.99 34.7 2.01 33.2 2.01 34.46 2.00 34.11

0.20 21.4 0.20 21.1 0.21 21.49 0.20 21.34

Average Stdev

YS 26.0 25.5 26.7 26.0 0.6

VS 6.3 5.9 6.2 6.1 0.2

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 108 115 90 105 13
D - 18

Set B3: CS-BX1 – BL23- L2 – 4 day – NIST code (folder SR 42-SR-40A)

SR-40A

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.21 17.5 0.20 19.8 0.20 16.9 0.20 18.03

2.64 36.5 2.63 44.3 2.65 35.5 2.64 38.75

5.09 53.3 5.10 67.2 5.11 52.7 5.10 57.76

7.52 70.0 7.52 87.6 7.52 67.7 7.52 75.10

10.00 84.9 10.00 106.5 10.00 82.8 10.00 91.42

12.41 100.7 12.41 123.9 12.41 97.7 12.41 107.40

14.90 115.2 14.90 142.1 14.90 112.8 14.90 123.35

17.31 129.4 17.31 156.7 17.31 127.0 17.31 137.72

19.79 144.9 19.79 171.2 19.79 139.4 19.79 151.85

22.21 156.7 22.21 182.9 22.28 155.5 22.23 165.04

24.69 169.6 24.69 198.0 24.69 165.7 24.69 177.75

27.10 184.1 27.17 211.0 27.17 178.7 27.15 191.25

29.59 193.1 29.59 221.5 29.59 190.7 29.59 201.76

32.07 203.6 32.00 231.7 32.00 200.1 32.02 211.79

34.48 215.7 34.48 231.9 34.48 211.0 34.48 219.55

34.48 230.8 34.48 262.3 34.48 219.7 34.48 237.59

32.69 216.1 32.69 253.8 32.69 209.1 32.69 226.32

30.90 201.9 30.83 235.4 30.90 197.4 30.87 211.58

29.03 191.3 29.03 219.9 29.03 181.8 29.03 197.68

27.24 181.3 27.24 206.7 27.24 176.9 27.24 188.30

25.45 170.7 25.45 195.0 25.45 164.5 25.45 176.72

23.66 160.0 23.66 179.6 23.66 158.8 23.66 166.13

21.86 149.3 21.86 169.2 21.86 147.0 21.86 155.18

20.07 136.2 20.07 155.9 20.07 132.6 20.07 141.53

18.21 126.8 18.28 144.8 18.28 124.2 18.25 131.94

16.41 119.3 16.41 134.5 16.41 116.7 16.41 123.50

14.62 107.4 14.62 120.0 14.62 104.4 14.62 110.62

12.83 96.4 12.83 109.9 12.83 92.7 12.83 99.65

11.03 85.6 11.03 95.9 11.03 82.9 11.03 88.17

9.24 74.5 9.24 84.2 9.24 72.3 9.24 76.99

7.45 62.8 7.45 70.2 7.45 60.2 7.45 64.41

5.61 51.3 5.61 57.0 5.60 49.6 5.61 52.64

3.80 39.2 3.81 43.5 3.81 38.1 3.81 40.25

2.01 25.5 2.00 27.4 2.01 24.6 2.01 25.86

0.20 13.3 0.19 13.4 0.20 12.6 0.20 13.11

Average Stdev

YS 15.9 15.5 15.7 15.7 0.2

VS 6.1 7.1 5.9 6.4 0.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 127 306 154 196 97
D - 19

Set B3: CS-BX1 – BL23- L1 – 4 day – NIST code (folder SR 42-SR-40B)

SR-40B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.23 25.6 0.21 21.09951 0.20 20.6 0.21 22.41

2.63 64.5 2.65 38.26 2.64 36.8 2.64 46.52

5.10 103.5 5.09 54.75 5.10 54.4 5.10 70.87

7.52 129.7 7.59 70.29 7.52 69.0 7.54 89.66

10.00 150.3 10.00 84.83 10.00 83.1 10.00 106.07

12.41 173.0 12.41 99.99 12.41 97.9 12.41 123.63

14.90 192.6 14.90 115.15 14.90 112.5 14.90 140.09

17.31 214.1 17.38 127.57 17.31 123.7 17.33 155.14

19.79 233.8 19.79 138.76 19.79 137.8 19.79 170.14

22.28 252.1 22.21 150.20 22.21 151.0 22.23 184.44

24.69 269.7 24.69 164.68 24.69 161.3 24.69 198.56

27.17 285.6 27.10 176.30 27.10 173.0 27.13 211.63

29.59 299.4 29.59 187.54 29.59 183.4 29.59 223.46

32.00 309.8 32.07 201.26 32.00 196.8 32.02 235.95

34.48 315.4 34.48 211.31 34.48 202.4 34.48 243.01

34.48 348.8 34.48 221.43 34.48 212.1 34.48 260.75

32.69 341.0 32.69 213.74 32.69 210.4 32.69 255.05

30.90 318.6 30.90 195.34 30.83 194.2 30.87 236.05

29.03 287.6 29.03 187.53 29.03 179.6 29.03 218.25

27.24 280.8 27.24 178.37 27.24 174.8 27.24 211.31

25.45 263.3 25.45 164.65 25.45 161.7 25.45 196.54

23.66 249.6 23.66 155.15 23.66 153.6 23.66 186.14

21.86 233.9 21.86 146.96 21.86 145.9 21.86 175.60

20.07 209.4 20.00 136.20 20.00 130.6 20.02 158.74

18.21 193.9 18.21 125.64 18.28 123.6 18.23 147.73

16.41 185.0 16.41 118.53 16.41 118.3 16.41 140.62

14.62 166.9 14.62 107.32 14.62 105.4 14.62 126.54

12.83 149.3 12.83 98.22 12.83 94.7 12.83 114.07

11.03 131.4 11.03 86.09 11.03 84.8 11.03 100.75

9.24 114.7 9.24 76.18 9.24 74.4 9.24 88.45

7.38 96.7 7.45 64.44 7.45 62.8 7.43 74.66

5.60 79.9 5.61 53.67 5.60 52.8 5.60 62.13

3.81 61.5 3.81 42.44 3.81 41.3 3.81 48.42

2.01 40.2 2.02 28.30 2.00 28.0 2.01 32.15

0.20 21.3 0.20 16.40 0.20 16.2 0.20 17.96

Average Stdev

YS 25.1 20.0 19.9 21.7 3.0

VS 9.4 5.8 5.7 7.0 2.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 499 80 83 221 241
D - 20

Set B3: CS-BX1 – BL28- L2 – 4 day – NIST code (folder SR 42-SR-40C)

SR-40C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 18.1 0.21 16.9 0.20 17.7 0.20 17.58

2.65 32.5 2.64 31.2 2.66 32.3 2.65 31.99

5.10 47.3 5.09 44.8 5.09 45.3 5.09 45.83

7.52 60.2 7.52 57.9 7.59 57.5 7.54 58.54

10.00 73.8 10.00 70.0 10.00 69.6 10.00 71.15

12.41 86.0 12.41 82.0 12.41 81.6 12.41 83.16

14.90 97.7 14.90 93.5 14.90 93.3 14.90 94.83

17.38 111.5 17.38 105.5 17.38 105.3 17.38 107.41

19.79 122.0 19.79 116.9 19.79 115.6 19.79 118.16

22.28 133.8 22.21 125.8 22.21 127.3 22.23 128.96

24.69 146.1 24.69 137.8 24.69 137.8 24.69 140.58

27.10 157.6 27.10 149.9 27.10 151.4 27.10 152.95

29.59 167.8 29.59 158.7 29.59 159.9 29.59 162.14

32.00 172.9 32.00 167.7 32.00 165.6 32.00 168.72

34.48 176.3 34.48 174.3 34.48 174.3 34.48 174.95

34.48 195.3 34.48 181.5 34.48 187.3 34.48 188.01

32.69 191.6 32.69 176.2 32.69 175.0 32.69 180.92

30.90 175.7 30.90 165.7 30.90 166.0 30.90 169.15

29.03 158.0 29.03 152.6 29.03 151.5 29.03 154.02

27.24 156.3 27.24 148.6 27.24 146.4 27.24 150.44

25.45 145.2 25.45 141.0 25.45 138.8 25.45 141.66

23.66 136.4 23.66 132.9 23.66 134.1 23.66 134.43

21.86 130.5 21.86 123.2 21.86 124.9 21.86 126.19

20.07 115.1 20.07 111.7 20.07 111.7 20.07 112.82

18.21 109.5 18.21 104.5 18.21 104.5 18.21 106.18

16.41 107.0 16.41 98.6 16.41 98.9 16.41 101.50

14.62 94.3 14.62 89.3 14.62 89.3 14.62 90.93

12.83 84.8 12.83 79.6 12.83 79.2 12.83 81.18

11.03 74.7 11.03 71.8 11.03 71.7 11.03 72.73

9.24 66.1 9.24 62.4 9.24 62.4 9.24 63.61

7.45 55.3 7.45 53.0 7.45 52.9 7.45 53.75

5.60 46.5 5.61 44.1 5.62 44.0 5.61 44.85

3.82 36.7 3.79 34.4 3.80 34.3 3.80 35.12

2.01 24.2 2.01 23.4 2.01 23.4 2.01 23.68

0.20 14.0 0.19 13.6 0.20 13.5 0.20 13.71

Average Stdev

YS 16.4 16.2 15.9 16.2 0.3

VS 5.2 4.9 4.9 5.0 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 59 74 78 70 10
D - 21

Set B3: CS-BX1 – BL28- L1 – 4 day – NIST code (folder SR 42-SR-40D)

SR-40D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 22.4 0.20 23.26 0.20 23.3 0.20 22.97

2.64 38.7 2.66 40.44 2.65 40.4 2.65 39.86

5.08 55.3 5.10 57.46 5.09 57.5 5.09 56.74

7.52 70.1 7.52 72.63 7.52 72.6 7.52 71.80

10.00 85.0 10.00 88.36 10.00 88.4 10.00 87.23

12.41 99.1 12.41 103.09 12.41 103.1 12.41 101.77

14.90 113.4 14.90 117.34 14.90 117.3 14.90 116.02

17.31 127.6 17.31 131.18 17.31 131.2 17.31 129.99

19.79 140.8 19.79 145.38 19.79 145.4 19.79 143.84

22.21 152.6 22.21 159.72 22.21 159.7 22.21 157.33

24.69 165.6 24.69 171.19 24.69 171.2 24.69 169.32

27.10 178.7 27.10 181.39 27.10 181.4 27.10 180.50

29.59 190.1 29.59 194.52 29.59 194.5 29.59 193.03

32.00 198.2 32.00 208.16 32.00 208.2 32.00 204.85

34.48 205.9 34.48 225.59 34.48 225.6 34.48 219.03

34.48 212.1 34.48 219.15 34.48 219.2 34.48 216.80

32.62 207.4 32.69 206.21 32.69 206.2 32.67 206.60

30.90 199.1 30.83 201.49 30.90 201.5 30.87 200.70

29.03 180.3 29.10 198.16 29.10 198.2 29.08 192.20

27.24 176.5 27.24 180.71 27.24 180.7 27.24 179.31

25.45 166.3 25.45 173.42 25.45 173.4 25.45 171.06

23.66 158.4 23.66 161.14 23.66 161.1 23.66 160.24

21.86 148.1 21.86 150.66 21.86 150.7 21.86 149.80

20.07 134.7 20.00 145.71 20.07 145.7 20.05 142.04

18.21 125.2 18.28 133.54 18.28 133.5 18.25 130.77

16.41 118.8 16.41 119.66 16.41 119.7 16.41 119.38

14.62 108.6 14.62 110.76 14.62 110.8 14.62 110.03

12.83 95.7 12.83 102.10 12.83 102.1 12.83 99.95

11.03 86.9 11.03 90.22 11.03 90.2 11.03 89.11

9.24 75.5 9.24 79.65 9.24 79.6 9.24 78.28

7.45 64.9 7.45 67.92 7.45 67.9 7.45 66.91

5.61 53.9 5.60 56.12 5.61 56.1 5.61 55.39

3.80 41.8 3.80 44.29 3.80 44.3 3.80 43.46

2.02 28.9 1.99 30.12 1.99 30.1 2.00 29.70

0.20 17.0 0.20 17.97 0.20 18.0 0.20 17.66

Average Stdev

YS 21.4 23.5 23.6 22.8 1.2

VS 5.7 5.8 5.8 5.8 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 113 122 123 119 5
D - 22

Set B7: CS-BX1 – BL23- L2 – 7 day – NIST code (folder SR 43-SR-40A)

SR-40A

Run# A Run# C Run# D Average

SR SS SR SS SR SS SR SS

0.26 13.7 0.20 23.3 0.21 17.5 0.22 18.19

2.65 37.6 2.66 57.4 2.65 36.7 2.65 43.92

5.09 54.5 5.10 83.8 5.10 55.6 5.10 64.63

7.52 69.9 7.52 108.2 7.59 73.0 7.54 83.73

10.00 86.3 10.00 128.6 10.00 89.9 10.00 101.57

12.41 102.0 12.41 148.1 12.41 106.7 12.41 118.95

14.90 117.1 14.90 168.8 14.90 123.0 14.90 136.33

17.38 133.6 17.31 185.9 17.38 138.9 17.36 152.78

19.79 146.9 19.79 201.6 19.79 154.7 19.79 167.74

22.21 163.3 22.21 214.4 22.21 169.8 22.21 182.51

24.69 174.6 24.69 232.4 24.69 182.4 24.69 196.47

27.10 184.7 27.10 247.6 27.10 199.6 27.10 210.62

29.59 199.1 29.59 257.9 29.59 211.6 29.59 222.88

32.00 209.0 32.00 269.0 32.00 220.9 32.00 232.98

34.48 223.1 34.48 284.0 34.48 232.9 34.48 246.67

34.48 229.5 34.48 304.9 34.48 236.3 34.48 256.91

32.62 208.6 32.69 286.7 32.62 233.4 32.64 242.89

30.90 201.8 30.90 272.6 30.90 222.6 30.90 232.35

29.03 193.7 29.10 250.7 29.03 202.6 29.06 215.65

27.24 182.8 27.24 239.3 27.24 194.1 27.24 205.41

25.45 176.5 25.45 226.6 25.45 181.9 25.45 195.03

23.66 164.4 23.66 216.0 23.66 174.8 23.66 185.10

21.86 151.9 21.86 198.9 21.86 163.3 21.86 171.37

20.07 144.2 20.07 185.4 20.07 150.4 20.07 160.02

18.21 130.9 18.21 170.1 18.21 138.5 18.21 146.48

16.41 116.5 16.41 152.2 16.41 129.9 16.41 132.86

14.62 109.3 14.62 142.0 14.62 118.7 14.62 123.32

12.83 96.8 12.83 124.9 12.83 104.2 12.83 108.65

11.03 87.2 11.03 112.0 11.03 93.9 11.03 97.72

9.24 75.1 9.24 96.5 9.24 81.0 9.24 84.19

7.45 64.6 7.45 82.4 7.45 68.6 7.45 71.88

5.61 50.9 5.61 65.3 5.61 56.1 5.61 57.45

3.81 38.1 3.81 48.6 3.79 42.1 3.80 42.95

2.01 25.1 1.99 31.1 2.01 27.4 2.01 27.86

0.20 12.4 0.21 14.5 0.20 13.6 0.20 13.53

Average Stdev

YS 16.7 18.2 18.9 17.9 1.1

VS 6.1 8.2 6.5 7.0 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 179 498 97 258 212
D - 23

Set B7: CS-BX1 – BL23- L1 – 7 day – NIST code (folder SR 43-SR-40B)

SR-40B

Run# E Run# F Run# G Average

SR SS SR SS SR SS SR SS

0.21 26.3 0.20 22.3 0.19 20.3 0.20 22.94

2.65 51.8 2.83 74.0 2.64 37.0 2.71 54.28

5.09 74.9 5.08 42.2 5.11 53.8 5.09 56.99

7.52 94.5 7.52 67.1 7.52 72.6 7.52 78.07

10.00 115.9 10.00 87.8 8.00 81.1 9.33 94.93

12.41 132.9 12.34 111.7 12.41 91.3 12.39 111.97

14.90 149.8 14.90 97.6 14.90 112.7 14.90 120.03

17.31 166.8 17.38 125.1 17.31 126.7 17.33 139.53

19.79 186.4 19.79 138.5 19.79 139.5 19.79 154.84

22.21 208.5 22.21 151.1 22.28 151.7 22.23 170.41

24.69 210.8 24.69 165.4 24.69 166.6 24.69 180.94

27.10 223.0 27.10 176.9 27.10 179.0 27.10 192.96

29.59 241.0 29.59 191.1 29.59 188.9 29.59 206.98

32.00 253.9 32.07 204.3 32.00 196.6 32.02 218.27

34.48 300.4 34.48 212.2 34.48 195.8 34.48 236.14

34.48 280.5 34.48 221.4 34.48 220.5 34.48 240.83

32.69 240.9 32.69 208.0 32.69 218.7 32.69 222.52

30.90 234.7 30.90 195.1 30.90 199.9 30.90 209.91

29.03 248.4 29.03 188.2 29.03 178.7 29.03 205.08

27.24 225.1 27.24 178.1 27.24 176.0 27.24 193.05

25.45 214.2 25.45 168.7 25.45 163.6 25.45 182.18

23.66 200.2 23.66 157.9 23.66 153.6 23.66 170.56

21.86 186.1 21.86 148.5 21.86 146.6 21.86 160.39

20.07 184.7 20.07 137.1 20.07 130.5 20.07 150.75

18.21 164.8 18.21 127.7 18.28 123.2 18.23 138.61

16.41 139.7 16.41 118.9 16.41 118.7 16.41 125.78

14.62 134.5 14.62 108.6 14.62 105.0 14.62 116.01

12.83 122.3 12.83 97.5 12.83 95.7 12.83 105.16

11.03 110.2 11.03 86.9 11.03 83.7 11.03 93.59

9.24 96.0 9.24 76.0 9.24 74.2 9.24 82.05

7.45 83.0 7.45 65.0 7.38 62.1 7.43 70.03

5.61 66.1 5.61 53.6 5.61 52.1 5.61 57.27

3.80 50.4 3.80 41.6 3.83 40.9 3.81 44.30

2.01 33.9 2.01 28.1 2.01 26.8 2.01 29.58

0.21 18.3 0.19 16.2 0.19 15.2 0.20 16.57

Average Stdev

YS 26.0 20.4 17.6 21.3 4.3

VS 7.2 5.8 5.9 6.3 0.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 366 127 104 199 145
D - 24

Set B7: CS-BX1 – BL28- L2 – 7 day – NIST code (folder SR 43-SR-40C)

SR-40C

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 23.1 0.20 24.4 0.20 26.7 0.20 24.72

2.66 50.0 2.65 50.3 2.66 68.7 2.65 56.35

5.10 73.3 5.10 76.0 5.10 109.0 5.10 86.08

7.52 96.0 7.59 100.2 7.52 152.6 7.54 116.29

10.00 116.3 10.00 115.9 10.00 170.4 10.00 134.19

12.41 134.0 12.41 133.6 12.41 188.3 12.41 151.97

14.90 149.6 14.90 152.6 14.90 206.8 14.90 169.65

17.31 167.9 17.31 168.6 17.31 225.2 17.31 187.25

19.79 184.1 19.79 184.7 19.79 241.8 19.79 203.50

22.21 206.1 22.28 203.1 22.21 259.7 22.23 222.95

24.69 209.9 24.69 218.8 24.69 270.6 24.69 233.11

27.10 219.0 27.10 231.8 27.10 287.9 27.10 246.27

29.59 237.8 29.59 243.6 29.59 307.1 29.59 262.84

32.00 253.5 32.07 256.1 32.00 321.2 32.02 276.94

34.48 289.2 34.48 261.8 34.48 346.8 34.48 299.26

34.48 270.6 34.48 288.5 34.48 365.8 34.48 308.28

32.69 257.9 32.69 277.2 32.69 328.1 32.69 287.75

30.83 246.1 30.90 257.6 30.83 315.7 30.85 273.13

29.03 250.7 29.03 239.9 29.10 312.5 29.06 267.70

27.24 225.7 27.24 227.8 27.24 287.4 27.24 246.97

25.45 210.7 25.45 214.7 25.45 273.6 25.45 232.98

23.66 192.4 23.66 201.6 23.66 256.2 23.66 216.77

21.86 182.2 21.86 190.5 21.86 236.0 21.86 202.90

20.00 173.5 20.07 173.5 20.07 221.1 20.05 189.38

18.28 161.7 18.21 160.4 18.28 202.2 18.25 174.76

16.41 149.6 16.41 152.2 16.41 185.8 16.41 162.57

14.62 133.2 14.62 136.5 14.62 171.3 14.62 146.99

12.83 124.7 12.83 123.1 12.83 149.7 12.83 132.50

11.03 106.2 11.03 108.6 11.03 135.7 11.03 116.81

9.17 94.0 9.24 95.4 9.24 116.4 9.22 101.90

7.38 78.9 7.45 80.2 7.45 98.8 7.43 85.94

5.61 65.4 5.61 65.8 5.61 79.8 5.61 70.32

3.81 50.7 3.81 50.5 3.81 59.8 3.81 53.64

2.00 31.9 2.01 32.8 1.99 38.5 2.00 34.43

0.20 16.6 0.21 17.1 0.20 19.0 0.20 17.58

Average Stdev

YS 23.3 21.1 24.2 22.9 1.6

VS 7.4 7.7 9.7 8.3 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 324 273 736 444 253
D - 25

