### Instructions for filling in the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate runs or sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. yellow are required. All cells that are shaded in green are populated using drop

- down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg +2 

### , or if the Ontario

- Hydro Method was used, you would need to enter Hg 0

### , HgP, and Hg Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please provide the values of all requested parameters for each of test run/sample. 2. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

- downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O 2 

### (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also enter these data.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg 0 

### and , HgP, and Hg +2 

### . However, both the Speciated Volatile Organic HAP worksheets allow you to use a drop

- down provided in the Constituent field to define as many records as needed to record each HAP that you have results for. General instructions

2. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples,

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and

(parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please alsoEIA

Facility Code Facility Name Boiler ID

3179 Hatfields Ferry

Power Station 1Control Device Configuraton

Listed (by

boiler) in Question 16 (page 17) of the questionnaireEIA

Facility Code Facility Name Boiler ID

3179 Hatfields Ferry

Power Station 1

Run Number Test Start Date Test Start TimeMe asured Value (ppm)

Test End Date Test End TimeBasis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DLL) CO Emission Test ResultsTest Method Comments lb/mmBtu ppmdv @ 7% O 2 Calculated Emission RateSteam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Moisture (%)Flue Gas CO 2(%) Flue Gas O 2(%) Flue Gas Flow Rate (dscfm)Fuel Input Rate Fuel Type

Flue Gas Temperature (F) Fuel #1Units of Measure Me asurement Method Fuel Input Rate Fuel #1Fuel Type Units of Measure Me asurement Method Fuel #2Fuel Input Rate Fuel Type Units of Measure Fuel #3Me asurement Method Fuel Input Rate Fuel Type Fuel #4Units of Measure Me asurement Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

M0011 1 12-May 7:10 12-May M0011 2 12-May 10:00 12-May M0011 3 12-May 12:35 12-May

Run Number Test Start Date Test Start Time Test End DateMe asured Value (ppm) Basis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DLL) 9:21 0.013 Dry U.S. EPA Method 0011 12:16 0.0087 Dry U.S. EPA Method 0011 14:52 0.015 Dry U.S. EPA Method 0011 Test End Time Formaldehyde Emission Test ResultsTest Method

Comments lb/mmBtu ppmdv @ 7% O 2 1.23E-05 1.07E-02 3613 8.58E-06 7.45E-03 3613 1.49E-05 1.31E-02 3613 Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr)Fuel Input Rate Fuel Type Units of Me asure 14.97 14.81 4.62 1200428 128.6 4344 bitum inous ton/day 14.24 14.73 4.7 1250701 129.1 4344 bitum inous ton/day 15.66 14.58 4.72 1233139 130.6 4344 bitum inous ton/day Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Fuel #1 Flue Gas Moisture (%) Flue Gas

CO 2(%) Flue Gas

O 2(%)Me asurement

Me thod Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Fuel Type Units of

Me asure Other 0.05 No.2 Fuel Oil (distillate) gallon/m inute

Other Other 0.05 No.2 Fuel Oil (distillate) gallon/m inute

Other Other 0.05 No.2 Fuel Oil (distillate) gallon/m inute

Other Fuel #2 Fuel #3Me asurement

Me thod Fuel Input

Rate Fuel Type Units of

Me asure Me asurement

Me thod Other Supporting Information Fuel #4EIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

M18 1 12-May 7:10 M18 2 12-May 10:00 M18 3 12-May 12:35

Run Number Test Start Date Test Start TimeMe asured Value (ppm) Basis (Wet or Dry)

12-May 9:21 0.1 We t 12-May 12:16 0.1 We t 12-May 14:52 0.1 We t Me thane Emission Test Results

Test End Date Test End TimeTest Method Used Data Flag (ADL, BDL, DLL) Test Method Comments lb/mmBtu

U.S. EPA Method 18 BDL 0 U.S. EPA Method 18 BDL 0 U.S. EPA Method 18 BDL 0 Me thane Emission Test Results Calculated Emission Rateppmdv @ 7% O 2

0 3613 14.97 14.81 4.62 1200428 0 3613 14.24 14.73 4.7 1250701 0 3613 15.66 14.58 4.72 1233139 Flue Gas Flow Rate (dscfm) Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas CO 2(%) Flue Gas

O 2(%)Fuel Input Rate Fuel Type Units of

Me asure Me asurement

Me thod Fuel

Input Rate Fuel Type Units of

Me asure

128.6 4344 bitum inous ton/day Other 0.05 No.2 Fuel Oil (distillate) gallon/m inute 129.1 4344 bitum inous ton/day Other 0.05 No.2 Fuel Oil (distillate) gallon/m inute 130.6 4344 bitum inous ton/day Other 0.05 No.2 Fuel Oil (distillate) gallon/m inute Flue Gas Temperat ure (F) Fuel #1 Fuel #2Me asurement

Me thod Fuel

Input Rate Fuel Type Units of

Me asure Me asurement

Me thod Fuel

Input Rate Fuel Type Units of

Me asure
Other Other Other Fuel #4 Fuel #3Me asurement

Me thod Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

Test End Date Run Number Test Start Date Test Start TimeMe asured Value (ppm) Basis (Wet or Dry) Test Method Used SO 2Emission Test Results Test End TimeData Flag (ADL,

BDL, DLL) Test Method

Comments lb/mmBtu ppmdv @ 7% O 2 Calculated Emission Rate Steam Output (1000 lb/hr)Fuel Input Rate Fuel Type Flue Gas Temperature (F) Fuel #1 Flue Gas Flow Rate (dscfm) Total Heat Input (mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO 2(%) Flue Gas

O 2(%)Units of

Me asure Me asurement

Method Fuel Input

Rate Fuel Type Units of

Me asure Me asurement

Me thod Fuel Input

Rate Fuel Type Fuel #1 Fuel #2 Fuel #3Units of

Me asure Me asurement

Method Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel #4 Fuel #3Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

