# ANALYTICAL REPORT Job Number: 500-53315-1 Job Description: John Deere Des Moines Works (JDDMW) For: Project Integration, Inc 1097 Highway 101 South Suite D-16 Greer, SC 29651 Attention: Mr. Robert Stevens

_____________________________________________Approved for release. Donna L Ingersoll Project Manager II 1/3/2013 4:44 PM 

# Donna L Ingersoll Project Manager II donna.ingersoll@testamericainc.com

01/03/2013

cc:Mr. David Kirby Mr. Robert Malcomson 

## These test results meet all the requirements of NELAC for accredited parameters. The Lab Certification ID# is 100201.
All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be reproduced only in its entirety.
Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street, University Park, IL 60484 Tel (708) 534-5200 Fax (708) 534-5211www.testamericainc.com 

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# Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 5 Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 6 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 9 Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 10 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 13 Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 15 Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 16 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 32 QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 35 Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 60 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 61 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 68 Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 75 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 99 Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .100 GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 100 Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 100 Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 101 Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 124 Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 130 Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 130 Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 160 Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 181 Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 181

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# Table of Contents
Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 184 Method 8260B MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 187 Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 189 Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 195 Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .198 Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 198 Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 199 Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 200 Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 205 Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 205 Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 216 Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 220 Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 234 Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 242 Met Dup/Trip . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 246 Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 248 Met Serial Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 254 Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 255 Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 267 Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 270 Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 276 Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 286 General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 294 Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 295 Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 296 Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 301

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# Table of Contents
Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 301 Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 305 Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 306 Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 310 Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 312 Gen Chem Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 330 Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 332 Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 340 Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 355 Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . .377 Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 382 Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

# 383

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### Job Narrative 500-53315-1 Comments 

### No additional comments. Receipt 

### The samples were received on 12/15/2012 9:10 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 2.7o C. GC/MS VOA 

### Method(s) 8260B:Due to the high concentration of Acetone, the matrix spike / matrix spike duplicate (3MS/3MSD) for sample -3 could not be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria. Method(s) 8260B: One internal standard response was outside of acceptance limits for the following samples:FC D DISCRETE 4 (500-53315-4), FC DISCRETE 4 (500-53315-3). The samples were re- analyzed at a dilution for Acetone. All internal standard area responses were within limits in the diluted runs. Both sets of data have been provided. No other analytical or quality issues were noted. Metals 

### Method(s) 6010B: The serial dilution performed for the following sample, 500-53315-1, was outside control limits for Ci,Ni,Pb,V-, and Zn. Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-53315-1 were outside control limits for Zn. The associated laboratory control sample (LCS) recovery met acceptance criteria. Method(s) 7470A: The matrix spike duplicate (MSD) recovery for sample 500-53315-6 was outside control limits for Hg. The associated laboratory control sample (LCS) recovery met acceptance criteria. No other analytical or quality issues were noted. General Chemistry 

### No analytical or quality issues were noted.



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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53315-1

Instrument ID: Analysis Batch Number: CMS16 170196 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD1 500-170196/6 IC 16I1119A.D 11/19/12 12:14 GC Column:DB624 ID:0.2(mm)

Acetone Poor chromatography wernerb 11/19/12 13:19 1.91

8260B 

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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53315-1

Instrument ID: Analysis Batch Number: CMS25 169636 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD3 500-169636/4 IC 25I1114c.D 11/14/12 10:29 GC Column: ID:

Acetonitrile Poor chromatography arndtb 11/14/12 10:48 2.17 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD4 500-169636/5 IC 25I1114d.D 11/14/12 10:53 GC Column: ID:

Acetone Poor chromatography arndtb 11/14/12 11:34 1.95 Acetonitrile Peak Tail arndtb 11/14/12 11:19 2.17 2-Butanone (MEK) Poor chromatography arndtb 11/14/12 11:35 3.03 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD5 500-169636/6 IC 25I1114e.D 11/14/12 11:18 GC Column: ID:

Bromomethane Peak Tail arndtb 11/14/12 11:58 1.36 Acetonitrile Peak Tail arndtb 11/14/12 11:35 2.17

8260B 

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### Lab Name: Job No.: SDG No.: GC/MS VOA MANUAL INTEGRATION SUMMARY
TestAmerica Chicago 500-53315-1

Instrument ID: Analysis Batch Number: CMS25 169637 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD3 500-169637/4 IC 25I1114c.D 11/14/12 10:29 GC Column: ID:

Acetonitrile Poor chromatography arndtb 11/14/12 10:48 2.17 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD4 500-169637/5 IC 25I1114d.D 11/14/12 10:53 GC Column: ID:

Acetone Poor chromatography arndtb 11/14/12 11:34 1.95 Acetonitrile Peak Tail arndtb 11/14/12 11:19 2.17 2-Butanone (MEK) Poor chromatography arndtb 11/14/12 11:35 3.03 Lab Sample ID: Client Sample ID: Date Analyzed: Lab File ID: COMPOUND NAME RETENTION TIME MANUAL INTEGRATION DATE ANALYST REASON STD5 500-169637/6 IC 25I1114e.D 11/14/12 11:18 GC Column: ID:

Bromomethane Peak Tail arndtb 11/14/12 11:58 1.36 Acetonitrile Peak Tail arndtb 11/14/12 11:35 2.17

8260B 

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## SAMPLE SUMMARY Client: Project Integration, Inc Job Number: 500-53315-1
Client Sample ID Lab Sample ID Client Matrix Sampled Received Date/Time Date/Time
500-53315-1 FC COMPOSITE 4 Solid 12/14/2012 1515 12/15/2012 0910 500-53315-2 FC D COMPOSITE 4 Solid 12/14/2012 1515 12/15/2012 0910 500-53315-3 FC DISCRETE 4 Solid 12/14/2012 1445 12/15/2012 0910 500-53315-4 FC D DISCRETE 4 Solid 12/14/2012 1445 12/15/2012 0910 500-53315-5 TRIP BLANK Water 12/14/2012 0000 12/15/2012 0910 500-53315-6 FC EB 4 Water 12/14/2012 1430 12/15/2012 0910

TestAmerica Chicago 

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## EXECUTIVE SUMMARY- Detections Client: Project Integration, Inc Job Number: 500-53315-1

Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier

500-53315-1 FC COMPOSITE 4 

### 3.70 mg/Kg 6010B 346 Barium 3.70 mg/Kg 6010B 834 Copper 3.70 mg/Kg 6010B 14400 V Chromium 3.70 mg/Kg 6010B 89.8 V Nickel 1.85 mg/Kg 6010B 209 B V Lead 1.85 mg/Kg 6010B 241 V Vanadium 7.41 mg/Kg 6010B 481 V Zinc 0.0595 mg/Kg 7471A 0.543 Mercury 40.0 Degrees F 1010 >176 Flashpoint 3.85 mg/Kg 7196A 3.97 Chromium, hexavalent 1.91 mg/Kg 9014 0.745 J B Cyanide,Total 93.3 mg/Kg 9034 739 Sulfide 0.200 SU 9045C 9.50 pH 1880 mg/Kg 9071B 11100 HEM (Oil & Grease) 0.10 % Moisture 74 Percent Moisture 0.10 % Moisture 26 Percent Solids 0.100 % SM 2540G 74.0 % Moisture 0.100 % SM 2540G 26.0 Total Solids 

### TCLP 0.500 mg/L 6010B 0.0194 J Barium 0.0250 mg/L 6010B 0.0487 Copper 0.0250 mg/L 6010B 0.0549 Nickel

TestAmerica Chicago 

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## EXECUTIVE SUMMARY- Detections Client: Project Integration, Inc Job Number: 500-53315-1

Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier
500-53315-2 FC D COMPOSITE 4 

### 3.46 mg/Kg 6010B 326 Barium 3.46 mg/Kg 6010B 784 Copper 3.46 mg/Kg 6010B 13200 Chromium 3.46 mg/Kg 6010B 86.4 Nickel 1.73 mg/Kg 6010B 188 B Lead 1.73 mg/Kg 6010B 221 Vanadium 6.92 mg/Kg 6010B 451 Zinc 0.0628 mg/Kg 7471A 0.248 Mercury 40.0 Degrees F 1010 >176 Flashpoint 3.76 mg/Kg 7196A 4.08 Chromium, hexavalent 1.66 mg/Kg 9014 0.765 J B Cyanide,Total 90.8 mg/Kg 9034 774 Sulfide 0.200 SU 9045C 9.58 pH 1830 mg/Kg 9071B 8910 HEM (Oil & Grease) 0.10 % Moisture 74 Percent Moisture 0.10 % Moisture 26 Percent Solids 0.100 % SM 2540G 74.0 % Moisture 0.100 % SM 2540G 26.0 Total Solids 

### TCLP 0.0250 mg/L 6010B 0.0483 Copper 0.0250 mg/L 6010B 0.0120 J Chromium 0.0250 mg/L 6010B 0.0582 Nickel

500-53315-3 FC DISCRETE 4 

### 864 ug/Kg 8260B 4220 Acetone 17.3 ug/Kg 8260B 145 2-Butanone (MEK) 0.10 % Moisture 71 Percent Moisture 0.10 % Moisture 29 Percent Solids

500-53315-4 FC D DISCRETE 4 

### 888 ug/Kg 8260B 8710 Acetone 17.8 ug/Kg 8260B 191 2-Butanone (MEK) 0.10 % Moisture 72 Percent Moisture 0.10 % Moisture 28 Percent Solids

TestAmerica Chicago 

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## EXECUTIVE SUMMARY- Detections Client: Project Integration, Inc Job Number: 500-53315-1

Analyte Result Reporting Limit Units Method Lab Sample ID Client Sample ID Qualifier
500-53315-6 FC EB 4 

### 5.00 ug/L 8260B 13.0 2-Butanone (MEK) 0.0100 mg/L 6010B 0.000580 J B Barium 0.0100 mg/L 6010B 0.00303 J Copper 0.0100 mg/L 6010B 0.00312 J B Chromium 0.00500 mg/L 6010B 0.00214 J B Lead 0.0200 mg/L 6010B 0.00724 J Zinc 0.000200 mg/L 7470A 0.000102 J Mercury

TestAmerica Chicago 

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## METHOD SUMMARY Client: Project Integration, Inc Job Number: 500-53315-1 Preparation Method Method Lab Location Description Matrix:Solid 

### Volatile Organic Compounds(GC/MS) TAL CHI SW846 8260B Purge andTrap TAL CHI SW846 5030B Metals (ICP) TAL CHI SW846 6010B Preparation, Metals TAL CHI SW846 3050B Metals (ICP) TAL CHI SW846 6010B TCLP Extraction TAL CHI SW846 1311 Preparation,Total Metals TAL CHI SW846 3010A Mercury (CVAA) TAL CHI SW846 7470A TCLP Extraction TAL CHI SW846 1311 Preparation, Mercury TAL CHI SW846 7470A Mercury (CVAA) TAL CHI SW846 7471A Preparation, Mercury TAL CHI SW846 7471A Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010 Chromium, Hexavalent TAL CHI SW846 7196A Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A Cyanide TAL CHI SW846 9014 Cyanide, Distillation TAL CHI SW846 9010B Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034 Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B Sulfide, Reactive TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 7.3.4 pH TAL CHI SW846 9045C HEM and SGT-HEM TAL CHI SW846 9071B Preparation, HEM and SGT-HEM TAL CHI SW846 9071B Percent Moisture TAL CHI EPA Moisture Total, Fixed,andVolatile Solids TAL CHI SM SM 2540G Matrix:Water 

### Volatile Organic Compounds(GC/MS) TAL CHI SW846 8260B Purge andTrap TAL CHI SW846 5030B Metals (ICP) TAL CHI SW846 6010B Preparation,Total Metals TAL CHI SW846 3010A Mercury (CVAA) TAL CHI SW846 7470A Preparation, Mercury TAL CHI SW846 7470A HEM and SGT-HEM TAL CHI 1664A1664A HEM and SGT-HEM (SPE) TAL CHI 1664A1664A Chromium, Hexavalent TAL CHI SW846 7196A Cyanide TAL CHI SW846 9014 Cyanide, Distillation TAL CHI SW846 9010B Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 9034 Sulfide, Reactive TAL CHI SW846 7.3.4 TestAmerica Chicago 

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## METHOD SUMMARY Client: Project Integration, Inc Job Number: 500-53315-1 Preparation Method Method Lab Location Description Lab References: TAL CHI=TestAmerica Chicago 

### Method References: 1664A=EPA-821-98-002 EPA=US Environmental ProtectionAgency SM = "Standard Methods For The Examination Of Water And Wastewater " SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago 

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## METHOD /ANALYST SUMMARY Client: Project Integration, Inc Job Number: 500-53315-1

Method Analyst Analyst ID Arndt, Brett D BDA SW846 8260B Werner, Brian D BDW SW846 8260B Smith,Todd D TDS SW846 6010B Bills, Brandon J BJB SW846 7470A Bills, Brandon J BJB SW846 7471A Wasowicz, Andrew P APW SW846 1010 Brogan,MaryT MTB 1664A1664A Wasowicz, Andrew P APW SW846 7196A Treadwell,ElianeA EAT SW846 9014 Boyd, Cheryl L CLB SW846 9034 Moore, Colleen L CLM SW846 9034 Moore, Colleen L CLM SW846 9045C Brogan,MaryT MTB SW846 9071B Veldhuizen, Chris M CMV EPA Moisture Veldhuizen, Chris M CMV SM SM 2540G

TestAmerica Chicago 

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC DISCRETE 4


### Client Matrix: % Moisture: 71.1 500-53315-3 Solid Date Sampled: 12/14/2012 1445 Date Received: 12/15/2012 0910 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/18/2012 0930 12/18/2012 0930 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53315-03.D 5 g 5 mL 5030B CMS16
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173225 N/A Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 145 17.3 6.25 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 116 70 - 134 1,2-Dichloroethane-d4 (Surr) 98 75 - 122 Toluene-d8 (Surr) 91 70 - 122 4-Bromofluorobenzene (Surr) 113 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC DISCRETE 4


### Client Matrix: % Moisture: 71.1 500-53315-3 Solid Date Sampled: 12/14/2012 1445 Date Received: 12/15/2012 0910 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/18/2012 0745 12/20/2012 0216 50 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53315-03.D 5 g 5 mL RunType: DL 5030B CMS25
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173509 500-173238 Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 4220 864 225 Acetone Surrogate %Rec Acceptance Limits Qualifier 109 75 - 125 1,2-Dichloroethane-d4 (Surr) 97 75 - 120 Toluene-d8 (Surr) 91 75 - 120 4-Bromofluorobenzene (Surr) 105 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC D DISCRETE 4


### Client Matrix: % Moisture: 71.8 500-53315-4 Solid Date Sampled: 12/14/2012 1445 Date Received: 12/15/2012 0910 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/18/2012 1040 12/18/2012 1040 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53315-04.D 5 g 5 mL 5030B CMS16
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173225 N/A Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 191 17.8 6.43 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 117 70 - 134 1,2-Dichloroethane-d4 (Surr) 97 75 - 122 Toluene-d8 (Surr) 85 70 - 122 4-Bromofluorobenzene (Surr) 112 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC D DISCRETE 4


### Client Matrix: % Moisture: 71.8 500-53315-4 Solid Date Sampled: 12/14/2012 1445 Date Received: 12/15/2012 0910 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/18/2012 0745 12/20/2012 0240 50 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53315-04.D 5 g 5 mL RunType: DL 5030B CMS25
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173509 500-173238 Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL 8710 888 231 Acetone Surrogate %Rec Acceptance Limits Qualifier 119 75 - 125 1,2-Dichloroethane-d4 (Surr) 93 75 - 120 Toluene-d8 (Surr) 90 75 - 120 4-Bromofluorobenzene (Surr) 116 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: TRIP BLANK


### Client Matrix: 500-53315-5 Water Date Sampled: 12/14/2012 0000 Date Received: 12/15/2012 0910 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/20/2012 0108 12/20/2012 0108 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53315-05.D 5 mL 5 mL 5030B CMS25
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173508 N/A Analysis Method: Prep Method:

Analyte Result (ug/L) Qualifier MDL RL <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 105 75 - 125 1,2-Dichloroethane-d4 (Surr) 100 75 - 120 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 109 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC EB 4


### Client Matrix: 500-53315-6 Water Date Sampled: 12/14/2012 1430 Date Received: 12/15/2012 0910 8260BVolatile Organic Compounds(GC/MS)



### Dilution: 12/20/2012 0149 12/20/2012 0149 1.0 8260B

FinalWeight /Volume: InitialWeight /Volume: Lab File ID: Instrument ID: 53315-06.D 5 mL 5 mL 5030B CMS25
Analysis Date: Prep Date: Analysis Batch: Prep Batch: 500-173508 N/A Analysis Method: Prep Method:

Analyte Result (ug/L) Qualifier MDL RL <5.00 5.00 1.29 Acetone 13.0 5.00 1.47 2-Butanone (MEK) Surrogate %Rec Acceptance Limits Qualifier 107 75 - 125 1,2-Dichloroethane-d4 (Surr) 99 75 - 120 Toluene-d8 (Surr) 94 75 - 120 4-Bromofluorobenzene (Surr) 107 75 - 120 Dibromofluoromethane

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC COMPOSITE 4


### Client Matrix: % Moisture: 74.1 500-53315-1 Solid Date Sampled: 12/14/2012 1515 Date Received: 12/15/2012 0910 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51217B Dilution: 1.0 InitialWeight /Volume: 1.0407 g 12/17/2012 2246 FinalWeight /Volume: 100 mL 12/17/2012 0850 3050B ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173224 500-173139 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 346 3.70 0.441 Barium 834 3.70 1.00 Copper 14400 V 3.70 0.618 Chromium 89.8 V 3.70 0.811 Nickel 209 B V 1.85 0.637 Lead 241 V 1.85 0.281 Vanadium 481 V 7.41 2.54 Zinc
6010B Metals (ICP)-TCLP 

### 6010B Instrument ID: Lab File ID: P51219B Dilution: 1.0 InitialWeight /Volume: 50 mL 12/19/2012 2229 FinalWeight /Volume: 50 mL 12/19/2012 0820 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173518 500-173406 500-173187 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/17/2012 1245 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL 0.0194 J 0.500 0.0100 Barium 0.0487 0.0250 0.0100 Copper <0.0250 0.0250 0.0100 Chromium 0.0549 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

7470A Mercury(CVAA)-TCLP 

### 7470A Instrument ID: Lab File ID: 121912RB.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/19/2012 1024 FinalWeight /Volume: 25 mL 12/18/2012 1300 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173438 500-173264 500-173187 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/17/2012 1245 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.000200 0.000200 0.0000200 Mercury

7471A Mercury(CVAA)

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC COMPOSITE 4


### Client Matrix: % Moisture: 74.1 500-53315-1 Solid Date Sampled: 12/14/2012 1515 Date Received: 12/15/2012 0910 7471A Mercury(CVAA) 

### 7471A Instrument ID: Lab File ID: 121812C.PRN Dilution: 1.0 InitialWeight /Volume: 0.6494 g 12/18/2012 1400 FinalWeight /Volume: 50 mL 12/17/2012 1400 7471A HG5
Analysis Date: Prep Date: Analysis Batch: 500-173328 500-173153 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 0.543 0.0595 0.0227 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC D COMPOSITE 4


### Client Matrix: % Moisture: 73.7 500-53315-2 Solid Date Sampled: 12/14/2012 1515 Date Received: 12/15/2012 0910 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51217B Dilution: 1.0 InitialWeight /Volume: 1.0994 g 12/17/2012 2317 FinalWeight /Volume: 100 mL 12/17/2012 0850 3050B ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173224 500-173139 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 326 3.46 0.411 Barium 784 3.46 0.937 Copper 13200 3.46 0.577 Chromium 86.4 3.46 0.757 Nickel 188 B 1.73 0.595 Lead 221 1.73 0.262 Vanadium 451 6.92 2.37 Zinc
6010B Metals (ICP)-TCLP 

### 6010B Instrument ID: Lab File ID: P51219B Dilution: 1.0 InitialWeight /Volume: 50 mL 12/19/2012 2235 FinalWeight /Volume: 50 mL 12/19/2012 0820 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173518 500-173406 500-173187 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/17/2012 1245 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.500 0.500 0.0100 Barium 0.0483 0.0250 0.0100 Copper 0.0120 J 0.0250 0.0100 Chromium 0.0582 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

7470A Mercury(CVAA)-TCLP 

### 7470A Instrument ID: Lab File ID: 121912RB.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/19/2012 1029 FinalWeight /Volume: 25 mL 12/18/2012 1300 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173438 500-173264 500-173187 Prep Batch: Analysis Method: Prep Method: Leach Batch:

12/17/2012 1245 Leach Date: Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL <0.000200 0.000200 0.0000200 Mercury

7471A Mercury(CVAA)

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC D COMPOSITE 4


### Client Matrix: % Moisture: 73.7 500-53315-2 Solid Date Sampled: 12/14/2012 1515 Date Received: 12/15/2012 0910 7471A Mercury(CVAA) 

### 7471A Instrument ID: Lab File ID: 121812C.PRN Dilution: 1.0 InitialWeight /Volume: 0.6068 g 12/18/2012 1401 FinalWeight /Volume: 50 mL 12/17/2012 1400 7471A HG5
Analysis Date: Prep Date: Analysis Batch: 500-173328 500-173153 Prep Batch: Analysis Method: Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL 0.248 0.0628 0.0239 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1 Client Sample ID: 

### Lab Sample ID: FC EB 4


### Client Matrix: 500-53315-6 Water Date Sampled: 12/14/2012 1430 Date Received: 12/15/2012 0910 6010B Metals (ICP) 

### 6010B Instrument ID: Lab File ID: P51219A Dilution: 1.0 InitialWeight /Volume: 50 mL 12/19/2012 1457 FinalWeight /Volume: 50 mL 12/18/2012 1530 3010A ICP5
Analysis Date: Prep Date: Analysis Batch: 500-173517 500-173349 Prep Batch: Analysis Method: Prep Method:

Analyte Result (mg/L) Qualifier MDL RL 0.000580 J B 0.0100 0.000440 Barium 0.00303 J 0.0100 0.00106 Copper 0.00312 J B 0.0100 0.000960 Chromium <0.0100 0.0100 0.00190 Nickel 0.00214 J B 0.00500 0.00158 Lead <0.00500 0.00500 0.000620 Vanadium 0.00724 J 0.0200 0.00472 Zinc

7470A Mercury(CVAA) 

### 7470A Instrument ID: Lab File ID: 121812RB.CSV Dilution: 1.0 InitialWeight /Volume: 25 mL 12/18/2012 0949 FinalWeight /Volume: 25 mL 12/17/2012 1300 7470A HG6
Analysis Date: Prep Date: Analysis Batch: 500-173280 500-173172 Prep Batch: Analysis Method: Prep Method:

Analyte Result (mg/L) Qualifier MDL RL 0.000102 J 0.000200 0.0000710 Mercury

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC COMPOSITE 4


### Client Matrix: 500-53315-1 Solid Date Sampled: 12/14/2012 1515 Date Received: 12/15/2012 0910 Analyte Result Qual Units MDL RL Dil Method Flashpoint >176 Degrees F 40.0 40.0 1.0 1010 DryWt Corrected: N Analysis Date (Start): 12/19/2012 1721 (End) 12/19/2012 1800 

### Analysis Batch: 500-173558 Chromium, hexavalent 3.97 mg/Kg 1.50 3.85 1.0 7196A DryWt Corrected: Y Analysis Date (Start): 12/18/2012 1549 (End) 12/18/2012 1550 

### Analysis Batch: 500-173341 Prep Batch: 500-173258 Prep Date: 12/18/2012 1000 Cyanide,Total 0.745 J B mg/Kg 0.630 1.91 1.0 9014 DryWt Corrected: Y Analysis Date (Start): 12/18/2012 1424 (End) 12/18/2012 1424 

### Analysis Batch: 500-173386 Prep Batch: 500-173250 Prep Date: 12/18/2012 1035 Sulfide 739 mg/Kg 14.9 93.3 1.0 9034 DryWt Corrected: Y Analysis Date: 12/19/2012 1336 Analysis Batch: 500-173474 Prep Batch: 500-173291 Prep Date: 12/19/20121125 Sulfide, Reactive <48.6 mg/Kg 3.79 48.6 1.0 9034 DryWt Corrected: N Analysis Date: 12/19/2012 1218 Analysis Batch: 500-173472 Prep Batch: 500-173290 Prep Date: 12/19/2012 1040 pH 9.50 SU 0.200 0.200 1.0 9045C DryWt Corrected: N Analysis Date (Start): 12/20/2012 1512 (End) 12/20/ 2012 1611 

### Analysis Batch: 500-173479 HEM (Oil & Grease) 11100 mg/Kg 835 1880 1.0 9071B DryWt Corrected: Y Analysis Date: 12/19/20121101 Analysis Batch: 500-173330 Prep Batch: 500-173324 Prep Date: 12/19/2012 0510 Percent Moisture 74 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/15/2012 1243 Analysis Batch: 500-173077 Percent Solids 26 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/15/2012 1243 Analysis Batch: 500-173077 % Moisture 74.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/18/2012 0734 Analysis Batch: 500-173236 Total Solids 26.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/18/2012 0734 Analysis Batch: 500-173236

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC D COMPOSITE 4


### Client Matrix: 500-53315-2 Solid Date Sampled: 12/14/2012 1515 Date Received: 12/15/2012 0910 Analyte Result Qual Units MDL RL Dil Method Flashpoint >176 Degrees F 40.0 40.0 1.0 1010 DryWt Corrected: N Analysis Date (Start): 12/19/2012 1800 (End) 12/19/2012 1840 

### Analysis Batch: 500-173558 Chromium, hexavalent 4.08 mg/Kg 1.46 3.76 1.0 7196A DryWt Corrected: Y Analysis Date (Start): 12/18/2012 1550 (End) 12/18/2012 1550 

### Analysis Batch: 500-173341 Prep Batch: 500-173258 Prep Date: 12/18/2012 1000 Cyanide,Total 0.765 J B mg/Kg 0.549 1.66 1.0 9014 DryWt Corrected: Y Analysis Date (Start): 12/18/2012 1424 (End) 12/18/2012 1425 

### Analysis Batch: 500-173386 Prep Batch: 500-173250 Prep Date: 12/18/2012 1035 Sulfide 774 mg/Kg 14.5 90.8 1.0 9034 DryWt Corrected: Y Analysis Date: 12/19/2012 1337 Analysis Batch: 500-173474 Prep Batch: 500-173291 Prep Date: 12/19/20121125 Sulfide, Reactive <49.3 mg/Kg 3.85 49.3 1.0 9034 DryWt Corrected: N Analysis Date: 12/19/2012 1219 Analysis Batch: 500-173472 Prep Batch: 500-173290 Prep Date: 12/19/2012 1045 pH 9.58 SU 0.200 0.200 1.0 9045C DryWt Corrected: N Analysis Date (Start): 12/20/ 2012 1611(End) 12/20/2012 1710 

### Analysis Batch: 500-173479 HEM (Oil & Grease) 8910 mg/Kg 811 1830 1.0 9071B DryWt Corrected: Y Analysis Date: 12/19/20121112 Analysis Batch: 500-173330 Prep Batch: 500-173324 Prep Date: 12/19/2012 0510 Percent Moisture 74 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/15/2012 1243 Analysis Batch: 500-173077 Percent Solids 26 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/15/2012 1243 Analysis Batch: 500-173077 % Moisture 74.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/18/2012 0734 Analysis Batch: 500-173236 Total Solids 26.0 % 0.100 0.100 1.0 SM 2540G DryWt Corrected: N Analysis Date: 12/18/2012 0734 Analysis Batch: 500-173236

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC DISCRETE 4


### Client Matrix: 500-53315-3 Solid Date Sampled: 12/14/2012 1445 Date Received: 12/15/2012 0910 Analyte Result Qual Units MDL RL Dil Method Percent Moisture 71 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/18/2012 1359 Analysis Batch: 500-173311 Percent Solids 29 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/18/2012 1359 Analysis Batch: 500-173311

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## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC D DISCRETE 4


### Client Matrix: 500-53315-4 Solid Date Sampled: 12/14/2012 1445 Date Received: 12/15/2012 0910 Analyte Result Qual Units MDL RL Dil Method Percent Moisture 72 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/18/2012 1359 Analysis Batch: 500-173311 Percent Solids 28 % 0.10 0.10 1.0 Moisture DryWt Corrected: N Analysis Date: 12/18/2012 1359 Analysis Batch: 500-173311

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## 01/03/2013 Page 30 of 383

## Analytical Data Client: Project Integration, Inc Job Number: 500-53315-1
General Chemistry Client Sample ID: 

### Lab Sample ID: FC EB 4


### Client Matrix: 500-53315-6 Water Date Sampled: 12/14/2012 1430 Date Received: 12/15/2012 0910 Analyte Result Qual Units MDL RL Dil Method HEM (Oil & Grease) <5.20 mg/L 1.51 5.20 1.0 1664A Analysis Date: 12/18/20121114 Analysis Batch: 500-173178 Prep Batch: 500-173173 Prep Date: 12/18/2012 0724 Chromium, hexavalent <0.0100 mg/L 0.00325 0.0100 1.0 7196A Analysis Date (Start): 12/15/2012 1322 (End) 12/15/2012 1322 

### Analysis Batch: 500-173079 Cyanide,Total <0.0100 mg/L 0.00331 0.0100 1.0 9014 Analysis Date (Start): 12/18/2012 1354 (End) 12/18/2012 1354 

### Analysis Batch: 500-173387 Prep Batch: 500-173245 Prep Date: 12/18/2012 0830 Sulfide <1.00 mg/L 0.230 1.00 1.0 9034 Analysis Date (Start): 12/17/ 2012 0111(End) 12/17/2012 0114 

### Analysis Batch: 500-173108 Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034 Analysis Date: 12/17/2012 0108 Analysis Batch: 500-173107 Prep Batch: 500-173106 Prep Date: 12/17/2012 0013

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## 01/03/2013 Page 31 of 383

## Quality Control Results Job Number: 500-53315-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix: Solid 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53315-3 FC DISCRETE 4 113 116 98 91 500-53315-4 FC D DISCRETE 4 112 117 97 85 MB 500-173225/4 106 106 113 104 LCS 500-173225/5 105 104 111 103 500-53315-3 MS FC DISCRETE 4 MS 118 117 95 85 500-53315-3 MSD FC DISCRETE 4 MSD 116 119 96 84

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 70-134 TOL=Toluene-d8 (Surr) 75-122 BFB = 4-Bromofluorobenzene (Surr) 70-122

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## 01/03/2013 Page 32 of 383

## Quality Control Results Job Number: 500-53315-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix: Solid 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53315-3 DL FC DISCRETE 4 DL 105 109 97 91 500-53315-4 DL FC D DISCRETE 4 DL 116 119 93 90 MB 500-173509/6 96 101 95 94 LCS 500-173509/4 98 102 97 99

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 75-125 TOL=Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

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## 01/03/2013 Page 33 of 383

## Quality Control Results Job Number: 500-53315-1 Client: Project Integration, Inc 

## Surrogate Recovery Report 8260BVolatile Organic Compounds(GC/MS)
Client Matrix:Water 

### Lab Sample ID Client Sample ID DBFM DCA TOL BFB %Rec %Rec %Rec %Rec 500-53315-5 TRIP BLANK 109 105 100 97 500-53315-6 FC EB 4 107 107 99 94 MB 500-173508/6 96 101 95 94 LCS 500-173508/4 98 102 97 99

Surrogate Acceptance Limits DBFM = Dibromofluoromethane 75-120 DCA= 1,2-Dichloroethane-d4 (Surr) 75-125 TOL=Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

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## 01/03/2013 Page 34 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173225

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 16M1218.D 5 g 5 mL Units: ug/Kg 

### Method: 8260B Preparation: 5030B
CMS16 MB 500-173225/4
Analysis Date: 12/18/2012 0830 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173225

Prep Date: Leach Date: 12/18/2012 0830 N/A Analyte RL MDL Qual Result <5.00 5.00 2.16 Acetone <5.00 5.00 1.81 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 106 70 - 134 Toluene-d8 (Surr) 113 75 - 122 4-Bromofluorobenzene (Surr) 104 70 - 122 Dibromofluoromethane 106 75 - 120

Solid 1.0 

### Lab Control Sample - Batch: 500-173225

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 16S1218.D 5 g 5 mL Units: ug/Kg 

### Method: 8260B Preparation: 5030B
CMS16 LCS 500-173225/5
Analysis Date: 12/18/2012 0853 Analysis Batch: Prep Batch: Leach Batch: 500-173225 N/A N/A Prep Date: Leach Date: 12/18/2012 0853 N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 45.56 91 50 - 138 Acetone 50.0 52.85 106 58 - 133 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 104 70 - 134 Toluene-d8 (Surr) 111 75 - 122 4-Bromofluorobenzene (Surr) 103 70 - 122 Dibromofluoromethane 105 75 - 120

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## 01/03/2013 Page 35 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Dilution: Dilution: Solid 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Solid 53315-03s.D 5 g 5 mL

53315-03t.D 5 g 5 mL 

### Method: 8260B Preparation: 5030B

CMS16

CMS16 500-53315-3

500-53315-3 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173225

12/18/2012 0954 N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173225 N/A N/A

Analysis Date: Prep Date: Leach Date: 12/18/2012 1017 12/18/2012 1017 N/A Analysis Batch: Prep Batch: Leach Batch: 500-173225 N/A N/A 12/18/2012 0954

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 104 399 50 - 138 7 30 E 4 E 4 Acetone 106 91 58 - 133 8 30 2-Butanone (MEK) Surrogate Acceptance Limits MS % Rec MSD % Rec 1,2-Dichloroethane-d4 (Surr) 117 119 70 - 134 Toluene-d8 (Surr) 95 96 75 - 122 4-Bromofluorobenzene (Surr) 85 84 70 - 122 Dibromofluoromethane 118 116 75 - 120

Solid 12/18/2012 0954 12/18/2012 1017 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Solid 

### Method: 8260B Preparation: 5030B

Units:ug/Kg 500-53315-3 500-53315-3 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173225

Analysis Date: Prep Date: Leach Date: 12/18/2012 0954 N/A Analysis Date: Prep Date: Leach Date: 12/18/2012 1017 N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
6940 173 173 7120 7629 E 4 E 4 Acetone 145 173 173 329.3 303.4 2-Butanone (MEK)

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## 01/03/2013 Page 36 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173508

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 25M1219p.D 5 mL 5 mL Units: ug/L 

### Method: 8260B Preparation: 5030B
CMS25 MB 500-173508/6
Analysis Date: 12/20/2012 0043 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173508

Prep Date: Leach Date: 12/20/2012 0043 N/A Analyte RL MDL Qual Result <5.00 5.00 1.29 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 101 75 - 125 Toluene-d8 (Surr) 95 75 - 120 4-Bromofluorobenzene (Surr) 94 75 - 120 Dibromofluoromethane 96 75 - 120

Water 1.0 

### Lab Control Sample - Batch: 500-173508

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 25S1219p.D 5 mL 5 mL Units: ug/L 

### Method: 8260B Preparation: 5030B
CMS25 LCS 500-173508/4
Analysis Date: 12/19/2012 2354 Analysis Batch: Prep Batch: Leach Batch: 500-173508 N/A N/A Prep Date: Leach Date: 12/19/2012 2354 N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 52.35 105 46 - 153 Acetone 50.0 53.39 107 54 - 138 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 102 75 - 125 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 99 75 - 120 Dibromofluoromethane 98 75 - 120

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## 01/03/2013 Page 37 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173509

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 25M1219p.D Units: ug/Kg 

### Method: 8260B Preparation: N/A
CMS25 MB 500-173509/6
Analysis Date: 12/20/2012 0043 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173509

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <5.00 5.00 1.30 Acetone <5.00 5.00 1.47 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 101 75 - 125 Toluene-d8 (Surr) 95 75 - 120 4-Bromofluorobenzene (Surr) 94 75 - 120 Dibromofluoromethane 96 75 - 120

Solid 1.0 

### Lab Control Sample - Batch: 500-173509

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 25S1219p.D Units: ug/Kg 

### Method: 8260B Preparation: N/A
CMS25 LCS 500-173509/4
Analysis Date: 12/19/2012 2354 Analysis Batch: Prep Batch: Leach Batch: 500-173509 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 50.0 52.35 105 46 - 153 Acetone 50.0 53.39 107 54 - 138 2-Butanone (MEK) Surrogate % Rec Acceptance Limits 1,2-Dichloroethane-d4 (Surr) 102 75 - 125 Toluene-d8 (Surr) 97 75 - 120 4-Bromofluorobenzene (Surr) 99 75 - 120 Dibromofluoromethane 98 75 - 120

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## 01/03/2013 Page 38 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173139

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51217B 1 g 100 mL Units: mg/Kg 

### Method: 6010B Preparation: 3050B
ICP5 MB 500-173139/1-A
Analysis Date: 12/17/2012 2104 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173224 500-173139
Prep Date: Leach Date: 12/17/2012 0850 N/A Analyte RL MDL Qual Result <1.00 1.00 0.119 Barium <1.00 1.00 0.271 Copper <1.00 1.00 0.167 Chromium <1.00 1.00 0.219 Nickel 0.2420 J 0.500 0.172 Lead <0.500 0.500 0.0759 Vanadium <2.00 2.00 0.686 Zinc

Solid 1.0 

### Lab Control Sample - Batch: 500-173139

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51217B 1 g 100 mL Units: mg/Kg 

### Method: 6010B Preparation: 3050B
ICP5 LCS 500-173139/2-A
Analysis Date: 12/17/2012 2110 Analysis Batch: Prep Batch: Leach Batch: 500-173224 500-173139 N/A Prep Date: Leach Date: 12/17/2012 0850 N/A Analyte Qual Limit % Rec. Result SpikeAmount 200 197.2 99 80 - 120 Barium 25.0 24.95 100 80 - 120 Copper 20.0 19.91 100 80 - 120 Chromium 50.0 49.11 98 80 - 120 Nickel 10.0 10.07 101 80 - 120 Lead 50.0 49.74 99 80 - 120 Vanadium 50.0 48.83 98 80 - 120 Zinc

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## 01/03/2013 Page 39 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Dilution: Dilution: Solid 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Solid P51217B 1.0117g 100 mL

P51217B 1.0566 g 100 mL 

### Method: 6010B Preparation: 3050B

ICP5

ICP5 500-53315-1

500-53315-1 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173139

12/17/2012 2304 N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173224 500-173139 N/A

Analysis Date: Prep Date: Leach Date: 12/17/2012 2310 12/17/2012 0850 N/A Analysis Batch: Prep Batch: Leach Batch: 500-173224 500-173139 N/A 12/17/2012 0850

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 84 82 75 - 125 4 20 Barium 2 -38 75 - 125 4 20 4 4 Copper

-1125 -1577 75 - 125 2 20 4 4 Chromium 82 81 75 - 125 4 20 Nickel 116 12 75 - 125 17 20 4 4 Lead 79 76 75 - 125 3 20 Vanadium 65 65 75 - 125 1 20 F F Zinc

Solid 12/17/2012 2304 12/17/2012 2310 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Solid 

### Method: 6010B Preparation: 3050B

Units:mg/Kg 500-53315-1 500-53315-1 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173139

Analysis Date: Prep Date: Leach Date: 12/17/2012 0850 N/A Analysis Date: Prep Date: Leach Date: 12/17/2012 0850 N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
346 762 729 987.2 943.9 Barium 834 95.2 91.2 836.2 799.8 4 4 Copper 14400 76.2 72.9 13510 13220 4 4 Chromium 89.8 190 182 246.8 237.5 Nickel 209 38.1 36.5 253.1 213.5 4 4 Lead 241 190 182 391.8 379.3 Vanadium 481 190 182 605.1 600.3 F F Zinc

TestAmerica Chicago 

## 01/03/2013 Page 40 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

mg/Kg Units: Solid Dilution: 5.0 

### Serial Dilution - Batch: 500-173139
Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51217B 1.0407 g 100 mL 

### Method: 6010B Preparation: 3050B
ICP5 500-53315-1
Analysis Date: 12/17/2012 2252 Analysis Batch: Prep Batch: Leach Batch: 500-173224 500-173139 N/A Prep Date: Leach Date: 12/17/2012 0850 N/A Analyte Sample Result/Qual Result Limit Qual %Diff Barium 346 377.6 9.2 10 Copper 834 868.4 4.1 10 Chromium 14400 16720 V 16 10 Nickel 89.8 102.4 V 14 10 Lead 209 239.4 V 15 10 Vanadium 241 281.4 V 17 10 Zinc 481 576.2 V 20 10

mg/Kg Units: Solid Dilution: 1.0 

### Duplicate - Batch: 500-173139
Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51217B 1.0334 g 100 mL 

### Method: 6010B Preparation: 3050B
ICP5 500-53315-1
Analysis Date: 12/17/2012 2258 Analysis Batch: Prep Batch: Leach Batch: 500-173224 500-173139 N/A Prep Date: Leach Date: 12/17/2012 0850 N/A Analyte Qual Limit RPD Result Sample Result/Qual 335.3 346 3 20 Barium 804.0 834 4 20 Copper 13970 14400 3 20 Chromium 88.38 89.8 2 20 Nickel 201.3 209 4 20 Lead 234.5 241 3 20 Vanadium 468.4 481 3 20 Zinc

TestAmerica Chicago 

## 01/03/2013 Page 41 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173349

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219A 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 MB 500-173349/1-A
Analysis Date: 12/19/2012 1352 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173517 500-173349
Prep Date: Leach Date: 12/18/2012 1530 N/A Analyte RL MDL Qual Result 0.002710 J 0.0100 0.000440 Barium <0.0100 0.0100 0.00106 Copper 0.001210 J 0.0100 0.000960 Chromium <0.0100 0.0100 0.00190 Nickel 0.002720 J 0.00500 0.00158 Lead <0.00500 0.00500 0.000620 Vanadium <0.0200 0.0200 0.00472 Zinc

Water 1.0 

### Lab Control Sample - Batch: 500-173349

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219A 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 LCS 500-173349/2-A
Analysis Date: 12/19/2012 1358 Analysis Batch: Prep Batch: Leach Batch: 500-173517 500-173349 N/A Prep Date: Leach Date: 12/18/2012 1530 N/A Analyte Qual Limit % Rec. Result SpikeAmount 2.00 1.955 98 80 - 120 Barium 0.250 0.2524 101 80 - 120 Copper 0.200 0.1989 99 80 - 120 Chromium 0.500 0.4934 99 80 - 120 Nickel 0.100 0.1010 101 80 - 120 Lead 0.500 0.4993 100 80 - 120 Vanadium 0.500 0.4858 97 80 - 120 Zinc

TestAmerica Chicago 

## 01/03/2013 Page 42 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPE Leachate Blank- Batch: 500-173406

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A TCLP ICP5 LB 500-173187/1-D
Analysis Date: 12/19/2012 2107 Analysis Batch: Prep Batch: Leach Batch: 500-173187 500-173518 500-173406
Prep Date: Leach Date: 12/19/2012 0820 12/17/2012 1245 Analyte RL MDL Qual Result <0.500 0.500 0.0100 Barium <0.0250 0.0250 0.0100 Copper <0.0250 0.0250 0.0100 Chromium <0.0250 0.0250 0.0100 Nickel <0.0500 0.0500 0.00500 Lead <0.0250 0.0250 0.00500 Vanadium <0.100 0.100 0.0200 Zinc

Water 1.0 

### Lab Control Sample - Batch: 500-173406

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: P51219B 50 mL 50 mL Units: mg/L 

### Method: 6010B Preparation: 3010A
ICP5 LCS 500-173406/3-A
Analysis Date: 12/19/2012 2120 Analysis Batch: Prep Batch: Leach Batch: 500-173518 500-173406 N/A Prep Date: Leach Date: 12/19/2012 0820 N/A Analyte Qual Limit % Rec. Result SpikeAmount 2.00 1.975 99 80 - 120 Barium 0.250 0.2464 99 80 - 120 Copper 0.200 0.1969 98 80 - 120 Chromium 0.500 0.4873 97 80 - 120 Nickel 0.100 0.09785 98 80 - 120 Lead 0.500 0.4959 99 80 - 120 Vanadium 0.500 0.4782 96 80 - 120 Zinc

TestAmerica Chicago 

## 01/03/2013 Page 43 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173172

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121812RB.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 MB 500-173172/7-A
Analysis Date: 12/18/2012 0909 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173280 500-173172
Prep Date: Leach Date: 12/17/2012 1300 N/A Analyte RL MDL Qual Result <0.000200 0.000200 0.0000710 Mercury

Water 1.0 

### Lab Control Sample - Batch: 500-173172

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121812RB.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 LCS 500-173172/8-A
Analysis Date: 12/18/2012 0911 Analysis Batch: Prep Batch: Leach Batch: 500-173280 500-173172 N/A Prep Date: Leach Date: 12/17/2012 1300 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.00200 0.002027 101 80 - 120 Mercury

Dilution: Dilution: Water 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Water 121812RB.CSV 25 mL 25 mL

121812RB.CSV 25 mL 25 mL 

### Method: 7470A Preparation: 7470A

HG6

HG6 500-53315-6

500-53315-6 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173172

12/18/2012 0957 N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173280 500-173172 N/A

Analysis Date: Prep Date: Leach Date: 12/18/2012 0959 12/17/2012 1300 N/A Analysis Batch: Prep Batch: Leach Batch: 500-173280 500-173172 N/A 12/17/2012 1300

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 86 69 75 - 125 20 20 F Mercury

TestAmerica Chicago 

## 01/03/2013 Page 44 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water 12/18/2012 0957 12/18/2012 0959 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Water 

### Method: 7470A Preparation: 7470A

Units:mg/L 500-53315-6 500-53315-6 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173172

Analysis Date: Prep Date: Leach Date: 12/17/2012 1300 N/A Analysis Date: Prep Date: Leach Date: 12/17/2012 1300 N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
0.000102 J 0.00100 0.00100 0.000960 0.000789 F Mercury

mg/L Units: Water Dilution: 1.0 

### Duplicate - Batch: 500-173172
Lab Sample ID: Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121812RB.CSV 25 mL 25 mL 

### Method: 7470A Preparation: 7470A
HG6 500-53315-6
Analysis Date: 12/18/2012 0955 Analysis Batch: Prep Batch: Leach Batch: 500-173280 500-173172 N/A Prep Date: Leach Date: 12/17/2012 1300 N/A Analyte Qual Limit RPD Result Sample Result/Qual 0.0001082 0.000102 J 6 20 J Mercury

TestAmerica Chicago 

## 01/03/2013 Page 45 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173264

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121912RB.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 MB 500-173264/7-A
Analysis Date: 12/19/2012 1008 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173438 500-173264
Prep Date: Leach Date: 12/18/2012 1300 N/A Analyte RL MDL Qual Result <0.000200 0.000200 0.0000200 Mercury

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### TCLP SPLPE Leachate Blank- Batch: 500-173264

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121912RB.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A TCLP HG6 LB 500-173187/1-B
Analysis Date: 12/19/2012 1012 Analysis Batch: Prep Batch: Leach Batch: 500-173187 500-173438 500-173264
Prep Date: Leach Date: 12/18/2012 1300 12/17/2012 1245 Analyte RL MDL Qual Result <0.000200 0.000200 0.0000200 Mercury

Water 1.0 

### Lab Control Sample - Batch: 500-173264

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121912RB.CSV 25 mL 25 mL Units: mg/L 

### Method: 7470A Preparation: 7470A
HG6 LCS 500-173264/8-A
Analysis Date: 12/19/2012 1010 Analysis Batch: Prep Batch: Leach Batch: 500-173438 500-173264 N/A Prep Date: Leach Date: 12/18/2012 1300 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.00200 0.002002 100 80 - 120 Mercury

TestAmerica Chicago 

## 01/03/2013 Page 46 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173153

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121812C.PRN 0.6 g 50 mL Units: mg/Kg 

### Method: 7471A Preparation: 7471A
HG5 MB 500-173153/7-A
Analysis Date: 12/18/2012 1304 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173328 500-173153
Prep Date: Leach Date: 12/17/2012 1400 N/A Analyte RL MDL Qual Result <0.0167 0.0167 0.00637 Mercury

Solid 1.0 

### Lab Control Sample - Batch: 500-173153

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 121812C.PRN 0.6 g 50 mL Units: mg/Kg 

### Method: 7471A Preparation: 7471A
HG5 LCS 500-173153/8-A
Analysis Date: 12/18/2012 1310 Analysis Batch: Prep Batch: Leach Batch: 500-173328 500-173153 N/A Prep Date: Leach Date: 12/17/2012 1400 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.167 0.1717 103 80 - 120 Mercury

TestAmerica Chicago 

## 01/03/2013 Page 47 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173173

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1000 mL 1000 mL Units: mg/L 

### Method: 1664A Preparation: 1664A

N/A No Equipment MB 500-173173/1-A
Analysis Date: 12/18/2012 1005 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173178 500-173173
Prep Date: Leach Date: 12/18/2012 0525 N/A Analyte RL MDL Qual Result <5.00 5.00 1.45 HEM (Oil & Grease)

Water 1.0 

### Lab Control Sample - Batch: 500-173173

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1000 mL 1000 mL Units: mg/L 

### Method: 1664A Preparation: 1664A

N/A No Equipment LCS 500-173173/2-A
Analysis Date: 12/18/2012 1011 Analysis Batch: Prep Batch: Leach Batch: 500-173178 500-173173 N/A Prep Date: Leach Date: 12/18/2012 0535 N/A Analyte Qual Limit % Rec. Result SpikeAmount 40.0 39.10 98 78 -114 HEM (Oil & Grease)

