Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility 

Pearl Harbor, Oahu, Hawaii 

Latitude: 21o

22’15” N 

Longitude: 157o

53’33” W 

HDOH Facility ID No. 9-102271 

HDOH Release ID No. 99051, 010011, 020028 

October 2008 

Prepared by: 

TEC Inc. 

1001 Bishop St. Suite 1400 

American Savings Bank Tower 

Honolulu, Hawaii 96813 

Prepared for: 

Commander 

Navy Region Hawaii 

Environmental Department, Code N45 

850 Ticonderoga Street, Suite 110 

Pearl Harbor, Hawaii 96860-5101 

Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

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Table of Contents 

Table of Contents ............................................................................................................................. i

Executive Summary ......................................................................................................................... 1

1.0 Introduction.......................................................................................................................... 4

1.1 Project Objective .............................................................................................................. 4

1.2 Previous Reports .............................................................................................................. 4

1.3 Background ...................................................................................................................... 5

1.3.1 Site Description ......................................................................................................... 5

1.3.2 Facility Information .................................................................................................. 5

1.3.3 UST Information ....................................................................................................... 5

1.4 Previous Environmental Investigations ............................................................................ 5

1.5 Regulatory Updates .......................................................................................................... 7

2.0 Sample Collection and Analyses .......................................................................................... 8

2.1 Monitoring Well Purging ................................................................................................. 8

2.2 Groundwater Sample Collection ...................................................................................... 8

2.3 Groundwater Sample Analyses ........................................................................................ 8

3.0 Groundwater Sample Analytical Results ............................................................................. 9

3.1 July 2008 Sample Analytical Results ............................................................................... 9

3.2 Groundwater Contaminant Trend ................................................................................... 11

3.3 Results of Oil-Water Interface Measurements ............................................................... 11

3.4 Groundwater Status ........................................................................................................ 12

4.0 Summary and Conclusions ................................................................................................. 15

5.0 References .......................................................................................................................... 18

List of Tables 

Table 1 Analytical Results for Quarterly Groundwater Sampling Release Response Report ..10 

Table 2 Oil-Water Interface Measurements ..............................................................................12 

Table 3 Action Levels for Compounds of Concern ..................................................................13 

Table 4 Responses to Groundwater Monitoring Results ..........................................................13 

 

List of Figures 

Figure 1 TPH Trends in Groundwater, Round 12 (July 29, 2008) .............................................16 

Figure 2 PAH Trends in Groundwater, Round 12 (July 29, 2008) ............................................17 

List of Appendices 

Appendix A – Laboratory Analytical Reports 

Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

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Executive Summary 

This Quarterly Groundwater Monitoring Report presents the results of groundwater sampling 

conducted on July 29, 2008 at the United States (US) Navy Bulk Fuel Storage Facility at Red 

Hill, Oahu, Hawaii (the Facility). The sampling and reporting was conducted by TEC Inc. (TEC) 

for the Air Force Center for Engineering and the Environment (AFCEE) and the Fleet Industrial 

Supply Center (FISC) at Pearl Harbor, Hawaii. This report is part of a series of quarterly 

groundwater monitoring reports provided by the US Navy to the State of Hawaii Department of 

Health (HDOH) in accordance with HDOH’s release response requirements. Currently, there are 

18 active and 2 inactive, 12.5 million gallon, field-constructed underground storage tanks (USTs) 

located at the Facility. 

Background 

In 2002, the United States (US) Navy installed a groundwater monitoring well (currently named 

RHMW01) into the basal aquifer, directly down-gradient from the Facility, within the lower 

access tunnel. Groundwater samples from this well indicated that petroleum from the Facility 

had migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly 

monitoring of the aquifer to protect their down-gradient drinking water resource associated with 

the US Navy Well 2254-01. The US Navy Well 2254-01 is located approximately 3,000 feet 

downgradient from the Red Hill Fuel Storage Facility and provides approximately 24 % of the 

potable water to the Pearl Harbor Water System (PHWS). 

By September 2005, the US Navy had installed two more groundwater monitoring wells 

(RHMW02 and RHMW03) within the Facility lower access tunnel, a background groundwater 

monitoring well (RHMW04) up-gradient from the Facility at ground surface adjacent to the US 

Navy Firing Range, and a groundwater monitoring well within the US Navy Well 2254-01 

infiltration gallery (RHMW2254-01). 

All five wells were sampled twice as part of a comprehensive environmental investigation and 

risk assessment (TEC, 2006). For this investigation, groundwater samples were analyzed for 

petroleum constituents and compared against HDOH Drinking Water Environmental Action 

Levels (EALs) (HDOH, 2005a). In addition, a three-dimensional (3-D) groundwater model was 

developed to produce site-specific risk-based action levels (SSRBLs) for compounds of concern. 

The results of this modeling effort indicated that Jet Propulsion (JP)–5 fuel presented the biggest 

risk to the US Navy water supply, due to its mobility and toxicity. Finally, the model indicated 

that a non-aqueous plume (free product) of JP-5 must migrate to within 1,100 feet of the US 

Navy Well 2254-01 infiltration gallery for HDOH EALs to be exceeded within the gallery. 

Based on this, free-product must be observed at RHMW01 for EALs to be exceeded at the US 

Navy Well 2254-01. 

During the Summer of 2008, HDOH updated their EALs, which resulted in significant changes 

to the action levels associated with methylnaphthalenes (total 1- and 2-). The drinking water 

toxicity EAL for these compounds was previously 240 μg/L, assuming they were not 

carcinogens. Evidence that they are carcinogenic to humans has now been accepted by the 

United States Environmental Protection Agency (USEPA), and HDOH adopted a more rigorous 
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EAL of 0.47 μg/L, corresponding to a residential tap water scenario, and a 1 in a million cancer 

risk. This equates to lowering the previous action level by a factor of 510 (HDOH, 2008). 

Groundwater Protection Plan 

In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater 

Protection Plan (TEC, 2008), or Plan, which specified SSRBLs for each well, and actions that 

would occur for the pertinent cases, based on categories for each groundwater monitoring well 

(Categories 1 through 4). The main object of the Plan is to protect groundwater quality entering 

the US Navy Well 2254-01, which provides potable water to the PHWS. This is accomplished 

by comparing petroleum concentrations in the Facility wells (RHMW01, RHMW02, and 

RHMW03) to the SSRBLs and taking the corresponding action. A secondary but important 

objective of the Plan is to identify leaking USTs by evaluating increasing concentration trends, 

or the sudden and lasting presence of free product in one or more groundwater monitoring wells. 

In the current quarterly groundwater monitoring report, the current water quality is compared to 

these categories and actions are recommended, based on those specified in the Plan. 

Current Results 

This quarterly groundwater monitoring report presents the analytical results from samples 

collected in July 2008 and compares them to State and site-specific action levels. Concentration 

trends for chemicals that exceeded HDOH Drinking Water EALs are also provided. Four normal 

samples were collected from RHMW2254-01, RHMW01, RHMW02 and RHMW03; a duplicate 

sample was collected at RHMW02; and the laboratory conducted matrix spike/matrix spike 

duplicate (MS/MSD) analysis on the sample aliquot from RHMW2254-01. Samples were 

analyzed for Total Petroleum Hydrocarbons (TPH) quantified as diesel-range organics (DRO) 

and gasoline range organics (GRO); volatile organic compounds (VOCs); polynuclear aromatic 

hydrocarbons (PAHs); and lead. 

Laboratory analytical results indicate that TPH-DRO and PAHs were detected in the 

groundwater from beneath the Facility at concentrations that exceed HDOH Drinking Water 

EALs. TPH-DRO was detected at 327 micrograms per liter (μg/L) in RHMW01, at 4,055 μg/L 

(average of normal and duplicate sample) in RHMW02, and 199 μg/L in RHMW03. The HDOH 

Drinking Water EAL for TPH-DRO is 100 μg/L. Three PAHs were detected in the normal and 

duplicate samples associated with RHMW02 at average concentrations above the HDOH 

Drinking Water EALs: naphthalene at 136 μg/L (HDOH EAL is 6.2 μg/L), 1-methylnaphthalene 

at 99 μg/L and 2-methylnaphthalene at 36.9 μg/L (HDOH EAL for total methylnaphthalenes [1- 

and 2-] is 0.47 μg/L). 

Trend Analysis 

At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005 but less than 25 percent of the SSRBL of 4,500 μg/L. TPH-DRO 

has been decreasing in concentration over the last three rounds, since January 2008. 

At RHMW02, concentrations of TPH-DRO have been greater than the HDOH Drinking Water 

EAL since September 2005 and greater than 50 percent of the SSRBL of 4,500 μg/L over that 

same period. TPH-DRO has been increasing in concentration over the last three rounds, since 

January 2008, and the average concentration from the July 2008 sampling event was 
Quarterly Groundwater Monitoring Report 

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approximately 91 percent of the SSRBL (solubility limit). Three PAHs (naphthalene, 1-

methylnaphthalene, and 2-methylnaphthalene) also have exceeded the EALs since September 

2005, and have been increasing in concentration since January 2008. There are no SSRBLs set 

for these PAHs to date. 

At RHMW03, concentrations of TPH-DRO have fluctuated around the HDOH EAL since 

September 2005 and are significantly lower than at RHMW01 and RHMW02. There are no 

significant trends observed in the results at RHMW03. 

Current Groundwater Status 

Based on the monitoring event that occurred in July 2008, no free product was observed at 

RHMW01, RHMW02, or RHMW03. Results from groundwater samples indicate that 

RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is greater than the 

HDOH EAL for drinking water (100 μg/L), but less than half the SSRBL of 4,500 μg/L 

(solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires: 

1. Quarterly reports to be sent to HDOH; and 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Results from groundwater samples indicate that RHM02 is presently in Category 3 status, since 

TPH-DRO (4,470 μg/L and 3,640 μg/L [duplicate]) is greater than the HDOH EAL for drinking 

water (100 μg/L), and greater than half the SSRBL of 4,500 μg/L (solubility limit of JP-5). 

Category 3 response at RHMW02 requires: 

1. Quarterly reports to be sent to HDOH; 

2. Initiation of a leak determination program to identify if tanks are leaking; 

3. Increase monitoring frequency to once per month if concentrations are increasing; 

4. Notify HDOH within 7 days and follow with written notification within 30 days; 

5. Measure product with interface probe in wells of concern; 

6. Immediately determine if tanks are leaking. 

Conclusions and Recommendations 

There is no indication of an imminent threat to the US Navy Well 2254-01 water resources based 

on this report, since petroleum concentrations at RHMW01 remain less than half the SSRBLs. It 

is recommended that RHMW01 and RHMW02 be evaluated monthly for the presence of fuel on 

groundwater, in accordance with the Plan. It is also recommended that quarterly groundwater 

sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and lead be continued as previously 

scheduled until new data indicates a different schedule is required.

Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

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1.0 Introduction

This report presents the results of the 12th groundwater sampling and analysis event, conducted 

in July 2008 at the Red Hill Fuel Storage Facility, Oahu, Hawaii (hereafter referred to as “the 

Facility”). The Facility consists of 18 active and 2 inactive underground storage tanks (USTs) 

operated by the Fleet Industrial and Supply Center (FISC), Pearl Harbor. The groundwater 

sampling and analysis event is part of a groundwater monitoring program for the UST site in 

response to past UST releases, previous environmental investigations, and recommendations 

from the Hawaii Department of Health (HDOH). 

1.1 Project Objective 

This groundwater sampling and analysis project was performed to evaluate the presence of 

chemicals of potential concern in groundwater underlying the Facility. The project was 

conducted to ensure the Navy remains in compliance with HDOH UST release response 

requirements as described in Hawaii Administrative Rules (HAR) 11-281 Subchapter 7, Release 

Response Action. The groundwater sampling and analysis procedures generally followed the 

procedures described in Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan (TEC 

Inc [TEC], 2008) (Also referred to as “the Plan”). 

This groundwater sampling and analysis event was conducted by TEC under Air Force Center 

for Engineering and the Environment (AFCEE) Contract Number F41624-03-D-8618, Task 

Order 021. 

1.2 Previous Reports 

The following groundwater monitoring reports were previously submitted to the HDOH: 

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 

2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 

3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 

4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 

5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 

6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 

7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 

8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 

9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 

10. Groundwater Monitoring Results, January 2008 (submitted March 2008); and 

11. Groundwater Monitoring Results, April 2008 (submitted May 2008); 
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1.3 Background 

The following sections provide a description of the site and information on the Facility and USTs. 

1.3.1 Site Description 

The Facility is located in Halawa Heights on Oahu, Hawaii. Land adjacent to the north of the 

Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south 

and west of the Facility includes the Coast Guard Reservation. Moanalua Valley is located east 

of the Facility (Dawson, 2006). 

The Navy Public Works Department operates a potable water infiltration tunnel approximately 

1,550 feet hydraulically downgradient from the Facility (Dawson, 2006). The US Navy Well 

2254-01 is located approximately 3,000 feet downgradient (west) of the Facility and provides 

approximately 24 % of the potable water to the Pearl Harbor Water System, which serves 

approximately 52,200 military consumers (TEC, 2008). 