M30B 1 11-May 8:05 M30B 2 11-May 11:05 M30B 3 11-May 13:40

Run Number Test Start Date Test Start TimePlease note QA/QC documentation starting in Column "AI"

Me asured Value (μg/dscm) Basis (Wet or Dry)

11-May 10:05 4.16 Dry 11-May 13:05 3.85 Dry 11-May 14:40 4.04 Dry

Test End Time Test End Date Total Vapor Phase Mercury Emission Test ResultsPlease note QA/QC documentation starting in Column "AI"

Test Method Used Data Flag (ADL, BDL, DLL) Test Method

Comments (lb/mmBtu)

U.S. EPA Method 30B 3.23E-06 3456 U.S. EPA Method 30B 3.07E-06 3456 U.S. EPA Method 30B 3.17E-06 3456 Steam Output (1000 lb/hr) Total Vapor Phase Mercury Emission Test ResultsFuel Input Rate

13.54 14.72 4.42 1158508 125.1 4128 14.62 14.29 4.82 1159417 125.1 4128 14.5 14.33 4.64 181644 125.8 4128 Flue Gas Moisture (%) Total Heat Input (mmBtu/hr) Flue Gas CO 2(%) Flue Gas

O 2(%) Flue Gas

Flow Rate (dscfm) Flue Gas

Temperature (F)Fuel Type Units of Me asure Me asurement

Method Fuel Input

Rate Fuel Type Units of

Me asure Me asurement

Me thod Fuel Input

Rate

bitum inous ton/day Other 6.42 No.2 Fuel Oil (distillate) gallon/m inute bitum inous ton/day Other 6.42 No.2 Fuel Oil (distillate) gallon/m inute bitum inous ton/day Other 6.42 No.2 Fuel Oil (distillate) gallon/m inute Fuel #1 Fuel #2Fuel Type Units of Me asure Me asurement

Method Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel #3 Fuel #4QA /QC Documentation

Trap ID Section 1

Ma ss (ng) Section 2

Ma ss (ng) Total

Ma ss (ng) Initial

Spike (ng) Total NonSpike (ng)

67570 148 0.7 148.7 0 148.7 67562 137 0.8 137.8 0 137.8 67529 142 0.6 142.6 0 142.6 Other Supporting InformationSample

Volume (dscm) Volume

Difference (%) Volume Diff. Limit Breaktrough

(%) Breaktrough

Limit Concentration

(μg/dscm) Trap ID

0.0354 0.472972973 4.200564972 59927 0.0356 0.583941606 3.870786517 60533 0.0356 0.422535211 4.005617978 59872 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! ≤ 20% of field recovery test ≤10% of Section 1 Hg

ma ss for Hg conc. >1

μg/dscm: or ≤ 20% of Section Trap #1Section 1

Ma ss Section 2

Ma ss Total

Ma ss Initial

Spike Total NonSpike Sample

Volume Volume

Difference (%) Volume Diff. Limit

248 1 249 100 149 0.0362 238 0.8 238.8 100 138.8 0.0363 247 0.9 247.9 100 147.9 0.0362 ≤ 20% of field recovery test Trap #2Breaktrough (%) Breaktrough Limit Concentration

(μg/dscm) Ab s. diff. RD (%) Limit C rec

0.403225806 4.116022099 0.084543 1.016557 2.7 0.336134454 3.82369146 0.047095 0.612063 2.7 0.36437247 4.085635359 0.080017 0.988937 2.8 #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! #DIV/0! ≥ 10 % RD mass for Hg conc. >1 μg/dscm: or

≤ 20% RD or ≤ 0.2 μg/dscm abs.diff. for Hg conc. ≤1 ≤10% of Section 1 Hg mass for Hg conc. >1

μg/dscm: or ≤ 20% of Section 1 for Hg conc. ≤1 Me asured Spike Recovery ( R ) Paired Trap Agreement (RD)R (%) by

Run Ravg(%) Limit

96.9 98.38 102.9 Average Recovery

, between 85 and 115% Me asured Spike Recovery ( R )

99.39333333EIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

Run Number Test Start Date Test Start TimeMe asured Hg 0Value (μg/dscm) Me asured Hg +2Value (μg/dscm) Test End Time Test End DateMe asured Hg PValue

(μg/dscm) Basis (Wet or Dry) Test Method Used Data Flag (ADL, BDL, DLL) Total Vapor Phase Mercury Emission Test ResultsTest Method

Comments Total Mercury (lb/mmBtu) Flue Gas CO 2(%) Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas

Moisture (%)Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel #1 Flue Gas O 2(%) Flue Gas

Flow Rate (dscfm) Flue Gas

Temperature (F)Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel #2 Fuel #3Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Me thod Other Supporting Information Fuel #4EIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

Speciated Volatile Organic HAP Emission Data

Methyl chloride 1 5/10/2010 Acetone 1 5/10/2010 Methyl bromide 1 5/10/2010 Trichlorofluoromethane 1 5/10/2010 Methyl iodide 1 5/10/2010 Methylene chloride 1 5/10/2010 Benzene 1 5/10/2010 Toluene 1 5/10/2010 Methyl chloride 2 5/11/2010 Methyl bromide 2 5/11/2010 Acetone 2 5/11/2010 Methyl iodide 2 5/11/2010 Methylene chloride 2 5/11/2010 Benzene 2 5/11/2010 Toluene 2 5/11/2010 Bromoform (tribromomethane) 2 5/11/2010 Methyl chloride 3 5/11/2010 Methyl bromide 3 5/11/2010 Methyl iodide 3 5/11/2010 Methylene chloride 3 5/11/2010 Chloroform 3 5/11/2010 Benzene 3 5/11/2010 Bromodichloromethane 3 5/11/2010 Dibromochloromethane 3 5/11/2010 Toluene 3 5/11/2010 Xylenes (isomer & mixtures) 3 5/11/2010 Bromoform (tribromomethane) 3 5/11/2010