TestAmerica Chicago 

## 01/03/2013 Page 48 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173079

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 7196A Preparation: N/A

N/A SPEC5 MB 500-173079/3
Analysis Date: 12/15/2012 1321 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173079

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.00325 Chromium, hexavalent

Water 1.0 

### Lab Control Sample - Batch: 500-173079

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 7196A Preparation: N/A

N/A SPEC5 LCS 500-173079/4
Analysis Date: 12/15/2012 1321 Analysis Batch: Prep Batch: Leach Batch: 500-173079 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.250 0.2497 100 85 -115 Chromium, hexavalent

Dilution: Dilution: Water 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Water 

### Method: 7196A Preparation: N/A

N/A

N/A SPEC5

SPEC5 500-53315-6

500-53315-6 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173079

12/15/2012 1322 N/A N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173079 N/A N/A

Analysis Date: Prep Date: Leach Date: 12/15/2012 1323 N/A N/A Analysis Batch: Prep Batch: Leach Batch: 500-173079 N/A N/A

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 100 100 85 -115 0 20 Chromium, hexavalent

TestAmerica Chicago 

## 01/03/2013 Page 49 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water 12/15/2012 1322 12/15/2012 1323 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Water 

### Method: 7196A Preparation: N/A

Units:mg/L 500-53315-6 500-53315-6 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173079

Analysis Date: Prep Date: Leach Date: N/A N/A Analysis Date: Prep Date: Leach Date: N/A N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
<0.0100 0.250 0.250 0.2500 0.2500 Chromium, hexavalent

TestAmerica Chicago 

## 01/03/2013 Page 50 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173258

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 MB 500-173258/1-A
Analysis Date: 12/18/2012 1546 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173341 500-173258
Prep Date: Leach Date: 12/18/2012 1000 N/A Analyte RL MDL Qual Result <1.00 1.00 0.389 Chromium, hexavalent

Solid 1.0 

### Lab Control Sample - Batch: 500-173258

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 LCS 500-173258/2-A
Analysis Date: 12/18/2012 1546 Analysis Batch: Prep Batch: Leach Batch: 500-173341 500-173258 N/A Prep Date: Leach Date: 12/18/2012 1000 N/A Analyte Qual Limit % Rec. Result SpikeAmount 10.0 8.252 83 80 - 120 Chromium, hexavalent

Solid 50 

### Lab Control Sample - Batch: 500-173258

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 2.5 g 100 mL Units: mg/Kg 

### Method: 7196A Preparation: 3060A

N/A SPEC5 LCS 500-173258/3-A
Analysis Date: 12/18/2012 1547 Analysis Batch: Prep Batch: Leach Batch: 500-173341 500-173258 N/A Prep Date: Leach Date: 12/18/2012 1000 N/A Analyte Qual Limit % Rec. Result SpikeAmount 1550 1601 104 80 - 120 Chromium, hexavalent

TestAmerica Chicago 

## 01/03/2013 Page 51 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173245

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 50 mL 50 mL Units: mg/L 

### Method: 9014 Preparation: 9010B

N/A SPEC5 MB 500-173245/1-A
Analysis Date: 12/18/2012 1345 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173387 500-173245
Prep Date: Leach Date: 12/18/2012 0830 N/A Analyte RL MDL Qual Result <0.0100 0.0100 0.00331 Cyanide,Total

Water 1.0 

### Lab Control Sample - Batch: 500-173245

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 50 mL 50 mL Units: mg/L 

### Method: 9014 Preparation: 9010B

N/A SPEC5 LCS 500-173245/2-A
Analysis Date: 12/18/2012 1345 Analysis Batch: Prep Batch: Leach Batch: 500-173387 500-173245 N/A Prep Date: Leach Date: 12/18/2012 0830 N/A Analyte Qual Limit % Rec. Result SpikeAmount 0.100 0.1057 106 80 - 120 Cyanide,Total

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## 01/03/2013 Page 52 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173250

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1.0000 g 50 mL Units: mg/Kg 

### Method: 9014 Preparation: 9010B

N/A SPEC5 MB 500-173250/1-A
Analysis Date: 12/18/2012 1423 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173386 500-173250
Prep Date: Leach Date: 12/18/2012 1035 N/A Analyte RL MDL Qual Result 0.1850 J 0.500 0.165 Cyanide,Total

Solid 1.0 

### Lab Control Sample - Batch: 500-173250

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 1.0000 g 50 mL Units: mg/Kg 

### Method: 9014 Preparation: 9010B

N/A SPEC5 LCS 500-173250/2-A
Analysis Date: 12/18/2012 1423 Analysis Batch: Prep Batch: Leach Batch: 500-173386 500-173250 N/A Prep Date: Leach Date: 12/18/2012 1035 N/A Analyte Qual Limit % Rec. Result SpikeAmount 5.00 5.235 105 80 - 120 Cyanide,Total

Dilution: Dilution: Solid 1.0

1.0 Client Matrix: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume:

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Client Matrix: Solid 1.1473 g 50 mL

1.1489 g 50 mL 

### Method: 9014 Preparation: 9010B

N/A

N/A SPEC5

SPEC5 500-53315-2

500-53315-2 MS Lab Sample ID:

MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173250

12/18/2012 1425 N/A Analysis Date: Prep Date: Leach Date: Analysis Batch: Prep Batch: Leach Batch: 500-173386 500-173250 N/A

Analysis Date: Prep Date: Leach Date: 12/18/2012 1425 12/18/2012 1035 N/A Analysis Batch: Prep Batch: Leach Batch: 500-173386 500-173250 N/A 12/18/2012 1035

Analyte RPD Limit RPD Limit % Rec. MS MSD MS Qual MSD Qual 81 89 75 - 125 8 20 Cyanide,Total

TestAmerica Chicago 

## 01/03/2013 Page 53 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid 12/18/2012 1425 12/18/2012 1425 Dilution: Dilution: 1.0 1.0 Client Matrix: Client Matrix: Solid 

### Method: 9014 Preparation: 9010B

Units:mg/Kg 500-53315-2 500-53315-2 MS Lab Sample ID: MSD Lab Sample ID: 

### Matrix Spike/ Matrix Spike Duplicate Recovery Report - Batch: 500-173250

Analysis Date: Prep Date: Leach Date: 12/18/2012 1035 N/A Analysis Date: Prep Date: Leach Date: 12/18/2012 1035 N/A

Amount Sample Analyte Result/Qual Amount Result/Qual Result/Qual MS MSD MS Spike MSD Spike
0.765 J 6.63 6.62 6.130 6.651 Cyanide,Total

TestAmerica Chicago 

## 01/03/2013 Page 54 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173106

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment MB 500-173106/1-A
Analysis Date: 12/17/2012 0019 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173107 500-173106
Prep Date: Leach Date: 12/17/2012 0001 N/A Analyte RL MDL Qual Result <1.00 1.00 1.00 Sulfide, Reactive

Water 1.0 

### Lab Control Sample - Batch: 500-173106

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 250 mL 250 mL Units: mg/L 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment LCS 500-173106/2-A
Analysis Date: 12/17/2012 0035 Analysis Batch: Prep Batch: Leach Batch: 500-173107 500-173106 N/A Prep Date: Leach Date: 12/17/2012 0005 N/A Analyte Qual Limit % Rec. Result SpikeAmount 3.60 3.292 91 80 - 120 Sulfide, Reactive

TestAmerica Chicago 

## 01/03/2013 Page 55 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Water Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173108

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 9034 Preparation: N/A

N/A No Equipment MB 500-173108/1
Analysis Date: 12/17/2012 0019 Analysis Batch: Prep Batch: Leach Batch: N/A N/A 500-173108

Prep Date: Leach Date: N/A N/A Analyte RL MDL Qual Result <1.00 1.00 0.230 Sulfide

Water 1.0 

### Lab Control Sample - Batch: 500-173108

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: Units: mg/L 

### Method: 9034 Preparation: N/A

N/A No Equipment LCS 500-173108/2
Analysis Date: 12/17/2012 0021 Analysis Batch: Prep Batch: Leach Batch: 500-173108 N/A N/A Prep Date: Leach Date: N/A N/A Analyte Qual Limit % Rec. Result SpikeAmount 3.60 3.286 91 80 - 120 Sulfide

TestAmerica Chicago 

## 01/03/2013 Page 56 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173290

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment MB 500-173290/1-A
Analysis Date: 12/19/2012 1215 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173472 500-173290
Prep Date: Leach Date: 12/19/2012 1005 N/A Analyte RL MDL Qual Result <50.0 50.0 3.90 Sulfide, Reactive

Solid 1.0 

### Lab Control Sample - Batch: 500-173290

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 7.3.4

N/A No Equipment LCS 500-173290/2-A
Analysis Date: 12/19/2012 1215 Analysis Batch: Prep Batch: Leach Batch: 500-173472 500-173290 N/A Prep Date: Leach Date: 12/19/2012 1010 N/A Analyte Qual Limit % Rec. Result SpikeAmount 180 168.6 94 80 - 120 Sulfide, Reactive

TestAmerica Chicago 

## 01/03/2013 Page 57 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173291

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 9030B

N/A No Equipment MB 500-173291/1-A
Analysis Date: 12/19/2012 1335 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173474 500-173291
Prep Date: Leach Date: 12/19/20121125 N/A Analyte RL MDL Qual Result <25.0 25.0 4.00 Sulfide

Solid 1.0 

### Lab Control Sample - Batch: 500-173291

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10.0000 g 10 mL Units: mg/Kg 

### Method: 9034 Preparation: 9030B

N/A No Equipment LCS 500-173291/2-A
Analysis Date: 12/19/2012 1335 Analysis Batch: Prep Batch: Leach Batch: 500-173474 500-173291 N/A Prep Date: Leach Date: 12/19/20121125 N/A Analyte Qual Limit % Rec. Result SpikeAmount 180 168.3 93 80 - 120 Sulfide

TestAmerica Chicago 

## 01/03/2013 Page 58 of 383

## Quality Control Results
Job Number: 500-53315-1 Client: Project Integration, Inc

Solid Client Matrix: 1.0 Dilution: Lab Sample ID: 

### Method Blank - Batch: 500-173324

Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10 g 10 mL Units: mg/Kg 

### Method: 9071B Preparation: 9071B

N/A No Equipment MB 500-173324/1-A
Analysis Date: 12/19/2012 0920 Analysis Batch: Prep Batch: Leach Batch: N/A 500-173330 500-173324
Prep Date: Leach Date: 12/19/2012 0510 N/A Analyte RL MDL Qual Result <500 500 222 HEM (Oil & Grease)

Solid 1.0 

### Lab Control Sample - Batch: 500-173324

Client Matrix: Lab Sample ID: Dilution: Instrument ID: Lab File ID: InitialWeight /Volume: FinalWeight /Volume: 10 g 10 mL Units: mg/Kg 

### Method: 9071B Preparation: 9071B

N/A No Equipment LCS 500-173324/2-A
Analysis Date: 12/19/2012 0931 Analysis Batch: Prep Batch: Leach Batch: 500-173330 500-173324 N/A Prep Date: Leach Date: 12/19/2012 0510 N/A Analyte Qual Limit % Rec. Result SpikeAmount 4000 4090 102 80 - 120 HEM (Oil & Grease)

TestAmerica Chicago 

## 01/03/2013 Page 59 of 383

## DATA REPORTING QUALIFIERS Client: Project Integration, Inc Job Number: 500-53315-1

Lab Section Qualifier Description 

### GC/MS VOA MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. 4
Result exceeded calibration range. E
Metals Compound was found in the blank and sample. B MS or MSD exceeds the control limits F MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. 4

Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J Serial Dilution exceeds the control limits V General Chemistry Compound was found in the blank and sample. B Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. J

TestAmerica Chicago 

## 01/03/2013 Page 60 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis GC/MS VOA Analysis Batch:500-173225 

### Lab Control Sample Solid 8260B LCS 500-173225/5 T Method Blank Solid 8260B MB 500-173225/4 T Solid FC DISCRETE 4 8260B 500-53315-3 T Matrix Spike Solid 8260B 500-53315-3MS T Matrix Spike Duplicate Solid 8260B 500-53315-3MSD T Solid FC D DISCRETE 4 8260B 500-53315-4 T Prep Batch: 500-173238 

### Solid FC DISCRETE 4 5030B 500-53315-3DL T Solid FC D DISCRETE 4 5030B 500-53315-4DL T Analysis Batch:500-173508 

### Lab Control Sample Water 8260B LCS 500-173508/4 T Method Blank Water 8260B MB 500-173508/6 T Water TRIP BLANK 8260B 500-53315-5 T Water FC EB 4 8260B 500-53315-6 T Analysis Batch:500-173509 

### Lab Control Sample Solid 8260B LCS 500-173509/4 T Method Blank Solid 8260B MB 500-173509/6 T Solid 500-173238 FC DISCRETE 4 8260B 500-53315-3DL T Solid 500-173238 FC D DISCRETE 4 8260B 500-53315-4DL T
Report Basis T=Total



### TestAmerica Chicago 

## 01/03/2013 Page 61 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Prep Batch: 500-173139 

### Lab Control Sample Solid 3050B LCS 500-173139/2-A T Method Blank Solid 3050B MB 500-173139/1-A T Solid FC COMPOSITE 4 3050B 500-53315-1 T Duplicate Solid 3050B 500-53315-1DU T Matrix Spike Solid 3050B 500-53315-1MS T Matrix Spike Duplicate Solid 3050B 500-53315-1MSD T Solid FC D COMPOSITE 4 3050B 500-53315-2 T Prep Batch: 500-173153 

### Lab Control Sample Solid 7471A LCS 500-173153/8-A T Method Blank Solid 7471A MB 500-173153/7-A T Solid FC COMPOSITE 4 7471A 500-53315-1 T Solid FC D COMPOSITE 4 7471A 500-53315-2 T Prep Batch: 500-173172 

### Lab Control Sample Water 7470A LCS 500-173172/8-A T Method Blank Water 7470A MB 500-173172/7-A T Water FC EB 4 7470A 500-53315-6 T Duplicate Water 7470A 500-53315-6DU T Matrix Spike Water 7470A 500-53315-6MS T Matrix Spike Duplicate Water 7470A 500-53315-6MSD T Prep Batch: 500-173187 

### TCLP SPLPE Leachate Blank Solid 1311 LB 500-173187/1-B P TCLP SPLPE Leachate Blank Solid 1311 LB 500-173187/1-D P Solid FC COMPOSITE 4 1311 500-53315-1 P Solid FC D COMPOSITE 4 1311 500-53315-2 P Analysis Batch:500-173224 

### Lab Control Sample Solid 500-173139 6010B LCS 500-173139/2-A T Method Blank Solid 500-173139 6010B MB 500-173139/1-A T Solid 500-173139 FC COMPOSITE 4 6010B 500-53315-1 T Duplicate Solid 500-173139 6010B 500-53315-1DU T Matrix Spike Solid 500-173139 6010B 500-53315-1MS T Matrix Spike Duplicate Solid 500-173139 6010B 500-53315-1MSD T Solid 500-173139 FC D COMPOSITE 4 6010B 500-53315-2 T Prep Batch: 500-173264 

### Lab Control Sample Water 7470A LCS 500-173264/8-A T Method Blank Water 7470A MB 500-173264/7-A T TCLP SPLPE Leachate Blank Solid 500-173187 7470A LB 500-173187/1-B P Solid 500-173187 FC COMPOSITE 4 7470A 500-53315-1 P Solid 500-173187 FC D COMPOSITE 4 7470A 500-53315-2 P

TestAmerica Chicago 

## 01/03/2013 Page 62 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis Metals Analysis Batch:500-173280 

### Lab Control Sample Water 500-173172 7470A LCS 500-173172/8-A T Method Blank Water 500-173172 7470A MB 500-173172/7-A T Water 500-173172 FC EB 4 7470A 500-53315-6 T Duplicate Water 500-173172 7470A 500-53315-6DU T Matrix Spike Water 500-173172 7470A 500-53315-6MS T Matrix Spike Duplicate Water 500-173172 7470A 500-53315-6MSD T Analysis Batch:500-173328 

### Lab Control Sample Solid 500-173153 7471A LCS 500-173153/8-A T Method Blank Solid 500-173153 7471A MB 500-173153/7-A T Solid 500-173153 FC COMPOSITE 4 7471A 500-53315-1 T Solid 500-173153 FC D COMPOSITE 4 7471A 500-53315-2 T Prep Batch: 500-173349 

### Lab Control Sample Water 3010A LCS 500-173349/2-A T Method Blank Water 3010A MB 500-173349/1-A T Water FC EB 4 3010A 500-53315-6 T Prep Batch: 500-173406 

### Lab Control Sample Water 3010A LCS 500-173406/3-A T TCLP SPLPE Leachate Blank Solid 500-173187 3010A LB 500-173187/1-D P Solid 500-173187 FC COMPOSITE 4 3010A 500-53315-1 P Solid 500-173187 FC D COMPOSITE 4 3010A 500-53315-2 P Analysis Batch:500-173438 

### TCLP SPLPE Leachate Blank Solid 500-173264 7470A LB 500-173187/1-B P Lab Control Sample Water 500-173264 7470A LCS 500-173264/8-A T Method Blank Water 500-173264 7470A MB 500-173264/7-A T Solid 500-173264 FC COMPOSITE 4 7470A 500-53315-1 P Solid 500-173264 FC D COMPOSITE 4 7470A 500-53315-2 P Analysis Batch:500-173517 

### Lab Control Sample Water 500-173349 6010B LCS 500-173349/2-A T Method Blank Water 500-173349 6010B MB 500-173349/1-A T Water 500-173349 FC EB 4 6010B 500-53315-6 T Analysis Batch:500-173518 

### TCLP SPLPE Leachate Blank Solid 500-173406 6010B LB 500-173187/1-D P Lab Control Sample Water 500-173406 6010B LCS 500-173406/3-A T Solid 500-173406 FC COMPOSITE 4 6010B 500-53315-1 P Solid 500-173406 FC D COMPOSITE 4 6010B 500-53315-2 P

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## 01/03/2013 Page 63 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis
Report Basis P= TCLP T=Total



### TestAmerica Chicago 

## 01/03/2013 Page 64 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-173077 

### Solid FC COMPOSITE 4 Moisture 500-53315-1 T Solid FC D COMPOSITE 4 Moisture 500-53315-2 T Analysis Batch:500-173079 

### Lab Control Sample Water 7196A LCS 500-173079/4 T Method Blank Water 7196A MB 500-173079/3 T Water FC EB 4 7196A 500-53315-6 T Matrix Spike Water 7196A 500-53315-6MS T Matrix Spike Duplicate Water 7196A 500-53315-6MSD T Prep Batch: 500-173106 

### Lab Control Sample Water 7.3.4 LCS 500-173106/2-A T Method Blank Water 7.3.4 MB 500-173106/1-A T Water FC EB 4 7.3.4 500-53315-6 T Analysis Batch:500-173107 

### Lab Control Sample Water 500-173106 9034 LCS 500-173106/2-A T Method Blank Water 500-173106 9034 MB 500-173106/1-A T Water 500-173106 FC EB 4 9034 500-53315-6 T Analysis Batch:500-173108 

### Lab Control Sample Water 9034 LCS 500-173108/2 T Method Blank Water 9034 MB 500-173108/1 T Water FC EB 4 9034 500-53315-6 T Prep Batch: 500-173173 

### Lab Control Sample Water 1664A LCS 500-173173/2-A T Method Blank Water 1664A MB 500-173173/1-A T Water FC EB 4 1664A 500-53315-6 T Analysis Batch:500-173178 

### Lab Control Sample Water 500-173173 1664A LCS 500-173173/2-A T Method Blank Water 500-173173 1664A MB 500-173173/1-A T Water 500-173173 FC EB 4 1664A 500-53315-6 T Analysis Batch:500-173236 

### Solid FC COMPOSITE 4 SM 2540G 500-53315-1 T Solid FC D COMPOSITE 4 SM 2540G 500-53315-2 T Prep Batch: 500-173245 

### Lab Control Sample Water 9010B LCS 500-173245/2-A T Method Blank Water 9010B MB 500-173245/1-A T Water FC EB 4 9010B 500-53315-6 T

TestAmerica Chicago 

## 01/03/2013 Page 65 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Prep Batch: 500-173250 

### Lab Control Sample Solid 9010B LCS 500-173250/2-A T Method Blank Solid 9010B MB 500-173250/1-A T Solid FC COMPOSITE 4 9010B 500-53315-1 T Solid FC D COMPOSITE 4 9010B 500-53315-2 T Matrix Spike Solid 9010B 500-53315-2MS T Matrix Spike Duplicate Solid 9010B 500-53315-2MSD T Prep Batch: 500-173258 

### Lab Control Sample Solid 3060A LCS 500-173258/2-A T Lab Control Sample Solid 3060A LCS 500-173258/3-A T Method Blank Solid 3060A MB 500-173258/1-A T Solid FC COMPOSITE 4 3060A 500-53315-1 T Solid FC D COMPOSITE 4 3060A 500-53315-2 T Prep Batch: 500-173290 

### Lab Control Sample Solid 7.3.4 LCS 500-173290/2-A T Method Blank Solid 7.3.4 MB 500-173290/1-A T Solid FC COMPOSITE 4 7.3.4 500-53315-1 T Solid FC D COMPOSITE 4 7.3.4 500-53315-2 T Prep Batch: 500-173291 

### Lab Control Sample Solid 9030B LCS 500-173291/2-A T Method Blank Solid 9030B MB 500-173291/1-A T Solid FC COMPOSITE 4 9030B 500-53315-1 T Solid FC D COMPOSITE 4 9030B 500-53315-2 T Analysis Batch:500-173311 

### Solid FC DISCRETE 4 Moisture 500-53315-3 T Solid FC D DISCRETE 4 Moisture 500-53315-4 T Prep Batch: 500-173324 

### Lab Control Sample Solid 9071B LCS 500-173324/2-A T Method Blank Solid 9071B MB 500-173324/1-A T Solid FC COMPOSITE 4 9071B 500-53315-1 T Solid FC D COMPOSITE 4 9071B 500-53315-2 T Analysis Batch:500-173330 

### Lab Control Sample Solid 500-173324 9071B LCS 500-173324/2-A T Method Blank Solid 500-173324 9071B MB 500-173324/1-A T Solid 500-173324 FC COMPOSITE 4 9071B 500-53315-1 T Solid 500-173324 FC D COMPOSITE 4 9071B 500-53315-2 T

TestAmerica Chicago 

## 01/03/2013 Page 66 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1


## QCAssociation Summary Lab Sample ID Client Sample ID Client Matrix Method Prep Batch Report Basis General Chemistry Analysis Batch:500-173341 

### Lab Control Sample Solid 500-173258 7196A LCS 500-173258/2-A T Lab Control Sample Solid 500-173258 7196A LCS 500-173258/3-A T Method Blank Solid 500-173258 7196A MB 500-173258/1-A T Solid 500-173258 FC COMPOSITE 4 7196A 500-53315-1 T Solid 500-173258 FC D COMPOSITE 4 7196A 500-53315-2 T Analysis Batch:500-173386 

### Lab Control Sample Solid 500-173250 9014 LCS 500-173250/2-A T Method Blank Solid 500-173250 9014 MB 500-173250/1-A T Solid 500-173250 FC COMPOSITE 4 9014 500-53315-1 T Solid 500-173250 FC D COMPOSITE 4 9014 500-53315-2 T Matrix Spike Solid 500-173250 9014 500-53315-2MS T Matrix Spike Duplicate Solid 500-173250 9014 500-53315-2MSD T Analysis Batch:500-173387 

### Lab Control Sample Water 500-173245 9014 LCS 500-173245/2-A T Method Blank Water 500-173245 9014 MB 500-173245/1-A T Water 500-173245 FC EB 4 9014 500-53315-6 T Analysis Batch:500-173472 

### Lab Control Sample Solid 500-173290 9034 LCS 500-173290/2-A T Method Blank Solid 500-173290 9034 MB 500-173290/1-A T Solid 500-173290 FC COMPOSITE 4 9034 500-53315-1 T Solid 500-173290 FC D COMPOSITE 4 9034 500-53315-2 T Analysis Batch:500-173474 

### Lab Control Sample Solid 500-173291 9034 LCS 500-173291/2-A T Method Blank Solid 500-173291 9034 MB 500-173291/1-A T Solid 500-173291 FC COMPOSITE 4 9034 500-53315-1 T Solid 500-173291 FC D COMPOSITE 4 9034 500-53315-2 T Analysis Batch:500-173479 

### Solid FC COMPOSITE 4 9045C 500-53315-1 T Solid FC D COMPOSITE 4 9045C 500-53315-2 T Analysis Batch:500-173558 

### Solid FC COMPOSITE 4 1010 500-53315-1 T Solid FC D COMPOSITE 4 1010 500-53315-2 T
Report Basis T=Total



### TestAmerica Chicago 

## 01/03/2013 Page 67 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-1 FC COMPOSITE 4



### P:3050B 500-53315-A-1-A 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B 500-53315-A-1-A 500-173224 500-173139 12/17/2012 22:46 TDS TAL CHI 1 P:3010A 500-53315-A-1-N 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B 500-53315-A-1-N 500-173518 500-173406 12/19/2012 22:29 TDS TAL CHI 1 P:7470A 500-53315-A-1-J 500-173438 500-173264 12/18/2012 13:00 BJB TAL CHI 1 A:7470A 500-53315-A-1-J 500-173438 500-173264 12/19/2012 10:24 BJB TAL CHI 1 P:7471A 500-53315-A-1-F 500-173328 500-173153 12/17/2012 14:00 BJB TAL CHI 1 A:7471A 500-53315-A-1-F 500-173328 500-173153 12/18/2012 14:00 BJB TAL CHI 1 A:1010 500-53315-A-1 500-173558 12/19/2012 17:21 APW TAL CHI 1 P:3060A 500-53315-A-1-I 500-173341 500-173258 12/18/2012 10:00 APW TAL CHI 1 A:7196A 500-53315-A-1-I 500-173341 500-173258 12/18/2012 15:49 APW TAL CHI 1 P:9010B 500-53315-A-1-H 500-173386 500-173250 12/18/2012 10:35 EAT TAL CHI 1 A:9014 500-53315-A-1-H 500-173386 500-173250 12/18/2012 14:24 EAT TAL CHI 1 P:7.3.4 500-53315-A-1-K 500-173472 500-173290 12/19/2012 10:40 CLM TAL CHI 1 A:9034 500-53315-A-1-K 500-173472 500-173290 12/19/2012 12:18 CLM TAL CHI 1 P:9030B 500-53315-A-1-L 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 500-53315-A-1-L 500-173474 500-173291 12/19/2012 13:36 CLM TAL CHI 1 A:9045C 500-53315-A-1 500-173479 12/20/2012 15:12 CLM TAL CHI 1 P:9071B 500-53315-A-1-M 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B 500-53315-A-1-M 500-173330 500-173324 12/19/201211:01 MTB TAL CHI 1 A:Moisture 500-53315-A-1 500-173077 12/15/2012 12:43 CMV TAL CHI 1 A:SM 2540G 500-53315-A-1 500-173236 12/18/2012 07:34 CMV TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-1 MS FC COMPOSITE 4



### P:3050B 500-53315-A-1-C MS 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B 500-53315-A-1-C MS 500-173224 500-173139 12/17/2012 23:04 TDS TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-1 MSD FC COMPOSITE 4



### P:3050B 500-53315-A-1-D MSD 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B 500-53315-A-1-D MSD 500-173224 500-173139 12/17/2012 23:10 TDS TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 68 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-1 DU FC COMPOSITE 4



### P:3050B 500-53315-A-1-B DU 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B 500-53315-A-1-B DU 500-173224 500-173139 12/17/2012 22:58 TDS TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-1 SD FC COMPOSITE 4



### P:3050B 500-53315-A-1-A SD ^5 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 5 A:6010B 500-53315-A-1-A SD ^5 500-173224 500-173139 12/17/2012 22:52 TDS TAL CHI 5

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-2 FC D COMPOSITE 4



### P:3050B 500-53315-A-2-A 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B 500-53315-A-2-A 500-173224 500-173139 12/17/2012 23:17 TDS TAL CHI 1 P:3010A 500-53315-A-2-L 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B 500-53315-A-2-L 500-173518 500-173406 12/19/2012 22:35 TDS TAL CHI 1 P:7470A 500-53315-A-2-H 500-173438 500-173264 12/18/2012 13:00 BJB TAL CHI 1 A:7470A 500-53315-A-2-H 500-173438 500-173264 12/19/2012 10:29 BJB TAL CHI 1 P:7471A 500-53315-A-2-B 500-173328 500-173153 12/17/2012 14:00 BJB TAL CHI 1 A:7471A 500-53315-A-2-B 500-173328 500-173153 12/18/2012 14:01 BJB TAL CHI 1 A:1010 500-53315-A-2 500-173558 12/19/2012 18:00 APW TAL CHI 1 P:3060A 500-53315-A-2-G 500-173341 500-173258 12/18/2012 10:00 APW TAL CHI 1 A:7196A 500-53315-A-2-G 500-173341 500-173258 12/18/2012 15:50 APW TAL CHI 1 P:9010B 500-53315-A-2-D 500-173386 500-173250 12/18/2012 10:35 EAT TAL CHI 1 A:9014 500-53315-A-2-D 500-173386 500-173250 12/18/2012 14:24 EAT TAL CHI 1 P:7.3.4 500-53315-A-2-I 500-173472 500-173290 12/19/2012 10:45 CLM TAL CHI 1 A:9034 500-53315-A-2-I 500-173472 500-173290 12/19/2012 12:19 CLM TAL CHI 1 P:9030B 500-53315-A-2-J 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 500-53315-A-2-J 500-173474 500-173291 12/19/2012 13:37 CLM TAL CHI 1 A:9045C 500-53315-A-2 500-173479 12/20/2012 16:11 CLM TAL CHI 1 P:9071B 500-53315-A-2-K 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B 500-53315-A-2-K 500-173330 500-173324 12/19/201211:12 MTB TAL CHI 1 A:Moisture 500-53315-A-2 500-173077 12/15/2012 12:43 CMV TAL CHI 1 A:SM 2540G 500-53315-A-2 500-173236 12/18/2012 07:34 CMV TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 69 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-2 MS FC D COMPOSITE 4



### P:9010B 500-53315-A-2-E MS 500-173386 500-173250 12/18/2012 10:35 EAT TAL CHI 1 A:9014 500-53315-A-2-E MS 500-173386 500-173250 12/18/2012 14:25 EAT TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 15:15 500-53315-2 MSD FC D COMPOSITE 4



### P:9010B 500-53315-A-2-F MSD 500-173386 500-173250 12/18/2012 10:35 EAT TAL CHI 1 A:9014 500-53315-A-2-F MSD 500-173386 500-173250 12/18/2012 14:25 EAT TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:45 500-53315-3 FC DISCRETE 4



### P:5030B 500-53315-A-3 500-173225 12/18/2012 09:30 BDW TAL CHI 1 A:8260B 500-53315-A-3 500-173225 12/18/2012 09:30 BDW TAL CHI 1 P:5030B 500-53315-A-3-A 500-173509 500-173238 12/18/2012 07:45 BDW TAL CHI DL 50 A:8260B 500-53315-A-3-A 500-173509 500-173238 12/20/2012 02:16 BDA TAL CHI DL 50 A:Moisture 500-53315-A-3 500-173311 12/18/2012 13:59 CMV TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:45 500-53315-3 MS FC DISCRETE 4



### P:5030B 500-53315-A-3 MS 500-173225 12/18/2012 09:54 BDW TAL CHI 1 A:8260B 500-53315-A-3 MS 500-173225 12/18/2012 09:54 BDW TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:45 500-53315-3 MSD FC DISCRETE 4



### P:5030B 500-53315-A-3 MSD 500-173225 12/18/2012 10:17 BDW TAL CHI 1 A:8260B 500-53315-A-3 MSD 500-173225 12/18/2012 10:17 BDW TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 70 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:45 500-53315-4 FC D DISCRETE 4



### P:5030B 500-53315-A-4 500-173225 12/18/2012 10:40 BDW TAL CHI 1 A:8260B 500-53315-A-4 500-173225 12/18/2012 10:40 BDW TAL CHI 1 P:5030B 500-53315-A-4-A 500-173509 500-173238 12/18/2012 07:45 BDW TAL CHI DL 50 A:8260B 500-53315-A-4-A 500-173509 500-173238 12/20/2012 02:40 BDA TAL CHI DL 50 A:Moisture 500-53315-A-4 500-173311 12/18/2012 13:59 CMV TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 00:00 500-53315-5 TRIP BLANK



### P:5030B 500-53315-B-5 500-173508 12/20/2012 01:08 BDA TAL CHI 1 A:8260B 500-53315-B-5 500-173508 12/20/2012 01:08 BDA TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:30 500-53315-6 FC EB 4



### P:5030B 500-53315-B-6 500-173508 12/20/2012 01:49 BDA TAL CHI 1 A:8260B 500-53315-B-6 500-173508 12/20/2012 01:49 BDA TAL CHI 1 P:3010A 500-53315-E-6-E 500-173517 500-173349 12/18/2012 15:30 RL TAL CHI 1 A:6010B 500-53315-E-6-E 500-173517 500-173349 12/19/2012 14:57 TDS TAL CHI 1 P:7470A 500-53315-E-6-A 500-173280 500-173172 12/17/2012 13:00 BJB TAL CHI 1 A:7470A 500-53315-E-6-A 500-173280 500-173172 12/18/2012 09:49 BJB TAL CHI 1 P:1664A 500-53315-H-6-A 500-173178 500-173173 12/18/2012 07:24 MTB TAL CHI 1 A:1664A 500-53315-H-6-A 500-173178 500-173173 12/18/201211:14 MTB TAL CHI 1 A:7196A 500-53315-F-6 500-173079 12/15/2012 13:22 APW TAL CHI 1 P:9010B 500-53315-D-6-A 500-173387 500-173245 12/18/2012 08:30 EAT TAL CHI 1 A:9014 500-53315-D-6-A 500-173387 500-173245 12/18/2012 13:54 EAT TAL CHI 1 P:7.3.4 500-53315-G-6-A 500-173107 500-173106 12/17/2012 00:13 CLB TAL CHI 1 A:9034 500-53315-G-6-A 500-173107 500-173106 12/17/2012 01:08 CLB TAL CHI 1 A:9034 500-53315-G-6 500-173108 12/17/2012 01:11 CLB TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:30 500-53315-6 MS FC EB 4



### P:7470A 500-53315-E-6-C MS 500-173280 500-173172 12/17/2012 13:00 BJB TAL CHI 1 A:7470A 500-53315-E-6-C MS 500-173280 500-173172 12/18/2012 09:57 BJB TAL CHI 1 A:7196A 500-53315-F-6 MS 500-173079 12/15/2012 13:22 APW TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 71 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:30 500-53315-6 MSD FC EB 4



### P:7470A 500-53315-E-6-D MSD 500-173280 500-173172 12/17/2012 13:00 BJB TAL CHI 1 A:7470A 500-53315-E-6-D MSD 500-173280 500-173172 12/18/2012 09:59 BJB TAL CHI 1 A:7196A 500-53315-F-6 MSD 500-173079 12/15/2012 13:23 APW TAL CHI 1

12/15/2012 09:10 Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: Received Date/Time: 12/14/2012 14:30 500-53315-6 DU FC EB 4



### P:7470A 500-53315-E-6-B DU 500-173280 500-173172 12/17/2012 13:00 BJB TAL CHI 1 A:7470A 500-53315-E-6-B DU 500-173280 500-173172 12/18/2012 09:55 BJB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 72 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A MB N/A



### P:5030B MB 500-173225/4 500-173225 12/18/2012 08:30 BDW TAL CHI 1 A:8260B MB 500-173225/4 500-173225 12/18/2012 08:30 BDW TAL CHI 1 P:5030B MB 500-173508/6 500-173508 12/20/2012 00:43 BDA TAL CHI 1 A:8260B MB 500-173508/6 500-173508 12/20/2012 00:43 BDA TAL CHI 1 A:8260B MB 500-173509/6 500-173509 12/20/2012 00:43 BDA TAL CHI 1 P:3050B MB 500-173139/1-A 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B MB 500-173139/1-A 500-173224 500-173139 12/17/2012 21:04 TDS TAL CHI 1 P:3010A MB 500-173349/1-A 500-173517 500-173349 12/18/2012 15:30 RL TAL CHI 1 A:6010B MB 500-173349/1-A 500-173517 500-173349 12/19/2012 13:52 TDS TAL CHI 1 P:7470A MB 500-173172/7-A 500-173280 500-173172 12/17/2012 13:00 BJB TAL CHI 1 A:7470A MB 500-173172/7-A 500-173280 500-173172 12/18/2012 09:09 BJB TAL CHI 1 P:7470A MB 500-173264/7-A 500-173438 500-173264 12/18/2012 13:00 BJB TAL CHI 1 A:7470A MB 500-173264/7-A 500-173438 500-173264 12/19/2012 10:08 BJB TAL CHI 1 P:7471A MB 500-173153/7-A 500-173328 500-173153 12/17/2012 14:00 BJB TAL CHI 1 A:7471A MB 500-173153/7-A 500-173328 500-173153 12/18/2012 13:04 BJB TAL CHI 1 P:1664A MB 500-173173/1-A 500-173178 500-173173 12/18/2012 05:25 MTB TAL CHI 1 A:1664A MB 500-173173/1-A 500-173178 500-173173 12/18/2012 10:05 MTB TAL CHI 1 A:7196A MB 500-173079/3 500-173079 12/15/2012 13:21 APW TAL CHI 1 P:3060A MB 500-173258/1-A 500-173341 500-173258 12/18/2012 10:00 APW TAL CHI 1 A:7196A MB 500-173258/1-A 500-173341 500-173258 12/18/2012 15:46 APW TAL CHI 1 P:9010B MB 500-173245/1-A 500-173387 500-173245 12/18/2012 08:30 EAT TAL CHI 1 A:9014 MB 500-173245/1-A 500-173387 500-173245 12/18/2012 13:45 EAT TAL CHI 1 P:9010B MB 500-173250/1-A 500-173386 500-173250 12/18/2012 10:35 EAT TAL CHI 1 A:9014 MB 500-173250/1-A 500-173386 500-173250 12/18/2012 14:23 EAT TAL CHI 1 P:7.3.4 MB 500-173106/1-A 500-173107 500-173106 12/17/2012 00:01 CLB TAL CHI 1 A:9034 MB 500-173106/1-A 500-173107 500-173106 12/17/2012 00:19 CLB TAL CHI 1 A:9034 MB 500-173108/1 500-173108 12/17/2012 00:19 CLB TAL CHI 1 P:7.3.4 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 10:05 CLM TAL CHI 1 A:9034 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 12:15 CLM TAL CHI 1 P:9030B MB 500-173291/1-A 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 MB 500-173291/1-A 500-173474 500-173291 12/19/2012 13:35 CLM TAL CHI 1 P:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 09:20 MTB TAL CHI 1
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LB N/A



### P:3010A LB 500-173187/1-D 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B LB 500-173187/1-D 500-173518 500-173406 12/19/2012 21:07 TDS TAL CHI 1 P:7470A LB 500-173187/1-B 500-173438 500-173264 12/18/2012 13:00 BJB TAL CHI 1 A:7470A LB 500-173187/1-B 500-173438 500-173264 12/19/2012 10:12 BJB TAL CHI 1

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 73 of 383

## Quality Control Results
Client: Project Integration, Inc Job Number: 500-53315-1 

## Laboratory Chronicle
Lab ID:

Method Bottle ID Run Analysis Batch Prep Batch Date Prepared / Analyzed Dil Lab Analyst Client ID: 

### Sample Date/Time: N/A Received Date/Time: N/A LCS N/A



### P:5030B LCS 500-173225/5 500-173225 12/18/2012 08:53 BDW TAL CHI 1 A:8260B LCS 500-173225/5 500-173225 12/18/2012 08:53 BDW TAL CHI 1 P:5030B LCS 500-173508/4 500-173508 12/19/2012 23:54 BDA TAL CHI 1 A:8260B LCS 500-173508/4 500-173508 12/19/2012 23:54 BDA TAL CHI 1 A:8260B LCS 500-173509/4 500-173509 12/19/2012 23:54 BDA TAL CHI 1 P:3050B LCS 500-173139/2-A 500-173224 500-173139 12/17/2012 08:50 LAH TAL CHI 1 A:6010B LCS 500-173139/2-A 500-173224 500-173139 12/17/2012 21:10 TDS TAL CHI 1 P:3010A LCS 500-173349/2-A 500-173517 500-173349 12/18/2012 15:30 RL TAL CHI 1 A:6010B LCS 500-173349/2-A 500-173517 500-173349 12/19/2012 13:58 TDS TAL CHI 1 P:3010A LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 08:20 LAH TAL CHI 1 A:6010B LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 21:20 TDS TAL CHI 1 P:7470A LCS 500-173172/8-A 500-173280 500-173172 12/17/2012 13:00 BJB TAL CHI 1 A:7470A LCS 500-173172/8-A 500-173280 500-173172 12/18/2012 09:11 BJB TAL CHI 1 P:7470A LCS 500-173264/8-A 500-173438 500-173264 12/18/2012 13:00 BJB TAL CHI 1 A:7470A LCS 500-173264/8-A 500-173438 500-173264 12/19/2012 10:10 BJB TAL CHI 1 P:7471A LCS 500-173153/8-A 500-173328 500-173153 12/17/2012 14:00 BJB TAL CHI 1 A:7471A LCS 500-173153/8-A 500-173328 500-173153 12/18/2012 13:10 BJB TAL CHI 1 P:1664A LCS 500-173173/2-A 500-173178 500-173173 12/18/2012 05:35 MTB TAL CHI 1 A:1664A LCS 500-173173/2-A 500-173178 500-173173 12/18/2012 10:11 MTB TAL CHI 1 A:7196A LCS 500-173079/4 500-173079 12/15/2012 13:21 APW TAL CHI 1 P:3060A LCS 500-173258/2-A 500-173341 500-173258 12/18/2012 10:00 APW TAL CHI 1 A:7196A LCS 500-173258/2-A 500-173341 500-173258 12/18/2012 15:46 APW TAL CHI 1 P:3060A LCS 500-173258/3-A 500-173341 500-173258 12/18/2012 10:00 APW TAL CHI 50 A:7196A LCS 500-173258/3-A 500-173341 500-173258 12/18/2012 15:47 APW TAL CHI 50 P:9010B LCS 500-173245/2-A 500-173387 500-173245 12/18/2012 08:30 EAT TAL CHI 1 A:9014 LCS 500-173245/2-A 500-173387 500-173245 12/18/2012 13:45 EAT TAL CHI 1 P:9010B LCS 500-173250/2-A 500-173386 500-173250 12/18/2012 10:35 EAT TAL CHI 1 A:9014 LCS 500-173250/2-A 500-173386 500-173250 12/18/2012 14:23 EAT TAL CHI 1 A:9034 LCS 500-173108/2 500-173108 12/17/2012 00:21 CLB TAL CHI 1 P:7.3.4 LCS 500-173106/2-A 500-173107 500-173106 12/17/2012 00:05 CLB TAL CHI 1 A:9034 LCS 500-173106/2-A 500-173107 500-173106 12/17/2012 00:35 CLB TAL CHI 1 P:7.3.4 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 10:10 CLM TAL CHI 1 A:9034 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 12:15 CLM TAL CHI 1 P:9030B LCS 500-173291/2-A 500-173474 500-173291 12/19/201211:25 CLM TAL CHI 1 A:9034 LCS 500-173291/2-A 500-173474 500-173291 12/19/2012 13:35 CLM TAL CHI 1 P:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 05:10 MTB TAL CHI 1 A:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 09:31 MTB TAL CHI 1 

### Lab References: TAL CHI=TestAmerica Chicago

A=Analytical MethodP= Prep Method TestAmerica Chicago 

## 01/03/2013 Page 74 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 04/26/13 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L Mallin / JTBaker, Lot E50600 / K19H00 1664 HEM_00060 SGT-HEM 4000 mg/L 8260 IS SK_00026 1,4-Dichlorobenzene-d4 250 ug/mL 5 mL 5 mL 12/03/1211/19/12 8260 IS WK_00381 1, Lot NA 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00026 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 IS SK_00026 1,4-Dichlorobenzene-d4 50 ug/mL 20 mL 4000 uL 11/20/1211/06/12 8260 LOW IS_00102 MEOH, Lot DA946 1,4-Difluorobenzene 50 ug/mL Chlorobenzene-d5 50 ug/mL Pentafluorobenzene 50 ug/mL 08/31/14 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL RESTEK, Lot AO88671 .8260 IS SK_00026 1,4-Difluorobenzene 250 ug/mL Chlorobenzene-d5 250 ug/mL Pentafluorobenzene 250 ug/mL 8260 SS SK_00031 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 11/20/1211/06/12 8260 LOW SS_00104 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00031 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 20 mL 4000 uL 12/27/1212/13/12 8260 LOW SS_00107 MEOH, Lot DA946 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 SS SK_00031 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 12/03/1211/19/12 8260 SS WK_00378 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 .8260 SS SK_00031 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 STD STK_00032 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 11/28/1211/14/12 8260 STD WK_00211 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 

## 01/03/2013 Page 75 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL 

## 01/03/2013 Page 76 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00032 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL 

## 01/03/2013 Page 77 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 8260 STD WK_00212 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL 

## 01/03/2013 Page 78 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 .8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 

## 01/03/2013 Page 79 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/21/1211/14/12 ACR/NITRSTDWK_00204 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 .ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/26/1211/19/12 ACR/NITRSTDWK_00205 METHANOL, Lot NA Acrolein 4000 ug/mL 

## 01/03/2013 Page 80 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 .ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 11/21/1211/14/12 GAS STD WK RE_00243 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 11/26/1211/19/12 GAS STD WK RE_00244 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 .GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 8260 SS WK_00385 1,2-Dichloroethane-d4 (Surr) 43.28 ug/L 5 mL 0.8656 uL 01/01/1312/18/12 INST16 IS/SS_00223 1, Lot NA 4-Bromofluorobenzene (Surr) 43.28 ug/L Dibromofluoromethane 43.28 ug/L Toluene-d8 (Surr) 43.28 ug/L 8260 SS SK_00032 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 01/01/1312/18/12 .8260 SS WK_00385 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 ..8260 SS SK_00032 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 11/28/1211/14/12 KET/CS2 STDWK_00179 METHANOL, Lot NA 2-Hexanone 100 ug/mL 

## 01/03/2013 Page 81 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 KET/CS2 STDWK_00180 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL KET/CS2 SK_00014 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/25/1212/11/12 KET/CS2 STDWK_00184 METHANOL, Lot NA Acetone 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 .KET/CS2 SK_00014 Acetone 100 ug/mL level1std5ppm_00006 Benzene 0.5 ug/mL 1 mL 100 uL 12/31/1603/20/12 level 1_00011 1, Lot CY647 Ethylbenzene 0.5 ug/mL m-Xylene & p-Xylene 1 ug/mL o-Xylene 0.5 ug/mL Toluene 0.5 ug/mL Trichloroethene 0.5 ug/mL Vinyl chloride 0.5 ug/mL level18260wk_00006 Benzene 5 ug/mL 2 mL 100 uL 02/28/1203/22/11 .level1std5ppm_00006 1, Lot CY647 Ethylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL o-Xylene 5 ug/mL Toluene 5 ug/mL Trichloroethene 5 ug/mL level1gaswk_00006 100 uLVinyl chloride 5 ug/mL level18260sk_00001 Benzene 100 ug/mL 1 mL 1 mL 06/30/1203/22/11 ..level18260wk_00006 1, Lot NA Ethylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL o-Xylene 100 ug/mL Toluene 100 ug/mL Trichloroethene 100 ug/mL 06/30/12 (Purchased Reagent) Benzene 100 ug/mL Restek, Lot AO67921 ...level18260sk_00001 Ethylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL o-Xylene 100 ug/mL Toluene 100 ug/mL 

## 01/03/2013 Page 82 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Trichloroethene 100 ug/mL 02/28/1203/22/11 2 mLlevel1gaspt_00005 100 uLVinyl chloride 100 ug/mL ..level1gaswk_00006 1, Lot CY647 02/28/1203/22/11 1 mLlevel1gassk_00001 1 mLVinyl chloride 2000 ug/mL ...level1gaspt_00005 MEOH, Lot NA 02/28/12 (Purchased Reagent) Vinyl chloride 2000 ug/mL SUPELCO, Lot LB65254 ....level1gassk_00001 8260 SS WK_00378 1,2-Dichloroethane-d4 (Surr) 50 ug/mL 1 mL 200 uL 12/03/1211/19/12 LOW8260SS WK_00042 1, Lot DA057 4-Bromofluorobenzene (Surr) 50 ug/mL Dibromofluoromethane 50 ug/mL Toluene-d8 (Surr) 50 ug/mL 8260 SS SK_00031 1,2-Dichloroethane-d4 (Surr) 250 ug/mL 5 mL 5 mL 12/03/1211/19/12 .8260 SS WK_00378 1, Lot NA 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 07/31/14 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL RESTEK, Lot A088175 ..8260 SS SK_00031 4-Bromofluorobenzene (Surr) 250 ug/mL Dibromofluoromethane 250 ug/mL Toluene-d8 (Surr) 250 ug/mL 8260 STD WK_00211 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 11/21/1211/14/12 LOW8260STD WK_00208 METHANOL, Lot DG596 1,1,1-Trichloroethane 5 ug/mL 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL 