Set B7: CS-BX1 – BL28- L1 – 7 day – NIST code (folder SR 43-SR-40D)

SR-40D

Run# M Run# N Average

SR SS SR SS SR SS SR SS

0.20 21.9 0.19 32.3 0.20 27.08

2.63 38.5 2.66 63.9 2.64 51.19

5.10 54.9 5.09 94.6 5.09 74.76

7.52 70.0 7.52 122.6 7.52 96.29

10.00 84.8 10.00 141.5 10.00 113.11

12.41 99.2 12.41 163.0 12.41 131.07

14.90 113.6 14.90 184.0 14.90 148.81

17.31 128.5 17.31 202.0 17.31 165.26

19.79 143.0 19.79 221.3 19.79 182.16

22.21 154.7 22.21 234.0 22.21 194.34

24.69 169.9 24.69 255.9 24.69 212.93

27.17 181.7 27.10 273.4 27.14 227.52

29.59 193.8 29.59 283.4 29.59 238.61

32.00 207.8 32.00 294.6 32.00 251.21

34.48 214.5 34.48 297.0 34.48 255.77

34.48 219.2 34.48 336.4 34.48 277.77

32.69 214.7 32.69 325.7 32.69 270.16

30.83 199.9 30.90 302.0 30.86 250.95

29.03 192.7 29.03 274.7 29.03 233.71

27.24 180.4 27.24 265.3 27.24 222.86

25.45 172.5 25.45 250.5 25.45 211.50

23.66 160.3 23.66 236.5 23.66 198.37

21.86 150.4 21.86 221.5 21.86 185.94

20.07 143.0 20.07 201.7 20.07 172.37

18.28 131.7 18.21 187.7 18.24 159.71

16.41 121.1 16.41 175.8 16.41 148.44

14.62 111.0 14.62 160.3 14.62 135.65

12.83 100.8 12.83 142.5 12.83 121.66

11.03 89.6 11.03 128.2 11.03 108.89

9.24 79.0 9.24 110.6 9.24 94.81

7.45 67.2 7.45 94.5 7.45 80.83

5.59 55.5 5.61 77.1 5.60 66.29

3.82 43.4 3.81 58.8 3.81 51.11

2.01 29.0 1.99 39.1 2.00 34.06

0.21 16.7 0.20 20.9 0.20 18.84

Average Stdev

YS 22.1 25.1 23.6 2.1

VS 5.9 9.0 7.4 2.2

R2 1.0 1.0 1.0 0.0

Hysteresis 50 422 236 263
D - 26

Set C1: CS-BX3 – BL30- L1 – Mixing Day – NIST code (folder SR 45-SR-44A)

SR-44A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.22 29.8 0.20 31.2 0.21 37.2 0.21 32.75

2.65 55.8 2.65 52.4 2.66 66.8 2.65 58.33

5.08 74.6 5.09 69.5 5.10 94.3 5.09 79.45

7.59 92.7 7.59 85.8 7.52 121.2 7.56 99.91

10.00 110.8 10.00 102.7 10.00 144.3 10.00 119.26

12.41 129.7 12.41 118.4 12.41 166.9 12.41 138.37

14.90 150.1 14.90 136.0 14.90 191.2 14.90 159.13

17.31 166.0 17.38 153.4 17.31 210.6 17.33 176.67

19.79 181.6 19.79 168.1 19.79 230.0 19.79 193.21

22.21 195.7 22.21 183.1 22.21 243.8 22.21 207.55

24.69 216.4 24.69 194.4 24.69 266.9 24.69 225.92

27.10 232.7 27.10 208.7 27.10 287.1 27.10 242.86

29.59 241.5 29.59 221.2 29.59 297.9 29.59 253.54

32.00 249.7 32.00 234.3 32.00 307.2 32.00 263.73

34.48 247.9 34.48 249.5 34.48 312.7 34.48 270.03

34.48 276.7 34.48 253.8 34.48 347.0 34.48 292.50

32.62 271.9 32.69 236.4 32.69 330.6 32.67 279.63

30.90 253.2 30.90 226.2 30.90 313.9 30.90 264.46

29.03 226.0 29.03 216.7 29.10 278.4 29.06 240.37

27.24 225.9 27.24 204.5 27.24 275.6 27.24 235.32

25.45 211.9 25.45 196.1 25.45 261.1 25.45 223.00

23.66 203.1 23.66 186.1 23.66 253.3 23.66 214.18

21.86 190.8 21.86 172.3 21.86 237.9 21.86 200.35

20.07 169.7 20.07 162.9 20.07 214.5 20.07 182.36

18.21 162.1 18.21 151.2 18.21 201.9 18.21 171.74

16.41 156.7 16.41 137.0 16.41 190.0 16.41 161.22

14.62 141.0 14.62 127.7 14.62 175.9 14.62 148.21

12.83 125.7 12.83 114.5 12.83 154.4 12.83 131.53

11.03 113.8 11.03 104.5 11.03 144.8 11.03 121.03

9.24 99.7 9.24 91.6 9.24 124.5 9.24 105.26

7.45 85.5 7.45 79.7 7.45 108.9 7.45 91.38

5.61 72.6 5.61 66.1 5.60 89.5 5.61 76.08

3.80 57.2 3.81 52.0 3.80 68.9 3.80 59.38

2.01 40.0 2.01 37.0 2.00 48.1 2.01 41.68

0.20 24.1 0.20 22.7 0.21 27.4 0.20 24.72

Average Stdev

YS 30.5 28.9 37.9 32.4 4.8

VS 7.2 6.5 8.9 7.5 1.2

R2 1.00 1.00 0.99 1.0 0.0

Hysteresis 141 193 266 200 62
D - 27

Set C1: CS-BX3 – BL3- L1 – Mixing Day – NIST code (folder SR 45-SR-44B)

SR-44A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.20 5.4 0.21 4.5 0.20 4.85 0.20 4.92

2.65 7.6 2.65 6.7 2.65 7.70 2.65 7.33

5.09 10.0 5.10 8.5 5.09 9.90 5.09 9.50

7.52 11.9 7.52 10.1 7.52 11.72 7.52 11.22

10.00 14.0 10.00 11.6 10.00 13.35 10.00 12.97

12.41 15.9 12.41 13.4 12.41 14.77 12.41 14.69

14.90 17.7 14.90 15.1 14.90 16.31 14.90 16.36

17.31 19.4 17.38 16.1 17.31 17.68 17.33 17.75

19.79 21.2 19.79 17.7 19.79 18.53 19.79 19.17

22.21 22.7 22.21 18.9 22.21 19.60 22.21 20.37

24.69 24.6 24.69 20.4 24.69 21.46 24.69 22.14

27.10 26.5 27.17 21.2 27.10 23.03 27.13 23.59

29.59 28.0 29.59 21.2 29.59 23.98 29.59 24.38

32.00 29.6 32.00 21.5 32.00 25.11 32.00 25.40

34.48 30.6 34.48 22.1 34.48 25.97 34.48 26.22

34.48 30.9 34.48 23.8 34.48 27.10 34.48 27.25

32.69 29.7 32.69 22.3 32.69 26.25 32.69 26.09

30.90 28.4 30.90 21.5 30.83 24.54 30.87 24.84

29.03 27.0 29.03 21.3 29.03 23.81 29.03 24.04

27.24 26.5 27.24 19.8 27.24 23.31 27.24 23.21

25.45 25.1 25.45 19.1 25.45 21.89 25.45 22.03

23.66 24.0 23.66 18.5 23.66 20.63 23.66 21.03

21.86 23.0 21.86 17.3 21.86 19.87 21.86 20.08

20.00 21.5 20.07 16.7 20.00 18.38 20.02 18.86

18.28 20.2 18.21 15.6 18.21 17.34 18.23 17.73

16.41 18.6 16.41 14.2 16.41 16.43 16.41 16.40

14.62 17.3 14.62 13.4 14.62 15.11 14.62 15.26

12.83 16.2 12.83 12.4 12.83 14.40 12.83 14.34

11.03 15.0 11.03 11.5 11.03 12.82 11.03 13.13

9.24 13.5 9.24 10.5 9.24 11.87 9.24 11.98

7.45 11.9 7.45 9.3 7.45 10.23 7.45 10.48

5.61 10.5 5.60 8.1 5.60 8.87 5.60 9.18

3.81 8.9 3.82 6.8 3.81 7.63 3.81 7.79

2.00 7.2 2.01 5.6 1.99 5.85 2.00 6.20

0.20 5.2 0.19 4.1 0.20 4.14 0.20 4.46

Average Stdev

YS 6.4 5.0 5.3 5.5 0.7

VS 0.7 0.6 0.6 0.6 0.1

R2 1.00 0.99 0.99 1.0 0.0

Hysteresis 9 84 55 50 38
D - 28

Set C1: CS-BX3 – BL3- L2 – Mixing Day – NIST code (folder SR 45-SR-44C)

SR-44C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 25.8 0.21 31.3 0.21 26.5 0.20 27.85

2.65 42.2 2.65 57.1 2.64 44.5 2.65 47.93

5.10 58.2 5.10 81.5 5.10 61.6 5.10 67.11

7.52 72.5 7.52 105.4 7.52 76.8 7.52 84.90

10.00 86.9 10.00 124.8 10.00 90.9 10.00 100.85

12.41 100.9 12.41 151.2 12.41 106.3 12.41 119.48

14.90 114.6 11.93 150.5 14.90 121.1 13.91 128.75

17.31 128.5 17.31 162.7 17.38 135.6 17.33 142.25

19.79 141.4 19.79 195.3 19.79 151.7 19.79 162.77

22.21 155.8 22.21 210.7 22.21 164.2 22.21 176.91

24.69 166.0 24.69 221.8 24.69 178.4 24.69 188.72

27.10 177.8 27.10 234.5 27.10 192.7 27.10 201.69

29.59 191.0 29.59 247.1 29.59 205.2 29.59 214.42

32.00 201.0 32.00 260.1 32.00 214.6 32.00 225.23

34.48 211.9 34.48 275.1 34.48 223.4 34.48 236.80

34.48 220.5 34.48 285.3 34.48 238.8 34.48 248.20

32.69 203.4 32.69 274.1 32.69 221.2 32.69 232.89

30.83 192.7 30.83 259.8 30.90 208.5 30.85 220.31

29.03 188.9 29.03 247.9 29.03 200.2 29.03 212.31

27.24 178.1 27.24 231.1 27.24 187.9 27.24 198.99

25.45 168.7 25.45 219.5 25.45 180.7 25.45 189.63

23.66 157.9 23.66 204.9 23.66 168.6 23.66 177.12

21.86 146.5 21.86 192.5 21.86 157.4 21.86 165.47

20.07 138.8 20.00 180.6 20.07 149.5 20.05 156.32

18.28 129.1 18.28 167.5 18.21 137.6 18.25 144.71

16.41 116.3 16.41 151.1 16.41 126.0 16.41 131.13

14.62 107.9 14.62 140.0 14.62 115.5 14.62 121.12

12.83 98.4 12.83 127.9 12.83 104.9 12.83 110.41

11.03 88.5 11.03 113.4 11.03 94.7 11.03 98.86

9.24 77.6 9.24 99.8 9.24 83.2 9.24 86.88

7.45 67.1 7.45 85.4 7.45 71.8 7.45 74.76

5.60 55.5 5.61 70.3 5.61 59.4 5.61 61.73

3.81 43.7 3.82 55.0 3.81 46.7 3.81 48.46

1.99 30.4 1.99 37.4 2.01 32.4 2.00 33.40

0.20 18.4 0.21 21.7 0.20 19.4 0.20 19.85

Average Stdev

YS 22.9 26.7 24.1 24.6 1.9

VS 5.7 7.6 6.1 6.5 1.0

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 136 355 111 201 134
D - 29

Set C1: CS-BX3 – BL30- L2 – Mixing Day – NIST code (folder SR 45-SR-44D)

SR-44D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 28.55 0.20 27.2 0.21 30.8 0.20 28.84

2.64 57.77 2.63 51.8 2.63 68.5 2.64 59.37

5.10 83.03 5.09 78.2 5.10 102.2 5.10 87.82

7.52 107.88 7.52 101.9 7.52 134.2 7.52 114.65

10.00 127.43 10.00 120.0 10.00 154.5 10.00 133.99

12.41 148.38 12.41 139.8 12.41 176.5 12.41 154.88

14.90 167.65 14.90 156.7 14.90 196.1 14.90 173.51

17.31 186.11 17.38 173.9 17.31 214.8 17.33 191.63

19.79 201.52 19.79 191.2 19.79 227.6 19.79 206.79

22.21 218.21 22.21 204.8 22.28 244.7 22.23 222.57

24.69 234.67 24.69 217.4 24.69 263.2 24.69 238.42

27.10 251.16 27.10 230.1 27.10 276.1 27.10 252.44

29.59 259.66 29.59 240.9 29.59 289.7 29.59 263.43

32.00 272.64 32.00 250.9 32.00 296.0 32.00 273.17

34.48 290.83 34.48 264.8 34.48 294.2 34.48 283.25

34.48 300.84 34.48 288.8 34.48 346.7 34.48 312.11

32.69 281.07 32.62 267.7 32.69 337.6 32.67 295.44

30.90 271.04 30.90 253.3 30.90 311.1 30.90 278.49

29.03 257.74 29.03 237.9 29.03 277.8 29.03 257.80

27.24 243.54 27.24 224.8 27.24 268.6 27.24 245.64

25.45 231.40 25.45 213.8 25.45 252.4 25.45 232.54

23.66 217.14 23.66 202.9 23.66 236.5 23.66 218.84

21.86 200.93 21.86 186.5 21.86 223.5 21.86 203.64

20.07 191.63 20.07 174.1 20.07 198.8 20.07 188.18

18.28 175.35 18.21 159.7 18.21 187.4 18.23 174.17

16.41 155.61 16.41 148.6 16.41 180.0 16.41 161.41

14.62 145.76 14.62 136.8 14.62 158.0 14.62 146.85

12.83 133.55 12.83 120.6 12.83 143.0 12.83 132.40

11.03 117.77 11.03 109.2 11.03 126.2 11.03 117.70

9.24 102.12 9.24 94.8 9.24 110.7 9.24 102.54

7.38 88.07 7.45 81.0 7.45 92.5 7.43 87.18

5.60 71.68 5.61 66.5 5.61 76.5 5.61 71.59

3.81 55.02 3.81 50.8 3.82 59.1 3.81 54.98

2.00 36.74 2.02 34.3 2.01 38.0 2.01 36.36

0.20 19.60 0.21 18.4 0.21 19.9 0.21 19.28

Average Stdev

YS 26.0 22.4 21.6 23.3 2.3

VS 8.0 7.6 9.3 8.3 0.9

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 407 380 632 473 138
D - 30

Set C3: CS-BX3 – BL30- L1 – 3 day – NIST code (folder SR 46-SR-44A)

SR-44A

Run# K Run# M Run# N Average

SR SS SR SS SR SS SR SS

0.28 22.2 0.20 26.5 0.20 33.6 0.23 27.40

2.65 49.0 2.64 46.5 2.65 72.7 2.65 56.07

5.08 64.8 5.10 65.1 4.06 106.0 4.75 78.64

7.59 80.9 7.52 82.1 7.59 133.5 7.56 98.82

10.00 97.3 10.00 98.6 10.00 164.8 10.00 120.25

12.41 112.1 12.41 115.5 12.41 186.7 12.41 138.10

14.90 128.0 14.90 131.2 14.90 208.3 14.90 155.86

17.38 144.2 17.31 146.7 17.38 228.5 17.36 173.14

19.79 157.6 19.79 162.3 19.79 244.8 19.79 188.25

22.21 172.8 22.21 175.2 22.21 259.5 22.21 202.48

24.69 185.5 24.69 192.0 24.69 278.6 24.69 218.71

27.10 201.3 27.10 204.5 27.10 294.7 27.10 233.53

29.59 215.2 29.59 214.0 29.59 306.5 29.59 245.23

32.00 222.6 32.00 225.3 32.00 321.5 32.00 256.46

34.48 231.4 34.48 234.0 34.48 330.1 34.48 265.17

34.48 246.7 34.48 250.3 34.48 361.1 34.48 286.02

32.69 235.0 32.69 241.4 32.62 349.5 32.67 275.30

30.90 222.1 30.90 224.4 30.90 330.1 30.90 258.85

29.03 205.3 29.03 209.1 29.03 303.7 29.03 239.36

27.24 196.8 27.24 201.6 27.24 289.7 27.24 229.35

25.45 186.9 25.45 189.5 25.45 271.6 25.45 216.00

23.66 176.3 23.66 179.0 23.66 256.4 23.66 203.91

21.86 166.2 21.86 168.9 21.86 240.3 21.86 191.82

20.07 150.1 20.07 152.8 20.07 219.2 20.07 174.05

18.21 140.9 18.21 187.0 18.21 205.6 18.21 177.84

16.41 132.3 16.41 108.2 16.41 191.3 16.41 143.91

14.62 120.5 14.62 93.1 14.62 172.1 14.62 128.56

12.83 108.0 12.83 111.2 12.83 155.6 12.83 124.91

11.03 97.1 11.03 99.0 11.03 138.6 11.03 111.55

9.24 85.0 9.24 87.3 9.24 121.1 9.24 97.80

7.45 72.7 7.38 74.6 7.45 103.0 7.43 83.40

5.61 60.6 5.60 62.4 5.61 84.9 5.61 69.28

3.81 47.6 3.81 49.5 3.81 65.5 3.81 54.20

2.01 33.1 2.01 33.8 2.01 44.0 2.01 37.00

0.21 19.6 0.20 19.9 0.20 24.7 0.20 21.41

Average Stdev

YS 23.3 22.6 28.6 24.8 3.3

VS 6.4 6.6 9.7 7.6 1.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 158 167 609 311 258
D - 31

Set C3: CS-BX3 – BL3- L1 – 3 day – NIST code (folder SR 46-SR-44B)

SR-44B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.26 9.8 0.21 14.9 0.21 13.2 0.23 12.63

2.63 19.8 2.65 26.2 2.65 22.4 2.64 22.82

5.10 23.8 5.10 32.9 5.10 27.3 5.10 28.00

7.52 28.0 7.52 36.9 7.52 32.0 7.52 32.30

10.00 32.5 10.00 41.6 10.00 35.6 10.00 36.55

12.41 36.1 12.41 46.1 12.41 39.5 12.41 40.57

14.90 39.6 14.90 51.0 14.90 43.1 14.90 44.54

17.31 42.9 17.31 55.8 17.31 46.6 17.31 48.43

19.79 46.0 19.79 59.8 19.79 50.9 19.79 52.24

22.21 49.1 22.21 64.1 22.21 54.3 22.21 55.85

24.69 52.2 24.69 68.6 24.69 58.5 24.69 59.78

27.17 55.3 27.10 73.0 27.10 62.5 27.13 63.62

29.59 59.2 29.59 76.9 29.59 66.1 29.59 67.41

32.00 62.2 32.00 80.9 32.00 70.7 32.00 71.26

34.48 64.9 34.48 84.1 34.48 74.4 34.48 74.47

34.48 66.9 34.48 88.4 34.48 74.5 34.48 76.60

32.69 64.0 32.69 84.3 32.69 71.1 32.69 73.14

30.83 61.3 30.83 79.8 30.83 68.2 30.83 69.77

29.03 57.8 29.03 75.6 29.10 65.6 29.06 66.33

27.24 55.6 27.24 72.8 27.24 62.7 27.24 63.66

25.45 53.2 25.45 68.8 25.45 59.7 25.45 60.58

23.66 51.0 23.66 65.4 23.66 56.8 23.66 57.74

21.86 48.1 21.86 62.4 21.86 54.2 21.86 54.92

20.07 44.9 20.07 58.3 20.07 51.3 20.07 51.52

18.21 42.8 18.21 55.2 18.28 48.0 18.23 48.66

16.41 40.9 16.41 52.2 16.41 57.6 16.41 50.22

14.62 37.8 14.62 48.5 14.62 33.3 14.62 39.85

12.83 34.8 12.83 44.6 12.83 30.8 12.83 36.72

11.03 32.3 11.03 41.2 11.03 36.0 11.03 36.48

9.24 29.4 9.24 37.3 9.17 32.9 9.22 33.20

7.45 26.0 7.45 33.4 7.38 29.4 7.43 29.61

5.60 23.2 5.60 29.1 5.59 25.7 5.60 26.03

3.82 20.0 3.81 24.4 3.81 21.7 3.81 22.03

2.01 16.0 2.00 19.6 1.99 17.5 2.00 17.71

0.21 10.7 0.20 13.2 0.21 11.8 0.20 11.90

Average Stdev

YS 14.0 16.8 14.9 15.2 1.4

VS 1.5 2.1 1.8 1.8 0.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 26 59 39 41 16.7
D - 32

Set C3: CS-BX3 – BL3- L2 – 3 day – NIST code (folder SR 46-SR-44C)

SR-44C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 34.5 0.20 27.5 0.21 27.2 0.20 29.74