Compound (use drop down to define for as many rows as

needed) Run Number Test Start DateMe asured Value (μg)

3:30 PM 5/10/2010 7:39 PM 0.21 3:30 PM 5/10/2010 7:39 PM 1.31 3:30 PM 5/10/2010 7:39 PM 0.02 3:30 PM 5/10/2010 7:39 PM 0.03 3:30 PM 5/10/2010 7:39 PM 0.02 3:30 PM 5/10/2010 7:39 PM 2.45 3:30 PM 5/10/2010 7:39 PM 0.09 3:30 PM 5/10/2010 7:39 PM 0.17 8:00 AM 5/11/2010 12:12 PM 0.26 8:00 AM 5/11/2010 12:12 PM 0.05 8:00 AM 5/11/2010 12:12 PM 1.15 8:00 AM 5/11/2010 12:12 PM 0.07 8:00 AM 5/11/2010 12:12 PM 2.45 8:00 AM 5/11/2010 12:12 PM 0.09 8:00 AM 5/11/2010 12:12 PM 0.1 8:00 AM 5/11/2010 12:12 PM 0.04 12:30 PM 5/11/2010 4:45 PM 0.04 12:30 PM 5/11/2010 4:45 PM 0.02 12:30 PM 5/11/2010 4:45 PM 0.02 12:30 PM 5/11/2010 4:45 PM 0.04 12:30 PM 5/11/2010 4:45 PM 0.22 12:30 PM 5/11/2010 4:45 PM 0.06 12:30 PM 5/11/2010 4:45 PM 0.26 12:30 PM 5/11/2010 4:45 PM 0.15 12:30 PM 5/11/2010 4:45 PM 0.06 12:30 PM 5/11/2010 4:45 PM 0.02 12:30 PM 5/11/2010 4:45 PM 0.05 Test Start Time Test End Date Test End TimeFootnotes:

* Front half fraction contains filter, cyclone, and cartridge ** Back half fraction contains condensate, solvent, impingers

Basis Test Method Used Data Flag (ADL, BDL, DLL) Front Half Mass (ng) Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.21 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.19 Dry u.S. EPA Method 0031 with SW -846 Method 8260B 0.02 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.03 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.02 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.29 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.09 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.13 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.26 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.05 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.11 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.07 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.17 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.09 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.1 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.04 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.04 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.02 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.02 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.04 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.22 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.06 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.26 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.15 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.06 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.02 Dry U.S. EPA Method 0031 with SW -846 Method 8260B 0.05Back Half Mass (ng) Total Mass (ng) Test Method Comments lb/mmBtu

0 0.21 4.00E-08 1.12 1.31 2.50E-07 0 0.02 3.81E-09 0 0.03 5.72E-09 0 0.02 3.81E-09 2.16 2.45 4.67E-07 0 0.09 1.70E-08 0.04 0.17 3.24E-08 0 0.26 4.96E-08 0 0.05 9.54E-09 1.04 1.15 2.19E-07 0 0.07 1.34E-08 2.28 2.45 4.67E-07 0 0.09 1.79E-08 0 0.1 1.91E-08 0 0.04 7.63E-09 0 0.04 7.63E-09 0 0.02 3.81E-09 0 0.02 3.81E-09 0 0.04 7.63E-09 0 0.22 4.20E-08 0 0.06 1.13E-08 0 0.26 4.96E-08 0 0.15 2.88E-08 0 0.06 1.14E-08 0 0.02 3.81E-09 0 0.05 9.54E-09 Calculated Emission Rateug/dscm @ 7% O2

2.63 2830 14.25 16.4 2830 14.25 0.25 2830 14.25 0.38 2830 14.25 0.25 2830 14.25 30.67 2830 14.25 1.11 2830 14.25 2.13 2830 14.25 3.25 3456 14.3 0.63 3456 14.3 14.38 3456 14.3 0.88 3456 14.3 30.63 3456 14.3 1.18 3456 14.3 1.25 3456 14.3 0.5 3456 14.3 0.51 3456 14.13 0.25 3456 14.13 0.25 3456 14.13 0.51 3456 14.13 2.79 3456 14.13 0.75 3456 14.13 3.3 3456 14.13 1.92 3456 14.13 0.76 3456 14.13 0.25 3456 14.13 0.63 3456 14.13 Flue Gas Moisture (%) Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr)14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.68 4.54 1212199 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.65 4.51 1177978 127.1 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 14.3 4.75 1195317 126.7 Flue Gas CO 2(%) Flue Gas O 2(%) Flue Gas Flow Rate (scfm) Flue Gas Temperature (F)Fuel Input Rate Fuel Type Units of Measure Me asurement Method

4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4080 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other 4128 bitum inous ton/day Other Fuel #1Fuel Input Rate Fuel Type Units of Measure Me asurement Method

7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 7.9 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other 6.4 No.2 Fuel Oil (distillate) gallon/m inute Other Fuel #2Fuel Input Rate Fuel Type Units of Measure Me asurement Method Fuel #3Fuel Input Rate Fuel Type Units of Measure Me asurement Method Fuel #4Other Supporting