## 01/03/2013 Page 83 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00243 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL Dichlorodifluoromethane 5 ug/mL Dichlorofluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00179 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00174 50 uLVinyl acetate 5 ug/mL 8260 STD STK_00032 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 11/28/1211/14/12 .8260 STD WK_00211 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 

## 01/03/2013 Page 84 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL 

## 01/03/2013 Page 85 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00032 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL 

## 01/03/2013 Page 86 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 11/21/1211/14/12 .GAS STD WK RE_00243 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Dichlorofluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 11/28/1211/14/12 .KET/CS2 STDWK_00179 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/21/1211/14/12 .VA/2CEVESTDWK_00174 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 8260 STD WK_00212 1,1,1,2-Tetrachloroethane 5 ug/mL 1 mL 50 uL 11/26/1211/19/12 LOW8260STD WK_00209 1, Lot DG596 1,1,1-Trichloroethane 5 ug/mL 1,1,2,2-Tetrachloroethane 5 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 5 ug/mL 

## 01/03/2013 Page 87 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,1,2-Trichloroethane 5 ug/mL 1,1-Dichloroethane 5 ug/mL 1,1-Dichloroethene 5 ug/mL 1,1-Dichloropropene 5 ug/mL 1,2,3-Trichlorobenzene 5 ug/mL 1,2,3-Trichloropropane 5 ug/mL 1,2,4-Trichlorobenzene 5 ug/mL 1,2,4-Trimethylbenzene 5 ug/mL 1,2-Dibromo-3-Chloropropane 5 ug/mL 1,2-Dichlorobenzene 5 ug/mL 1,2-Dichloroethane 5 ug/mL 1,2-Dichloropropane 5 ug/mL 1,3,5-Trimethylbenzene 5 ug/mL 1,3-Dichlorobenzene 5 ug/mL 1,3-Dichloropropane 5 ug/mL 1,4-Dichlorobenzene 5 ug/mL 1-Chlorohexane 5 ug/mL 2,2-Dichloropropane 5 ug/mL 2-Chlorotoluene 5 ug/mL 4-Chlorotoluene 5 ug/mL 4-Isopropyltoluene 5 ug/mL Benzene 5 ug/mL Bromobenzene 5 ug/mL Bromoform 5 ug/mL Carbon tetrachloride 5 ug/mL Chlorobenzene 5 ug/mL Chlorobromomethane 5 ug/mL Chlorodibromomethane 5 ug/mL Chloroform 5 ug/mL cis-1,2-Dichloroethene 5 ug/mL cis-1,3-Dichloropropene 5 ug/mL Dibromomethane 5 ug/mL Dichlorobromomethane 5 ug/mL Ethylbenzene 5 ug/mL Ethylene Dibromide 5 ug/mL Hexachlorobutadiene 5 ug/mL Isopropylbenzene 5 ug/mL m-Xylene & p-Xylene 10 ug/mL Methyl tert-butyl ether 5 ug/mL Methylene Chloride 5 ug/mL n-Butylbenzene 5 ug/mL N-Propylbenzene 5 ug/mL Naphthalene 5 ug/mL o-Xylene 5 ug/mL sec-Butylbenzene 5 ug/mL Styrene 5 ug/mL tert-Butylbenzene 5 ug/mL Tetrachloroethene 5 ug/mL 

## 01/03/2013 Page 88 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Tetrahydrofuran 5 ug/mL Toluene 5 ug/mL trans-1,2-Dichloroethene 5 ug/mL trans-1,3-Dichloropropene 5 ug/mL Trichloroethene 5 ug/mL Bromomethane 5 ug/mL GAS STD WK RE_00244 50 uLChloroethane 5 ug/mL Chloromethane 5 ug/mL Dichlorodifluoromethane 5 ug/mL Trichlorofluoromethane 5 ug/mL Vinyl chloride 5 ug/mL 2-Butanone (MEK) 5 ug/mL KET/CS2 STDWK_00180 50 uL2-Hexanone 5 ug/mL 4-Methyl-2-pentanone (MIBK) 5 ug/mL Acetone 5 ug/mL Carbon disulfide 5 ug/mL 2-Chloroethyl vinyl ether 5 ug/mL VA/2CEVESTDWK_00175 50 uLVinyl acetate 5 ug/mL 8260 STD STK_00033 1,1,1,2-Tetrachloroethane 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 .8260 STD WK_00212 METHANOL, Lot NA 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL 

## 01/03/2013 Page 89 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL 08/31/14 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL Restek, Lot A088677 ..8260 STD STK_00033 1,1,1-Trichloroethane 100 ug/mL 1,1,2,2-Tetrachloroethane 100 ug/mL 1,1,2-Trichloro-1,2,2-trifluor oethane 100 ug/mL 1,1,2-Trichloroethane 100 ug/mL 1,1-Dichloroethane 100 ug/mL 1,1-Dichloroethene 100 ug/mL 1,1-Dichloropropene 100 ug/mL 1,2,3-Trichlorobenzene 100 ug/mL 1,2,3-Trichloropropane 100 ug/mL 1,2,4-Trichlorobenzene 100 ug/mL 1,2,4-Trimethylbenzene 100 ug/mL 1,2-Dibromo-3-Chloropropane 100 ug/mL 1,2-Dichlorobenzene 100 ug/mL 1,2-Dichloroethane 100 ug/mL 1,2-Dichloropropane 100 ug/mL 1,3,5-Trimethylbenzene 100 ug/mL 1,3-Dichlorobenzene 100 ug/mL 1,3-Dichloropropane 100 ug/mL 

## 01/03/2013 Page 90 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 1,4-Dichlorobenzene 100 ug/mL 1-Chlorohexane 100 ug/mL 2,2-Dichloropropane 100 ug/mL 2-Chlorotoluene 100 ug/mL 4-Chlorotoluene 100 ug/mL 4-Isopropyltoluene 100 ug/mL Benzene 100 ug/mL Bromobenzene 100 ug/mL Bromoform 100 ug/mL Carbon tetrachloride 100 ug/mL Chlorobenzene 100 ug/mL Chlorobromomethane 100 ug/mL Chlorodibromomethane 100 ug/mL Chloroform 100 ug/mL cis-1,2-Dichloroethene 100 ug/mL cis-1,3-Dichloropropene 100 ug/mL Dibromomethane 100 ug/mL Dichlorobromomethane 100 ug/mL Ethylbenzene 100 ug/mL Ethylene Dibromide 100 ug/mL Hexachlorobutadiene 100 ug/mL Isopropylbenzene 100 ug/mL m-Xylene & p-Xylene 200 ug/mL Methyl tert-butyl ether 100 ug/mL Methylene Chloride 100 ug/mL n-Butylbenzene 100 ug/mL N-Propylbenzene 100 ug/mL Naphthalene 100 ug/mL o-Xylene 100 ug/mL sec-Butylbenzene 100 ug/mL Styrene 100 ug/mL tert-Butylbenzene 100 ug/mL Tetrachloroethene 100 ug/mL Tetrahydrofuran 100 ug/mL Toluene 100 ug/mL trans-1,2-Dichloroethene 100 ug/mL trans-1,3-Dichloropropene 100 ug/mL Trichloroethene 100 ug/mL GAS STD SK_00027 Bromomethane 100 ug/mL 2 mL 2 mL 11/26/1211/19/12 .GAS STD WK RE_00244 METHANOL, Lot NA Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL 08/31/14 (Purchased Reagent) Bromomethane 100 ug/mL RESTEK, Lot A088739 ..GAS STD SK_00027 Chloroethane 100 ug/mL Chloromethane 100 ug/mL Dichlorodifluoromethane 100 ug/mL 

## 01/03/2013 Page 91 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Trichlorofluoromethane 100 ug/mL Vinyl chloride 100 ug/mL KET/CS2 SK_00013 2-Butanone (MEK) 100 ug/mL 2 mL 2 mL 12/03/1211/19/12 .KET/CS2 STDWK_00180 METHANOL, Lot NA 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 11/30/13 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL Restek, Lot A088681 ..KET/CS2 SK_00013 2-Hexanone 100 ug/mL 4-Methyl-2-pentanone (MIBK) 100 ug/mL Acetone 100 ug/mL Carbon disulfide 100 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/26/1211/19/12 .VA/2CEVESTDWK_00175 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL ..2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ...2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL ..VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ...VA STD SK_00007 ACR/NITRSTDWK_00204 Acetonitrile 80 ug/mL 1 mL 100 uL 11/21/1211/14/12 LOWACRSTD WK_00188 MEOH, Lot DG596 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/21/1211/14/12 .ACR/NITRSTDWK_00204 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 ..ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL ACR/NITRSTDWK_00205 Acetonitrile 80 ug/mL 1 mL 100 uL 11/26/1211/19/12 LOWACRSTD WK_00189 MEOH, Lot DG596 Acrolein 400 ug/mL Acrylonitrile 80 ug/mL Propionitrile 80 ug/mL ACRNITSTDSK_00032 Acetonitrile 800 ug/mL 2 mL 2 mL 11/26/1211/19/12 .ACR/NITRSTDWK_00205 METHANOL, Lot NA Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 12/31/12 (Purchased Reagent) Acetonitrile 800 ug/mL Restek, Lot A090686 ..ACRNITSTDSK_00032 Acrolein 4000 ug/mL Acrylonitrile 800 ug/mL Propionitrile 800 ug/mL 05/31/17 (Purchased Reagent) Mercury 1000 ug/mL ULTRA, Lot L00365 M11FSTKHG_00001 01/01/13 (Purchased Reagent) Mercury 1000 ug/mL Inorganic Ventures, Lot E2-HG02091 M12ASTKHG_00001 M12ESTKIC_00003 As 10 ug/mL 500 mL 3 mL 05/23/1310/04/12 M12JSPKIC_00002 1, Lot N\A Lead 10 ug/mL M12ESTKIC_00006 4 mL 

## 01/03/2013 Page 92 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Tl 10 ug/mL M12ESTKIC_00010 2.5 mLAl 200 ug/mL M12ESTKIC_00011 50 mLBarium 200 ug/mL Ca 1000 ug/mL K 1000 ug/mL Mg 1000 ug/mL Na 1000 ug/mL As 10 ug/mL M12ESTKIC_00012 50 mLB 100 ug/mL Be 5 ug/mL Bi 50 ug/mL Cd 5 ug/mL Chromium 20 ug/mL Co 50 ug/mL Copper 25 ug/mL Fe 100 ug/mL Lead 10 ug/mL Li 50 ug/mL Mn 50 ug/mL Nickel 50 ug/mL Se 10 ug/mL Sr 100 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 50 ug/mL Ag 5 ug/mL M12ESTKIC_00013 50 mLMo 100 ug/mL Sb 50 ug/mL Si 500 ug/mL Sn 100 ug/mL Ti 100 ug/mL M12ISTKIC_00004 4.5 mLSe 10 ug/mL 06/01/13 (Purchased Reagent) As 1000 ug/mL IV, Lot F2-AS02083 .M12ESTKIC_00003 06/01/13 (Purchased Reagent) Lead 1000 ug/mL IV, Lot F2-PB03035 .M12ESTKIC_00006 06/01/13 (Purchased Reagent) Tl 1000 ug/mL IV, Lot E2-TL01124 .M12ESTKIC_00010 05/23/13 (Purchased Reagent) Al 2000 ug/mL EE, Lot 1214205 .M12ESTKIC_00011 Barium 2000 ug/mL Ca 10000 ug/mL K 10000 ug/mL Mg 10000 ug/mL Na 10000 ug/mL 05/23/13 (Purchased Reagent) As 40 ug/mL EE, Lot 1214206 .M12ESTKIC_00012 B 1000 ug/mL Be 50 ug/mL Bi 500 ug/mL Cd 50 ug/mL Chromium 200 ug/mL Co 500 ug/mL 

## 01/03/2013 Page 93 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Copper 250 ug/mL Fe 1000 ug/mL Lead 20 ug/mL Li 500 ug/mL Mn 500 ug/mL Nickel 500 ug/mL Se 10 ug/mL Sr 1000 ug/mL Tl 50 ug/mL Vanadium 500 ug/mL Zinc 500 ug/mL 05/23/13 (Purchased Reagent) Ag 50 ug/mL EE, Lot 1214331 .M12ESTKIC_00013 Mo 1000 ug/mL Sb 500 ug/mL Si 5000 ug/mL Sn 1000 ug/mL Ti 1000 ug/mL 09/01/13 (Purchased Reagent) Se 1000 ug/mL IV, Lot E2-SE02033 .M12ISTKIC_00004 M12ESTKIC_00003 As 10 ug/mL 500 mL 3 mL 05/23/1311/20/12 M12KSPKIC_00001 1, Lot N\A Lead 10 ug/mL M12ESTKIC_00006 4 mLTl 10 ug/mL M12ESTKIC_00010 2.5 mLAl 200 ug/mL M12ESTKIC_00011 50 mLBarium 200 ug/mL Ca 1000 ug/mL K 1000 ug/mL Mg 1000 ug/mL Na 1000 ug/mL As 10 ug/mL M12ESTKIC_00012 50 mLB 100 ug/mL Be 5 ug/mL Bi 50 ug/mL Cd 5 ug/mL Chromium 20 ug/mL Co 50 ug/mL Copper 25 ug/mL Fe 100 ug/mL Lead 10 ug/mL Li 50 ug/mL Mn 50 ug/mL Nickel 50 ug/mL Se 10 ug/mL Sr 100 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 50 ug/mL Ag 5 ug/mL M12ESTKIC_00013 50 mLMo 100 ug/mL 

## 01/03/2013 Page 94 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Sb 50 ug/mL Si 500 ug/mL Sn 100 ug/mL Ti 100 ug/mL M12ISTKIC_00004 4.5 mLSe 10 ug/mL 06/01/13 (Purchased Reagent) As 1000 ug/mL IV, Lot F2-AS02083 .M12ESTKIC_00003 06/01/13 (Purchased Reagent) Lead 1000 ug/mL IV, Lot F2-PB03035 .M12ESTKIC_00006 06/01/13 (Purchased Reagent) Tl 1000 ug/mL IV, Lot E2-TL01124 .M12ESTKIC_00010 05/23/13 (Purchased Reagent) Al 2000 ug/mL EE, Lot 1214205 .M12ESTKIC_00011 Barium 2000 ug/mL Ca 10000 ug/mL K 10000 ug/mL Mg 10000 ug/mL Na 10000 ug/mL 05/23/13 (Purchased Reagent) As 40 ug/mL EE, Lot 1214206 .M12ESTKIC_00012 B 1000 ug/mL Be 50 ug/mL Bi 500 ug/mL Cd 50 ug/mL Chromium 200 ug/mL Co 500 ug/mL Copper 250 ug/mL Fe 1000 ug/mL Lead 20 ug/mL Li 500 ug/mL Mn 500 ug/mL Nickel 500 ug/mL Se 10 ug/mL Sr 1000 ug/mL Tl 50 ug/mL Vanadium 500 ug/mL Zinc 500 ug/mL 05/23/13 (Purchased Reagent) Ag 50 ug/mL EE, Lot 1214331 .M12ESTKIC_00013 Mo 1000 ug/mL Sb 500 ug/mL Si 5000 ug/mL Sn 1000 ug/mL Ti 1000 ug/mL 09/01/13 (Purchased Reagent) Se 1000 ug/mL IV, Lot E2-SE02033 .M12ISTKIC_00004 M12GSTKIC_00002 Barium 0.5 ug/mL 1000 mL 10 mL 07/10/1312/10/12 M12LCCVIC_00001 1, Lot N/A Chromium 0.5 ug/mL Copper 0.5 ug/mL Lead 0.5 ug/mL Nickel 0.5 ug/mL Vanadium 5 ug/mL Zinc 0.5 ug/mL 07/10/13 (Purchased Reagent) Barium 50 ug/mL HP, Lot 1219103 .M12GSTKIC_00002 

## 01/03/2013 Page 95 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Chromium 50 ug/mL Copper 50 ug/mL Lead 50 ug/mL Nickel 50 ug/mL Vanadium 500 ug/mL Zinc 50 ug/mL M12ESTKIC_00002 Barium 20 ug/L 1000 mL 2 mL 06/01/1312/03/12 M12LCRIIC_00001 1, Lot NA Chromium 20 ug/L Copper 20 ug/L Lead 10 ug/L Nickel 20 ug/L Vanadium 10 ug/L Zinc 40 ug/L 06/01/13 (Purchased Reagent) Barium 10 ug/mL IV, Lot F2-MEB423074 .M12ESTKIC_00002 Chromium 10 ug/mL Copper 10 ug/mL Lead 5 ug/mL Nickel 10 ug/mL Vanadium 5 ug/mL Zinc 20 ug/mL M12GSTKIC_00002 Barium 0.4 ug/mL 1000 mL 8 mL 07/10/1312/06/12 M12LICVIC_00001 1, Lot N/A Chromium 0.4 ug/mL Copper 0.4 ug/mL Lead 0.4 ug/mL Nickel 0.4 ug/mL Vanadium 4 ug/mL Zinc 0.4 ug/mL 07/10/13 (Purchased Reagent) Barium 50 ug/mL HP, Lot 1219103 .M12GSTKIC_00002 Chromium 50 ug/mL Copper 50 ug/mL Lead 50 ug/mL Nickel 50 ug/mL Vanadium 500 ug/mL Zinc 50 ug/mL M12KSTKIC_00003 Al 500 ug/mL 1000 mL 100 mL 12/01/1312/03/12 M12LISAIC_00001 1, Lot na Ca 500 ug/mL Fe 200 ug/mL Mg 500 ug/mL 12/01/13 (Purchased Reagent) Al 5000 ug/mL IV, Lot F2-meb414132 .M12KSTKIC_00003 Ca 5000 ug/mL Fe 2000 ug/mL Mg 5000 ug/mL M12ISTKIC_00003 Ag 0.2 ug/mL 1000 mL 10 mL 09/01/1312/03/12 M12LISBIC_00001 1, Lot B51037 As 0.1 ug/mL Barium 0.5 ug/mL Be 0.5 ug/mL 

## 01/03/2013 Page 96 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte Cd 1 ug/mL Chromium 0.5 ug/mL Co 0.5 ug/mL Copper 0.5 ug/mL Lead 0.05 ug/mL Mn 0.5 ug/mL Nickel 1 ug/mL Sb 0.6 ug/mL Se 0.05 ug/mL Tl 0.1 ug/mL Vanadium 0.5 ug/mL Zinc 1 ug/mL Al 500 ug/mL M12KSTKIC_00003 100 mLCa 500 ug/mL Fe 200 ug/mL Mg 500 ug/mL 09/01/13 (Purchased Reagent) Ag 20 ug/mL IV, Lot E2-MEB399019 .M12ISTKIC_00003 As 10 ug/mL Barium 50 ug/mL Be 50 ug/mL Cd 100 ug/mL Chromium 50 ug/mL Co 50 ug/mL Copper 50 ug/mL Lead 5 ug/mL Mn 50 ug/mL Nickel 100 ug/mL Sb 60 ug/mL Se 5 ug/mL Tl 10 ug/mL Vanadium 50 ug/mL Zinc 100 ug/mL 12/01/13 (Purchased Reagent) Al 5000 ug/mL IV, Lot F2-meb414132 .M12KSTKIC_00003 Ca 5000 ug/mL Fe 2000 ug/mL Mg 5000 ug/mL 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/21/1211/14/12 VA/2CEVESTDWK_00174 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00024 METHANOL, Lot NA 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 2-CEVE STD PT_00023 2-Chloroethyl vinyl ether 100 ug/mL 2 mL 100 uL 11/26/1211/19/12 VA/2CEVESTDWK_00175 METHANOL, Lot DG860 VA STD PT_00024 100 uLVinyl acetate 100 ug/mL 01/08/1310/08/12 1 mL2-CEVESTDSK_00005 1 mL2-Chloroethyl vinyl ether 2000 ug/mL .2-CEVE STD PT_00023 METHANOL, Lot NA 11/30/16 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL Restek, Lot A085117 ..2-CEVESTDSK_00005 01/10/1310/11/12 1 mLVA STD SK_00007 1 mLVinyl acetate 2000 ug/mL .VA STD PT_00024 METHANOL, Lot NA 

## 01/03/2013 Page 97 of 383

### REAGENT TRACEABILITY SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Reagent ID Exp Date Date Prep Dilutant Used Reagent Final Volume Parent Reagent Reagent ID Volume Added Concentration Analyte 03/31/14 (Purchased Reagent) Vinyl acetate 2000 ug/mL RESTEK, Lot A090525 ..VA STD SK_00007 8260ADDSPKPT_00024 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 11/19/1211/13/12 VOC/THF SPK_00122 1, Lot DG596 Acetone 50 mg/L 8260ADDSPKSK_00014 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 11/19/1210/08/12 .8260ADDSPKPT_00024 1, Lot NA Acetone 2000 mg/L 11/19/12 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212071076 ..8260ADDSPKSK_00014 Acetone 2000 mg/L 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/03/1211/19/12 VOC/THF SPK_00124 1, Lot DG596 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 8260ADDSPKPT_00025 2-Butanone (MEK) 50 mg/L 2 mL 50 uL 12/25/1212/11/12 VOC/THF SPK_00127 1, Lot DG860 Acetone 50 mg/L 8260ADDSPKSK_00015 2-Butanone (MEK) 2000 mg/L 1 mL 1 mL 01/19/1311/19/12 .8260ADDSPKPT_00025 1, Lot NA Acetone 2000 mg/L 01/19/13 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L ACCUSTD, Lot 212091219 ..8260ADDSPKSK_00015 Acetone 2000 mg/L 04/30/15 (Purchased Reagent) Chromium, hexavalent 1000 mg/L ERA, Lot 160412 WSTCR1_00008 12/25/12 (Purchased Reagent) Chromium, hexavalent 38.64 mg/L STL, Lot Lead(II)Chrom_00001 WSTCR13_00623 05/31/17 (Purchased Reagent) Chromium, hexavalent 1000 mg/L Ultra Scientific, Lot L00439 WSTCR2_00008 12/18/1212/18/12 100 mLWSTCN1_00011 1 mLCyanide, Total 10 mg/L WSTINCN1_00567 DI WATER, Lot NA 01/31/14 (Purchased Reagent) Cyanide, Total 1000 mg/L ERA, Lot 060112 .WSTCN1_00011 WSTCN2_00028 Cyanide, Amenable 10 mg/L 100 mL 1 mL 12/18/1212/18/12 WSTINCN2_00559 DI WATER, Lot NA Cyanide, Free 10 mg/L Cyanide, Reactive 10 mg/L Cyanide, Total 10 mg/L Cyanide, Weak Acid Dissociable 10 mg/L 03/31/13 (Purchased Reagent) Cyanide, Amenable 1000 mg/L RICCA, Lot 4204518 .WSTCN2_00028 Cyanide, Free 1000 mg/L Cyanide, Reactive 1000 mg/L Cyanide, Total 1000 mg/L Cyanide, Weak Acid Dissociable 1000 mg/L 11/15/13 (Purchased Reagent) Sulfide 180 mg/L NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL WSTSF1_00036 Sulfide as H2S 209.1 mg/L Sulfide, Reactive 180 mg/L



## 01/03/2013 Page 98 of 383

# Certification Summary Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1 Project/Site:John Deere Des MoinesWorks(JDDMW)

Laboratory Authority Program EPA Region Certification ID TestAmerica Chicago 40461 State Program Alabama 4 TestAmerica Chicago 01132CA NELAP California 9 TestAmerica Chicago 939 State Program Georgia 4 TestAmerica Chicago N/A State Program Georgia 4 TestAmerica Chicago N/A State Program Hawaii 9 TestAmerica Chicago 100201 NELAP Illinois 5 TestAmerica Chicago C-IL-02 State Program Indiana 5 TestAmerica Chicago 82 State Program Iowa 7 TestAmerica Chicago E-10161 NELAP Kansas 7 TestAmerica Chicago 90023 State Program Kentucky 4 TestAmerica Chicago 66 State Program Kentucky (UST) 4 TestAmerica Chicago L2304 DoD ELAP L-A-B TestAmerica Chicago L2304 ISO/IEC 17025 L-A-B TestAmerica Chicago 30720 NELAP Louisiana 6 TestAmerica Chicago M-IL035 State Program Massachusetts 1 TestAmerica Chicago N/A State Program Mississippi 4 TestAmerica Chicago 291 State Program North Carolina DENR 4 TestAmerica Chicago R-194 State Program North Dakota 8 TestAmerica Chicago 8908 State Program Oklahoma 6 TestAmerica Chicago 77001 State Program South Carolina 4 TestAmerica Chicago T104704252-09-TX NELAP Texas 6 TestAmerica Chicago P330-12-00038 Federal USDA TestAmerica Chicago 460142 NELAP Virginia 3 TestAmerica Chicago 999580010 State Program Wisconsin 5 TestAmerica Chicago 8TMS-Q State Program Wyoming 8 Accreditation may not be offered or required for all methods and analytes reported in this package

.Please contact your project manager for the laboratory’s current list of certified methods and analytes.



### TestAmerica Chicago 

## 01/03/2013 Page 99 of 383

# Method 8260B Volatile Organic Compounds (GC/MS) by Method 8260B

01/03/2013

Page 100 of 383

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53315-1 SDG No.: Matrix:Solid Level:Low TestAmerica Chicago

GC Column (1):DB624 ID:0.2(mm)
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53315-3 FC DISCRETE 4 113 116 98 91 500-53315-4 FC D DISCRETE 4 112 117 97 85 MB 500-173225/4 106 106 113 104 LCS 500-173225/5 105 104 111 103 500-53315-3 MS FC DISCRETE 4 MS 118 117 95 85 500-53315-3 MSD FC DISCRETE 4 MSD 116 119 96 84



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 70-134 TOL = Toluene-d8 (Surr) 75-122 BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B # Column to be used to flag recovery values


## 01/03/2013 Page 101 of 383

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53315-1 SDG No.: Matrix:Solid Level:Medium TestAmerica Chicago

GC Column (1): ID:
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53315-3 DL FC DISCRETE 4 DL 105 109 97 91 500-53315-4 DL FC D DISCRETE 4 DL 116 119 93 90 MB 500-173509/6 96 101 95 94 LCS 500-173509/4 98 102 97 99



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 75-125 TOL = Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B # Column to be used to flag recovery values


## 01/03/2013 Page 102 of 383

### FORM II GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.:500-53315-1 SDG No.: Matrix:Water Level:Low TestAmerica Chicago

GC Column (1): ID:
# Lab Sample ID Client Sample ID # # # DBFM DCA TOL BFB 500-53315-5 TRIP BLANK 109 105 100 97 500-53315-6 FC EB 4 107 107 99 94 MB 500-173508/6 96 101 95 94 LCS 500-173508/4 98 102 97 99



### QC LIMITS QC LIMITS DBFM = Dibromofluoromethane 75-120 DCA = 1,2-Dichloroethane-d4 (Surr) 75-125 TOL = Toluene-d8 (Surr) 75-120 BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B # Column to be used to flag recovery values


## 01/03/2013 Page 103 of 383

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53315-1

Lab File ID:16S1218.D Solid Lab ID:LCS 500-173225/5 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/Kg) SPIKE ADDED (ug/Kg) # LCS LCS COMPOUND Acetone 50.0 45.56 50-138 91 2-Butanone (MEK) 50.0 52.85 58-133 106

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/03/2013 Page 104 of 383

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53315-1

Lab File ID:25S1219p.D Water Lab ID:LCS 500-173508/4 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/L) SPIKE ADDED (ug/L) # LCS LCS COMPOUND Acetone 50.0 52.35 46-153 105 2-Butanone (MEK) 50.0 53.39 54-138 107

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/03/2013 Page 105 of 383

### GC/MS VOA LAB CONTROL SAMPLE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Medium 500-53315-1

Lab File ID:25S1219p.D Solid Lab ID:LCS 500-173509/4 Client ID: TestAmerica Chicago

REC % REC QC LIMITS CONCENTRATION (ug/Kg) SPIKE ADDED (ug/Kg) # LCS LCS COMPOUND Acetone 50.0 52.35 46-153 105 2-Butanone (MEK) 50.0 53.39 54-138 107

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/03/2013 Page 106 of 383

### GC/MS VOA MATRIX SPIKE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53315-1

Lab File ID:53315-03s.D Solid Lab ID:500-53315-3 MS Client ID:FC DISCRETE 4 MS TestAmerica Chicago

LIMITS COMPOUND CONCENTRATION % REC QC REC SAMPLE CONCENTRATION SPIKE ADDED (ug/Kg) (ug/Kg) (ug/Kg) # MS MS

173 7120 50-138 Acetone 104 6940 E 4 173 329.3 58-133 2-Butanone (MEK) 106 145

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/03/2013 Page 107 of 383

### GC/MS VOA MATRIX SPIKE DUPLICATE RECOVERY FORM III

Job No.: Lab Name: SDG No.: Level: Matrix: Matrix: Low 500-53315-1

Lab File ID:53315-03t.D Solid Lab ID:500-53315-3 MSD Client ID:FC DISCRETE 4 MSD TestAmerica Chicago

COMPOUND SPIKE ADDED CONCENTRATION % REC % RPD QC LIMITS
RPD REC (ug/Kg) (ug/Kg) # MSD MSD

173 7629 30 50-138 Acetone 7 399 E 4 173 303.4 30 58-133 2-Butanone (MEK) 8 91

FORM III 8260B # Column to be used to flag recovery and RPD values


## 01/03/2013 Page 108 of 383

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/20/2012 00:43 N Heated Purge:(Y/N) CMS25 25M1219p.D Lab File ID: Lab Sample ID:MB 500-173509/6 Solid Matrix:

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/19/2012 23:54 25S1219p.D LCS 500-173509/4 12/20/2012 02:16 53315-03.D 500-53315-3 DL FC DISCRETE 4 DL 12/20/2012 02:40 53315-04.D 500-53315-4 DL FC D DISCRETE 4 DL

FORM IV 8260B 

## 01/03/2013 Page 109 of 383

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/18/2012 08:30 DB624 Y Heated Purge:(Y/N) CMS16 16M1218.D Lab File ID: Lab Sample ID:MB 500-173225/4 Solid Matrix:
0.2(mm) THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/18/2012 08:53 16S1218.D LCS 500-173225/5 12/18/2012 09:30 53315-03.D 500-53315-3 FC DISCRETE 4 12/18/2012 09:54 53315-03s.D 500-53315-3 MS FC DISCRETE 4 MS 12/18/2012 10:17 53315-03t.D 500-53315-3 MSD FC DISCRETE 4 MSD 12/18/2012 10:40 53315-04.D 500-53315-4 FC D DISCRETE 4

FORM IV 8260B 

## 01/03/2013 Page 110 of 383

### FORM IV GC/MS VOA METHOD BLANK SUMMARY

Lab Name: SDG No.: Job No.:500-53315-1 TestAmerica Chicago

Date Analyzed: GC Column: ID: Instrument ID: 12/20/2012 00:43 N Heated Purge:(Y/N) CMS25 25M1219p.D Lab File ID: Lab Sample ID:MB 500-173508/6 Water Matrix:

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID LAB FILE ID DATE ANALYZED CLIENT SAMPLE ID 12/19/2012 23:54 25S1219p.D LCS 500-173508/4 12/20/2012 01:08 53315-05.D 500-53315-5 TRIP BLANK 12/20/2012 01:49 53315-06.D 500-53315-6 FC EB 4

FORM IV 8260B 

## 01/03/2013 Page 111 of 383

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53315-1

Lab File ID: Instrument ID:16B1119c.D CMS16 11/19/2012 11:14 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 170196

5015.0 - 40.0 % of mass 95 19.7 7530.0 - 60.0 % of mass 95 53.5 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.5 173Less than 2.0 % of mass 174 0.7 (1.0)1 17450.0 - 120.00 % of mass 95 75.9 1755.0 - 9.0 % of mass 174 5.3 (6.9)1 17695.0 - 101.0 % of mass 174 74.4 (98.0)1 1775.0 - 9.0 % of mass 176 5.8 (7.8)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 16I1119A.D 11/19/2012 12:14 STD1 500-170196/6 16I1119B.D 11/19/2012 12:37 STD2 500-170196/7 16I1119C.D 11/19/2012 13:00 STD3 500-170196/8 16I1119D.D 11/19/2012 13:23 STD4 500-170196/9 16I1119E.D 11/19/2012 13:46 STD5 500-170196/10 16I1119F.D 11/19/2012 14:09 STD6 500-170196/11 16S1119.D 11/19/2012 17:14 ICV 500-170196/19

FORM V 8260B 

## 01/03/2013 Page 112 of 383

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53315-1

Lab File ID: Instrument ID:16B1218.D CMS16 12/18/2012 07:09 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173225

5015.0 - 40.0 % of mass 95 19.8 7530.0 - 60.0 % of mass 95 50.0 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 7.8 173Less than 2.0 % of mass 174 0.2 (0.3)1 17450.0 - 120.00 % of mass 95 74.6 1755.0 - 9.0 % of mass 174 6.4 (8.6)1 17695.0 - 101.0 % of mass 174 71.2 (95.4)1 1775.0 - 9.0 % of mass 176 3.9 (5.4)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 16C1218.D 12/18/2012 07:43 CCV 500-173225/2 16D1218.D 12/18/2012 08:07 CCV 500-173225/3 16M1218.D 12/18/2012 08:30 MB 500-173225/4 16S1218.D 12/18/2012 08:53 LCS 500-173225/5 FC DISCRETE 4 53315-03.D 12/18/2012 09:30 500-53315-3 FC DISCRETE 4 MS 53315-03s. D 12/18/2012 09:54 500-53315-3 MS FC DISCRETE 4 MSD 53315-03t. D 12/18/2012 10:17 500-53315-3 MSD FC D DISCRETE 4 53315-04.D 12/18/2012 10:40 500-53315-4

FORM V 8260B 

## 01/03/2013 Page 113 of 383

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53315-1

Lab File ID: Instrument ID:25B1114.D CMS25 11/14/2012 09:17 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 169636

5015.0 - 40.0 % of mass 95 26.1 7530.0 - 60.0 % of mass 95 46.8 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 6.8 173Less than 2.0 % of mass 174 0.8 (1.0)1 17450.0 - 120.00 % of mass 95 78.1 1755.0 - 9.0 % of mass 174 5.6 (7.2)1 17695.0 - 101.0 % of mass 174 77.7 (99.5)1 1775.0 - 9.0 % of mass 176 5.0 (6.4)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 25I1114a.D 11/14/2012 09:41 STD1 500-169636/2 25I1114b.D 11/14/2012 10:05 STD2 500-169636/3 25I1114c.D 11/14/2012 10:29 STD3 500-169636/4 25I1114d.D 11/14/2012 10:53 STD4 500-169636/5 25I1114e.D 11/14/2012 11:18 STD5 500-169636/6 25I1114f.D 11/14/2012 11:42 STD6 500-169636/7 25I1114g.D 11/14/2012 12:06 STD7 500-169636/8 25I1114h.D 11/14/2012 12:30 STD8 500-169636/9 25I1114i.D 11/14/2012 12:54 STD9 500-169636/10 25S1114.D 11/14/2012 16:57 ICV 500-169636/20

FORM V 8260B 

## 01/03/2013 Page 114 of 383

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53315-1

Lab File ID: Instrument ID:25B1114.D CMS25 11/14/2012 09:17 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 169637

5015.0 - 40.0 % of mass 95 26.1 7530.0 - 60.0 % of mass 95 46.8 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 6.8 173Less than 2.0 % of mass 174 0.8 (1.0)1 17450.0 - 120.00 % of mass 95 78.1 1755.0 - 9.0 % of mass 174 5.6 (7.2)1 17695.0 - 101.0 % of mass 174 77.7 (99.5)1 1775.0 - 9.0 % of mass 176 5.0 (6.4)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 25I1114a.D 11/14/2012 09:41 STD1 500-169637/2 25I1114b.D 11/14/2012 10:05 STD2 500-169637/3 25I1114c.D 11/14/2012 10:29 STD3 500-169637/4 25I1114d.D 11/14/2012 10:53 STD4 500-169637/5 25I1114e.D 11/14/2012 11:18 STD5 500-169637/6 25I1114f.D 11/14/2012 11:42 STD6 500-169637/7 25I1114g.D 11/14/2012 12:06 STD7 500-169637/8 25I1114h.D 11/14/2012 12:30 STD8 500-169637/9 25I1114i.D 11/14/2012 12:54 STD9 500-169637/10 25S1114.D 11/14/2012 16:57 ICV 500-169637/20

FORM V 8260B 

## 01/03/2013 Page 115 of 383

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53315-1

Lab File ID: Instrument ID:25B1219p.D CMS25 12/19/2012 22:40 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173508

5015.0 - 40.0 % of mass 95 20.1 7530.0 - 60.0 % of mass 95 45.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 5.6 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 112.8 1755.0 - 9.0 % of mass 174 7.3 (6.4)1 17695.0 - 101.0 % of mass 174 109.9 (97.5)1 1775.0 - 9.0 % of mass 176 6.9 (6.2)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 25C1219p.D 12/19/2012 23:06 CCV 500-173508/2 25D1219p.D 12/19/2012 23:30 CCV 500-173508/3 25S1219p.D 12/19/2012 23:54 LCS 500-173508/4 25M1219p.D 12/20/2012 00:43 MB 500-173508/6 TRIP BLANK 53315-05.D 12/20/2012 01:08 500-53315-5 FC EB 4 53315-06.D 12/20/2012 01:49 500-53315-6

FORM V 8260B 

## 01/03/2013 Page 116 of 383

### FORM V BROMOFLUOROBENZENE (BFB)

Lab Name: SDG No.: Job No.:500-53315-1

Lab File ID: Instrument ID:25B1219p.D CMS25 12/19/2012 22:40 BFB Injection Date: BFB Injection Time:

M/EION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE Analysis Batch No.: 173509

5015.0 - 40.0 % of mass 95 20.1 7530.0 - 60.0 % of mass 95 45.2 95Base Peak, 100% relative abundance 100.0 965.0 - 9.0 % of mass 95 5.6 173Less than 2.0 % of mass 174 0.0 (0.0)1 17450.0 - 120.00 % of mass 95 112.8 1755.0 - 9.0 % of mass 174 7.3 (6.4)1 17695.0 - 101.0 % of mass 174 109.9 (97.5)1 1775.0 - 9.0 % of mass 176 6.9 (6.2)2 1-Value is % mass 174 2-Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS: GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID LAB FILE ID LAB SAMPLE ID DATE ANALYZED TIME ANALYZED 25C1219p.D 12/19/2012 23:06 CCV 500-173509/2 25D1219p.D 12/19/2012 23:30 CCV 500-173509/3 25S1219p.D 12/19/2012 23:54 LCS 500-173509/4 25M1219p.D 12/20/2012 00:43 MB 500-173509/6 FC DISCRETE 4 DL 53315-03.D 12/20/2012 02:16 500-53315-3 DL FC D DISCRETE 4 DL 53315-04.D 12/20/2012 02:40 500-53315-4 DL

FORM V 8260B 

## 01/03/2013 Page 117 of 383

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53315-1
Sample No.:STD3 500-170196/8 Date Analyzed:11/19/2012 13:00
Lab File ID (Standard): 16I1119C.D Instrument ID:CMS16 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) Y Calibration ID:10620

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 464716 116179 170040 680160 134826 539304 3.42 3.99 6.38 INITIAL CALIBRATION MID-POINT 3.92 2.92 4.49 3.49 6.88 5.88 232358 340080 269652

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-170196/19 258949 378895 285510 3.42 3.99 6.38 CCV 500-173225/2 300281 435506 330057 3.41 3.99 6.38 CCV 500-173225/3 292123 413832 322880 3.42 3.99 6.38 MB 500-173225/4 272848 399265 312018 3.42 3.99 6.38 LCS 500-173225/5 290208 418105 323317 3.42 3.99 6.38 500-53315-3 FC DISCRETE 4 227570 339047 220989 3.42 3.99 6.38 500-53315-3 MS FC DISCRETE 4 MS 213499 331660 210155 3.42 3.99 6.38 500-53315-3 MSD FC DISCRETE 4 MSD 222386 342573 213812 3.42 3.99 6.38 500-53315-4 FC D DISCRETE 4 234392 348797 222533 3.42 3.99 6.38



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/03/2013 Page 118 of 383

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53315-1
Sample No.:STD3 500-170196/8 Date Analyzed:11/19/2012 13:00
Lab File ID (Standard): 16I1119C.D Instrument ID:CMS16 GC Column:DB624 ID:0.2(mm) Heated Purge: (Y/N) Y Calibration ID:10620

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 283260 70815 8.21 INITIAL CALIBRATION MID-POINT 8.71 7.71 141630

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-170196/19 139276 8.21 CCV 500-173225/2 157799 8.21 CCV 500-173225/3 156710 8.21 MB 500-173225/4 155307 8.21 LCS 500-173225/5 156529 8.22 500-53315-3 FC DISCRETE 4 65296* 8.22 500-53315-3 MS FC DISCRETE 4 MS 58501* 8.21 500-53315-3 MSD FC DISCRETE 4 MSD 57059* 8.21 500-53315-4 FC D DISCRETE 4 59961* 8.21



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/03/2013 Page 119 of 383

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53315-1
Sample No.:STD6 500-169636/7 Date Analyzed:11/14/2012 11:42
Lab File ID (Standard): 25I1114f.D Instrument ID:CMS25 GC Column: ID:() Heated Purge: (Y/N) N Calibration ID:10605

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 957684 239421 344275 1377100 275429 1101714 3.40 4.05 6.49 INITIAL CALIBRATION MID-POINT 3.90 2.90 4.55 3.55 6.99 5.99 478842 688550 550857

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-169636/20 466984 692259 555803 3.40 4.05 6.49 CCV 500-173509/2 480196 684781 547136 3.40 4.05 6.49 CCV 500-173509/3 505330 709189 565358 3.40 4.05 6.49 LCS 500-173509/4 497255 699991 565828 3.40 4.05 6.49 MB 500-173509/6 498155 711732 565897 3.40 4.05 6.49 500-53315-3 DL FC DISCRETE 4 DL 476846 702694 561857 3.40 4.05 6.49 500-53315-4 DL FC D DISCRETE 4 DL 428304 644386 482292 3.40 4.05 6.49



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/03/2013 Page 120 of 383

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53315-1
Sample No.:STD6 500-169636/7 Date Analyzed:11/14/2012 11:42
Lab File ID (Standard): 25I1114f.D Instrument ID:CMS25 GC Column: ID:() Heated Purge: (Y/N) N Calibration ID:10605

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 491836 122959 8.35 INITIAL CALIBRATION MID-POINT 8.85 7.85 245918

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-169636/20 239626 8.35 CCV 500-173509/2 250328 8.35 CCV 500-173509/3 267460 8.35 LCS 500-173509/4 265281 8.35 MB 500-173509/6 255019 8.35 500-53315-3 DL FC DISCRETE 4 DL 234564 8.35 500-53315-4 DL FC D DISCRETE 4 DL 181036 8.35



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/03/2013 Page 121 of 383

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53315-1
Sample No.:STD6 500-169637/7 Date Analyzed:11/14/2012 11:42
Lab File ID (Standard): 25I1114f.D Instrument ID:CMS25 GC Column: ID:() Heated Purge: (Y/N) N Calibration ID:10606

AREA# RT# AREA RT# AREA# RT# # PFB DFB CBZ

UPPER LIMIT LOWER LIMIT 957684 239421 344275 1377100 275429 1101714 3.40 4.05 6.49 INITIAL CALIBRATION MID-POINT 3.90 2.90 4.55 3.55 6.99 5.99 478842 688550 550857

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-169637/20 466984 692259 555803 3.40 4.05 6.49 CCV 500-173508/2 480196 684781 547136 3.40 4.05 6.49 CCV 500-173508/3 505330 709189 565358 3.40 4.05 6.49 LCS 500-173508/4 497255 699991 565828 3.40 4.05 6.49 MB 500-173508/6 498155 711732 565897 3.40 4.05 6.49 500-53315-5 TRIP BLANK 488133 739413 586574 3.40 4.05 6.49 500-53315-6 FC EB 4 499196 746245 595648 3.40 4.05 6.49



### PFB = Pentafluorobenzene DFB = 1,4-Difluorobenzene CBZ = Chlorobenzene-d5 Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/03/2013 Page 122 of 383

### GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.: SDG No.: FORM VIII

TestAmerica Chicago 500-53315-1
Sample No.:STD6 500-169637/7 Date Analyzed:11/14/2012 11:42
Lab File ID (Standard): 25I1114f.D Instrument ID:CMS25 GC Column: ID:() Heated Purge: (Y/N) N Calibration ID:10606

AREA# RT# AREA RT# AREA# RT# # DCB

UPPER LIMIT LOWER LIMIT 491836 122959 8.35 INITIAL CALIBRATION MID-POINT 8.85 7.85 245918

LAB SAMPLE ID CLIENT SAMPLE ID ICV 500-169637/20 239626 8.35 CCV 500-173508/2 250328 8.35 CCV 500-173508/3 267460 8.35 LCS 500-173508/4 265281 8.35 MB 500-173508/6 255019 8.35 500-53315-5 TRIP BLANK 252464 8.35 500-53315-6 FC EB 4 252293 8.35



### DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area RT Limit = ± 0.5 minutes of internal standard RT # Column used to flag values outside QC limits FORM VIII 8260B 

## 01/03/2013 Page 123 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC DISCRETE 4 SDG No.: 500-53315-1
Lab Sample ID:500-53315-3 Matrix: 53315-03.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/14/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

71.1 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/18/2012 09:30

ID: DB624
Analysis Batch No.: 173225 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL17.3 6.25 78-93-3 2-Butanone (MEK) 145


### %REC CAS NO. LIMITS Q SURROGATE 116 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 98 75-122 2037-26-5 Toluene-d8 (Surr) 91 70-122 460-00-4 4-Bromofluorobenzene (Surr) 113 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 124 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC DISCRETE 4 DL SDG No.: 500-53315-1
Lab Sample ID:500-53315-3 DL Matrix: 53315-03.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/14/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

71.1 50
Level: (low/med)Medium 5(g) 5 (mL) 5(mL) Date Analyzed:12/20/2012 02:16

ID:
Analysis Batch No.: 173509 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL864 225 67-64-1 Acetone 4220


### %REC CAS NO. LIMITS Q SURROGATE 109 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 91 75-120 460-00-4 4-Bromofluorobenzene (Surr) 105 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 125 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC D DISCRETE 4 SDG No.: 500-53315-1
Lab Sample ID:500-53315-4 Matrix: 53315-04.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/14/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

71.8 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/18/2012 10:40

ID: DB624
Analysis Batch No.: 173225 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL17.8 6.43 78-93-3 2-Butanone (MEK) 191


### %REC CAS NO. LIMITS Q SURROGATE 117 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-122 2037-26-5 Toluene-d8 (Surr) 85 70-122 460-00-4 4-Bromofluorobenzene (Surr) 112 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 126 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC D DISCRETE 4 DL SDG No.: 500-53315-1
Lab Sample ID:500-53315-4 DL Matrix: 53315-04.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/14/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

71.8 50
Level: (low/med)Medium 5(g) 5 (mL) 5(mL) Date Analyzed:12/20/2012 02:40

ID:
Analysis Batch No.: 173509 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL888 231 67-64-1 Acetone 8710


### %REC CAS NO. LIMITS Q SURROGATE 119 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 93 75-120 2037-26-5 Toluene-d8 (Surr) 90 75-120 460-00-4 4-Bromofluorobenzene (Surr) 116 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 127 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

TRIP BLANK SDG No.: 500-53315-1
Lab Sample ID:500-53315-5 Matrix: 53315-05.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

12/14/2012 00:00 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL) Date Analyzed:12/20/2012 01:08

ID:
Analysis Batch No.: 173508 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 105 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 100 75-120 2037-26-5 Toluene-d8 (Surr) 97 75-120 460-00-4 4-Bromofluorobenzene (Surr) 109 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 128 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC EB 4 SDG No.: 500-53315-1
Lab Sample ID:500-53315-6 Matrix: 53315-06.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

12/14/2012 14:30 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL) Date Analyzed:12/20/2012 01:49

ID:
Analysis Batch No.: 173508 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) 13.0


### %REC CAS NO. LIMITS Q SURROGATE 107 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 99 75-120 2037-26-5 Toluene-d8 (Surr) 94 75-120 460-00-4 4-Bromofluorobenzene (Surr) 107 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 129 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1 500-170196/6 16I1119A.D 2 Level STD2 500-170196/7 16I1119B.D 3 Level STD3 500-170196/8 16I1119C.D 4 Level STD4 500-170196/9 16I1119D.D 5 Level STD5 500-170196/10 16I1119E.D 6 Level STD6 500-170196/11 16I1119F.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Dichlorodifluoromethane 0.5101 0.4328 0.4745 0.4472 0.4791Ave 5.9 0.4553 0.0100 15.0 0.4665 Chloromethane 0.6409 0.5486 0.6042 0.5514 0.5726Ave 6.2 0.5611 0.1000 15.0 0.5798 Vinyl chloride 0.5489 0.4879 0.5232 0.4889 0.5055Ave 4.9 0.4889 0.0100 15.0 0.5072 Bromomethane 0.2173 0.1622 0.1619 0.1577 0.1599Lin2 0.9990 0.1594 0.0100 0.9900 0.30230.1550 Chloroethane 0.2848 0.2512 0.2658 0.2550 0.2653Ave 4.4 0.2627 0.0100 15.0 0.2641 Trichlorofluoromethane 0.6410 0.5479 0.5898 0.5813 0.5855Ave 5.1 0.5792 0.0100 15.0 0.5875 Acrolein 0.0833 0.0649 0.0739 0.0632 0.0635Lin2 0.9920 0.0576 0.0010 0.9900 4.11290.0627 1,1-Dichloroethene 0.3883 0.3810 0.3940 0.3681 0.3657Ave 4.2 0.3520 0.0100 15.0 0.3748 1,1,2-Trichloro-1,2,2-trifluoroethane 0.4271 0.3940 0.4076 0.3784 0.3788Ave 6.6 0.3531 0.0100 15.0 0.3898 Acetone 0.2177 0.1065 0.1169 0.1078 0.1047Lin1 0.9950 0.0952 0.0100 0.9900 0.55990.0976 Carbon disulfide 1.2281 1.2015 1.3462 1.3937 1.2778Ave 5.7 1.2592 0.0100 15.0 1.2844 Acetonitrile 0.0349 0.0327 0.0349 0.0328 0.0329Ave 6.1 0.0294 0.0010 15.0 0.0330 Methylene Chloride 0.4402 0.4262 0.4539 0.4254 0.4228Ave 4.4 0.3973 0.0100 15.0 0.4276 Acrylonitrile 0.1608 0.1223 0.1370 0.1213 0.1263Lin2 0.9950 0.1142 0.0010 0.9900 1.55620.1209 trans-1,2-Dichloroethene 0.4687 0.4410 0.4603 0.4325 0.4314Ave 4.6 0.4139 0.0100 15.0 0.4413