2.63 77.8 2.65 52.6 2.64 50.7 2.64 60.38

5.10 130.8 5.10 75.3 5.10 71.2 5.10 92.43

7.52 171.1 7.52 97.8 7.52 88.5 7.52 119.12

10.00 195.4 10.00 116.9 10.00 106.9 10.00 139.73

12.41 218.8 12.41 133.6 12.41 124.7 12.41 159.03

14.90 230.6 14.90 152.6 14.90 140.8 14.90 174.67

17.31 237.9 17.31 168.6 17.31 158.8 17.31 188.42

19.79 258.8 19.79 184.0 19.79 174.2 19.79 205.66

22.21 280.5 22.21 199.5 22.21 189.7 22.21 223.25

24.69 289.9 24.69 214.8 24.69 203.1 24.69 235.92

27.10 304.7 27.10 231.6 27.17 219.1 27.13 251.81

29.59 326.9 29.59 243.5 29.59 233.6 29.59 268.01

32.00 339.7 32.00 255.9 32.00 245.3 32.00 280.30

34.48 370.4 34.48 268.9 34.48 258.3 34.48 299.23

34.48 385.2 34.48 285.8 34.48 271.1 34.48 314.05

32.69 366.4 32.69 268.8 32.69 257.0 32.69 297.38

30.90 348.4 30.90 253.2 30.83 241.4 30.87 280.97

29.03 315.7 29.10 236.5 29.03 228.0 29.06 260.06

27.24 307.0 27.24 224.8 27.24 218.5 27.24 250.11

25.45 289.0 25.45 214.7 25.45 205.3 25.45 236.36

23.66 274.4 23.66 201.6 23.66 193.6 23.66 223.21

21.86 254.2 21.86 188.6 21.86 182.3 21.86 208.36

20.07 229.9 20.07 176.5 20.07 167.5 20.07 191.29

18.21 215.0 18.21 162.2 18.28 155.0 18.23 177.41

16.41 202.3 16.41 148.3 16.41 143.4 16.41 164.68

14.62 181.8 14.62 169.2 14.62 129.5 14.62 160.15

12.83 161.8 12.83 97.1 12.83 118.3 12.83 125.73

11.03 146.1 11.03 90.3 11.03 105.6 11.03 113.99

9.24 126.2 9.24 96.0 9.24 92.3 9.24 104.81

7.38 106.6 7.45 81.7 7.38 78.7 7.40 88.98

5.60 87.9 5.59 67.3 5.61 65.2 5.60 73.47

3.81 67.6 3.81 52.6 3.82 51.1 3.82 57.10

2.02 44.8 1.99 35.6 2.01 34.7 2.01 38.39

0.20 23.7 0.20 20.5 0.20 20.0 0.20 21.38

Average Stdev

YS 28.3 22.6 24.0 25.0 3.0

VS 10.3 7.6 7.1 8.3 1.7

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 910 309 189 469 387
D - 33

Set C3: CS-BX3 – BL30- L2 – 3 day – NIST code (folder SR 46-SR-44D)

SR-44D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 19.0 0.20 22.7 0.19 23.3 0.20 21.67

2.64 39.4 2.65 48.6 2.64 53.7 2.64 47.24

5.10 59.9 5.08 73.8 5.08 82.2 5.09 71.96

7.52 77.4 7.52 96.0 7.52 106.8 7.52 93.41

10.00 93.4 10.00 116.3 10.00 124.8 10.00 111.50

12.41 107.4 12.41 135.3 12.41 144.2 12.41 128.98

14.90 122.2 14.90 153.1 14.90 161.2 14.90 145.49

17.31 135.6 17.38 171.6 17.38 177.5 17.36 161.56

19.79 148.8 19.79 188.8 19.79 195.6 19.79 177.72

22.21 160.6 22.21 204.9 22.21 213.1 22.21 192.85

24.69 175.9 24.69 218.6 24.69 222.7 24.69 205.72

27.17 189.0 27.10 232.5 27.10 237.0 27.13 219.50

29.59 198.1 29.59 159.1 29.59 250.8 29.59 202.68

32.00 214.0 32.07 207.6 32.00 265.6 32.02 229.05

34.48 220.7 34.48 510.3 34.48 287.1 34.48 339.36

34.48 237.0 34.48 289.3 34.48 299.6 34.48 275.32

32.69 226.9 32.69 271.1 32.69 272.8 32.69 256.92

30.83 205.8 30.83 255.6 30.90 261.6 30.85 241.00

29.03 201.5 29.03 251.2 29.03 253.1 29.03 235.28

27.24 188.8 27.24 234.1 27.24 235.2 27.24 219.36

25.45 173.1 25.45 217.0 25.45 224.6 25.45 204.90

23.66 160.2 23.66 200.5 23.66 206.7 23.66 189.14

21.86 154.1 21.86 188.9 21.86 193.3 21.86 178.75

20.07 143.6 20.07 177.1 20.07 183.3 20.07 168.03

18.28 133.8 18.21 162.9 18.21 167.8 18.23 154.86

16.41 124.7 16.41 147.8 16.41 151.3 16.41 141.27

14.62 111.4 14.62 134.8 14.62 138.4 14.62 128.19

12.83 102.4 12.83 121.8 12.83 125.2 12.83 116.45

11.03 89.2 11.03 106.8 11.03 111.7 11.03 102.58

9.24 79.1 9.24 93.5 9.24 96.8 9.24 89.78

7.45 66.7 7.45 79.2 7.45 82.7 7.45 76.20

5.61 54.9 5.61 64.4 5.61 66.6 5.61 61.95

3.81 42.7 3.81 49.4 3.81 50.4 3.81 47.50

2.01 27.8 2.01 32.3 2.01 33.2 2.01 31.10

0.21 14.9 0.20 16.8 0.20 17.0 0.20 16.22

Average Stdev

YS 18.4 19.5 21.1 19.7 1.4

VS 6.3 7.8 7.9 7.3 0.9

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 158 251 419 276 132
D - 34

Set C7: CS-BX3 – BL30- L1 – 7 day – NIST code (folder SR 47-SR-44A)

SR-44A

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 40.8 0.19 27.0 0.21 26.8 0.20 31.52

2.64 93.8 2.64 47.4 2.65 47.3 2.64 62.83

5.08 143.6 5.10 66.1 5.10 68.9 5.09 92.88

7.52 185.2 7.52 83.2 7.52 85.7 7.52 118.05

10.00 208.0 10.00 100.6 10.00 102.1 10.00 136.91

12.41 232.1 12.41 117.6 12.48 120.4 12.44 156.71

14.90 252.8 14.90 133.8 14.90 139.9 14.90 175.49

17.31 276.4 17.31 150.5 17.31 154.1 17.31 193.67

19.79 292.4 19.79 165.6 19.79 167.4 19.79 208.47

22.28 315.7 22.28 179.0 22.21 179.1 22.25 224.59

24.69 318.4 24.69 192.3 24.69 200.9 24.69 237.18

27.10 336.2 27.10 207.6 27.17 214.9 27.13 252.88

29.59 355.3 29.59 219.7 29.59 222.0 29.59 265.68

32.00 361.9 32.00 225.9 32.00 234.9 32.00 274.23

34.48 412.2 34.48 236.7 34.48 227.8 34.48 292.24

34.41 420.2 34.48 253.7 34.48 259.1 34.46 311.02

32.62 368.0 32.62 237.4 32.69 260.6 32.64 288.68

30.90 373.9 30.90 226.9 30.83 236.6 30.87 279.11

29.10 336.8 29.03 207.7 29.03 218.9 29.06 254.49

27.24 331.1 27.24 200.6 27.24 212.6 27.24 248.10

25.45 306.0 25.45 191.5 25.45 195.1 25.45 230.85

23.66 302.0 23.66 181.1 23.66 180.4 23.66 221.19

21.86 275.9 21.86 167.7 21.86 173.7 21.86 205.78

20.07 241.8 20.07 154.8 20.07 154.4 20.07 183.65

18.21 227.0 18.21 144.5 18.21 147.7 18.21 173.10

16.41 217.5 16.41 133.1 16.41 143.6 16.41 164.77

14.62 197.1 14.62 122.2 14.62 126.5 14.62 148.61

12.83 166.4 12.83 107.6 12.83 117.0 12.83 130.34

11.03 154.9 11.03 98.9 11.03 101.6 11.03 118.45

9.24 133.7 9.24 85.6 9.24 90.9 9.24 103.44

7.45 113.3 7.45 73.7 7.45 76.1 7.45 87.70

5.60 93.1 5.61 60.9 5.60 64.1 5.60 72.70

3.79 70.7 3.81 46.8 3.82 51.2 3.81 56.23

2.01 47.6 2.01 32.8 2.01 34.1 2.01 38.16

0.20 25.4 0.21 19.4 0.20 20.2 0.20 21.68

Average Stdev

YS 29.8 22.6 23.6 25.3 3.9

VS 11.0 6.6 6.9 8.2 2.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1302 241 139 561 644
D - 35

Set C7: CS-BX3 – BL3- L1 – 7 day – NIST code (folder SR 47-SR-44B)

SR-44B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 12.4 0.21 12.8 0.20 12.8 0.23 12.67

2.65 26.7 2.63 20.9 2.64 20.4 2.64 22.64

5.10 31.1 5.10 27.1 5.10 25.0 5.10 27.75

7.52 35.4 7.52 32.6 7.52 28.9 7.52 32.32

10.00 39.4 10.00 37.7 10.00 31.9 10.00 36.33

12.41 43.6 12.41 43.2 12.41 35.0 12.41 40.61

14.90 47.7 14.90 48.3 14.90 38.3 14.90 44.77

17.31 52.2 17.38 53.2 17.31 41.6 17.33 48.98

19.79 42.1 19.79 58.1 19.79 44.7 19.79 48.32

22.21 47.9 22.28 62.9 22.21 48.9 22.23 53.22

24.69 84.2 24.69 67.4 24.69 53.2 24.69 68.28

27.17 68.5 27.17 71.9 27.17 57.4 27.17 65.93

29.59 72.9 29.59 76.7 29.59 61.1 29.59 70.23

32.00 75.7 32.00 81.5 32.00 65.0 32.00 74.04

34.48 79.9 34.48 87.2 34.48 66.9 34.48 78.01

34.48 82.3 34.48 86.4 34.48 67.1 34.48 78.59

32.69 78.3 32.69 126.6 32.69 66.0 32.69 90.31

30.83 74.8 30.83 62.9 30.83 63.0 30.83 66.90

29.03 71.2 29.03 39.2 29.03 59.3 29.03 56.58

27.24 68.6 27.24 71.7 27.24 57.3 27.24 65.88

25.45 65.0 25.45 68.8 25.45 55.0 25.45 62.95

23.66 61.5 23.66 65.6 23.66 52.9 23.66 60.02

21.86 58.8 21.86 61.7 21.86 50.4 21.86 56.97

20.07 55.1 20.07 58.4 20.07 47.4 20.07 53.65

18.28 51.8 18.28 54.9 18.28 45.4 18.28 50.68

16.41 48.8 16.41 51.7 16.41 43.8 16.41 48.07

14.62 45.5 14.62 48.0 14.62 40.6 14.62 44.70

12.83 42.2 12.83 44.2 12.83 38.0 12.83 41.49

11.03 38.2 11.03 41.1 11.03 35.0 11.03 38.10

9.24 34.9 9.24 37.2 9.24 32.1 9.24 34.77

7.45 31.1 7.38 33.3 7.38 28.5 7.40 30.95

5.61 26.9 5.61 29.1 5.61 25.3 5.61 27.11

3.81 22.8 3.81 24.5 3.82 21.6 3.82 22.99

2.02 18.0 2.01 19.6 2.00 16.8 2.01 18.15

0.20 12.1 0.21 13.2 0.20 11.5 0.20 12.26

Average Stdev

YS 15.6 16.3 16.2 16.0 0.4

VS 2.0 2.1 1.5 1.8 0.3

R2 1.0 0.7 1.0 0.9 0.2

Hysteresis 50 6 27 28 22
D - 36

Set C7: CS-BX3 – BL3- L2 – 7 day – NIST code (folder SR 47-SR-44C)

SR-44C

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 28.2 0.20 21.9 0.20 39.3 0.20 29.78

2.63 61.1 2.65 39.7 2.66 86.9 2.65 62.56

5.10 95.0 5.10 57.1 5.09 145.1 5.09 99.08

7.52 126.7 7.52 72.8 7.59 184.7 7.54 128.06

10.00 145.8 10.00 87.7 10.00 218.0 10.00 150.51

12.41 166.6 12.41 102.2 12.41 251.2 12.41 173.35

14.90 177.4 14.90 116.7 14.90 279.8 14.90 191.28

17.38 189.9 17.31 131.4 17.38 304.3 17.36 208.56

19.79 209.2 19.79 144.2 19.79 327.8 19.79 227.07

22.21 229.2 22.21 161.2 22.21 353.2 22.21 247.88

24.69 243.7 24.69 171.2 24.69 383.3 24.69 266.07

27.17 258.0 27.10 182.9 27.10 407.3 27.13 282.75

29.59 275.5 29.59 195.7 29.59 421.3 29.59 297.49

32.00 288.3 32.00 207.9 32.00 439.2 32.00 311.81

34.48 302.4 34.48 230.7 34.48 439.7 34.48 324.24

34.48 326.7 34.48 224.1 34.48 499.1 34.48 349.97

32.69 307.2 32.69 202.2 32.62 490.3 32.67 333.25

30.90 287.9 30.90 196.7 30.90 459.5 30.90 314.68

29.03 265.1 29.10 197.4 29.03 416.0 29.06 292.79

27.24 256.9 27.24 183.0 27.24 399.1 27.24 279.68

25.45 244.2 25.45 172.2 25.45 372.3 25.45 262.92

23.66 228.2 23.66 161.4 23.66 349.4 23.66 246.33

21.86 214.5 21.86 151.4 21.86 327.9 21.86 231.29

20.07 194.6 20.00 146.6 20.07 295.8 20.05 212.33

18.21 181.9 18.28 133.1 18.21 276.1 18.23 197.01

16.41 171.3 16.41 115.0 16.41 262.0 16.41 182.76

14.62 154.5 14.62 109.9 14.62 234.2 14.62 166.20

12.83 138.0 12.83 101.7 12.83 207.2 12.83 148.94

11.03 122.8 11.03 89.6 11.03 185.5 11.03 132.65

9.24 107.9 9.24 78.9 9.24 160.9 9.24 115.88

7.45 91.3 7.45 67.8 7.45 133.7 7.45 97.56

5.61 75.2 5.61 55.3 5.61 109.3 5.61 79.92

3.82 58.1 3.81 43.2 3.80 82.3 3.81 61.22

2.01 38.5 1.99 29.3 2.02 51.4 2.01 39.72

0.20 20.7 0.20 17.2 0.19 23.5 0.20 20.47

Average Stdev

YS 25.4 22.6 28.8 25.6 3.1

VS 8.6 5.8 13.7 9.4 4.0

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 471 154 741 456 294
D - 37

Set C7: CS-BX3 – BL30- L2 – 7 day – NIST code (folder SR 47-SR-44D)

SR-44D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 18.0 0.21 23.6 0.20 25.6 0.21 22.40

2.65 39.0 2.66 60.4 2.65 62.2 2.65 53.91

5.08 58.8 5.10 98.8 5.10 97.7 5.09 85.08

7.59 76.1 7.52 135.6 7.52 128.8 7.54 113.49

10.00 93.4 10.00 164.0 10.00 149.2 10.00 135.55

12.41 110.4 12.41 190.6 12.41 169.9 12.41 156.97

14.90 126.8 14.90 213.3 14.90 185.4 14.90 175.15

17.38 142.5 17.31 233.6 17.31 200.7 17.33 192.26

19.79 158.3 19.79 245.8 19.79 216.8 19.79 206.96

22.21 173.4 22.21 253.5 22.21 241.3 22.21 222.74

24.69 183.2 24.69 259.6 24.69 243.6 24.69 228.84

27.10 197.8 27.10 273.2 27.10 256.0 27.10 242.32

29.59 213.4 29.59 286.2 29.59 273.8 29.59 257.80

32.00 226.3 32.00 300.0 32.00 287.0 32.00 271.10

34.48 244.8 34.48 316.8 34.48 332.9 34.48 298.20

34.48 240.0 34.48 354.3 34.48 329.0 34.48 307.77

32.69 226.7 32.69 327.8 32.69 282.7 32.69 279.05

30.90 219.1 30.83 306.3 30.90 277.8 30.87 267.74

29.03 212.0 29.03 293.5 29.10 280.3 29.06 261.95

27.24 198.6 27.24 273.1 27.24 254.5 27.24 242.07

25.45 188.0 25.45 258.0 25.45 245.1 25.45 230.39

23.66 176.0 23.66 235.6 23.66 228.8 23.66 213.48

21.86 165.5 21.86 222.2 21.86 209.1 21.86 198.92

20.07 156.3 20.00 210.2 20.07 205.9 20.05 190.81

18.21 143.2 18.28 190.1 18.28 184.0 18.25 172.44

16.41 129.0 16.41 174.2 16.41 154.8 16.41 152.69

14.62 119.4 14.62 159.4 14.62 149.0 14.62 142.58

12.83 108.2 12.83 142.8 12.83 136.3 12.83 129.10

11.03 95.5 11.03 126.7 11.03 119.5 11.03 113.91

9.24 83.3 9.24 110.2 9.24 103.9 9.24 99.13

7.45 70.9 7.45 92.7 7.45 89.2 7.45 84.30

5.61 57.5 5.61 74.8 5.60 70.4 5.61 67.58

3.81 44.0 3.81 56.4 3.81 52.9 3.81 51.10

2.01 29.1 1.99 35.8 1.99 34.1 2.00 32.99

0.21 14.9 0.20 17.3 0.20 17.0 0.20 16.40

Average Stdev

YS 21.2 19.7 21.8 20.9 1.1

VS 6.5 9.4 8.6 8.2 1.5

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 40 2085 594 906 1058
D - 38

Set D1: CS-BX5 – BL11- L2 – Mixing Day – NIST code (folder SR 49-SR-48A)

SR-48A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.21 40.9 0.20 28.2 0.21 34.2 0.21 34.43

2.65 93.6 2.66 46.4 2.64 61.5 2.65 67.18

5.10 147.1 5.08 65.7 5.10 90.0 5.09 100.94

7.52 202.1 7.52 83.3 7.52 116.1 7.52 133.84

10.00 223.3 10.00 99.6 10.00 136.1 10.00 152.99

12.48 249.4 12.41 116.3 12.41 155.7 12.44 173.80

14.90 269.9 14.90 132.6 14.90 173.7 14.90 192.08

17.31 285.4 17.38 148.7 17.31 193.2 17.33 209.11

19.79 302.7 19.79 163.4 19.79 209.3 19.79 225.15

22.21 335.7 22.21 178.4 22.28 227.7 22.23 247.29

24.69 341.4 24.69 192.5 24.69 242.0 24.69 258.63

27.10 365.1 27.10 206.7 27.10 258.0 27.10 276.60

29.59 387.2 29.59 221.6 29.59 271.3 29.59 293.34

32.00 389.7 32.07 232.7 32.00 281.8 32.02 301.41

34.48 449.6 34.48 243.9 34.48 294.6 34.48 329.40

34.48 445.2 34.48 254.7 34.48 316.4 34.48 338.75

32.69 377.6 32.69 243.0 32.69 292.5 32.69 304.40

30.90 383.3 30.90 227.4 30.90 279.9 30.90 296.88

29.10 386.2 29.03 216.9 29.03 264.2 29.06 289.10

27.24 351.8 27.24 205.7 27.24 253.6 27.24 270.39

25.45 344.4 25.45 195.2 25.45 240.0 25.45 259.86

23.66 324.1 23.66 183.2 23.66 229.3 23.66 245.53

21.86 294.6 21.86 172.6 21.86 212.3 21.86 226.48

20.07 294.0 20.07 161.7 20.07 197.8 20.07 217.83

18.21 263.2 18.21 149.9 18.28 182.9 18.23 198.66

16.41 220.2 16.41 138.5 16.41 168.9 16.41 175.87

14.62 212.9 14.62 126.6 14.62 155.2 14.62 164.91

12.83 196.5 12.83 115.4 12.83 138.6 12.83 150.15

11.03 176.6 11.03 103.5 11.03 125.8 11.03 135.27

9.24 153.5 9.24 91.1 9.24 109.3 9.24 117.96

7.38 133.9 7.45 78.1 7.45 94.1 7.43 102.04

5.61 106.4 5.62 65.2 5.60 77.3 5.61 82.98

3.81 81.5 3.80 51.4 3.82 60.2 3.81 64.34

1.99 53.7 2.01 35.6 2.02 40.8 2.01 43.37

0.20 29.0 0.20 21.5 0.19 23.5 0.20 24.64

Average Stdev

YS 42.8 27.1 30.5 33.5 8.3

VS 11.5 6.6 8.2 8.8 2.5

R2 0.99 1.00 1.00 1.0 0.0

Hysteresis 1115 88 382 528 529
D - 39

Set D1: CS-BX5 – BL36- L1 – Mixing Day – NIST code (folder SR 49-SR-48B)

SR-48B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 23.9 0.20 26.2 0.19 22.8 0.20 24.29