1.3.2 Facility Information 

The Facility consists of 18 active and 2 inactive USTs operated by Navy FISC Pearl Harbor. 

Each UST has a capacity of 12.5 million gallons. The Facility is located approximately 100 feet 

above the basal aquifer (Dawson, 2006). 

1.3.3 UST Information 

The USTs were constructed in the early 1940s. The tanks were constructed of steel and currently 

contain Jet Propulsion (JP)–5 fuel and F-76 (diesel marine fuel). Previously, several tanks stored 

Navy Special Fuel Oil, Navy Distillate, aviation gasoline, and motor gasoline. Each tank 

measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the 

tanks lie at depths varying between approximately 100 feet and 200 feet below the existing 

ground surface (TEC, 2006). 

1.4 Previous Environmental Investigations 

1998 to 2001: From 1998 to 2001, the Navy conducted an investigation at the Facility to assess 

potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy 

installed a one-inch diameter sentinel well RHMW01 (previously known as MW-V1D) to 

monitor for contamination of the basal aquifer underlying the Facility. The well was installed 

and completed at approximately 100 feet below grade within the underground access tunnel. At 

the time of well completion, depth to water in RHMW01 was measured at 86 feet below grade 

(Dawson, 2006). 

In February 2001, groundwater samples collected from sentinel well RHMW01 contained total 

petroleum hydrocarbons (TPH) concentrations ranging from 883 micrograms per liter (μg/L) to 

1,050 μg/L and total lead ranging from 10.4 μg/L to 15 μg/L. The maximum total lead 

concentration in the samples was equal to the primary drinking water standard of 15 μg/L for 

lead and exceeded the HDOH Tier 1 groundwater action level of 5.6 μg/L (Dawson, 2006). 
Quarterly Groundwater Monitoring Report 

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2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing 

monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 

and the Red Hill Navy Pump Station (US Navy Well 2254-01) in February, June, September, and 

December 2005. 

Samples collected in February and June 2005 were not filtered in the field prior to analysis for 

lead. Analytical results for samples collected from RHMW01 indicated concentrations of total 

lead were above the HDOH Tier 1 action level of 5.6 μg/L. The results were not considered 

appropriate for risk assessment since the sample had not been filtered. In addition, lead was not 

a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility 

construction material (TEC, 2007). 

Samples were filtered in September and December 2005, and dissolved lead concentrations were 

below the HDOH Tier 1 action level. Concentrations of all other contaminants of potential 

concern were below HDOH Tier 1 action levels. 

2005 – Site Investigation: As part of a site investigation, TEC installed three groundwater 

monitoring wells at the Facility between June and September 2005. Well RHMW02 was 

installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the 

lower access tunnel near Tanks 13 and 14. Well RHMW04 was installed hydraulically 

upgradient of the USTs to provide geochemistry for water moving through the basal aquifer 

beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of 

approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of 

approximately 300 feet below ground surface outside the tunnel. Groundwater samples were 

collected from the three newly installed wells and two existing wells (RHMW01 and US Navy 

Well 2254-01) in September 2005. 

Naphthalene and trichloroethylene were detected in samples collected from RHMW02 at 

concentrations greater than the HDOH Tier 1 action levels. Lead was detected in the sample 

collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; 

however, the sample was not filtered in the field prior to analysis. Analytical results for filtered 

samples obtained by Dawson during the same period indicated concentrations of dissolved lead 

were below the HDOH Tier 1 action level. 

2006 – Site Investigation: Dedicated sampling pumps were installed in five wells (RHMW01, 

RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater 

samples from the wells in July 2006. The groundwater samples were analyzed for petroleum 

constituents. Naphthalene was detected in samples collected from RHMW02 at concentrations 

above the HDOH Tier 1 action level. 

In September 2005, with concurrence from the HDOH, the Navy decided to use the newer 

HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk 

Assessment project. The EALs are current and provide action levels for more chemicals, and are 

much more useful for conducting screening risk assessments. Since the HDOH June 2005 Policy 

Letter stated that the two sets of action levels should not be mixed, the Tier 1 screening levels 
Quarterly Groundwater Monitoring Report 

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presented in HAR Section 11-281-78 would no longer be used to evaluate environmental impact 

at the Facility. 

2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. 

Analytical results indicated the following: 

• No chemicals were detected in groundwater from US Navy Well 2254-01 or RHMW03; 

• TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH 

Drinking Water EALs in RHMW01; and 

• TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected 

in groundwater above the HDOH Drinking Water EALs in RHMW02. 

2007 – Groundwater Sampling: Groundwater samples were collected in March, June, and 

September 2007. Analytical results indicated the following: 

• No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three 

sampling events; 

• TPH-GRO exceeded HDOH Drinking Water EALs at RHMW02 in March; 

• TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during 

all three sampling events; 

• 1-methylnaphthalene and 2-methylnaphthalene exceeded HDOH Drinking Water EAL 

for taste and odor at RHMW02 during all three sampling events; and 

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03 in June. 

2008 – Groundwater Sampling: Groundwater samples were collected in January and April 

2008. Analytical results indicated the following: 

• No chemicals were detected above HDOH Drinking Water EALs at US Navy Well 

2254-01; 

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01; 

• TPH-GRO did not exceed HDOH Drinking Water EALs at RHMW02; 

• TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02; 

• 1-methylnaphthalene and 2-methylnaphthalene exceeded HDOH Drinking Water EAL 

for taste and odor at RHMW02; and 

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03. 

1.5 Regulatory Updates 

During the Summer of 2008, HDOH updated their EALs, which resulted in significant changes 

to the action levels associated with methylnaphthalenes (total 1- and 2-). The drinking water 

toxicity EAL for these compounds was previously 240 μg/L, assuming they were not 

carcinogens. Evidence that they are carcinogenic to humans has now been accepted by the 

United States Environmental Protection Agency (USEPA), and HDOH adopted a more rigorous 

EAL of 0.47 μg/L, corresponding to a residential tap water scenario, and a 1 in a million cancer 

risk. This equates to lowering the previous action level by a factor of 510. 
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Red Hill Fuel Storage Facility October 2008 

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2.0 Sample Collection and Analyses 

Field activities relating to groundwater sample collection were conducted on July 29, 2008. 

Groundwater samples were collected from three monitoring wells located inside the Facility 

lower access tunnel and one monitoring well located at the Red Hill Navy Pump Station. 

Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility 

Groundwater Protection Plan (TEC, 2008). A total of seven samples were collected; one normal 

sample from monitoring wells US Navy Well 2254-01, RHMW01, RHMW02 and RHMW03, 

one duplicate sample from RHMW02 (Sampled as RHMWA01 and reported as RHMW02-

WG11D), and one matrix spike and matrix spike duplicate from US Navy Well 2254-01. 

2.1 Monitoring Well Purging 

The groundwater monitoring wells were purged and sampled using a dedicated pump system. 

Well purging was considered complete when no less than three successive water quality 

parameter measurements had stabilized within approximately 10 percent. Field parameters were 

measured at regular intervals during well purging and included pH, temperature, specific 

conductivity, dissolved oxygen, and turbidity. Purge water was disposed in the Facility oil/water 

separator system. 

2.2 Groundwater Sample Collection 

Each monitoring well was sampled immediately following purging. All wells were sampled 

directly from their dedicated bladder pump system. Samples were placed into sampling 

containers with appropriate preservatives (i.e., hydrochloric acid [HCl] for volatile organic 

analysis, nitric acid [HNO3] for dissolved lead). Dissolved lead samples were filtered in the field 

and placed in preserved bottles. Sample containers were labeled with the date, sample 

identification number, type of analysis, and sampler’s name. The containers were placed on ice 

in sample coolers and transported under chain-of-custody procedures to the certified laboratory 

for analysis. 

2.3 Groundwater Sample Analyses 

Groundwater samples were analyzed by SGS Environmental Service, Inc. in Anchorage, Alaska 

for TPH-DRO and TPH-GRO by EPA Method 8015B, volatile organic compounds (VOCs) by 

EPA Method 8260B, polynuclear aromatic hydrocarbons (PAHs) by EPA Method 8270C SIMS, 

and dissolved lead by EPA Method 6020. 
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3.0 Groundwater Sample Analytical Results 

This section provides a summary of analytical results for groundwater samples collected from 

three monitoring wells located in the lower access tunnel of the Facility and one monitoring well 

located at the Red Hill Navy Pump Station. Duplicate sample results from monitoring well 

RHMW02 are reported in this document as RHMW02D. A summary of groundwater analytical 

results is included in Table 1. Complete analytical laboratory reports are provided in Appendix 

A. 

3.1 July 2008 Sample Analytical Results 

All groundwater samples were analyzed for TPH-DRO, TPH-GRO, VOCs, PAHs, and dissolved 

lead. Bromomethane was detected at US Navy Well 2254-01 at 1.26F μg/L, which is below the 

HDOH Drinking Water EAL of 8.5 μg/L. Data qualifier “F” indicates the result is between the 

method detection limit (MDL) and the reporting limit (RL) and considered an estimated value. 

TPH-DRO was detected at RHMW01 at 327 μg/L, which is above the HDOH Drinking Water 

EAL of 100 μg/L. All other chemicals of potential concern were below HDOH Drinking Water 

EALs at RHMW01. 

TPH-DRO was detected at RHMW02 and duplicate sample at 4,470 and 3,640 μg/L, 

respectively (HDOH EAL is 100 μg/L). Naphthalene was analyzed by EPA Method 8270 SIM 

and EPA Method 8260B and detected by both methods at RHMW02. EPA Method 8260B 

produced the highest naphthalene concentrations, which were 320 and 309 μg/L for the normal 

and duplicate sample, respectively (HDOH EAL is 6.2 μg/L). The concentrations of 

1-methylnaphthalene and 2-methylnapthalene were above the new HDOH Drinking Water EALs 

toxicity of 0.47 μg/L. All other chemicals of potential concern were below HDOH Drinking 

Water EALs at RHMW02. 

Only three compounds were detected at RHMW03: TPH-DRO, naphthalene, and 1-

methylnaphthylene. TPH-DRO was detected at RHMW03 at 199 μg/L, (HDOH EAL is 100 

μg/L). All other chemicals of potential concern were below HDOH Drinking Water EALs at 

RHMW03. 
Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (July 29, 2008)

Red Hill Fuel Storage Facility, Pearl Harbor, Hawaii

Result Q MDL RL Result Q MDL RL Result Q MDL 

TPH (middle distillates) 208 100 327 F 80 400 4470 83.3 417 3640 80 

TPH (gasolines) 100 100 ND U 10 100 61.7 F 10 100 61.2 F 10 

METHYLNAPHTHALENE,1- 0.47 10 ND U 0.015 0.05 102 0.773 2.58 96.0 0.773 2

METHYLNAPHTHALENE,2- 0.47 10 ND U 0.015 0.05 31.5 0.773 2.58 42.2 0.773 2

METHYLNAPHTHALENE (total 1- & 2-) 0.47 10 ND 133.5 138.2 ACENAPHTHENE 365 20 ND U 0.015 0.05 0.470 F 0.155 0.515 0.45 F 0.155 0

ACENAPHTHYLENE 243 1965 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0ANTHRACENE 1825 21.7 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0

BENZO(a)ANTHRACENE 0.09 4.7 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0

Method HDOH Residential 

Drinking Water EALs1

UG/L

HDOH Drinking 

Water Ceiling 

EALs2

UG/L

Chemical

RHMW01

UG/L

SW8015B 

(Petroleum)

RHMW02

UG/L

RHMW02D

UG/L

July 29, 2008 July 29, 2008 July 29, 2008 

BENZO(a)ANTHRACENE 0.09 4.7 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0BENZO(a)PYRENE 0.2 0.81 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0BENZO(b)FLUORANTHENE 0.09 0.75 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0BENZO(g,h,i)PERYLENE 1460 0.13 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0BENZO(k)FLUORANTHENE 0.92 0.4 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0CHRYSENE 9.2 1 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0DIBENZO(a,h)ANTHTRACENE 0.01 0.515 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0FLUORANTHENE 1460 130 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0FLUORENE 243 945 0.0206 F 0.015 0.05 0.324 F 0.155 0.515 0.304 F 0.155 0INDENO(1,2,3-cd)PYRENE 0.09 0.095 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0NAPHTHALENE 6.2 21 0.114 0.031 0.1 140 3.2 10.3 132 3.2 1

PHENANTHRENE 243 408 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0PYRENE 182.5 67.5 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0TETRACHLOROETHANE, 1,1,1,2- 0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 TRICHLOROETHANE, 1,1,1- 200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 TETRACHLOROETHANE, 1,1,2,2- 0.07 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 TRICHLOROETHANE, 1,1,2- 5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 TRICHLOROBENZENE, 1,2,4- 70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 DIBROMO,1,2- CHLOROPROPANE,3- 0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 DICHLOROPROPANE, 1,2- 5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 DICHLOROBENZENE, 1,3- 183 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 

SW8270SIM 

(PAHs)