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 130 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 Methyl tert-butyl ether 1.2409 1.0967 1.2053 1.0887 1.1030Ave 7.6 1.0084 0.0100 15.0 1.1238 1,1-Dichloroethane 0.9158 0.8754 0.8985 0.8573 0.8580Ave 4.0 0.8171 0.1000 15.0 0.8704 Vinyl acetate 0.7794 0.7899 0.8439 0.8848 0.9027Ave 6.1 0.8075 0.0100 15.0 0.8347 2,2-Dichloropropane 0.5123 0.4762 0.4910 0.4760 0.4692Ave 5.5 0.4333 0.0100 15.0 0.4764 cis-1,2-Dichloroethene 0.5178 0.4752 0.4900 0.4699 0.4727Ave 4.9 0.4468 0.0100 15.0 0.4787 2-Butanone (MEK) 0.1907 0.1661 0.1744 0.1666 0.1738Ave 7.0 0.1547 0.0100 15.0 0.1710 Propionitrile 0.0377 0.0303 0.0325 0.0300 0.0310Ave 10.0 0.0283 0.0010 15.0 0.0316 Bromochloromethane 0.2134 0.1810 0.1955 0.1835 0.1826Ave 7.7 0.1724 0.0100 15.0 0.1881 Tetrahydrofuran 0.1362 0.1110 0.1157 0.1060 0.1101Lin2 0.9970 0.0981 0.0100 0.9900 0.15500.1053 Chloroform 0.8071 0.7676 0.7909 0.7569 0.7592Ave 3.9 0.7200 0.0100 15.0 0.7669 1,1,1-Trichloroethane 0.6379 0.6227 0.6514 0.6248 0.6266Ave 3.7 0.5828 0.0100 15.0 0.6244 Carbon tetrachloride 0.3601 0.3514 0.3626 0.3590 0.3620Ave 1.9 0.3457 0.0100 15.0 0.3568 1,1-Dichloropropene 0.6628 0.6440 0.6397 0.6320 0.6326Ave 3.2 0.6014 0.0100 15.0 0.6354 Benzene 1.2960 1.2332 1.2212 1.1893 1.1679Ave 5.2 1.1124 0.0100 15.0 1.2033 1,2-Dichloroethane 0.4036 0.3828 0.3925 0.3773 0.3822Ave 3.7 0.3615 0.0100 15.0 0.3833 Trichloroethene 0.3071 0.2871 0.2880 0.2787 0.2819Ave 4.3 0.2706 0.0100 15.0 0.2856 1,2-Dichloropropane 0.2945 0.3110 0.2983 0.3002 0.3013Ave 2.3 0.2903 0.0100 15.0 0.2993 Dibromomethane 0.1499 0.1401 0.1448 0.1410 0.1445Ave 3.6 0.1346 0.0100 15.0 0.1425 Bromodichloromethane 0.3131 0.3276 0.3492 0.3570 0.3677Ave 5.9 0.3548 0.0100 15.0 0.3449 2-Chloroethyl vinyl ether 0.1275 0.1289 0.1333 0.1400 0.1446Ave 5.1 0.1302 0.0100 15.0 0.1341



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 131 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 cis-1,3-Dichloropropene 0.3823 0.3878 0.3955 0.4081 0.4277Ave 4.1 0.4075 0.0100 15.0 0.4015 4-Methyl-2-pentanone (MIBK) 0.2134 0.2212 0.2438 0.2360 0.2310Ave 5.2 0.2176 0.0100 15.0 0.2272 Toluene 0.7563 0.7457 0.7103 0.7065 0.7016Ave 4.3 0.6724 0.0100 15.0 0.7155 trans-1,3-Dichloropropene 0.3019 0.3263 0.3366 0.3455 0.3644Ave 6.4 0.3505 0.0100 15.0 0.3375 1,1,2-Trichloroethane 0.2720 0.2647 0.2830 0.2757 0.2832Ave 2.6 0.2710 0.0100 15.0 0.2749 Tetrachloroethene 0.3877 0.3857 0.3641 0.3770 0.3714Ave 3.1 0.3585 0.0100 15.0 0.3741 1,3-Dichloropropane 0.4386 0.4678 0.4537 0.4585 0.4651Ave 2.7 0.4404 0.0100 15.0 0.4540 2-Hexanone 0.1953 0.1931 0.1955 0.2045 0.1961Ave 2.7 0.1880 0.0100 15.0 0.1954 Dibromochloromethane 0.2040 0.2329 0.2507 0.2602 0.2677Ave 9.7 0.2616 0.0100 15.0 0.2462 1,2-Dibromoethane 0.1811 0.1775 0.1848 0.1786 0.1848Ave 2.7 0.1720 0.0100 15.0 0.1798 1-Chlorohexane 0.6093 0.5831 0.5505 0.5582 0.5737Ave 4.3 0.5435 0.0100 15.0 0.5697 Chlorobenzene 0.9184 0.9225 0.9033 0.9116 0.9054Ave 2.2 0.8681 0.3000 15.0 0.9049 1,1,1,2-Tetrachloroethane 0.2930 0.2979 0.3101 0.3188 0.3208Ave 3.6 0.3132 0.0100 15.0 0.3090 Ethylbenzene 0.5544 0.5503 0.5126 0.5352 0.5171Ave 4.1 0.5009 0.0100 15.0 0.5284 m&p-Xylene 1.3686 1.3827 1.3012 1.2861 1.2289Ave 6.9 1.1453 0.0100 15.0 1.2855 o-Xylene 1.3495 1.4372 1.3698 1.3557 1.3252Ave 4.5 1.2528 0.0100 15.0 1.3484 Styrene 0.9608 1.0612 1.0145 1.0388 1.0303Ave 3.6 0.9843 0.0100 15.0 1.0150 Bromoform 0.1125 0.1362 0.1408 0.1514 0.1643Ave 13.0 0.1539 0.1000 15.0 0.1432 Isopropylbenzene 3.1539 3.6540 3.1572 3.3315 3.1688Ave 6.7 3.0455 0.0100 15.0 3.2518 Bromobenzene 0.6695 0.7563 0.7093 0.7420 0.7361Ave 4.2 0.7199 0.0100 15.0 0.7222



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 132 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 1,1,2,2-Tetrachloroethane 0.5452 0.5696 0.5597 0.5706 0.5758Ave 3.0 0.5328 0.3000 15.0 0.5589 1,2,3-Trichloropropane 0.1912 0.1794 0.1660 0.1701 0.1701Ave 6.1 0.1622 0.0100 15.0 0.1732 N-Propylbenzene 3.9287 4.2993 3.7879 3.9367 3.7362Ave 6.3 3.5832 0.0100 15.0 3.8787 2-Chlorotoluene 2.3554 2.5038 2.2305 2.3361 2.2656Ave 4.9 2.1830 0.0100 15.0 2.3124 1,3,5-Trimethylbenzene 2.6219 2.9360 2.6333 2.7109 2.6361Ave 5.3 2.5201 0.0100 15.0 2.6764 4-Chlorotoluene 2.6491 2.9401 2.6216 2.7188 2.6440Ave 5.1 2.5353 0.0100 15.0 2.6848 tert-Butylbenzene 2.2801 2.5455 2.2199 2.2982 2.2247Ave 6.1 2.1418 0.0100 15.0 2.2850 1,2,4-Trimethylbenzene 2.7631 3.0061 2.6438 2.7255 2.6458Ave 5.8 2.5511 0.0100 15.0 2.7226 sec-Butylbenzene 3.5331 3.8935 3.3623 3.4462 3.3180Ave 7.1 3.1870 0.0100 15.0 3.4567 1,3-Dichlorobenzene 1.4471 1.5053 1.3813 1.4255 1.3778Ave 4.0 1.3501 0.0100 15.0 1.4145 p-Isopropyltoluene 2.9586 3.2474 2.8310 2.8845 2.8017Ave 6.6 2.6869 0.0100 15.0 2.9017 1,4-Dichlorobenzene 1.3977 1.4878 1.3669 1.4117 1.3954Ave 3.8 1.3295 0.0100 15.0 1.3982 n-Butylbenzene 2.8602 3.1543 2.7994 2.7899 2.7599Ave 6.2 2.6239 0.0100 15.0 2.8313 1,2-Dichlorobenzene 1.2797 1.3306 1.2155 1.2573 1.2376Ave 3.9 1.1916 0.0100 15.0 1.2521 1,2-Dibromo-3-Chloropropane 0.0873 0.0832 0.0794 0.0812 0.0900Ave 4.7 0.0826 0.0100 15.0 0.0839 1,2,4-Trichlorobenzene 0.9789 0.9823 0.8678 0.7520 0.7794Ave 13.0 0.7396 0.0100 15.0 0.8500 Hexachlorobutadiene 0.6292 0.6291 0.5100 0.4198 0.4138Qua1 0.9940 +++++ 0.0100 0.9900 0.74170.5403-0.001 Naphthalene 1.6968 1.5945 1.4268 1.3407 1.4423Lin2 0.9970 1.3291 0.0100 0.9900 1.66281.3908 1,2,3-Trichlorobenzene 0.7531 0.7667 0.6080 0.5315 0.5708Qua2 0.9900 0.5407 0.0100 0.9900 0.46540.6784-0.001 Dibromofluoromethane 0.4012 0.4120 0.3878 0.4079Ave 4.3 0.3703 0.0100 15.0 0.3958



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 133 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 0.2(mm) DB624 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 1,2-Dichloroethane-d4 (Surr) 0.3252 0.3396 0.3092 0.3325Ave 6.0 0.2918 0.0100 15.0 0.3196 Toluene-d8 (Surr) 1.0538 1.0512 0.9999 1.0425Ave 4.8 0.9393 0.0100 15.0 1.0174 4-Bromofluorobenzene (Surr) 0.5024 0.5042 0.4741 0.5018Ave 5.3 0.4456 0.0100 15.0 0.4856



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 134 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1 500-170196/6 16I1119A.D Level2 STD2 500-170196/7 16I1119B.D Level3 STD3 500-170196/8 16I1119C.D Level4 STD4 500-170196/9 16I1119D.D Level5 STD5 500-170196/10 16I1119E.D Level6 STD6 500-170196/11 16I1119F.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Dichlorodifluoromethane Ave PFB 12902 50070 127370 264568 422626 553924 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 16213 63463 162200 326211 505093 682571 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 13885 56436 140448 289222 445896 594740 5.00 20.0 50.0 100 150 200 Bromomethane Lin2 PFB 5496 18758 43458 93314 141095 193922 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 7205 29060 71345 150837 234006 319655 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 16215 63387 158331 343881 516513 704692 5.00 20.0 50.0 100 150 200 Acrolein Lin2 PFB 84258 300252 793200 1494545 2240120 2801943 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 9821 44072 105755 217759 322621 428198 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 10804 45578 109401 223828 334178 429549 5.00 20.0 50.0 100 150 200 Acetone Lin1 PFB 5507 12315 31383 63749 92368 115814 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 31066 138989 361364 824494 1127201 1531938 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 7059 30299 75012 155141 232468 286410 40.0 160 400 800 1200 1600 Methylene Chloride Ave PFB 11136 49301 121856 251650 373003 483310 5.00 20.0 50.0 100 150 200 Acrylonitrile Lin2 PFB 32531 113188 294241 574185 891617 1111839 40.0 160 400 800 1200 1600 trans-1,2-Dichloroethene Ave PFB 11855 51013 123566 255847 380526 503496 5.00 20.0 50.0 100 150 200 Methyl tert-butyl ether Ave PFB 31388 126868 323557 644017 972967 1226790 5.00 20.0 50.0 100 150 200


### FORM VI 8260B 

## 01/03/2013 Page 135 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 1,1-Dichloroethane Ave PFB 23166 101272 241193 507139 756847 994036 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB 19714 91380 226543 523396 796266 982422 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 12960 55088 131791 281610 413914 527180 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 13099 54969 131526 277962 416945 543539 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB 4823 19213 46819 98580 153328 188153 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 11092 40835 102296 208849 323908 406897 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 5399 20944 52481 108571 161097 209785 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Lin2 PFB 3446 12837 31053 62700 97150 119315 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 20416 88794 212306 447767 669705 875928 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 16137 72040 174862 369627 552754 709015 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 13245 59272 142459 312633 472055 620557 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 16767 74498 171713 373900 558058 731603 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 47671 208006 479794 1035802 1523052 1996925 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 14847 64572 154226 328584 498369 649012 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 11297 48428 113149 242684 367651 485784 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 10834 52448 117184 261424 392941 521104 5.00 20.0 50.0 100 150 200 Dibromomethane Ave DFB 5515 23635 56895 122814 188390 241667 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 11517 55249 137199 310916 479512 636972 5.00 20.0 50.0 100 150 200 2-Chloroethyl vinyl ether Ave DFB 4691 21736 52381 121903 188565 233764 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 14063 65411 155392 355410 557705 731626 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB 7850 37307 95785 205560 301187 390574 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 136 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 Toluene Ave DFB 27820 125770 279057 615277 914875 1207131 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 11105 55044 132225 300866 475199 629293 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave PFB 6881 30616 75972 163072 249804 329645 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 11739 49681 113412 247302 371178 488872 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 13281 60253 141339 300730 464793 600568 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ 5913 24867 60900 134127 195945 256358 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 6176 29991 78104 170673 267577 356811 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 6662 29944 72598 155572 240952 308703 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 15413 67451 147771 330227 506094 661180 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 27808 118815 281396 597934 904889 1183858 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 8870 38367 96602 209122 320615 427140 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 16785 70876 159684 351002 516773 683074 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 82877 356156 810673 1687130 2456378 3123829 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 40858 185102 426723 889192 1324449 1708514 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 29090 136679 316041 681314 1029721 1342275 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 3407 17540 43862 99282 164184 209852 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 51019 228406 516591 1065124 1575324 2017775 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 10830 47272 116055 237235 365963 476962 5.00 20.0 50.0 100 150 200 1,1,2,2-Tetrachloroethane Ave DCB 8819 35605 91578 182439 286268 352978 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 3093 11214 27159 54392 84576 107459 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 63553 268743 619776 1258627 1857403 2373990 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 137 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6 2-Chlorotoluene Ave DCB 38102 156509 364951 746878 1126306 1446295 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 42413 183522 430864 866728 1310538 1669636 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 42853 183778 428943 869237 1314457 1679760 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 36885 159113 363220 734777 1106000 1419051 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 44697 187908 432579 871394 1315353 1690213 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 57153 243374 550146 1101803 1649521 2111505 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 23410 94092 226011 455769 684977 894523 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 47861 202992 463212 922211 1392838 1780196 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 22610 92998 223660 451341 693731 880833 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 46268 197168 458033 891981 1372078 1738419 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 20701 83175 198883 401981 615248 789503 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 1412 5199 12985 25946 44755 54754 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 15835 61405 141991 240412 387497 490028 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Qua1 DCB 10179 39324 83450 134222 205730 +++++ 5.00 20.0 50.0 100 150 +++++ Naphthalene Lin2 DCB 27448 99668 233455 428628 717029 880550 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Qua2 DCB 12182 47927 99479 169921 283755 358235 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 46408 110602 229403 359839 450525 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 54848 133405 269262 433613 523883 20.0 50.0 100 150 200 Toluene-d8 (Surr) Ave DFB 177743 413010 870860 1359449 1686334 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 64705 157084 310979 501486 607718 20.0 50.0 100 150 200



### FORM VI 8260B 

## 01/03/2013 Page 138 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16 Analy Batch No.:170196

10620 Calibration Start Date: Calibration End Date: 11/19/2012 12:14 Y 11/19/2012 14:09 GC Column:DB624 ID:0.2(mm) INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend: Ave = Average ISTD Lin1 = Linear 1/conc ISTD Lin2 = Linear 1/conc^2 ISTD Qua1 = Quadratic 1/conc ISTD Qua2 = Quadratic 1/conc^2 ISTD



### FORM VI 8260B 

## 01/03/2013 Page 139 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1 500-169636/2 25I1114a.D 2 Level STD2 500-169636/3 25I1114b.D 3 Level STD3 500-169636/4 25I1114c.D 4 Level STD4 500-169636/5 25I1114d.D 5 Level STD5 500-169636/6 25I1114e.D 6 Level STD6 500-169636/7 25I1114f.D 7 Level STD7 500-169636/8 25I1114g.D 8 Level STD8 500-169636/9 25I1114h.D 9 Level STD9 500-169636/10 25I1114i.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane 0.6267 0.6059 0.5583 0.5593Ave 11.0 0.7116 0.7140 0.6992 0.7051 0.0100 15.0 0.6475 Chloromethane 1.3015 1.0453 0.9025 0.8641Ave 13.0 0.9958 0.9920 0.9583 0.9520 0.1000 15.0 1.0014 Vinyl chloride 0.7381 0.7395 0.7007 0.7169 0.7202Ave 8.2 0.8411 0.8539 0.8325 0.8376 0.0100 15.0 0.7756 Bromomethane 0.0930 0.0874 0.1319 0.0939Qua1 0.9980 0.1431 0.1678 0.1774 0.1911 0.0100 0.9900 -0.0540.12500.0003 Chloroethane 0.3725 0.3490 0.3073 0.2815Ave 8.8 0.3535 0.3570 0.3479 0.3478 0.0100 15.0 0.3396 Trichlorofluoromethane 0.7867 0.7170 0.7355 0.7044Ave 5.7 0.8073 0.8108 0.7973 0.7996 0.0100 15.0 0.7698 Dichlorofluoromethane 0.9181 0.8585 0.8326 0.8292Ave 6.3 0.9602 0.9591 0.9448 0.9451 0.0100 15.0 0.9059 1,1,2-Trichloro-1,2,2-trifluoroethane 0.5594 0.5039 0.5013 0.5075Ave 4.0 0.5451 0.5404 0.5331 0.5266 0.0100 15.0 0.5272 Acrolein 0.0653 0.0508 0.0519 0.0506Ave 9.3 0.0513 0.0528 0.0510 0.0514 0.0010 15.0 0.0531 1,1-Dichloroethene 0.4814 0.4114 0.4116 0.4186Ave 5.6 0.4529 0.4536 0.4471 0.4401 0.0100 15.0 0.4396 Acetone 0.0862 0.0669Lin1 0.9990 0.0603 0.0638 0.0605 0.0585 0.0100 0.9900 0.13960.0593 Carbon disulfide 1.6120 1.5896Ave 3.6 1.7255 1.7217 1.7163 1.6755 0.0100 15.0 1.6734 Acetonitrile 0.0417 0.0334 0.0357 0.0342Ave 10.0 0.0308 0.0320 0.0316 0.0319 0.0010 15.0 0.0339



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 140 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Methylene Chloride 0.4134 0.3950Ave 2.4 0.4162 0.4214 0.4201 0.4205 0.0100 15.0 0.4144 Methyl tert-butyl ether 0.5873 0.5558 0.5767 0.5751Ave 4.8 0.5964 0.6288 0.6193 0.6376 0.0100 15.0 0.5971 trans-1,2-Dichloroethene 0.4969 0.4714 0.4802 0.4690Ave 2.8 0.4994 0.5012 0.4981 0.5021 0.0100 15.0 0.4898 Acrylonitrile 0.1233 0.0964 0.0989 0.0964Ave 9.1 0.0964 0.1003 0.0974 0.0986 0.0010 15.0 0.1009 1,1-Dichloroethane 1.1443 1.0662 1.0334 1.0546Ave 3.4 1.1127 1.1107 1.1090 1.1012 0.1000 15.0 1.0915 Vinyl acetate 0.6064 0.5706 0.5890 0.6136Ave 4.3 0.6078 0.6455 0.6277 0.6463 0.0100 15.0 0.6134 2,2-Dichloropropane 0.6725 0.6011 0.6452 0.6474Ave 5.7 0.6930 0.7023 0.7076 0.7102 0.0100 15.0 0.6724 cis-1,2-Dichloroethene 0.4779 0.4805 0.4654 0.4786Ave 3.4 0.4977 0.5122 0.5050 0.5029 0.0100 15.0 0.4900 2-Butanone (MEK) 0.0855 0.0852Ave 2.0 0.0835 0.0880 0.0857 0.0876 0.0100 15.0 0.0859 Propionitrile 0.0258 0.0211 0.0203 0.0239Ave 7.3 0.0234 0.0234 0.0227 0.0228 0.0010 15.0 0.0229 Bromochloromethane 0.1759 0.1659 0.1645 0.1732Ave 5.1 0.1800 0.1876 0.1852 0.1869 0.0100 15.0 0.1774 Tetrahydrofuran 0.0608 0.0559Ave 4.1 0.0598 0.0632 0.0600 0.0616 0.0100 15.0 0.0602 Chloroform 0.7642 0.7420 0.7427 0.7512Ave 2.7 0.7819 0.7901 0.7886 0.7819 0.0100 15.0 0.7678 1,1,1-Trichloroethane 0.8037 0.6853 0.7017 0.7217Ave 5.3 0.7638 0.7628 0.7655 0.7624 0.0100 15.0 0.7459 Carbon tetrachloride 0.5656 0.4815 0.4809 0.4715Ave 6.0 0.5066 0.5007 0.4941 0.4813 0.0100 15.0 0.4978 1,1-Dichloropropene 0.8371 0.6861 0.6672 0.6998Ave 7.1 0.7343 0.7197 0.7159 0.7187 0.0100 15.0 0.7224 Benzene 1.3416 1.3682 1.2676 1.2584 1.2711Ave 3.1 1.3139 1.3047 1.2916 1.2506 0.0100 15.0 1.2964 1,2-Dichloroethane 0.3620 0.3300 0.3466 0.3363Ave 2.9 0.3488 0.3529 0.3482 0.3416 0.0100 15.0 0.3458 Trichloroethene 0.2999 0.3740 0.3420 0.3534 0.3550Ave 6.2 0.3698 0.3628 0.3591 0.3525 0.0100 15.0 0.3521 1,2-Dichloropropane 0.4011 0.3552 0.3669 0.3810Ave 4.0 0.3930 0.3945 0.3896 0.3817 0.0100 15.0 0.3829



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 141 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dibromomethane 0.1339 0.1208 0.1203 0.1225Ave 3.5 0.1265 0.1272 0.1238 0.1230 0.0100 15.0 0.1248 Bromodichloromethane 0.3886 0.3333 0.3435 0.3500Ave 4.7 0.3658 0.3672 0.3638 0.3596 0.0100 15.0 0.3590 2-Chloroethyl vinyl ether 0.1009 0.1066 0.1211Ave 9.8 0.1214 0.1319 0.1282 0.1282 0.0100 15.0 0.1198 cis-1,3-Dichloropropene 0.3681 0.3335 0.3673 0.3812Ave 6.9 0.4024 0.4120 0.4061 0.3997 0.0100 15.0 0.3838 4-Methyl-2-pentanone (MIBK) 0.1174 0.1312Ave 6.9 0.1296 0.1461 0.1321 0.1310 0.0100 15.0 0.1313 Toluene 0.7622 0.8254 0.7315 0.7621 0.8038Ave 4.3 0.8309 0.8194 0.8076 0.7815 0.0100 15.0 0.7916 trans-1,3-Dichloropropene 0.2661 0.2721 0.2745 0.2910Ave 7.1 0.3072 0.3166 0.3129 0.3138 0.0100 15.0 0.2943 1,1,2-Trichloroethane 0.2405 0.2127 0.2226 0.2354Ave 5.3 0.2434 0.2491 0.2432 0.2459 0.0100 15.0 0.2366 Tetrachloroethene 0.4912 0.4634 0.4661 0.4689Ave 2.0 0.4810 0.4775 0.4709 0.4639 0.0100 15.0 0.4729 1,3-Dichloropropane 0.3521 0.3430 0.3631 0.3655Ave 3.4 0.3768 0.3815 0.3700 0.3681 0.0100 15.0 0.3650 2-Hexanone 0.0898 0.0958Ave 7.8 0.1054 0.1085 0.1086 0.1081 0.0100 15.0 0.1027 Dibromochloromethane 0.2353 0.2499 0.2582 0.2578Ave 6.0 0.2748 0.2829 0.2742 0.2741 0.0100 15.0 0.2634 1,2-Dibromoethane 0.1484 0.1529 0.1471 0.1529Ave 3.2 0.1580 0.1623 0.1566 0.1551 0.0100 15.0 0.1542 1-Chlorohexane 0.8430 0.7044 0.6586 0.6853Ave 7.5 0.7341 0.7299 0.7197 0.7224 0.0100 15.0 0.7247 Chlorobenzene 1.0912 1.0617 1.0296 1.0316Ave 2.7 1.0644 1.0581 1.0326 0.9989 0.3000 15.0 1.0460 Ethylbenzene 0.6126 0.6262 0.5910 0.6046 0.6108Ave 2.3 0.6314 0.6272 0.6147 0.5959 0.0100 15.0 0.6127 1,1,1,2-Tetrachloroethane 0.3598 0.3180 0.3265 0.3245Ave 4.2 0.3471 0.3481 0.3435 0.3360 0.0100 15.0 0.3379 m&p-Xylene 1.4172 1.5184 1.3883 1.4484 1.4772Ave 3.7 1.5193 1.4949 1.4390 1.3765 0.0100 15.0 1.4532 o-Xylene 1.2710 1.4168 1.3402 1.3803 1.4253Ave 4.9 1.4830 1.4858 1.4466 1.4030 0.0100 15.0 1.4058 Styrene 1.0367 0.9413 1.0331 1.0877Ave 6.0 1.1364 1.1327 1.1029 1.0651 0.0100 15.0 1.0670



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 142 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Bromoform 0.1342 0.1290 0.1300 0.1378Ave 5.5 0.1457 0.1487 0.1442 0.1448 0.1000 15.0 0.1393 Isopropylbenzene 4.0836 3.8956 4.0253 4.3396Ave 4.7 4.4728 4.3280 4.2696 4.0726 0.0100 15.0 4.1859 Bromobenzene 0.8418 0.7730 0.8017 0.8435Ave 4.2 0.8804 0.8655 0.8558 0.8324 0.0100 15.0 0.8368 1,1,2,2-Tetrachloroethane 0.4992 0.4183 0.4339 0.4409Ave 5.5 0.4564 0.4527 0.4413 0.4280 0.3000 15.0 0.4463 N-Propylbenzene 4.8751 4.7238 4.8139 5.1431Ave 4.3 5.3576 5.1063 5.0181 4.7949 0.0100 15.0 4.9791 1,2,3-Trichloropropane 0.3705 0.3219 0.3365 0.3427Ave 4.5 0.3594 0.3570 0.3470 0.3367 0.0100 15.0 0.3465 2-Chlorotoluene 2.8872 2.5986 2.6727 2.7903Ave 3.8 2.8784 2.7818 2.7435 2.6466 0.0100 15.0 2.7499 1,3,5-Trimethylbenzene 3.0596 2.9605 3.1481 3.3739Ave 5.8 3.5164 3.4113 3.3441 3.2179 0.0100 15.0 3.2540 4-Chlorotoluene 2.9487 2.6742 2.8692 2.9235Ave 4.2 3.0173 2.9214 2.8681 2.6996 0.0100 15.0 2.8652 tert-Butylbenzene 2.9337 2.7766 2.7908 3.0593Ave 4.7 3.1788 3.0617 3.0246 2.9064 0.0100 15.0 2.9665 1,2,4-Trimethylbenzene 3.0577 2.8570 3.0570 3.2743Ave 5.5 3.3951 3.3096 3.2537 3.1107 0.0100 15.0 3.1644 sec-Butylbenzene 4.5072 4.2877 4.5644 4.7518Ave 4.4 4.9370 4.7434 4.6299 4.4303 0.0100 15.0 4.6065 1,3-Dichlorobenzene 1.7557 1.6307 1.6126 1.6403Ave 3.8 1.6868 1.6471 1.5962 1.5498 0.0100 15.0 1.6399 p-Isopropyltoluene 3.6787 3.3647 3.6682 3.8530Ave 5.1 3.9915 3.8347 3.7475 3.6085 0.0100 15.0 3.7184 1,4-Dichlorobenzene 1.8501 1.5676 1.5917 1.6102Ave 6.4 1.6205 1.5924 1.5568 1.5065 0.0100 15.0 1.6120 n-Butylbenzene 3.7246 3.5101 3.5034 3.7147Ave 3.5 3.8020 3.7046 3.5925 3.4543 0.0100 15.0 3.6258 1,2-Dichlorobenzene 1.5125 1.3182 1.3353 1.3471Ave 5.0 1.3736 1.3441 1.3224 1.2938 0.0100 15.0 1.3559 1,2-Dibromo-3-Chloropropane 0.0640 0.0557 0.0607Ave 4.2 0.0613 0.0622 0.0619 0.0622 0.0100 15.0 0.0611 1,2,4-Trichlorobenzene 1.0559 1.0114 0.9472 0.9754Ave 3.3 0.9959 1.0112 0.9823 0.9714 0.0100 15.0 0.9938 Hexachlorobutadiene 0.9048 0.7841 0.7828 0.8164Ave 5.0 0.8362 0.8060 0.8013 0.7837 0.0100 15.0 0.8144



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 143 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Naphthalene 1.1523 1.0892 1.1043 1.2375Ave 8.4 1.3088 1.3385 1.3265 1.3042 0.0100 15.0 1.2326 1,2,3-Trichlorobenzene 0.8054 0.7453 0.7397 0.7760Ave 3.1 0.8024 0.7863 0.7665 0.7673 0.0100 15.0 0.7736 Dibromofluoromethane 0.4286Ave 3.4 0.3921 0.4016 0.4001 0.4056 0.0100 15.0 0.4056 1,2-Dichloroethane-d4 (Surr) 0.2801Ave 3.9 0.2563 0.2610 0.2563 0.2563 0.0100 15.0 0.2620 Toluene-d8 (Surr) 1.2583Ave 5.3 1.1460 1.1369 1.1272 1.1002 0.0100 15.0 1.1537 4-Bromofluorobenzene (Surr) 0.5135Ave 6.4 0.4530 0.4548 0.4445 0.4423 0.0100 15.0 0.4616



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 144 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1 500-169636/2 25I1114a.D Level2 STD2 500-169636/3 25I1114b.D Level3 STD3 500-169636/4 25I1114c.D Level4 STD4 500-169636/5 25I1114d.D Level5 STD5 500-169636/6 25I1114e.D Level6 STD6 500-169636/7 25I1114f.D Level7 STD7 500-169636/8 25I1114g.D Level8 STD8 500-169636/9 25I1114h.D Level9 STD9 500-169636/10 25I1114i.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane Ave PFB 5925 11401 26997 105234 340727 680574 999908 1334171 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 12304 19668 43637 162579 476834 945596 1370421 1801235 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 1792 6991 13184 34662 135512 402756 813940 1190617 1584805 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromomethane Qua1 PFB 879 1644 6380 17675 68531 159903 253688 361489 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 3522 6566 14857 52973 169260 340269 497534 658073 1.00 2.00 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 7437 13491 35562 132537 386583 772790 1140271 1512970 1.00 2.00 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 8680 16153 40257 156008 459802 914190 1351103 1788177 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 5289 9481 24240 95490 261022 515069 762341 996359 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 24682 38238 100342 380499 983163 2013878 2919532 3889511 40.0 80.0 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 4551 7740 19901 78752 216853 432374 639336 832639 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetone Lin1 PFB 4169 12583 28863 60844 86556 110714 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 77944 299089 826236 1641126 2454485 3170249 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 3153 5029 13796 51503 118119 244233 361545 482815 8.00 16.0 40.0 160 400 800 1200 1600 Methylene Chloride Ave PFB 19989 74311 199298 401716 600718 795639 5.00 20.0 50.0 100 150 200



### FORM VI 8260B 

## 01/03/2013 Page 145 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Methyl tert-butyl ether Ave PFB 5552 10458 27883 108208 285591 599368 885704 1206318 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,2-Dichloroethene Ave PFB 4698 8869 23219 88248 239156 477780 712403 950052 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrylonitrile Ave PFB 9328 14508 38240 145047 369309 764494 1113946 1491801 8.00 16.0 40.0 160 400 800 1200 1600 1,1-Dichloroethane Ave PFB 10818 20062 49965 198420 532819 1058676 1586028 2083577 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB 5733 10737 28478 115450 291043 615281 897688 1222863 1.00 2.00 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 6358 11310 31195 121815 331849 669389 1011997 1343669 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 4518 9041 22503 90050 238305 488203 722208 951477 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB 4135 16024 39966 83903 122589 165782 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 2803 4571 11330 51048 128688 261136 380813 514481 8.00 16.0 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 1663 3122 7953 32593 86204 178800 264811 353545 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB 2940 10518 28655 60287 85848 116463 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 7225 13962 35909 141343 374395 753081 1127839 1479445 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 7598 12895 33927 135798 365728 727123 1094771 1442540 1.00 2.00 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 7696 13009 33599 126143 348829 697542 1036343 1360424 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 7914 12910 32262 131672 351635 685994 1023811 1359894 1.00 2.00 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 4675 18616 34246 87925 340025 904704 1817615 2709239 3534956 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 4925 8914 24218 89957 240180 491653 730359 965547 1.00 2.00 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 1045 5088 9239 24694 94975 254660 505411 753283 996319 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 5457 9597 25633 101917 270576 549582 817263 1078941 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromomethane Ave DFB 1822 3264 8408 32759 87117 177217 259724 347677 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 5287 9005 24000 93640 251902 511588 763207 1016509 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 146 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 2-Chloroethyl vinyl ether Ave DFB 2725 7449 32403 83592 183720 268867 362477 2.00 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 5008 9009 25666 101987 277068 573893 851744 1129853 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB 8206 35107 89269 203592 277039 370296 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 2656 11230 19763 53245 215017 572099 1141442 1694075 2209045 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 3620 7351 19177 77839 211555 441063 656430 886925 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave PFB 2274 4002 10765 44295 116554 237405 347788 465322 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 5346 10002 25680 101199 264948 529023 785866 1043336 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 3832 7403 20002 78881 207573 422657 617363 827757 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ 4945 20677 58037 120168 181279 243107 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 2561 5394 14227 55644 151370 313439 457571 616524 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 2019 4131 10278 40903 108765 226089 328523 438293 1.00 2.00 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 7970 13254 31843 128940 351499 695727 1029228 1366789 1.00 2.00 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 11876 22914 56723 222644 586311 1172309 1723186 2246503 1.00 2.00 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 1668 6815 12754 33309 131824 347791 694878 1025850 1340093 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 3916 6863 17989 70044 191190 385705 573138 755649 1.00 2.00 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 7718 33049 59926 159589 637599 1673870 3312548 4802496 6191326 0.500 2.00 4.00 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 3461 15419 28925 76044 307606 816927 1646151 2414005 3155235 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 11282 20316 56914 234746 626017 1254918 1840518 2395297 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 1460 2785 7164 29735 80261 164803 240639 325699 1.00 2.00 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 20214 38535 102851 424056 1099936 2200629 3227532 4168680 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 4167 7647 20483 82422 216512 440051 646947 852077 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 147 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 1,1,2,2-Tetrachloroethane Ave DCB 2471 4138 11086 43083 112230 230162 333588 438075 1.00 2.00 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 24132 46728 123000 502575 1317540 2596340 3793324 4908027 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 1834 3184 8599 33490 88390 181542 262321 344689 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 14292 25705 68289 272668 707862 1414432 2073876 2709003 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 15145 29285 80436 329695 864754 1734520 2527907 3293833 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 14596 26453 73310 285677 742016 1485407 2168057 2763304 1.00 2.00 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 14522 27466 71308 298955 781727 1556746 2286383 2974995 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 15136 28261 78110 319956 834910 1682789 2459601 3184071 1.00 2.00 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 22311 42414 116625 464344 1214094 2411809 3499921 4534829 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 8691 16131 41203 160290 414806 837508 1206617 1586342 1.00 2.00 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 18210 33284 93726 376512 981590 1949768 2832864 3693602 1.00 2.00 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 9158 15507 40669 157342 398505 809665 1176872 1542031 1.00 2.00 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 18437 34722 89516 362997 934982 1883655 2715730 3535815 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 7487 13040 34119 131641 337786 683433 999636 1324326 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 633 1424 5930 15066 31633 46778 63674 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 5227 10005 24201 95311 244912 514149 742574 994295 1.00 2.00 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Ave DCB 4479 7756 20002 79780 205629 409810 605699 802196 1.00 2.00 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 5704 10774 28215 120923 321854 680580 1002739 1334973 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Ave DCB 3987 7373 18899 75826 197329 399786 579399 785372 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 80643 187757 382786 572130 767393 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 74925 176491 363647 537534 724583 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 148 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169636

10605 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Toluene-d8 (Surr) Ave DFB 336603 789050 1583796 2364398 3109931 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 110828 249531 503840 741720 994763 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD Lin1 = Linear 1/conc ISTD Qua1 = Quadratic 1/conc ISTD



### FORM VI 8260B 

## 01/03/2013 Page 149 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: 1 Level STD1 500-169637/2 25I1114a.D 2 Level STD2 500-169637/3 25I1114b.D 3 Level STD3 500-169637/4 25I1114c.D 4 Level STD4 500-169637/5 25I1114d.D 5 Level STD5 500-169637/6 25I1114e.D 6 Level STD6 500-169637/7 25I1114f.D 7 Level STD7 500-169637/8 25I1114g.D 8 Level STD8 500-169637/9 25I1114h.D 9 Level STD9 500-169637/10 25I1114i.D

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane 0.6267 0.6059 0.5583 0.5593Ave 11.0 0.7116 0.7140 0.6992 0.7051 0.0100 15.0 0.6475 Chloromethane 1.3015 1.0453 0.9025 0.8641Ave 13.0 0.9958 0.9920 0.9583 0.9520 0.1000 15.0 1.0014 Vinyl chloride 0.7381 0.7395 0.7007 0.7169 0.7202Ave 8.2 0.8411 0.8539 0.8325 0.8376 0.0100 15.0 0.7756 Bromomethane 0.0930 0.0874 0.1319 0.0939Qua1 0.9980 0.1431 0.1678 0.1774 0.1911 0.0100 0.9900 -0.0540.12500.0003 Chloroethane 0.3725 0.3490 0.3073 0.2815Ave 8.8 0.3535 0.3570 0.3479 0.3478 0.0100 15.0 0.3396 Trichlorofluoromethane 0.7867 0.7170 0.7355 0.7044Ave 5.7 0.8073 0.8108 0.7973 0.7996 0.0100 15.0 0.7698 Dichlorofluoromethane 0.9181 0.8585 0.8326 0.8292Ave 6.3 0.9602 0.9591 0.9448 0.9451 0.0100 15.0 0.9059 1,1,2-Trichloro-1,2,2-trifluoroethane 0.5594 0.5039 0.5013 0.5075Ave 4.0 0.5451 0.5404 0.5331 0.5266 0.0100 15.0 0.5272 Acrolein 0.0653 0.0508 0.0519 0.0506Ave 9.3 0.0513 0.0528 0.0510 0.0514 0.0010 15.0 0.0531 1,1-Dichloroethene 0.4814 0.4114 0.4116 0.4186Ave 5.6 0.4529 0.4536 0.4471 0.4401 0.0100 15.0 0.4396 Acetone 0.0862 0.0669Lin1 0.9990 0.0603 0.0638 0.0605 0.0585 0.0100 0.9900 0.13960.0593 Carbon disulfide 1.6120 1.5896Ave 3.6 1.7255 1.7217 1.7163 1.6755 0.0100 15.0 1.6734 Acetonitrile 0.0417 0.0334 0.0357 0.0342Ave 10.0 0.0308 0.0320 0.0316 0.0319 0.0010 15.0 0.0339



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 150 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Methylene Chloride 0.4134 0.3950Ave 2.4 0.4162 0.4214 0.4201 0.4205 0.0100 15.0 0.4144 Methyl tert-butyl ether 0.5873 0.5558 0.5767 0.5751Ave 4.8 0.5964 0.6288 0.6193 0.6376 0.0100 15.0 0.5971 trans-1,2-Dichloroethene 0.4969 0.4714 0.4802 0.4690Ave 2.8 0.4994 0.5012 0.4981 0.5021 0.0100 15.0 0.4898 Acrylonitrile 0.1233 0.0964 0.0989 0.0964Ave 9.1 0.0964 0.1003 0.0974 0.0986 0.0010 15.0 0.1009 1,1-Dichloroethane 1.1443 1.0662 1.0334 1.0546Ave 3.4 1.1127 1.1107 1.1090 1.1012 0.1000 15.0 1.0915 Vinyl acetate 0.6064 0.5706 0.5890 0.6136Ave 4.3 0.6078 0.6455 0.6277 0.6463 0.0100 15.0 0.6134 2,2-Dichloropropane 0.6725 0.6011 0.6452 0.6474Ave 5.7 0.6930 0.7023 0.7076 0.7102 0.0100 15.0 0.6724 cis-1,2-Dichloroethene 0.4779 0.4805 0.4654 0.4786Ave 3.4 0.4977 0.5122 0.5050 0.5029 0.0100 15.0 0.4900 2-Butanone (MEK) 0.0855 0.0852Ave 2.0 0.0835 0.0880 0.0857 0.0876 0.0100 15.0 0.0859 Propionitrile 0.0258 0.0211 0.0203 0.0239Ave 7.3 0.0234 0.0234 0.0227 0.0228 0.0010 15.0 0.0229 Bromochloromethane 0.1759 0.1659 0.1645 0.1732Ave 5.1 0.1800 0.1876 0.1852 0.1869 0.0100 15.0 0.1774 Tetrahydrofuran 0.0608 0.0559Ave 4.1 0.0598 0.0632 0.0600 0.0616 0.0100 15.0 0.0602 Chloroform 0.7642 0.7420 0.7427 0.7512Ave 2.7 0.7819 0.7901 0.7886 0.7819 0.0100 15.0 0.7678 1,1,1-Trichloroethane 0.8037 0.6853 0.7017 0.7217Ave 5.3 0.7638 0.7628 0.7655 0.7624 0.0100 15.0 0.7459 Carbon tetrachloride 0.5656 0.4815 0.4809 0.4715Ave 6.0 0.5066 0.5007 0.4941 0.4813 0.0100 15.0 0.4978 1,1-Dichloropropene 0.8371 0.6861 0.6672 0.6998Ave 7.1 0.7343 0.7197 0.7159 0.7187 0.0100 15.0 0.7224 Benzene 1.3416 1.3682 1.2676 1.2584 1.2711Ave 3.1 1.3139 1.3047 1.2916 1.2506 0.0100 15.0 1.2964 1,2-Dichloroethane 0.3620 0.3300 0.3466 0.3363Ave 2.9 0.3488 0.3529 0.3482 0.3416 0.0100 15.0 0.3458 Trichloroethene 0.2999 0.3740 0.3420 0.3534 0.3550Ave 6.2 0.3698 0.3628 0.3591 0.3525 0.0100 15.0 0.3521 1,2-Dichloropropane 0.4011 0.3552 0.3669 0.3810Ave 4.0 0.3930 0.3945 0.3896 0.3817 0.0100 15.0 0.3829



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 151 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Dibromomethane 0.1339 0.1208 0.1203 0.1225Ave 3.5 0.1265 0.1272 0.1238 0.1230 0.0100 15.0 0.1248 Bromodichloromethane 0.3886 0.3333 0.3435 0.3500Ave 4.7 0.3658 0.3672 0.3638 0.3596 0.0100 15.0 0.3590 2-Chloroethyl vinyl ether 0.1009 0.1066 0.1211Ave 9.8 0.1214 0.1319 0.1282 0.1282 0.0100 15.0 0.1198 cis-1,3-Dichloropropene 0.3681 0.3335 0.3673 0.3812Ave 6.9 0.4024 0.4120 0.4061 0.3997 0.0100 15.0 0.3838 4-Methyl-2-pentanone (MIBK) 0.1174 0.1312Ave 6.9 0.1296 0.1461 0.1321 0.1310 0.0100 15.0 0.1313 Toluene 0.7622 0.8254 0.7315 0.7621 0.8038Ave 4.3 0.8309 0.8194 0.8076 0.7815 0.0100 15.0 0.7916 trans-1,3-Dichloropropene 0.2661 0.2721 0.2745 0.2910Ave 7.1 0.3072 0.3166 0.3129 0.3138 0.0100 15.0 0.2943 1,1,2-Trichloroethane 0.2405 0.2127 0.2226 0.2354Ave 5.3 0.2434 0.2491 0.2432 0.2459 0.0100 15.0 0.2366 Tetrachloroethene 0.4912 0.4634 0.4661 0.4689Ave 2.0 0.4810 0.4775 0.4709 0.4639 0.0100 15.0 0.4729 1,3-Dichloropropane 0.3521 0.3430 0.3631 0.3655Ave 3.4 0.3768 0.3815 0.3700 0.3681 0.0100 15.0 0.3650 2-Hexanone 0.0898 0.0958Ave 7.8 0.1054 0.1085 0.1086 0.1081 0.0100 15.0 0.1027 Dibromochloromethane 0.2353 0.2499 0.2582 0.2578Ave 6.0 0.2748 0.2829 0.2742 0.2741 0.0100 15.0 0.2634 1,2-Dibromoethane 0.1484 0.1529 0.1471 0.1529Ave 3.2 0.1580 0.1623 0.1566 0.1551 0.0100 15.0 0.1542 1-Chlorohexane 0.8430 0.7044 0.6586 0.6853Ave 7.5 0.7341 0.7299 0.7197 0.7224 0.0100 15.0 0.7247 Chlorobenzene 1.0912 1.0617 1.0296 1.0316Ave 2.7 1.0644 1.0581 1.0326 0.9989 0.3000 15.0 1.0460 Ethylbenzene 0.6126 0.6262 0.5910 0.6046 0.6108Ave 2.3 0.6314 0.6272 0.6147 0.5959 0.0100 15.0 0.6127 1,1,1,2-Tetrachloroethane 0.3598 0.3180 0.3265 0.3245Ave 4.2 0.3471 0.3481 0.3435 0.3360 0.0100 15.0 0.3379 m&p-Xylene 1.4172 1.5184 1.3883 1.4484 1.4772Ave 3.7 1.5193 1.4949 1.4390 1.3765 0.0100 15.0 1.4532 o-Xylene 1.2710 1.4168 1.3402 1.3803 1.4253Ave 4.9 1.4830 1.4858 1.4466 1.4030 0.0100 15.0 1.4058 Styrene 1.0367 0.9413 1.0331 1.0877Ave 6.0 1.1364 1.1327 1.1029 1.0651 0.0100 15.0 1.0670



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 152 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Bromoform 0.1342 0.1290 0.1300 0.1378Ave 5.5 0.1457 0.1487 0.1442 0.1448 0.1000 15.0 0.1393 Isopropylbenzene 4.0836 3.8956 4.0253 4.3396Ave 4.7 4.4728 4.3280 4.2696 4.0726 0.0100 15.0 4.1859 Bromobenzene 0.8418 0.7730 0.8017 0.8435Ave 4.2 0.8804 0.8655 0.8558 0.8324 0.0100 15.0 0.8368 1,1,2,2-Tetrachloroethane 0.4992 0.4183 0.4339 0.4409Ave 5.5 0.4564 0.4527 0.4413 0.4280 0.3000 15.0 0.4463 N-Propylbenzene 4.8751 4.7238 4.8139 5.1431Ave 4.3 5.3576 5.1063 5.0181 4.7949 0.0100 15.0 4.9791 1,2,3-Trichloropropane 0.3705 0.3219 0.3365 0.3427Ave 4.5 0.3594 0.3570 0.3470 0.3367 0.0100 15.0 0.3465 2-Chlorotoluene 2.8872 2.5986 2.6727 2.7903Ave 3.8 2.8784 2.7818 2.7435 2.6466 0.0100 15.0 2.7499 1,3,5-Trimethylbenzene 3.0596 2.9605 3.1481 3.3739Ave 5.8 3.5164 3.4113 3.3441 3.2179 0.0100 15.0 3.2540 4-Chlorotoluene 2.9487 2.6742 2.8692 2.9235Ave 4.2 3.0173 2.9214 2.8681 2.6996 0.0100 15.0 2.8652 tert-Butylbenzene 2.9337 2.7766 2.7908 3.0593Ave 4.7 3.1788 3.0617 3.0246 2.9064 0.0100 15.0 2.9665 1,2,4-Trimethylbenzene 3.0577 2.8570 3.0570 3.2743Ave 5.5 3.3951 3.3096 3.2537 3.1107 0.0100 15.0 3.1644 sec-Butylbenzene 4.5072 4.2877 4.5644 4.7518Ave 4.4 4.9370 4.7434 4.6299 4.4303 0.0100 15.0 4.6065 1,3-Dichlorobenzene 1.7557 1.6307 1.6126 1.6403Ave 3.8 1.6868 1.6471 1.5962 1.5498 0.0100 15.0 1.6399 p-Isopropyltoluene 3.6787 3.3647 3.6682 3.8530Ave 5.1 3.9915 3.8347 3.7475 3.6085 0.0100 15.0 3.7184 1,4-Dichlorobenzene 1.8501 1.5676 1.5917 1.6102Ave 6.4 1.6205 1.5924 1.5568 1.5065 0.0100 15.0 1.6120 n-Butylbenzene 3.7246 3.5101 3.5034 3.7147Ave 3.5 3.8020 3.7046 3.5925 3.4543 0.0100 15.0 3.6258 1,2-Dichlorobenzene 1.5125 1.3182 1.3353 1.3471Ave 5.0 1.3736 1.3441 1.3224 1.2938 0.0100 15.0 1.3559 1,2-Dibromo-3-Chloropropane 0.0640 0.0557 0.0607Ave 4.2 0.0613 0.0622 0.0619 0.0622 0.0100 15.0 0.0611 1,2,4-Trichlorobenzene 1.0559 1.0114 0.9472 0.9754Ave 3.3 0.9959 1.0112 0.9823 0.9714 0.0100 15.0 0.9938 Hexachlorobutadiene 0.9048 0.7841 0.7828 0.8164Ave 5.0 0.8362 0.8060 0.8013 0.7837 0.0100 15.0 0.8144