2.63 47.6 2.64 52.5 2.63 43.9 2.64 48.00

5.10 70.0 5.10 78.5 5.10 61.9 5.10 70.13

7.52 98.1 7.52 103.3 7.52 78.3 7.52 93.22

10.00 116.9 10.00 116.3 10.00 93.7 10.00 108.95

12.41 137.7 12.41 134.7 12.48 107.2 12.44 126.54

14.90 155.4 14.90 151.7 14.90 122.4 14.90 143.19

17.31 170.4 17.31 167.4 17.31 136.8 17.31 158.18

19.79 183.6 19.79 182.5 19.79 148.2 19.79 171.44

22.21 195.3 22.28 195.9 22.28 162.9 22.25 184.71

24.69 209.1 24.69 212.0 24.69 175.0 24.69 198.69

27.17 219.2 27.10 226.7 27.10 187.6 27.13 211.20

29.59 226.8 29.59 236.1 29.59 199.0 29.59 220.64

32.00 236.4 32.00 243.1 32.00 205.3 32.00 228.30

34.48 240.8 34.48 240.3 34.48 209.7 34.48 230.28

34.48 276.1 34.48 281.4 34.48 228.5 34.48 262.00

32.69 266.3 32.69 275.9 32.69 223.7 32.69 255.30

30.83 244.0 30.90 250.6 30.90 209.2 30.87 234.61

29.03 228.7 29.03 227.2 29.03 189.0 29.03 214.95

27.24 214.1 27.24 218.5 27.24 184.0 27.24 205.54

25.45 200.3 25.45 205.3 25.45 173.9 25.45 193.18

23.66 180.8 23.66 191.5 23.66 164.7 23.66 179.00

21.86 174.9 21.86 183.5 21.86 154.5 21.86 170.98

20.07 163.6 20.07 165.4 20.07 138.0 20.07 155.66

18.28 151.0 18.28 154.1 18.21 129.9 18.25 145.02

16.41 139.2 16.41 146.6 16.41 124.8 16.41 136.91

14.62 126.6 14.62 132.8 14.62 112.0 14.62 123.79

12.83 118.3 12.83 119.9 12.83 100.4 12.83 112.90

11.03 102.0 11.03 104.7 11.03 89.0 11.03 98.55

9.24 90.0 9.24 93.1 9.24 78.1 9.24 87.07

7.38 76.6 7.45 78.2 7.38 66.4 7.40 73.73

5.61 63.3 5.60 65.1 5.61 55.5 5.60 61.31

3.81 49.4 3.82 50.9 3.82 43.4 3.82 47.88

2.01 32.2 2.01 33.1 2.01 28.8 2.01 31.35

0.20 17.6 0.19 18.1 0.20 16.3 0.20 17.34

Average Stdev

YS 19.8 21.0 20.0 20.3 0.6

VS 7.3 7.4 6.1 6.9 0.7

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 391 338 194 308 102
D - 40

Set D1: CS-BX5 – BL11- L1 – Mixing Day – NIST code (folder SR 49-SR-48C)

SR-48C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 35.8 0.20 32.1 0.20 32.5 0.20 33.47

2.65 78.2 2.65 62.4 2.65 65.6 2.65 68.72

5.10 129.1 5.10 97.3 5.10 94.0 5.10 106.82

7.52 168.7 7.52 127.0 7.52 124.9 7.52 140.20

10.00 193.7 10.00 147.8 10.00 146.6 10.00 162.69

12.41 221.0 12.41 167.9 12.41 169.2 12.41 186.01

14.90 245.1 14.90 186.3 14.90 190.0 14.90 207.17

17.31 260.3 17.31 205.7 17.31 209.6 17.31 225.20

19.79 277.5 19.79 225.6 19.79 225.9 19.79 243.03

22.21 284.1 22.21 244.9 22.28 242.9 22.23 257.28

24.69 317.1 24.69 251.4 24.69 263.5 24.69 277.34

27.10 342.5 27.10 264.4 27.17 277.8 27.13 294.90

29.59 350.0 29.59 279.5 29.59 292.1 29.59 307.17

32.00 353.6 32.00 296.6 32.00 301.9 32.00 317.40

34.48 334.5 34.48 329.7 34.48 299.1 34.48 321.13

34.41 421.2 34.48 327.9 34.48 343.5 34.46 364.20

32.69 397.7 32.69 302.8 32.69 335.7 32.69 345.39

30.90 374.5 30.83 288.8 30.90 307.9 30.87 323.72

29.10 326.3 29.03 293.3 29.03 277.1 29.06 298.89

27.24 320.3 27.24 267.4 27.24 276.0 27.24 287.90

25.45 308.8 25.45 252.0 25.45 258.4 25.45 273.08

23.66 298.6 23.66 233.5 23.66 243.9 23.66 258.66

21.86 274.3 21.86 219.5 21.86 229.4 21.86 241.05

20.07 252.2 20.00 210.4 20.07 207.1 20.05 223.22

18.21 233.6 18.28 191.9 18.28 195.1 18.25 206.85

16.41 211.2 16.41 173.1 16.41 185.5 16.41 189.94

14.62 197.6 14.62 160.8 14.62 165.6 14.62 174.66

12.83 172.1 12.83 147.6 12.83 148.1 12.83 155.91

11.03 159.4 11.03 127.9 11.03 133.4 11.03 140.26

9.24 136.1 9.17 112.9 9.24 116.2 9.22 121.73

7.45 116.7 7.38 96.4 7.45 97.9 7.43 103.66

5.61 93.8 5.61 79.1 5.61 81.2 5.61 84.72

3.81 70.7 3.81 61.1 3.81 63.1 3.81 64.98

2.00 47.5 1.99 39.7 2.01 41.4 2.00 42.85

0.21 24.4 0.20 21.5 0.21 22.3 0.21 22.72

Average Stdev

YS 30.0 29.5 28.3 29.3 0.9

VS 11.1 8.7 9.1 9.6 1.3

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 771 511 388 557 196
D - 41

Set D1: CS-BX5 – BL36- L2 – Mixing Day – NIST code (folder SR 49-SR-48D)

SR-48D

Run# J Run# K Run# M Average

SR SS SR SS SR SS SR SS

0.20 30.1 0.19 26.0 0.21 26.1 0.20 27.38

2.64 56.9 2.65 46.4 2.63 53.4 2.64 52.25

5.10 80.1 5.10 67.1 5.10 76.7 5.10 74.63

7.52 104.5 7.59 86.9 7.52 98.1 7.54 96.52

10.00 122.1 10.00 102.7 10.00 116.1 10.00 113.65

12.41 141.9 12.41 119.1 12.41 132.9 12.41 131.30

14.90 161.6 14.90 134.5 14.90 149.1 14.90 148.40

17.38 176.4 17.38 149.3 17.31 164.5 17.36 163.39

19.79 193.9 19.79 161.9 19.79 180.3 19.79 178.71

22.21 203.7 22.21 171.9 22.21 190.6 22.21 188.75

24.69 222.7 24.69 189.0 24.69 209.8 24.69 207.20

27.17 236.8 27.10 200.3 27.17 222.6 27.15 219.89

29.59 247.2 29.59 208.6 29.59 231.3 29.59 229.02

32.00 261.7 32.00 215.0 32.00 245.1 32.00 240.61

34.48 260.9 34.48 216.3 34.48 251.7 34.48 242.98

34.48 293.8 34.48 242.8 34.48 278.7 34.48 271.76

32.69 284.0 32.62 238.9 32.69 254.7 32.67 259.22

30.83 259.2 30.90 224.1 30.83 239.3 30.85 240.86

29.03 245.1 29.03 199.2 29.03 241.0 29.03 228.44

27.24 235.2 27.24 192.0 27.24 218.9 27.24 215.35

25.45 222.3 25.45 181.9 25.45 208.0 25.45 204.09

23.66 203.7 23.66 174.8 23.66 191.8 23.66 190.13

21.86 193.4 21.86 163.3 21.86 179.1 21.86 178.58

20.07 179.8 20.07 146.9 20.07 172.9 20.07 166.50

18.21 168.2 18.21 137.5 18.28 157.7 18.23 154.48

16.41 155.8 16.41 133.2 16.41 141.9 16.41 143.63

14.62 142.8 14.62 119.3 14.62 130.6 14.62 130.91

12.83 130.8 12.83 104.5 12.83 118.7 12.83 118.02

11.03 114.6 11.03 95.3 11.03 106.1 11.03 105.37

9.24 100.5 9.24 82.9 9.24 92.2 9.24 91.89

7.38 87.0 7.45 70.9 7.38 79.5 7.40 79.13

5.61 71.5 5.61 59.1 5.60 64.8 5.61 65.15

3.81 55.6 3.81 45.7 3.82 50.2 3.81 50.51

2.01 37.1 2.01 31.5 2.01 33.9 2.01 34.14

0.21 20.7 0.20 18.1 0.20 18.9 0.20 19.27

Average Stdev

YS 26.5 21.4 22.9 23.6 2.6

VS 7.7 6.4 7.3 7.1 0.6

R2 1.00 1.00 1.00 1.0 0.0

Hysteresis 274 266 306 282 21
D - 42

Set D3: CS-BX5 – BL11- L2 – 3 day – NIST code (folder SR 50-SR-48A)

SR-48A

Run# G Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 23.6 0.21 27.9 0.20 32.3 0.20 27.93

2.63 40.6 2.65 55.6 2.64 67.0 2.64 54.39

5.10 57.1 5.10 81.7 5.09 97.6 5.10 78.78

7.52 72.3 7.52 107.5 7.52 129.1 7.52 102.98

10.00 86.2 10.00 126.1 10.00 142.9 10.00 118.38

12.41 101.0 12.41 145.1 12.48 162.8 12.44 136.29

14.90 115.0 14.90 161.6 14.90 181.5 14.90 152.69

17.38 129.4 17.31 177.3 17.31 199.2 17.33 168.60

19.79 143.0 19.79 195.1 19.79 215.3 19.79 184.48

22.21 153.1 22.21 208.0 22.28 232.4 22.23 197.86

24.69 165.8 24.69 222.0 24.69 248.2 24.69 212.02

27.17 179.2 27.10 235.9 27.10 265.8 27.13 226.97

29.59 188.4 29.59 245.7 29.59 278.6 29.59 237.58

32.00 201.2 32.00 259.6 32.00 286.0 32.00 248.92

34.48 206.8 34.48 260.9 34.48 300.9 34.48 256.19

34.48 215.6 34.48 298.7 34.48 322.7 34.48 279.03

32.69 211.1 32.69 287.6 32.62 292.3 32.67 263.67

30.83 199.0 30.83 264.1 30.90 286.1 30.85 249.75

29.03 185.4 29.03 240.1 29.03 271.3 29.03 232.27

27.24 178.3 27.24 233.2 27.24 256.3 27.24 222.60

25.45 167.5 25.45 217.3 25.45 244.9 25.45 209.90

23.66 156.0 23.66 203.7 23.66 235.1 23.66 198.27

21.86 148.5 21.86 193.1 21.86 214.8 21.86 185.47

20.07 137.1 20.07 172.7 20.07 201.5 20.07 170.39

18.21 127.7 18.21 160.8 18.21 186.4 18.21 158.31

16.41 118.3 16.41 155.6 16.41 165.9 16.41 146.58

14.62 107.4 14.62 138.5 14.62 155.8 14.62 133.89

12.83 98.5 12.83 122.9 12.83 137.5 12.83 119.62

11.03 87.2 11.03 110.4 11.03 125.1 11.03 107.54

9.24 76.7 9.24 96.2 9.24 107.9 9.24 93.62

7.38 65.7 7.45 81.1 7.45 93.2 7.43 79.98

5.61 54.6 5.60 67.6 5.62 75.6 5.61 65.92

3.82 43.0 3.81 52.3 3.80 57.5 3.81 50.94

2.01 29.6 1.99 34.9 2.02 39.3 2.01 34.61

0.20 17.6 0.19 19.6 0.21 21.8 0.20 19.66

Average Stdev

YS 21.7 20.9 29.3 24.0 4.6

VS 5.7 7.9 8.5 7.4 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 114 397 485 332 194
D - 43

Set D3: CS-BX5 – BL36- L1 – 3 day – NIST code (folder SR 50-SR-48B)

SR-48B

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.26 14.4 0.20 16.3 0.20 22.3 0.22 17.67

2.65 33.8 2.65 31.1 2.65 46.8 2.65 37.21

5.09 46.6 5.08 45.6 5.08 70.2 5.09 54.12

7.52 59.4 7.52 58.1 7.59 91.3 7.54 69.60

10.00 71.9 10.00 69.9 10.00 107.1 10.00 82.94

12.41 85.1 12.41 82.3 12.41 123.6 12.41 97.00

14.90 97.6 14.90 94.8 14.90 138.1 14.90 110.16

17.38 110.1 17.31 106.7 17.31 154.0 17.33 123.61

19.79 121.5 19.79 117.7 19.79 166.9 19.79 135.37

22.21 132.9 22.21 126.7 22.21 182.5 22.21 147.39

24.69 144.8 24.69 138.7 24.69 193.9 24.69 159.12

27.10 155.2 27.10 150.8 27.10 207.0 27.10 170.97

29.59 164.1 29.59 161.3 29.59 219.6 29.59 181.63

32.00 174.8 32.00 169.7 32.00 229.5 32.00 191.33

34.48 184.7 34.48 171.0 34.48 243.5 34.48 199.72

34.48 191.8 34.48 189.1 34.48 256.4 34.48 212.39

32.62 184.1 32.69 179.6 32.62 245.7 32.64 203.14

30.90 171.7 30.90 166.6 30.90 232.5 30.90 190.26

29.03 160.4 29.03 156.0 29.03 211.1 29.03 175.84

27.24 152.7 27.24 148.3 27.24 202.7 27.24 167.91

25.45 144.4 25.45 140.0 25.45 191.5 25.45 158.62

23.66 140.3 23.66 131.6 23.66 181.1 23.66 151.02

21.86 129.3 21.86 125.3 21.86 169.7 21.86 141.43

20.07 117.0 20.07 113.0 20.07 157.2 20.07 129.07

18.21 109.8 18.21 105.3 18.21 142.5 18.21 119.19

16.41 102.9 16.41 100.5 16.41 132.5 16.41 111.98

14.62 93.6 14.62 90.2 14.62 121.5 14.62 101.78

12.83 83.3 12.83 81.5 12.83 106.5 12.83 90.43

11.03 75.6 11.03 72.5 11.03 97.1 11.03 81.72

9.24 65.4 9.24 63.8 9.24 83.6 9.24 70.92

7.45 55.9 7.45 53.8 7.45 71.7 7.45 60.43

5.61 46.2 5.61 45.0 5.61 58.1 5.61 49.79

3.81 35.7 3.81 35.2 3.81 43.9 3.81 38.27

2.02 24.3 2.01 23.7 2.01 29.4 2.02 25.77

0.20 13.2 0.20 13.0 0.20 15.2 0.20 13.83

Average Stdev

YS 16.9 16.1 18.1 17.0 1.0

VS 5.1 4.9 6.9 5.6 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 67 58 337 154 159
D - 44

Set D3: CS-BX5 – BL11- L1 – 3 day – NIST code (folder SR 50-SR-48C)

SR-48C

Run# K Run# L Run# N Average

SR SS SR SS SR SS SR SS

0.21 22.2 0.19 22.5 0.20 24.0 0.20 22.89

2.64 40.1 2.65 42.6 2.64 44.0 2.64 42.25

5.09 58.8 5.09 60.6 5.09 62.6 5.09 60.67

7.52 75.0 7.59 77.2 7.52 79.9 7.54 77.36

10.00 90.9 10.00 93.6 10.00 97.0 10.00 93.84

12.41 107.0 12.41 109.6 12.41 114.0 12.41 110.20

14.90 121.8 14.90 126.4 14.90 130.2 14.90 126.13

17.38 135.6 17.38 142.5 17.31 146.0 17.36 141.38

19.79 150.6 19.79 156.1 19.79 157.7 19.79 154.81

22.21 161.8 22.21 168.6 22.28 171.0 22.23 167.14

24.69 177.5 24.69 184.2 24.69 190.0 24.69 183.88

27.10 190.3 27.10 199.8 27.10 203.4 27.10 197.82

29.59 201.5 29.59 210.0 29.59 215.8 29.59 209.11

32.00 211.0 32.07 218.1 32.00 220.9 32.02 216.68

34.48 216.6 34.48 224.7 34.48 218.0 34.48 219.78

34.48 237.0 34.48 241.9 34.48 246.3 34.48 241.74

32.69 222.3 32.62 232.3 32.62 245.3 32.64 233.31

30.90 210.8 30.90 220.3 30.90 229.1 30.90 220.06

29.03 196.4 29.03 202.6 29.03 199.5 29.03 199.47

27.24 185.5 27.24 194.1 27.24 198.2 27.24 192.60

25.45 176.9 25.45 184.2 25.45 185.4 25.45 182.16

23.66 166.2 23.66 175.8 23.66 177.8 23.66 173.25

21.86 155.5 21.86 162.4 21.86 168.7 21.86 162.19

20.07 144.2 20.07 147.7 20.07 147.5 20.07 146.46

18.21 133.5 18.21 138.7 18.21 139.5 18.21 137.27

16.41 124.8 16.41 128.7 16.41 135.3 16.41 129.60

14.62 113.2 14.62 117.1 14.62 120.3 14.62 116.87

12.83 101.4 12.83 103.8 12.83 106.0 12.83 103.73

11.03 91.2 11.03 93.7 11.03 96.3 11.03 93.71

9.24 79.4 9.24 81.6 9.24 83.5 9.24 81.49

7.45 67.7 7.45 69.7 7.45 70.9 7.45 69.41

5.62 56.2 5.61 57.2 5.61 59.3 5.62 57.55

3.79 43.6 3.80 44.0 3.81 45.8 3.80 44.47

2.01 29.6 2.01 29.9 2.01 31.0 2.01 30.16

0.20 17.0 0.19 16.8 0.21 17.5 0.20 17.13

Average Stdev

YS 20.2 20.0 20.5 20.2 0.3

VS 6.2 6.5 6.6 6.4 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 134 150 146 143 8
D - 45

Set D3: CS-BX5 – BL36- L2 – 3 day – NIST code (folder SR 50-SR-48D)

SR-48D

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 22.7 0.21 22.5 0.20 17.4 0.20 20.87

2.64 51.4 2.64 46.9 2.63 32.0 2.64 43.44

5.08 80.5 5.10 73.4 5.10 46.2 5.09 66.70

7.52 104.9 7.52 96.9 7.52 57.9 7.52 86.59

10.00 124.5 10.00 115.7 10.00 70.1 10.00 103.39

12.41 140.9 12.41 133.5 12.48 81.5 12.44 118.66

14.90 157.5 14.90 149.4 14.90 93.9 14.90 133.60

17.38 174.8 17.31 157.7 17.31 105.8 17.33 146.13

19.79 191.9 19.79 166.2 19.79 117.0 19.79 158.36

22.21 208.1 22.21 175.7 22.28 128.2 22.23 170.63

24.69 216.4 24.69 189.1 24.69 137.4 24.69 180.95

27.10 225.0 27.10 202.3 27.17 148.1 27.13 191.82

29.59 237.6 29.59 211.2 29.59 157.5 29.59 202.11

32.07 253.6 32.00 221.3 32.00 164.7 32.02 213.20

34.48 275.6 34.48 225.7 34.48 173.4 34.48 224.90

34.48 284.9 34.48 255.2 34.48 180.6 34.48 240.24

32.69 267.9 32.69 243.8 32.69 178.2 32.69 229.96

30.90 251.1 30.83 227.9 30.90 166.2 30.87 215.10

29.03 245.7 29.10 211.1 29.03 148.4 29.06 201.71

27.24 224.8 27.24 198.4 27.24 145.5 27.24 189.59

25.45 212.6 25.45 185.1 25.45 137.9 25.45 178.54

23.66 194.5 23.66 174.5 23.66 131.0 23.66 166.70

21.86 183.7 21.86 164.5 21.86 123.2 21.86 157.13

20.07 175.3 20.07 150.1 20.07 112.0 20.07 145.79

18.21 159.5 18.21 139.6 18.28 104.5 18.23 134.53

16.41 145.7 16.41 129.6 16.41 98.8 16.41 124.68

14.62 132.6 14.62 117.8 14.62 88.9 14.62 113.09

12.83 121.3 12.83 105.8 12.83 80.2 12.83 102.45

11.03 106.7 11.03 94.4 11.03 70.9 11.03 90.65

9.24 93.1 9.24 82.3 9.24 62.6 9.24 79.33

7.45 79.0 7.45 69.4 7.45 52.9 7.45 67.09

5.61 64.2 5.60 57.3 5.60 44.3 5.60 55.27

3.81 49.2 3.81 44.3 3.82 34.7 3.81 42.73

2.01 32.1 1.99 29.6 2.02 23.3 2.01 28.31

0.20 17.0 0.21 16.3 0.20 13.4 0.20 15.56

Average Stdev

YS 20.2 17.5 16.4 18.0 2.0

VS 7.6 6.8 4.8 6.4 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 459 433 88 327 207
D - 46

Set D7: CS-BX5 – BL11- L2 – 7 day – NIST code (folder SR 51-SR-48A)

SR-48A

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.21 26.9 0.19 25.8 0.20 22.2 0.20 24.96