DICHLOROPROPENE, 1,3- 0.43 50000 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 DICHLOROBENZENE, 1,4- 75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 ACETONE 21783 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 BENZENE 5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 BROMODICHLOROMETHANE 0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 BROMOFORM 100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 BROMOMETHANE 8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 CARBON TETRACHLORIDE 5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 CHLOROBENZENE 100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 CHLOROETHANE 8588 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 CHLOROFORM 70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 CHLOROMETHANE 1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 DICHLOROETHYLENE, Cis 1,2- 70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 DIBROMOETHANE, 1,2- 0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 ETHYLBENZENE 700 30 ND U 0.31 1 0.580 F 0.31 1 0.560 F 0.31 HEXACHLOROBUTADIENE 0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 XYLENES 10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 METHYL ETHYL KETONE 7065 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 METHYL ISOBUTYL KETONE 1991 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 METHYLENE CHLORIDE 4.8 9100 ND U 1 5 ND U 1 5 ND U 1 NAPHTHALENE 6 2 21 ND U 0 62 2 320 6 2 20 309 6 2 

SW8260 

(VOCs)

NAPHTHALENE 6.2 21 ND U 0.62 2 320 6.2 20 309 6.2 STYRENE 100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 TETRACHLOROETHYLENE 5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 TOLUENE 1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 DICHLOROETHYLENE, Trans 1,2- 100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 TRICHLOROETHYLENE 5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 VINYL CHLORIDE 2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 

SW6020 LEAD 15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 

PAHs - Polynuclear aromatic hydrocarbons MDL - Method detection limit

VOCs - Volatile organic compounds RL - Reporting limit

UG/L - Micrograms per Liter TPH - Total petroleum hydrocarbons 

Q - Data qualifier ND - Indicates that the compound was not detected above 

U - Indicates that the compound was analyzed for but not detected at or above the stated limit

F - Indicates that the compound was identified but the concentration was above the MDL and below the RL

- Result exceeds one or both HDOH EAL's

12

Toxicity-based environmental action levels, Table D-1b, Screening For Environmental Hazards At Sites With Contaminated Soil and Groundwater, HDOH, 2008Taste, odor and solubility thresholds, Table D-1b, Screening For Environmental Hazards At Sites With Contaminated Soil and Groundwater, HDOH, 2008

200

Page 1 of 1

Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

 ____________________________________________________________________________________________ 

11 

3.2 Groundwater Contaminant Trend 

Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 

shows TPH trends in groundwater at the Facility. Figure 2 shows PAH trends in groundwater at 

the Facility. In these figures, open icons (without fill) represent the method detection limit for 

chemicals that were not detected. 

RHMW01

TPH-GRO has only been detected in April 2008 at 13.6F μg/L, which is below the HDOH 

Drinking Water EAL of 100 μg/L. In July 2008, TPH-GRO was not detected. TPH-DRO was 

detected above the HDOH Drinking Water EAL of 100 μg/L during all groundwater sampling 

events and had shown a decreasing trend until the January 2008 sampling event. Concentration 

of TPH-DRO observed during the July 2008 sampling event was lower than the concentrations 

observed in January and April 2008, but higher than the previous four rounds. 

RHMW02

TPH-GRO was detected in eight of nine sampling events since September 2005, and exceeded 

the HDOH Drinking Water EAL three times during 2006 and 2007. The maximum 

concentration detected was 148 μg/L, which is slightly above the EAL of 100 μg/L. The 

concentration of TPH-DRO was relatively stable at RHMW02 until January 2008, ranging from 

2,250 to 3,180 μg/L. However, since January 2008 it has shown an increasing trend with 

concentrations up to 4,470 μg/L, well above the HDOH Drinking Water EAL of 100 μg/L. 

PAHs at RHMW02 remain above the HDOH Drinking Water EALs, and concentrations have 

also been increasing since January 2008. 

RHMW03

TPH-GRO has never been detected. TPH-DRO had shown a decreasing trend until the January 

2008 sampling event. Concentrations of TPH-DRO observed during the July 2008 sampling 

event were lower than the concentrations observed in January 2008, but higher than the previous 

rounds. In general, concentrations of petroleum-related compounds at RHMW03 have been the 

lowest of the three wells located within the Facility. 

3.3 Results of Oil-Water Interface Measurements 

The presence and thickness of light-non aqueous phased liquids (LNAPL), otherwise known as 

free product, released from the USTs were measured during this sampling event using a 100 ft 

Heron Oil/Water Interface Meter. The static water levels were measured to a precision of ± 0.01 

ft and fuel thickness was measured to a precision of ± 0.01 ft with this equipment. 

In January 2008, fuel was measured in monitoring wells RHMW01 and RHMW02 at a thickness 

of < 0.01 ft, but has not been observed in other monitoring wells to date. 

Measurements to determine the presence and thickness of fuel were conducted at RHMW01, 

RHMW02, and RHMW03 during the current sampling round. No fuel product was observed in 

any of these wells during this event (see Table 2). 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

 ____________________________________________________________________________________________ 

12 

Table 2. Oil-Water Interface Measurements 

Date 

RHMW01 RHMW02 RHMW03 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

SWL 

(ft) 

LNAPL 

(ft) 

 January 2008 17.74 < 0.01 18.78 < 0.01 NT NT 

 April 2008 NT NT NT NT NT NT 

 July 2008 19.04 0.00 18.91 0.00 18.86 0.00 

SWL Static water level, elevation above mean sea level 

LNAPL Light Non-Aqueous Phased Liquid, fuel product on groundwater 

ft Feet 

NT Not Taken 

3.4 Groundwater Status 

Compounds of concern are defined as those petroleum-related chemicals that have been observed 

in the groundwater samples above the HDOH EALs. In accordance with the Red Hill Bulk Fuel 

Storage Facility Final Groundwater Protection Plan (TEC, 2008), the following categories may 

be applicable based on the concentration of a compound at a specific well related to site-specific 

risk-based action levels (SSRBL) and EALs (see Table 3) and groundwater concentration trends. 

Table 3. Action Levels for Compounds of Concern 

Chemical EAL (μg/L) SSRBL (μg/L) 

Petroleum Mixtures 

TPH-DRO 100 4,500 

TPH-GRO 100 4,500 

Semi-Volatile Compounds 

1-Methylnaphthalene 0.47 NA 

2-Methylnaphthalene 0.47 NA 

Naphthalene 6.22 NA 

NA – Not applicable or not determined 

SSRBLs are applicable at RHMW01, RHMW02, and RHMW03 

EALs are applicable at US Navy Well 2254-01 

Based on the monitoring event that occurred in July 2008, no free product was observed at 

RHMW01, RHMW02, or RHMW03. Results from groundwater samples indicate that 

RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is greater than the 

HDOH EAL for drinking water (100 μg/L), but less than half the SSRBL of 4,500 μg/L 

(solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires: 

1. Quarterly reports to be sent to HDOH; and 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

 ____________________________________________________________________________________________ 

13 

2. Initiation of a leak determination program to identify if tanks are leaking. 

Results from groundwater samples indicate that RHM02 is presently in Category 3 status, since 

TPH-DRO (4,470 μg/L and 3,640 μg/L [duplicate]) is greater than the HDOH EAL for drinking 

water (100 μg/L), and greater than half the SSRBL of 4,500 μg/L (solubility limit of JP-5). 

Category 3 response at RHMW02 requires: 

1. Quarterly reports to be sent to HDOH; 

2. Initiation of a leak determination program to identify if tanks are leaking; 

3. Increase monitoring frequency to once per month if concentrations are increasing; 

4. Notify HDOH within 7 days and follow with written notification within 30 days; 

5. Measure product with interface probe in wells of concern; 

6. Immediately determine if tanks are leaking. 

Table 4 describes each category and identifies response actions to be taken in accordance with 

the Plan. 

Table 4. Responses to Groundwater Monitoring Results 

Results Category RHMW02 or 

RHMW03 

RHMW01 U.S. Navy 

Pumping Well 

2254-01 

Results Category 1: Result above 

detection limit but below drinking 

water EAL and trend for all 

compounds stable or decreasing 

A A A,D,M,E,P 

Results Category 2: Trend for any 

compound increasing or drinking 

water EAL exceeded 

A, B A, B A,B,C,D,E,F,G,K, 

L,O 

Results Category 3: Result 

Between 1/10X SSRBL and 

SSRBL for benzene, or between 

1/2X SSRBL and SSRBL for TPH 

A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J,

K,L,O 

Results Category 4: Result 

Exceeding any SSRBL or 

petroleum product measured or 

observed 

A,C,D,E,F,I,J, 

K,M,N 

A,C,D,E,F,I, 

J,K,M,N,O 

A,C,D,E,F,G,I,J,K,

L,O 

Specific Responses: 

A. Send quarterly reports to HDOH 

B. Begin program to determine the source of leak 

C. Notify HDOH verbally within 1 day and follow with written notification in 30 days 

D. Notify FISC Chain of Command within 1 day 

E. Send Type 1 Report (see box below) to HDOH 

F. Send Type 2 Report (see box below) to HDOH 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

 ____________________________________________________________________________________________ 

14 

G. Increase monitoring frequency to once per month (if concentrations increasing) 

H. Notify HDOH verbally within 7 days and follow with written notification in 30 days 

I. Remove sampling pumps (see Appendix C), measure product in pertinent wells with interface probe, 

re-install pumps if product is not detected. 

J. Immediately determine leaking tank 

K. Collect samples from nearby Halawa Deep Monitoring Well (2253-03) and OWDF MW01 

 For permission to sample 2253-03, call DLNR Commission on Water Resource Management 

 (808) 587-0214, DLNR.CWRM@Hawaii.gov

L. Provide alternative water source at 2254-01 

M. Prepare for alternative water source at US Navy Well 2254-01 

N. Re-measure for product every month with reports to HDOH 

O. Install additional monitoring well downgradient 

Report Types 

HDOH Type 1 Report 

• Re-evaluate Tier 3 Risk Assessment/groundwater model results 

• Proposal to HDOH on a course of action 

HDOH Type 2 Report 

• Proposal for groundwater treatment 
Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

 ____________________________________________________________________________________________ 

15 

4.0 Summary and Conclusions 

TPH-DRO and PAHs are present in the groundwater beneath the Facility at concentrations that 

exceed HDOH Drinking Water EALs. There is no indication of an imminent threat to the US 

Navy Well 2254-01 water resources, since petroleum concentrations at RHMW01 remain less 

than half the SSRBLs. 

It is recommended that RHMW01 and RHMW02 be evaluated monthly for the presence of fuel 

on groundwater, in accordance with the Plan. It is also recommended that quarterly 

groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs, and lead be continued as 

previously scheduled until new data indicates a different schedule is required. The quarterly 

collection and analysis of groundwater samples will continue to monitor the quality of the 

groundwater located beneath the Facility. Groundwater monitoring reports will be submitted to 

the HDOH upon receipt and evaluation of laboratory analytical results. 



Quarterly Groundwater Monitoring Report 

Red Hill Fuel Storage Facility October 2008 

 ____________________________________________________________________________________________ 

18 

5.0 References 

AMEC. 2002. Red Hill Bulk Fuel Storage Facility Investigation Report, Prepared for NAVFAC 

Pacific, August 2002. 

Dawson Group, Inc. 2006. Fourth Quarter 2005 Groundwater Sampling Report, Red Hill Fuel 

Storage Facility, Hawaii. February 2006. 

Hawaii Administrative Rules, Title 11, Chapter 281, Subchapter 7. 

State of Hawaii Department of Health (HDOH). 2005. Screening for Environmental Concerns 

at Sites with Contaminated Soil and Groundwater, Volume 1: Summary Tier 1 Lookup Tables. 

Interim Final. May 2005. 

HDOH. 2008. Screening for Environmental Hazards at Sites With Contaminated Soil and 

Groundwater. Summer 2008. 

State of Hawaii Department of Health. 2005b. Use of May 2005 Environmental Action Levels 

(“EALs”) at Leaking Underground Storage Tank Sites. Memo. 15 July. 

The Environmental Company, Inc. and AMEC. 2005. Red Hill Bulk Fuel Storage Facility Work 

Plan, Pearl Harbor, Hawaii. June. 

TEC Inc. 2006. Red Hill Bulk Fuel Storage Facility, Final – Addendum Planning Documents, 

Pearl Harbor, Hawaii. May. 

TEC Inc. 2007. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, 

Hawaii. August. 

TEC Inc. 2008. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl 

Harbor, Hawaii. January. 

Appendix A 

Laboratory Analytical Reports 

SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS Environmental Services

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

9121-003 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1083866
CASE NARRATIVE Print Date: 9/9/2008

Workorder No.: 1083866

Project Name: 9121-003 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

1083866002

AK102 - The pattern is consistent with a weathered gasoline.

PS RHMWA01-WG-12

1083866003

AK102 - The pattern is consistent with a weathered gasoline.

PS RHMW02-WG-12

1083866006

AK101 - BMS recovery for GRO does not meet QC goals. The associated LCS/LCSD meet all QC goals.

BMS RHMW2254-WG-12 MS

1083866007

AK101 - BMS/BMSD recoveries do not meet RPD goals. The associated LCS/LCSD meet all QC goals.

BMSD RHMW2254-WG-12 MSD

847977

8260B - Initial calibration verification (ICV) recovery for several analytes did not meet QC goals (biased high). These 

analytes were not detected above the PQL in the associated samples.