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 153 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: GC Column: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 ID: INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CURVE TYPE COEFFICIENT B M1 M2 # %RSD#MAX %RSD R^2 OR COD#MIN R^2 OR COD MIN RRF
LVL 6 LVL 7 LVL 8 LVL 9 Naphthalene 1.1523 1.0892 1.1043 1.2375Ave 8.4 1.3088 1.3385 1.3265 1.3042 0.0100 15.0 1.2326 1,2,3-Trichlorobenzene 0.8054 0.7453 0.7397 0.7760Ave 3.1 0.8024 0.7863 0.7665 0.7673 0.0100 15.0 0.7736 Dibromofluoromethane 0.4286Ave 3.4 0.3921 0.4016 0.4001 0.4056 0.0100 15.0 0.4056 1,2-Dichloroethane-d4 (Surr) 0.2801Ave 3.9 0.2563 0.2610 0.2563 0.2563 0.0100 15.0 0.2620 Toluene-d8 (Surr) 1.2583Ave 5.3 1.1460 1.1369 1.1272 1.1002 0.0100 15.0 1.1537 4-Bromofluorobenzene (Surr) 0.5135Ave 6.4 0.4530 0.4548 0.4445 0.4423 0.0100 15.0 0.4616



### FORM VI 8260B Note: The m1 coefficient is the same as Ave RRF for an Ave curve type. 

## 01/03/2013 Page 154 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files: LEVEL: LAB SAMPLE ID: LAB FILE ID: Level1 STD1 500-169637/2 25I1114a.D Level2 STD2 500-169637/3 25I1114b.D Level3 STD3 500-169637/4 25I1114c.D Level4 STD4 500-169637/5 25I1114d.D Level5 STD5 500-169637/6 25I1114e.D Level6 STD6 500-169637/7 25I1114f.D Level7 STD7 500-169637/8 25I1114g.D Level8 STD8 500-169637/9 25I1114h.D Level9 STD9 500-169637/10 25I1114i.D

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Dichlorodifluoromethane Ave PFB 5925 11401 26997 105234 340727 680574 999908 1334171 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloromethane Ave PFB 12304 19668 43637 162579 476834 945596 1370421 1801235 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl chloride Ave PFB 1792 6991 13184 34662 135512 402756 813940 1190617 1584805 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromomethane Qua1 PFB 879 1644 6380 17675 68531 159903 253688 361489 1.00 2.00 5.00 20.0 50.0 100 150 200 Chloroethane Ave PFB 3522 6566 14857 52973 169260 340269 497534 658073 1.00 2.00 5.00 20.0 50.0 100 150 200 Trichlorofluoromethane Ave PFB 7437 13491 35562 132537 386583 772790 1140271 1512970 1.00 2.00 5.00 20.0 50.0 100 150 200 Dichlorofluoromethane Ave PFB 8680 16153 40257 156008 459802 914190 1351103 1788177 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloro-1,2,2-trifluoroetha ne Ave PFB 5289 9481 24240 95490 261022 515069 762341 996359 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrolein Ave PFB 24682 38238 100342 380499 983163 2013878 2919532 3889511 40.0 80.0 200 800 2000 4000 6000 8000 1,1-Dichloroethene Ave PFB 4551 7740 19901 78752 216853 432374 639336 832639 1.00 2.00 5.00 20.0 50.0 100 150 200 Acetone Lin1 PFB 4169 12583 28863 60844 86556 110714 5.00 20.0 50.0 100 150 200 Carbon disulfide Ave PFB 77944 299089 826236 1641126 2454485 3170249 5.00 20.0 50.0 100 150 200 Acetonitrile Ave PFB 3153 5029 13796 51503 118119 244233 361545 482815 8.00 16.0 40.0 160 400 800 1200 1600 Methylene Chloride Ave PFB 19989 74311 199298 401716 600718 795639 5.00 20.0 50.0 100 150 200



### FORM VI 8260B 

## 01/03/2013 Page 155 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Methyl tert-butyl ether Ave PFB 5552 10458 27883 108208 285591 599368 885704 1206318 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,2-Dichloroethene Ave PFB 4698 8869 23219 88248 239156 477780 712403 950052 1.00 2.00 5.00 20.0 50.0 100 150 200 Acrylonitrile Ave PFB 9328 14508 38240 145047 369309 764494 1113946 1491801 8.00 16.0 40.0 160 400 800 1200 1600 1,1-Dichloroethane Ave PFB 10818 20062 49965 198420 532819 1058676 1586028 2083577 1.00 2.00 5.00 20.0 50.0 100 150 200 Vinyl acetate Ave PFB 5733 10737 28478 115450 291043 615281 897688 1222863 1.00 2.00 5.00 20.0 50.0 100 150 200 2,2-Dichloropropane Ave PFB 6358 11310 31195 121815 331849 669389 1011997 1343669 1.00 2.00 5.00 20.0 50.0 100 150 200 cis-1,2-Dichloroethene Ave PFB 4518 9041 22503 90050 238305 488203 722208 951477 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Butanone (MEK) Ave PFB 4135 16024 39966 83903 122589 165782 5.00 20.0 50.0 100 150 200 Propionitrile Ave DFB 2803 4571 11330 51048 128688 261136 380813 514481 8.00 16.0 40.0 160 400 800 1200 1600 Bromochloromethane Ave PFB 1663 3122 7953 32593 86204 178800 264811 353545 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrahydrofuran Ave PFB 2940 10518 28655 60287 85848 116463 5.00 20.0 50.0 100 150 200 Chloroform Ave PFB 7225 13962 35909 141343 374395 753081 1127839 1479445 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1-Trichloroethane Ave PFB 7598 12895 33927 135798 365728 727123 1094771 1442540 1.00 2.00 5.00 20.0 50.0 100 150 200 Carbon tetrachloride Ave DFB 7696 13009 33599 126143 348829 697542 1036343 1360424 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1-Dichloropropene Ave PFB 7914 12910 32262 131672 351635 685994 1023811 1359894 1.00 2.00 5.00 20.0 50.0 100 150 200 Benzene Ave DFB 4675 18616 34246 87925 340025 904704 1817615 2709239 3534956 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloroethane Ave DFB 4925 8914 24218 89957 240180 491653 730359 965547 1.00 2.00 5.00 20.0 50.0 100 150 200 Trichloroethene Ave DFB 1045 5088 9239 24694 94975 254660 505411 753283 996319 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichloropropane Ave DFB 5457 9597 25633 101917 270576 549582 817263 1078941 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromomethane Ave DFB 1822 3264 8408 32759 87117 177217 259724 347677 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromodichloromethane Ave DFB 5287 9005 24000 93640 251902 511588 763207 1016509 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 156 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 2-Chloroethyl vinyl ether Ave DFB 2725 7449 32403 83592 183720 268867 362477 2.00 5.00 20.0 50.0 100 150 200 cis-1,3-Dichloropropene Ave DFB 5008 9009 25666 101987 277068 573893 851744 1129853 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Methyl-2-pentanone (MIBK) Ave DFB 8206 35107 89269 203592 277039 370296 5.00 20.0 50.0 100 150 200 Toluene Ave DFB 2656 11230 19763 53245 215017 572099 1141442 1694075 2209045 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 trans-1,3-Dichloropropene Ave DFB 3620 7351 19177 77839 211555 441063 656430 886925 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,2-Trichloroethane Ave PFB 2274 4002 10765 44295 116554 237405 347788 465322 1.00 2.00 5.00 20.0 50.0 100 150 200 Tetrachloroethene Ave CBZ 5346 10002 25680 101199 264948 529023 785866 1043336 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichloropropane Ave CBZ 3832 7403 20002 78881 207573 422657 617363 827757 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Hexanone Ave CBZ 4945 20677 58037 120168 181279 243107 5.00 20.0 50.0 100 150 200 Dibromochloromethane Ave CBZ 2561 5394 14227 55644 151370 313439 457571 616524 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromoethane Ave DFB 2019 4131 10278 40903 108765 226089 328523 438293 1.00 2.00 5.00 20.0 50.0 100 150 200 1-Chlorohexane Ave PFB 7970 13254 31843 128940 351499 695727 1029228 1366789 1.00 2.00 5.00 20.0 50.0 100 150 200 Chlorobenzene Ave CBZ 11876 22914 56723 222644 586311 1172309 1723186 2246503 1.00 2.00 5.00 20.0 50.0 100 150 200 Ethylbenzene Ave CBZ 1668 6815 12754 33309 131824 347791 694878 1025850 1340093 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 1,1,1,2-Tetrachloroethane Ave CBZ 3916 6863 17989 70044 191190 385705 573138 755649 1.00 2.00 5.00 20.0 50.0 100 150 200 m&p-Xylene Ave CBZ 7718 33049 59926 159589 637599 1673870 3312548 4802496 6191326 0.500 2.00 4.00 10.0 40.0 100 200 300 400 o-Xylene Ave CBZ 3461 15419 28925 76044 307606 816927 1646151 2414005 3155235 0.250 1.00 2.00 5.00 20.0 50.0 100 150 200 Styrene Ave CBZ 11282 20316 56914 234746 626017 1254918 1840518 2395297 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromoform Ave CBZ 1460 2785 7164 29735 80261 164803 240639 325699 1.00 2.00 5.00 20.0 50.0 100 150 200 Isopropylbenzene Ave DCB 20214 38535 102851 424056 1099936 2200629 3227532 4168680 1.00 2.00 5.00 20.0 50.0 100 150 200 Bromobenzene Ave DCB 4167 7647 20483 82422 216512 440051 646947 852077 1.00 2.00 5.00 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 157 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 1,1,2,2-Tetrachloroethane Ave DCB 2471 4138 11086 43083 112230 230162 333588 438075 1.00 2.00 5.00 20.0 50.0 100 150 200 N-Propylbenzene Ave DCB 24132 46728 123000 502575 1317540 2596340 3793324 4908027 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichloropropane Ave DCB 1834 3184 8599 33490 88390 181542 262321 344689 1.00 2.00 5.00 20.0 50.0 100 150 200 2-Chlorotoluene Ave DCB 14292 25705 68289 272668 707862 1414432 2073876 2709003 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3,5-Trimethylbenzene Ave DCB 15145 29285 80436 329695 864754 1734520 2527907 3293833 1.00 2.00 5.00 20.0 50.0 100 150 200 4-Chlorotoluene Ave DCB 14596 26453 73310 285677 742016 1485407 2168057 2763304 1.00 2.00 5.00 20.0 50.0 100 150 200 tert-Butylbenzene Ave DCB 14522 27466 71308 298955 781727 1556746 2286383 2974995 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trimethylbenzene Ave DCB 15136 28261 78110 319956 834910 1682789 2459601 3184071 1.00 2.00 5.00 20.0 50.0 100 150 200 sec-Butylbenzene Ave DCB 22311 42414 116625 464344 1214094 2411809 3499921 4534829 1.00 2.00 5.00 20.0 50.0 100 150 200 1,3-Dichlorobenzene Ave DCB 8691 16131 41203 160290 414806 837508 1206617 1586342 1.00 2.00 5.00 20.0 50.0 100 150 200 p-Isopropyltoluene Ave DCB 18210 33284 93726 376512 981590 1949768 2832864 3693602 1.00 2.00 5.00 20.0 50.0 100 150 200 1,4-Dichlorobenzene Ave DCB 9158 15507 40669 157342 398505 809665 1176872 1542031 1.00 2.00 5.00 20.0 50.0 100 150 200 n-Butylbenzene Ave DCB 18437 34722 89516 362997 934982 1883655 2715730 3535815 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dichlorobenzene Ave DCB 7487 13040 34119 131641 337786 683433 999636 1324326 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2-Dibromo-3-Chloropropane Ave DCB 633 1424 5930 15066 31633 46778 63674 2.00 5.00 20.0 50.0 100 150 200 1,2,4-Trichlorobenzene Ave DCB 5227 10005 24201 95311 244912 514149 742574 994295 1.00 2.00 5.00 20.0 50.0 100 150 200 Hexachlorobutadiene Ave DCB 4479 7756 20002 79780 205629 409810 605699 802196 1.00 2.00 5.00 20.0 50.0 100 150 200 Naphthalene Ave DCB 5704 10774 28215 120923 321854 680580 1002739 1334973 1.00 2.00 5.00 20.0 50.0 100 150 200 1,2,3-Trichlorobenzene Ave DCB 3987 7373 18899 75826 197329 399786 579399 785372 1.00 2.00 5.00 20.0 50.0 100 150 200 Dibromofluoromethane Ave PFB 80643 187757 382786 572130 767393 20.0 50.0 100 150 200 1,2-Dichloroethane-d4 (Surr) Ave DFB 74925 176491 363647 537534 724583 20.0 50.0 100 150 200 

### FORM VI 8260B 

## 01/03/2013 Page 158 of 383

### FORM VI

Lab Name: Job No.:

Calibration ID: SDG No.: Instrument ID: Heated Purge: (Y/N) GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25 Analy Batch No.:169637

10606 Calibration Start Date: Calibration End Date: 11/14/2012 09:41 N 11/14/2012 12:54 GC Column: ID: INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE TYPE IS REF RESPONSE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 CONCENTRATION (UG/L) LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9 Toluene-d8 (Surr) Ave DFB 336603 789050 1583796 2364398 3109931 20.0 50.0 100 150 200 4-Bromofluorobenzene (Surr) Ave CBZ 110828 249531 503840 741720 994763 20.0 50.0 100 150 200 Curve Type Legend: Ave = Average ISTD Lin1 = Linear 1/conc ISTD Qua1 = Quadratic 1/conc ISTD



### FORM VI 8260B 

## 01/03/2013 Page 159 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 11/19/2012 17:14 11/19/2012 12:14 11/19/2012 14:09 ICV 500-170196/19

DB624 TestAmerica Chicago

Lab File ID:16S1119.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4279 0.4665 0.0100 45.9 50.0 -8.3 25.0 Ave Chloromethane 0.5246 0.5798 0.1000 45.2 50.0 -9.5 25.0 Ave Vinyl chloride 0.5248 0.5072 0.0100 51.7 50.0 3.5 25.0 Ave Bromomethane 0.1523 0.0100 47.2 50.0 -5.7 25.0 Lin2 Chloroethane 0.2426 0.2641 0.0100 45.9 50.0 -8.2 25.0 Ave Trichlorofluoromethane 0.5702 0.5875 0.0100 48.5 50.0 -2.9 25.0 Ave Acrolein 0.0673 0.0010 2080 2000 4.0 25.0 Lin2 1,1-Dichloroethene 0.3758 0.3748 0.0100 50.1 50.0 0.2 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.3311 0.3898 0.0100 42.5 50.0 -15.1 25.0 Ave Acetone 0.1027 0.0100 46.9 50.0 -6.2 25.0 Lin1 Carbon disulfide 1.296 1.284 0.0100 50.4 50.0 0.9 25.0 Ave Acetonitrile 0.0367 0.0330 0.0010 446 400 11.4 25.0 Ave Methylene Chloride 0.4290 0.4276 0.0100 50.2 50.0 0.3 25.0 Ave Acrylonitrile 0.1268 0.0010 407 400 1.7 25.0 Lin2 trans-1,2-Dichloroethene 0.4669 0.4413 0.0100 52.9 50.0 5.8 25.0 Ave Methyl tert-butyl ether 1.023 1.124 0.0100 45.5 50.0 -9.0 25.0 Ave 1,1-Dichloroethane 0.8721 0.8704 0.1000 50.1 50.0 0.2 25.0 Ave Vinyl acetate 0.8804 0.8347 0.0100 52.7 50.0 5.5 25.0 Ave 2,2-Dichloropropane 0.4986 0.4764 0.0100 52.3 50.0 4.7 25.0 Ave cis-1,2-Dichloroethene 0.4840 0.4787 0.0100 50.6 50.0 1.1 25.0 Ave 2-Butanone (MEK) 0.1524 0.1710 0.0100 44.6 50.0 -10.9 25.0 Ave Propionitrile 0.0316 0.0316 0.0010 399 400 -0.2 25.0 Ave Bromochloromethane 0.1702 0.1881 0.0100 45.2 50.0 -9.5 25.0 Ave Tetrahydrofuran 0.1042 0.0100 48.0 50.0 -4.0 25.0 Lin2 Chloroform 0.7748 0.7669 0.0100 50.5 50.0 1.0 25.0 Ave 1,1,1-Trichloroethane 0.6555 0.6244 0.0100 52.5 50.0 5.0 25.0 Ave Carbon tetrachloride 0.3724 0.3568 0.0100 52.2 50.0 4.4 25.0 Ave 1,1-Dichloropropene 0.6306 0.6354 0.0100 49.6 50.0 -0.8 25.0 Ave Benzene 1.216 1.203 0.0100 50.5 50.0 1.1 25.0 Ave 1,2-Dichloroethane 0.3697 0.3833 0.0100 48.2 50.0 -3.5 25.0 Ave Trichloroethene 0.2917 0.2856 0.0100 51.1 50.0 2.1 25.0 Ave 1,2-Dichloropropane 0.2959 0.2993 0.0100 49.4 50.0 -1.1 25.0 Ave Dibromomethane 0.1397 0.1425 0.0100 49.0 50.0 -2.0 25.0 Ave Bromodichloromethane 0.3379 0.3449 0.0100 49.0 50.0 -2.0 25.0 Ave 2-Chloroethyl vinyl ether 0.1258 0.1341 0.0100 46.9 50.0 -6.2 25.0 Ave cis-1,3-Dichloropropene 0.4011 0.4015 0.0100 53.7 53.8 -0.1 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.2120 0.2272 0.0100 46.7 50.0 -6.7 25.0 Ave Toluene 0.7132 0.7155 0.0100 49.8 50.0 -0.3 25.0 Ave trans-1,3-Dichloropropene 0.3348 0.3375 0.0100 48.2 48.6 -0.8 25.0 Ave 1,1,2-Trichloroethane 0.2675 0.2749 0.0100 48.6 50.0 -2.7 25.0 Ave


### FORM VII 8260B 

## 01/03/2013 Page 160 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 11/19/2012 17:14 11/19/2012 12:14 11/19/2012 14:09 ICV 500-170196/19

DB624 TestAmerica Chicago

Lab File ID:16S1119.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Tetrachloroethene 0.3914 0.3741 0.0100 52.3 50.0 4.6 25.0 Ave 1,3-Dichloropropane 0.4541 0.4540 0.0100 50.0 50.0 0.0 25.0 Ave 2-Hexanone 0.1831 0.1954 0.0100 46.9 50.0 -6.3 25.0 Ave Dibromochloromethane 0.2483 0.2462 0.0100 50.4 50.0 0.9 25.0 Ave 1,2-Dibromoethane 0.1719 0.1798 0.0100 47.8 50.0 -4.4 25.0 Ave 1-Chlorohexane 0.5208 0.5697 0.0100 45.7 50.0 -8.6 25.0 Ave Chlorobenzene 0.8647 0.9049 0.3000 47.8 50.0 -4.4 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3084 0.3090 0.0100 49.9 50.0 -0.2 25.0 Ave Ethylbenzene 0.5301 0.5284 0.0100 50.2 50.0 0.3 25.0 Ave m&p-Xylene 1.283 1.285 0.0100 99.8 100 -0.2 25.0 Ave o-Xylene 1.295 1.348 0.0100 48.0 50.0 -4.0 25.0 Ave Styrene 1.029 1.015 0.0100 50.7 50.0 1.4 25.0 Ave Bromoform 0.1401 0.1432 0.1000 48.9 50.0 -2.2 25.0 Ave Isopropylbenzene 3.211 3.252 0.0100 49.4 50.0 -1.3 25.0 Ave Bromobenzene 0.7556 0.7222 0.0100 52.3 50.0 4.6 25.0 Ave 1,1,2,2-Tetrachloroethane 0.5584 0.5589 0.3000 50.0 50.0 -0.1 25.0 Ave 1,2,3-Trichloropropane 0.1680 0.1732 0.0100 48.5 50.0 -3.0 25.0 Ave N-Propylbenzene 3.806 3.879 0.0100 49.1 50.0 -1.9 25.0 Ave 2-Chlorotoluene 2.300 2.312 0.0100 49.7 50.0 -0.6 25.0 Ave 1,3,5-Trimethylbenzene 2.896 2.676 0.0100 54.1 50.0 8.2 25.0 Ave 4-Chlorotoluene 2.597 2.685 0.0100 48.4 50.0 -3.3 25.0 Ave tert-Butylbenzene 2.273 2.285 0.0100 49.7 50.0 -0.5 25.0 Ave 1,2,4-Trimethylbenzene 2.842 2.723 0.0100 52.2 50.0 4.4 25.0 Ave sec-Butylbenzene 3.410 3.457 0.0100 49.3 50.0 -1.4 25.0 Ave 1,3-Dichlorobenzene 1.361 1.415 0.0100 48.1 50.0 -3.8 25.0 Ave p-Isopropyltoluene 2.828 2.902 0.0100 48.7 50.0 -2.5 25.0 Ave 1,4-Dichlorobenzene 1.440 1.398 0.0100 51.5 50.0 3.0 25.0 Ave n-Butylbenzene 2.940 2.831 0.0100 51.9 50.0 3.8 25.0 Ave 1,2-Dichlorobenzene 1.205 1.252 0.0100 48.1 50.0 -3.8 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0784 0.0839 0.0100 46.7 50.0 -6.6 25.0 Ave 1,2,4-Trichlorobenzene 0.8024 0.8500 0.0100 47.2 50.0 -5.6 25.0 Ave Hexachlorobutadiene 0.5223 0.0100 51.7 50.0 3.4 25.0 Qua1 Naphthalene 1.356 0.0100 47.5 50.0 -4.9 25.0 Lin2 1,2,3-Trichlorobenzene 0.5963 0.0100 45.8 50.0 -8.3 25.0 Qua2 Dibromofluoromethane 0.3997 0.3958 0.0100 43.7 43.3 1.0 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3112 0.3196 0.0100 42.1 43.3 -2.6 25.0 Ave Toluene-d8 (Surr) 1.099 1.017 0.0100 46.8 43.3 8.1 25.0 Ave 4-Bromofluorobenzene (Surr) 0.5002 0.4856 0.0100 44.6 43.3 3.0 25.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 161 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 11/19/2012 17:14 11/19/2012 14:32 11/19/2012 16:28 ICV 500-170196/19

DB624 TestAmerica Chicago

Lab File ID:16S1119.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.3493 0.4262 0.0100 41.0 50.0 -18.0 25.0 Ave Iodomethane 0.6405 0.5737 0.0100 55.8 50.0 11.6 25.0 Ave Methyl acetate 0.2295 0.3675 0.0100 31.2 50.0 -37.6* 25.0 Ave Hexane 0.6708 0.7834 0.0100 42.8 50.0 -14.4 25.0 Ave Cyclohexane 0.8544 0.0100 46.7 50.0 -6.6 25.0 Lin2 Heptane 0.5269 0.5932 0.0100 44.4 50.0 -11.2 25.0 Ave Methylcyclohexane 0.5154 0.5531 0.0100 46.6 50.0 -6.8 25.0 Ave 1,3,5-Trichlorobenzene 1.063 1.012 0.0100 52.5 50.0 5.0 25.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 162 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 12/18/2012 07:43 11/19/2012 12:14 11/19/2012 14:09 CCV 500-173225/2

DB624 TestAmerica Chicago

Lab File ID:16C1218.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4528 0.4665 0.0100 48.5 50.0 -2.9 50.0 Ave Chloromethane 0.5416 0.5798 0.1000 46.7 50.0 -6.6 50.0 Ave Vinyl chloride 0.5144 0.5072 0.0100 50.7 50.0 1.4 20.0 Ave Bromomethane 0.1435 0.0100 44.3 50.0 -11.4 50.0 Lin2 Chloroethane 0.2551 0.2641 0.0100 48.3 50.0 -3.4 50.0 Ave Trichlorofluoromethane 0.6000 0.5875 0.0100 51.1 50.0 2.1 50.0 Ave Acrolein 0.0644 0.0010 1988 2000 -0.6 50.0 Lin2 1,1-Dichloroethene 0.3809 0.3748 0.0100 50.8 50.0 1.6 20.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.3839 0.3898 0.0100 49.2 50.0 -1.5 50.0 Ave Acetone 0.0931 0.0100 41.9 50.0 -16.1 50.0 Lin1 Carbon disulfide 1.002 1.284 0.0100 39.0 50.0 -22.0 50.0 Ave Acetonitrile 0.0321 0.0330 0.0010 389 400 -2.7 50.0 Ave Methylene Chloride 0.4215 0.4276 0.0100 49.3 50.0 -1.4 50.0 Ave Acrylonitrile 0.1212 0.0010 388 400 -3.0 50.0 Lin2 trans-1,2-Dichloroethene 0.4513 0.4413 0.0100 51.1 50.0 2.3 50.0 Ave Methyl tert-butyl ether 1.091 1.124 0.0100 48.5 50.0 -2.9 50.0 Ave 1,1-Dichloroethane 0.8832 0.8704 0.1000 50.7 50.0 1.5 50.0 Ave Vinyl acetate 0.6282 0.8347 0.0100 37.6 50.0 -24.7 50.0 Ave 2,2-Dichloropropane 0.4671 0.4764 0.0100 49.0 50.0 -1.9 50.0 Ave cis-1,2-Dichloroethene 0.4935 0.4787 0.0100 51.5 50.0 3.1 50.0 Ave 2-Butanone (MEK) 0.1457 0.1710 0.0100 42.6 50.0 -14.8 50.0 Ave Propionitrile 0.0308 0.0316 0.0010 389 400 -2.6 50.0 Ave Bromochloromethane 0.1879 0.1881 0.0100 50.0 50.0 -0.1 50.0 Ave Tetrahydrofuran 0.1049 0.0100 48.3 50.0 -3.3 50.0 Lin2 Chloroform 0.7777 0.7669 0.0100 50.7 50.0 1.4 20.0 Ave 1,1,1-Trichloroethane 0.6405 0.6244 0.0100 51.3 50.0 2.6 50.0 Ave Carbon tetrachloride 0.3789 0.3568 0.0100 53.1 50.0 6.2 50.0 Ave 1,1-Dichloropropene 0.6530 0.6354 0.0100 51.4 50.0 2.8 50.0 Ave Benzene 1.248 1.203 0.0100 51.9 50.0 3.7 50.0 Ave 1,2-Dichloroethane 0.3859 0.3833 0.0100 50.3 50.0 0.7 50.0 Ave Trichloroethene 0.3001 0.2856 0.0100 52.5 50.0 5.1 50.0 Ave 1,2-Dichloropropane 0.3094 0.2993 0.0100 51.7 50.0 3.4 20.0 Ave Dibromomethane 0.1436 0.1425 0.0100 50.4 50.0 0.8 50.0 Ave Bromodichloromethane 0.3562 0.3449 0.0100 51.6 50.0 3.3 50.0 Ave 2-Chloroethyl vinyl ether 0.1255 0.1341 0.0100 46.8 50.0 -6.4 50.0 Ave cis-1,3-Dichloropropene 0.4120 0.4015 0.0100 51.3 50.0 2.6 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.2008 0.2272 0.0100 44.2 50.0 -11.6 50.0 Ave Toluene 0.7440 0.7155 0.0100 52.0 50.0 4.0 20.0 Ave trans-1,3-Dichloropropene 0.3462 0.3375 0.0100 51.3 50.0 2.6 50.0 Ave 1,1,2-Trichloroethane 0.2819 0.2749 0.0100 51.3 50.0 2.5 50.0 Ave


### FORM VII 8260B 

## 01/03/2013 Page 163 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 12/18/2012 07:43 11/19/2012 12:14 11/19/2012 14:09 CCV 500-173225/2

DB624 TestAmerica Chicago

Lab File ID:16C1218.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Tetrachloroethene 0.4095 0.3741 0.0100 54.7 50.0 9.5 50.0 Ave 1,3-Dichloropropane 0.4772 0.4540 0.0100 52.6 50.0 5.1 50.0 Ave 2-Hexanone 0.1760 0.1954 0.0100 45.0 50.0 -9.9 50.0 Ave Dibromochloromethane 0.2600 0.2462 0.0100 52.8 50.0 5.6 50.0 Ave 1,2-Dibromoethane 0.1840 0.1798 0.0100 51.2 50.0 2.4 50.0 Ave 1-Chlorohexane 0.5919 0.5697 0.0100 52.0 50.0 3.9 50.0 Ave Chlorobenzene 0.9618 0.9049 0.3000 53.1 50.0 6.3 50.0 Ave 1,1,1,2-Tetrachloroethane 0.3251 0.3090 0.0100 52.6 50.0 5.2 50.0 Ave Ethylbenzene 0.5580 0.5284 0.0100 52.8 50.0 5.6 20.0 Ave m&p-Xylene 1.371 1.285 0.0100 107 100 6.6 50.0 Ave o-Xylene 1.408 1.348 0.0100 52.2 50.0 4.4 50.0 Ave Styrene 1.072 1.015 0.0100 52.8 50.0 5.7 50.0 Ave Bromoform 0.1438 0.1432 0.1000 50.2 50.0 0.4 50.0 Ave Isopropylbenzene 3.568 3.252 0.0100 54.9 50.0 9.7 50.0 Ave Bromobenzene 0.7961 0.7222 0.0100 55.1 50.0 10.2 50.0 Ave 1,1,2,2-Tetrachloroethane 0.5755 0.5589 0.3000 51.5 50.0 3.0 50.0 Ave 1,2,3-Trichloropropane 0.1783 0.1732 0.0100 51.5 50.0 3.0 50.0 Ave N-Propylbenzene 4.216 3.879 0.0100 54.4 50.0 8.7 50.0 Ave 2-Chlorotoluene 2.440 2.312 0.0100 52.8 50.0 5.5 50.0 Ave 1,3,5-Trimethylbenzene 2.871 2.676 0.0100 53.6 50.0 7.3 50.0 Ave 4-Chlorotoluene 2.874 2.685 0.0100 53.5 50.0 7.0 50.0 Ave tert-Butylbenzene 2.462 2.285 0.0100 53.9 50.0 7.7 50.0 Ave 1,2,4-Trimethylbenzene 2.888 2.723 0.0100 53.1 50.0 6.1 50.0 Ave sec-Butylbenzene 3.724 3.457 0.0100 53.9 50.0 7.7 50.0 Ave 1,3-Dichlorobenzene 1.495 1.415 0.0100 52.9 50.0 5.7 50.0 Ave p-Isopropyltoluene 3.112 2.902 0.0100 53.6 50.0 7.2 50.0 Ave 1,4-Dichlorobenzene 1.476 1.398 0.0100 52.8 50.0 5.5 50.0 Ave n-Butylbenzene 3.012 2.831 0.0100 53.2 50.0 6.4 50.0 Ave 1,2-Dichlorobenzene 1.285 1.252 0.0100 51.3 50.0 2.7 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0733 0.0839 0.0100 43.7 50.0 -12.7 50.0 Ave 1,2,4-Trichlorobenzene 0.7890 0.8500 0.0100 46.4 50.0 -7.2 50.0 Ave Hexachlorobutadiene 0.4997 0.0100 49.2 50.0 -1.7 50.0 Qua1 Naphthalene 1.201 0.0100 42.0 50.0 -16.1 50.0 Lin2 1,2,3-Trichlorobenzene 0.5323 0.0100 40.6 50.0 -18.9 50.0 Qua2 Dibromofluoromethane 0.4098 0.3958 0.0100 44.8 43.3 3.5 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3114 0.3196 0.0100 42.2 43.3 -2.6 50.0 Ave Toluene-d8 (Surr) 1.098 1.017 0.0100 46.7 43.3 7.9 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4926 0.4856 0.0100 43.9 43.3 1.4 50.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 164 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 12/18/2012 08:07 11/19/2012 12:14 11/19/2012 14:09 CCV 500-173225/3

DB624 TestAmerica Chicago

Lab File ID:16D1218.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.3999 0.3958 0.0100 43.7 43.3 1.0 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.3212 0.3196 0.0100 43.5 43.3 0.5 50.0 Ave Toluene-d8 (Surr) 1.127 1.017 0.0100 47.9 43.3 10.8 50.0 Ave 4-Bromofluorobenzene (Surr) 0.5066 0.4856 0.0100 45.2 43.3 4.3 50.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 165 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm) 500-53315-1

CMS16 12/18/2012 08:07 11/19/2012 14:32 11/19/2012 16:28 CCV 500-173225/3

DB624 TestAmerica Chicago

Lab File ID:16D1218.D Heated Purge: (Y/N) Y Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.3993 0.5997 0.0100 33.3 50.0 -33.4 50.0 Ave Ethyl ether 0.3686 0.4262 0.0100 43.2 50.0 -13.5 50.0 Ave Iodomethane 0.5127 0.5737 0.0100 89.4 100 -10.6 50.0 Ave 3-Chloropropene 0.2090 0.2319 0.0100 90.1 100 -9.9 50.0 Ave Methyl acetate 0.3591 0.3675 0.0100 48.8 50.0 -2.3 50.0 Ave Hexane 0.6754 0.7834 0.0100 43.1 50.0 -13.8 50.0 Ave Isopropyl ether 1.573 1.776 0.0100 44.3 50.0 -11.4 50.0 Ave 2-Chloro-1,3-butadiene 0.7886 0.8947 0.0100 44.1 50.0 -11.9 50.0 Ave Ethyl acetate 0.2917 0.3031 0.0100 481 500 -3.8 50.0 Ave Methacrylonitrile 0.2133 0.2264 0.0100 94.2 100 -5.8 50.0 Ave Cyclohexane 0.8119 0.0100 44.3 50.0 -11.4 50.0 Lin2 Isobutyl alcohol 0.0103 0.0107 0.0010 3867 4000 -3.3 50.0 Ave 2,2,4-Trimethylpentane 1.309 1.405 0.0100 46.6 50.0 -6.8 50.0 Ave Heptane 0.5496 0.5932 0.0100 46.3 50.0 -7.4 50.0 Ave n-Butyl alcohol 0.0063 0.0063 0.0010 3996 4000 -0.1 50.0 Ave Methylcyclohexane 0.5110 0.5531 0.0100 46.2 50.0 -7.6 50.0 Ave Methyl methacrylate 0.2175 0.2123 0.0100 102 100 2.4 50.0 Ave 2-Nitropropane 0.0780 0.0771 0.0100 4048 4000 1.2 50.0 Ave Ethyl methacrylate 0.3633 0.3579 0.0100 102 100 1.5 50.0 Ave Cyclohexanone 0.0493 0.0100 4009 4000 0.2 50.0 Lin1 trans-1,4-Dichloro-2-butene 0.0828 0.0868 0.0100 95.4 100 -4.6 50.0 Ave Pentachloroethane 0.2096 0.2111 0.0100 99.3 100 -0.7 50.0 Ave 1,3,5-Trichlorobenzene 1.023 1.012 0.0100 50.5 50.0 1.0 50.0 Ave 2-Methylnaphthalene 0.4760 0.0100 35.6 50.0 -28.8 50.0 Qua2



### FORM VII 8260B 

## 01/03/2013 Page 166 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 11/14/2012 16:57 11/14/2012 09:41 11/14/2012 12:54 ICV 500-169636/20 TestAmerica Chicago

Lab File ID:25S1114.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4588 0.6475 0.0100 35.4 50.0 -29.1* 25.0 Ave Chloromethane 0.7458 1.001 0.1000 37.2 50.0 -25.5* 25.0 Ave Vinyl chloride 0.7960 0.7756 0.0100 51.3 50.0 2.6 25.0 Ave Bromomethane 0.1019 0.0100 37.4 50.0 -25.3* 25.0 Qua1 Chloroethane 0.3008 0.3396 0.0100 44.3 50.0 -11.4 25.0 Ave Trichlorofluoromethane 0.7439 0.7698 0.0100 48.3 50.0 -3.4 25.0 Ave Dichlorofluoromethane 0.8663 0.9059 0.0100 47.8 50.0 -4.4 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5075 0.5272 0.0100 48.1 50.0 -3.7 25.0 Ave Acrolein 0.0541 0.0531 0.0010 2035 2000 1.8 25.0 Ave 1,1-Dichloroethene 0.4548 0.4396 0.0100 51.7 50.0 3.5 25.0 Ave Acetone 0.0598 0.0100 48.1 50.0 -3.9 25.0 Lin1 Carbon disulfide 1.384 1.673 0.0100 41.4 50.0 -17.3 25.0 Ave Acetonitrile 0.0336 0.0339 0.0010 396 400 -1.0 25.0 Ave Methylene Chloride 0.4378 0.4144 0.0100 52.8 50.0 5.6 25.0 Ave Methyl tert-butyl ether 0.6540 0.5971 0.0100 54.8 50.0 9.5 25.0 Ave trans-1,2-Dichloroethene 0.5297 0.4898 0.0100 54.1 50.0 8.1 25.0 Ave Acrylonitrile 0.0983 0.1009 0.0010 389 400 -2.7 25.0 Ave 1,1-Dichloroethane 1.147 1.092 0.1000 52.6 50.0 5.1 25.0 Ave Vinyl acetate 0.7013 0.6134 0.0100 57.2 50.0 14.3 25.0 Ave 2,2-Dichloropropane 0.7339 0.6724 0.0100 54.6 50.0 9.1 25.0 Ave cis-1,2-Dichloroethene 0.5238 0.4900 0.0100 53.5 50.0 6.9 25.0 Ave 2-Butanone (MEK) 0.0921 0.0859 0.0100 53.6 50.0 7.2 25.0 Ave Propionitrile 0.0238 0.0229 0.0010 415 400 3.8 25.0 Ave Bromochloromethane 0.1858 0.1774 0.0100 52.4 50.0 4.8 25.0 Ave Tetrahydrofuran 0.0614 0.0602 0.0100 51.0 50.0 2.0 25.0 Ave Chloroform 0.8241 0.7678 0.0100 53.7 50.0 7.3 25.0 Ave 1,1,1-Trichloroethane 0.8093 0.7459 0.0100 54.3 50.0 8.5 25.0 Ave Carbon tetrachloride 0.5159 0.4978 0.0100 51.8 50.0 3.6 25.0 Ave 1,1-Dichloropropene 0.7388 0.7224 0.0100 51.1 50.0 2.3 25.0 Ave Benzene 1.298 1.296 0.0100 50.1 50.0 0.1 25.0 Ave 1,2-Dichloroethane 0.3449 0.3458 0.0100 49.9 50.0 -0.3 25.0 Ave Trichloroethene 0.3677 0.3521 0.0100 52.2 50.0 4.5 25.0 Ave 1,2-Dichloropropane 0.3892 0.3829 0.0100 50.8 50.0 1.6 25.0 Ave Dibromomethane 0.1220 0.1248 0.0100 48.9 50.0 -2.2 25.0 Ave Bromodichloromethane 0.3555 0.3590 0.0100 49.5 50.0 -1.0 25.0 Ave 2-Chloroethyl vinyl ether 0.1332 0.1198 0.0100 55.6 50.0 11.2 25.0 Ave cis-1,3-Dichloropropene 0.4012 0.3838 0.0100 56.2 53.8 4.5 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1388 0.1313 0.0100 52.9 50.0 5.8 25.0 Ave Toluene 0.8148 0.7916 0.0100 51.5 50.0 2.9 25.0 Ave trans-1,3-Dichloropropene 0.3017 0.2943 0.0100 49.8 48.6 2.5 25.0 Ave


### FORM VII 8260B 

## 01/03/2013 Page 167 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 11/14/2012 16:57 11/14/2012 09:41 11/14/2012 12:54 ICV 500-169636/20 TestAmerica Chicago

Lab File ID:25S1114.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2447 0.2366 0.0100 51.7 50.0 3.4 25.0 Ave Tetrachloroethene 0.4874 0.4729 0.0100 51.5 50.0 3.1 25.0 Ave 1,3-Dichloropropane 0.3709 0.3650 0.0100 50.8 50.0 1.6 25.0 Ave 2-Hexanone 0.1093 0.1027 0.0100 53.2 50.0 6.5 25.0 Ave Dibromochloromethane 0.2674 0.2634 0.0100 50.8 50.0 1.5 25.0 Ave 1,2-Dibromoethane 0.1557 0.1542 0.0100 50.5 50.0 1.0 25.0 Ave 1-Chlorohexane 0.7340 0.7247 0.0100 50.6 50.0 1.3 25.0 Ave Chlorobenzene 0.9841 1.046 0.3000 47.0 50.0 -5.9 25.0 Ave Ethylbenzene 0.6167 0.6127 0.0100 50.3 50.0 0.7 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3414 0.3379 0.0100 50.5 50.0 1.0 25.0 Ave m&p-Xylene 1.430 1.453 0.0100 98.4 100 -1.6 25.0 Ave o-Xylene 1.361 1.406 0.0100 48.4 50.0 -3.2 25.0 Ave Styrene 1.088 1.067 0.0100 51.0 50.0 1.9 25.0 Ave Bromoform 0.1458 0.1393 0.1000 52.3 50.0 4.6 25.0 Ave Isopropylbenzene 4.271 4.186 0.0100 51.0 50.0 2.0 25.0 Ave Bromobenzene 0.8982 0.8368 0.0100 53.7 50.0 7.3 25.0 Ave 1,1,2,2-Tetrachloroethane 0.4729 0.4463 0.3000 53.0 50.0 6.0 25.0 Ave N-Propylbenzene 4.914 4.979 0.0100 49.4 50.0 -1.3 25.0 Ave 1,2,3-Trichloropropane 0.3629 0.3465 0.0100 52.4 50.0 4.7 25.0 Ave 2-Chlorotoluene 2.767 2.750 0.0100 50.3 50.0 0.6 25.0 Ave 1,3,5-Trimethylbenzene 3.643 3.254 0.0100 56.0 50.0 12.0 25.0 Ave 4-Chlorotoluene 2.758 2.865 0.0100 48.1 50.0 -3.7 25.0 Ave tert-Butylbenzene 3.068 2.966 0.0100 51.7 50.0 3.4 25.0 Ave 1,2,4-Trimethylbenzene 3.425 3.164 0.0100 54.1 50.0 8.2 25.0 Ave sec-Butylbenzene 4.675 4.606 0.0100 50.7 50.0 1.5 25.0 Ave 1,3-Dichlorobenzene 1.554 1.640 0.0100 47.4 50.0 -5.2 25.0 Ave p-Isopropyltoluene 3.713 3.718 0.0100 49.9 50.0 -0.1 25.0 Ave 1,4-Dichlorobenzene 1.618 1.612 0.0100 50.2 50.0 0.4 25.0 Ave n-Butylbenzene 3.588 3.626 0.0100 49.5 50.0 -1.1 25.0 Ave 1,2-Dichlorobenzene 1.308 1.356 0.0100 48.2 50.0 -3.5 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0608 0.0611 0.0100 49.7 50.0 -0.6 25.0 Ave 1,2,4-Trichlorobenzene 0.9093 0.9938 0.0100 45.8 50.0 -8.5 25.0 Ave Hexachlorobutadiene 0.8368 0.8144 0.0100 51.4 50.0 2.8 25.0 Ave Naphthalene 1.319 1.233 0.0100 53.5 50.0 7.0 25.0 Ave 1,2,3-Trichlorobenzene 0.7753 0.7736 0.0100 50.1 50.0 0.2 25.0 Ave Dibromofluoromethane 0.4174 0.4056 0.0100 51.5 50.0 2.9 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2583 0.2620 0.0100 49.3 50.0 -1.4 25.0 Ave Toluene-d8 (Surr) 1.171 1.154 0.0100 50.7 50.0 1.5 25.0 Ave 4-Bromofluorobenzene (Surr) 0.4512 0.4616 0.0100 48.9 50.0 -2.3 25.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 168 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 11/14/2012 16:57 11/14/2012 09:41 11/14/2012 12:54 ICV 500-169637/20 TestAmerica Chicago

Lab File ID:25S1114.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4588 0.6475 0.0100 35.4 50.0 -29.1* 25.0 Ave Chloromethane 0.7458 1.001 0.1000 37.2 50.0 -25.5* 25.0 Ave Vinyl chloride 0.7960 0.7756 0.0100 51.3 50.0 2.6 25.0 Ave Bromomethane 0.1019 0.0100 37.4 50.0 -25.3* 25.0 Qua1 Chloroethane 0.3008 0.3396 0.0100 44.3 50.0 -11.4 25.0 Ave Trichlorofluoromethane 0.7439 0.7698 0.0100 48.3 50.0 -3.4 25.0 Ave Dichlorofluoromethane 0.8663 0.9059 0.0100 47.8 50.0 -4.4 25.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5075 0.5272 0.0100 48.1 50.0 -3.7 25.0 Ave Acrolein 0.0541 0.0531 0.0010 2035 2000 1.8 25.0 Ave 1,1-Dichloroethene 0.4548 0.4396 0.0100 51.7 50.0 3.5 25.0 Ave Acetone 0.0598 0.0100 48.1 50.0 -3.9 25.0 Lin1 Carbon disulfide 1.384 1.673 0.0100 41.4 50.0 -17.3 25.0 Ave Acetonitrile 0.0336 0.0339 0.0010 396 400 -1.0 25.0 Ave Methylene Chloride 0.4378 0.4144 0.0100 52.8 50.0 5.6 25.0 Ave Methyl tert-butyl ether 0.6540 0.5971 0.0100 54.8 50.0 9.5 25.0 Ave trans-1,2-Dichloroethene 0.5297 0.4898 0.0100 54.1 50.0 8.1 25.0 Ave Acrylonitrile 0.0983 0.1009 0.0010 389 400 -2.7 25.0 Ave 1,1-Dichloroethane 1.147 1.092 0.1000 52.6 50.0 5.1 25.0 Ave Vinyl acetate 0.7013 0.6134 0.0100 57.2 50.0 14.3 25.0 Ave 2,2-Dichloropropane 0.7339 0.6724 0.0100 54.6 50.0 9.1 25.0 Ave cis-1,2-Dichloroethene 0.5238 0.4900 0.0100 53.5 50.0 6.9 25.0 Ave 2-Butanone (MEK) 0.0921 0.0859 0.0100 53.6 50.0 7.2 25.0 Ave Propionitrile 0.0238 0.0229 0.0010 415 400 3.8 25.0 Ave Bromochloromethane 0.1858 0.1774 0.0100 52.4 50.0 4.8 25.0 Ave Tetrahydrofuran 0.0614 0.0602 0.0100 51.0 50.0 2.0 25.0 Ave Chloroform 0.8241 0.7678 0.0100 53.7 50.0 7.3 25.0 Ave 1,1,1-Trichloroethane 0.8093 0.7459 0.0100 54.3 50.0 8.5 25.0 Ave Carbon tetrachloride 0.5159 0.4978 0.0100 51.8 50.0 3.6 25.0 Ave 1,1-Dichloropropene 0.7388 0.7224 0.0100 51.1 50.0 2.3 25.0 Ave Benzene 1.298 1.296 0.0100 50.1 50.0 0.1 25.0 Ave 1,2-Dichloroethane 0.3449 0.3458 0.0100 49.9 50.0 -0.3 25.0 Ave Trichloroethene 0.3677 0.3521 0.0100 52.2 50.0 4.5 25.0 Ave 1,2-Dichloropropane 0.3892 0.3829 0.0100 50.8 50.0 1.6 25.0 Ave Dibromomethane 0.1220 0.1248 0.0100 48.9 50.0 -2.2 25.0 Ave Bromodichloromethane 0.3555 0.3590 0.0100 49.5 50.0 -1.0 25.0 Ave 2-Chloroethyl vinyl ether 0.1332 0.1198 0.0100 55.6 50.0 11.2 25.0 Ave cis-1,3-Dichloropropene 0.4012 0.3838 0.0100 56.2 53.8 4.5 25.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1388 0.1313 0.0100 52.9 50.0 5.8 25.0 Ave Toluene 0.8148 0.7916 0.0100 51.5 50.0 2.9 25.0 Ave trans-1,3-Dichloropropene 0.3017 0.2943 0.0100 49.8 48.6 2.5 25.0 Ave