2.64 52.2 2.64 50.3 2.63 40.3 2.64 47.58

5.10 79.8 5.08 72.6 5.10 59.0 5.10 70.48

7.52 105.9 7.52 92.6 7.52 76.6 7.52 91.72

10.00 122.6 10.00 110.1 10.00 91.2 10.00 107.96

12.41 142.4 12.41 126.9 12.41 105.8 12.41 125.05

14.90 161.3 14.90 143.2 14.90 121.4 14.90 141.96

17.31 180.8 17.38 161.5 17.31 138.0 17.33 160.08

19.79 195.8 19.79 177.4 19.79 147.4 19.79 173.51

22.28 212.9 22.21 192.4 22.28 159.4 22.25 188.21

24.69 226.7 24.69 206.3 24.69 179.4 24.69 204.14

27.17 240.5 27.10 221.8 27.17 190.2 27.15 217.50

29.59 253.2 29.59 235.5 29.59 197.9 29.59 228.87

32.00 263.7 32.00 246.1 32.00 211.5 32.00 240.42

34.48 278.7 34.48 255.9 34.48 206.5 34.48 247.03

34.48 300.5 34.48 275.3 34.48 237.9 34.48 271.21

32.69 282.2 32.62 255.1 32.69 230.7 32.67 256.01

30.90 264.2 30.90 242.0 30.83 208.2 30.87 238.11

29.03 247.5 29.03 230.3 29.03 204.1 29.03 227.29

27.24 235.5 27.24 217.0 27.24 182.8 27.24 211.80

25.45 221.1 25.45 207.4 25.45 175.8 25.45 201.44

23.66 208.2 23.66 196.3 23.66 160.6 23.66 188.37

21.86 193.8 21.86 181.3 21.86 149.6 21.86 174.89

20.07 180.9 20.07 170.6 20.07 151.2 20.07 167.55

18.28 165.7 18.21 156.1 18.28 137.4 18.25 153.07

16.41 154.3 16.41 143.5 16.41 115.7 16.41 137.86

14.62 140.5 14.62 131.7 14.62 111.4 14.62 127.87

12.83 124.0 12.83 118.5 12.83 102.7 12.83 115.07

11.03 112.0 11.03 106.5 11.03 91.8 11.03 103.43

9.24 97.3 9.24 92.6 9.24 80.1 9.24 89.97

7.38 82.6 7.45 79.5 7.45 70.1 7.43 77.41

5.61 67.9 5.61 64.9 5.61 55.7 5.61 62.87

3.81 52.2 3.80 49.9 3.82 42.9 3.81 48.35

2.00 34.5 2.02 33.9 2.01 29.9 2.01 32.75

0.21 18.7 0.20 19.2 0.19 17.3 0.20 18.37

Average Stdev

YS 21.7 23.7 19.5 21.6 2.1

VS 7.9 7.2 6.2 7.1 0.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 398 238 107 248 146
D - 47

Set D7: CS-BX5 – BL36- L1 – 7 day – NIST code (folder SR 51-SR-48B)

SR-48B

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 18.5 0.20 15.1 0.21 15.5 0.20 16.38

2.66 40.6 2.65 28.7 2.65 30.2 2.65 33.16

5.10 57.4 5.10 42.4 5.10 43.9 5.10 47.90

7.52 74.0 7.52 54.3 7.59 55.8 7.54 61.38

10.00 90.6 10.00 66.2 10.00 67.2 10.00 74.67

12.41 105.5 12.41 78.2 12.41 78.7 12.41 87.48

14.90 119.8 14.90 89.8 14.90 90.2 14.90 99.95

17.31 133.2 17.38 101.8 17.31 102.0 17.33 112.33

19.79 145.7 19.79 113.2 19.79 112.8 19.79 123.90

22.21 164.1 22.28 122.2 22.28 124.6 22.25 136.99

24.69 168.6 24.69 134.3 24.69 132.8 24.69 145.24

27.10 180.9 27.17 146.3 27.10 141.9 27.13 156.36

29.59 195.2 29.59 155.7 29.59 152.6 29.59 167.82

32.00 204.7 32.00 162.3 32.00 162.1 32.00 176.34

34.48 235.0 34.48 165.7 34.48 174.1 34.48 191.57

34.48 228.2 34.48 177.9 34.48 182.9 34.48 196.32

32.69 199.3 32.69 175.5 32.69 170.5 32.69 181.76

30.90 195.1 30.90 163.6 30.90 158.9 30.90 172.54

29.10 194.3 29.03 148.2 29.03 148.2 29.06 163.55

27.24 179.2 27.24 141.7 27.24 141.7 27.24 154.19

25.45 175.0 25.45 133.3 25.45 133.3 25.45 147.18

23.66 159.4 23.66 128.4 23.66 128.4 23.66 138.70

21.86 147.1 21.86 120.3 21.86 120.5 21.86 129.32

20.00 145.8 20.07 108.5 20.07 109.7 20.05 121.34

18.28 130.8 18.28 101.7 18.21 101.7 18.25 111.41

16.41 111.6 16.41 96.3 16.41 95.2 16.41 101.02

14.62 105.7 14.62 86.3 14.62 86.4 14.62 92.80

12.83 98.4 12.83 78.0 12.83 76.2 12.83 84.19

11.03 86.4 11.03 69.1 11.03 69.3 11.03 74.89

9.24 75.2 9.24 60.7 9.24 59.9 9.24 65.26

7.38 64.4 7.45 51.0 7.45 51.1 7.43 55.50

5.61 51.7 5.60 42.5 5.61 42.1 5.60 45.41

3.81 39.5 3.82 33.5 3.81 32.3 3.81 35.11

1.99 25.8 2.01 22.0 2.02 21.7 2.01 23.20

0.20 13.4 0.20 12.2 0.21 12.0 0.20 12.53

Average Stdev

YS 18.2 14.9 14.5 15.9 2.1

VS 5.9 4.8 4.8 5.2 0.7

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 267 46 76 130 120
D - 48

Set D7: CS-BX5 – BL11- L1 – 7 day – NIST code (folder SR 51-SR-48C)

SR-48C

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.21 21.4 0.20 28.8 0.20 27.1 0.20 25.74

2.65 40.3 2.64 62.4 2.65 59.4 2.65 54.02

5.08 59.3 5.11 96.9 5.10 88.9 5.10 81.71

7.52 75.8 7.52 127.8 7.59 111.9 7.54 105.17

10.00 92.3 10.00 150.9 10.00 130.0 10.00 124.38

12.41 108.2 12.41 176.0 12.48 150.8 12.44 145.00

14.90 123.9 14.90 198.0 14.90 171.6 14.90 164.49

17.38 140.7 17.31 220.0 17.38 188.5 17.36 183.07

19.79 154.3 19.79 239.0 19.79 204.8 19.79 199.37

22.21 166.8 22.21 259.3 22.21 218.3 22.21 214.80

24.69 182.4 24.69 275.2 24.69 240.3 24.69 232.62

27.10 198.0 27.10 289.8 27.10 256.5 27.10 248.12

29.59 208.8 29.59 304.2 29.59 266.6 29.59 259.86

32.00 214.5 32.00 315.9 32.00 280.3 32.00 270.22

34.48 216.8 34.48 329.8 34.48 291.1 34.48 279.26

34.48 239.2 34.48 358.1 34.48 316.6 34.48 304.65

32.62 229.6 32.69 340.4 32.62 297.3 32.64 289.12

30.90 214.9 30.90 321.1 30.90 280.4 30.90 272.11

29.03 198.6 29.03 295.9 29.03 258.8 29.03 251.09

27.24 192.3 27.24 285.6 27.24 250.7 27.24 242.87

25.45 180.2 25.45 268.2 25.45 235.7 25.45 228.03

23.66 173.1 23.66 251.1 23.66 223.1 23.66 215.76

21.86 161.5 21.86 234.9 21.86 208.0 21.86 201.48

20.07 148.6 20.07 215.7 20.07 189.6 20.07 184.62

18.21 136.7 18.21 199.1 18.21 175.4 18.21 170.40

16.41 126.6 16.41 184.7 16.41 163.2 16.41 158.18

14.62 116.3 14.62 168.1 14.62 149.0 14.62 144.48

12.83 102.0 12.83 149.1 12.83 132.3 12.83 127.81

11.03 93.5 11.03 132.5 11.03 119.5 11.03 115.17

9.24 80.7 9.24 116.2 9.24 103.0 9.24 99.96

7.45 69.3 7.45 97.3 7.45 87.5 7.45 84.71

5.61 56.5 5.61 79.2 5.61 71.6 5.61 69.08

3.80 43.1 3.82 60.4 3.81 54.4 3.81 52.61

2.01 29.5 2.00 38.8 2.02 36.2 2.01 34.83

0.19 16.3 0.20 19.2 0.20 19.4 0.20 18.30

Average Stdev

YS 20.0 23.4 23.0 22.2 1.9

VS 6.4 9.7 8.4 8.1 1.7

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 139 548 406 364 207
D - 49

Set D7: CS-BX5 – BL36- L2– 7 day – NIST code (folder SR 51-SR-48D)

SR-48D

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.19 19.6 0.20 16.4 0.20 21.7 0.20 19.24

2.65 42.4 2.65 30.4 2.64 47.3 2.65 40.04

5.10 63.9 5.10 44.1 5.10 71.7 5.10 59.91

7.52 84.1 7.52 55.5 7.52 94.6 7.52 78.07

10.00 99.3 10.00 66.8 10.00 111.6 10.00 92.53

12.41 114.3 12.41 78.1 12.41 129.1 12.41 107.17

14.90 129.0 14.90 89.1 14.90 146.3 14.90 121.48

17.38 143.9 17.38 100.8 17.38 160.0 17.38 134.90

19.79 157.4 19.79 110.9 19.79 176.1 19.79 148.13

22.21 170.1 22.21 121.6 22.21 188.5 22.21 160.08

24.69 181.6 24.69 130.6 24.69 204.9 24.69 172.38

27.10 194.7 27.10 141.6 27.17 216.3 27.13 184.22

29.59 203.9 29.59 153.7 29.59 228.5 29.59 195.38

32.07 213.1 32.00 161.2 32.00 241.8 32.02 205.37

34.48 227.2 34.48 173.2 34.48 243.2 34.48 214.53

34.48 245.5 34.48 168.6 34.48 268.5 34.48 227.52

32.69 226.6 32.69 161.0 32.69 261.3 32.69 216.31

30.90 212.6 30.83 156.5 30.90 241.5 30.87 203.55

29.03 200.6 29.03 151.2 29.03 227.7 29.03 193.20

27.24 188.5 27.24 140.5 27.24 214.1 27.24 181.04

25.45 180.0 25.45 135.8 25.45 200.3 25.45 172.04

23.66 168.0 23.66 126.0 23.66 185.0 23.66 159.66

21.86 157.5 21.86 117.2 21.86 176.5 21.86 150.39

20.07 146.5 20.07 111.5 20.07 163.6 20.07 140.55

18.21 133.1 18.21 102.0 18.28 148.1 18.23 127.73

16.41 121.7 16.41 92.0 16.41 137.7 16.41 117.15

14.62 112.5 14.62 85.4 14.62 126.4 14.62 108.09

12.83 100.2 12.83 77.4 12.83 114.1 12.83 97.26

11.03 89.7 11.03 68.7 11.03 99.6 11.03 86.00

9.24 77.7 9.24 60.4 9.24 87.0 9.24 75.03

7.45 66.4 7.45 51.8 7.38 73.4 7.43 63.86

5.62 54.0 5.61 42.2 5.61 60.2 5.62 52.14

3.81 40.9 3.81 32.6 3.82 46.6 3.81 40.05

2.01 27.5 2.01 22.4 2.01 30.1 2.01 26.65

0.19 14.8 0.21 12.5 0.20 15.8 0.20 14.37

Average Stdev

YS 16.5 16.7 17.9 17.0 0.8

VS 6.4 4.6 7.3 6.1 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 313 85 329 242 137
D - 50

Set E1: CS-BX5 – BL11- L2 – Mixing Day – NIST code (folder SR 53-SR-52A)

SR-52A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.21 28.7 0.19 30.7 0.21 37.2 0.20 32.20

2.63 63.3 2.64 60.1 2.65 74.3 2.64 65.90

5.10 89.4 5.09 84.4 5.08 125.8 5.09 99.86

7.52 117.8 7.52 109.6 7.52 167.7 7.52 131.72

10.00 136.5 10.00 128.2 10.00 190.8 10.00 151.85

12.41 156.1 12.41 146.0 12.41 216.1 12.41 172.76

14.90 176.8 14.90 165.4 14.90 231.9 14.90 191.37

17.31 192.9 17.38 183.3 17.31 247.4 17.33 207.89

19.79 209.5 19.79 197.9 19.79 264.9 19.79 224.10

22.21 226.2 22.21 216.7 22.21 287.9 22.21 243.59

24.69 241.3 24.69 226.3 24.69 292.9 24.69 253.49

27.10 258.0 27.10 242.1 27.10 308.1 27.10 269.41

29.59 272.9 29.59 255.5 29.59 331.6 29.59 286.67

32.00 284.7 32.00 263.4 32.00 343.1 32.00 297.07

34.48 295.5 34.48 280.5 34.48 379.1 34.48 318.35

34.48 319.1 34.48 298.6 34.48 390.0 34.48 335.88

32.69 306.7 32.62 271.9 32.62 362.2 32.64 313.59

30.90 285.8 30.90 262.9 30.90 347.2 30.90 298.59

29.03 264.4 29.03 248.3 29.03 320.1 29.03 277.63

27.24 254.9 27.24 236.6 27.24 309.0 27.24 266.81

25.45 239.1 25.45 226.5 25.45 294.7 25.45 253.43

23.66 226.3 23.66 215.7 23.66 278.5 23.66 240.17

21.86 212.6 21.86 199.9 21.86 257.9 21.86 223.45

20.07 194.8 20.07 186.3 20.07 240.6 20.07 207.25

18.28 181.1 18.21 170.7 18.21 221.7 18.23 191.18

16.41 169.8 16.41 155.5 16.41 200.5 16.41 175.23

14.62 156.1 14.62 145.1 14.62 186.6 14.62 162.61

12.83 140.7 12.83 129.4 12.83 166.0 12.83 145.36

11.03 125.2 11.03 116.7 11.03 150.8 11.03 130.90

9.24 109.9 9.24 101.7 9.24 129.8 9.24 113.77

7.38 94.4 7.45 87.8 7.45 112.4 7.43 98.18

5.61 78.5 5.62 71.9 5.61 91.4 5.62 80.60

3.82 61.3 3.81 55.4 3.79 69.8 3.81 62.18

2.00 41.7 2.01 38.6 2.01 47.3 2.00 42.52

0.21 24.0 0.20 22.1 0.20 25.7 0.20 23.93

Average Stdev

YS 29.2 27.8 32.3 29.8 2.3

VS 8.5 7.7 10.3 8.8 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 270 404 854 509 306
D - 51

Set E1: CS-BX5 – BL36- L1 – Mixing Day – NIST code (folder SR 53-SR-52B)

SR-52B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 39.3 0.21 23.0 0.20 28.4 0.20 30.24

2.64 80.1 2.66 39.7 2.65 54.3 2.65 58.02

5.10 133.4 5.10 56.6 5.09 83.1 5.10 91.01

7.52 172.3 7.52 71.2 7.52 108.9 7.52 117.47

10.00 191.2 10.00 85.3 10.00 128.6 10.00 135.01

12.41 217.5 12.41 99.2 12.41 146.2 12.41 154.30

14.90 240.7 14.90 113.4 14.90 161.5 14.90 171.86

17.31 263.0 17.31 128.8 17.31 177.2 17.31 189.65

19.79 281.9 19.79 139.4 19.79 194.9 19.79 205.39

22.21 303.4 22.21 152.6 22.21 211.6 22.21 222.54

24.69 316.5 24.69 165.6 24.69 221.3 24.69 234.46

27.10 334.6 27.10 178.7 27.10 232.8 27.10 248.69

29.59 357.8 29.59 190.1 29.59 247.1 29.59 264.99

32.00 377.4 32.00 201.9 32.00 263.8 32.00 281.01

34.48 406.3 34.48 216.1 34.48 285.3 34.48 302.54

34.48 420.2 34.48 214.7 34.48 286.2 34.48 307.04

32.69 397.4 32.69 204.6 32.69 269.3 32.69 290.43

30.90 376.8 30.83 198.6 30.83 257.7 30.85 277.71

29.03 354.1 29.10 185.1 29.03 258.3 29.06 265.83

27.24 340.3 27.24 176.4 27.24 232.6 27.24 249.78

25.45 318.5 25.45 168.4 25.45 221.8 25.45 236.24

23.66 301.1 23.66 159.0 23.66 204.4 23.66 221.51

21.86 281.3 21.86 148.2 21.86 191.0 21.86 206.81

20.07 257.8 20.07 138.8 20.00 182.4 20.05 193.00

18.21 240.5 18.28 129.1 18.28 169.3 18.25 179.62

16.41 222.5 16.41 116.7 16.41 154.4 16.41 164.54

14.62 203.7 14.62 108.3 14.62 141.9 14.62 151.31

12.83 182.1 12.83 98.1 12.83 130.0 12.83 136.72

11.03 162.0 11.03 88.4 11.03 113.7 11.03 121.40

9.24 141.4 9.24 77.1 9.24 100.3 9.24 106.27

7.45 120.7 7.45 66.3 7.38 85.4 7.43 90.81

5.60 98.4 5.60 54.7 5.61 70.2 5.60 74.39

3.81 75.2 3.80 42.7 3.81 54.4 3.81 57.46

2.01 48.6 1.99 29.5 1.99 35.6 2.00 37.88

0.20 24.7 0.20 17.3 0.20 19.5 0.20 20.52

Average Stdev

YS 33.5 22.5 26.6 27.5 5.6

VS 11.2 5.7 7.6 8.2 2.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 718 107 390 405 306
D - 52

Set E1: CS-BX5 – BL11- L1 – Mixing Day – NIST code (folder SR 53-SR-52C)

SR-52C

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.20 26.5 0.20 33.8 0.21 33.7 0.20 31.31

2.63 44.0 2.64 60.1 2.65 67.0 2.64 57.00

5.11 61.6 5.10 93.1 5.10 97.9 5.10 84.20

7.52 77.6 7.52 120.2 7.52 128.5 7.52 108.77

10.00 92.5 10.00 140.5 10.00 147.5 10.00 126.86

12.41 107.6 12.41 154.3 12.41 167.7 12.41 143.19

14.90 122.6 14.90 172.0 14.90 187.4 14.90 160.68

17.31 138.6 17.31 190.0 17.31 205.5 17.31 178.04

19.79 152.6 19.79 205.6 19.79 225.7 19.79 194.63

22.28 164.7 22.21 218.5 22.21 242.3 22.23 208.49

24.69 180.9 24.69 233.4 24.69 255.3 24.69 223.20

27.10 197.4 27.17 241.7 27.17 268.1 27.15 235.73

29.59 206.7 29.59 248.0 29.59 284.2 29.59 246.33

32.00 215.7 32.00 264.5 32.00 304.5 32.00 261.54

34.48 216.0 34.48 273.0 34.48 328.2 34.48 272.40

34.48 235.6 34.48 305.8 34.48 339.0 34.48 293.47

32.69 229.8 32.69 286.2 32.69 307.0 32.69 274.32

30.83 213.8 30.83 266.9 30.83 294.3 30.83 258.35

29.03 200.5 29.03 260.1 29.03 294.8 29.03 251.79

27.24 192.0 27.24 238.2 27.24 271.9 27.24 234.03

25.45 181.3 25.45 228.2 25.45 259.4 25.45 222.98

23.66 166.5 23.66 208.8 23.66 243.1 23.66 206.12

21.86 160.3 21.86 198.1 21.86 225.3 21.86 194.57

20.07 149.2 20.07 185.6 20.07 216.0 20.07 183.63

18.21 138.4 18.28 171.8 18.21 196.6 18.23 168.95

16.41 131.0 16.41 160.3 16.41 174.8 16.41 155.39

14.62 119.0 14.62 146.6 14.62 205.8 14.62 157.14

12.83 109.4 12.83 134.7 12.83 117.6 12.83 120.57

11.03 96.6 11.03 116.9 11.03 109.6 11.03 107.67

9.24 85.4 9.24 103.8 9.24 116.6 9.24 101.93

7.38 73.3 7.45 87.6 7.45 100.3 7.43 87.07

5.61 61.6 5.61 73.3 5.61 81.3 5.61 72.07

3.82 48.8 3.81 57.8 3.82 62.9 3.82 56.49

2.01 32.9 2.01 38.3 2.00 42.6 2.01 37.93

0.20 19.8 0.20 21.8 0.21 23.6 0.20 21.72

Average Stdev

YS 25.7 26.9 29.2 27.3 1.7

VS 6.1 7.9 8.9 7.7 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 71 471 449 330 225
D - 53

Set E1: CS-BX5 – BL36- L2 – Mixing Day – NIST code (folder SR 53-SR-52D)

SR-52D

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.19 24.4 0.20 28.7 0.20 21.8 0.20 24.96