InformationEIA

Facility Code Facility Name 3179 Hatfields Ferry

Power Station

Speciated Semi-Volatile Organic HAP Emission Data

1-methylnapthalene 1 Benzoic acid 1 Biphenyl 1 Bis(2-ethylhexyl) phthalate 1 Diethyl phthalate 1 Di-n-butyl phthalate 1 Fluorene 1 Naphthalene 1 Phenanthrene 1 1-methylnapthalene 2 2-Methylnaphthalene 2 Acenaphthylene 2 Benzoic acid 2 Biphenyl 2 Bis(2-ethylhexyl) phthalate 2 Diethyl phthalate 2 Di-n-butyl phthalate 2 Fluoranthene 2 Fluorene 2 Naphthalene 2 Phenanthrene 2 Phenol 2 2-Methylnaphthalene 3 Benzoic acid 3 Biphenyl 3 Bis(2-ethylhexyl) phthalate 3 Di-n-butyl phthalate 3 Naphthalene 3 Phenanthrene 3

Compound (use drop down to define for as many rows as

needed) Run NumberBoiler ID 1

5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 7:10 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 10:00 AM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 5/12/2010 12:35 PM 5/12/2010 Test Start Date Test Start Time Test End DateFootnotes: * Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses *** Condensate Composite contains condensate and Impinger contents and the glassware solvent rinses

Me asured Value (μg) Basis (Wet or Dry)

9:21 AM 0.39 Dry 9:21 AM 34 Dry 9:21 AM 0.48 Dry 9:21 AM 19 Dry 9:21 AM 3 Dry 9:21 AM 21 Dry 9:21 AM 0.84 Dry 9:21 AM 4.35 Dry 9:21 AM 0.3 Dry 12:16 PM 0.33 Dry 12:16 PM 1.14 Dry 12:16 PM 0.39 Dry 12:16 PM 85 Dry 12:16 PM 0.72 Dry 12:16 PM 28 Dry 12:16 PM 3 Dry 12:16 PM 14 Dry 12:16 PM 0.24 Dry 12:16 PM 0.72 Dry 12:16 PM 3.78 Dry 12:16 PM 0.48 Dry 12:16 PM 5 Dry 2:52 PM 0.54 Dry 2:52 PM 57 Dry 2:52 PM 0.3 Dry 2:52 PM 24 Dry 2:52 PM 3 Dry 2:52 PM 2 Dry 2:52 PM 0.57 Dry Test End Time* Front Half Composite contains particulate filter, front half of the filter holder, and probe solvent rinses ** Back Half Composite contains XAD-2 resin tube, back half of the filter holder, and coil condenser solvent rinses *** Condensate Composite contains condensate and Impinger contents and the glassware solvent rinses

Test Method Used Data Flag (ADL, BDL, DLL) Front Half mass* (ng)

U.S. EPA Method 0010 with SW -846 Method 8270D 0.39 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.48 U.S. EPA Method 0010 with SW -846 Method 8270D 19 U.S. EPA Method 0010 with SW -846 Method 8270D 3 U.S. EPA Method 0010 with SW -846 Method 8270D 16 U.S. EPA Method 0010 with SW -846 Method 8270D 0.6 U.S. EPA Method 0010 with SW -846 Method 8270D 3 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.33 U.S. EPA Method 0010 with SW -846 Method 8270D 0.72 U.S. EPA Method 0010 with SW -846 Method 8270D 0.39 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.42 U.S. EPA Method 0010 with SW -846 Method 8270D 13 U.S. EPA Method 0010 with SW -846 Method 8270D 3 U.S. EPA Method 0010 with SW -846 Method 8270D 14 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.54 U.S. EPA Method 0010 with SW -846 Method 8270D 2.73 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.21 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.3 U.S. EPA Method 0010 with SW -846 Method 8270D 16 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0 U.S. EPA Method 0010 with SW -846 Method 8270D 0.3 Semi-Volatile Organic HAP Emission Test ResultsBack Half mass* (ng) Condensate Mass*** (ng) Total Composite (ng)

0 0 0.39 34 0 34 0 0 0.48 0 0 19 0 0 3 5 0 21 0.24 0 0.84 1.35 0 4.35 0.39 0 0.39 0 0 0.33 0.42 0 1.14 0 0 0.39 85 0 85 0.3 0 0.72 15 0 28 0 0 3 0 0 14 0.24 0 0.24 0.18 0 0.72 1.05 0 3.78 0.48 0 0.48 5 0 5 0.33 0 0.54 57 0 57 0 0 0.3 8 0 24 3 0 3 2 0 2 0.27 0 0.57 Semi-Volatile Organic HAP Emission Test ResultsTest Method Comments lb/mmBtu ug/dscm @ 7% O2

1.50E-07 0.16 1.31E-05 14.22 1.85E-07 0.2 7.31E-06 7.95 1.15E-06 1.25 8.08E-06 8.78 3.23E-07 0.35 1.67E-06 1.82 1.50E-07 0.16 1.13E-07 0.12 3.90E-07 0.42 1.33E-07 0.14 2.91E-05 31.48 2.46E-07 0.27 9.58E-06 10.37 1.03E-06 1.11 4.79E-06 5.19 8.21E-08 0.09 2.46E-07 0.27 1.29E-06 1.4 1.64E-07 0.18 1.71E-06 1.85 1.99E-07 0.22 2.10E-05 23.01 1.11E-07 0.12 8.84E-06 9.69 1.11E-06 1.21 7.37E-07 0.81 2.10E-07 0.23 Calculated Emission Rate3613 14.15 3613 14.15 3613 14.15 3613 14.15 3613 14.15 3613 14.15 3613 14.15 3613 14.15 3613 14.15 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 13.4 3613 14.32 3613 14.32 3613 14.32 3613 14.32 3613 14.32 3613 14.32 3613 14.32 Flue Gas Moisture (%) Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr)14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.81 4.62 1212912 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.72 4.7 1275899 14.58 4.72 1255165 14.58 4.72 1255165 14.58 4.72 1255165 14.58 4.72 1255165 14.58 4.72 1255165 14.58 4.72 1255165 14.58 4.72 1255165 Flue Gas CO 2(%) Flue Gas O 2(%) Flue Gas Flow Rate (scfm)Fuel Input Rate Fuel Type