### FORM VII 8260B 

## 01/03/2013 Page 169 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 11/14/2012 16:57 11/14/2012 09:41 11/14/2012 12:54 ICV 500-169637/20 TestAmerica Chicago

Lab File ID:25S1114.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2447 0.2366 0.0100 51.7 50.0 3.4 25.0 Ave Tetrachloroethene 0.4874 0.4729 0.0100 51.5 50.0 3.1 25.0 Ave 1,3-Dichloropropane 0.3709 0.3650 0.0100 50.8 50.0 1.6 25.0 Ave 2-Hexanone 0.1093 0.1027 0.0100 53.2 50.0 6.5 25.0 Ave Dibromochloromethane 0.2674 0.2634 0.0100 50.8 50.0 1.5 25.0 Ave 1,2-Dibromoethane 0.1557 0.1542 0.0100 50.5 50.0 1.0 25.0 Ave 1-Chlorohexane 0.7340 0.7247 0.0100 50.6 50.0 1.3 25.0 Ave Chlorobenzene 0.9841 1.046 0.3000 47.0 50.0 -5.9 25.0 Ave Ethylbenzene 0.6167 0.6127 0.0100 50.3 50.0 0.7 25.0 Ave 1,1,1,2-Tetrachloroethane 0.3414 0.3379 0.0100 50.5 50.0 1.0 25.0 Ave m&p-Xylene 1.430 1.453 0.0100 98.4 100 -1.6 25.0 Ave o-Xylene 1.361 1.406 0.0100 48.4 50.0 -3.2 25.0 Ave Styrene 1.088 1.067 0.0100 51.0 50.0 1.9 25.0 Ave Bromoform 0.1458 0.1393 0.1000 52.3 50.0 4.6 25.0 Ave Isopropylbenzene 4.271 4.186 0.0100 51.0 50.0 2.0 25.0 Ave Bromobenzene 0.8982 0.8368 0.0100 53.7 50.0 7.3 25.0 Ave 1,1,2,2-Tetrachloroethane 0.4729 0.4463 0.3000 53.0 50.0 6.0 25.0 Ave N-Propylbenzene 4.914 4.979 0.0100 49.4 50.0 -1.3 25.0 Ave 1,2,3-Trichloropropane 0.3629 0.3465 0.0100 52.4 50.0 4.7 25.0 Ave 2-Chlorotoluene 2.767 2.750 0.0100 50.3 50.0 0.6 25.0 Ave 1,3,5-Trimethylbenzene 3.643 3.254 0.0100 56.0 50.0 12.0 25.0 Ave 4-Chlorotoluene 2.758 2.865 0.0100 48.1 50.0 -3.7 25.0 Ave tert-Butylbenzene 3.068 2.966 0.0100 51.7 50.0 3.4 25.0 Ave 1,2,4-Trimethylbenzene 3.425 3.164 0.0100 54.1 50.0 8.2 25.0 Ave sec-Butylbenzene 4.675 4.606 0.0100 50.7 50.0 1.5 25.0 Ave 1,3-Dichlorobenzene 1.554 1.640 0.0100 47.4 50.0 -5.2 25.0 Ave p-Isopropyltoluene 3.713 3.718 0.0100 49.9 50.0 -0.1 25.0 Ave 1,4-Dichlorobenzene 1.618 1.612 0.0100 50.2 50.0 0.4 25.0 Ave n-Butylbenzene 3.588 3.626 0.0100 49.5 50.0 -1.1 25.0 Ave 1,2-Dichlorobenzene 1.308 1.356 0.0100 48.2 50.0 -3.5 25.0 Ave 1,2-Dibromo-3-Chloropropane 0.0608 0.0611 0.0100 49.7 50.0 -0.6 25.0 Ave 1,2,4-Trichlorobenzene 0.9093 0.9938 0.0100 45.8 50.0 -8.5 25.0 Ave Hexachlorobutadiene 0.8368 0.8144 0.0100 51.4 50.0 2.8 25.0 Ave Naphthalene 1.319 1.233 0.0100 53.5 50.0 7.0 25.0 Ave 1,2,3-Trichlorobenzene 0.7753 0.7736 0.0100 50.1 50.0 0.2 25.0 Ave Dibromofluoromethane 0.4174 0.4056 0.0100 51.5 50.0 2.9 25.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2583 0.2620 0.0100 49.3 50.0 -1.4 25.0 Ave Toluene-d8 (Surr) 1.171 1.154 0.0100 50.7 50.0 1.5 25.0 Ave 4-Bromofluorobenzene (Surr) 0.4512 0.4616 0.0100 48.9 50.0 -2.3 25.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 170 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 11/14/2012 16:57 11/14/2012 13:19 11/14/2012 16:08 ICV 500-169636/20 TestAmerica Chicago

Lab File ID:25S1114.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.3200 0.3493 0.0100 45.8 50.0 -8.4 25.0 Ave Iodomethane 0.7644 0.0100 89.2 50.0 78.3* 25.0 Qua1 Methyl acetate 0.1672 0.2344 0.0100 35.7 50.0 -28.6* 25.0 Ave Hexane 1.237 1.324 0.0100 46.7 50.0 -6.6 25.0 Ave Cyclohexane 1.502 1.508 0.0100 49.8 50.0 -0.4 25.0 Ave Heptane 0.8903 0.9508 0.0100 46.8 50.0 -6.4 25.0 Ave Methylcyclohexane 0.6725 0.6690 0.0100 50.3 50.0 0.5 25.0 Ave 1,3,5-Trichlorobenzene 1.242 1.274 0.0100 48.8 50.0 -2.5 25.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 171 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 11/14/2012 16:57 11/14/2012 13:19 11/14/2012 16:08 ICV 500-169637/20 TestAmerica Chicago

Lab File ID:25S1114.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF
Ethyl ether 0.3200 0.3493 0.0100 45.8 50.0 -8.4 25.0 Ave Iodomethane 0.7644 0.0100 89.2 50.0 78.3* 25.0 Qua1 Methyl acetate 0.1672 0.2344 0.0100 35.7 50.0 -28.6* 25.0 Ave Hexane 1.237 1.324 0.0100 46.7 50.0 -6.6 25.0 Ave Cyclohexane 1.502 1.508 0.0100 49.8 50.0 -0.4 25.0 Ave Heptane 0.8903 0.9508 0.0100 46.8 50.0 -6.4 25.0 Ave Methylcyclohexane 0.6725 0.6690 0.0100 50.3 50.0 0.5 25.0 Ave 1,3,5-Trichlorobenzene 1.242 1.274 0.0100 48.8 50.0 -2.5 25.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 172 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:06 11/14/2012 09:41 11/14/2012 12:54 CCV 500-173509/2 TestAmerica Chicago

Lab File ID:25C1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4729 0.6475 0.0100 36.5 50.0 -27.0 50.0 Ave Chloromethane 0.9148 1.001 0.1000 45.7 50.0 -8.7 50.0 Ave Vinyl chloride 0.7427 0.7756 0.0100 47.9 50.0 -4.2 20.0 Ave Bromomethane 0.1501 0.0100 52.8 50.0 5.6 50.0 Qua1 Chloroethane 0.3693 0.3396 0.0100 54.4 50.0 8.8 50.0 Ave Trichlorofluoromethane 0.9122 0.7698 0.0100 59.3 50.0 18.5 50.0 Ave Dichlorofluoromethane 1.034 0.9059 0.0100 57.1 50.0 14.1 50.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5503 0.5272 0.0100 52.2 50.0 4.4 50.0 Ave Acrolein 0.0347 0.0531 0.0010 1306 2000 -34.7 50.0 Ave 1,1-Dichloroethene 0.4452 0.4396 0.0100 50.6 50.0 1.3 20.0 Ave Acetone 0.0619 0.0100 49.9 50.0 -0.2 50.0 Lin1 Carbon disulfide 1.432 1.673 0.0100 42.8 50.0 -14.4 50.0 Ave Acetonitrile 0.0349 0.0339 0.0010 412 400 3.0 50.0 Ave Methylene Chloride 0.3952 0.4144 0.0100 47.7 50.0 -4.6 50.0 Ave Methyl tert-butyl ether 0.5759 0.5971 0.0100 48.2 50.0 -3.5 50.0 Ave trans-1,2-Dichloroethene 0.4990 0.4898 0.0100 50.9 50.0 1.9 50.0 Ave Acrylonitrile 0.0990 0.1009 0.0010 392 400 -1.9 50.0 Ave 1,1-Dichloroethane 1.098 1.092 0.1000 50.3 50.0 0.6 50.0 Ave Vinyl acetate 0.6029 0.6134 0.0100 49.1 50.0 -1.7 50.0 Ave 2,2-Dichloropropane 0.7827 0.6724 0.0100 58.2 50.0 16.4 50.0 Ave cis-1,2-Dichloroethene 0.4882 0.4900 0.0100 49.8 50.0 -0.4 50.0 Ave 2-Butanone (MEK) 0.0910 0.0859 0.0100 53.0 50.0 6.0 50.0 Ave Propionitrile 0.0241 0.0229 0.0010 421 400 5.3 50.0 Ave Bromochloromethane 0.1806 0.1774 0.0100 50.9 50.0 1.8 50.0 Ave Tetrahydrofuran 0.0614 0.0602 0.0100 51.0 50.0 1.9 50.0 Ave Chloroform 0.8007 0.7678 0.0100 52.1 50.0 4.3 20.0 Ave 1,1,1-Trichloroethane 0.8363 0.7459 0.0100 56.1 50.0 12.1 50.0 Ave Carbon tetrachloride 0.5702 0.4978 0.0100 57.3 50.0 14.5 50.0 Ave 1,1-Dichloropropene 0.7188 0.7224 0.0100 49.8 50.0 -0.5 50.0 Ave Benzene 1.253 1.296 0.0100 48.3 50.0 -3.3 50.0 Ave 1,2-Dichloroethane 0.3615 0.3458 0.0100 52.3 50.0 4.5 50.0 Ave Trichloroethene 0.3757 0.3521 0.0100 53.4 50.0 6.7 50.0 Ave 1,2-Dichloropropane 0.3748 0.3829 0.0100 48.9 50.0 -2.1 20.0 Ave Dibromomethane 0.1225 0.1248 0.0100 49.1 50.0 -1.8 50.0 Ave Bromodichloromethane 0.3756 0.3590 0.0100 52.3 50.0 4.6 50.0 Ave 2-Chloroethyl vinyl ether 0.1159 0.1198 0.0100 48.4 50.0 -3.2 50.0 Ave cis-1,3-Dichloropropene 0.3948 0.3838 0.0100 51.4 50.0 2.9 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1304 0.1313 0.0100 49.7 50.0 -0.7 50.0 Ave Toluene 0.8138 0.7916 0.0100 51.4 50.0 2.8 20.0 Ave trans-1,3-Dichloropropene 0.3074 0.2943 0.0100 52.2 50.0 4.4 50.0 Ave


### FORM VII 8260B 

## 01/03/2013 Page 173 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:06 11/14/2012 09:41 11/14/2012 12:54 CCV 500-173509/2 TestAmerica Chicago

Lab File ID:25C1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2272 0.2366 0.0100 48.0 50.0 -4.0 50.0 Ave Tetrachloroethene 0.5085 0.4729 0.0100 53.8 50.0 7.5 50.0 Ave 1,3-Dichloropropane 0.3531 0.3650 0.0100 48.4 50.0 -3.3 50.0 Ave 2-Hexanone 0.1051 0.1027 0.0100 51.2 50.0 2.3 50.0 Ave Dibromochloromethane 0.2777 0.2634 0.0100 52.7 50.0 5.4 50.0 Ave 1,2-Dibromoethane 0.1520 0.1542 0.0100 49.3 50.0 -1.4 50.0 Ave 1-Chlorohexane 0.7315 0.7247 0.0100 50.5 50.0 0.9 50.0 Ave Chlorobenzene 1.062 1.046 0.3000 50.8 50.0 1.6 50.0 Ave Ethylbenzene 0.6405 0.6127 0.0100 52.3 50.0 4.5 20.0 Ave 1,1,1,2-Tetrachloroethane 0.3577 0.3379 0.0100 52.9 50.0 5.8 50.0 Ave m&p-Xylene 1.549 1.453 0.0100 107 100 6.6 50.0 Ave o-Xylene 1.493 1.406 0.0100 53.1 50.0 6.2 50.0 Ave Styrene 1.104 1.067 0.0100 51.7 50.0 3.5 50.0 Ave Bromoform 0.1427 0.1393 0.1000 51.2 50.0 2.4 50.0 Ave Isopropylbenzene 4.518 4.186 0.0100 54.0 50.0 7.9 50.0 Ave Bromobenzene 0.8578 0.8368 0.0100 51.3 50.0 2.5 50.0 Ave 1,1,2,2-Tetrachloroethane 0.4009 0.4463 0.3000 44.9 50.0 -10.2 50.0 Ave N-Propylbenzene 5.379 4.979 0.0100 54.0 50.0 8.0 50.0 Ave 1,2,3-Trichloropropane 0.3321 0.3465 0.0100 47.9 50.0 -4.2 50.0 Ave 2-Chlorotoluene 2.880 2.750 0.0100 52.4 50.0 4.7 50.0 Ave 1,3,5-Trimethylbenzene 3.566 3.254 0.0100 54.8 50.0 9.6 50.0 Ave 4-Chlorotoluene 3.008 2.865 0.0100 52.5 50.0 5.0 50.0 Ave tert-Butylbenzene 3.183 2.966 0.0100 53.6 50.0 7.3 50.0 Ave 1,2,4-Trimethylbenzene 3.489 3.164 0.0100 55.1 50.0 10.3 50.0 Ave sec-Butylbenzene 5.007 4.606 0.0100 54.4 50.0 8.7 50.0 Ave 1,3-Dichlorobenzene 1.686 1.640 0.0100 51.4 50.0 2.8 50.0 Ave p-Isopropyltoluene 4.120 3.718 0.0100 55.4 50.0 10.8 50.0 Ave 1,4-Dichlorobenzene 1.654 1.612 0.0100 51.3 50.0 2.6 50.0 Ave n-Butylbenzene 4.016 3.626 0.0100 55.4 50.0 10.8 50.0 Ave 1,2-Dichlorobenzene 1.354 1.356 0.0100 49.9 50.0 -0.2 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0607 0.0611 0.0100 49.7 50.0 -0.7 50.0 Ave 1,2,4-Trichlorobenzene 1.041 0.9938 0.0100 52.4 50.0 4.7 50.0 Ave Hexachlorobutadiene 0.8913 0.8144 0.0100 54.7 50.0 9.4 50.0 Ave Naphthalene 1.216 1.233 0.0100 49.3 50.0 -1.3 50.0 Ave 1,2,3-Trichlorobenzene 0.7901 0.7736 0.0100 51.1 50.0 2.1 50.0 Ave Dibromofluoromethane 0.3816 0.4056 0.0100 47.0 50.0 -5.9 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2511 0.2620 0.0100 47.9 50.0 -4.2 50.0 Ave Toluene-d8 (Surr) 1.089 1.154 0.0100 47.2 50.0 -5.6 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4426 0.4616 0.0100 47.9 50.0 -4.1 50.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 174 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:06 11/14/2012 09:41 11/14/2012 12:54 CCV 500-173508/2 TestAmerica Chicago

Lab File ID:25C1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dichlorodifluoromethane 0.4729 0.6475 0.0100 36.5 50.0 -27.0 50.0 Ave Chloromethane 0.9148 1.001 0.1000 45.7 50.0 -8.7 50.0 Ave Vinyl chloride 0.7427 0.7756 0.0100 47.9 50.0 -4.2 20.0 Ave Bromomethane 0.1501 0.0100 52.8 50.0 5.6 50.0 Qua1 Chloroethane 0.3693 0.3396 0.0100 54.4 50.0 8.8 50.0 Ave Trichlorofluoromethane 0.9122 0.7698 0.0100 59.3 50.0 18.5 50.0 Ave Dichlorofluoromethane 1.034 0.9059 0.0100 57.1 50.0 14.1 50.0 Ave 1,1,2-Trichloro-1,2,2-triflu oroethane 0.5503 0.5272 0.0100 52.2 50.0 4.4 50.0 Ave Acrolein 0.0347 0.0531 0.0010 1306 2000 -34.7 50.0 Ave 1,1-Dichloroethene 0.4452 0.4396 0.0100 50.6 50.0 1.3 20.0 Ave Acetone 0.0619 0.0100 49.9 50.0 -0.2 50.0 Lin1 Carbon disulfide 1.432 1.673 0.0100 42.8 50.0 -14.4 50.0 Ave Acetonitrile 0.0349 0.0339 0.0010 412 400 3.0 50.0 Ave Methylene Chloride 0.3952 0.4144 0.0100 47.7 50.0 -4.6 50.0 Ave Methyl tert-butyl ether 0.5759 0.5971 0.0100 48.2 50.0 -3.5 50.0 Ave trans-1,2-Dichloroethene 0.4990 0.4898 0.0100 50.9 50.0 1.9 50.0 Ave Acrylonitrile 0.0990 0.1009 0.0010 392 400 -1.9 50.0 Ave 1,1-Dichloroethane 1.098 1.092 0.1000 50.3 50.0 0.6 50.0 Ave Vinyl acetate 0.6029 0.6134 0.0100 49.1 50.0 -1.7 50.0 Ave 2,2-Dichloropropane 0.7827 0.6724 0.0100 58.2 50.0 16.4 50.0 Ave cis-1,2-Dichloroethene 0.4882 0.4900 0.0100 49.8 50.0 -0.4 50.0 Ave 2-Butanone (MEK) 0.0910 0.0859 0.0100 53.0 50.0 6.0 50.0 Ave Propionitrile 0.0241 0.0229 0.0010 421 400 5.3 50.0 Ave Bromochloromethane 0.1806 0.1774 0.0100 50.9 50.0 1.8 50.0 Ave Tetrahydrofuran 0.0614 0.0602 0.0100 51.0 50.0 1.9 50.0 Ave Chloroform 0.8007 0.7678 0.0100 52.1 50.0 4.3 20.0 Ave 1,1,1-Trichloroethane 0.8363 0.7459 0.0100 56.1 50.0 12.1 50.0 Ave Carbon tetrachloride 0.5702 0.4978 0.0100 57.3 50.0 14.5 50.0 Ave 1,1-Dichloropropene 0.7188 0.7224 0.0100 49.8 50.0 -0.5 50.0 Ave Benzene 1.253 1.296 0.0100 48.3 50.0 -3.3 50.0 Ave 1,2-Dichloroethane 0.3615 0.3458 0.0100 52.3 50.0 4.5 50.0 Ave Trichloroethene 0.3757 0.3521 0.0100 53.4 50.0 6.7 50.0 Ave 1,2-Dichloropropane 0.3748 0.3829 0.0100 48.9 50.0 -2.1 20.0 Ave Dibromomethane 0.1225 0.1248 0.0100 49.1 50.0 -1.8 50.0 Ave Bromodichloromethane 0.3756 0.3590 0.0100 52.3 50.0 4.6 50.0 Ave 2-Chloroethyl vinyl ether 0.1159 0.1198 0.0100 48.4 50.0 -3.2 50.0 Ave cis-1,3-Dichloropropene 0.3948 0.3838 0.0100 51.4 50.0 2.9 50.0 Ave 4-Methyl-2-pentanone (MIBK) 0.1304 0.1313 0.0100 49.7 50.0 -0.7 50.0 Ave Toluene 0.8138 0.7916 0.0100 51.4 50.0 2.8 20.0 Ave trans-1,3-Dichloropropene 0.3074 0.2943 0.0100 52.2 50.0 4.4 50.0 Ave


### FORM VII 8260B 

## 01/03/2013 Page 175 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:06 11/14/2012 09:41 11/14/2012 12:54 CCV 500-173508/2 TestAmerica Chicago

Lab File ID:25C1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

1,1,2-Trichloroethane 0.2272 0.2366 0.0100 48.0 50.0 -4.0 50.0 Ave Tetrachloroethene 0.5085 0.4729 0.0100 53.8 50.0 7.5 50.0 Ave 1,3-Dichloropropane 0.3531 0.3650 0.0100 48.4 50.0 -3.3 50.0 Ave 2-Hexanone 0.1051 0.1027 0.0100 51.2 50.0 2.3 50.0 Ave Dibromochloromethane 0.2777 0.2634 0.0100 52.7 50.0 5.4 50.0 Ave 1,2-Dibromoethane 0.1520 0.1542 0.0100 49.3 50.0 -1.4 50.0 Ave 1-Chlorohexane 0.7315 0.7247 0.0100 50.5 50.0 0.9 50.0 Ave Chlorobenzene 1.062 1.046 0.3000 50.8 50.0 1.6 50.0 Ave Ethylbenzene 0.6405 0.6127 0.0100 52.3 50.0 4.5 20.0 Ave 1,1,1,2-Tetrachloroethane 0.3577 0.3379 0.0100 52.9 50.0 5.8 50.0 Ave m&p-Xylene 1.549 1.453 0.0100 107 100 6.6 50.0 Ave o-Xylene 1.493 1.406 0.0100 53.1 50.0 6.2 50.0 Ave Styrene 1.104 1.067 0.0100 51.7 50.0 3.5 50.0 Ave Bromoform 0.1427 0.1393 0.1000 51.2 50.0 2.4 50.0 Ave Isopropylbenzene 4.518 4.186 0.0100 54.0 50.0 7.9 50.0 Ave Bromobenzene 0.8578 0.8368 0.0100 51.3 50.0 2.5 50.0 Ave 1,1,2,2-Tetrachloroethane 0.4009 0.4463 0.3000 44.9 50.0 -10.2 50.0 Ave N-Propylbenzene 5.379 4.979 0.0100 54.0 50.0 8.0 50.0 Ave 1,2,3-Trichloropropane 0.3321 0.3465 0.0100 47.9 50.0 -4.2 50.0 Ave 2-Chlorotoluene 2.880 2.750 0.0100 52.4 50.0 4.7 50.0 Ave 1,3,5-Trimethylbenzene 3.566 3.254 0.0100 54.8 50.0 9.6 50.0 Ave 4-Chlorotoluene 3.008 2.865 0.0100 52.5 50.0 5.0 50.0 Ave tert-Butylbenzene 3.183 2.966 0.0100 53.6 50.0 7.3 50.0 Ave 1,2,4-Trimethylbenzene 3.489 3.164 0.0100 55.1 50.0 10.3 50.0 Ave sec-Butylbenzene 5.007 4.606 0.0100 54.4 50.0 8.7 50.0 Ave 1,3-Dichlorobenzene 1.686 1.640 0.0100 51.4 50.0 2.8 50.0 Ave p-Isopropyltoluene 4.120 3.718 0.0100 55.4 50.0 10.8 50.0 Ave 1,4-Dichlorobenzene 1.654 1.612 0.0100 51.3 50.0 2.6 50.0 Ave n-Butylbenzene 4.016 3.626 0.0100 55.4 50.0 10.8 50.0 Ave 1,2-Dichlorobenzene 1.354 1.356 0.0100 49.9 50.0 -0.2 50.0 Ave 1,2-Dibromo-3-Chloropropane 0.0607 0.0611 0.0100 49.7 50.0 -0.7 50.0 Ave 1,2,4-Trichlorobenzene 1.041 0.9938 0.0100 52.4 50.0 4.7 50.0 Ave Hexachlorobutadiene 0.8913 0.8144 0.0100 54.7 50.0 9.4 50.0 Ave Naphthalene 1.216 1.233 0.0100 49.3 50.0 -1.3 50.0 Ave 1,2,3-Trichlorobenzene 0.7901 0.7736 0.0100 51.1 50.0 2.1 50.0 Ave Dibromofluoromethane 0.3816 0.4056 0.0100 47.0 50.0 -5.9 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2511 0.2620 0.0100 47.9 50.0 -4.2 50.0 Ave Toluene-d8 (Surr) 1.089 1.154 0.0100 47.2 50.0 -5.6 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4426 0.4616 0.0100 47.9 50.0 -4.1 50.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 176 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:30 11/14/2012 09:41 11/14/2012 12:54 CCV 500-173509/3 TestAmerica Chicago

Lab File ID:25D1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.3919 0.4056 0.0100 48.3 50.0 -3.4 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2685 0.2620 0.0100 51.2 50.0 2.5 50.0 Ave Toluene-d8 (Surr) 1.117 1.154 0.0100 48.4 50.0 -3.2 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4672 0.4616 0.0100 50.6 50.0 1.2 50.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 177 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:30 11/14/2012 09:41 11/14/2012 12:54 CCV 500-173508/3 TestAmerica Chicago

Lab File ID:25D1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Dibromofluoromethane 0.3919 0.4056 0.0100 48.3 50.0 -3.4 50.0 Ave 1,2-Dichloroethane-d4 (Surr) 0.2685 0.2620 0.0100 51.2 50.0 2.5 50.0 Ave Toluene-d8 (Surr) 1.117 1.154 0.0100 48.4 50.0 -3.2 50.0 Ave 4-Bromofluorobenzene (Surr) 0.4672 0.4616 0.0100 50.6 50.0 1.2 50.0 Ave



### FORM VII 8260B 

## 01/03/2013 Page 178 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:30 11/14/2012 13:19 11/14/2012 16:08 CCV 500-173509/3 TestAmerica Chicago

Lab File ID:25D1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.8362 0.8678 0.0100 48.2 50.0 -3.6 50.0 Ave Ethyl ether 0.3065 0.3493 0.0100 43.9 50.0 -12.3 50.0 Ave Iodomethane 0.4434 0.0100 102 100 1.8 50.0 Qua1 3-Chloropropene 0.2460 0.2207 0.0100 112 100 11.5 50.0 Ave Methyl acetate 0.2757 0.2344 0.0100 58.8 50.0 17.7 50.0 Ave Hexane 1.247 1.324 0.0100 47.1 50.0 -5.8 50.0 Ave Isopropyl ether 1.840 1.845 0.0100 49.9 50.0 -0.3 50.0 Ave 2-Chloro-1,3-butadiene 1.252 1.221 0.0100 51.3 50.0 2.6 50.0 Ave Ethyl acetate 0.2034 0.1818 0.0100 560 500 11.9 50.0 Ave Methacrylonitrile 0.1554 0.1326 0.0100 117 100 17.2 50.0 Ave Cyclohexane 1.444 1.508 0.0100 47.9 50.0 -4.2 50.0 Ave 2,2,4-Trimethylpentane 2.437 2.411 0.0100 50.5 50.0 1.1 50.0 Ave Isobutyl alcohol 0.0108 0.0090 0.0010 4794 4000 19.9 50.0 Ave Heptane 1.035 0.9508 0.0100 54.5 50.0 8.9 50.0 Ave n-Butyl alcohol 0.0032 0.0010 4486 4000 12.1 50.0 Lin1 Methylcyclohexane 0.6666 0.6690 0.0100 49.8 50.0 -0.4 50.0 Ave Methyl methacrylate 0.1573 0.1324 0.0100 119 100 18.8 50.0 Ave 2-Nitropropane 0.0554 0.0447 0.0100 4957 4000 23.9 50.0 Ave Ethyl methacrylate 0.2201 0.0100 102 100 2.0 50.0 Lin1 Cyclohexanone 0.0519 0.0100 9878 4000 147.0* 50.0 Qua1 trans-1,4-Dichloro-2-butene 0.0685 0.0100 115 100 14.9 50.0 Qua1 Pentachloroethane 0.2646 0.2187 0.0100 121 100 21.0 50.0 Ave 1,3,5-Trichlorobenzene 1.360 1.274 0.0100 53.4 50.0 6.8 50.0 Ave 2-Methylnaphthalene 0.6356 0.0100 45.2 50.0 -9.5 50.0 Qua1



### FORM VII 8260B 

## 01/03/2013 Page 179 of 383

### FORM VII

Lab Name: Job No.: SDG No.:

Instrument ID: Calibration Date: Calib Start Date: Lab Sample ID:

Calib End Date: GC Column: ID: GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25 12/19/2012 23:30 11/14/2012 13:19 11/14/2012 16:08 CCV 500-173508/3 TestAmerica Chicago

Lab File ID:25D1219p.D Heated Purge: (Y/N) N Conc. Units:ug/L

ANALYTE CURVE CALC SPIKE %D MAX TYPE AMOUNTAMOUNT %D AVE RRF RRF MIN RRF

Butadiene 0.8362 0.8678 0.0100 48.2 50.0 -3.6 50.0 Ave Ethyl ether 0.3065 0.3493 0.0100 43.9 50.0 -12.3 50.0 Ave Iodomethane 0.4434 0.0100 102 100 1.8 50.0 Qua1 3-Chloropropene 0.2460 0.2207 0.0100 112 100 11.5 50.0 Ave Methyl acetate 0.2757 0.2344 0.0100 58.8 50.0 17.7 50.0 Ave Hexane 1.247 1.324 0.0100 47.1 50.0 -5.8 50.0 Ave Isopropyl ether 1.840 1.845 0.0100 49.9 50.0 -0.3 50.0 Ave 2-Chloro-1,3-butadiene 1.252 1.221 0.0100 51.3 50.0 2.6 50.0 Ave Ethyl acetate 0.2034 0.1818 0.0100 560 500 11.9 50.0 Ave Methacrylonitrile 0.1554 0.1326 0.0100 117 100 17.2 50.0 Ave Cyclohexane 1.444 1.508 0.0100 47.9 50.0 -4.2 50.0 Ave 2,2,4-Trimethylpentane 2.437 2.411 0.0100 50.5 50.0 1.1 50.0 Ave Isobutyl alcohol 0.0108 0.0090 0.0010 4794 4000 19.9 50.0 Ave Heptane 1.035 0.9508 0.0100 54.5 50.0 8.9 50.0 Ave n-Butyl alcohol 0.0032 0.0010 4486 4000 12.1 50.0 Lin1 Methylcyclohexane 0.6666 0.6690 0.0100 49.8 50.0 -0.4 50.0 Ave Methyl methacrylate 0.1573 0.1324 0.0100 119 100 18.8 50.0 Ave 2-Nitropropane 0.0554 0.0447 0.0100 4957 4000 23.9 50.0 Ave Ethyl methacrylate 0.2201 0.0100 102 100 2.0 50.0 Lin1 Cyclohexanone 0.0519 0.0100 9878 4000 147.0* 50.0 Qua1 trans-1,4-Dichloro-2-butene 0.0685 0.0100 115 100 14.9 50.0 Qua1 Pentachloroethane 0.2646 0.2187 0.0100 121 100 21.0 50.0 Ave 1,3,5-Trichlorobenzene 1.360 1.274 0.0100 53.4 50.0 6.8 50.0 Ave 2-Methylnaphthalene 0.6356 0.0100 45.2 50.0 -9.5 50.0 Qua1



### FORM VII 8260B 

## 01/03/2013 Page 180 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53315-1
Lab Sample ID:MB 500-173225/4 Matrix: 16M1218.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/18/2012 08:30

ID: DB624
Analysis Batch No.: 173225 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone <5.00 5.00 1.81 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 106 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 113 75-122 2037-26-5 Toluene-d8 (Surr) 104 70-122 460-00-4 4-Bromofluorobenzene (Surr) 106 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 181 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53315-1
Lab Sample ID:MB 500-173508/6 Matrix: 25M1219p.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL) Date Analyzed:12/20/2012 00:43

ID:
Analysis Batch No.: 173508 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 101 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 75-120 2037-26-5 Toluene-d8 (Surr) 94 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 182 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53315-1
Lab Sample ID:MB 500-173509/6 Matrix: 25M1219p.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Medium 5(mL) 5 (mL) 5(mL) Date Analyzed:12/20/2012 00:43

ID:
Analysis Batch No.: 173509 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.30 67-64-1 Acetone <5.00 5.00 1.47 78-93-3 2-Butanone (MEK) <5.00


### %REC CAS NO. LIMITS Q SURROGATE 101 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 75-120 2037-26-5 Toluene-d8 (Surr) 94 75-120 460-00-4 4-Bromofluorobenzene (Surr) 96 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 183 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53315-1
Lab Sample ID:LCS 500-173225/5 Matrix: 16S1218.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/18/2012 08:53

ID: DB624
Analysis Batch No.: 173225 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 2.16 67-64-1 Acetone 45.56 5.00 1.81 78-93-3 2-Butanone (MEK) 52.85


### %REC CAS NO. LIMITS Q SURROGATE 104 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 111 75-122 2037-26-5 Toluene-d8 (Surr) 103 70-122 460-00-4 4-Bromofluorobenzene (Surr) 105 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 184 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53315-1
Lab Sample ID:LCS 500-173508/4 Matrix: 25S1219p.D Lab File ID: Date Collected: 8260B Analysis Method: Water TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med) Low 5(mL) Date Analyzed:12/19/2012 23:54

ID:
Analysis Batch No.: 173508 ug/L Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.29 67-64-1 Acetone 52.35 5.00 1.47 78-93-3 2-Butanone (MEK) 53.39


### %REC CAS NO. LIMITS Q SURROGATE 102 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 99 75-120 460-00-4 4-Bromofluorobenzene (Surr) 98 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 185 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG No.: 500-53315-1
Lab Sample ID:LCS 500-173509/4 Matrix: 25S1219p.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol: 1
Level: (low/med)Medium 5(mL) 5 (mL) 5(mL) Date Analyzed:12/19/2012 23:54

ID:
Analysis Batch No.: 173509 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL5.00 1.30 67-64-1 Acetone 52.35 5.00 1.47 78-93-3 2-Butanone (MEK) 53.39


### %REC CAS NO. LIMITS Q SURROGATE 102 75-125 17060-07-0 1,2-Dichloroethane-d4 (Surr) 97 75-120 2037-26-5 Toluene-d8 (Surr) 99 75-120 460-00-4 4-Bromofluorobenzene (Surr) 98 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 186 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC DISCRETE 4 MS SDG No.: 500-53315-1
Lab Sample ID:500-53315-3 MS Matrix: 53315-03s.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/14/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

71.1 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/18/2012 09:54

ID: DB624
Analysis Batch No.: 173225 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL17.3 7.46 67-64-1 Acetone 7120 17.3 6.25 78-93-3 2-Butanone (MEK) 329.3


### %REC CAS NO. LIMITS Q SURROGATE 117 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 95 75-122 2037-26-5 Toluene-d8 (Surr) 85 70-122 460-00-4 4-Bromofluorobenzene (Surr) 118 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 187 of 383

### FORM I Form 1 GC/MS VOA ORGANICS ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.:

FC DISCRETE 4 MSD SDG No.: 500-53315-1
Lab Sample ID:500-53315-3 MSD Matrix: 53315-03t.D Lab File ID: Date Collected: 8260B Analysis Method: Solid TestAmerica Chicago

12/14/2012 14:45 Sample wt/vol:

% Moisture: GC Column: Soil Extract Vol.: Dilution Factor: Soil Aliquot Vol:

71.1 1
Level: (low/med) Low 5(g)
0.2(mm) Date Analyzed:12/18/2012 10:17

ID: DB624
Analysis Batch No.: 173225 ug/Kg Units:
CAS NO. COMPOUND NAME RESULT Q MDL RL17.3 7.46 67-64-1 Acetone 7629 17.3 6.25 78-93-3 2-Butanone (MEK) 303.4


### %REC CAS NO. LIMITS Q SURROGATE 119 70-134 17060-07-0 1,2-Dichloroethane-d4 (Surr) 96 75-122 2037-26-5 Toluene-d8 (Surr) 84 70-122 460-00-4 4-Bromofluorobenzene (Surr) 116 75-120 1868-53-7 Dibromofluoromethane



### FORM I 8260B 

## 01/03/2013 Page 188 of 383

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53315-1

CMS16 170196 Start Date: End Date:11/19/2012 17:14 11/19/2012 11:14

BFB 500-170196/5 DB624 0.2(mm) 1 11/19/2012 11:14 16B1119c.D STD1 500-170196/6 IC DB624 0.2(mm) 1 11/19/2012 12:14 16I1119A.D STD2 500-170196/7 IC DB624 0.2(mm) 1 11/19/2012 12:37 16I1119B.D STD3 500-170196/8 ICIS DB624 0.2(mm) 1 11/19/2012 13:00 16I1119C.D STD4 500-170196/9 IC DB624 0.2(mm) 1 11/19/2012 13:23 16I1119D.D STD5 500-170196/10 IC DB624 0.2(mm) 1 11/19/2012 13:46 16I1119E.D STD6 500-170196/11 IC DB624 0.2(mm) 1 11/19/2012 14:09 16I1119F.D STD1AP 500-170196/12 IC DB624 0.2(mm) 1 11/19/2012 14:32 STD2AP 500-170196/13 IC DB624 0.2(mm) 1 11/19/2012 14:55 STD3AP 500-170196/14 IC DB624 0.2(mm) 1 11/19/2012 15:18 STD4AP 500-170196/15 IC DB624 0.2(mm) 1 11/19/2012 15:42 STD5AP 500-170196/16 IC DB624 0.2(mm) 1 11/19/2012 16:05 STD6AP 500-170196/17 IC DB624 0.2(mm) 1 11/19/2012 16:28 ICV 500-170196/19 DB624 0.2(mm) 1 11/19/2012 17:14 16S1119.D



### 8260B 

## 01/03/2013 Page 189 of 383

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53315-1

CMS16 173225 Start Date: End Date:12/18/2012 10:40 12/18/2012 07:09

BFB 500-173225/1 DB624 0.2(mm) 1 12/18/2012 07:09 16B1218.D CCV 500-173225/2 DB624 0.2(mm) 1 12/18/2012 07:43 16C1218.D CCV 500-173225/3 DB624 0.2(mm) 1 12/18/2012 08:07 16D1218.D MB 500-173225/4 DB624 0.2(mm) 1 12/18/2012 08:30 16M1218.D LCS 500-173225/5 DB624 0.2(mm) 1 12/18/2012 08:53 16S1218.D 500-53315-3 FC DISCRETE 4 DB624 0.2(mm) 1 12/18/2012 09:30 53315-03.D 500-53315-3 MS FC DISCRETE 4 MS DB624 0.2(mm) 1 12/18/2012 09:54 53315-03s.D 500-53315-3 MSD FC DISCRETE 4 MSD DB624 0.2(mm) 1 12/18/2012 10:17 53315-03t.D 500-53315-4 FC D DISCRETE 4 DB624 0.2(mm) 1 12/18/2012 10:40 53315-04.D



### 8260B 

## 01/03/2013 Page 190 of 383

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53315-1

CMS25 169636 Start Date: End Date:11/14/2012 16:57 11/14/2012 09:17

BFB 500-169636/1 1 11/14/2012 09:17 25B1114.D STD1 500-169636/2 IC 1 11/14/2012 09:41 25I1114a.D STD2 500-169636/3 IC 1 11/14/2012 10:05 25I1114b.D STD3 500-169636/4 IC 1 11/14/2012 10:29 25I1114c.D STD4 500-169636/5 IC 1 11/14/2012 10:53 25I1114d.D STD5 500-169636/6 IC 1 11/14/2012 11:18 25I1114e.D STD6 500-169636/7 ICIS 1 11/14/2012 11:42 25I1114f.D STD7 500-169636/8 IC 1 11/14/2012 12:06 25I1114g.D STD8 500-169636/9 IC 1 11/14/2012 12:30 25I1114h.D STD9 500-169636/10 IC 1 11/14/2012 12:54 25I1114i.D STD2AP 500-169636/11 IC 1 11/14/2012 13:19 STD3AP 500-169636/12 IC 1 11/14/2012 13:43 STD4AP 500-169636/13 IC 1 11/14/2012 14:07 STD5AP 500-169636/14 IC 1 11/14/2012 14:31 STD6AP 500-169636/15 IC 1 11/14/2012 14:55 STD7AP 500-169636/16 IC 1 11/14/2012 15:20 STD8AP 500-169636/17 IC 1 11/14/2012 15:44 STD9AP 500-169636/18 IC 1 11/14/2012 16:08 ICV 500-169636/20 1 11/14/2012 16:57 25S1114.D



### 8260B 

## 01/03/2013 Page 191 of 383

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53315-1

CMS25 169637 Start Date: End Date:11/14/2012 16:57 11/14/2012 09:17

BFB 500-169637/1 1 11/14/2012 09:17 25B1114.D STD1 500-169637/2 IC 1 11/14/2012 09:41 25I1114a.D STD2 500-169637/3 IC 1 11/14/2012 10:05 25I1114b.D STD3 500-169637/4 IC 1 11/14/2012 10:29 25I1114c.D STD4 500-169637/5 IC 1 11/14/2012 10:53 25I1114d.D STD5 500-169637/6 IC 1 11/14/2012 11:18 25I1114e.D STD6 500-169637/7 ICIS 1 11/14/2012 11:42 25I1114f.D STD7 500-169637/8 IC 1 11/14/2012 12:06 25I1114g.D STD8 500-169637/9 IC 1 11/14/2012 12:30 25I1114h.D STD9 500-169637/10 IC 1 11/14/2012 12:54 25I1114i.D STD2AP 500-169637/11 IC 1 11/14/2012 13:19 STD3AP 500-169637/12 IC 1 11/14/2012 13:43 STD4AP 500-169637/13 IC 1 11/14/2012 14:07 STD5AP 500-169637/14 IC 1 11/14/2012 14:31 STD6AP 500-169637/15 IC 1 11/14/2012 14:55 STD7AP 500-169637/16 IC 1 11/14/2012 15:20 STD8AP 500-169637/17 IC 1 11/14/2012 15:44 STD9AP 500-169637/18 IC 1 11/14/2012 16:08 ICV 500-169637/20 1 11/14/2012 16:57 25S1114.D



### 8260B 

## 01/03/2013 Page 192 of 383

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53315-1

CMS25 173508 Start Date: End Date:12/20/2012 08:59 12/19/2012 22:40

BFB 500-173508/1 1 12/19/2012 22:40 25B1219p.D CCV 500-173508/2 1 12/19/2012 23:06 25C1219p.D CCV 500-173508/3 1 12/19/2012 23:30 25D1219p.D LCS 500-173508/4 1 12/19/2012 23:54 25S1219p.D MB 500-173508/6 1 12/20/2012 00:43 25M1219p.D 500-53315-5 TRIP BLANK 1 12/20/2012 01:08 53315-05.D 500-53315-6 FC EB 4 1 12/20/2012 01:49 53315-06.D ZZZZZ 1 12/20/2012 04:42 ZZZZZ 1 12/20/2012 05:19 ZZZZZ 1 12/20/2012 05:43 ZZZZZ 1 12/20/2012 06:07 ZZZZZ 1 12/20/2012 06:32 ZZZZZ 1 12/20/2012 06:56 ZZZZZ 1 12/20/2012 07:21 ZZZZZ 1 12/20/2012 07:45 ZZZZZ 1 12/20/2012 08:10 ZZZZZ 1 12/20/2012 08:34 ZZZZZ 1 12/20/2012 08:59



### 8260B 

## 01/03/2013 Page 193 of 383

### Lab Name: Job No.: SDG No.: Instrument ID: Analysis Batch Number: GC/MS VOA ANALYSIS RUN LOG

DILUTION FACTOR COLUMN ID DATE ANALYZED LAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID 

### TestAmerica Chicago 500-53315-1

CMS25 173509 Start Date: End Date:12/20/2012 04:18 12/19/2012 22:40

BFB 500-173509/1 1 12/19/2012 22:40 25B1219p.D CCV 500-173509/2 1 12/19/2012 23:06 25C1219p.D CCV 500-173509/3 1 12/19/2012 23:30 25D1219p.D LCS 500-173509/4 1 12/19/2012 23:54 25S1219p.D MB 500-173509/6 1 12/20/2012 00:43 25M1219p.D 500-53315-3 DL FC DISCRETE 4 DL 50 12/20/2012 02:16 53315-03.D 500-53315-4 DL FC D DISCRETE 4 DL 50 12/20/2012 02:40 53315-04.D ZZZZZ 50 12/20/2012 03:05 ZZZZZ 50 12/20/2012 03:29 ZZZZZ 50 12/20/2012 03:54 ZZZZZ 50 12/20/2012 04:18



### 8260B 

## 01/03/2013 Page 194 of 383

### Lab Name: Job No.: SDG No.: GC/MS VOA BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Werner, Brian D 12/18/12 07:45 173238 Batch Method: TestAmerica Chicago

5030B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount AnalysisComment FC DISCRETE 4 5 g 5 mL meoh 500-53315-A-3 5030B, 8260B T FC D DISCRETE 4 5 g 5 mL meoh 500-53315-A-4 5030B, 8260B T
Batch Notes Balance ID C-0133 Methanol Lot Number DH247 Pipette ID C-2207
Basis Basis Description T Total/NA



### Page 1 of 1 8260B 

## 01/03/2013 Page 195 of 383

# 01/03/2013 Page 196 of 383

# 01/03/2013 Page 197 of 383

# METALS

01/03/2013 Page 198 of 383

### COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID METALS

Project:John Deere Des Moines Works (JDDMW) SDG No.: 500-53315-1 TestAmerica Chicago

500-53315-1 FC COMPOSITE 4 500-53315-2 FC D COMPOSITE 4 500-53315-6 FC EB 4

Comments:



## 01/03/2013 Page 199 of 383

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10 500-53315-1 FC COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: DRY 

### METALS

TestAmerica Chicago

% Solids: 25.9

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 346 mg/Kg 3.70 0.441 1 6010B 7440-50-8 Copper 834 mg/Kg 3.70 1.00 1 6010B 7440-47-3 Chromium 14400 mg/Kg V 3.70 0.618 1 6010B 7440-02-0 Nickel 89.8 mg/Kg V 3.70 0.811 1 6010B 7439-92-1 Lead 209 mg/Kg B V 1.85 0.637 1 6010B 7440-62-2 Vanadium 241 mg/Kg V 1.85 0.281 1 6010B 7440-66-6 Zinc 481 mg/Kg V 7.41 2.54 1 6010B 7439-97-6 Mercury 0.543 mg/Kg 0.0595 0.0227 1 7471A



### FORM IA-IN 

## 01/03/2013 Page 200 of 383

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10 500-53315-1 FC COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: WET 

### METALS - TCLP

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 0.0194 J mg/L 0.500 0.0100 1 6010B 7440-50-8 Copper 0.0487 mg/L 0.0250 0.0100 1 6010B 7440-47-3 Chromium <0.0250 mg/L 0.0250 0.0100 1 6010B 7440-02-0 Nickel 0.0549 mg/L 0.0250 0.0100 1 6010B 7439-92-1 Lead <0.0500 mg/L 0.0500 0.00500 1 6010B 7440-62-2 Vanadium <0.0250 mg/L 0.0250 0.00500 1 6010B 7440-66-6 Zinc <0.100 mg/L 0.100 0.0200 1 6010B 7439-97-6 Mercury <0.000200 mg/L 0.000200 0.000020 0 1 7470A



### FORM IA-IN 

## 01/03/2013 Page 201 of 383

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10 500-53315-1 FC D COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: DRY 

### METALS

TestAmerica Chicago

% Solids: 26.3

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 326 mg/Kg 3.46 0.411 1 6010B 7440-50-8 Copper 784 mg/Kg 3.46 0.937 1 6010B 7440-47-3 Chromium 13200 mg/Kg 3.46 0.577 1 6010B 7440-02-0 Nickel 86.4 mg/Kg 3.46 0.757 1 6010B 7439-92-1 Lead 188 mg/Kg B 1.73 0.595 1 6010B 7440-62-2 Vanadium 221 mg/Kg 1.73 0.262 1 6010B 7440-66-6 Zinc 451 mg/Kg 6.92 2.37 1 6010B 7439-97-6 Mercury 0.248 mg/Kg 0.0628 0.0239 1 7471A



### FORM IA-IN 

## 01/03/2013 Page 202 of 383

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10 500-53315-1 FC D COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: WET 

### METALS - TCLP

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium <0.500 mg/L 0.500 0.0100 1 6010B 7440-50-8 Copper 0.0483 mg/L 0.0250 0.0100 1 6010B 7440-47-3 Chromium 0.0120 J mg/L 0.0250 0.0100 1 6010B 7440-02-0 Nickel 0.0582 mg/L 0.0250 0.0100 1 6010B 7439-92-1 Lead <0.0500 mg/L 0.0500 0.00500 1 6010B 7440-62-2 Vanadium <0.0250 mg/L 0.0250 0.00500 1 6010B 7440-66-6 Zinc <0.100 mg/L 0.100 0.0200 1 6010B 7439-97-6 Mercury <0.000200 mg/L 0.000200 0.000020 0 1 7470A



### FORM IA-IN 

## 01/03/2013 Page 203 of 383

### 1A-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-6

Date Received: 12/15/2012 09:10 500-53315-1 FC EB 4

Water 12/14/2012 14:30 Date Sampled: Reporting Basis: WET 

### METALS

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
7440-39-3 Barium 0.000580 J mg/L B 0.0100 0.000440 1 6010B 7440-50-8 Copper 0.00303 J mg/L 0.0100 0.00106 1 6010B 7440-47-3 Chromium 0.00312 J mg/L B 0.0100 0.000960 1 6010B 7440-02-0 Nickel <0.0100 mg/L 0.0100 0.00190 1 6010B 7439-92-1 Lead 0.00214 J mg/L B 0.00500 0.00158 1 6010B 7440-62-2 Vanadium <0.00500 mg/L 0.00500 0.000620 1 6010B 7440-66-6 Zinc 0.00724 J mg/L 0.0200 0.00472 1 6010B 7439-97-6 Mercury 0.000102 J mg/L 0.000200 0.000071 0 1 7470A