2.65 41.9 2.65 62.1 2.64 39.5 2.65 47.84

5.09 57.2 5.10 92.4 5.10 56.8 5.10 68.80

7.59 72.7 7.59 121.5 7.52 71.9 7.56 88.70

10.00 87.6 10.00 141.7 10.00 86.6 10.00 105.31

12.41 101.2 12.41 160.8 12.41 102.0 12.41 121.33

14.90 114.3 14.90 180.1 14.90 117.0 14.90 137.13

17.31 128.5 17.31 198.6 17.31 130.3 17.31 152.43

19.79 142.4 19.79 216.1 19.79 144.5 19.79 167.68

22.21 158.2 22.21 235.4 22.21 157.6 22.21 183.73

24.69 165.5 24.69 243.4 24.69 170.1 24.69 193.00

27.10 176.1 27.10 257.9 27.17 184.9 27.13 206.30

29.59 189.3 29.59 276.0 29.59 196.8 29.59 220.69

32.00 201.6 32.00 290.6 32.00 205.7 32.00 232.63

34.48 221.2 34.48 318.5 34.48 211.2 34.48 250.29

34.48 213.8 34.48 327.6 34.48 226.7 34.48 256.04

32.69 198.9 32.69 299.6 32.69 218.0 32.69 238.82

30.90 191.3 30.90 281.7 30.83 203.4 30.87 225.46

29.03 191.6 29.03 279.8 29.03 192.5 29.03 221.26

27.24 177.8 27.24 260.2 27.24 181.6 27.24 206.54

25.45 167.6 25.45 247.8 25.45 172.2 25.45 195.89

23.66 158.7 23.66 227.3 23.66 161.4 23.66 182.48

21.86 147.4 21.86 212.2 21.86 152.0 21.86 170.54

20.07 142.7 20.07 203.6 20.07 141.2 20.07 162.50

18.21 129.9 18.28 184.3 18.28 131.3 18.25 148.49

16.48 115.2 16.41 167.4 16.41 123.5 16.44 135.37

14.62 107.8 14.62 156.4 14.62 111.5 14.62 125.22

12.83 99.4 12.83 141.9 12.83 101.7 12.83 114.32

11.03 87.9 11.03 124.3 11.03 89.5 11.03 100.60

9.24 77.4 9.24 109.0 9.24 78.7 9.24 88.38

7.45 66.9 7.45 93.3 7.38 67.2 7.43 75.78

5.61 54.5 5.61 75.7 5.61 55.3 5.61 61.85

3.81 42.4 3.81 57.6 3.81 43.2 3.81 47.74

2.01 28.9 2.01 37.3 2.01 28.4 2.01 31.56

0.20 16.8 0.19 19.6 0.20 15.9 0.20 17.43

Average Stdev

YS 23.0 26.1 20.9 23.3 2.6

VS 5.6 8.6 6.0 6.7 1.6

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 158 479 76 238 213
D - 54

Set E3: CS-BX5 – BL11- L2 – 3 day – NIST code (folder SR 54-SR-52A)

SR-52A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 17.71 0.20 21.6 0.20 21.2 0.23 20.18

2.64 40.90 2.65 41.6 2.65 39.0 2.65 40.50

5.10 56.90 5.09 58.1 5.10 55.7 5.09 56.91

7.52 71.43 7.59 72.5 7.52 70.5 7.54 71.47

10.00 85.46 10.00 88.5 10.00 84.1 10.00 86.01

12.41 98.93 12.41 104.1 12.41 98.3 12.41 100.43

14.90 113.42 14.90 119.5 14.90 111.9 14.90 114.91

17.31 128.77 17.38 134.1 17.31 126.7 17.33 129.88

19.79 140.48 19.79 147.6 19.79 139.9 19.79 142.66

22.21 154.94 22.21 161.5 22.21 151.7 22.21 156.03

24.69 166.46 24.69 175.7 24.69 163.3 24.69 168.49

27.10 179.60 27.10 188.5 27.10 175.2 27.10 181.09

29.59 190.96 29.59 199.7 29.59 186.6 29.59 192.44

32.00 199.14 32.00 212.9 32.00 195.3 32.00 202.45

34.48 206.80 34.48 224.9 34.48 208.3 34.48 213.35

34.48 220.54 34.48 230.3 34.48 215.1 34.48 221.96

32.69 208.98 32.69 222.6 32.62 200.8 32.67 210.79

30.83 198.36 30.90 209.6 30.90 192.6 30.87 200.18

29.03 183.38 29.03 194.1 29.03 181.0 29.03 186.15

27.24 175.33 27.24 187.9 27.24 173.6 27.24 178.92

25.45 166.62 25.45 175.7 25.45 164.8 25.45 169.05

23.66 157.25 23.66 166.5 23.66 155.5 23.66 159.74

21.86 146.42 21.86 156.3 21.86 144.6 21.86 149.11

20.07 136.46 20.07 143.3 20.07 134.7 20.07 138.14

18.21 125.70 18.21 133.2 18.21 123.9 18.21 127.62

16.41 117.34 16.48 123.9 16.41 114.2 16.44 118.49

14.62 107.61 14.62 111.8 14.62 106.1 14.62 108.49

12.83 94.90 12.83 100.4 12.83 93.7 12.83 96.32

11.03 86.48 11.03 90.3 11.03 85.0 11.03 87.26

9.24 75.24 9.24 78.6 9.24 73.9 9.24 75.91

7.45 64.16 7.45 67.0 7.45 64.1 7.45 65.06

5.61 53.51 5.61 55.5 5.61 52.4 5.61 53.80

3.82 41.71 3.81 43.6 3.80 40.3 3.81 41.85

2.01 28.65 2.01 29.7 2.01 28.3 2.01 28.88

0.19 16.42 0.20 16.8 0.21 16.3 0.20 16.53

Average Stdev

YS 19.9 20.2 20.2 20.1 0.2

VS 5.8 6.1 5.6 5.9 0.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 134 122 145 134 12
D - 55

Set E3: CS-BX5 – BL36- L1 – 3 day – NIST code (folder SR 54-SR-52B)

SR-52B

Run# D Run# E Run# F Average

SR SS SR SS SR SS SR SS

0.20 22.8 0.20 21.9 0.21 25.1 0.20 23.28

2.65 48.4 2.65 45.8 2.65 54.3 2.65 49.50

5.08 74.1 5.10 69.8 5.09 79.1 5.09 74.34

7.59 94.9 7.52 92.7 7.52 103.5 7.54 97.03

10.00 113.1 10.00 108.0 10.00 125.8 10.00 115.66

12.41 131.1 12.41 125.2 12.41 143.9 12.41 133.42

14.90 148.0 14.90 140.9 14.90 163.0 14.90 150.63

17.31 165.0 17.31 157.6 17.38 180.5 17.33 167.71

19.79 179.4 19.79 173.1 19.79 198.8 19.79 183.75

22.21 192.3 22.21 187.3 22.21 216.1 22.21 198.60

24.69 206.4 24.69 201.4 24.69 228.4 24.69 212.05

27.10 222.1 27.10 214.1 27.10 243.8 27.10 226.64

29.59 232.8 29.59 226.6 29.59 258.8 29.59 239.40

32.00 240.4 32.00 239.6 32.00 273.0 32.00 250.98

34.48 245.8 34.48 254.8 34.48 292.4 34.48 264.32

34.48 268.7 34.48 264.9 34.48 295.6 34.48 276.42

32.62 261.0 32.69 246.3 32.62 275.7 32.64 260.99

30.90 246.4 30.90 234.8 30.90 267.9 30.90 249.74

29.03 225.1 29.03 224.1 29.03 258.4 29.03 235.88

27.24 218.0 27.24 210.8 27.24 240.6 27.24 223.11

25.45 205.5 25.45 201.2 25.45 227.7 25.45 211.44

23.66 193.9 23.66 188.0 23.66 215.4 23.66 199.09

21.86 179.4 21.86 174.3 21.86 201.1 21.86 184.91

20.07 165.2 20.07 163.5 20.07 187.8 20.07 172.16

18.21 152.1 18.21 150.3 18.21 172.3 18.21 158.25

16.41 142.4 16.41 137.6 16.41 155.8 16.41 145.26

14.62 129.2 14.62 127.1 14.62 144.2 14.62 133.49

12.83 114.3 12.83 115.2 12.83 130.9 12.83 120.13

11.03 103.1 11.03 102.3 11.03 115.0 11.03 106.79

9.24 89.2 9.24 89.1 9.24 100.0 9.24 92.76

7.45 75.7 7.45 75.9 7.45 85.6 7.45 79.08

5.61 62.3 5.59 61.6 5.62 68.9 5.61 64.26

3.80 47.7 3.81 47.4 3.81 52.4 3.81 49.15

2.01 32.0 1.99 31.4 2.01 34.6 2.00 32.66

0.20 17.2 0.20 16.8 0.20 17.7 0.20 17.23

Average Stdev

YS 20.2 21.7 24.0 22.0 1.9

VS 7.3 7.0 8.0 7.4 0.5

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 319 284 370 324 43
D - 56

Set E3: CS-BX5 – BL11- L1 – 3 day – NIST code (folder SR 54-SR-52C)

SR-52C

Run# J Run# K Run# L Average

SR SS SR SS SR SS SR SS

0.20 23.0 0.20 22.8 0.20 20.4 0.20 22.08

2.63 45.4 2.65 44.4 2.66 40.0 2.64 43.25

5.10 67.3 5.09 64.9 5.08 62.4 5.09 64.87

7.52 87.3 7.59 83.8 7.59 83.1 7.56 84.70

10.00 104.9 10.00 100.1 10.00 100.0 10.00 101.66

12.41 121.5 12.41 115.7 12.41 114.9 12.41 117.41

14.90 136.6 14.90 131.0 14.90 128.3 14.90 131.93

17.31 151.1 17.31 147.8 17.38 142.8 17.33 147.21

19.79 166.5 19.79 162.0 19.79 159.9 19.79 162.78

22.21 180.8 22.21 176.3 22.21 172.4 22.21 176.50

24.69 191.7 24.69 186.3 24.69 182.5 24.69 186.83

27.17 203.6 27.10 198.1 27.10 195.6 27.13 199.10

29.59 215.6 29.59 210.8 29.59 206.5 29.59 210.95

32.00 228.7 32.00 217.6 32.07 220.6 32.02 222.29

34.48 245.9 34.48 230.5 34.48 239.4 34.48 238.60

34.48 257.0 34.48 244.1 34.48 243.2 34.48 248.08

32.69 239.9 32.69 229.4 32.69 225.7 32.69 231.69

30.83 223.0 30.90 217.9 30.90 212.9 30.87 217.94

29.03 215.9 29.03 203.5 29.03 212.2 29.03 210.51

27.24 202.5 27.24 195.0 27.24 195.9 27.24 197.80

25.45 192.1 25.45 185.1 25.45 182.5 25.45 186.57

23.66 178.7 23.66 176.7 23.66 170.4 23.66 175.25

21.86 166.4 21.86 163.3 21.86 161.1 21.86 163.58

20.07 155.4 20.07 150.4 20.07 153.7 20.07 153.18

18.21 143.6 18.21 138.5 18.21 138.9 18.21 140.34

16.41 132.3 16.41 128.4 16.41 126.0 16.41 128.87

14.62 120.5 14.62 118.2 14.62 116.5 14.62 118.41

12.83 108.5 12.83 104.7 12.83 105.9 12.83 106.39

11.03 97.3 11.03 94.7 11.03 94.0 11.03 95.34

9.24 84.8 9.24 82.0 9.24 82.2 9.24 83.01

7.45 72.6 7.45 70.2 7.45 70.5 7.45 71.12

5.61 59.2 5.61 57.8 5.61 57.8 5.61 58.29

3.81 46.0 3.81 44.6 3.81 44.7 3.81 45.10

2.00 31.0 2.01 30.7 2.01 30.3 2.00 30.67

0.20 17.5 0.20 17.3 0.19 17.2 0.20 17.35

Average Stdev

YS 20.4 20.9 21.1 20.8 0.4

VS 6.7 6.4 6.4 6.5 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 281 265 215 254 35
D - 57

Set E3: CS-BX5 – BL36- L2 – 3 day – NIST code (folder SR 54-SR-52D)

SR-52D

Run# G Run# H Run# I Average

SR SS SR SS SR SS SR SS

0.19 18.7 0.21 17.6 0.20 22.0 0.20 19.42

2.64 38.2 2.65 35.6 2.64 48.4 2.64 40.72

5.08 56.8 5.10 53.8 5.08 70.3 5.09 60.29

7.52 72.3 7.52 68.9 7.52 86.6 7.52 75.92

10.00 87.5 10.00 83.5 10.00 123.9 10.00 98.32

12.41 102.2 12.41 97.6 12.41 144.0 12.41 114.62

14.90 116.4 14.90 111.2 14.90 160.1 14.90 129.20

17.31 130.3 17.31 124.9 17.38 181.1 17.33 145.44

19.79 144.5 19.79 137.8 19.79 199.4 19.79 160.57

22.21 157.6 22.21 152.3 22.21 218.0 22.21 175.94

24.69 167.8 24.69 162.4 24.69 231.4 24.69 187.19

27.10 181.1 27.10 174.3 27.10 248.0 27.10 201.13

29.59 195.6 29.59 185.7 29.59 262.5 29.59 214.61

32.00 203.6 32.00 196.3 32.00 274.7 32.00 224.88

34.48 214.5 34.48 212.5 34.48 294.1 34.48 240.40

34.48 221.2 34.48 209.4 34.48 304.7 34.48 245.13

32.62 209.8 32.69 200.1 32.62 286.5 32.64 232.15

30.90 203.1 30.90 193.3 30.90 273.6 30.90 223.32

29.03 190.1 29.10 181.6 29.03 256.8 29.06 209.52

27.24 176.8 27.24 170.0 27.24 245.1 27.24 197.29

25.45 169.6 25.45 163.4 25.45 229.3 25.45 187.42

23.66 160.9 23.66 152.5 23.66 218.7 23.66 177.35

21.86 150.2 21.86 141.2 21.86 203.5 21.86 164.96

20.07 140.6 20.07 134.7 20.07 185.1 20.07 153.48

18.21 127.1 18.21 123.4 18.21 170.9 18.21 140.46

16.41 116.7 16.41 110.7 16.41 158.8 16.41 128.73

14.62 108.4 14.62 102.7 14.62 144.6 14.62 118.54

12.83 96.1 12.83 91.6 12.83 127.9 12.83 105.19

11.03 86.2 11.03 82.6 11.03 114.1 11.03 94.31

9.24 74.7 9.24 71.4 9.24 98.8 9.24 81.63

7.45 64.0 7.45 61.4 7.45 83.7 7.45 69.71

5.61 52.1 5.61 49.4 5.61 68.1 5.61 56.52

3.81 39.5 3.81 37.6 3.81 51.1 3.81 42.72

2.02 26.6 1.99 25.2 2.01 33.0 2.01 28.27

0.21 14.3 0.20 13.7 0.20 15.7 0.20 14.53

Average Stdev

YS 18.1 17.4 20.4 18.6 1.6

VS 6.0 5.7 8.3 6.6 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 170 187 283 213 61
D - 58

Set E7: CS-BX5 – BL11- L2 – 7 day – NIST code (folder SR 55-SR-52A)

SR-52A

Run# L Run# M Run# N Average

SR SS SR SS SR SS SR SS

0.21 20.8 0.20 20.4 0.20 20.2 0.20 20.47

2.65 38.5 2.65 37.1 2.65 36.9 2.65 37.50

5.10 56.0 5.10 53.2 5.10 54.4 5.10 54.51

7.52 71.6 7.52 66.8 7.52 68.9 7.52 69.11

10.00 86.5 10.00 80.4 10.00 82.8 10.00 83.24

12.41 101.1 12.41 94.7 12.41 97.4 12.41 97.72

14.90 115.6 14.90 108.9 14.90 111.5 14.90 111.97

17.31 129.4 17.38 122.4 17.31 125.8 17.33 125.89

19.79 143.6 19.79 135.7 19.79 140.0 19.79 139.77

22.21 156.7 22.21 144.5 22.21 154.4 22.21 151.87

24.69 167.8 24.69 160.0 24.69 167.2 24.69 165.02

27.17 181.4 27.17 174.8 27.10 178.7 27.15 178.31

29.59 193.3 29.59 182.2 29.59 190.1 29.59 188.53

32.00 206.4 32.00 193.2 32.00 201.9 32.00 200.47

34.48 223.8 34.48 195.5 34.48 216.1 34.48 211.81

34.48 224.1 34.48 209.4 34.48 221.4 34.48 218.31

32.69 206.9 32.69 204.9 32.69 207.0 32.69 206.28

30.83 198.9 30.83 190.1 30.83 195.1 30.83 194.71

29.03 193.8 29.03 180.4 29.03 188.9 29.03 187.70

27.24 180.7 27.24 171.8 27.24 178.1 27.24 176.86

25.45 173.6 25.45 160.2 25.45 166.4 25.45 166.75

23.66 159.4 23.66 148.6 23.66 159.0 23.66 155.66

21.86 149.5 21.86 142.4 21.86 148.2 21.86 146.68

20.07 144.0 20.07 132.6 20.07 140.0 20.07 138.86

18.28 131.3 18.21 123.3 18.21 127.9 18.23 127.51

16.41 118.2 16.41 112.6 16.41 117.2 16.41 115.98

14.62 109.7 14.62 102.5 14.62 108.4 14.62 106.87

12.83 98.8 12.83 95.0 12.83 97.6 12.83 97.15

11.03 88.7 11.03 82.9 11.03 87.4 11.03 86.30

9.24 77.5 9.24 72.9 9.24 76.5 9.24 75.66

7.45 66.6 7.38 62.8 7.45 65.5 7.43 64.98

5.60 54.3 5.61 51.5 5.60 53.6 5.60 53.12

3.82 42.0 3.81 40.2 3.81 41.7 3.81 41.31

2.01 28.8 2.01 27.0 2.00 28.3 2.01 28.05

0.20 16.4 0.20 15.6 0.20 16.2 0.20 16.11

Average Stdev

YS 21.0 19.4 20.7 20.4 0.8

VS 5.9 5.6 5.8 5.8 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 109 73 73 85 21
D - 59

Set E7: CS-BX5 – BL36- L1 – 7 day – NIST code (folder SR 55-SR-52B)

SR-52B

Run# A Run# B Run# D Average

SR SS SR SS SR SS SR SS

0.20 23.8 0.21 22.0 0.26 14.0 0.22 19.95

2.65 58.3 2.65 49.7 2.63 34.5 2.64 47.51

5.09 93.1 5.10 79.5 5.09 50.7 5.09 74.43

7.52 120.7 7.52 109.9 7.52 65.4 7.52 98.69

10.00 140.4 10.00 129.6 10.00 79.5 10.00 116.49

12.41 159.3 12.41 150.6 12.41 92.9 12.41 134.26

14.90 178.1 14.90 160.9 14.90 105.3 14.90 148.09

17.31 198.8 17.31 171.9 17.31 118.4 17.31 163.05

19.79 215.2 19.79 191.8 19.79 131.4 19.79 179.46

22.21 235.7 22.21 211.1 22.21 143.3 22.21 196.72

24.69 247.8 24.69 224.8 24.69 150.9 24.69 207.85

27.10 261.6 27.10 240.3 27.10 161.8 27.10 221.24

29.59 276.6 29.59 253.6 29.59 176.9 29.59 235.68

32.00 292.6 32.00 264.6 32.00 187.3 32.00 248.19

34.48 315.1 34.48 282.9 34.48 203.7 34.48 267.24

34.48 323.5 34.48 293.8 34.48 201.4 34.48 272.90

32.69 305.4 32.69 272.7 32.69 186.4 32.69 254.82

30.90 290.0 30.83 265.0 30.90 178.8 30.87 244.59

29.03 277.0 29.10 254.1 29.03 176.6 29.06 235.88

27.24 260.2 27.24 234.3 27.24 164.1 27.24 219.55

25.45 248.4 25.45 224.6 25.45 153.8 25.45 208.92

23.66 231.5 23.66 206.7 23.66 146.2 23.66 194.81

21.86 215.5 21.86 193.3 21.86 136.7 21.86 181.85

20.07 202.6 20.07 183.3 20.07 130.3 20.07 172.08

18.21 185.9 18.21 167.8 18.21 117.5 18.21 157.09

16.41 169.8 16.41 151.3 16.41 104.9 16.41 142.00

14.62 155.7 14.62 138.4 14.62 98.1 14.62 130.73

12.83 138.9 12.83 125.6 12.83 88.4 12.83 117.62

11.03 123.9 11.03 111.3 11.03 79.4 11.03 104.87

9.24 107.6 9.24 96.8 9.24 68.9 9.24 91.11

7.45 91.4 7.45 82.2 7.45 59.3 7.45 77.62

5.61 73.8 5.61 66.7 5.61 47.9 5.61 62.80

3.80 55.7 3.81 51.1 3.79 36.8 3.80 47.88

2.01 36.2 1.99 33.1 2.02 24.9 2.01 31.41

0.20 17.9 0.20 17.3 0.20 13.5 0.20 16.24

Average Stdev

YS 24.1 21.5 17.8 21.1 3.2

VS 8.7 7.9 5.4 7.3 1.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 460 419 137 339 176
D - 60

Set E7: CS-BX5 – BL11- L1 – 7 day – NIST code (folder SR 55-SR-52C)