126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.5 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 126.6 4344 bitum inous 127 4344 bitum inous 127 4344 bitum inous 127 4344 bitum inous 127 4344 bitum inous 127 4344 bitum inous 127 4344 bitum inous 127 4344 bitum inous Flue Gas Temperature (F) Fuel #1Units of Measure Me asurement Method Fuel Input Rate

ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 0.05 ton/day Other 1.05 ton/day Other 2.05 ton/day Other 3.05 ton/day Other 4.05 ton/day Other 5.05 ton/day Other 6.05 Fuel #1Fuel Type Units of Measure Me asurement Method

No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other No.2 Fuel Oil (distillate) gallon/m inute Other Fuel #2Fuel Input Rate Fuel Type Units of Measure Fuel #3Me asurement Method Fuel Input Rate Fuel Type Fuel #4Units of Measure Me asurement Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID

3179 Hatfields Ferry

Power Station 1

M033 R1 13-May 7:25 13-May M033 R2 13-May 8:55 13-May M033 R3 13-May 10:20 13-May Run Number Test Start Date Test Start Time Test End DateMe asured Value (ppm) Basis (Wet or Dry) Test Method Used

8:33 2.21 Dry U.S. EPA Conditional Test Method 033 (CTM-033) 10:04 2.17 Dry U.S. EPA Conditional Test Method 033 (CTM-033) 11:31 2.24 Dry U.S. EPA Conditional Test Method 033 (CTM-033) Hydrogen Cyanide Emission Test Results Test End TimeData Flag (ADL,

BDL, DLL) Test Method

Comments U.S. EPA Conditional Test Method 033 (CTM-033) 1.94E-03 14.29 14.63 U.S. EPA Conditional Test Method 033 (CTM-033) 1.92E-03 14.26 14.62 U.S. EPA Conditional Test Method 033 (CTM-033) 1.97E-03 14.23 14.59 Calculated Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Flue Gas CO 2(%) Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr)Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate 4.64 1231633 126.9 4.64 1254990 126.8 4.66 1237338 126.8 Flue Gas Temperature (F) Fuel #1 Flue Gas O 2(%) Flue Gas

Flow Rate (dscfm)Fuel Type Units of Me asure Me asurement

Method Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Me asure Me asurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID

3179 Hatfields Ferry

Power Station 1

Run Number Test Start Date Test Start Time Test End DateMe asured Value (ppm) Basis (Wet or Dry) Test Method Used Test End Time Hydrogen Chloride Emission Test ResultsData Flag (ADL,

BDL, DLL) Test Method

Comments Hydrogen Chloride Emission Test Results Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Calculated Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Flue Gas CO 2(%)Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Flue Gas Flow Rate (dscfm) Flue Gas

Temperature (F) Fuel #1 Flue Gas O 2(%)Fuel Type Units of Me asure Me asurement

Method Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Me asure Me asurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID

3179 Hatfields Ferry

Power Station 1

Run Number Test Start Date Test Start Time Test End DateMe asured Value (ppm) Basis (Wet or Dry) Test Method Used Hydrogen Flouride Emission Test Results Test End TimeData Flag (ADL,

BDL, DLL) Test Method

Comments Calculated

Emission Rate (lb/mmBtu) Flue Gas Moisture (%) Hydrogen Flouride Emission Test Results Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr)Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Flue Gas Temperature (F) Fuel #1 Flue Gas CO 2(%) Flue Gas

O 2(%) Flue Gas

Flow Rate (dscfm)Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Method Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel #2 Fuel #3Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

Run Number Test Start Date Test Start TimeMe asured NO (ppm)

Test End Date Test End TimeMe asured NO 2(ppm) Basis (Wet or Dry) Test Method Used NO XEmission Test ResultsData Flag (ADL, BDL, DLL) Test Method Comments (lb/mmBtu) Total NO XCalculated Emission Rateppmdv @ 7% O 2 Calculated Emission Rate Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr) Flue Gas

Moisture (%) Flue Gas

CO 2(%) Flue Gas

O 2(%)Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Flue Gas Temperature (F) Fuel #1 Flue Gas Flow Rate (dscfm)Fuel Type Units of Me asure Me asurement

Method Fuel Input

Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input

Rate Fuel #2 Fuel #3Fuel Type Units of Me asure Me asurement

Method Fuel #4 Other Supporting InformationEIA

Facility Code Facility Name Boiler ID 3179 Hatfields Ferry

Power Station 1

1 10-May 2 11-May 3 11-May Run Number Test Start Date Test Start TimeTotal Dissolved Solids (mg solids/liter) Total Suspended Solids (mg solids/liter) 10-May 29700 120000 11-May 29600 210000 11-May 32000 110000

Test End Time Test End DateTest Method Used Data Flag (ADL, BDL, DLL)

Standard Methods of the Examination of W ater and W astewater Method 2540B Standard Methods of the Examination of W ater and W astewater Method 2540B Standard Methods of the Examination of W ater and W astewater Method 2540B

Constisuent Emission Test ResultsTest Method Comments Fuel Input Rate Flue Gas Temperat ure (F) Flue Gas Flow Rate (dscfm) Steam Output (1000 lb/hr) Total Heat Input

(mmBtu/hr)Fuel Type Units of Me asure Me asurement

Method Fuel Input Rate Fuel Type Units of Me asure Me asurement

Me thod Fuel Input Rate Fuel #1 Fuel #2Fuel Type Units of Me asure Me asurement

Method Fuel Input

Rate Fuel Type Units of

Me asure Me asurement

Me thod Fuel #3 Fuel #4Other Supporting InformationFuel

anthracite bitum inous subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) synfuel petroleum coke other