CCV CCV for HBN 204112 [VMS/9995]

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 ww w.us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1083866

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street Ste 1400

ASB Tower

Honolulu, HI 96813

Attn: Jeff Hart

T: (808)528-1445 F:(808)528-0768

jshart@tecinc.com

Barbara Hager

Barbara.Hager@sgs.com

Project Manager

9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The laboratory certification numbers are AK971-05 (DW), UST-005 (CS) and AK00971 (Micro) for ADEC and 001992 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A,7471A,9040B,9045C, 9056, 9060, 9065, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343.

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 9/9/2008

Notes: All DRO/RRO analysese are integrated per SOP.

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M em ber of SG S G roup
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 9121-003 Red Hill BFSF

Workorder No.: 1083866

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015B (W) SW8015C

GRO (W) SW8015C

Print Date: 9/9/2008

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1083866001 RHMW03-WG-12

1083866002 RHMWA01-WG-12

1083866003 RHMW02-WG-12

1083866004 RHMW01-WG-12

1083866005 RHMW2254-WG-12

1083866006 RHMW2254-WG-12 MS

1083866007 RHMW2254-WG-12 MSD

1083866008 TB01

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518

t (907) 562.2343 f (907) 561.5301 ww w.us.sgs.com

M em ber of SG S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW03-WG-12

SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5551 MXX20608

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5551

Analytical Method: SW6020

Analysis Date/Time: 08/05/08 19:24

Prep Batch: MXX20608

Prep Method: SW3010A

Prep Date/Time: 08/04/08 16:00 Container ID:1083866001-G

Dilution Factor: 5 Analyst: MH

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t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW03-WG-12

SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 10.0 ug/L 1 VFC9090 VXX18484

4-Bromofluorobenzene <surr> 105 50-150 % 1 VFC9090 VXX18484

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9090

Analytical Method: SW8015C

Analysis Date/Time: 08/05/08 11:15

Prep Batch: VXX18484

Prep Method: SW5030B

Prep Date/Time: 08/05/08 10:00 Container ID:1083866001-A

Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW03-WG-12

SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.199 J 0.412 0.0825 mg/L 1 XFC8106 XXX19765

5a Androstane <surr> 98 50-150 % 1 XFC8106 XXX19765

Batch Information

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8106

Analytical Method: SW8015C

Analysis Date/Time: 08/11/08 16:31

Prep Batch: XXX19765

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:40 Container ID:1083866001-J

Dilution Factor: 1 Analyst: HKG

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t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW03-WG-12

SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

Toluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Styrene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromomethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Acetone ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9995 VXX18532

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

Chloroform ND 1.00 0.300 ug/L 1 VMS9995 VXX18532

Bromobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromomethane ND 3.00 0.940 ug/L 1 VMS9995 VXX18532

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW03-WG-12

SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

Methylene chloride ND 5.00 1.00 ug/L 1 VMS9995 VXX18532

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Naphthalene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

o-Xylene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromoform ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Trichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS9995 VXX18532

Toluene-d8 <surr> 100 80-120 % 1 VMS9995 VXX18532

4-Bromofluorobenzene <surr> 99.6 76-120 % 1 VMS9995 VXX18532

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS9995

Analytical Method: SW8260B

Analysis Date/Time: 08/09/08 13:16

Prep Batch: VXX18532

Prep Method: SW5030B

Prep Date/Time: 08/09/08 05:28 Container ID:1083866001-D

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW03-WG-12

SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Acenaphthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Fluorene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Phenanthrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Anthracene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Pyrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo(a)Anthracene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Chrysene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[b]Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[k]fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[a]pyrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Indeno[1,2,3-c,d] pyrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Dibenzo[a,h]anthracene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[g,h,i]perylene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Naphthalene 0.0689 J 0.104 0.0323 ug/L 1 XMS4671 XXX19761

1-Methylnaphthalene 0.0294 J 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

2-Methylnaphthalene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Terphenyl-d14 <surr> 89.9 50-135 % 1 XMS4671 XXX19761

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4671

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/26/08 14:25

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866001-H

Dilution Factor: 1 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5551 MXX20608

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5551

Analytical Method: SW6020

Analysis Date/Time: 08/05/08 19:31

Prep Batch: MXX20608

Prep Method: SW3010A

Prep Date/Time: 08/04/08 16:00 Container ID:1083866002-G

Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 61.2 J 100 10.0 ug/L 1 VFC9090 VXX18484

4-Bromofluorobenzene <surr> 142 50-150 % 1 VFC9090 VXX18484

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9090

Analytical Method: SW8015C

Analysis Date/Time: 08/05/08 11:33

Prep Batch: VXX18484

Prep Method: SW5030B

Prep Date/Time: 08/05/08 10:00 Container ID:1083866002-A

Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 3.64 0.400 0.0800 mg/L 1 XFC8106 XXX19765

5a Androstane <surr> 83.3 50-150 % 1 XFC8106 XXX19765

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8106

Analytical Method: SW8015C

Analysis Date/Time: 08/11/08 16:41

Prep Batch: XXX19765

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:40 Container ID:1083866002-J

Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.120 J 0.400 0.120 ug/L 1 VMS9995 VXX18532

Toluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Ethylbenzene 0.560 J 1.00 0.310 ug/L 1 VMS9995 VXX18532

n-Butylbenzene 9.10 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

n-Propylbenzene 12.1 1.00 0.310 ug/L 1 VMS9995 VXX18532

Styrene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromomethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Acetone ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9995 VXX18532

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

Chloroform ND 1.00 0.300 ug/L 1 VMS9995 VXX18532

Bromobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromomethane ND 3.00 0.940 ug/L 1 VMS9995 VXX18532

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

sec-Butylbenzene 8.34 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

Methylene chloride ND 5.00 1.00 ug/L 1 VMS9995 VXX18532

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Naphthalene 309 20.0 6.20 ug/L 10 VMS10000 VXX18539

o-Xylene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromoform ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

tert-Butylbenzene 1.33 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Trichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Isopropylbenzene (Cumene) 7.24 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS9995 VXX18532

Toluene-d8 <surr> 99.4 80-120 % 1 VMS9995 VXX18532

4-Bromofluorobenzene <surr> 92.1 76-120 % 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10000

Analytical Method: SW8260B

Analysis Date/Time: 08/11/08 19:33

Prep Batch: VXX18539

Prep Method: SW5030B

Prep Date/Time: 08/11/08 15:11 Container ID:1083866002-E

Dilution Factor: 10 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS9995

Analytical Method: SW8260B

Analysis Date/Time: 08/09/08 13:50

Prep Batch: VXX18532

Prep Method: SW5030B

Prep Date/Time: 08/09/08 05:28 Container ID:1083866002-D

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMWA01-WG-12

SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Acenaphthene 0.450 J 0.515 0.155 ug/L 10 XMS4677 XXX19761

Fluorene 0.304 J 0.515 0.155 ug/L 10 XMS4677 XXX19761

Phenanthrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Anthracene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Fluoranthene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Pyrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo(a)Anthracene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Chrysene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[b]Fluoranthene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[k]fluoranthene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[a]pyrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Indeno[1,2,3-c,d] pyrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Dibenzo[a,h]anthracene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[g,h,i]perylene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Naphthalene 132 10.3 3.20 ug/L 100 XMS4683 XXX19761

1-Methylnaphthalene 96.0 2.58 0.773 ug/L 50 XMS4682 XXX19761

2-Methylnaphthalene 42.2 2.58 0.773 ug/L 50 XMS4682 XXX19761

Terphenyl-d14 <surr> 78.7 50-135 % 10 XMS4677 XXX19761

Batch Information

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4677

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/29/08 02:45

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866002-H

Dilution Factor: 10 Analyst: JDH

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4682

Analytical Method: 8270D SIMS

Analysis Date/Time: 09/04/08 04:46

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866002-H

Dilution Factor: 50 Analyst: JDH

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4683

Analytical Method: 8270D SIMS

Analysis Date/Time: 09/05/08 14:22

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866002-H

Dilution Factor: 100 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5551 MXX20608

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5551

Analytical Method: SW6020

Analysis Date/Time: 08/05/08 20:06

Prep Batch: MXX20608

Prep Method: SW3010A

Prep Date/Time: 08/04/08 16:00 Container ID:1083866003-G

Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics 61.7 J 100 10.0 ug/L 1 VFC9090 VXX18484

4-Bromofluorobenzene <surr> 145 50-150 % 1 VFC9090 VXX18484

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9090

Analytical Method: SW8015C

Analysis Date/Time: 08/05/08 11:51

Prep Batch: VXX18484

Prep Method: SW5030B

Prep Date/Time: 08/05/08 10:00 Container ID:1083866003-A

Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 4.47 0.417 0.0833 mg/L 1 XFC8106 XXX19765

5a Androstane <surr> 94.2 50-150 % 1 XFC8106 XXX19765

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8106

Analytical Method: SW8015C

Analysis Date/Time: 08/11/08 16:50

Prep Batch: XXX19765

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:40 Container ID:1083866003-J

Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

Toluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Ethylbenzene 0.580 J 1.00 0.310 ug/L 1 VMS9995 VXX18532

n-Butylbenzene 9.52 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

n-Propylbenzene 12.3 1.00 0.310 ug/L 1 VMS9995 VXX18532

Styrene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromomethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Acetone ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9995 VXX18532

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

Chloroform ND 1.00 0.300 ug/L 1 VMS9995 VXX18532

Bromobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromomethane ND 3.00 0.940 ug/L 1 VMS9995 VXX18532

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

sec-Butylbenzene 8.55 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

Methylene chloride ND 5.00 1.00 ug/L 1 VMS9995 VXX18532

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Naphthalene 320 20.0 6.20 ug/L 10 VMS10000 VXX18539

o-Xylene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromoform ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

tert-Butylbenzene 1.31 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Trichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Isopropylbenzene (Cumene) 7.22 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS9995 VXX18532

Toluene-d8 <surr> 99 80-120 % 1 VMS9995 VXX18532

4-Bromofluorobenzene <surr> 90.9 76-120 % 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10000

Analytical Method: SW8260B

Analysis Date/Time: 08/11/08 20:07

Prep Batch: VXX18539

Prep Method: SW5030B

Prep Date/Time: 08/11/08 15:11 Container ID:1083866003-E

Dilution Factor: 10 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS9995

Analytical Method: SW8260B

Analysis Date/Time: 08/09/08 14:24

Prep Batch: VXX18532

Prep Method: SW5030B

Prep Date/Time: 08/09/08 05:28 Container ID:1083866003-D

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW02-WG-12

SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Acenaphthene 0.470 J 0.515 0.155 ug/L 10 XMS4677 XXX19761

Fluorene 0.324 J 0.515 0.155 ug/L 10 XMS4677 XXX19761

Phenanthrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Anthracene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Fluoranthene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Pyrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo(a)Anthracene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Chrysene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[b]Fluoranthene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[k]fluoranthene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[a]pyrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Indeno[1,2,3-c,d] pyrene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Dibenzo[a,h]anthracene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Benzo[g,h,i]perylene ND 0.515 0.155 ug/L 10 XMS4677 XXX19761

Naphthalene 140 10.3 3.20 ug/L 100 XMS4683 XXX19761

1-Methylnaphthalene 102 2.58 0.773 ug/L 50 XMS4682 XXX19761

2-Methylnaphthalene 31.5 2.58 0.773 ug/L 50 XMS4682 XXX19761

Terphenyl-d14 <surr> 80.5 50-135 % 10 XMS4677 XXX19761

Batch Information

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4677

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/29/08 03:18

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866003-H

Dilution Factor: 10 Analyst: JDH

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4682

Analytical Method: 8270D SIMS

Analysis Date/Time: 09/04/08 05:18

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866003-H

Dilution Factor: 50 Analyst: JDH

Initial Prep Wt./Vol.: 970 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4683

Analytical Method: 8270D SIMS

Analysis Date/Time: 09/05/08 14:55

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866003-H

Dilution Factor: 100 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5551 MXX20608

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5551

Analytical Method: SW6020

Analysis Date/Time: 08/05/08 20:13

Prep Batch: MXX20608

Prep Method: SW3010A

Prep Date/Time: 08/04/08 16:00 Container ID:1083866004-G

Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 10.0 ug/L 1 VFC9090 VXX18484

4-Bromofluorobenzene <surr> 109 50-150 % 1 VFC9090 VXX18484

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9090

Analytical Method: SW8015C

Analysis Date/Time: 08/05/08 12:10

Prep Batch: VXX18484

Prep Method: SW5030B

Prep Date/Time: 08/05/08 10:00 Container ID:1083866004-A

Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.327 J 0.400 0.0800 mg/L 1 XFC8106 XXX19765

5a Androstane <surr> 94.7 50-150 % 1 XFC8106 XXX19765

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8106

Analytical Method: SW8015C

Analysis Date/Time: 08/11/08 16:59

Prep Batch: XXX19765

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:40 Container ID:1083866004-J

Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

Toluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Isopropyltoluene 0.400 J 1.00 0.310 ug/L 1 VMS9995 VXX18532

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Styrene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromomethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Acetone ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9995 VXX18532