SR-52C

Run# E Run# F Run# G Average

SR SS SR SS SR SS SR SS

0.20 34.2 0.21 19.7 0.20 19.2 0.20 24.37

2.65 74.7 2.63 35.7 2.65 35.2 2.64 48.52

5.08 117.4 5.10 52.1 5.09 51.8 5.09 73.73

7.52 169.8 7.52 66.5 7.59 65.2 7.54 100.50

10.00 192.7 10.00 80.4 10.00 79.8 10.00 117.67

12.41 218.6 12.41 94.1 12.41 93.5 12.41 135.38

14.90 236.3 14.90 107.5 14.90 106.4 14.90 150.06

17.31 256.1 17.31 120.6 17.31 119.8 17.31 165.51

19.79 274.0 19.79 132.9 19.79 133.4 19.79 180.06

22.21 290.5 22.28 145.1 22.21 147.8 22.23 194.48

24.69 301.4 24.69 157.3 24.69 155.2 24.69 204.65

27.10 313.8 27.10 170.1 27.10 164.5 27.10 216.11

29.59 331.3 29.59 180.1 29.59 179.1 29.59 230.14

32.00 354.9 32.00 186.6 32.07 190.0 32.02 243.80

34.48 371.0 34.48 187.8 34.48 207.7 34.48 255.50

34.48 403.4 34.48 211.7 34.48 205.9 34.48 273.67

32.69 390.0 32.69 201.1 32.69 195.7 32.69 262.25

30.83 360.5 30.90 189.4 30.83 183.6 30.85 244.51

29.03 339.9 29.03 171.3 29.03 181.2 29.03 230.83

27.24 320.5 27.24 165.2 27.24 168.8 27.24 218.16

25.45 297.3 25.45 156.3 25.45 158.7 25.45 204.11

23.66 276.1 23.66 148.3 23.66 145.7 23.66 190.03

21.86 259.2 21.86 139.3 21.86 138.9 21.86 179.14

20.00 235.4 20.07 126.3 20.07 130.8 20.05 164.16

18.21 219.6 18.28 118.0 18.21 120.9 18.23 152.80

16.41 207.7 16.41 112.1 16.41 110.8 16.41 143.56

14.62 186.0 14.62 100.5 14.62 101.3 14.62 129.27

12.83 166.1 12.83 89.8 12.83 93.0 12.83 116.29

11.03 145.7 11.03 80.3 11.03 81.4 11.03 102.49

9.24 127.5 9.24 70.4 9.24 71.9 9.24 89.95

7.45 105.9 7.45 59.1 7.45 61.2 7.45 75.42

5.59 87.1 5.60 49.7 5.61 50.3 5.60 62.38

3.81 66.0 3.81 38.9 3.81 39.4 3.81 48.07

1.99 41.4 2.01 26.1 2.02 26.2 2.01 31.23

0.20 20.0 0.21 15.0 0.20 14.9 0.20 16.65

Average Stdev

YS 22.4 17.3 19.2 19.6 2.6

VS 11.0 5.5 5.5 7.3 3.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 924 154 131 403 451
D - 61

Set E7: CS-BX5 – BL36- L2– 7 day – NIST code (folder SR 55-SR-52D)

SR-52D

Run# I Run# J Run# K Average

SR SS SR SS SR SS SR SS

0.19 39.1 0.21 16.7 0.20 22.9 0.20 26.22

2.64 113.2 2.65 33.4 2.65 56.2 2.65 67.61

5.10 182.7 5.08 49.2 5.10 82.8 5.10 104.93

7.52 243.4 7.59 63.0 7.52 108.6 7.54 138.35

10.00 280.6 10.00 77.8 10.00 126.9 10.00 161.76

12.41 307.1 12.41 90.5 12.41 147.3 12.41 181.61

14.90 328.6 14.90 103.0 14.90 167.9 14.90 199.81

17.31 361.6 17.31 116.5 17.31 185.0 17.31 221.02

19.79 382.0 19.79 129.5 19.79 201.3 19.79 237.61

22.28 437.3 22.21 145.4 22.28 215.8 22.25 266.20

24.69 410.6 24.69 150.1 24.69 234.5 24.69 265.03

27.10 430.1 27.10 160.9 27.10 248.7 27.10 279.92

29.59 476.7 29.59 174.3 29.59 257.6 29.59 302.87

31.93 475.8 32.00 185.3 32.00 268.3 31.98 309.81

34.48 561.1 34.48 207.1 34.48 274.8 34.48 347.67

34.41 551.3 34.48 198.8 34.48 313.4 34.46 354.50

32.62 443.4 32.69 178.1 32.69 296.7 32.67 306.06

30.90 478.4 30.90 175.8 30.90 273.3 30.90 309.18

29.10 452.1 29.03 177.0 29.03 249.5 29.06 292.86

27.24 423.6 27.24 159.9 27.24 243.6 27.24 275.69

25.52 409.3 25.45 155.5 25.45 226.3 25.47 263.71

23.66 403.0 23.66 145.1 23.66 215.1 23.66 254.38

21.86 357.4 21.86 131.3 21.86 199.8 21.86 229.51

20.07 332.8 20.07 129.7 20.07 181.7 20.07 214.77

18.21 301.5 18.21 118.0 18.28 171.2 18.23 196.90

16.41 263.9 16.41 101.4 16.41 158.5 16.41 174.60

14.62 251.1 14.62 95.7 14.62 142.3 14.62 163.01

12.83 211.8 12.83 87.6 12.83 127.0 12.83 142.13

11.03 200.0 11.03 77.6 11.03 114.5 11.03 130.72

9.24 166.7 9.24 67.8 9.24 98.9 9.24 111.11

7.45 143.9 7.45 58.4 7.45 82.9 7.45 95.07

5.61 112.2 5.61 46.4 5.61 67.6 5.61 75.40

3.81 81.1 3.81 35.2 3.82 51.5 3.81 55.92

2.01 51.9 2.01 23.6 2.01 32.8 2.01 36.13

0.20 20.2 0.19 12.6 0.20 16.1 0.20 16.30

Average Stdev

YS 31.0 17.1 19.0 22.3 7.6

VS 14.5 5.3 8.3 9.4 4.7

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1997 200 457 884 972
D - 62

Set F1: CS-BX1 – BL33- L1 – Mixing Day – NIST code (folder SR 57-SR-56A)

SR-56A

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.24 21.0 0.20 21.5 0.21 20.3 0.22 20.93

2.63 49.4 2.65 37.6 2.64 36.4 2.64 41.12

5.10 69.7 5.10 53.3 5.08 52.9 5.09 58.61

7.52 88.3 7.52 67.0 7.52 66.7 7.52 73.98

10.00 105.0 10.00 81.0 10.00 80.4 10.00 88.82

12.41 122.4 12.41 94.8 12.41 93.9 12.41 103.70

14.90 137.4 14.90 108.5 14.90 106.7 14.90 117.54

17.31 152.9 17.31 122.6 17.38 120.1 17.33 131.85

19.79 168.5 19.79 135.2 19.79 132.5 19.79 145.41

22.21 180.2 22.21 145.7 22.21 146.6 22.21 157.51

24.69 196.6 24.69 160.2 24.69 154.1 24.69 170.32

27.17 212.5 27.10 171.9 27.10 167.8 27.13 184.05

29.59 222.5 29.59 181.9 29.59 180.7 29.59 195.04

32.00 236.3 32.00 193.8 32.00 188.0 32.00 206.04

34.48 246.2 34.48 204.8 34.48 206.4 34.48 219.10

34.48 258.2 34.48 209.4 34.48 205.0 34.48 224.20

32.69 248.3 32.69 203.0 32.69 192.8 32.69 214.68

30.83 235.1 30.90 188.5 30.90 183.8 30.87 202.51

29.03 221.8 29.03 178.1 29.03 176.8 29.03 192.20

27.24 209.9 27.24 171.5 27.24 167.9 27.24 183.11

25.45 198.0 25.45 162.0 25.45 156.2 25.45 172.06

23.66 186.1 23.66 152.5 23.66 150.1 23.66 162.90

21.86 174.3 21.86 143.0 21.86 139.1 21.86 152.12

20.07 162.4 20.07 133.5 20.07 131.1 20.07 142.30

18.28 151.5 18.28 123.4 18.28 121.7 18.28 132.21

16.41 138.4 16.41 115.8 16.41 110.4 16.41 121.50

14.62 125.7 14.62 105.3 14.62 101.9 14.62 110.99

12.83 116.0 12.83 95.7 12.83 91.5 12.83 101.06

11.03 102.1 11.03 85.1 11.03 82.9 11.03 90.04

9.24 89.4 9.24 75.0 9.24 72.2 9.24 78.87

7.38 76.3 7.38 64.0 7.45 62.0 7.40 67.43

5.61 62.9 5.60 53.1 5.61 50.9 5.61 55.64

3.82 49.1 3.83 41.8 3.80 39.7 3.82 43.52

2.02 33.0 2.00 28.5 2.01 27.5 2.01 29.64

0.21 18.3 0.20 16.4 0.21 15.7 0.21 16.82

Average Stdev

YS 23.4 21.7 20.5 21.9 1.5

VS 6.9 5.5 5.4 5.9 0.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 177 56 105 113 61
D - 63

Set F1: CS-BX1 – BL6- L2 – Mixing Day – NIST code (folder SR 57-SR-56B)

SR-56B

Run# D Run# E Run# G Average

SR SS SR SS SR SS SR SS

0.19 22.9 0.21 28.7 0.20 26.1 0.20 25.89

2.65 37.7 2.65 54.1 2.65 47.5 2.65 46.44

5.09 53.0 5.10 81.9 5.10 71.3 5.09 68.73

7.52 66.2 7.52 106.0 7.52 91.8 7.52 87.99

10.00 79.4 10.00 123.4 10.00 107.7 10.00 103.52

12.41 93.0 12.41 143.9 12.41 125.2 12.41 120.72

14.90 106.3 14.90 162.5 14.90 140.9 14.90 136.57

17.31 119.6 17.31 179.4 17.31 157.6 17.31 152.21

19.79 132.3 19.79 198.4 19.79 172.1 19.79 167.59

22.21 144.2 22.21 213.8 22.21 185.0 22.21 180.99

24.69 154.6 24.69 227.5 24.69 201.8 24.69 194.63

27.10 166.5 27.10 242.9 27.10 214.3 27.10 207.91

29.59 176.7 29.59 256.2 29.59 225.4 29.59 219.45

32.00 187.3 32.00 269.1 32.00 239.9 32.00 232.10

34.48 200.4 34.48 290.6 34.48 249.7 34.48 246.89

34.48 204.1 34.48 297.3 34.48 266.7 34.48 256.04

32.69 191.9 32.69 279.1 32.69 253.8 32.69 241.58

30.90 183.0 30.83 263.6 30.90 239.5 30.87 228.70

29.03 175.9 29.03 254.1 29.03 221.6 29.03 217.18

27.24 164.6 27.24 239.7 27.24 212.0 27.24 205.44

25.45 156.4 25.45 229.0 25.45 198.6 25.45 194.70

23.66 148.9 23.66 213.3 23.66 188.2 23.66 183.47

21.86 137.5 21.86 195.7 21.86 176.8 21.86 170.01

20.07 128.7 20.00 187.1 20.07 162.6 20.05 159.47

18.21 120.8 18.28 172.9 18.21 152.4 18.23 148.67

16.41 112.3 16.41 155.3 16.41 139.7 16.41 135.76

14.62 103.1 14.62 144.2 14.62 127.9 14.62 125.06

12.83 92.0 12.83 128.5 12.83 115.1 12.83 111.85

11.03 83.4 11.03 115.7 11.03 103.2 11.03 100.80

9.24 73.0 9.24 101.3 9.24 90.3 9.24 88.21

7.45 63.3 7.45 86.6 7.45 77.6 7.45 75.81

5.61 52.6 5.59 70.6 5.61 63.5 5.60 62.25

3.80 41.0 3.81 54.3 3.81 49.4 3.80 48.23

2.01 29.0 1.99 36.7 1.99 33.8 2.00 33.15

0.20 17.6 0.20 20.3 0.20 19.3 0.20 19.08

Average Stdev

YS 22.3 25.6 23.1 23.7 1.7

VS 5.3 7.9 7.0 6.7 1.3

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 78 356 230 222 139
D - 64

Set F1: CS-BX1 – BL33- L2 – Mixing Day – NIST code (folder SR 57-SR-56C)

SR-56C

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.19 25.9 0.20 23.4 0.20 27.4 0.20 25.56

2.65 47.9 2.64 43.7 2.64 55.9 2.64 49.18

5.10 69.5 5.10 64.0 5.08 82.5 5.09 71.99

7.52 89.2 7.52 81.2 7.52 106.6 7.52 92.34

10.00 106.2 10.00 96.5 10.00 124.0 10.00 108.87

12.41 124.0 12.41 112.9 12.41 142.4 12.41 126.46

14.90 141.0 14.90 127.5 14.90 160.3 14.90 142.95

17.31 156.7 17.31 142.1 17.38 177.5 17.33 158.80

19.79 171.2 19.79 156.2 19.79 193.7 19.79 173.70

22.21 184.1 22.21 171.9 22.21 207.3 22.21 187.74

24.69 202.3 24.69 183.2 24.69 226.7 24.69 204.06

27.10 216.1 27.10 196.3 27.10 241.6 27.10 217.98

29.59 225.4 29.59 208.9 29.59 252.2 29.59 228.84

32.00 236.2 32.00 220.6 32.00 264.1 32.00 240.31

34.48 239.6 34.48 238.0 34.48 268.6 34.48 248.73

34.48 265.8 34.48 236.5 34.48 292.9 34.48 265.07

32.69 254.5 32.69 222.2 32.62 284.3 32.67 253.66

30.83 237.5 30.83 213.7 30.90 268.5 30.85 239.90

29.03 219.2 29.10 207.9 29.03 245.9 29.06 224.36

27.24 211.1 27.24 195.2 27.24 235.2 27.24 213.82

25.45 197.7 25.45 185.4 25.45 222.9 25.45 202.01

23.66 187.3 23.66 171.3 23.66 210.0 23.66 189.52

21.86 177.1 21.86 161.3 21.86 195.6 21.86 177.99

20.00 160.6 20.00 153.5 20.07 180.1 20.02 164.70

18.21 149.0 18.28 141.4 18.21 168.7 18.23 153.04

16.41 140.0 16.41 126.2 16.41 156.4 16.41 140.87

14.62 128.1 14.62 117.7 14.62 143.5 14.62 129.78

12.83 114.2 12.83 107.7 12.83 126.7 12.83 116.21

11.03 102.1 11.03 95.4 11.03 113.6 11.03 103.73

9.24 89.6 9.24 83.8 9.24 99.1 9.24 90.84

7.45 76.3 7.45 72.0 7.45 84.8 7.45 77.68

5.61 63.1 5.61 58.9 5.61 70.2 5.61 64.05

3.81 49.3 3.81 45.9 3.80 53.9 3.81 49.72

2.00 33.4 1.99 31.5 2.01 36.5 2.00 33.81

0.19 18.9 0.21 18.2 0.21 20.1 0.20 19.08

Average Stdev

YS 22.5 23.6 24.5 23.5 1.0

VS 7.0 6.3 7.8 7.0 0.8

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 219 199 329 249 70
D - 65

Set F1: CS-BX1 – BL6- L1 – Mixing Day – NIST code (folder SR 57-SR-56D)

SR-56D

Run# k Run# L Run# M Average

SR SS SR SS SR SS SR SS

0.19 27.1 0.19 26.1 0.20 25.4 0.20 26.18

2.64 50.9 2.64 49.3 2.64 45.6 2.64 48.63

5.08 75.1 5.10 73.6 5.10 68.8 5.09 72.51

7.52 96.9 7.52 94.3 7.52 89.0 7.52 93.41

10.00 113.9 10.00 110.8 10.00 104.7 10.00 109.82

12.41 131.1 12.41 128.5 12.41 120.6 12.41 126.73

14.90 147.8 14.90 145.5 14.90 136.6 14.90 143.29

17.38 163.8 17.31 160.3 17.31 151.1 17.33 158.39

19.79 179.9 19.79 174.5 19.79 165.4 19.79 173.25

22.21 194.8 22.21 188.8 22.21 178.4 22.21 187.33

24.69 211.5 24.69 202.4 24.69 193.5 24.69 202.47

27.10 225.4 27.17 218.5 27.17 208.1 27.15 217.31

29.59 239.1 29.59 229.9 29.59 219.9 29.59 229.61

32.00 247.8 32.00 240.5 32.00 230.0 32.00 239.42

34.48 254.4 34.48 252.4 34.48 233.4 34.48 246.72

34.48 272.3 34.48 262.6 34.48 253.8 34.48 262.91

32.62 261.8 32.69 252.7 32.69 247.9 32.67 254.12

30.90 248.5 30.83 242.2 30.90 232.1 30.87 240.94

29.03 229.6 29.03 227.6 29.03 213.1 29.03 223.44

27.24 220.0 27.24 213.5 27.24 203.3 27.24 212.26

25.45 208.9 25.45 203.8 25.45 193.6 25.45 202.11

23.66 199.3 23.66 190.6 23.66 181.7 23.66 190.53

21.86 186.7 21.86 176.9 21.86 167.9 21.86 177.15

20.07 169.4 20.07 165.0 20.07 155.5 20.07 163.31

18.21 157.7 18.28 154.1 18.28 145.8 18.25 152.56

16.41 146.6 16.41 142.5 16.41 138.3 16.41 142.46

14.62 134.8 14.62 128.6 14.62 124.3 14.62 129.23

12.83 119.0 12.83 117.3 12.83 110.5 12.83 115.59

11.03 108.0 11.03 104.6 11.03 99.0 11.03 103.85

9.24 94.2 9.24 92.0 9.24 86.7 9.24 90.97

7.45 81.0 7.45 78.0 7.38 73.7 7.43 77.57

5.61 66.6 5.61 64.2 5.61 61.4 5.61 64.08

3.81 51.2 3.82 50.1 3.81 48.1 3.81 49.79

2.01 35.3 2.01 33.5 2.01 32.0 2.01 33.60

0.20 19.8 0.20 18.7 0.19 18.3 0.20 18.96

Average Stdev

YS 24.9 23.8 22.1 23.6 1.4

VS 7.2 7.0 6.8 7.0 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 267 269 217 251 30
D - 66

Set F3: CS-BX1 – BL33- L1 – 3 day – NIST code (folder SR 58-SR-56A)

SR-56A

Run# E Run# F Run# G Average

SR SS SR SS SR SS SR SS

0.20 22.6 0.20 24.1 0.20 17.2 0.20 21.32

2.63 45.6 2.65 51.5 2.65 32.5 2.64 43.21

5.10 71.0 5.08 78.2 5.10 48.2 5.09 65.78

7.52 91.9 7.59 102.0 7.59 61.8 7.56 85.25

10.00 105.8 10.00 122.3 10.00 75.5 10.00 101.17

12.41 123.2 12.41 141.3 12.41 88.2 12.41 117.53

14.90 140.3 14.90 160.7 14.90 101.6 14.90 134.17

17.31 154.7 17.31 177.8 17.38 115.4 17.33 149.31

19.79 171.4 19.79 195.5 19.79 127.2 19.79 164.68

22.21 185.6 22.21 214.7 22.21 137.4 22.21 179.22

24.69 199.1 24.69 229.6 24.69 149.2 24.69 192.64

27.17 210.7 27.10 246.2 27.10 161.2 27.13 206.04

29.59 224.3 29.59 260.7 29.59 173.0 29.59 219.35

32.00 241.7 32.00 271.1 32.00 183.1 32.00 231.99

34.48 258.1 34.48 287.3 34.48 190.9 34.48 245.41

34.48 264.9 34.48 303.0 34.48 193.0 34.48 253.63

32.69 242.3 32.62 284.8 32.69 187.7 32.67 238.27

30.83 233.3 30.90 271.8 30.90 180.0 30.87 228.36

29.03 225.8 29.03 252.6 29.03 168.0 29.03 215.48

27.24 214.1 27.24 239.6 27.24 160.5 27.24 204.74

25.45 198.6 25.45 229.6 25.45 150.8 25.45 193.02

23.66 190.3 23.66 217.5 23.66 142.6 23.66 183.49

21.86 177.6 21.86 199.9 21.86 134.4 21.86 170.62

20.07 162.4 20.07 186.3 20.00 123.2 20.05 157.28

18.28 151.5 18.21 172.3 18.21 115.7 18.23 146.49

16.41 139.8 16.41 157.3 16.41 107.9 16.41 135.01

14.62 127.3 14.62 144.4 14.62 97.8 14.62 123.13

12.83 113.1 12.83 127.6 12.83 88.3 12.83 109.65

11.03 102.0 11.03 116.4 11.03 78.3 11.03 98.93

9.24 88.8 9.24 99.8 9.24 68.8 9.24 85.79

7.45 75.3 7.45 84.6 7.45 58.4 7.45 72.79

5.60 61.7 5.61 68.9 5.61 48.0 5.61 59.53

3.81 47.3 3.79 52.2 3.80 37.2 3.80 45.55

2.01 31.2 2.01 34.3 2.01 24.8 2.01 30.09

0.20 16.3 0.20 17.1 0.19 13.4 0.20 15.63

Average Stdev

YS 21.6 22.3 18.6 20.8 2.0

VS 7.0 8.1 5.2 6.8 1.5

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 246 303 71 206 121
D - 67

Set F3: CS-BX1 – BL6- L2 – 3 day – NIST code (folder SR 58-SR-56B)