Relative to Control Device Upstream Downstream

Fuel Input Units of Measure MMBtu/hr standard cubic feet per minute (scfm) gallon/m inute lb/hour ton/day

Exhaust Flow Rate Units of Measure acfm dscfm

Exhaust Temperature Units of Measure deg C deg F

Test Method Used for Fuel Input Rate F-Factor gas fuel meter boiler efficiency

calculation Other

CO Test Method U.S. EPA Method 10A U.S. EPA Method 10B

Formaldehyde Test Method

U.S. EPA Method 320U.S. EPA Method 0011

U.S. EPA Method 316

CH4 Test Method U.S. EPA Method 18 U.S. EPA Method 320

SO2 Test Method U.S. EPA Method 6

Hg Test Method U.S. EPA Method 30B

Speciated Volatile Organic HAP M ethod U.S. EPA Method 0031 with SW -846 Method 8260B U.S. EPA Method 0031/TO-15

Speciated Semi-Volatile Organic HAP M ethod U.S. EPA Method 0010 with SW -846 Method 8270C U.S. EPA Method 0010 with SW -846 Method 8270D

HCN Test Method U.S. EPA Conditional Test Method 033 (CTM-033) U.S. EPA Method 320 CARB 426 U.S. EPA Method 26A-Mod

O2/CO2 Test Method U.S. EPA Method 3B

NOX Test Method U.S. EPA Method 7 U.S. EPA Method 7A

U.S. EPA Method 7B U.S. EPA Method 7C U.S. EPA Method 7D

TDS/TSS Test Method Standard Test Method for Filterable and Nonfilterable Matter in W ater ASTM D5907 Standard Methods of the Examination of W ater and W astewater Method 2540B

Control Configuration 

### Listed (by boiler) in Question 16 (page 17) of the questionnaire Listed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICRHg Ontario Hydro Test Method

ASTM Method D6784

HCL Test Methods U.S. EPA Method 320 U.S. EPA Method 26

HF Test Methods U.S. EPA Method 320 U.S. EPA Method 26

Basis We t DryConstituent CAS Methyl chloride 74-87-3 1,1,2-Trichloroethane 79-00-5 1,1-Dimethylhydrazine 57-14-7 1,2,4-Trichlorobenzene 120-82-1 1,2-Dibromo-3-chloropropane 96-12-8 1,2-Epoxybutane (1,2-butylene oxide) 106-88-7 1,2-Propyleneim ine (2-methylaziridine) 75-55-8 1,3-Butadiene 106-99-0 1,3-Dichloropropene 542-75-6 1,3-Propane sultone 1120-71-4 1,4-Dichlorobenzene (p-) 106-46-7 1,4-Dioxane (1,4-Diethylene oxide) 123-91-1 2,2,4-Trimethyl pentane 540-84-1 2-Nitropropane 79-46-9 Acetaldehyde 75-07-0 Acetonitrile (cyanom ethane) 75-05-8 Acetone 67-64-1 Acetophenone 98-86-2 Acrolein (2-propenal) 107-02-8 Acrylam ide 79-06-1 Acrylic acid 79-10-7 Acrylonitrile (2-propenenitrile) 107-13-1 Allyl chloride (3-chloropropene) 107-05-1 Aniline (am inobenzene) 62-53-3 Benzene 71-43-2 Benzyl chloride (a-chlorotoluene) 100-44-7 Beta-Propiolactone 57-57-8 Bis(2-Chloroethyl)ether 111-44-4 Bis(chloromethyl) ether 542-88-1 Bromodichloromethane 75-27-4 Bromoform (tribromomethane) 75-25-2 Carbon disulfide 75-15-0 Carbon tetrachloride 56-23-5 Carbonyl sulfide 463-58-1 Catechol (o-hydroxyphenol) 120-80-9 Chloroacetic acid 79-11-8 Chlorobenzene 108-90-7 Chloroform 67-66-3 Chloromethyl m ethyl ether 107-30-2 Chloroprene (2-chloro-1,3-butadiene) 126-99-8 Cresylic acid (cresol isomer mixture) 1319-77-3 Cumene (isopropylbenzene) 98-82-8 Diazom ethane 334-88-3 Dibromochloromethane 124-48-1 Diethyl sulfate 64-67-5 Dim ethyl sulfate 77-78-1 Dim ethylcarbamyl chloride 79-44-7 Epichlorohydrin (1-chloro-2,3-epoxy propane) 106-89-8 Speciated Volatile Organic HAPsEthyl acrylate 140-88-5 Ethyl carbamate (urethane) 51-79-6 Ethyl chloride 75-00-3 Ethylbenzene 100-41-4 Ethylene dibrom ide (1,2-dibromoethane) 106-93-4 Ethylene dichloride (1,2-dichloroethane) 107-06-2 Ethylene oxide 75-21-8 Ethyleneim ine (aziridine) 151-56-4 Ethylidene dichloride (1,1-dichloroethane) 75-34-3 Formaldehyde 50-00-0 Hexachlorobutadiene 87-68-3 Hexachloroethane 67-72-1 Hexane 110-54-3 Isophorone 78-59-1 1, 1, 2, 2-Tetrachloroethane 79-34-5 Methanol 67-56-1 Methyl bromide 74-83-9. Methyl chloroform (1,1,1-trichloroethane) 71-55-6 Methyl ethyl ketone (2-butanone) 78-93-3 Methyl iodide 74-88-4 Methyl isobutyl ketone (hexone) 108-10-1 Methyl isocyanate 624-83-9 Methyl m ethacrylate 80-62-6 Methyl tert-butyl ether 1634-04-4 Methylene chloride 75-09-2 Methylhydrazine 60-34-4 m-Xylene 108-38-3 N,N-Dimethylaniline 100-23-2 N,N-Dimethylformamide 68-12-2 Nitrobenzene 98-95-3 N-Nitrosodimethylam ine 62-75-9 N-Nitrosomorpholine 59-89-2 N-Nitroso-N-methylurea 684-93-5 o-Cresol 95-48-7 o-Xylene 95-47-6 Phenol 108-95-2 Phosgene 75-44-5 Propionaldehyde 123-38-6