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

Chloroform ND 1.00 0.300 ug/L 1 VMS9995 VXX18532

Bromobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromomethane ND 3.00 0.940 ug/L 1 VMS9995 VXX18532

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

Methylene chloride ND 5.00 1.00 ug/L 1 VMS9995 VXX18532

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Naphthalene ND 2.00 0.620 ug/L 1 VMS10000 VXX18539

o-Xylene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromoform ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Trichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS9995 VXX18532

Toluene-d8 <surr> 100 80-120 % 1 VMS9995 VXX18532

4-Bromofluorobenzene <surr> 95.8 76-120 % 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10000

Analytical Method: SW8260B

Analysis Date/Time: 08/11/08 19:00

Prep Batch: VXX18539

Prep Method: SW5030B

Prep Date/Time: 08/11/08 15:11 Container ID:1083866004-E

Dilution Factor: 1 Analyst: DSH

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS9995

Analytical Method: SW8260B

Analysis Date/Time: 08/09/08 14:58

Prep Batch: VXX18532

Prep Method: SW5030B

Prep Date/Time: 08/09/08 05:28 Container ID:1083866004-D

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW01-WG-12

SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Acenaphthene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Fluorene 0.0206 J 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Phenanthrene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Anthracene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Pyrene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Chrysene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Naphthalene 0.114 0.100 0.0310 ug/L 1 XMS4671 XXX19761

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 1 XMS4671 XXX19761

Terphenyl-d14 <surr> 84.9 50-135 % 1 XMS4671 XXX19761

Batch Information

Initial Prep Wt./Vol.: 1000 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4671

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/26/08 16:06

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866004-H

Dilution Factor: 1 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW2254-WG-12

SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS5551 MXX20608

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS5551

Analytical Method: SW6020

Analysis Date/Time: 08/05/08 17:30

Prep Batch: MXX20608

Prep Method: SW3010A

Prep Date/Time: 08/04/08 16:00 Container ID:1083866005-G

Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW2254-WG-12

SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 10.0 ug/L 1 VFC9090 VXX18484

4-Bromofluorobenzene <surr> 109 50-150 % 1 VFC9090 VXX18484

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9090

Analytical Method: SW8015C

Analysis Date/Time: 08/05/08 12:28

Prep Batch: VXX18484

Prep Method: SW5030B

Prep Date/Time: 08/05/08 10:00 Container ID:1083866005-A

Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW2254-WG-12

SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.417 0.0833 mg/L 1 XFC8106 XXX19765

5a Androstane <surr> 94.1 50-150 % 1 XFC8106 XXX19765

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8106

Analytical Method: SW8015C

Analysis Date/Time: 08/11/08 17:09

Prep Batch: XXX19765

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:40 Container ID:1083866005-J

Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW2254-WG-12

SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

Toluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Styrene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromomethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Acetone ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9995 VXX18532

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

Chloroform ND 1.00 0.300 ug/L 1 VMS9995 VXX18532

Bromobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromomethane 1.26 J 3.00 0.940 ug/L 1 VMS9995 VXX18532

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW2254-WG-12

SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

Methylene chloride ND 5.00 1.00 ug/L 1 VMS9995 VXX18532

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Naphthalene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

o-Xylene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromoform ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Trichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS9995 VXX18532

Toluene-d8 <surr> 99.2 80-120 % 1 VMS9995 VXX18532

4-Bromofluorobenzene <surr> 100 76-120 % 1 VMS9995 VXX18532

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS9995

Analytical Method: SW8260B

Analysis Date/Time: 08/09/08 12:42

Prep Batch: VXX18532

Prep Method: SW5030B

Prep Date/Time: 08/09/08 05:28 Container ID:1083866005-D

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: RHMW2254-WG-12

SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Acenaphthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Fluorene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Phenanthrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Anthracene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Pyrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo(a)Anthracene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Chrysene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[b]Fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[k]fluoranthene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[a]pyrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Indeno[1,2,3-c,d] pyrene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Dibenzo[a,h]anthracene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Benzo[g,h,i]perylene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Naphthalene ND 0.104 0.0323 ug/L 1 XMS4671 XXX19761

1-Methylnaphthalene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

2-Methylnaphthalene ND 0.0521 0.0156 ug/L 1 XMS4671 XXX19761

Terphenyl-d14 <surr> 97 50-135 % 1 XMS4671 XXX19761

Batch Information

Initial Prep Wt./Vol.: 960 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS4671

Analytical Method: 8270D SIMS

Analysis Date/Time: 08/26/08 16:39

Prep Batch: XXX19761

Prep Method: SW3520C

Prep Date/Time: 08/05/08 09:15 Container ID:1083866005-H

Dilution Factor: 1 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: TB01

SGS Ref. #: 1083866008 Collection Date/Time: 07/29/08 08:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

Toluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Styrene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromomethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Acetone ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS9995 VXX18532

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS9995 VXX18532

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

Chloroform ND 1.00 0.300 ug/L 1 VMS9995 VXX18532

Bromobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Chloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromomethane 1.36 J 3.00 0.940 ug/L 1 VMS9995 VXX18532

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: TB01

SGS Ref. #: 1083866008 Collection Date/Time: 07/29/08 08:05

Project ID: 9121-003 Red Hill BFSF Receipt Date/Time: 07/31/08 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS9995 VXX18532

Methylene chloride ND 5.00 1.00 ug/L 1 VMS9995 VXX18532

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

Naphthalene ND 2.00 0.620 ug/L 1 VMS9995 VXX18532

o-Xylene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Bromoform ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Trichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS9995 VXX18532

1,2-Dichloroethane-D4 <surr> 102 73-120 % 1 VMS9995 VXX18532

Toluene-d8 <surr> 100 80-120 % 1 VMS9995 VXX18532

4-Bromofluorobenzene <surr> 99.5 76-120 % 1 VMS9995 VXX18532

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS9995

Analytical Method: SW8260B

Analysis Date/Time: 08/09/08 12:08

Prep Batch: VXX18532

Prep Method: SW5030B

Prep Date/Time: 08/09/08 05:28 Container ID:1083866008-A

Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907) 562.2343 f (907) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846324 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX20608

SW3010A

08/04/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 08/05/08

Instrument

Method

Batch MMS5551

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846350 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX19761

SW3520C

08/05/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 08/27/08

Acenaphthene ND 0.0500 0.0150 ug/L 08/27/08

Fluorene ND 0.0500 0.0150 ug/L 08/27/08

Phenanthrene ND 0.0500 0.0150 ug/L 08/27/08

Anthracene ND 0.0500 0.0150 ug/L 08/27/08

Fluoranthene ND 0.0500 0.0150 ug/L 08/27/08

Pyrene ND 0.0500 0.0150 ug/L 08/27/08

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 08/27/08

Chrysene ND 0.0500 0.0150 ug/L 08/27/08

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 08/27/08

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 08/27/08

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 08/27/08

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 08/27/08

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 08/27/08

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 08/27/08

Naphthalene ND 0.100 0.0310 ug/L 08/27/08

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 08/27/08

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 08/27/08

Surrogates 

Terphenyl-d14 <surr> 122 50-135 % 08/27/08

Instrument

Method

Batch XMS4673

8270D SIMS

HP 5890 Series II MS2 SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846380 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX19765

SW3520C

08/05/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics ND 0.400 0.0800 mg/L 08/11/08

Surrogates 

5a Androstane <surr> 100 60-120 % 08/11/08

Instrument

Method

Batch XFC8106

SW8015C

HP 5890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846453 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18484

SW5030B

08/05/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics ND 100 10.0 ug/L 08/05/08

Surrogates 

4-Bromofluorobenzene <surr> 99.4 50-150 % 08/05/08

Instrument

Method

Batch VFC9090

SW8015C

HP 5890 Series II PID+FID VCA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847971 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005, 1083866008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847971 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 08/09/08

Toluene ND 1.00 0.310 ug/L 08/09/08

Ethylbenzene ND 1.00 0.310 ug/L 08/09/08

n-Butylbenzene ND 1.00 0.310 ug/L 08/09/08

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 08/09/08

1,2-Dichloroethane ND 0.500 0.150 ug/L 08/09/08

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 08/09/08

4-Chlorotoluene ND 1.00 0.310 ug/L 08/09/08

Chlorobenzene ND 0.500 0.150 ug/L 08/09/08

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 08/09/08

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 08/09/08

4-Isopropyltoluene ND 1.00 0.310 ug/L 08/09/08

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 08/09/08

n-Propylbenzene ND 1.00 0.310 ug/L 08/09/08

Styrene ND 1.00 0.310 ug/L 08/09/08

Dibromomethane ND 1.00 0.310 ug/L 08/09/08

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 08/09/08

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 08/09/08

Acetone ND 10.0 3.10 ug/L 08/09/08

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/09/08

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 08/09/08

Methyl-t-butyl ether ND 5.00 1.50 ug/L 08/09/08

Tetrachloroethene ND 1.00 0.310 ug/L 08/09/08

Dibromochloromethane ND 0.500 0.150 ug/L 08/09/08

1,3-Dichloropropane ND 0.400 0.120 ug/L 08/09/08

1,2-Dibromoethane ND 1.00 0.310 ug/L 08/09/08

Carbon tetrachloride ND 1.00 0.310 ug/L 08/09/08

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 08/09/08

Chloroform ND 1.00 0.300 ug/L 08/09/08

Bromobenzene ND 1.00 0.310 ug/L 08/09/08

Chloromethane ND 1.00 0.310 ug/L 08/09/08

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 08/09/08

Bromomethane ND 3.00 0.940 ug/L 08/09/08

Bromochloromethane ND 1.00 0.310 ug/L 08/09/08

Vinyl chloride ND 1.00 0.310 ug/L 08/09/08

Dichlorodifluoromethane ND 1.00 0.310 ug/L 08/09/08

Chloroethane ND 1.00 0.310 ug/L 08/09/08

sec-Butylbenzene ND 1.00 0.310 ug/L 08/09/08

Bromodichloromethane ND 0.500 0.150 ug/L 08/09/08
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847971 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene ND 1.00 0.310 ug/L 08/09/08

2-Butanone (MEK) ND 10.0 3.10 ug/L 08/09/08

Methylene chloride ND 5.00 1.00 ug/L 08/09/08

Trichlorofluoromethane ND 1.00 0.310 ug/L 08/09/08

P & M -Xylene ND 2.00 0.620 ug/L 08/09/08

Naphthalene ND 2.00 0.620 ug/L 08/09/08

o-Xylene ND 1.00 0.310 ug/L 08/09/08

Bromoform ND 1.00 0.310 ug/L 08/09/08

1-Chlorohexane ND 1.00 0.310 ug/L 08/09/08

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 08/09/08

tert-Butylbenzene ND 1.00 0.310 ug/L 08/09/08

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 08/09/08

1,1-Dichloroethane ND 1.00 0.310 ug/L 08/09/08

2-Chlorotoluene ND 1.00 0.310 ug/L 08/09/08

Trichloroethene ND 1.00 0.310 ug/L 08/09/08

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 08/09/08

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 08/09/08

2,2-Dichloropropane ND 1.00 0.310 ug/L 08/09/08

Hexachlorobutadiene ND 1.00 0.310 ug/L 08/09/08

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 08/09/08

1,2-Dichloropropane ND 1.00 0.310 ug/L 08/09/08

1,1-Dichloropropene ND 1.00 0.310 ug/L 08/09/08

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 08/09/08

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 08/09/08

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 08/09/08

Surrogates 

1,2-Dichloroethane-D4 <surr> 102 73-120 % 08/09/08

Toluene-d8 <surr> 101 80-120 % 08/09/08

4-Bromofluorobenzene <surr> 97.4 76-120 % 08/09/08

Instrument

Method

Batch VMS9995

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

848185 Method Blank

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18539

SW5030B

08/11/2008

QC results affect the following production samples:

1083866002, 1083866003, 1083866004

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Naphthalene ND 2.00 0.620 ug/L 08/11/08

Surrogates 

1,2-Dichloroethane-D4 <surr> 108 73-120 % 08/11/08

Toluene-d8 <surr> 102 80-120 % 08/11/08

Instrument

Method

Batch VMS10000

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846325 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX20608

SW3010A

08/04/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1080 108 ( 80-120 ) 1000 ug/L 08/05/2008

Batch

Method

Instrument

MMS5551

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846351 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX19761

SW3520C

08/05/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846351 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX19761

SW3520C

08/05/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.315 63 ( 50-105 ) 0.5 ug/L 08/26/2008