### FORM IA-IN 

## 01/03/2013 Page 204 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173224/10 12/17/2012 20:16
Found C True %R 

### CCV 500-173224/15 12/17/2012 20:51 CCV 500-173224/27 12/17/2012 22:08
Found Found C C True %R True %R 

### Barium 

### 0.4024 0.5143 0.5097 0.400 0.500 0.500 101 103 102 Chromium 

### 0.4131 0.5169 0.5182 0.400 0.500 0.500 103 103 104 Copper 

### 0.4072 0.5205 0.5167 0.400 0.500 0.500 102 104 103 Lead 

### 0.4153 0.5177 0.5172 0.400 0.500 0.500 104 104 103 Nickel 

### 0.4084 0.5133 0.5128 0.400 0.500 0.500 102 103 103 Vanadium 

### 4.073 5.138 5.132 4.00 5.00 5.00 102 103 103 Zinc 

### 0.4113 0.5095 0.5127 0.400 0.500 0.500 103 102 103

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 205 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173224/39 12/17/2012 23:25
Found C True %R Found Found C C True %R True %R 

### Barium 

### 0.5136 0.500103 Chromium 

### 0.5134 0.500103 Copper 

### 0.5217 0.500104 Lead 

### 0.5147 0.500103 Nickel 

### 0.5122 0.500102 Vanadium 

### 5.141 5.00103 Zinc 

### 0.5079 0.500102

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 206 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173517/10 12/19/2012 09:45
Found C True %R 

### CCV 500-173517/39 12/19/2012 13:02 CCV 500-173517/51 12/19/2012 14:26
Found Found C C True %R True %R 

### Barium 

### 0.4009 0.5058 0.4985 0.400 0.500 0.500 100 101 100 Chromium 

### 0.4092 0.5060 0.5069 0.400 0.500 0.500 102 101 101 Copper 

### 0.4066 0.5141 0.5071 0.400 0.500 0.500 102 103 101 Lead 

### 0.4102 0.5023 0.5049 0.400 0.500 0.500 103 100 101 Nickel 

### 0.4046 0.5009 0.5041 0.400 0.500 0.500 101 100 101 Vanadium 

### 4.040 5.029 5.027 4.00 5.00 5.00 101 101 101 Zinc 

### 0.4049 0.4922 0.5013 0.400 0.500 0.500 101 98 100

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 207 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173517/63 12/19/2012 15:47
Found C True %R Found Found C C True %R True %R 

### Barium 

### 0.5064 0.500101 Chromium 

### 0.5161 0.500103 Copper 

### 0.5146 0.500103 Lead 

### 0.5134 0.500103 Nickel 

### 0.5121 0.500102 Vanadium 

### 5.116 5.00102 Zinc 

### 0.5102 0.500102

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 208 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte ICV 500-173518/10 12/19/2012 18:41
Found C True %R 

### CCV 500-173518/27 12/19/2012 20:32 CCV 500-173518/39 12/19/2012 21:57
Found Found C C True %R True %R 

### Barium 

### 0.4028 0.5103 0.5135 0.400 0.500 0.500 101 102 103 Chromium 

### 0.4072 0.5110 0.5092 0.400 0.500 0.500 102 102 102 Copper 

### 0.4055 0.5154 0.5149 0.400 0.500 0.500 101 103 103 Lead 

### 0.4072 0.5098 0.5055 0.400 0.500 0.500 102 102 101 Nickel 

### 0.4012 0.5034 0.5014 0.400 0.500 0.500 100 101 100 Vanadium 

### 4.032 5.081 5.067 4.00 5.00 5.00 101 102 101 Zinc 

### 0.4013 0.4996 0.4948 0.400 0.500 0.500 100 100 99

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 209 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1mg/L M12LICVIC_00001 M12LCCVIC_00001

Analyte CCV 500-173518/51 12/19/2012 23:21
Found C True %R Found Found C C True %R True %R 

### Barium 

### 0.5130 0.500103 Chromium 

### 0.5100 0.500102 Copper 

### 0.5146 0.500103 Lead 

### 0.5098 0.500102 Nickel 

### 0.5037 0.500101 Vanadium 

### 5.078 5.00102 Zinc 

### 0.4979 0.500100

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 210 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173328/8 12/18/2012 12:59
Found C True %R 

### CCV 500-173328/12 12/18/2012 13:06 CCV 500-173328/24 12/18/2012 13:29
Found Found C C True %R True %R 

### Mercury 

### 2.050 1.030 1.110 2.00 1.00 1.00 103 103 111

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 211 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte CCV 500-173328/36 12/18/2012 13:52
Found C True %R 

### CCV 500-173328/42 12/18/2012 14:03
Found Found C C True %R True %R 

### Mercury 

### 1.070 0.8470 1.00 1.00 107 85

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 212 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173280/7 12/18/2012 09:03
Found C True %R 

### CCV 500-173280/19 12/18/2012 09:26 CCV 500-173280/31 12/18/2012 09:51
Found Found C C True %R True %R 

### Mercury 

### 2.167 0.9179 0.9846 2.00 1.00 1.00 108 92 98

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 213 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte CCV 500-173280/38 12/18/2012 10:19
Found C True %R Found Found C C True %R True %R 

### Mercury 

### 1.063 1.00106

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 214 of 383

### 2A-IN

Lab Name: Job No.: SDG No.: Concentration Units: CALIBRATION VERIFICATIONS METALS

ICV Source: CCV Source:TestAmerica Chicago 500-53315-1ug/L M11FSTKHG_00001 M11FSTKHG_00001

Analyte ICV 500-173438/7 12/19/2012 10:02
Found C True %R 

### CCV 500-173438/19 12/19/2012 10:26 CCV 500-173438/28 12/19/2012 10:42
Found Found C C True %R True %R 

### Mercury 

### 1.885 1.056 1.092 2.00 1.00 1.00 94 106 109 J J J

FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results. Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 215 of 383

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53315-1 CRQL CHECK STANDARD METALS

Method:6010B Instrument ID:ICP5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173224/12

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units: mg/L

50-150 Barium 0.0200 0.02010 101 50-150 Copper 0.0200 0.02010 101 50-150 Chromium 0.0200 0.02702 135 50-150 Nickel 0.0200 0.02103 105 50-150 Lead 0.0100 0.01151 115 50-150 Vanadium 0.0100 0.01001 100 50-150 Zinc 0.0400 0.04154 104 Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173517/12

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units: mg/L

50-150 Barium 0.0200 0.01990 100 50-150 Copper 0.0200 0.01955 98 50-150 Chromium 0.0200 0.02070 104 50-150 Nickel 0.0200 0.02010 101 50-150 Lead 0.0100 0.01229 123 50-150 Vanadium 0.0100 0.01023 102 50-150 Zinc 0.0400 0.04138 103 Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173517/75

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units: mg/L

50-150 Barium 0.0200 0.02015 101 50-150 Copper 0.0200 0.01926 96 50-150 Chromium 0.0200 0.02135 107 50-150 Nickel 0.0200 0.02068 103 50-150 Lead 0.0100 0.01158 116 50-150 Vanadium 0.0100 0.01071 107 50-150 Zinc 0.0400 0.04222 106

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 216 of 383

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53315-1 CRQL CHECK STANDARD METALS

Method:6010B Instrument ID:ICP5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRI 500-173518/12

CRQL Check Standard CRQL Check Standard Source: M12LCRIIC_00001 Concentration Units: mg/L

50-150 Barium 0.0200 0.02016 101 50-150 Copper 0.0200 0.01972 99 50-150 Chromium 0.0200 0.02105 105 50-150 Nickel 0.0200 0.01981 99 50-150 Lead 0.0100 0.01011 101 50-150 Vanadium 0.0100 0.01023 102 50-150 Zinc 0.0400 0.04064 102

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 217 of 383

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53315-1 CRQL CHECK STANDARD METALS

Method:7470A Instrument ID:HG6 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173280/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units: ug/L

50-150 Mercury 0.200 0.2957 148 Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173438/9

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units: ug/L

50-150 Mercury 0.200 <2.00 93

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 218 of 383

### 2B-IN

Lab Name: Job No.: SDG No.: 500-53315-1 CRQL CHECK STANDARD METALS

Method:7471A Instrument ID:HG5 TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits CRA 500-173328/10

CRQL Check Standard CRQL Check Standard Source: M12ASTKHG_00001 Concentration Units: ug/L

50-150 Mercury 0.200 0.2100 105

FORM IIB-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 219 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173224/11 CCB 500-173224/16 CCB 500-173224/28 CCB 500-173224/40 12/17/2012 20:24 12/17/2012 20:58 12/17/2012 22:14 12/17/2012 23:31 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### 0.002520 <0.00500 <0.00500 <0.00500 0.00500 J Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 220 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173517/11 CCB 500-173517/40 CCB 500-173517/52 CCB 500-173517/64 12/19/2012 09:53 12/19/2012 13:08 12/19/2012 14:32 12/19/2012 15:53 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 221 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 mg/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173518/11 CCB 500-173518/28 CCB 500-173518/40 CCB 500-173518/52 12/19/2012 18:48 12/19/2012 20:38 12/19/2012 22:04 12/19/2012 23:27 

### 3-IN

Barium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Chromium 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Copper 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Lead 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Nickel 

### <0.0100 <0.0100 <0.0100 <0.0100 0.0100 Vanadium 

### <0.00500 <0.00500 <0.00500 <0.00500 0.00500 Zinc 

### <0.0200 <0.0200 <0.0200 <0.0200 0.0200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 222 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173328/9 CCB 500-173328/13 CCB 500-173328/25 CCB 500-173328/37 12/18/2012 13:01 12/18/2012 13:08 12/18/2012 13:31 12/18/2012 13:54 

### 3-IN

Mercury 

### <0.200 <0.200 <0.200 <0.200 0.200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 223 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 ug/L

C Found C Found C Found C Found RL 

### Analyte CCB 500-173328/43 12/18/2012 14:05 

### 3-IN

Mercury 

### <0.200 0.200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 224 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173280/8 CCB 500-173280/20 CCB 500-173280/32 CCB 500-173280/39 12/18/2012 09:04 12/18/2012 09:28 12/18/2012 09:53 12/18/2012 10:21 

### 3-IN

Mercury 

### <0.200 <0.200 <0.200 <0.200 0.200

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 225 of 383

### Lab Name: Job No.:

Concentration Units: SDG No.: INSTRUMENT BLANKS METALS
TestAmerica Chicago 500-53315-1 ug/L

C Found C Found C Found C Found RL 

### Analyte ICB 500-173438/8 CCB 500-173438/20 CCB 500-173438/29 12/19/2012 10:04 12/19/2012 10:27 12/19/2012 10:44 

### 3-IN

Mercury 

### <2.00 <2.00 <2.00 2.00

FORM III-IN Italicized analytes were not requested for this sequence. 

## 01/03/2013 Page 226 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173139/1-A Concentration Units: mg/Kg

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:ICP5 METHOD BLANK METALS

173224 TestAmerica Chicago

7440-39-3 Barium <1.00 6010B 7440-50-8 Copper <1.00 6010B 7440-47-3 Chromium <1.00 6010B 7440-02-0 Nickel <1.00 6010B 7439-92-1 Lead 0.2420 J 6010B 7440-62-2 Vanadium <0.500 6010B 7440-66-6 Zinc <2.00 6010B

FORM III-IN 

## 01/03/2013 Page 227 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173349/1-A Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:ICP5 METHOD BLANK METALS

173517 TestAmerica Chicago

7440-39-3 Barium 0.002710 J 6010B 7440-50-8 Copper <0.0100 6010B 7440-47-3 Chromium 0.001210 J 6010B 7440-02-0 Nickel <0.0100 6010B 7439-92-1 Lead 0.002720 J 6010B 7440-62-2 Vanadium <0.00500 6010B 7440-66-6 Zinc <0.0200 6010B

FORM III-IN 

## 01/03/2013 Page 228 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB 500-173187/1-D Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:ICP5 METHOD BLANK METALS - TCLP

173518 TestAmerica Chicago

7440-39-3 Barium <0.500 6010B 7440-50-8 Copper <0.0250 6010B 7440-47-3 Chromium <0.0250 6010B 7440-02-0 Nickel <0.0250 6010B 7439-92-1 Lead <0.0500 6010B 7440-62-2 Vanadium <0.0250 6010B 7440-66-6 Zinc <0.100 6010B

FORM III-IN 

## 01/03/2013 Page 229 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173172/7-A Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:HG6 METHOD BLANK METALS

173280 TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN 

## 01/03/2013 Page 230 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173264/7-A Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:HG6 METHOD BLANK METALS

173438 TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN 

## 01/03/2013 Page 231 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:LB 500-173187/1-B Concentration Units: mg/L

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:HG6 METHOD BLANK METALS - TCLP

173438 TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN 

## 01/03/2013 Page 232 of 383

### Lab Name: Job No.: SDG No.: Lab Sample ID:MB 500-173153/7-A Concentration Units: mg/Kg

CAS No. Analyte Concentration C Q Method 3-IN

Batch No.:500-53315-1

Instrument Code:HG5 METHOD BLANK METALS

173328 TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN 

## 01/03/2013 Page 233 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSA 500-173224/13 P51217Bmg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0000 Barium 0.0019 Chromium -0.0023 Copper 0.0032 Lead 0.0013 Nickel 0.0041 Vanadium 0.0078 Zinc 

### 511 Aluminum 500 102 0.0001 Antimony 0.0014 Arsenic -0.0001 Beryllium 0.0003 Boron 0.0039 Cadmium 483 Calcium 500 97 0.0004 Cobalt 191 Iron 200 96 526 Magnesium 500 105 0.0032 Manganese 0.0103 Molybdenum -0.0018 Potassium 0.0006 Selenium 0.0089 Silicon 0.0000 Silver 0.0237 Sodium 0.0023 Strontium 0.0004 Thallium 0.0026 Tin 0.0005 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 234 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSAB 500-173224/14 P51217Bmg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.523 Barium 0.500 105 0.488 Chromium 0.500 98 0.564 Copper 0.500 113 0.0540 Lead 0.0500 108 0.974 Nickel 1.00 97 0.516 Vanadium 0.500 103 0.917 Zinc 1.00 92 

### 515 Aluminum 500 103 0.620 Antimony 0.600 103 0.103 Arsenic 0.100 103 0.487 Beryllium 0.500 97 0.0004 Boron 0.959 Cadmium 1.00 96 481 Calcium 500 96 0.481 Cobalt 0.500 96 192 Iron 200 96 528 Magnesium 500 106 0.507 Manganese 0.500 101 0.0109 Molybdenum -0.0110 Potassium 0.0497 Selenium 0.0500 99 0.0121 Silicon 0.223 Silver 0.200 111 0.0226 Sodium 0.0023 Strontium 0.107 Thallium 0.100 107 0.0011 Tin 0.0005 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 235 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSA 500-173517/13 P51219Amg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0000 Barium 0.0020 Chromium -0.0022 Copper 0.0054 Lead 0.0008 Nickel 0.0041 Vanadium 0.0081 Zinc 

### 509 Aluminum 500 102 -0.0017 Antimony -0.0012 Arsenic 0.0000 Beryllium 0.0004 Boron 0.0040 Cadmium 479 Calcium 500 96 0.0001 Cobalt 189 Iron 200 95 517 Magnesium 500 103 0.0035 Manganese 0.0125 Molybdenum -0.0053 Potassium 0.0002 Selenium 0.0151 Silicon 0.0000 Silver 0.0079 Sodium 0.0023 Strontium 0.0073 Thallium 0.0014 Tin 0.0008 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 236 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSAB 500-173517/14 P51219Amg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.518 Barium 0.500 104 0.482 Chromium 0.500 96 0.560 Copper 0.500 112 0.0528 Lead 0.0500 106 0.948 Nickel 1.00 95 0.508 Vanadium 0.500 102 0.902 Zinc 1.00 90 

### 511 Aluminum 500 102 0.617 Antimony 0.600 103 0.104 Arsenic 0.100 104 0.481 Beryllium 0.500 96 0.0011 Boron 0.941 Cadmium 1.00 94 479 Calcium 500 96 0.472 Cobalt 0.500 94 191 Iron 200 95 519 Magnesium 500 104 0.501 Manganese 0.500 100 0.0124 Molybdenum -0.0129 Potassium 0.0472 Selenium 0.0500 94 0.0159 Silicon 0.223 Silver 0.200 111 0.0129 Sodium 0.0023 Strontium 0.104 Thallium 0.100 104 0.0020 Tin 0.0009 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 237 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSA 500-173517/76 P51219Amg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0003 Barium 0.0021 Chromium -0.0025 Copper 0.0038 Lead 0.0004 Nickel 0.0041 Vanadium 0.0080 Zinc 

### 507 Aluminum 500 101 0.0003 Antimony -0.0005 Arsenic -0.0001 Beryllium 0.0010 Boron 0.0035 Cadmium 488 Calcium 500 98 0.0000 Cobalt 193 Iron 200 97 522 Magnesium 500 104 0.0045 Manganese 0.0127 Molybdenum -0.0103 Potassium -0.0026 Selenium 0.0155 Silicon 0.0002 Silver 0.0106 Sodium 0.0022 Strontium 0.0042 Thallium -0.0011 Tin 0.0008 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 238 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSAB 500-173517/77 P51219Amg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.508 Barium 0.500 102 0.490 Chromium 0.500 98 0.553 Copper 0.500 111 0.0533 Lead 0.0500 107 0.965 Nickel 1.00 97 0.513 Vanadium 0.500 103 0.935 Zinc 1.00 93 

### 509 Aluminum 500 102 0.623 Antimony 0.600 104 0.104 Arsenic 0.100 104 0.490 Beryllium 0.500 98 0.0012 Boron 0.965 Cadmium 1.00 96 488 Calcium 500 98 0.479 Cobalt 0.500 96 194 Iron 200 97 523 Magnesium 500 105 0.508 Manganese 0.500 102 0.0145 Molybdenum -0.0103 Potassium 0.0481 Selenium 0.0500 96 0.0146 Silicon 0.223 Silver 0.200 111 0.0169 Sodium 0.0022 Strontium 0.108 Thallium 0.100 108 -0.0003 Tin 0.0009 Titanium



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 239 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution A Solution A Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSA 500-173518/13 P51219Bmg/L M12LISAIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.0000 Barium 0.0019 Chromium -0.0021 Copper 0.0018 Lead 0.0005 Nickel 0.0039 Vanadium 0.0075 Zinc 

### 509 Aluminum 500 102 -0.0009 Antimony 0.0002 Arsenic -0.0001 Beryllium 0.0007 Boron 0.0025 Cadmium 478 Calcium 500 96 0.0000 Cobalt 189 Iron 200 94 519 Magnesium 500 104 0.0048 Manganese 0.0125 Molybdenum -0.0137 Potassium -0.0021 Selenium 0.0145 Silicon 0.0002 Silver 0.0138 Sodium 0.0022 Strontium 0.0058 Thallium -0.0017 Tin 0.0008 Titanium 0.0025 Total Heavy Metals



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 240 of 383

### 4A-IN

Lab Name: Job No.:

Instrument ID: ICS Source: Concentration Units:

Analyte True Percent Recovery Found SDG No.:

Lab File ID:

Solution AB Solution AB Lab Sample ID: TestAmerica Chicago 500-53315-1
ICSAB 500-173518/14 P51219Bmg/L M12LISBIC_00001 ICP5 INTERFERENCE CHECK STANDARD METALS

0.518 Barium 0.500 104 0.483 Chromium 0.500 97 0.556 Copper 0.500 111 0.0504 Lead 0.0500 101 0.943 Nickel 1.00 94 0.508 Vanadium 0.500 102 0.902 Zinc 1.00 90 

### 510 Aluminum 500 102 0.613 Antimony 0.600 102 0.107 Arsenic 0.100 107 0.480 Beryllium 0.500 96 0.0009 Boron 0.935 Cadmium 1.00 93 481 Calcium 500 96 0.470 Cobalt 0.500 94 190 Iron 200 95 522 Magnesium 500 104 0.501 Manganese 0.500 100 0.0115 Molybdenum -0.0099 Potassium 0.0483 Selenium 0.0500 97 0.0130 Silicon 0.222 Silver 0.200 111 0.0206 Sodium 0.0022 Strontium 0.104 Thallium 0.100 104 0.0005 Tin 0.0008 Titanium 3.87 Total Heavy Metals 4.05 96



### FORM IVA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 241 of 383

### MATRIX SPIKE SAMPLE RECOVERY METALS 5A-IN

FC COMPOSITE 4 MS Lab Name: Job No.: SDG No.: Client ID: Lab ID:500-53315-1 MS 500-53315-1

Matrix: Concentration Units: mg/Kg Solid TestAmerica Chicago

% Solids:25.9
Control Limit %R Analyte SSR C Sample Result (SR) C Spike Added (SA) %R Q Method
Barium 75-125 987.2 346 762 84 6010B Copper 75-125 836.2 834 95.2 2 4 6010B Chromium 75-125 13510 14400 76.2 -1125 4 6010B Nickel 75-125 246.8 89.8 190 82 6010B Lead 75-125 253.1 209 38.1 116 4 6010B Vanadium 75-125 391.8 241 190 79 6010B Zinc 75-125 605.1 481 190 65 F 6010B SSR = Spiked Sample Result



### FORM VA - IN Note - Results and Reporting Limits have been adjusted for dry weight. Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 242 of 383

### MATRIX SPIKE SAMPLE RECOVERY METALS 5A-IN

FC EB 4 MS Lab Name: Job No.: SDG No.: Client ID: Lab ID:500-53315-6 MS 500-53315-1

Matrix: Concentration Units: mg/L Water TestAmerica Chicago

% Solids:
Control Limit %R Analyte SSR C Sample Result (SR) C Spike Added (SA) %R Q Method Mercury 75-125 0.0009604 0.000102 0.00100 86 7470A J SSR = Spiked Sample Result



### FORM VA - IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 243 of 383

### MATRIX SPIKE DUPLICATE SAMPLE RECOVERY METALS 5A-IN

FC COMPOSITE 4 MSD Lab Name: Job No.: SDG No.: Client ID: Lab ID:500-53315-1 MSD 500-53315-1

Matrix: Concentration Units: mg/Kg Solid TestAmerica Chicago

% Solids:25.9

Analyte (SDR) C Control Limit %R %R RPD RPD Limit Q Method Spike Added (SA)
Barium 943.9 729 82 75-125 4 20 6010B Copper 799.8 91.2 -38 75-125 4 20 4 6010B Chromium 13220 72.9 -1577 75-125 2 20 4 6010B Nickel 237.5 182 81 75-125 4 20 6010B Lead 213.5 36.5 12 75-125 17 20 4 6010B Vanadium 379.3 182 76 75-125 3 20 6010B Zinc 600.3 182 65 75-125 1 20 F 6010B SDR = Sample Duplicate Result



### FORM VD - IN Note - Results and Reporting Limits have been adjusted for dry weight. Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 244 of 383

### MATRIX SPIKE DUPLICATE SAMPLE RECOVERY METALS 5A-IN

FC EB 4 MSD Lab Name: Job No.: SDG No.: Client ID: Lab ID:500-53315-6 MSD 500-53315-1

Matrix: Concentration Units: mg/L Water TestAmerica Chicago

% Solids:

Analyte (SDR) C Control Limit %R %R RPD RPD Limit Q Method Spike Added (SA) Mercury 0.0007896 0.00100 69 75-125 20 20 F 7470A SDR = Sample Duplicate Result



### FORM VD - IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 245 of 383

### 6-IN DUPLICATES

FC COMPOSITE 4 DU Lab Name: Job No.: SDG No.:

Matrix: Concentration Units: mg/Kg

Analyte Control Limit Sample (S)CDuplicate (D)C RPD Q Method 500-53315-1

Solid METALS

% Solids for Sample: 25.9 % Solids for Duplicate: Client ID: Lab ID:500-53315-1 DU

25.9 TestAmerica Chicago

Barium 335.3 346 3.73 3 6010B Copper 804.0 834 3.73 4 6010B Chromium 13970 14400 3.73 3 6010B Nickel 88.38 89.8 3.73 2 6010B Lead 201.3 209 1.86 4 6010B Vanadium 234.5 241 1.86 3 6010B Zinc 468.4 481 7.46 3 6010B

FORM VI-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 246 of 383

### 6-IN DUPLICATES

FC EB 4 DU Lab Name: Job No.: SDG No.:

Matrix: Concentration Units: mg/L

Analyte Control Limit Sample (S)CDuplicate (D)C RPD Q Method 500-53315-1

Water METALS

% Solids for Sample: % Solids for Duplicate: Client ID: Lab ID:500-53315-6 DU TestAmerica Chicago

Mercury 0.0001082J 0.000102 0.000200 6 7470A J

FORM VI-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 247 of 383

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173139/2-A Lab Name: Job No.:500-53315-1 Sample Matrix:Solid LCS Source:M12KSPKIC_00001 TestAmerica Chicago

Analyte Solid(mg/Kg)
True Found C %R Limits Q Method Barium 200 197.2 99 6010B 80 120 Copper 25.0 24.95 100 6010B 80 120 Chromium 20.0 19.91 100 6010B 80 120 Nickel 50.0 49.11 98 6010B 80 120 Lead 10.0 10.07 101 6010B 80 120 Vanadium 50.0 49.74 99 6010B 80 120 Zinc 50.0 48.83 98 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results. 

### FORM VIIA - IN



## 01/03/2013 Page 248 of 383

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173349/2-A Lab Name: Job No.:500-53315-1 Sample Matrix:Water LCS Source:M12JSPKIC_00002 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Barium 2.00 1.955 98 6010B 80 120 Copper 0.250 0.2524 101 6010B 80 120 Chromium 0.200 0.1989 99 6010B 80 120 Nickel 0.500 0.4934 99 6010B 80 120 Lead 0.100 0.1010 101 6010B 80 120 Vanadium 0.500 0.4993 100 6010B 80 120 Zinc 0.500 0.4858 97 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results. 

### FORM VIIA - IN



## 01/03/2013 Page 249 of 383

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173406/3-A Lab Name: Job No.:500-53315-1 Sample Matrix:Water LCS Source:M12KSPKIC_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Barium 2.00 1.975 99 6010B 80 120 Copper 0.250 0.2464 99 6010B 80 120 Chromium 0.200 0.1969 98 6010B 80 120 Nickel 0.500 0.4873 97 6010B 80 120 Lead 0.100 0.09785 98 6010B 80 120 Vanadium 0.500 0.4959 99 6010B 80 120 Zinc 0.500 0.4782 96 6010B 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results. 

### FORM VIIA - IN



## 01/03/2013 Page 250 of 383

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173172/8-A Lab Name: Job No.:500-53315-1 Sample Matrix:Water LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Mercury 0.00200 0.002027 101 7470A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results. 

### FORM VIIA - IN



## 01/03/2013 Page 251 of 383

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173264/8-A Lab Name: Job No.:500-53315-1 Sample Matrix:Water LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Water(mg/L)
True Found C %R Limits Q Method Mercury 0.00200 0.002002 100 7470A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results. 

### FORM VIIA - IN



## 01/03/2013 Page 252 of 383

### 7A-IN LAB CONTROL SAMPLE METALS

Lab ID:LCS 500-173153/8-A Lab Name: Job No.:500-53315-1 Sample Matrix:Solid LCS Source:M11FSTKHG_00001 TestAmerica Chicago

Analyte Solid(mg/Kg)
True Found C %R Limits Q Method Mercury 0.167 0.1717 103 7471A 80 120

Calculations are performed before rounding to avoid round-off errors in calculated results. 

### FORM VIIA - IN



## 01/03/2013 Page 253 of 383

### 8-IN

Lab ID:500-53315-1

Lab Name: Job No: Matrix: Concentration Units: mg/Kg

Analyte Initial Sample Result (I) C Serial Dilution Result (S) C % Difference Q Method SDG No:

Solid 500-53315-1 ICP-AES AND ICP-MS SERIAL DILUTIONS METALS

TestAmerica Chicago

Barium 346 377.6 9.2 6010B Copper 834 868.4 4.1 6010B Chromium 14400 16720 16V 6010B Nickel 89.8 102.4 14V 6010B Lead 209 239.4 15V 6010B Vanadium 241 281.4 17V 6010B Zinc 481 576.2 20V 6010B



### FORM VIII-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 254 of 383

### 9-IN

Instrument ID:ICP5 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 02/20/2012 13:03 Method: 3010A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Barium 0.00044 0.01 Chromium 0.00096 0.01 Copper 0.00106 0.01 Lead 0.00158 0.005 Nickel 0.0019 0.01 Vanadium 0.00062 0.005 Zinc 0.00472 0.02

FORM IX - IN 

## 01/03/2013 Page 255 of 383

### 9-IN

Instrument ID:ICP5 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 05/25/2006 09:07 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.005 0.01 Chromium 0.005 0.01 Copper 0.005 0.01 Lead 0.0025 0.005 Nickel 0.005 0.01 Vanadium 0.0025 0.005 Zinc 0.01 0.02

FORM IX - IN 

## 01/03/2013 Page 256 of 383

### 9-IN

Instrument ID:ICP5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 02/20/2012 13:20 Method: 3050B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Barium 0.119 1 Chromium 0.167 1 Copper 0.271 1 Lead 0.172 0.5 Nickel 0.219 1 Vanadium 0.0759 0.5 Zinc 0.686 2

FORM IX - IN 

## 01/03/2013 Page 257 of 383

### 9-IN

Instrument ID:ICP5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 05/25/2006 09:03 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.005 0.01 Chromium 0.005 0.01 Copper 0.005 0.01 Lead 0.0025 0.005 Nickel 0.005 0.01 Vanadium 0.0025 0.005 Zinc 0.01 0.02

FORM IX - IN 

## 01/03/2013 Page 258 of 383

### 9-IN

Instrument ID:ICP5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica Chicago DETECTION LIMITS

6010B MDL Date: 11/01/2005 15:36 Method: 3010A Prep Method: 1311 Leach Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Barium 0.01 0.5 Chromium 0.01 0.025 Copper 0.01 0.025 Lead 0.005 0.05 Nickel 0.01 0.025 Vanadium 0.005 0.025 Zinc 0.02 0.1

FORM IX - IN 

## 01/03/2013 Page 259 of 383

### 9-IN

Instrument ID:ICP5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

6010B XMDL Date: 01/28/2008 10:37 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Barium 0.01 0.01 Chromium 0.01 0.01 Copper 0.01 0.01 Lead 0.005 0.005 Nickel 0.01 0.01 Vanadium 0.005 0.005 Zinc 0.02 0.02

FORM IX - IN 

## 01/03/2013 Page 260 of 383

### 9-IN

Instrument ID:HG6 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

7470A MDL Date: 08/31/2012 10:08 Method: 7470A Prep Method: Analyte Wavelength/ Mass RL MDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/03/2013 Page 261 of 383

### 9-IN

Instrument ID:HG6 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7470A XMDL Date: 08/31/2012 10:08 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/03/2013 Page 262 of 383

### 9-IN

Instrument ID:HG6 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica Chicago DETECTION LIMITS

7470A MDL Date: 11/01/2005 11:39 Method: 7470A Prep Method: 1311 Leach Method: Analyte Wavelength/ Mass RL MDL (ug/L) (ug/L) Mercury 0.2 2

FORM IX - IN 

## 01/03/2013 Page 263 of 383

### 9-IN

Instrument ID:HG6 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS - TCLP
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7470A XMDL Date: 09/16/2006 08:48 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 1 2

FORM IX - IN 

## 01/03/2013 Page 264 of 383

### 9-IN

Instrument ID:HG5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica Chicago DETECTION LIMITS

7471A MDL Date: 08/31/2012 10:15 Method: 7471A Prep Method: Analyte Wavelength/ Mass RL MDL (ug/Kg) (ug/Kg) Mercury 6.37 16.7

FORM IX - IN 

## 01/03/2013 Page 265 of 383

### 9-IN

Instrument ID:HG5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: METALS
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7471A XMDL Date: 08/31/2012 10:16 Method: Analyte Wavelength/ Mass XRL XMDL (ug/L) (ug/L) Mercury 0.071 0.2

FORM IX - IN 

## 01/03/2013 Page 266 of 383

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53315-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

ICP5 SDG No.:

(mg/L) 11/19/2012 14:31 METALS

Barium 206010B Copper 206010B Chromium 506010B Nickel 506010B Lead 506010B Vanadium 1006010B Zinc 206010B

FORM XI - IN 

## 01/03/2013 Page 267 of 383

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53315-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

HG5 SDG No.:

(ug/L) 03/01/2008 11:18 METALS

Mercury 5.07471A

FORM XI - IN 

## 01/03/2013 Page 268 of 383

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53315-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

HG6 SDG No.:

(ug/L) 11/01/2010 11:39 METALS

Mercury 5.07470A

FORM XI - IN 

## 01/03/2013 Page 269 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 METALS
TestAmerica Chicago
Prep Method:3050B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/17/2012 08:50 173139 MB 500-173139/1-A 100 1 12/17/2012 08:50 173139 LCS 500-173139/2-A 100 1 12/17/2012 08:50 173139 500-53315-1 100 1.0407 12/17/2012 08:50 173139 500-53315-1 DU 100 1.0334 12/17/2012 08:50 173139 500-53315-1 MS 100 1.0117 12/17/2012 08:50 173139 500-53315-1 MSD 100 1.0566 12/17/2012 08:50 173139 500-53315-2 100 1.0994

FORM XII-IN 

## 01/03/2013 Page 270 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 METALS
TestAmerica Chicago
Prep Method:3010A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/18/2012 15:30 173349 MB 500-173349/1-A 50 50 12/18/2012 15:30 173349 LCS 500-173349/2-A 50 50 12/18/2012 15:30 173349 500-53315-6 50 50

FORM XII-IN 

## 01/03/2013 Page 271 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 METALS
TestAmerica Chicago
Prep Method:3010A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/19/2012 08:20 173406 LB 500-173187/1-D 50 50 12/19/2012 08:20 173406 LCS 500-173406/3-A 50 50 12/19/2012 08:20 173406 500-53315-1 50 50 12/19/2012 08:20 173406 500-53315-2 50 50

FORM XII-IN 

## 01/03/2013 Page 272 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 METALS
TestAmerica Chicago
Prep Method:7471A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/17/2012 14:00 173153 MB 500-173153/7-A 50 0.6 12/17/2012 14:00 173153 LCS 500-173153/8-A 50 0.6 12/17/2012 14:00 173153 500-53315-1 50 0.6494 12/17/2012 14:00 173153 500-53315-2 50 0.6068

FORM XII-IN 

## 01/03/2013 Page 273 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 METALS
TestAmerica Chicago
Prep Method:7470A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/17/2012 13:00 173172 MB 500-173172/7-A 25 25 12/17/2012 13:00 173172 LCS 500-173172/8-A 25 25 12/17/2012 13:00 173172 500-53315-6 25 25 12/17/2012 13:00 173172 500-53315-6 DU 25 25 12/17/2012 13:00 173172 500-53315-6 MS 25 25 12/17/2012 13:00 173172 500-53315-6 MSD 25 25

FORM XII-IN 

## 01/03/2013 Page 274 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 METALS
TestAmerica Chicago
Prep Method:7470A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/18/2012 13:00 173264 MB 500-173264/7-A 25 25 12/18/2012 13:00 173264 LCS 500-173264/8-A 25 25 12/18/2012 13:00 173264 LB 500-173187/1-B 25 25 12/18/2012 13:00 173264 500-53315-1 25 25 12/18/2012 13:00 173264 500-53315-2 25 25

FORM XII-IN 

## 01/03/2013 Page 275 of 383

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

ICP5 12/17/2012 19:16 12/18/2012 02:45 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 19:16 ZZZZZZ 19:22 ZZZZZZ 19:29 ZZZZZZ 19:35 ZZZZZZ 19:41 ZZZZZZ 19:46 ZZZZZZ 19:51 ZZZZZZ 19:59 ZZZZZZ 20:07 ZZZZZZ 1 20:16 XXX XXXX ICV 500-173224/10 1 20:24 XXX XXXX ICB 500-173224/11 1 20:30 XXX XXXX CRI 500-173224/12 1 20:37 XXX XXXX ICSA 500-173224/13 1 20:43 XXX XXXX ICSAB 500-173224/14 1 20:51 XXX XXXX CCV 500-173224/15 1 20:58 XXX XXXX CCB 500-173224/16 1 21:04 XXX XXXX MB 500-173139/1-A T 1 21:10 XXX XXXX LCS 500-173139/2-A T 21:16 ZZZZZZ 21:22 ZZZZZZ 21:29 ZZZZZZ 21:35 ZZZZZZ 21:41 ZZZZZZ 21:47 ZZZZZZ 21:54 ZZZZZZ 22:00 ZZZZZZ 1 22:08 XXX XXXX CCV 500-173224/27 1 22:14 XXX XXXX CCB 500-173224/28 22:21 ZZZZZZ 22:27 ZZZZZZ 22:33 ZZZZZZ 22:39 ZZZZZZ 1 22:46 XXX XXXX 500-53315-1 T 5 22:52 XXX XXXX 500-53315-1 SD T 1 22:58 XXX XXXX 500-53315-1 DU T 1 23:04 XXX XXXX 500-53315-1 MS T 1 23:10 XXX XXXX 500-53315-1 MSD T 1 23:17 XXX XXXX 500-53315-2 T 1 23:25 XXX XXXX CCV 500-173224/39 1 23:31 XXX XXXX CCB 500-173224/40 23:38 ZZZZZZ 23:44 ZZZZZZ



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

ICP5 12/17/2012 19:16 12/18/2012 02:45 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 23:50 ZZZZZZ 23:56 ZZZZZZ 00:02 ZZZZZZ 00:09 ZZZZZZ 00:15 ZZZZZZ 00:21 ZZZZZZ 00:27 ZZZZZZ 00:33 ZZZZZZ 00:42 CCV 500-173224/51 00:48 CCB 500-173224/52 00:54 ZZZZZZ 01:01 ZZZZZZ 01:07 ZZZZZZ 01:13 ZZZZZZ 01:19 ZZZZZZ 01:26 ZZZZZZ 01:32 ZZZZZZ 01:38 ZZZZZZ 01:44 ZZZZZZ 01:50 ZZZZZZ 01:59 CCV 500-173224/63 02:05 CCB 500-173224/64 02:11 ZZZZZZ 02:18 ZZZZZZ 02:24 ZZZZZZ 02:30 ZZZZZZ 02:39 CCV 500-173224/69 02:45 CCB 500-173224/70 Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

ICP5 12/19/2012 08:45 12/19/2012 17:31 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 08:45 ZZZZZZ 08:51 ZZZZZZ 08:57 ZZZZZZ 09:04 ZZZZZZ 09:10 ZZZZZZ 09:15 ZZZZZZ 09:20 ZZZZZZ 09:28 ZZZZZZ 09:36 ZZZZZZ 1 09:45 XXX XXXX ICV 500-173517/10 1 09:53 XXX XXXX ICB 500-173517/11 1 09:59 XXX XXXX CRI 500-173517/12 1 10:05 XXX XXXX ICSA 500-173517/13 1 10:12 XXX XXXX ICSAB 500-173517/14 10:20 CCV 500-173517/15 10:26 CCB 500-173517/16 10:33 ZZZZZZ 10:39 ZZZZZZ 10:45 ZZZZZZ 10:52 ZZZZZZ 10:58 ZZZZZZ 11:04 ZZZZZZ 11:11 ZZZZZZ 11:17 ZZZZZZ 11:30 ZZZZZZ 11:37 ZZZZZZ 11:45 CCV 500-173517/27 11:51 CCB 500-173517/28 11:57 ZZZZZZ 12:04 ZZZZZZ 12:10 ZZZZZZ 12:16 ZZZZZZ 12:22 ZZZZZZ 12:28 ZZZZZZ 12:35 ZZZZZZ 12:41 ZZZZZZ 12:47 ZZZZZZ 12:53 ZZZZZZ 1 13:02 XXX XXXX CCV 500-173517/39 1 13:08 XXX XXXX CCB 500-173517/40 13:14 ZZZZZZ 13:21 ZZZZZZ



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

ICP5 12/19/2012 08:45 12/19/2012 17:31 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 13:27 ZZZZZZ 13:33 ZZZZZZ 13:39 ZZZZZZ 1 13:52 XXX XXXX MB 500-173349/1-A T 1 13:58 XXX XXXX LCS 500-173349/2-A T 14:04 ZZZZZZ 14:11 ZZZZZZ 14:18 ZZZZZZ 1 14:26 XXX XXXX CCV 500-173517/51 1 14:32 XXX XXXX CCB 500-173517/52 14:38 ZZZZZZ 14:45 ZZZZZZ 14:51 ZZZZZZ 1 14:57 XXX XXXX 500-53315-6 T 15:03 ZZZZZZ 15:14 ZZZZZZ 15:20 ZZZZZZ 15:26 ZZZZZZ 15:33 ZZZZZZ 15:39 ZZZZZZ 1 15:47 XXX XXXX CCV 500-173517/63 1 15:53 XXX XXXX CCB 500-173517/64 16:00 ZZZZZZ 16:06 ZZZZZZ 16:12 ZZZZZZ 16:18 ZZZZZZ 16:25 ZZZZZZ 16:31 ZZZZZZ 16:37 ZZZZZZ 16:43 ZZZZZZ 16:52 CCV 500-173517/73 16:58 CCB 500-173517/74 1 17:04 XXX XXXX CRI 500-173517/75 1 17:10 XXX XXXX ICSA 500-173517/76 1 17:16 XXX XXXX ICSAB 500-173517/77 17:25 CCV 500-173517/78 17:31 CCB 500-173517/79 Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

ICP5 12/19/2012 17:42 12/20/2012 00:26 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 17:42 ZZZZZZ 17:48 ZZZZZZ 17:54 ZZZZZZ 18:01 ZZZZZZ 18:07 ZZZZZZ 18:12 ZZZZZZ 18:17 ZZZZZZ 18:24 ZZZZZZ 18:33 ZZZZZZ 1 18:41 XXX XXXX ICV 500-173518/10 1 18:48 XXX XXXX ICB 500-173518/11 1 18:54 XXX XXXX CRI 500-173518/12 1 19:00 XXX XXXX ICSA 500-173518/13 1 19:06 XXX XXXX ICSAB 500-173518/14 19:15 CCV 500-173518/15 19:21 CCB 500-173518/16 19:27 ZZZZZZ 19:33 ZZZZZZ 19:40 ZZZZZZ 19:46 ZZZZZZ 19:52 ZZZZZZ 19:58 ZZZZZZ 20:04 ZZZZZZ 20:11 ZZZZZZ 20:17 ZZZZZZ 20:23 ZZZZZZ 1 20:32 XXX XXXX CCV 500-173518/27 1 20:38 XXX XXXX CCB 500-173518/28 20:44 ZZZZZZ 20:50 ZZZZZZ 20:56 ZZZZZZ 1 21:07 XXX XXXX LB 500-173187/1-D P 21:13 ZZZZZZ 1 21:20 XXX XXXX LCS 500-173406/3-A T 21:26 ZZZZZZ 21:32 ZZZZZZ 21:43 ZZZZZZ 21:49 ZZZZZZ 1 21:57 XXX XXXX CCV 500-173518/39 1 22:04 XXX XXXX CCB 500-173518/40 22:10 ZZZZZZ 22:16 ZZZZZZ



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

ICP5 12/19/2012 17:42 12/20/2012 00:26 6010B METALS

Lab Sample ID D / F Time 

### Analytes B aC rC uN iP bVZ n T y p e 22:22 ZZZZZZ 1 22:29 XXX XXXX 500-53315-1 P 1 22:35 XXX XXXX 500-53315-2 P 22:41 ZZZZZZ 22:54 ZZZZZZ 23:00 ZZZZZZ 23:06 ZZZZZZ 23:13 ZZZZZZ 1 23:21 XXX XXXX CCV 500-173518/51 1 23:27 XXX XXXX CCB 500-173518/52 23:34 ZZZZZZ 23:40 ZZZZZZ 23:46 ZZZZZZ 23:52 ZZZZZZ 23:59 ZZZZZZ 00:05 ZZZZZZ 00:11 ZZZZZZ 00:19 CCV 500-173518/60 00:26 CCB 500-173518/61 Prep Types P = TCLP T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

HG6 12/18/2012 08:48 12/18/2012 10:21 7470A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 08:48 ZZZZZZ 08:50 ZZZZZZ 08:52 ZZZZZZ 08:54 ZZZZZZ 08:56 ZZZZZZ 08:59 ZZZZZZ 1 09:03 X ICV 500-173280/7 1 09:04 X ICB 500-173280/8 1 09:07 X CRA 500-173280/9 1 09:09 X MB 500-173172/7-A T 1 09:11 X LCS 500-173172/8-A T 09:13 ZZZZZZ 09:15 ZZZZZZ 09:17 ZZZZZZ 09:19 ZZZZZZ 09:21 ZZZZZZ 09:23 ZZZZZZ 09:25 ZZZZZZ 1 09:26 X CCV 500-173280/19 1 09:28 X CCB 500-173280/20 09:31 ZZZZZZ 09:32 ZZZZZZ 09:35 ZZZZZZ 09:37 ZZZZZZ 09:40 ZZZZZZ 09:42 ZZZZZZ 09:44 ZZZZZZ 09:45 ZZZZZZ 09:47 ZZZZZZ 1 09:49 X 500-53315-6 T 1 09:51 X CCV 500-173280/31 1 09:53 X CCB 500-173280/32 1 09:55 X 500-53315-6 DU T 1 09:57 X 500-53315-6 MS T 1 09:59 X 500-53315-6 MSD T 10:01 CCV 500-173280/36 10:04 CCB 500-173280/37 1 10:19 X CCV 500-173280/38 1 10:21 X CCB 500-173280/39 Prep Types T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

HG6 12/19/2012 09:50 12/19/2012 10:50 7470A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 09:50 ZZZZZZ 09:52 ZZZZZZ 09:54 ZZZZZZ 09:56 ZZZZZZ 09:58 ZZZZZZ 10:00 ZZZZZZ 1 10:02 X ICV 500-173438/7 1 10:04 X ICB 500-173438/8 1 10:07 X CRA 500-173438/9 1 10:08 X MB 500-173264/7-A T 1 10:10 X LCS 500-173264/8-A T 1 10:12 X LB 500-173187/1-B P 10:14 ZZZZZZ 10:16 ZZZZZZ 10:18 ZZZZZZ 10:20 ZZZZZZ 10:22 ZZZZZZ 1 10:24 X 500-53315-1 P 1 10:26 X CCV 500-173438/19 1 10:27 X CCB 500-173438/20 1 10:29 X 500-53315-2 P 10:31 ZZZZZZ 10:33 ZZZZZZ 10:35 ZZZZZZ 10:37 ZZZZZZ 10:39 ZZZZZZ 10:40 ZZZZZZ 1 10:42 X CCV 500-173438/28 1 10:44 X CCB 500-173438/29 10:46 ZZZZZZ 10:48 CCV 500-173438/31 10:50 CCB 500-173438/32 Prep Types P = TCLP T = Total/NA



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

HG5 12/18/2012 12:44 12/18/2012 14:19 7471A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 12:44 X STD01REP1 500-173328/1 IC 12:46 X STD02REP1 500-173328/2 IC 12:47 X STD03REP1 500-173328/3 IC 12:49 X STD04REP1 500-173328/4 IC 12:51 X STD05REP1 500-173328/5 IC 12:53 X STD06REP1 500-173328/6 IC 12:55 ICV 500-173328/7 1 12:59 X ICV 500-173328/8 1 13:01 X ICB 500-173328/9 1 13:02 X CRA 500-173328/10 1 13:04 X MB 500-173153/7-A T 1 13:06 X CCV 500-173328/12 1 13:08 X CCB 500-173328/13 1 13:10 X LCS 500-173153/8-A T 13:12 ZZZZZZ 13:14 ZZZZZZ 13:16 ZZZZZZ 13:18 ZZZZZZ 13:20 ZZZZZZ 13:21 ZZZZZZ 13:24 ZZZZZZ 13:25 ZZZZZZ 13:27 ZZZZZZ 1 13:29 X CCV 500-173328/24 1 13:31 X CCB 500-173328/25 13:33 ZZZZZZ 13:35 ZZZZZZ 13:37 ZZZZZZ 13:39 ZZZZZZ 13:41 ZZZZZZ 13:43 ZZZZZZ 13:45 ZZZZZZ 13:47 ZZZZZZ 13:48 ZZZZZZ 13:50 ZZZZZZ 1 13:52 X CCV 500-173328/36 1 13:54 X CCB 500-173328/37 13:56 ZZZZZZ 13:58 ZZZZZZ



### FORM XIII-IN 

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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

HG5 12/18/2012 12:44 12/18/2012 14:19 7471A METALS

Lab Sample ID D / F Time 

### Analytes H g T y p e 1 14:00 X 500-53315-1 T 1 14:01 X 500-53315-2 T 1 14:03 X CCV 500-173328/42 1 14:05 X CCB 500-173328/43 14:07 ZZZZZZ 14:09 ZZZZZZ 14:11 ZZZZZZ 14:13 ZZZZZZ 14:15 ZZZZZZ 14:17 CCV 500-173328/49 14:19 CCB 500-173328/50 Prep Types T = Total/NA



### FORM XIII-IN 

## 01/03/2013 Page 285 of 383

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Hudson, Lawrence A 12/17/12 09:20 12/17/12 08:50 173139 Batch Method: TestAmerica Chicago