Propylene dichloride (1,2-dichloropropane) 78-87-5 Propylene oxide 75-56-9 p-Xylene 106-42-3 Styrene 100-42-5 Styrene oxide 96-09-3 Tetrachloroethylene 127-18-4 Toluene 108-88-3 Trichlorofluoromethane 75-69-4 Trichloroethylene 79-01-6 Triethylam ine 121-44-8 Vinyl acetate 108-05-04 

### Listed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICR Vinyl bromide 593-60-2Vinyl chloride (chloroethene) 75-01-4 Vinylidene chloride 75-35-4 Xylenes (isomer & mixtures) 1330-20-7Speciated Semi-volatile Organic HAPs

Constituent CAS 2-Methylnaphthalene 91-57-6 1-methylnapthalene 90-12-0 Acenaphthene 83-32-9 Acenaphthylene 208-96-8 Anthracene 120-12-7 Benzo(a)anthracene 56-55-3 Benzo(a)pyrene 50-32-8 Benzo(b)fluoranthene 205-99-2 Benzo(e)pyrene 192-97-2 Benzo(g,h,i)perylene 191-24-2 Benzo(k)fluoranthene 207-08-9 Biphenyl 92-51-3 Chrysene 218-01-9 Dibenzo(a,h)anthracene 53-70-3 Fluoranthene 206-44-0 Fluorene 86-73-7 Indeno(1,2,3-cd)pyrene 193-39-5 Naphthalene 91-20-3 Perylene 77392-71-3 Phenanthrene 85-01-8 Pyrene 129-00-0 Acetophenone 98-86-2 2-Acetylam inofluorene 53-96-3 1-Acetyl-2-thiourea 591-08-2 Aldrin 309-00-2 2-Aminoanthraquinone 117-79-3 Am inoazobenzene 60-09-3 4-Aminobiphenyl 92-67-1 3-Amino-9-ethylcarbazole 132-32-1 Anilazine 101-05-3 Aniline 62-53-3 o-Anisidine 90-04-0 Aramite 140-57-8 Aroclor 1016 12674-11-2 Aroclor 1221 11104-28-2 Aroclor 1232 11141-16-5 Aroclor 1242 53469-21-9 Aroclor 1248 12672-29-6 Aroclor 1254 11097-69-1 Aroclor 1260 11096-82-5 Azinphos-m ethyl 86-50-0 Barban 101-27-9 Benzidine 92-87-5 Benzoic acid 65-85-0 p-Benzoquinone 106-51-4 Benzyl alcohol 100-51-6 α-BHC 319-84-6

β-BHC 319-85-7δ-BHC 319-86-8

γ-BHC (Lindane) 58-89-9 Bis(2-chloroethoxy)methane 111-91-1 Bis(2-chloroethyl) ether 111-44-4 Bis(2-chloroisopropyl) ether 39638-32-9 Bis(2-ethylhexyl) phthalate 117-81-7 4-Bromophenyl phenyl ether 101-55-3 Bromoxynil 1689-84-5 Butyl benzyl phthalate 85-68-7 Captafol 2425-06-1 Captan 133-06-2 Carbaryl 63-25-2 Carbofuran 1563-66-2 Carbophenothion 786-19-6 Chlordane (NOS) 57-74-9 Chlorfenvinphos 470-90-6 4-Chloroaniline 106-47-8 Chlorobenzilate 510-15-6 5-Chloro-2-methylaniline 95-79-4 4-Chloro-3-methylphenol 59-50-7 3-(Chloromethyl)pyridine hydrochloride 6959-48-4 1-Chloronaphthalene 90-13-1 2-Chloronaphthalene 91-58-7 2-Chlorophenol 95-57-8 4-Chloro-1,2-phenylenediam ine 95-83-0 4-Chloro-1,3-phenylenediam ine 5131-60-2 4-Chlorophenyl phenyl ether 7005-72-3 Coumaphos 56-72-4 p-Cresidine 120-71-8 Crotoxyphos 7700-17-6 2-Cyclohexyl-4,6-dinitro-phenol 131-89-5 4,4'-DDD 72-54-8 4,4'-DDE 72-55-9 4,4'-DDT 50-29-3 Demeton-O 298-03-3 Demeton-S 126-75-0 Diallate (cis or trans) 2303-16-4 2,4-Diaminotoluene 95-80-7

Dibenz(a,j)acridine 224-42-0 Dibenzofuran 132-64-9 Dibenzo(a,e)pyrene 192-65-4 1,2-Dibromo-3-chloropropane 96-12-8 Di-n-butyl phthalate 84-74-2 Dichlone 117-80-6 1,2-Dichlorobenzene 95-50-1 1,3-Dichlorobenzene 541-73-1 1,4-Dichlorobenzene 106-46-7 3,3'-Dichlorobenzidine 91-94-1 2,4-Dichlorophenol 120-83-2 2,6-Dichlorophenol 87-65-0Dichlorovos 62-73-7