Acenaphthene LCS 0.317 63 ( 45-110 ) 0.5 ug/L 08/26/2008

Fluorene LCS 0.324 65 ( 50-110 ) 0.5 ug/L 08/26/2008

Phenanthrene LCS 0.334 67 ( 50-115 ) 0.5 ug/L 08/26/2008

Anthracene LCS 0.327 66 ( 55-110 ) 0.5 ug/L 08/26/2008

Fluoranthene LCS 0.378 76 ( 55-125 ) 0.5 ug/L 08/26/2008

Pyrene LCS 0.365 73 ( 50-130 ) 0.5 ug/L 08/26/2008

Benzo(a)Anthracene LCS 0.399 80 ( 55-120 ) 0.5 ug/L 08/26/2008

Chrysene LCS 0.368 74 ( 55-120 ) 0.5 ug/L 08/26/2008

Benzo[b]Fluoranthene LCS 0.380 76 ( 46-130 ) 0.5 ug/L 08/26/2008

Benzo[k]fluoranthene LCS 0.381 76 ( 60-125 ) 0.5 ug/L 08/26/2008

Benzo[a]pyrene LCS 0.423 85 ( 55-120 ) 0.5 ug/L 08/26/2008

Indeno[1,2,3-c,d] pyrene LCS 0.393 79 ( 45-125 ) 0.5 ug/L 08/26/2008

Dibenzo[a,h]anthracene LCS 0.405 81 ( 41-140 ) 0.5 ug/L 08/26/2008

Benzo[g,h,i]perylene LCS 0.391 78 ( 46-125 ) 0.5 ug/L 08/26/2008

Naphthalene LCS 0.344 69 ( 42-100 ) 0.5 ug/L 08/26/2008

1-Methylnaphthalene LCS 0.328 66 ( 46-115 ) 0.5 ug/L 08/26/2008

2-Methylnaphthalene LCS 0.311 62 ( 45-105 ) 0.5 ug/L 08/26/2008

Surrogates 

Terphenyl-d14 <surr> LCS 120 ( 50-135 ) 08/26/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846351 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX19761

SW3520C

08/05/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4671

8270D SIMS

HP 5890 Series II MS2 SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846381 Lab Control Sample

846382 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX19765

SW3520C

08/05/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.61 92 ( 75-125 ) 5 mg/L 08/11/2008

LCSD 4.97 99 8 (< 20 ) 5 mg/L 08/11/2008

Surrogates 

5a Androstane <surr> LCS 106 ( 60-120 ) 08/11/2008

LCSD 117 9 08/11/2008

Batch

Method

Instrument

XFC8106

SW8015C

HP 5890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

846454 Lab Control Sample

846455 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18484

SW5030B

08/05/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 191 95 ( 79-108 ) 200 ug/L 08/05/2008

LCSD 192 96 1 (< 20 ) 200 ug/L 08/05/2008

Surrogates 

4-Bromofluorobenzene <surr> LCS 109 ( 50-150 ) 08/05/2008

LCSD 110 1 08/05/2008

Batch

Method

Instrument

VFC9090

SW8015C

HP 5890 Series II PID+FID VCA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847972 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005, 1083866008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847972 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 28.4 95 ( 80-120 ) 30 ug/L 08/09/2008

Toluene LCS 29.2 97 ( 77-120 ) 30 ug/L 08/09/2008

Ethylbenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 08/09/2008

n-Butylbenzene LCS 27.6 92 ( 80-124 ) 30 ug/L 08/09/2008

1,4-Dichlorobenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 08/09/2008

1,2-Dichloroethane LCS 31.9 106 ( 80-129 ) 30 ug/L 08/09/2008

1,3,5-Trimethylbenzene LCS 29.1 97 ( 80-128 ) 30 ug/L 08/09/2008

4-Chlorotoluene LCS 28.3 94 ( 79-128 ) 30 ug/L 08/09/2008

Chlorobenzene LCS 31.7 106 ( 80-120 ) 30 ug/L 08/09/2008

4-Methyl-2-pentanone (MIBK) LCS 91.0 101 ( 69-134 ) 90 ug/L 08/09/2008

cis-1,2-Dichloroethene LCS 30.2 101 ( 80-125 ) 30 ug/L 08/09/2008

4-Isopropyltoluene LCS 29.1 97 ( 80-125 ) 30 ug/L 08/09/2008

cis-1,3-Dichloropropene LCS 25.6 85 ( 80-120 ) 30 ug/L 08/09/2008

n-Propylbenzene LCS 29.9 100 ( 80-129 ) 30 ug/L 08/09/2008

Styrene LCS 31.8 106 ( 80-120 ) 30 ug/L 08/09/2008

Dibromomethane LCS 31.6 105 ( 80-120 ) 30 ug/L 08/09/2008

trans-1,3-Dichloropropene LCS 27.4 91 ( 80-124 ) 30 ug/L 08/09/2008

1,2,4-Trichlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 08/09/2008

Acetone LCS 81.6 91 ( 50-135 ) 90 ug/L 08/09/2008

1,1,2,2-Tetrachloroethane LCS 29.8 99 ( 76-123 ) 30 ug/L 08/09/2008

1,2-Dibromo-3-chloropropane LCS 26.9 90 ( 73-130 ) 30 ug/L 08/09/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847972 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methyl-t-butyl ether LCS 40.9 91 ( 80-120 ) 45 ug/L 08/09/2008

Tetrachloroethene LCS 30.6 102 ( 79-122 ) 30 ug/L 08/09/2008

Dibromochloromethane LCS 30.5 102 ( 80-120 ) 30 ug/L 08/09/2008

1,3-Dichloropropane LCS 29.2 97 ( 80-121 ) 30 ug/L 08/09/2008

1,2-Dibromoethane LCS 31.7 106 ( 80-120 ) 30 ug/L 08/09/2008

Carbon tetrachloride LCS 29.0 97 ( 80-126 ) 30 ug/L 08/09/2008

1,1,1,2-Tetrachloroethane LCS 30.4 101 ( 80-120 ) 30 ug/L 08/09/2008

Chloroform LCS 30.7 102 ( 80-124 ) 30 ug/L 08/09/2008

Bromobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 08/09/2008

Chloromethane LCS 26.4 88 ( 67-125 ) 30 ug/L 08/09/2008

1,2,3-Trichloropropane LCS 29.4 98 ( 80-120 ) 30 ug/L 08/09/2008

Bromomethane LCS 26.2 87 ( 30-140 ) 30 ug/L 08/09/2008

Bromochloromethane LCS 31.9 106 ( 77-129 ) 30 ug/L 08/09/2008

Vinyl chloride LCS 26.5 88 ( 72-145 ) 30 ug/L 08/09/2008

Dichlorodifluoromethane LCS 24.8 83 ( 62-153 ) 30 ug/L 08/09/2008

Chloroethane LCS 26.0 87 ( 67-133 ) 30 ug/L 08/09/2008

sec-Butylbenzene LCS 29.3 98 ( 80-120 ) 30 ug/L 08/09/2008

Bromodichloromethane LCS 28.9 96 ( 80-120 ) 30 ug/L 08/09/2008

1,1-Dichloroethene LCS 29.9 100 ( 76-130 ) 30 ug/L 08/09/2008

2-Butanone (MEK) LCS 87.7 97 ( 66-136 ) 90 ug/L 08/09/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847972 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 28.7 96 ( 63-131 ) 30 ug/L 08/09/2008

Trichlorofluoromethane LCS 31.6 105 ( 68-145 ) 30 ug/L 08/09/2008

P & M -Xylene LCS 61.9 103 ( 80-120 ) 60 ug/L 08/09/2008

Naphthalene LCS 30.2 101 ( 75-120 ) 30 ug/L 08/09/2008

o-Xylene LCS 31.4 105 ( 80-120 ) 30 ug/L 08/09/2008

Bromoform LCS 31.8 106 ( 80-120 ) 30 ug/L 08/09/2008

1-Chlorohexane LCS 40.8 91 ( 70-125 ) 45 ug/L 08/09/2008

1,2,4-Trimethylbenzene LCS 29.8 99 ( 80-125 ) 30 ug/L 08/09/2008

tert-Butylbenzene LCS 28.8 96 ( 80-122 ) 30 ug/L 08/09/2008

1,1,1-Trichloroethane LCS 27.8 93 ( 80-122 ) 30 ug/L 08/09/2008

1,1-Dichloroethane LCS 29.6 99 ( 80-120 ) 30 ug/L 08/09/2008

2-Chlorotoluene LCS 28.4 95 ( 80-125 ) 30 ug/L 08/09/2008

Trichloroethene LCS 30.0 100 ( 80-125 ) 30 ug/L 08/09/2008

trans-1,2-Dichloroethene LCS 28.7 96 ( 79-132 ) 30 ug/L 08/09/2008

1,2-Dichlorobenzene LCS 30.7 102 ( 80-120 ) 30 ug/L 08/09/2008

2,2-Dichloropropane LCS 27.3 91 ( 80-132 ) 30 ug/L 08/09/2008

Hexachlorobutadiene LCS 28.5 95 ( 77-125 ) 30 ug/L 08/09/2008

Isopropylbenzene (Cumene) LCS 31.3 104 ( 80-121 ) 30 ug/L 08/09/2008

1,2-Dichloropropane LCS 30.2 101 ( 80-121 ) 30 ug/L 08/09/2008

1,1-Dichloropropene LCS 28.9 96 ( 80-122 ) 30 ug/L 08/09/2008

1,1,2-Trichloroethane LCS 29.2 97 ( 77-120 ) 30 ug/L 08/09/2008
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

847972 Lab Control Sample

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18532

SW5030B

08/09/2008

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,3-Dichlorobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 08/09/2008

1,2,3-Trichlorobenzene LCS 31.8 106 ( 77-120 ) 30 ug/L 08/09/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 08/09/2008

Toluene-d8 <surr> LCS 99 ( 80-120 ) 08/09/2008

4-Bromofluorobenzene <surr> LCS 91 ( 76-120 ) 08/09/2008

Batch

Method

Instrument

VMS9995

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Prep

848186 Lab Control Sample

848187 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

9121-003 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX18539

SW5030B

08/11/2008

QC results affect the following production samples:

1083866002, 1083866003, 1083866004

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Naphthalene LCS 32.7 109 ( 75-120 ) 30 ug/L 08/11/2008

LCSD 32.9 110 1 (< 20 ) 30 ug/L 08/11/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 106 ( 73-120 ) 08/11/2008

LCSD 103 3 08/11/2008

Toluene-d8 <surr> LCS 100 ( 80-120 ) 08/11/2008

LCSD 99 0 08/11/2008

4-Bromofluorobenzene <surr> LCS 90 ( 76-120 ) 08/11/2008

LCSD 94 4 08/11/2008

Batch

Method

Instrument

VMS10000

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

846326 Matrix Spike

846327 Matrix Spike Duplicate

1083829004

Water (Surface, Eff., Ground)

MXX20608

3010 H20 Digest for Metals ICP-MS

08/04/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Metals by ICP/MS

Lead MS 128 1210 108 ( 80-120 ) 1000 ug/L 08/05/2008

MSD 1180 105 2 (< 15 ) 1000 ug/L 08/05/2008

Batch

Method

Instrument

MMS5551

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

846328 Bench Spike DIGESTED

1083829004

Water (Surface, Eff., Ground)

MXX20608

3010 H20 Digest for Metals ICP-MS

08/04/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Metals by ICP/MS

Lead BND 128 1440 105 ( 75-125 ) 1250 ug/L 08/05/2008

Batch

Method

Instrument

MMS5551

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

846397 Bench Spike DIGESTED

1083866005

Water (Surface, Eff., Ground)

MXX20608

3010 H20 Digest for Metals ICP-MS

08/04/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Metals by ICP/MS

Lead BND ND 1200 96 ( 75-125 ) 1250 ug/L 08/05/2008

Batch

Method

Instrument

MMS5551

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

847974 Matrix Spike

847975 Matrix Spike Duplicate

847973

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

QC results affect the following production samples:

1083866001, 1083866002, 1083866003, 1083866004, 1083866005, 1083866008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

847974 Matrix Spike

847975 Matrix Spike Duplicate

847973

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene MS ND 31.1 104 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 28.0 93 10 (< 20 ) 30.0 ug/L 08/09/2008

Toluene MS ND 31.8 106 ( 77-120 ) 30.0 ug/L 08/09/2008

MSD 29.5 98 7 (< 20 ) 30.0 ug/L 08/09/2008

Ethylbenzene MS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 30.1 100 9 (< 20 ) 30.0 ug/L 08/09/2008

n-Butylbenzene MS ND 29.8 99 ( 80-124 ) 30.0 ug/L 08/09/2008

MSD 26.9 90 10 (< 20 ) 30.0 ug/L 08/09/2008

1,4-Dichlorobenzene MS ND 34 113 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 31.0 103 9 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dichloroethane MS ND 34.1 114 ( 80-129 ) 30.0 ug/L 08/09/2008

MSD 31.6 105 8 (< 20 ) 30.0 ug/L 08/09/2008

1,3,5-Trimethylbenzene MS ND 31.6 105 ( 80-128 ) 30.0 ug/L 08/09/2008

MSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008

4-Chlorotoluene MS ND 30.9 103 ( 79-128 ) 30.0 ug/L 08/09/2008

MSD 28.6 96 8 (< 20 ) 30.0 ug/L 08/09/2008

Chlorobenzene MS ND 33.9 113 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 31.3 104 8 (< 20 ) 30.0 ug/L 08/09/2008

4-Methyl-2-pentanone (MIBK) MS ND 100 111 ( 69-134 ) 90.0 ug/L 08/09/2008

MSD 93.7 104 7 (< 20 ) 90.0 ug/L 08/09/2008

cis-1,2-Dichloroethene MS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008

