# LaboratoryServices

;TANtPA ELECTRIC 5012 Causeway Blvd • Tampa FI. 33619 • Ph (813)630-7490 • Fax (813)630-7360 • DOH #E54272 

## Report For: Ray McDarby 

## ReportDate: 8/31/2010 

# Laboratory 10: 

# AB07088 Location Code: Sample 

# Information Description: Big Bend Unit#1 (4/20-4/22) Sampled 

## By: SCOTT GIVEN ProjectAccount Code: W4 Dateand Time Collected: 4128/201012:00:00

## AM Sample Collection Method: Date ofSample Receipt: 4128/2010 

# Laboratory Results Qualifier Test Analysis Lower Upper Violation PARAMETER Result Units MDL Code Method Analyst Date&Time Limit Limit Check Chloride Duplicate result, Run 1 a 22.769 ug/ml 0,05 Method 26a KASZS 

### 4/26/201012:16:00PM Chloride Duplicate result Run 2a 20.949 ugiml 0.05 Method26a KASZS 412612010 12:16:00 PM Chloride Duplicate result. Run 3a 2.697 ug/ml Method26a KASZS 41261201012:16:00 PM Chloride Duplicate result. Run 4A 2.747 uglml Method 26a KASZS 

### 4/261201012:16:00 PM Chloride result. Run 1a 22.945 uglml 0.05 Method26a KASZS 

### 4126/20101216:00 PM Chloride result. Run 2a 21.189 uglml 0.05 Method26a KASZS 412612010121600 PM Chloride result. Run 3a 2.676 uglml 0.05 Method 26a KASZS 

### 4126/201012:16:00 PM Chloride result, Run 4A 2.746 uglml 0.05 Method 26a KASZS 

### 4126/201012:1600PM Chloride, Duplicate Blank result < uglmL 

## u EPA Method 26a KASZS 

### 4/26/2010 12:16:00 PM Final Sample Volume, Run 1 a 440 mL EPA Method26a KASZS 

### 4/261201012:16:00 PM Final Sample Volume, Run 2a 495 mL EPA Method 26a KASZS 

### 4/26/201012:1600 PM Final Sample Volume, Run 3a 488 mL EPA Method 26a KASZS 

### 4126/201012:16:00 PM Final Sample Volume, Run4a 472 mL EPA Method 26a KASZS 

### 4/26/201012:16:00PM Fluoride Duplicate result, Run 1a 0.287 uglmL 0.05 Method26a KASZS 41261201012:16:00 PM Fluoride Duplicate result. Run 2a 0.282 uglmL 0.05 Method26a KASZS 

### 4/261201012:16:00 PM Fluoride Duplicate result, Run 3a 0.168 uglmL 0.05 Method 26a KASZS 

### 4/261201012:16:00PM Fluoride Duplicate result. Run 4A 0205 uglmL 0.05 Method26a KASZS 41261201012:16:00 PM Fluoride. Duplicate Blank result < uglml 

## u EPA Method26a KASZS 

### 4/2612010 12:1600 PM HCl result. Run 1 a 10339 ug Method 26a KASZS 41261201012:16:00 PM HCl result. Run 2a 10721 ug Method 26a KASZS 

### 4/261201012:16:00 PM HCl result. Run 3a 1347 u9 Method 26a KASZS 41261201012:1600 PM HClresult. Run 4A 1332 ug Method 26a KASZS 

### 4/261201012:16:00 PM HF result. Run 1 a 131 u9 Method 26a KASZS 

### 4126/201012:16:00 PM HF result. Run2a 147 ug Method26a KASZS 

### 4/2612010 1216:00 PM HF result. Run3a 

### 874 u9 Method 26a KASZS 412612010 12:16:00 PM

Laboratory Services certifies that the test results in this report meet all requirements ofthe 

### NElAC standards, unless indicated otherwise in the body ofthe report. Unlessotherwise noted, all methodsfollowed are perthe mostcurrent published version of40 CFR Part 136, Table B. Results reported on this report pertain to the above referenced sample only.

Report Number: AB07088-083110-09 

### Page I of2 "GeneralReport"

# LaboratoryServices

TAMPA ELECTRIC 

### 5012 Causeway Blvd • Tampa 

### FI. 33619 • Ph 

### (813)630-7490 • Fax

### (813)630-7360 • DOH 

### #E54272 

### Qualifier Test Analysis Lower Upper Violation PARAMETER Result Units MOL Code Method Analyst Date

## & Time Limit Limit Check HF result, Run4A 

### 100 ug Method26a KASZS 

### 4/26/201012:16:00PM 

## Comments All resultscalculatedon

### awettowet basis, unless otherwise indicated. Data QualifierCodes Explanation: U - Indicatesthatthe compound was analyzed for but not detected. I - The reported value is between the laboratory method detection limit (MOL) and the laboratory practical quantitation limit (POL). POL 4 x MOL. 

### Should there be any questions regarding this report, please contact:

Cheryl Howard, Designeefor Peggy Penner, Manager, Laboratory Services (813) 630-7490

Laboratory Services certifiesthatthe test results in this report meet all reqUirements ofthe NELAC standards, unless indicated otherwise in the body ofthe report. Unless otherwise noted, all methods followed are perthe mostcurrent published version of

### 40 CFR Part 136, Table B. Results reported on this report pertain tothe above referenced sample only.



### Report Number: "GeneralReport" 

### AB07088-083110-09 

### Page 2 of2