Dicrotophos 141-66-2 Dieldrin 60-57-1 Diethyl phthalate 84-66-2 Diethylstilbestrol 56-53-1 Diethyl sulfate 64-67-5 Dim ethoate 60-51-5 3,3'-Dimethoxybenzidine 119-90-4 Dim ethylam inoazobenzene 60-11-7 7,12-Dimethylbenz(a)-anthracene 57-97-6 3,3'-Dimethylbenzidine 119-93-7 α,α-Dimethylphenethylam ine 122-09-8 2,4-Dimethylphenol 105-67-9 Dim ethyl phthalate 131-11-3 1,2-Dinitrobenzene 528-29-0 1,3-Dinitrobenzene 99-65-0 1,4-Dinitrobenzene 100-25-4 4,6-Dinitro-2-methylphenol 534-52-1 2,4-Dinitrophenol 51-28-5 2,4-Dinitrotoluene 121-14-2 2,6-Dinitrotoluene 606-20-2 Dinocap 39300-45-3 Dinoseb 88-85-7 Diphenylam ine 122-39-4 5,5-Diphenylhydantoin 57-41-0 1,2-Diphenylhydrazine 122-66-7 Di-n-octyl phthalate 117-84-0 Disulfoton 298-04-4 Endosulfan I 959-98-8 Endosulfan II 33213-65-9 Endosulfan sulfate 1031-07-8 Endrin 72-20-8 Endrin aldehyde 7421-93-4 Endrin ketone 53494-70-5 X X ND X X 53494-70-5 EPN 2104-64-5 Ethion 563-12-2 Ethyl carbamate 51-79-6 Ethyl m ethanesulfonate 62-50-0 Famphur 52-85-7 Fensulfothion 115-90-2 Fenthion 55-38-9 Fluchloralin 33245-39-5 2-Fluorobiphenyl (surr) 321-60-8 2-Fluorophenol (surr) 367-12-4 Heptachlor 76-44-8 Heptachlor epoxide 1024-57-3 Hexachlorobenzene 118-74-1 Hexachlorobutadiene 87-68-3 Hexachlorocyclopentadiene 77-47-4 Hexachloroethane 67-72-1 Hexachlorophene 70-30-4 Hexachloropropene 1888-71-7 Hexamethylphosphoramide 680-31-9 Hydroquinone 123-31-9Isodrin 465-73-6

Isophorone 78-59-1 Isosafrole 120-58-1 Kepone 143-50-0 Leptophos 21609-90-5 Malathion 121-75-5 Maleic anhydride 108-31-6 Mestranol 72-33-3 Methapyrilene 91-80-5 Methoxychlor 72-43-5 3-Methylcholanthrene 56-49-5 4,4'-Methylenebis (2-chloroaniline) 101-14-4 4,4'-Methylenebis(N,N-dimethylaniline) 101-61-1 Methyl m ethanesulfonate 66-27-3 Methyl parathion 298-00-0 2-Methylphenol 95-48-7 3-Methylphenol 108-39-4 4-Methylphenol 106-44-5 Mevinphos 7786-34-7 Mexacarbate 315-18-4 Mirex 2385-85-5 Monocrotophos 6923-22-4 Naled 300-76-5 1,4-Naphthoquinone 130-15-4 1-Naphthylam ine 134-32-7 2-Naphthylam ine 91-59-8 Nicotine 54-11-5 5-Nitroacenaphthene 602-87-9 2-Nitroaniline 88-74-4 3-Nitroaniline 99-09-2 4-Nitroaniline 100-01-6 5-Nitro-o-anisidine 99-59-2 Nitrobenzene 98-95-3 4-Nitrobiphenyl 92-93-3 Nitrofen 1836-75-5 2-Nitrophenol 88-75-5 4-Nitrophenol 100-02-7 5-Nitro-o-toluidine 99-55-8 Nitroquinoline-1-oxide 56-57-5 N-Nitrosodi-n-butylam ine 924-16-3 N-Nitrosodiethylam ine 55-18-5 N-Nitrosodimethylam ine 62-75-9 N-Nitrosodiphenylam ine 86-30-6 N-Nitrosodi-n-propylam ine 621-64-7 N-Nitrosomethylethylam ine 10595-95-6 N-Nitrosomorpholine 59-89-2 N-Nitrosopiperidine 100-75-4 N-Nitrosopyrrolidine 930-55-2 Octamethyl pyrophosphoramide 152-16-9 4,4'-Oxydianiline 101-80-4 Parathion 56-38-2 Pentachlorobenzene 608-93-5 Pentachloronitrobenzene 82-68-8 Pentachlorophenol 87-86-5 Phenacetin 62-44-2Phenobarbital 50-06-6

Phenol 108-95-2 1,4-Phenylenediam ine 106-50-3 Phorate 298-02-2 Phosalone 2310-17-0 Phosmet 732-11-6 Phosphamidon 13171-21-6 Phthalic anhydride 85-44-9 2-Picoline (2-Methylpyridine) 109-06-8 Piperonyl sulfoxide 120-62-7 Pronamide 23950-58-5 Propylthiouracil 51-52-5 Resorcinol 108-46-3 Safrole 94-59-7 Strychnine 57-24-9 Sulfallate 95-06-7 Terbufos 13071-79-9 1,2,4,5-Tetrachlorobenzene 95-94-3 2,3,4,6-Tetrachlorophenol 58-90-2 Tetrachlorvinphos 961-11-5 Tetraethyl dithiopyrophosphate 3689-24-5 Tetraethyl pyrophosphate 107-49-3 Thionazine 297-97-2 Thiophenol (Benzenethiol) 108-98-5 Toluene diisocyanate 584-84-9 o-Toluidine 95-53-4 Toxaphene 8001-35-2 1,2,4-Trichlorobenzene 120-82-1 2,4,5-Trichlorophenol 95-95-4 2,4,6-Trichlorophenol 88-06-2 Trifluralin 1582-09-8 2,4,5-Trimethylaniline 137-17-7 Trimethyl phosphate 512-56-1 1,3,5-Trinitrobenzene 99-35-4 Tris(2,3-dibromopropyl) phosphate 126-72-7 Tri-p-tolyl phosphate 78-32-0 O,O,O-Triethyl phosphorothioate 126-68-1