MSD 30.4 101 7 (< 20 ) 30.0 ug/L 08/09/2008

4-Isopropyltoluene MS ND 31.3 104 ( 80-125 ) 30.0 ug/L 08/09/2008

MSD 28.7 96 9 (< 20 ) 30.0 ug/L 08/09/2008

cis-1,3-Dichloropropene MS ND 28.3 94 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 26.4 88 7 (< 20 ) 30.0 ug/L 08/09/2008

n-Propylbenzene MS ND 32.2 107 ( 80-129 ) 30.0 ug/L 08/09/2008

MSD 29.7 99 8 (< 20 ) 30.0 ug/L 08/09/2008

Styrene MS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 30.6 102 8 (< 20 ) 30.0 ug/L 08/09/2008

Dibromomethane MS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 31.5 105 6 (< 20 ) 30.0 ug/L 08/09/2008

trans-1,3-Dichloropropene MS ND 30 100 ( 80-124 ) 30.0 ug/L 08/09/2008

MSD 28.7 96 5 (< 20 ) 30.0 ug/L 08/09/2008

1,2,4-Trichlorobenzene MS ND 33.4 111 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 30.1 100 10 (< 20 ) 30.0 ug/L 08/09/2008

Acetone MS ND 90.6 101 ( 50-135 ) 90.0 ug/L 08/09/2008

MSD 80.2 89 12 (< 20 ) 90.0 ug/L 08/09/2008

1,1,2,2-Tetrachloroethane MS ND 32.1 107 ( 76-123 ) 30.0 ug/L 08/09/2008

MSD 30.6 102 5 (< 20 ) 30.0 ug/L 08/09/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

847974 Matrix Spike

847975 Matrix Spike Duplicate

847973

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane MS ND 32 107 ( 73-130 ) 30.0 ug/L 08/09/2008

MSD 27.7 93 14 (< 20 ) 30.0 ug/L 08/09/2008

Methyl-t-butyl ether MS ND 44.8 99 ( 80-120 ) 45.0 ug/L 08/09/2008

MSD 41.6 93 7 (< 20 ) 45.0 ug/L 08/09/2008

Tetrachloroethene MS ND 33.3 111 ( 79-122 ) 30.0 ug/L 08/09/2008

MSD 30.7 102 8 (< 20 ) 30.0 ug/L 08/09/2008

Dibromochloromethane MS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 32.8 109 2 (< 20 ) 30.0 ug/L 08/09/2008

1,3-Dichloropropane MS ND 31.1 104 ( 80-121 ) 30.0 ug/L 08/09/2008

MSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dibromoethane MS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 29.4 98 13 (< 20 ) 30.0 ug/L 08/09/2008

Carbon tetrachloride MS ND 32.4 108 ( 80-126 ) 30.0 ug/L 08/09/2008

MSD 31.9 106 2 (< 20 ) 30.0 ug/L 08/09/2008

1,1,1,2-Tetrachloroethane MS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 31.9 106 3 (< 20 ) 30.0 ug/L 08/09/2008

Chloroform MS ND 33.8 113 ( 80-124 ) 30.0 ug/L 08/09/2008

MSD 30.5 102 10 (< 20 ) 30.0 ug/L 08/09/2008

Bromobenzene MS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 30.3 101 8 (< 20 ) 30.0 ug/L 08/09/2008

Chloromethane MS ND 30 100 ( 67-125 ) 30.0 ug/L 08/09/2008

MSD 27.4 91 9 (< 20 ) 30.0 ug/L 08/09/2008

1,2,3-Trichloropropane MS ND 30.7 102 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 29.3 98 5 (< 20 ) 30.0 ug/L 08/09/2008

Bromomethane MS 1.26 J 29.1 93 ( 30-140 ) 30.0 ug/L 08/09/2008

MSD 27.4 87 6 (< 20 ) 30.0 ug/L 08/09/2008

Bromochloromethane MS ND 34.5 115 ( 77-129 ) 30.0 ug/L 08/09/2008

MSD 32.0 107 8 (< 20 ) 30.0 ug/L 08/09/2008

Vinyl chloride MS ND 29.7 99 ( 72-145 ) 30.0 ug/L 08/09/2008

MSD 27.2 91 9 (< 20 ) 30.0 ug/L 08/09/2008

Dichlorodifluoromethane MS ND 28.4 95 ( 62-153 ) 30.0 ug/L 08/09/2008

MSD 25.3 84 12 (< 20 ) 30.0 ug/L 08/09/2008

Chloroethane MS ND 27.7 93 ( 67-133 ) 30.0 ug/L 08/09/2008

MSD 24.4 81 13 (< 20 ) 30.0 ug/L 08/09/2008

sec-Butylbenzene MS ND 30.8 103 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 28.5 95 8 (< 20 ) 30.0 ug/L 08/09/2008

Bromodichloromethane MS ND 30.9 103 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008

1,1-Dichloroethene MS ND 32.6 109 ( 76-130 ) 30.0 ug/L 08/09/2008

MSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

847974 Matrix Spike

847975 Matrix Spike Duplicate

847973

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) MS ND 97.5 108 ( 66-136 ) 90.0 ug/L 08/09/2008

MSD 89.6 100 9 (< 20 ) 90.0 ug/L 08/09/2008

Methylene chloride MS ND 31 103 ( 63-131 ) 30.0 ug/L 08/09/2008

MSD 28.5 95 9 (< 20 ) 30.0 ug/L 08/09/2008

Trichlorofluoromethane MS ND 34.1 114 ( 68-145 ) 30.0 ug/L 08/09/2008

MSD 30.2 101 12 (< 20 ) 30.0 ug/L 08/09/2008

P & M -Xylene MS ND 66.9 112 ( 80-120 ) 60.0 ug/L 08/09/2008

MSD 61.8 103 8 (< 20 ) 60.0 ug/L 08/09/2008

Naphthalene MS ND 33.4 111 ( 75-120 ) 30.0 ug/L 08/09/2008

MSD 30.7 102 9 (< 20 ) 30.0 ug/L 08/09/2008

o-Xylene MS ND 33.3 111 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 31.4 105 6 (< 20 ) 30.0 ug/L 08/09/2008

Bromoform MS ND 34.4 115 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 34.5 115 0 (< 20 ) 30.0 ug/L 08/09/2008

1-Chlorohexane MS ND 44.2 98 ( 70-125 ) 45.0 ug/L 08/09/2008

MSD 40.2 89 10 (< 20 ) 45.0 ug/L 08/09/2008

1,2,4-Trimethylbenzene MS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008

MSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008

tert-Butylbenzene MS ND 31 103 ( 80-122 ) 30.0 ug/L 08/09/2008

MSD 28.6 95 8 (< 20 ) 30.0 ug/L 08/09/2008

1,1,1-Trichloroethane MS ND 30.7 102 ( 80-122 ) 30.0 ug/L 08/09/2008

MSD 28.8 96 7 (< 20 ) 30.0 ug/L 08/09/2008

1,1-Dichloroethane MS ND 32.3 108 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 29.4 98 9 (< 20 ) 30.0 ug/L 08/09/2008

2-Chlorotoluene MS ND 30.2 101 ( 80-125 ) 30.0 ug/L 08/09/2008

MSD 28.1 94 7 (< 20 ) 30.0 ug/L 08/09/2008

Trichloroethene MS ND 32.2 107 ( 80-125 ) 30.0 ug/L 08/09/2008

MSD 29.6 99 9 (< 20 ) 30.0 ug/L 08/09/2008

trans-1,2-Dichloroethene MS ND 30.9 103 ( 79-132 ) 30.0 ug/L 08/09/2008

MSD 28.7 96 7 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dichlorobenzene MS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 30.8 103 9 (< 20 ) 30.0 ug/L 08/09/2008

2,2-Dichloropropane MS ND 29.3 98 ( 80-132 ) 30.0 ug/L 08/09/2008

MSD 27.7 92 6 (< 20 ) 30.0 ug/L 08/09/2008

Hexachlorobutadiene MS ND 31.1 104 ( 77-125 ) 30.0 ug/L 08/09/2008

MSD 27.5 92 13 (< 20 ) 30.0 ug/L 08/09/2008

Isopropylbenzene (Cumene) MS ND 34.2 114 ( 80-121 ) 30.0 ug/L 08/09/2008

MSD 31.5 105 8 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dichloropropane MS ND 32.2 107 ( 80-121 ) 30.0 ug/L 08/09/2008

MSD 29.9 100 7 (< 20 ) 30.0 ug/L 08/09/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

847974 Matrix Spike

847975 Matrix Spike Duplicate

847973

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene MS ND 31.9 106 ( 80-122 ) 30.0 ug/L 08/09/2008

MSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008

1,1,2-Trichloroethane MS ND 31.3 104 ( 77-120 ) 30.0 ug/L 08/09/2008

MSD 29.1 97 8 (< 20 ) 30.0 ug/L 08/09/2008

1,3-Dichlorobenzene MS ND 32.5 108 ( 80-120 ) 30.0 ug/L 08/09/2008

MSD 30.2 101 7 (< 20 ) 30.0 ug/L 08/09/2008

1,2,3-Trichlorobenzene MS ND 34.4 115 ( 77-120 ) 30.0 ug/L 08/09/2008

MSD 31.4 105 9 (< 20 ) 30.0 ug/L 08/09/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> MS 30.9 103 ( 73-120 ) 08/09/2008

MSD 30.4 101 1 08/09/2008

Toluene-d8 <surr> MS 29.8 99 ( 80-120 ) 08/09/2008

MSD 30.1 100 1 08/09/2008

4-Bromofluorobenzene <surr> MS 27.9 93 ( 76-120 ) 08/09/2008

MSD 27.6 92 1 08/09/2008

Batch

Method

Instrument

VMS9995

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

MXX20608

3010 H20 Digest for Metals ICP-MS

08/04/2008

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS ND 1060 106 ( 80-120 ) 1000 ug/L 08/05/2008

BMSD 1060 106 0 (< 15 ) 1000 ug/L 08/05/2008

Batch

Method

Instrument

MMS5551

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS ND 515 114* ( 79-108 ) 450 ug/L 08/05/2008

BMSD 412 92 22 * (< 20 ) 450 ug/L 08/05/2008

Surrogates 

4-Bromofluorobenzene <surr> BMS 56.2 112 ( 50-150 ) 08/05/2008

BMSD 55.6 111 1 08/05/2008

Batch

Method

Instrument

VFC9090

SW8015C

HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS ND 4.82 94 ( 75-125 ) 5.15 mg/L 08/11/2008

BMSD 4.78 91 1 (< 30 ) 5.26 mg/L 08/11/2008

Surrogates 

5a Androstane <surr> BMS .112 109 ( 50-150 ) 08/11/2008

BMSD 0.110 105 2 08/11/2008

Batch

Method

Instrument

XFC8106

SW8015C

HP 5890 Series II FID SV D R

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 28.0 93 10 (< 20 ) 30.0 ug/L 08/09/2008

Toluene BMS ND 31.8 106 ( 77-120 ) 30.0 ug/L 08/09/2008

BMSD 29.5 98 7 (< 20 ) 30.0 ug/L 08/09/2008

Ethylbenzene BMS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 30.1 100 9 (< 20 ) 30.0 ug/L 08/09/2008

n-Butylbenzene BMS ND 29.8 99 ( 80-124 ) 30.0 ug/L 08/09/2008

BMSD 26.9 90 10 (< 20 ) 30.0 ug/L 08/09/2008

1,4-Dichlorobenzene BMS ND 34 113 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 31.0 103 9 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dichloroethane BMS ND 34.1 114 ( 80-129 ) 30.0 ug/L 08/09/2008

BMSD 31.6 105 8 (< 20 ) 30.0 ug/L 08/09/2008

1,3,5-Trimethylbenzene BMS ND 31.6 105 ( 80-128 ) 30.0 ug/L 08/09/2008

BMSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008

4-Chlorotoluene BMS ND 30.9 103 ( 79-128 ) 30.0 ug/L 08/09/2008

BMSD 28.6 96 8 (< 20 ) 30.0 ug/L 08/09/2008

Chlorobenzene BMS ND 33.9 113 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 31.3 104 8 (< 20 ) 30.0 ug/L 08/09/2008

4-Methyl-2-pentanone (MIBK) BMS ND 100 111 ( 69-134 ) 90.0 ug/L 08/09/2008

BMSD 93.7 104 7 (< 20 ) 90.0 ug/L 08/09/2008

cis-1,2-Dichloroethene BMS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008

BMSD 30.4 101 7 (< 20 ) 30.0 ug/L 08/09/2008

4-Isopropyltoluene BMS ND 31.3 104 ( 80-125 ) 30.0 ug/L 08/09/2008

BMSD 28.7 96 9 (< 20 ) 30.0 ug/L 08/09/2008

cis-1,3-Dichloropropene BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 26.4 88 7 (< 20 ) 30.0 ug/L 08/09/2008

n-Propylbenzene BMS ND 32.2 107 ( 80-129 ) 30.0 ug/L 08/09/2008

BMSD 29.7 99 8 (< 20 ) 30.0 ug/L 08/09/2008

Styrene BMS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 30.6 102 8 (< 20 ) 30.0 ug/L 08/09/2008