SR-56B

Run# A Run# C Run# D Average

SR SS SR SS SR SS SR SS

0.26 17.5 0.20 22.8 0.20 21.5 0.22 20.60

2.65 45.9 2.64 46.8 2.63 42.9 2.64 45.22

5.10 65.5 5.10 67.8 5.09 64.5 5.10 65.93

7.52 87.3 7.52 88.7 7.52 84.0 7.52 86.67

10.00 101.5 10.00 105.1 10.00 99.9 10.00 102.14

12.41 118.6 12.41 121.3 12.41 116.5 12.41 118.80

14.90 135.8 14.90 138.5 14.90 132.1 14.90 135.47

17.31 149.3 17.31 152.9 17.31 146.6 17.31 149.61

19.79 163.6 19.79 169.6 19.79 160.9 19.79 164.71

22.21 176.6 22.21 182.5 22.21 174.0 22.21 177.71

24.69 190.8 24.69 197.5 24.69 189.5 24.69 192.62

27.10 203.6 27.17 213.4 27.10 203.6 27.13 206.89

29.59 214.9 29.59 225.1 29.59 214.2 29.59 218.07

32.00 226.2 32.00 238.3 32.07 227.4 32.02 230.62

34.48 234.9 34.48 242.9 34.48 235.2 34.48 237.66

34.48 256.1 34.48 265.8 34.48 243.6 34.48 255.16

32.69 239.0 32.69 255.7 32.69 237.8 32.69 244.19

30.83 224.8 30.90 237.4 30.83 224.5 30.85 228.88

29.03 211.2 29.03 220.9 29.03 215.0 29.03 215.71

27.24 200.7 27.24 209.9 27.24 199.2 27.24 203.26

25.45 190.9 25.45 198.0 25.45 187.8 25.45 192.26

23.66 179.0 23.66 186.1 23.66 177.8 23.66 180.99

21.86 167.1 21.86 174.3 21.86 167.2 21.86 169.55

20.07 152.8 20.07 162.4 20.07 158.1 20.07 157.76

18.21 143.9 18.28 149.8 18.21 145.0 18.23 146.25

16.41 132.6 16.41 139.5 16.41 130.8 16.41 134.29

14.62 119.6 14.62 128.1 14.62 121.0 14.62 122.92

12.83 107.5 12.83 114.9 12.83 109.9 12.83 110.76

11.03 96.7 11.03 101.9 11.03 97.6 11.03 98.72

9.24 83.8 9.24 89.3 9.24 85.3 9.24 86.13

7.45 71.9 7.38 75.5 7.45 72.8 7.43 73.37

5.61 58.5 5.61 62.8 5.61 56.5 5.61 59.27

3.81 44.8 3.83 48.7 3.05 45.3 3.56 46.28

1.99 29.9 2.01 31.9 2.01 30.4 2.01 30.72

0.20 16.1 0.19 17.2 0.20 16.2 0.20 16.50

Average Stdev

YS 19.5 21.6 22.1 21.0 1.4

VS 6.7 7.0 6.6 6.8 0.2

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 237 173 175 195 37
D - 68

Set F3: CS-BX1 – BL33- L2 – 3 day – NIST code (folder SR 58-SR-56C)

SR-56C

Run# K Run# L Run# M Average

SR SS SR SS SR SS SR SS

0.21 23.3 0.20 27.9 0.20 18.9 0.20 23.38

2.65 48.7 2.64 65.1 2.65 34.3 2.65 49.36

5.10 70.5 5.10 100.2 5.10 49.4 5.10 73.35

7.52 89.3 7.52 133.9 7.52 62.6 7.52 95.25

10.00 107.4 10.00 149.5 10.00 76.4 10.00 111.09

12.41 124.5 12.41 169.7 12.41 89.4 12.41 127.85

14.90 140.8 14.90 187.4 14.90 101.4 14.90 143.20

17.31 156.9 17.31 204.3 17.38 114.1 17.33 158.44

19.79 168.3 19.79 224.4 19.79 127.2 19.79 173.31

22.28 184.3 22.21 242.3 22.21 137.4 22.23 187.99

24.69 199.0 24.69 257.2 24.69 149.2 24.69 201.81

27.10 214.0 27.10 272.3 27.10 159.6 27.10 215.33

29.59 226.5 29.59 288.8 29.59 170.2 29.59 228.49

32.00 233.4 32.00 303.7 32.00 180.4 32.00 239.19

34.48 233.7 34.48 315.7 34.48 184.9 34.48 244.76

34.48 264.9 34.48 345.8 34.48 196.2 34.48 268.96

32.69 254.9 32.69 325.1 32.62 191.4 32.67 257.11

30.90 236.5 30.90 304.5 30.90 180.4 30.90 240.45

29.03 217.6 29.03 285.4 29.03 162.9 29.03 221.96

27.24 212.6 27.24 268.9 27.24 156.6 27.24 212.69

25.45 197.9 25.45 253.4 25.45 149.0 25.45 200.12

23.66 185.5 23.66 240.1 23.66 143.0 23.66 189.54

21.86 174.1 21.86 223.3 21.86 132.0 21.86 176.48

20.07 158.8 20.07 208.0 20.07 119.8 20.07 162.22

18.28 147.6 18.28 190.3 18.21 112.4 18.25 150.11

16.41 140.1 16.41 175.1 16.41 106.9 16.41 140.73

14.62 126.1 14.62 160.3 14.62 95.9 14.62 127.44

12.83 114.2 12.83 143.7 12.83 86.0 12.83 114.63

11.03 100.4 11.03 127.0 11.03 77.2 11.03 101.54

9.24 88.1 9.24 110.2 9.24 67.5 9.24 88.58

7.45 74.1 7.38 94.0 7.45 57.1 7.43 75.07

5.61 61.4 5.61 76.8 5.61 47.7 5.61 61.96

3.82 47.8 3.81 58.7 3.79 37.5 3.81 47.98

2.01 31.4 2.01 38.3 2.02 25.2 2.01 31.62

0.20 17.1 0.19 19.9 0.20 14.6 0.20 17.21

Average Stdev

YS 20.5 23.3 17.5 20.4 2.9

VS 7.0 9.2 5.2 7.1 2.0

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 236 534 99 290 222
D - 69

Set F3: CS-BX1 – BL6- L1 – 3 day – NIST code (folder SR 58-SR-56D)

SR-56D

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 25.9 0.19 25.0 0.20 19.0 0.20 23.28

2.65 56.4 2.66 52.9 2.63 35.0 2.64 48.10

5.10 85.7 5.09 74.0 5.10 53.0 5.10 70.89

7.52 111.6 7.52 94.5 7.52 67.3 7.52 91.13

10.00 129.6 10.00 112.4 10.00 79.8 10.00 107.28

12.41 149.3 12.41 131.1 12.41 93.4 12.41 124.59

14.90 167.9 14.90 147.7 14.90 107.7 14.90 141.09

17.31 183.8 17.38 164.1 17.31 120.9 17.33 156.25

19.79 200.4 19.79 178.4 19.79 133.2 19.79 170.66

22.21 215.9 22.28 195.0 22.21 145.1 22.23 185.33

24.69 231.0 24.69 209.6 24.69 156.8 24.69 199.14

27.10 245.0 27.10 224.5 27.10 170.1 27.10 213.17

29.59 260.3 29.59 238.2 29.59 180.1 29.59 226.21

32.00 272.2 32.00 248.8 32.00 192.1 32.00 237.67

34.48 279.8 34.48 258.6 34.48 203.0 34.48 247.14

34.48 307.6 34.48 273.2 34.48 206.8 34.48 262.49

32.69 289.3 32.62 268.3 32.69 197.4 32.67 251.70

30.90 271.3 30.90 252.4 30.90 187.1 30.90 236.90

29.03 254.6 29.03 226.2 29.03 177.6 29.03 219.50

27.24 242.7 27.24 220.3 27.24 168.8 27.24 210.58

25.45 230.5 25.45 210.0 25.45 159.3 25.45 199.93

23.66 216.3 23.66 198.4 23.66 149.8 23.66 188.15

21.86 202.0 21.86 183.8 21.86 140.3 21.86 175.37

20.07 186.9 20.07 167.9 20.07 132.0 20.07 162.27

18.21 172.7 18.21 157.7 18.21 121.2 18.21 150.56

16.41 159.1 16.41 148.1 16.41 111.2 16.41 139.46

14.62 146.2 14.62 135.0 14.62 101.9 14.62 127.68

12.83 130.6 12.83 119.1 12.83 92.5 12.83 114.04

11.03 116.9 11.03 106.9 11.03 82.3 11.03 102.05

9.24 101.7 9.24 93.0 9.24 72.3 9.24 88.99

7.45 86.2 7.45 78.9 7.45 61.7 7.45 75.57

5.61 69.9 5.61 65.2 5.61 50.5 5.61 61.87

3.81 53.4 3.81 50.0 3.82 39.5 3.81 47.65

1.99 35.1 2.01 33.2 2.01 26.7 2.01 31.66

0.21 18.5 0.20 17.7 0.21 15.4 0.20 17.21

Average Stdev

YS 23.3 22.6 19.4 21.8 2.1

VS 8.1 7.4 5.5 7.0 1.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 387 260 93 247 148
D - 70

Set F7: CS-BX1 – BL33- L1 – 7 day – NIST code (folder SR 59-SR-56A)

SR-56A

Run# H Run# I Run# J Average

SR SS SR SS SR SS SR SS

0.20 33.4 0.20 16.6 0.20 21.5 0.20 23.82

2.64 86.0 2.64 31.3 2.65 48.5 2.64 55.25

5.10 140.9 5.09 45.6 5.09 70.9 5.09 85.81

7.52 191.1 7.59 58.0 7.59 93.5 7.56 114.20

10.00 220.2 10.00 70.3 10.00 113.2 10.00 134.55

12.41 249.5 12.41 82.5 12.41 130.2 12.41 154.09

14.90 277.6 14.90 94.3 14.90 147.1 14.90 173.01

17.31 307.9 17.38 106.4 17.31 164.1 17.33 192.82

19.79 328.5 19.79 118.3 19.79 179.5 19.79 208.79

22.21 366.5 22.21 126.7 22.21 195.0 22.21 229.40

24.69 372.6 24.69 138.7 24.69 210.3 24.69 240.52

27.10 393.5 27.10 150.8 27.10 225.6 27.10 256.61

29.59 422.2 29.59 159.2 29.59 237.9 29.59 273.11

32.00 424.1 32.07 168.5 32.00 249.9 32.02 280.83

34.48 453.5 34.48 176.1 34.48 254.4 34.48 294.68

34.48 495.1 34.48 182.3 34.48 278.8 34.48 318.73

32.62 490.9 32.69 177.1 32.62 267.2 32.64 311.72

30.90 455.9 30.90 169.3 30.90 250.0 30.90 291.71

29.03 386.6 29.03 154.8 29.03 233.7 29.03 258.38

27.24 385.9 27.24 148.6 27.24 221.6 27.24 252.02

25.45 359.4 25.45 138.8 25.45 208.5 25.45 235.57

23.66 342.7 23.66 131.9 23.66 195.4 23.66 223.33

21.86 321.0 21.86 126.1 21.86 182.3 21.86 209.78

20.07 276.6 20.07 112.8 20.07 168.5 20.07 185.95

18.21 261.8 18.21 104.7 18.21 155.5 18.21 174.03

16.41 259.2 16.41 99.0 16.41 144.5 16.41 167.56

14.62 227.0 14.62 89.5 14.62 130.1 14.62 148.89

12.83 198.3 12.83 79.7 12.83 116.4 12.83 131.47

11.03 176.5 11.03 71.4 11.03 103.5 11.03 117.09

9.24 151.5 9.24 62.1 9.24 90.2 9.24 101.26

7.38 126.2 7.45 52.5 7.45 75.7 7.43 84.80

5.60 103.8 5.60 43.7 5.61 62.1 5.60 69.86

3.82 77.2 3.79 33.7 3.79 47.5 3.80 52.80

2.01 47.0 2.02 22.6 2.01 30.8 2.01 33.50

0.20 19.5 0.20 12.7 0.21 15.6 0.20 15.94

Average Stdev

YS 22.6 15.4 18.4 18.8 3.6

VS 13.6 4.9 7.5 8.7 4.4

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 1008 86 290 461 484
D - 71

Set F7: CS-BX1 – BL6- L2 – 7 day – NIST code (folder SR 59-SR-56B)

SR-56B

Run# D Run# E Run# G Average

SR SS SR SS SR SS SR SS

0.19 22.9 0.21 18.3 0.20 23.1 0.20 21.42

2.65 46.8 2.65 34.1 2.64 49.5 2.65 43.48

5.10 68.8 5.10 49.7 5.10 77.4 5.10 65.31

7.52 88.1 7.52 62.9 7.52 103.8 7.52 84.92

10.00 105.6 10.00 75.5 10.00 118.6 10.00 99.89

12.41 123.1 12.41 88.6 12.41 134.9 12.41 115.55

14.90 139.1 14.90 100.7 14.90 150.7 14.90 130.15

17.38 153.8 17.38 112.6 17.31 166.5 17.36 144.28

19.79 171.0 19.79 127.4 19.79 181.8 19.79 160.06

22.21 183.4 22.21 138.9 22.21 198.6 22.21 173.64

24.69 197.1 24.69 149.2 24.69 208.4 24.69 184.89

27.17 213.2 27.10 159.6 27.10 220.1 27.13 197.63

29.59 224.6 29.59 169.8 29.59 234.1 29.59 209.46

32.00 233.3 32.07 184.0 32.00 242.7 32.02 220.00

34.48 242.0 34.48 196.3 34.48 261.9 34.48 233.37

34.48 262.3 34.48 198.8 34.48 277.9 34.48 246.31

32.69 249.3 32.69 185.7 32.69 263.6 32.69 232.88

30.90 235.1 30.83 175.0 30.90 245.4 30.87 218.50

29.03 217.1 29.03 175.0 29.03 225.1 29.03 205.75

27.24 207.5 27.24 160.2 27.24 218.0 27.24 195.23

25.45 194.2 25.45 151.4 25.45 203.3 25.45 182.94

23.66 183.8 23.66 140.3 23.66 195.1 23.66 173.07

21.86 172.4 21.86 131.6 21.86 183.0 21.86 162.31

20.07 158.8 20.07 125.5 20.07 162.3 20.07 148.85

18.28 146.3 18.28 115.8 18.21 151.9 18.25 137.98

16.41 136.0 16.41 105.6 16.41 143.6 16.41 128.39

14.62 124.6 14.62 96.7 14.62 129.2 14.62 116.84

12.83 110.3 12.83 88.3 12.83 115.3 12.83 104.62

11.03 98.9 11.03 77.8 11.03 102.5 11.03 93.08

9.24 86.0 9.24 68.3 9.24 88.9 9.24 81.05

7.45 72.7 7.45 58.1 7.38 74.9 7.43 68.58

5.60 60.0 5.61 47.9 5.60 61.8 5.60 56.56

3.83 46.2 3.79 37.2 3.81 47.4 3.81 43.60

2.01 30.4 2.01 25.0 2.01 30.9 2.01 28.76

0.20 16.4 0.20 14.1 0.20 16.4 0.20 15.64

Average Stdev

YS 19.3 18.0 18.8 18.7 0.7

VS 7.0 5.2 7.4 6.5 1.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 280 83 429 264 174
D - 72

Set F7: CS-BX1 – BL33- L2 – 7 day – NIST code (folder SR 59-SR-56C)

SR-56C

Run# K Run# L Run# M Average

SR SS SR SS SR SS SR SS

0.20 18.3 0.20 18.3 0.21 18.5 0.20 18.39

2.65 33.5 2.65 33.9 2.65 35.3 2.65 34.22

5.10 49.4 5.09 50.1 5.09 51.8 5.09 50.43

7.52 62.6 7.52 63.8 7.52 66.3 7.52 64.25

10.00 75.1 10.00 77.5 10.00 80.3 10.00 77.63

12.41 88.3 12.41 91.7 12.41 93.5 12.41 91.16

14.90 100.9 14.90 105.2 14.90 106.8 14.90 104.27

17.31 113.1 17.38 118.3 17.38 121.5 17.36 117.62

19.79 127.0 19.79 132.1 19.79 133.6 19.79 130.91

22.21 138.9 22.21 142.2 22.21 145.1 22.21 142.06

24.69 147.9 24.69 155.3 24.69 155.5 24.69 152.88

27.10 158.5 27.10 165.6 27.10 168.9 27.10 164.35

29.59 170.5 29.59 177.0 29.59 180.4 29.59 175.95

32.00 181.1 32.07 189.4 32.00 189.1 32.02 186.52

34.48 194.2 34.48 201.6 34.48 202.1 34.48 199.30

34.48 197.9 34.48 203.2 34.48 205.0 34.48 202.03

32.69 184.8 32.69 191.0 32.69 195.6 32.69 190.49

30.83 176.7 30.90 182.1 30.90 185.3 30.87 181.36

29.03 170.3 29.03 177.5 29.03 175.9 29.03 174.55

27.24 158.4 27.24 165.0 27.24 167.0 27.24 163.46

25.45 150.2 25.45 154.7 25.45 157.5 25.45 154.14

23.66 140.6 23.66 147.1 23.66 148.0 23.66 145.25

21.86 131.8 21.86 137.6 21.86 138.5 21.86 135.99

20.00 124.6 20.07 129.3 20.07 130.2 20.05 128.05

18.28 115.1 18.21 118.3 18.21 118.8 18.23 117.39

16.41 104.8 16.41 107.8 16.41 109.6 16.41 107.40

14.62 95.8 14.62 99.2 14.62 100.5 14.62 98.49

12.83 87.0 12.83 90.2 12.83 90.3 12.83 89.15

11.03 77.1 11.03 80.2 11.03 80.9 11.03 79.41

9.24 67.7 9.24 70.3 9.24 70.8 9.24 69.60

7.45 57.6 7.45 59.8 7.45 60.2 7.45 59.22

5.60 47.2 5.61 49.3 5.61 49.6 5.61 48.68

3.81 36.9 3.81 38.2 3.81 38.5 3.81 37.85

2.01 24.8 2.01 25.9 2.02 26.1 2.01 25.60

0.20 14.3 0.21 14.6 0.21 14.8 0.20 14.57

Average Stdev

YS 17.7 18.5 18.4 18.2 0.5

VS 5.2 5.4 5.5 5.4 0.1

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 92 101 128 107 19
D - 73

Set F7: CS-BX1 – BL6- L1 – 7 day – NIST code (folder SR 59-SR-56D)

SR-56D

Run# A Run# B Run# C Average

SR SS SR SS SR SS SR SS

0.28 14.1 0.20 44.7 0.19 16.7 0.22 25.18

2.63 34.2 2.66 131.9 2.65 31.3 2.65 65.78

5.10 49.1 5.10 209.5 5.10 46.2 5.10 101.60

7.52 62.9 7.59 299.0 7.52 58.7 7.54 140.18

10.00 76.2 10.00 326.6 10.00 71.2 10.00 158.02

12.41 89.7 12.41 378.7 12.41 83.2 12.41 183.86

14.90 103.0 14.90 420.3 14.90 95.2 14.90 206.14

17.31 115.7 17.31 457.7 17.31 107.2 17.31 226.86

19.79 127.7 19.79 484.5 19.79 118.3 19.79 243.49

22.21 138.3 22.21 507.7 22.21 132.7 22.21 259.55

24.69 150.1 24.69 549.3 24.69 140.3 24.69 279.91

27.10 160.5 27.10 587.7 27.10 149.6 27.10 299.27

29.59 171.1 29.59 599.4 29.59 163.3 29.59 311.27

32.00 184.9 32.00 612.5 32.00 174.0 32.00 323.81

34.48 195.9 34.48 626.4 34.48 187.1 34.48 336.48

34.48 199.7 34.48 731.5 34.48 190.8 34.48 374.00

32.69 189.4 32.62 709.6 32.69 181.4 32.67 360.14

30.83 177.3 30.90 655.7 30.90 168.4 30.87 333.82

29.03 172.4 29.10 572.4 29.03 155.3 29.06 300.03

27.24 161.4 27.24 560.8 27.24 151.2 27.24 291.13

25.45 151.1 25.45 523.9 25.45 143.7 25.45 272.89

23.66 143.6 23.66 498.6 23.66 135.5 23.66 259.22

21.86 132.1 21.86 462.8 21.86 125.9 21.86 240.26

20.07 125.7 20.07 412.0 20.07 114.9 20.07 217.55

18.28 115.5 18.21 384.4 18.21 108.0 18.23 202.64

16.41 104.7 16.41 364.3 16.41 101.6 16.41 190.19

14.62 96.6 14.62 325.6 14.62 91.5 14.62 171.23

12.83 86.8 12.83 284.4 12.83 81.8 12.83 151.02

11.03 77.4 11.03 255.8 11.03 73.4 11.03 135.54

9.24 67.8 9.24 218.8 9.24 64.4 9.24 117.02

7.45 57.8 7.45 184.6 7.45 54.2 7.45 98.85

5.61 47.1 5.59 147.5 5.61 44.8 5.60 79.81

3.82 36.6 3.81 108.5 3.82 34.8 3.82 59.97

2.01 24.6 2.01 66.7 2.01 23.4 2.01 38.25

0.20 13.7 0.21 25.3 0.19 13.0 0.20 17.32

Average Stdev

YS 16.9 28.9 16.0 20.6 7.2

VS 5.3 19.9 5.0 10.1 8.5

R2 1.0 1.0 1.0 1.0 0.0

Hysteresis 98 1615 80 598 881