Dibromomethane BMS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 31.5 105 6 (< 20 ) 30.0 ug/L 08/09/2008

trans-1,3-Dichloropropene BMS ND 30 100 ( 80-124 ) 30.0 ug/L 08/09/2008

BMSD 28.7 96 5 (< 20 ) 30.0 ug/L 08/09/2008

1,2,4-Trichlorobenzene BMS ND 33.4 111 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 30.1 100 10 (< 20 ) 30.0 ug/L 08/09/2008

Acetone BMS ND 90.6 101 ( 50-135 ) 90.0 ug/L 08/09/2008

BMSD 80.2 89 12 (< 20 ) 90.0 ug/L 08/09/2008

1,1,2,2-Tetrachloroethane BMS ND 32.1 107 ( 76-123 ) 30.0 ug/L 08/09/2008

BMSD 30.6 102 5 (< 20 ) 30.0 ug/L 08/09/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS ND 32 107 ( 73-130 ) 30.0 ug/L 08/09/2008

BMSD 27.7 93 14 (< 20 ) 30.0 ug/L 08/09/2008

Methyl-t-butyl ether BMS ND 44.8 99 ( 80-120 ) 45.0 ug/L 08/09/2008

BMSD 41.6 93 7 (< 20 ) 45.0 ug/L 08/09/2008

Tetrachloroethene BMS ND 33.3 111 ( 79-122 ) 30.0 ug/L 08/09/2008

BMSD 30.7 102 8 (< 20 ) 30.0 ug/L 08/09/2008

Dibromochloromethane BMS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 32.8 109 2 (< 20 ) 30.0 ug/L 08/09/2008

1,3-Dichloropropane BMS ND 31.1 104 ( 80-121 ) 30.0 ug/L 08/09/2008

BMSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dibromoethane BMS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 29.4 98 13 (< 20 ) 30.0 ug/L 08/09/2008

Carbon tetrachloride BMS ND 32.4 108 ( 80-126 ) 30.0 ug/L 08/09/2008

BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 08/09/2008

1,1,1,2-Tetrachloroethane BMS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 31.9 106 3 (< 20 ) 30.0 ug/L 08/09/2008

Chloroform BMS ND 33.8 113 ( 80-124 ) 30.0 ug/L 08/09/2008

BMSD 30.5 102 10 (< 20 ) 30.0 ug/L 08/09/2008

Bromobenzene BMS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 30.3 101 8 (< 20 ) 30.0 ug/L 08/09/2008

Chloromethane BMS ND 30 100 ( 67-125 ) 30.0 ug/L 08/09/2008

BMSD 27.4 91 9 (< 20 ) 30.0 ug/L 08/09/2008

1,2,3-Trichloropropane BMS ND 30.7 102 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 29.3 98 5 (< 20 ) 30.0 ug/L 08/09/2008

Bromomethane BMS 1.26 J 29.1 93 ( 30-140 ) 30.0 ug/L 08/09/2008

BMSD 27.4 87 6 (< 20 ) 30.0 ug/L 08/09/2008

Bromochloromethane BMS ND 34.5 115 ( 77-129 ) 30.0 ug/L 08/09/2008

BMSD 32.0 107 8 (< 20 ) 30.0 ug/L 08/09/2008

Vinyl chloride BMS ND 29.7 99 ( 72-145 ) 30.0 ug/L 08/09/2008

BMSD 27.2 91 9 (< 20 ) 30.0 ug/L 08/09/2008

Dichlorodifluoromethane BMS ND 28.4 95 ( 62-153 ) 30.0 ug/L 08/09/2008

BMSD 25.3 84 12 (< 20 ) 30.0 ug/L 08/09/2008

Chloroethane BMS ND 27.7 93 ( 67-133 ) 30.0 ug/L 08/09/2008

BMSD 24.4 81 13 (< 20 ) 30.0 ug/L 08/09/2008

sec-Butylbenzene BMS ND 30.8 103 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 28.5 95 8 (< 20 ) 30.0 ug/L 08/09/2008

Bromodichloromethane BMS ND 30.9 103 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008

1,1-Dichloroethene BMS ND 32.6 109 ( 76-130 ) 30.0 ug/L 08/09/2008

BMSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS ND 97.5 108 ( 66-136 ) 90.0 ug/L 08/09/2008

BMSD 89.6 100 9 (< 20 ) 90.0 ug/L 08/09/2008

Methylene chloride BMS ND 31 103 ( 63-131 ) 30.0 ug/L 08/09/2008

BMSD 28.5 95 9 (< 20 ) 30.0 ug/L 08/09/2008

Trichlorofluoromethane BMS ND 34.1 114 ( 68-145 ) 30.0 ug/L 08/09/2008

BMSD 30.2 101 12 (< 20 ) 30.0 ug/L 08/09/2008

P & M -Xylene BMS ND 66.9 112 ( 80-120 ) 60.0 ug/L 08/09/2008

BMSD 61.8 103 8 (< 20 ) 60.0 ug/L 08/09/2008

Naphthalene BMS ND 33.4 111 ( 75-120 ) 30.0 ug/L 08/09/2008

BMSD 30.7 102 9 (< 20 ) 30.0 ug/L 08/09/2008

o-Xylene BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 31.4 105 6 (< 20 ) 30.0 ug/L 08/09/2008

Bromoform BMS ND 34.4 115 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 34.5 115 0 (< 20 ) 30.0 ug/L 08/09/2008

1-Chlorohexane BMS ND 44.2 98 ( 70-125 ) 45.0 ug/L 08/09/2008

BMSD 40.2 89 10 (< 20 ) 45.0 ug/L 08/09/2008

1,2,4-Trimethylbenzene BMS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008

BMSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008

tert-Butylbenzene BMS ND 31 103 ( 80-122 ) 30.0 ug/L 08/09/2008

BMSD 28.6 95 8 (< 20 ) 30.0 ug/L 08/09/2008

1,1,1-Trichloroethane BMS ND 30.7 102 ( 80-122 ) 30.0 ug/L 08/09/2008

BMSD 28.8 96 7 (< 20 ) 30.0 ug/L 08/09/2008

1,1-Dichloroethane BMS ND 32.3 108 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 29.4 98 9 (< 20 ) 30.0 ug/L 08/09/2008

2-Chlorotoluene BMS ND 30.2 101 ( 80-125 ) 30.0 ug/L 08/09/2008

BMSD 28.1 94 7 (< 20 ) 30.0 ug/L 08/09/2008

Trichloroethene BMS ND 32.2 107 ( 80-125 ) 30.0 ug/L 08/09/2008

BMSD 29.6 99 9 (< 20 ) 30.0 ug/L 08/09/2008

trans-1,2-Dichloroethene BMS ND 30.9 103 ( 79-132 ) 30.0 ug/L 08/09/2008

BMSD 28.7 96 7 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dichlorobenzene BMS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 30.8 103 9 (< 20 ) 30.0 ug/L 08/09/2008

2,2-Dichloropropane BMS ND 29.3 98 ( 80-132 ) 30.0 ug/L 08/09/2008

BMSD 27.7 92 6 (< 20 ) 30.0 ug/L 08/09/2008

Hexachlorobutadiene BMS ND 31.1 104 ( 77-125 ) 30.0 ug/L 08/09/2008

BMSD 27.5 92 13 (< 20 ) 30.0 ug/L 08/09/2008

Isopropylbenzene (Cumene) BMS ND 34.2 114 ( 80-121 ) 30.0 ug/L 08/09/2008

BMSD 31.5 105 8 (< 20 ) 30.0 ug/L 08/09/2008

1,2-Dichloropropane BMS ND 32.2 107 ( 80-121 ) 30.0 ug/L 08/09/2008

BMSD 29.9 100 7 (< 20 ) 30.0 ug/L 08/09/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

VXX18532

Volatiles Extraction AFCEE 3.1 8260 (

08/09/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS ND 31.9 106 ( 80-122 ) 30.0 ug/L 08/09/2008

BMSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008

1,1,2-Trichloroethane BMS ND 31.3 104 ( 77-120 ) 30.0 ug/L 08/09/2008

BMSD 29.1 97 8 (< 20 ) 30.0 ug/L 08/09/2008

1,3-Dichlorobenzene BMS ND 32.5 108 ( 80-120 ) 30.0 ug/L 08/09/2008

BMSD 30.2 101 7 (< 20 ) 30.0 ug/L 08/09/2008

1,2,3-Trichlorobenzene BMS ND 34.4 115 ( 77-120 ) 30.0 ug/L 08/09/2008

BMSD 31.4 105 9 (< 20 ) 30.0 ug/L 08/09/2008

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 30.9 103 ( 73-120 ) 08/09/2008

BMSD 30.4 101 1 08/09/2008

Toluene-d8 <surr> BMS 29.8 99 ( 80-120 ) 08/09/2008

BMSD 30.1 100 1 08/09/2008

4-Bromofluorobenzene <surr> BMS 27.9 93 ( 76-120 ) 08/09/2008

BMSD 27.6 92 1 08/09/2008

Batch

Method

Instrument

VMS9995

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

XXX19761

3520 Liquid/Liquid Ext for 8270 SIM

08/05/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS ND .326 63 ( 50-105 ) 0.521 ug/L 08/26/2008

BMSD 0.305 59 7 (< 30 ) 0.521 ug/L 08/26/2008

Acenaphthene BMS ND .321 62 ( 45-110 ) 0.521 ug/L 08/26/2008

BMSD 0.308 59 4 (< 30 ) 0.521 ug/L 08/26/2008

Fluorene BMS ND .331 64 ( 50-110 ) 0.521 ug/L 08/26/2008

BMSD 0.306 59 8 (< 30 ) 0.521 ug/L 08/26/2008

Phenanthrene BMS ND .331 64 ( 50-115 ) 0.521 ug/L 08/26/2008

BMSD 0.302 58 9 (< 30 ) 0.521 ug/L 08/26/2008

Anthracene BMS ND .353 68 ( 55-110 ) 0.521 ug/L 08/26/2008

BMSD 0.321 62 10 (< 30 ) 0.521 ug/L 08/26/2008

Fluoranthene BMS ND .356 68 ( 55-125 ) 0.521 ug/L 08/26/2008

BMSD 0.335 64 6 (< 30 ) 0.521 ug/L 08/26/2008

Pyrene BMS ND .338 65 ( 50-130 ) 0.521 ug/L 08/26/2008

BMSD 0.320 62 6 (< 30 ) 0.521 ug/L 08/26/2008

Benzo(a)Anthracene BMS ND .409 79 ( 55-120 ) 0.521 ug/L 08/26/2008

BMSD 0.382 73 7 (< 30 ) 0.521 ug/L 08/26/2008

Chrysene BMS ND .347 67 ( 55-120 ) 0.521 ug/L 08/26/2008

BMSD 0.329 63 5 (< 30 ) 0.521 ug/L 08/26/2008

Benzo[b]Fluoranthene BMS ND .383 74 ( 46-130 ) 0.521 ug/L 08/26/2008

BMSD 0.340 65 12 (< 30 ) 0.521 ug/L 08/26/2008

Benzo[k]fluoranthene BMS ND .358 69 ( 60-125 ) 0.521 ug/L 08/26/2008

BMSD 0.326 63 9 (< 30 ) 0.521 ug/L 08/26/2008

Benzo[a]pyrene BMS ND .434 83 ( 55-120 ) 0.521 ug/L 08/26/2008

BMSD 0.385 74 12 (< 30 ) 0.521 ug/L 08/26/2008

Indeno[1,2,3-c,d] pyrene BMS ND .379 73 ( 45-125 ) 0.521 ug/L 08/26/2008

BMSD 0.328 63 14 (< 30 ) 0.521 ug/L 08/26/2008

Dibenzo[a,h]anthracene BMS ND .395 76 ( 41-140 ) 0.521 ug/L 08/26/2008

BMSD 0.338 65 15 (< 30 ) 0.521 ug/L 08/26/2008

Benzo[g,h,i]perylene BMS ND .372 71 ( 46-125 ) 0.521 ug/L 08/26/2008

BMSD 0.328 63 13 (< 30 ) 0.521 ug/L 08/26/2008

Naphthalene BMS ND .306 59 ( 42-100 ) 0.521 ug/L 08/26/2008

BMSD 0.305 59 0 (< 30 ) 0.521 ug/L 08/26/2008

1-Methylnaphthalene BMS ND .313 60 ( 46-115 ) 0.521 ug/L 08/26/2008

BMSD 0.306 59 2 (< 30 ) 0.521 ug/L 08/26/2008

2-Methylnaphthalene BMS ND .308 59 ( 45-105 ) 0.521 ug/L 08/26/2008

BMSD 0.298 57 3 (< 30 ) 0.521 ug/L 08/26/2008

Surrogates 

Terphenyl-d14 <surr> BMS .479 92 ( 50-135 ) 08/26/2008

BMSD 0.386 74 21 08/26/2008
Matrix

SGS Ref.# Printed Date/Time 09/09/2008 8:32

Batch

Method

Date

Original

Prep

1083866006 Billable Matrix Spike

1083866007 Billable Matrix Spike Dup.

1083866005

Water (Surface, Eff., Ground)

XXX19761

3520 Liquid/Liquid Ext for 8270 SIM

08/05/2008

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS4671

8270D SIMS

HP 5890 Series II MS2 SVOA