3050B Lab Sample ID Client Sample IDMethod ChainBasis CalcMsg InitialAmount FinalAmount M12KSPKIC 00001 CALC NOT SET TO RUN 1 g 100 mL MB 500-173139/1 3050B, 6010B CALC NOT SET TO RUN 1 g 100 mL 1 mL LCS 500-173139/2 3050B, 6010B FC COMPOSITE 4 CALC NOT SET TO RUN 1.0407 g 100 mL 500-53315-A-1 3050B, 6010B T FC COMPOSITE 4 CALC NOT SET TO RUN 1.0334 g 100 mL 500-53315-A-1 DU 3050B, 6010B T FC COMPOSITE 4 CALC NOT SET TO RUN 1.0117 g 100 mL 1 mL 500-53315-A-1 MS 3050B, 6010B T FC COMPOSITE 4 CALC NOT SET TO RUN 1.0566 g 100 mL 1 mL 500-53315-A-1 MSD 3050B, 6010B T FC D COMPOSITE 4 CALC NOT SET TO RUN 1.0994 g 100 mL 500-53315-A-2 3050B, 6010B T

Batch Notes Analyst LH Balance ID C-1966 First End time 0920 Hydrogen peroxide lot number L08A06 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L08022 Hood ID or number 3 Hot Block ID number 8 Oven, Bath or Block Temperature 1 90 Degrees C Oven, Bath or Block Temperature 2 90 Degrees C Pipette ID 1628 Person's name who witnessed reagent drop DB First Start time 0850 ID number of the thermometer J59717 Digestion Tube/Cup Lot # MF06LKK01
Basis Basis Description T Total/NA



### Page 1 of 1 6010B 

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### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Laird, Rebecca 12/18/12 16:00 12/18/12 15:30 173349 Batch Method: TestAmerica Chicago

3010A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M12JSPKIC 00002 50 mL 50 mL MB 500-173349/1 3010A, 6010B 50 mL 50 mL 0.5 mL LCS 500-173349/2 3010A, 6010B FC EB 4 50 mL 50 mL 500-53315-E-6 3010A, 6010B T
Batch Notes First End time 1600 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L08022 Hot Block ID number 4 Pipette ID 1627 First Start time 1530 ID number of the thermometer J59688 Digestion Tube/Cup Lot # 20313760 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description T Total/NA



### Page 1 of 1 6010B 

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### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Hudson, Lawrence A 12/19/12 08:50 12/19/12 08:20 173406 Batch Method: TestAmerica Chicago

3010A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment 50 mL 50 mL T-744 LB 500-173187/1-A 3010A, 6010B 50 mL 50 mL 0.5 mL LCS 500-173406/3 3010A, 6010B FC COMPOSITE 4 50 mL 50 mL 500-53315-A-1-G 3010A, 6010B P FC D COMPOSITE 4 50 mL 50 mL 500-53315-A-2-C 3010A, 6010B P
Batch Notes Batch Comment T-744, T-748 First End time 0850 Lot # of hydrochloric acid 0000013500 Lot # of Nitric Acid L10022 Hot Block ID number 4 Pipette ID 1627 First Start time 0820 ID number of the thermometer J59688 Digestion Tube/Cup Lot # 20313760 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius
Basis Basis Description P TCLP



### Page 1 of 1 6010B 

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### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/17/12 15:00 12/17/12 13:00 173172 Batch Method: TestAmerica Chicago

7470A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 M12ASTKHG 00001 25 mL 25 mL MB 500-173172/7 7470A, 7470A 25 mL 25 mL 0.00005 mL LCS 500-173172/8 7470A, 7470A FC EB 4 25 mL 25 mL 500-53315-E-6 7470A, 7470A T FC EB 4 25 mL 25 mL 500-53315-E-6 DU 7470A, 7470A T FC EB 4 25 mL 25 mL 0.000025 mL 500-53315-E-6 MS 7470A, 7470A T FC EB 4 25 mL 25 mL 0.000025 mL 500-53315-E-6 MSD 7470A, 7470A T

Batch Notes Hydroxylamine Hydrochloride Lot 19333 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 6 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 88 Oven, Bath or Block Temperature 2 88 Pipette ID 2240 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Temperature 88 Celsius ID number of the thermometer hb305412 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Visual ck - digestate F.V. consistency OK



### Page 1 of 2 7470A 

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### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/17/12 15:00 12/17/12 13:00 173172 Batch Method: TestAmerica Chicago

7470A
Basis Basis Description T Total/NA



### Page 2 of 2 7470A 

## 01/03/2013 Page 290 of 383

### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/18/12 15:00 12/18/12 13:00 173264 Batch Method: TestAmerica Chicago

7470A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 25 mL 25 mL MB 500-173264/7 7470A, 7470A 25 mL 25 mL 0.00005 mL LCS 500-173264/8 7470A, 7470A 25 mL 25 mL LB 500-173187/1-A 7470A, 7470A FC COMPOSITE 4 25 mL 25 mL 500-53315-A-1-G 7470A, 7470A P FC D COMPOSITE 4 25 mL 25 mL 500-53315-A-2-C 7470A, 7470A P
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 6 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 88 Oven, Bath or Block Temperature 2 88 Pipette ID 2240 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Temperature 88 Celsius ID number of the thermometer hb305412 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Visual ck - digestate F.V. consistency OK
Basis Basis Description P TCLP 

### Page 1 of 1 7470A 

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### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/17/12 14:30 12/17/12 14:00 173153 Batch Method: TestAmerica Chicago

7471A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount M11FSTKHG 00001 0.6 g 50 mL MB 500-173153/7 7471A, 7471A 0.6 g 50 mL 0.0001 mL LCS 500-173153/8 7471A, 7471A FC COMPOSITE 4 0.6494 g 50 mL 500-53315-A-1 7471A, 7471A T FC D COMPOSITE 4 0.6068 g 50 mL 500-53315-A-2 7471A, 7471A T
Batch Notes Hydroxylamine Hydrochloride Lot 19333 Balance ID c0975 Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 (Curve) Blank Soil Lot Number teflon strip_00001 Filter Lot # 21782182 Sulfuric Acid Lot Number k20042 Lot # of hydrochloric acid 0000007153 Lot # of Nitric Acid L03021 Hood ID or number c0454 Hot Block ID number 2 Potassium Persulfate Lot Number k43467 Potassium Permanganate Lot Number k35621 NaCL Lot # UF30BZEMS Oven, Bath or Block Temperature 1 90 Oven, Bath or Block Temperature 2 90 Pipette ID 1631 Repittetor Volume Check OK Stannous Chloride Lot Number k21597 Syringe Lot # 1292669 ID number of the thermometer j60025 Digestion Tube/Cup Lot # 1207143 Uncorrected Temperature 90 Celsius Uncorrected Temperature 2 90 Celsius



### Page 1 of 2 7471A 

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### Lab Name: Job No.: SDG No.: METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Bills, Brandon J 12/17/12 14:30 12/17/12 14:00 173153 Batch Method: TestAmerica Chicago

7471A
Basis Basis Description T Total/NA



### Page 2 of 2 7471A 

## 01/03/2013 Page 293 of 383

# GENERAL CHEMISTRY

01/03/2013 Page 294 of 383

### COVER PAGE

Lab Name: Job Number:

Client Sample ID Lab Sample ID GENERAL CHEMISTRY

Project:John Deere Des Moines Works (JDDMW) SDG No.: 500-53315-1 TestAmerica Chicago

500-53315-1 FC COMPOSITE 4 500-53315-2 FC D COMPOSITE 4 500-53315-3 FC DISCRETE 4 500-53315-4 FC D DISCRETE 4 500-53315-6 FC EB 4

Comments:



## 01/03/2013 Page 295 of 383

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10 500-53315-1 FC COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: DRY 

### GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 25.9

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent 3.97 mg/Kg 3.85 1.50 1 7196A 57-12-5 Cyanide, Total 0.745 J mg/Kg B 1.91 0.630 1 9014 18496-25-8 Sulfide 739 mg/Kg 93.3 14.9 1 9034 HEM (Oil & Grease) 11100 mg/Kg 1880 835 1 9071B



### FORM IB-IN 

## 01/03/2013 Page 296 of 383

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10 500-53315-1 FC COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result Sulfide, Reactive <48.6 mg/Kg 48.6 3.79 1 9034 Flashpoint >176 Degrees F 40.0 40.0 1 1010 pH 9.50 SU 0.200 0.200 1 9045C % Moisture 74.0 % 0.100 0.100 1 SM 2540G Total Solids 26.0 % 0.100 0.100 1 SM 2540G



### FORM IB-IN 

## 01/03/2013 Page 297 of 383

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10 500-53315-1 FC D COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: DRY 

### GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 26.3

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent 4.08 mg/Kg 3.76 1.46 1 7196A 57-12-5 Cyanide, Total 0.765 J mg/Kg B 1.66 0.549 1 9014 18496-25-8 Sulfide 774 mg/Kg 90.8 14.5 1 9034 HEM (Oil & Grease) 8910 mg/Kg 1830 811 1 9071B



### FORM IB-IN 

## 01/03/2013 Page 298 of 383

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10 500-53315-1 FC D COMPOSITE 4

Solid 12/14/2012 15:15 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result Sulfide, Reactive <49.3 mg/Kg 49.3 3.85 1 9034 Flashpoint >176 Degrees F 40.0 40.0 1 1010 pH 9.58 SU 0.200 0.200 1 9045C % Moisture 74.0 % 0.100 0.100 1 SM 2540G Total Solids 26.0 % 0.100 0.100 1 SM 2540G



### FORM IB-IN 

## 01/03/2013 Page 299 of 383

### 1B-IN INORGANIC ANALYSIS DATA SHEET

Client Sample ID: Lab Name: Job No.: SDG ID.: Matrix: Lab Sample ID: 500-53315-6

Date Received: 12/15/2012 09:10 500-53315-1 FC EB 4

Water 12/14/2012 14:30 Date Sampled: Reporting Basis: WET 

### GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte C Units Q Method RL MDL DIL Result
18540-29-9 Chromium, hexavalent <0.0100 mg/L 0.0100 0.00325 1 7196A 57-12-5 Cyanide, Total <0.0100 mg/L 0.0100 0.00331 1 9014 Sulfide, Reactive <1.00 mg/L 1.00 1.00 1 9034 HEM (Oil & Grease) <5.20 mg/L 5.20 1.51 1 1664A 18496-25-8 Sulfide <1.00 mg/L 1.00 0.230 1 9034



### FORM IB-IN 

## 01/03/2013 Page 300 of 383

### 2-IN

Lab Name: Job No.: SDG No.: 500-53315-1
Analyst:APW Batch Start Date: 12/15/2012 Reporting Units:mg/L Analytical Batch No.: 173079 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 13:20 Chromium, hexavalent 0.2500 0.250 100 90-110 WSTCR2_00008 1ICB 13:20 Chromium, hexavalent <0.0100 2CCV 13:23 Chromium, hexavalent 0.4943 0.500 99 90-110 WSTCR1_00008 8CCB 13:24 Chromium, hexavalent <0.0100 9



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 301 of 383

### 2-IN

Lab Name: Job No.: SDG No.: 500-53315-1
Analyst:APW Batch Start Date: 12/18/2012 Reporting Units:mg/L Analytical Batch No.: 173341 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 15:45 Chromium, hexavalent 0.2699 0.250 108 90-110 WSTCR2_00008 1ICB 15:45 Chromium, hexavalent <0.0200 2CCV 15:50 Chromium, hexavalent 0.5250 0.500 105 90-110 WSTCR1_00008 10CCB 15:51 Chromium, hexavalent <0.0200 11



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 302 of 383

### 2-IN

Lab Name: Job No.: SDG No.: 500-53315-1
Analyst:EAT Batch Start Date: 12/18/2012 Reporting Units:mg/L Analytical Batch No.: 173386 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 14:23 Cyanide, Total 0.09250 0.100 93 90-110 WSTINCN2_00559 1ICB 14:23 Cyanide, Total <0.0100 2CCV 14:26 Cyanide, Total 0.1913 0.200 96 90-110 WSTINCN1_00567 13CCB 14:27 Cyanide, Total <0.0100 14



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 303 of 383

### 2-IN

Lab Name: Job No.: SDG No.: 500-53315-1
Analyst:EAT Batch Start Date: 12/18/2012 Reporting Units:mg/L Analytical Batch No.: 173387 CALIBRATION QUALITY CONTROL GENERAL CHEMISTRY

Sample NumberQC Type Time Analyte Result Spike Amount(%) Recovery Limits Qual Reagent 

### TestAmerica Chicago

ICV 13:45 Cyanide, Total 0.1041 0.100 104 90-110 WSTINCN2_00559 1ICB 13:45 Cyanide, Total <0.0100 2CCV 13:48 Cyanide, Total 0.1929 0.200 96 90-110 WSTINCN1_00567 13CCB 13:49 Cyanide, Total <0.0100 14CCV 13:52 Cyanide, Total 0.1927 0.200 96 90-110 WSTINCN1_00567 25CCB 13:52 Cyanide, Total <0.0100 26CCV 13:54 Cyanide, Total 0.1924 0.200 96 90-110 WSTINCN1_00567 31CCB 13:54 Cyanide, Total <0.0100 32



### FORM II-IN Note! Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 304 of 383

### Lab Name: Job No.: SDG No.:

Method Analyte ResultQual Dil 

### 3-IN

500-53315-1

Lab Sample ID Units 

### TestAmerica Chicago METHOD BLANK GENERAL CHEMISTRY

RL
Batch ID:173178 Date:12/18/2012 10:05 173173 Date:12/18/2012 05:25 Prep Batch: <5.00 MB 500-173173/1-A 1 5.00 mg/L HEM (Oil & Grease) 1664A Batch ID:173079 Date:12/15/2012 13:21 <0.0100 MB 500-173079/3 1 0.0100 mg/L Chromium, hexavalent 7196A Batch ID:173341 Date:12/18/2012 15:46 173258 Date:12/18/2012 10:00 Prep Batch: <1.00 MB 500-173258/1-A 1 1.00 mg/Kg Chromium, hexavalent 7196A Batch ID:173387 Date:12/18/2012 13:45 173245 Date:12/18/2012 08:30 Prep Batch:<0.0100 MB 500-173245/1-A 1 0.0100 mg/L Cyanide, Total 9014 Batch ID:173386 Date:12/18/2012 14:23 173250 Date:12/18/2012 10:35 Prep Batch:0.1850 MB 500-173250/1-A J 1 0.500 mg/Kg Cyanide, Total 9014 Batch ID:173107 Date:12/17/2012 00:19 173106 Date:12/17/2012 00:01 Prep Batch: <1.00 MB 500-173106/1-A 1 1.00 mg/L Sulfide, Reactive 9034 Batch ID:173108 Date:12/17/2012 00:19 <1.00 MB 500-173108/1 1 1.00 mg/L Sulfide 9034 Batch ID:173472 Date:12/19/2012 12:15 173290 Date:12/19/2012 10:05 Prep Batch: <50.0 MB 500-173290/1-A 1 50.0 mg/Kg Sulfide, Reactive 9034 Batch ID:173474 Date:12/19/2012 13:35 173291 Date:12/19/2012 11:25 Prep Batch: <25.0 MB 500-173291/1-A 1 25.0 mg/Kg Sulfide 9034 Batch ID:173330 Date:12/19/2012 09:20 173324 Date:12/19/2012 05:10 Prep Batch: <500 MB 500-173324/1-A 1 500 mg/Kg HEM (Oil & Grease) 9071B



### FORM III-IN 

## 01/03/2013 Page 305 of 383

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53315-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Solid 5-IN MATRIX SPIKE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173386 Date:12/18/2012 14:25 Prep Batch:173250 Date:12/18/2012 10:35 Cyanide, Total 9014 mg/Kg 0.765 500-53315-2 B J 9014 500-53315-2 MS Cyanide, Total 6.130 mg/Kg 6.63 75-125 81



### FORM V-IN Note - Results and Reporting Limits have been adjusted for dry weight. Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 306 of 383

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53315-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Water 5-IN MATRIX SPIKE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173079 Date:12/15/2012 13:22 Chromium, hexavalent 7196A mg/L <0.0100 500-53315-6 7196A 500-53315-6 MS Chromium, hexavalent 0.2500 mg/L 0.250 85-115 100



### FORM V-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 307 of 383

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53315-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Solid 5-IN MATRIX SPIKE DUPLICATE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173386 Date:12/18/2012 14:25 Prep Batch:173250 Date:12/18/2012 10:35 9014 500-53315-2 MSD Cyanide, Total 6.651 mg/Kg 6.62 89 75-125 8 20



### FORM V-IN Note - Results and Reporting Limits have been adjusted for dry weight. Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 308 of 383

### Lab Name: Job No.: SDG No.: Matrix:

Analyte 

### 500-53315-1

Method Lab Sample ID Result Unit Spike Amount Pct. Rec. Limits C RPD RPD Limit Q 

### Water 5-IN MATRIX SPIKE DUPLICATE SAMPLE RECOVERY GENERAL CHEMISTRY
TestAmerica Chicago

Batch ID:173079 Date:12/15/2012 13:23 7196A 500-53315-6 MSD Chromium, hexavalent 0.2500 mg/L 0.250 100 85-115 0 20



### FORM V-IN Calculations are performed before rounding to avoid round-off errors in calculated results.



## 01/03/2013 Page 309 of 383

### 7A-IN

Job No.:500-53315-1 LAB CONTROL SAMPLE GENERAL CHEMISTRY

Lab Name: SDG No.:

Q RPD Limit RPD Limits Pct. Rec. Spike Amount Unit C Result Analyte Lab Sample ID Method 

### Matrix:Solid TestAmerica Chicago

Batch ID:173341 Date:12/18/2012 15:46 173258 Date:12/18/2012 10:00 Prep Batch: LCS Source: WSTCR2_00008 10.0 83 7196A LCS 500-173258/2- A Chromium, hexavalent 8.252 mg/Kg 80-120

Batch ID:173341 Date:12/18/2012 15:47 173258 Date:12/18/2012 10:00 Prep Batch: LCS Source: WSTCR13_00623 1550 104 7196A LCS 500-173258/3- A Chromium, hexavalent 1601 mg/Kg 80-120

Batch ID:173386 Date:12/18/2012 14:23 173250 Date:12/18/2012 10:35 Prep Batch: LCS Source: WSTINCN2_00559 5.00 105 9014 LCS 500-173250/2- A Cyanide, Total 5.235 mg/Kg 80-120

Batch ID:173472 Date:12/19/2012 12:15 173290 Date:12/19/2012 10:10 Prep Batch: LCS Source: WSTSF1_00036 180 94 9034 LCS 500-173290/2- A Sulfide, Reactive 168.6 mg/Kg 80-120

Batch ID:173474 Date:12/19/2012 13:35 173291 Date:12/19/2012 11:25 Prep Batch: LCS Source: WSTSF1_00036 180 93 9034 LCS 500-173291/2- A Sulfide 168.3 mg/Kg 80-120

Batch ID:173330 Date:12/19/2012 09:31 173324 Date:12/19/2012 05:10 Prep Batch: LCS Source: 1664 HEM_00060 4000 102 9071B LCS 500-173324/2- A HEM (Oil & Grease) 4090 mg/Kg 80-120



### FORM VIIA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 310 of 383

### 7A-IN

Job No.:500-53315-1 LAB CONTROL SAMPLE GENERAL CHEMISTRY

Lab Name: SDG No.:

Q RPD Limit RPD Limits Pct. Rec. Spike Amount Unit C Result Analyte Lab Sample ID Method 

### Matrix:Water TestAmerica Chicago

Batch ID:173178 Date:12/18/2012 10:11 173173 Date:12/18/2012 05:35 Prep Batch: LCS Source: 1664 HEM_00060 40.0 98 1664A LCS 500-173173/2- A HEM (Oil & Grease) 39.10 mg/L 78-114

Batch ID:173079 Date:12/15/2012 13:21 LCS Source: WSTCR2_00008 0.250 100 7196A LCS 500-173079/4 Chromium, hexavalent 0.2497 mg/L 85-115 Batch ID:173387 Date:12/18/2012 13:45 173245 Date:12/18/2012 08:30 Prep Batch: LCS Source: WSTINCN2_00559 0.100 106 9014 LCS 500-173245/2- A Cyanide, Total 0.1057 mg/L 80-120

Batch ID:173108 Date:12/17/2012 00:21 LCS Source: WSTSF1_00036 3.60 91 9034 LCS 500-173108/2 Sulfide 3.286 mg/L 80-120 Batch ID:173107 Date:12/17/2012 00:35 173106 Date:12/17/2012 00:05 Prep Batch: LCS Source: WSTSF1_00036 3.60 91 9034 LCS 500-173106/2- A Sulfide, Reactive 3.292 mg/L 80-120



### FORM VIIA-IN Calculations are performed before rounding to avoid round-off errors in calculated results.


## 01/03/2013 Page 311 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

7196A MDL Date: 05/29/2012 10:43 Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.01

FORM IX - IN 

## 01/03/2013 Page 312 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7196A XMDL Date: 05/29/2012 10:44 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.01

FORM IX - IN 

## 01/03/2013 Page 313 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

7196A MDL Date: 05/29/2012 14:44 Method: 3060A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Chromium, hexavalent 0.389 1

FORM IX - IN 

## 01/03/2013 Page 314 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

7196A XMDL Date: 05/29/2012 10:45 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Chromium, hexavalent 0.00325 0.02

FORM IX - IN 

## 01/03/2013 Page 315 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9014 MDL Date: 06/18/2012 16:18 Method: 9010B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Cyanide, Total 0.165 0.5

FORM IX - IN 

## 01/03/2013 Page 316 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

9014 XMDL Date: 06/18/2012 16:19 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/03/2013 Page 317 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9014 MDL Date: 06/18/2012 16:22 Method: 9010B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/03/2013 Page 318 of 383

### 9-IN

Instrument ID:SPEC5 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica ChicagoCALIBRATION BLANK DETECTION LIMITS

9014 XMDL Date: 06/18/2012 16:22 Method: Analyte Wavelength/ Mass XRL XMDL (mg/L) (mg/L) Cyanide, Total 0.00331 0.01

FORM IX - IN 

## 01/03/2013 Page 319 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 16:25 Method: 7.3.4 Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Sulfide, Reactive 3.9 50

FORM IX - IN 

## 01/03/2013 Page 320 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 01/02/2006 09:18 Method: 7.3.4 Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Sulfide, Reactive 1 1

FORM IX - IN 

## 01/03/2013 Page 321 of 383

### 9-IN

Instrument ID:FP4 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

1010 MDL Date: 11/11/2005 10:25 Method: Analyte Wavelength/ Mass RL MDL (Degrees (Degrees F) Flashpoint 40 40

FORM IX - IN 

## 01/03/2013 Page 322 of 383

### 9-IN

Instrument ID:NoEquip 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

1664A MDL Date: 05/29/2012 15:22 Method: 1664A Prep Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) HEM (Oil & Grease) 1.45 5

FORM IX - IN 

## 01/03/2013 Page 323 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Water Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 15:57 Method: Analyte Wavelength/ Mass RL MDL (mg/L) (mg/L) Sulfide 0.23 1

FORM IX - IN 

## 01/03/2013 Page 324 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9034 MDL Date: 05/29/2012 15:59 Method: 9030B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) Sulfide 4 25

FORM IX - IN 

## 01/03/2013 Page 325 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9045C MDL Date: 11/01/2005 06:06 Method: Analyte Wavelength/ Mass RL MDL (SU) (SU) pH 0.2 0.2

FORM IX - IN 

## 01/03/2013 Page 326 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

9071B MDL Date: 05/29/2012 15:24 Method: 9071B Prep Method: Analyte Wavelength/ Mass RL MDL (mg/Kg) (mg/Kg) HEM (Oil & Grease) 222 500

FORM IX - IN 

## 01/03/2013 Page 327 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

Moisture MDL Date: 11/01/2005 09:02 Method: Analyte Wavelength/ Mass RL MDL (%) (%) Percent Moisture 0.1 0.1 Percent Solids 0.1 0.1

FORM IX - IN 

## 01/03/2013 Page 328 of 383

### 9-IN

Instrument ID:NOEQUIP 500-53315-1 Job Number:

Solid Matrix: SDG Number: Lab Name: GENERAL CHEMISTRY
TestAmerica Chicago DETECTION LIMITS

SM 2540G MDL Date: 11/01/2005 09:02 Method: Analyte Wavelength/ Mass RL MDL (%) (%) % Moisture 0.1 0.1 Total Solids 0.1 0.1

FORM IX - IN 

## 01/03/2013 Page 329 of 383

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53315-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

SPEC5 SDG No.:

(mg/L) 05/03/2010 07:21 GENERAL CHEMISTRY

Chromium, hexavalent 0.57196A Cyanide, Total 0.4009014

FORM XI - IN 

## 01/03/2013 Page 330 of 383

### 11-IN

Lab Name:TestAmerica Chicago Job No:500-53315-1

Instrument ID: Date:

Analyte Integ. Time (Sec.) Concentration Method LINEAR RANGES

SPEC5 SDG No.:

(mg/L) 05/03/2010 07:27 GENERAL CHEMISTRY

Chromium, hexavalent 1.07196A

FORM XI - IN 

## 01/03/2013 Page 331 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:7.3.4
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/17/2012 00:01 173106 MB 500-173106/1-A 250 250 12/17/2012 00:05 173106 LCS 500-173106/2-A 250 250 12/17/2012 00:13 173106 500-53315-6 250 250

FORM XII-IN 

## 01/03/2013 Page 332 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9010B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/18/2012 08:30 173245 MB 500-173245/1-A 50 50 12/18/2012 08:30 173245 LCS 500-173245/2-A 50 50 12/18/2012 08:30 173245 500-53315-6 50 50

FORM XII-IN 

## 01/03/2013 Page 333 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9010B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/18/2012 10:35 173250 MB 500-173250/1-A 50 1.0000 12/18/2012 10:35 173250 LCS 500-173250/2-A 50 1.0000 12/18/2012 10:35 173250 500-53315-1 50 1.0092 12/18/2012 10:35 173250 500-53315-2 50 1.1423 12/18/2012 10:35 173250 500-53315-2 MS 50 1.1473 12/18/2012 10:35 173250 500-53315-2 MSD 50 1.1489

FORM XII-IN 

## 01/03/2013 Page 334 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:3060A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/18/2012 10:00 173258 MB 500-173258/1-A 100 2.5 12/18/2012 10:00 173258 LCS 500-173258/2-A 100 2.5 12/18/2012 10:00 173258 LCS 500-173258/3-A 100 2.5 12/18/2012 10:00 173258 500-53315-1 100 2.5027 12/18/2012 10:00 173258 500-53315-2 100 2.5245

FORM XII-IN 

## 01/03/2013 Page 335 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:7.3.4
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 10:05 173290 MB 500-173290/1-A 10 10.0000 12/19/2012 10:10 173290 LCS 500-173290/2-A 10 10.0000 12/19/2012 10:40 173290 500-53315-1 10 10.2894 12/19/2012 10:45 173290 500-53315-2 10 10.1413

FORM XII-IN 

## 01/03/2013 Page 336 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:1664A
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (mL) (mL) 12/18/2012 05:25 173173 MB 500-173173/1-A 1000 1000 12/18/2012 05:35 173173 LCS 500-173173/2-A 1000 1000 12/18/2012 07:24 173173 500-53315-6 1000 961

FORM XII-IN 

## 01/03/2013 Page 337 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9030B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 11:25 173291 MB 500-173291/1-A 10 10.0000 12/19/2012 11:25 173291 LCS 500-173291/2-A 10 10.0000 12/19/2012 11:25 173291 500-53315-1 10 10.3275 12/19/2012 11:25 173291 500-53315-2 10 10.4669

FORM XII-IN 

## 01/03/2013 Page 338 of 383

### 12-IN PREPARATION LOG

Lab Name: Job No.: SDG No.: 500-53315-1 GENERAL CHEMISTRY
TestAmerica Chicago
Prep Method:9071B
Lab Sample ID Preparation Date Initial Weight Final Volume Prep Batch Initial Volume (g) (mL) 12/19/2012 05:10 173324 MB 500-173324/1-A 10 10 12/19/2012 05:10 173324 LCS 500-173324/2-A 10 10 12/19/2012 05:10 173324 500-53315-1 10 10.2484 12/19/2012 05:10 173324 500-53315-2 10 10.4122

FORM XII-IN 

## 01/03/2013 Page 339 of 383

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

SPEC5 12/15/2012 13:20 12/15/2012 13:24 7196A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C r 6 T y p e 1 13:20 X ICV 500-173079/1 1 13:20 X ICB 500-173079/2 1 13:21 X MB 500-173079/3 T 1 13:21 X LCS 500-173079/4 T 1 13:22 X 500-53315-6 T 1 13:22 X 500-53315-6 MS T 1 13:23 X 500-53315-6 MSD T 1 13:23 X CCV 500-173079/8 1 13:24 X CCB 500-173079/9 13:24 ZZZZZZ Prep Types T = Total/NA



### FORM XIII-IN 

## 01/03/2013 Page 340 of 383

### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

SPEC5 12/18/2012 15:45 12/18/2012 15:59 7196A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C r 6 T y p e 1 15:45 X ICV 500-173341/1 1 15:45 X ICB 500-173341/2 1 15:46 X MB 500-173258/1-A T 1 15:46 X LCS 500-173258/2-A T 50 15:47 X LCS 500-173258/3-A T 15:48 ZZZZZZ 15:48 ZZZZZZ 1 15:49 X 500-53315-1 T 1 15:50 X 500-53315-2 T 1 15:50 X CCV 500-173341/10 1 15:51 X CCB 500-173341/11 15:52 ZZZZZZ 15:52 ZZZZZZ 15:53 ZZZZZZ 15:54 ZZZZZZ 15:54 ZZZZZZ 15:55 ZZZZZZ 15:56 ZZZZZZ 15:56 CCV 500-173341/19 15:57 CCB 500-173341/20 15:58 ZZZZZZ 15:58 CCV 500-173341/22 15:59 CCB 500-173341/23 Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

SPEC5 12/18/2012 13:45 12/18/2012 13:54 9014 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C N T y p e 1 13:45 X ICV 500-173387/1 1 13:45 X ICB 500-173387/2 1 13:45 X MB 500-173245/1-A T 1 13:45 X LCS 500-173245/2-A T 13:46 ZZZZZZ 13:46 ZZZZZZ 13:46 ZZZZZZ 13:47 ZZZZZZ 13:47 ZZZZZZ 13:47 ZZZZZZ 13:48 ZZZZZZ 13:48 ZZZZZZ 1 13:48 X CCV 500-173387/13 1 13:49 X CCB 500-173387/14 13:49 ZZZZZZ 13:49 ZZZZZZ 13:50 ZZZZZZ 13:50 ZZZZZZ 13:50 ZZZZZZ 13:50 ZZZZZZ 13:51 ZZZZZZ 13:51 ZZZZZZ 13:51 ZZZZZZ 13:52 ZZZZZZ 1 13:52 X CCV 500-173387/25 1 13:52 X CCB 500-173387/26 13:53 ZZZZZZ 13:53 ZZZZZZ 13:53 ZZZZZZ 1 13:54 X 500-53315-6 T 1 13:54 X CCV 500-173387/31 1 13:54 X CCB 500-173387/32 Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

SPEC5 12/18/2012 14:23 12/18/2012 14:29 9014 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes C N T y p e 1 14:23 X ICV 500-173386/1 1 14:23 X ICB 500-173386/2 1 14:23 X MB 500-173250/1-A T 1 14:23 X LCS 500-173250/2-A T 14:24 ZZZZZZ 1 14:24 X 500-53315-1 T 1 14:24 X 500-53315-2 T 1 14:25 X 500-53315-2 MS T 1 14:25 X 500-53315-2 MSD T 14:25 ZZZZZZ 14:26 ZZZZZZ 14:26 ZZZZZZ 1 14:26 X CCV 500-173386/13 1 14:27 X CCB 500-173386/14 14:27 ZZZZZZ 14:27 ZZZZZZ 14:28 ZZZZZZ 14:28 ZZZZZZ 14:28 ZZZZZZ 14:29 ZZZZZZ 14:29 CCV 500-173386/21 14:29 CCB 500-173386/22 Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/17/2012 00:19 12/17/2012 01:08 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 R e a c T y p e 1 00:19 X MB 500-173106/1-A T 1 00:35 X LCS 500-173106/2-A T 00:52 ZZZZZZ 1 01:08 X 500-53315-6 T Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/19/2012 12:15 12/19/2012 12:24 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 R e a c T y p e 1 12:15 X MB 500-173290/1-A T 1 12:15 X LCS 500-173290/2-A T 12:16 ZZZZZZ 12:17 ZZZZZZ 12:17 ZZZZZZ 1 12:18 X 500-53315-1 T 1 12:19 X 500-53315-2 T 12:19 ZZZZZZ 12:20 ZZZZZZ 12:21 ZZZZZZ 12:22 ZZZZZZ 12:22 ZZZZZZ 12:23 ZZZZZZ 12:24 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

FP4 12/19/2012 14:45 12/19/2012 18:00 1010 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes F P T y p e 14:45 ZZZZZZ 15:24 ZZZZZZ 16:03 ZZZZZZ 16:42 ZZZZZZ 1 17:21 X 500-53315-1 T 1 18:00 X 500-53315-2 T Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1
NoEquip 12/18/2012 10:05 12/18/2012 12:23 1664A GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes H E M T y p e 1 10:05 X MB 500-173173/1-A T 1 10:11 X LCS 500-173173/2-A T 10:17 ZZZZZZ 10:23 ZZZZZZ 10:30 ZZZZZZ 10:36 ZZZZZZ 10:42 ZZZZZZ 10:49 ZZZZZZ 10:55 ZZZZZZ 11:01 ZZZZZZ 11:08 ZZZZZZ 1 11:14 X 500-53315-6 T 11:20 ZZZZZZ 11:26 ZZZZZZ 11:33 ZZZZZZ 11:39 ZZZZZZ 11:45 ZZZZZZ 11:52 ZZZZZZ 11:58 ZZZZZZ 12:04 ZZZZZZ 12:11 ZZZZZZ 12:17 ZZZZZZ 12:23 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/17/2012 00:19 12/17/2012 01:22 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 T y p e 1 00:19 X MB 500-173108/1 T 1 00:21 X LCS 500-173108/2 T 00:24 ZZZZZZ 00:27 ZZZZZZ 00:30 ZZZZZZ 00:32 ZZZZZZ 00:35 ZZZZZZ 00:38 ZZZZZZ 00:41 ZZZZZZ 00:43 ZZZZZZ 00:46 ZZZZZZ 00:49 ZZZZZZ 00:52 ZZZZZZ 00:54 ZZZZZZ 00:57 ZZZZZZ 01:00 ZZZZZZ 01:03 ZZZZZZ 01:05 ZZZZZZ 01:08 ZZZZZZ 1 01:11 X 500-53315-6 T 01:14 ZZZZZZ 01:16 ZZZZZZ 01:19 ZZZZZZ 01:22 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/19/2012 13:35 12/19/2012 13:39 9034 GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes S 2 T y p e 1 13:35 X MB 500-173291/1-A T 1 13:35 X LCS 500-173291/2-A T 13:36 ZZZZZZ 1 13:36 X 500-53315-1 T 1 13:37 X 500-53315-2 T 13:38 ZZZZZZ 13:38 ZZZZZZ 13:39 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/19/2012 13:35 12/20/2012 17:10 9045C GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes p H T y p e 13:35 ZZZZZZ 13:41 ZZZZZZ 13:47 ZZZZZZ 13:53 ZZZZZZ 13:59 ZZZZZZ 18:30 ZZZZZZ 19:29 ZZZZZZ 20:28 ZZZZZZ 21:28 ZZZZZZ 22:27 ZZZZZZ 23:26 ZZZZZZ 00:25 ZZZZZZ 01:24 ZZZZZZ 02:23 ZZZZZZ 03:22 ZZZZZZ 04:22 ZZZZZZ 05:21 ZZZZZZ 06:20 ZZZZZZ 07:19 ZZZZZZ 08:18 ZZZZZZ 09:17 ZZZZZZ 10:16 ZZZZZZ 11:16 ZZZZZZ 12:15 ZZZZZZ 13:14 ZZZZZZ 14:13 ZZZZZZ 1 15:12 X 500-53315-1 T 1 16:11 X 500-53315-2 T 17:10 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/19/2012 09:20 12/19/2012 11:23 9071B GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes H E M T y p e 1 09:20 X MB 500-173324/1-A T 1 09:31 X LCS 500-173324/2-A T 09:42 ZZZZZZ 09:53 ZZZZZZ 10:05 ZZZZZZ 10:16 ZZZZZZ 10:27 ZZZZZZ 10:38 ZZZZZZ 10:50 ZZZZZZ 1 11:01 X 500-53315-1 T 1 11:12 X 500-53315-2 T 11:23 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/15/2012 12:43 12/15/2012 12:43 Moisture GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes % S o lM o i s t T y p e 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 12:43 ZZZZZZ 1 12:43 XX 500-53315-1 T 1 12:43 XX 500-53315-2 T Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/18/2012 12:44 12/18/2012 14:38 Moisture GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes % S o lM o i s t T y p e 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 12:44 ZZZZZZ 1 13:59 XX 500-53315-3 T 1 13:59 XX 500-53315-4 T 14:12 ZZZZZZ 14:12 ZZZZZZ 14:12 ZZZZZZ 14:12 ZZZZZZ 14:12 ZZZZZZ 14:12 ZZZZZZ 14:12 ZZZZZZ 14:12 ZZZZZZ 14:26 ZZZZZZ 14:26 ZZZZZZ 14:26 ZZZZZZ 14:38 ZZZZZZ Prep Types T = Total/NA



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### 13-IN ANALYSIS RUN LOG

Lab Name: Job No.: SDG No.: Instrument ID: Method: Start Date: End Date: TestAmerica Chicago 500-53315-1

NOEQUIP 12/18/2012 07:34 12/18/2012 07:34 SM 2540G GENERAL CHEMISTRY

Lab Sample ID D / F Time 

### Analytes M o i s tT S T y p e 1 07:34 XX 500-53315-1 T 1 07:34 XX 500-53315-2 T Prep Types T = Total/NA



### FORM XIII-IN 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/15/12 13:25 12/15/12 13:20 173079 Batch Method: TestAmerica Chicago

7196A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008 100 mL 100 mL Color Resp. is Blank 25 uL ICV 500-173079/1 7196A Color Resp. is Blank ICB 500-173079/2 7196A Color Resp. is Blank MB 500-173079/3 7196A 100 mL 100 mL Color Resp. is Blank 25 uL LCS 500-173079/4 7196A FC EB 4 Color Resp. is Blank 500-53315-F-6 7196A T FC EB 4 100 mL 100 mL Color Resp. is Blank 25 uL 500-53315-F-6 MS 7196A T FC EB 4 100 mL 100 mL Color Resp. is Blank 25 uL 500-53315-F-6 MSD 7196A T 100 mL 100 mL Color Resp. is Blank 50 uL CCV 500-173079/8 7196A Color Resp. is Blank CCB 500-173079/9 7196A

Batch Notes Batch Comment filter paper lot# 100232 Spectrophotometer Cell Path Length 540NM1CM cm Color Reagent ID Number Hexa Chrome Color Reagent-00007 First End time See Start Date/Time First Start time See Start Date/Time Sulfuric Acid Reagent ID Number H2SO4 00007
Basis Basis Description T Total/NA



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500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/18/12 11:00 12/18/12 10:00 173258 Batch Method: TestAmerica Chicago

3060A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount Initial pH Final pH WSTCR13 00623 WSTCR2 00008 2.5 g 100 mL 13 SU 7.5 SU MB 500-173258/1 3060A, 7196A 2.5 g 100 mL 13 SU 7.5 SU 25 uL LCS 500-173258/2 3060A, 7196A 2.5 g 100 mL 13 SU 7.5 SU 100 mL LCS 500-173258/3 3060A, 7196A FC COMPOSITE 4 2.5027 g 100 mL 13 SU 7.5 SU 500-53315-A-1 3060A, 7196A T FC D COMPOSITE 4 2.5245 g 100 mL 13 SU 7.5 SU 500-53315-A-2 3060A, 7196A T Lab Sample ID Client Sample IDMethod ChainBasisAnalysisComment MB 500-173258/1 3060A, 7196A soluble LCS 500-173258/2 3060A, 7196A insoluble 0.0240 LCS 500-173258/3 3060A, 7196A FC COMPOSITE 4 500-53315-A-1 3060A, 7196A T FC D COMPOSITE 4 500-53315-A-2 3060A, 7196A T
Batch Notes Alkaline Digestion Solution Reagent ID CR6digestion_00028 Batch Comment Filter Paper Lot # 100727 First End time see above Potassium Chromate Lot # K00741 Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002 Lead Chromate Lot # 15813PE Lead Chromate Vendor ID Lead(II)Chrom_00001 Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002) Magnesium Chloride Vendor JT Baker First Start time see above Ending Temperature 90 Celsius Starting Temperature 90 Celsius
Basis Basis Description T Total/NA 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/18/12 16:00 12/18/12 15:45 173341 Batch Method: TestAmerica Chicago

7196A Lab Sample ID Client Sample IDMethod ChainBasis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008 100 mL Color Resp. is Blank 25 uL ICV 500-173341/1 7196A Color Resp. is Blank ICB 500-173341/2 7196A Color Resp. is Blank MB 500-173258/1-A 7196A Color Resp. is Blank LCS 500-173258/2-A 7196A Color Resp. is Blank LCS 500-173258/3-A 7196A FC COMPOSITE 4 Color Resp. is Blank 500-53315-A-1-I 7196A T FC D COMPOSITE 4 Color Resp. is Blank 500-53315-A-2-G 7196A T 100 mL Color Resp. is Blank 50 uL CCV 500-173341/10 7196A Color Resp. is Blank CCB 500-173341/11 7196A

Batch Notes Spectrophotometer Cell Path Length 540NM1CM cm Color Reagent ID Number CR+6 ColorRGT_00007 Sulfuric Acid Reagent ID Number H2SO4_00007
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/18/12 10:00 12/18/12 08:30 173245 Batch Method: TestAmerica Chicago

9010B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount SulfideCheck WSTINCN2 00559 50 mL 50 mL y MB 500-173245/1 9010B, 9014 50 mL 50 mL y 500 uL LCS 500-173245/2 9010B, 9014 FC EB 4 50 mL 50 mL y 500-53315-D-6 9010B, 9014 T
Batch Notes Bismuth Nitrate Lot # BismuthNO3_00017 Ca(OCl)2 Reagent ID Number CaCL2O2_00006 Distillation Temperature REFLUXING Degrees C KI-Starch Paper Lot # 071409 Lead Acetate Lot # 121109 Methyl Red Indicator Reagent ID Meth_Red_IN_00001 Magnesium Chloride Reagent ID Number MagChloride_00010 NaAsO2 Reagent ID Number AscorbicAcid_00003 Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005 Sulfamic Acid Reagent ID Number SulfamicAcid_00022 Sulfuric Acid Reagent ID Number 50%H2SO4_00007 Zinc Acetate Buffer Reagent ID Number IO8ARCN14
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/18/12 12:05 12/18/12 10:35 173250 Batch Method: TestAmerica Chicago

9010B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount SulfideCheck WSTINCN2 00559 1.0000 g 50 mL y MB 500-173250/1 9010B, 9014 1.0000 g 50 mL y 500 uL LCS 500-173250/2 9010B, 9014 FC COMPOSITE 4 1.0092 g 50 mL y 500-53315-A-1 9010B, 9014 T FC D COMPOSITE 4 1.1423 g 50 mL y 500-53315-A-2 9010B, 9014 T FC D COMPOSITE 4 1.1473 g 50 mL y 200 uL 500-53315-A-2 MS 9010B, 9014 T FC D COMPOSITE 4 1.1489 g 50 mL y 200 uL 500-53315-A-2 MSD 9010B, 9014 T

Batch Notes Bismuth Nitrate Lot # BismuthNO3_00017 Ca(OCl)2 Reagent ID Number CaCL2O2_00006 Distillation Temperature REFLUXING Degrees C KI-Starch Paper Lot # 071409 Lead Acetate Lot # 121109 Methyl Red Indicator Reagent ID Meth_Red_IN_00001 Magnesium Chloride Reagent ID Number MagChloride_00010 NaAsO2 Reagent ID Number AscorbicAcid_00003 Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005 Sulfamic Acid Reagent ID Number SulfamicAcid_00022 Sulfuric Acid Reagent ID Number 50%H2SO4_00007 Zinc Acetate Buffer Reagent ID Number IO8ARCN14
Basis Basis Description T Total/NA



### Page 1 of 1 9014 

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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/18/12 14:30 12/18/12 14:23 173386 Batch Method: TestAmerica Chicago

9014 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTINCN1 00567 WSTINCN2 00559 25 mL 25 mL 250 uL ICV 500-173386/1 9014 25 mL 25 mL 500 uL CCV 500-173386/13 9014

Batch Notes Buffer Reagent ID Number SPMM Buffer_00044 Chloramine-T Reagent ID Number Chloramine-T_00002 KI-Starch Paper Lot # 110510 NaOH Lot # NaOH_00005 Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015 Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022 Scrubber Solution ID NaOH_00005 Sodium Phosphate Solution ID SPMM Buffer_00044 Spectrophotometer Wavelength 578NM
Basis Basis Description



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Treadwell, Eliane A 12/18/12 13:55 12/18/12 13:45 173387 Batch Method: TestAmerica Chicago

9014 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTINCN1 00567 WSTINCN2 00559 25 mL 25 mL 250 uL ICV 500-173387/1 9014 25 mL 25 mL 500 uL CCV 500-173387/13 9014 25 mL 25 mL 500 uL CCV 500-173387/25 9014 25 mL 25 mL 500 uL CCV 500-173387/31 9014

Batch Notes Buffer Reagent ID Number SPMM Buffer_00044 Chloramine-T Reagent ID Number Chloramine-T_00002 KI-Starch Paper Lot # 110510 NaOH Lot # NaOH_00005 Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015 Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022 Scrubber Solution ID NaOH_00005 Sodium Phosphate Solution ID SPMM Buffer_00044 Spectrophotometer Wavelength 578NM
Basis Basis Description



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/17/12 00:18 12/17/12 00:01 173106 Batch Method: TestAmerica Chicago

7.3.4 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount 250 mL 250 mL MB 500-173106/1 7.3.4, 9034 250 mL 250 mL LCS 500-173106/2 7.3.4, 9034 FC EB 4 250 mL 250 mL 500-53315-G-6 7.3.4, 9034 T
Batch Notes

Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/17/12 01:25 12/17/12 00:19 173107 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036 250 mL 5 mL 4.89 mL OK 250 mL MB 500-173106/1-A 9034 250 mL 5 mL 2.73 mL OK 250 mL 5 mL LCS 500-173106/2-A 9034 FC EB 4 250 mL 5 mL 5.25 mL OK 250 mL 500-53315-G-6-A 9034 T
Batch Notes Normality of Iodine Solution 0.0237 N Nominal Amount Used 250 mL Perform Calculation (0=No, 1=Yes) 1 Normality of first Titrant 0.0246 N
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 11:15 12/19/12 10:05 173290 Batch Method: TestAmerica Chicago

7.3.4 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTSF1 00036 10.0000 g 10 mL MB 500-173290/1 7.3.4, 9034 10.0000 g 10 mL 10 mL LCS 500-173290/2 7.3.4, 9034 FC COMPOSITE 4 10.2894 g 10 mL 500-53315-A-1 7.3.4, 9034 T FC D COMPOSITE 4 10.1413 g 10 mL 500-53315-A-2 7.3.4, 9034 T
Batch Notes Batch Comment Balance ID # 2489
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 12:25 12/19/12 12:15 173472 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount 10 mL 5 mL 4.86 mL OK 10 mL MB 500-173290/1-A 9034 10 mL 5 mL 0.44 mL OK 10 mL LCS 500-173290/2-A 9034 FC COMPOSITE 4 10 mL 5 mL 4.72 mL OK 10 mL 500-53315-A-1-K 9034 T FC D COMPOSITE 4 10 mL 5 mL 4.68 mL OK 10 mL 500-53315-A-2-I 9034 T
Batch Notes Normality of Iodine Solution 0.0232 N Nominal Amount Used 10 g Perform Calculation (0=No, 1=Yes) 1 Normality of first Titrant 0.0246 N
Basis Basis Description T Total/NA



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500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Wasowicz, Andrew P 12/19/12 18:40 12/19/12 14:45 173558 Batch Method: TestAmerica Chicago

1010 Lab Sample ID Client Sample IDMethod ChainBasisAnalysisComment FC COMPOSITE 4 gray-brown clay 500-53315-A-1 1010 T FC D COMPOSITE 4 gray-brown clay 500-53315-A-2 1010 T
Batch Notes Equipment ID HFP 339
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/18/12 09:35 12/18/12 05:25 173173 Batch Method: TestAmerica Chicago

1664A Lab Sample ID Client Sample IDMethod ChainBasis GrossWeight TareWeight InitialAmount FinalAmount 1390 g 390 g 1000 mL 1000 mL MB 500-173173/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL LCS 500-173173/2 1664A, 1664A FC EB 4 1351 g 390 g 961 mL 1000 mL 500-53315-H-6 1664A, 1664A T
Batch Notes Batch Comment phase separating filter lot # 6711653 Concentration End Time See end date/time Concentration Start Time See start date/time Person's name who did the concentration See analyst name Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, pf-70610210 Evaporator Temperature 50 DEG. Degrees C Extraction Analyst see analyst name Sulfuric Acid Lot Number MALG35029 Hexane Lot# HEXANES_00012 Manifold ID 1851 Methanol Lot Number Methanol_00007 Na2SO4 Lot Number Na2SO4_00006 Nominal Amount Used 1000 mL Sufficient volume for MS/MSD? NO
Basis Basis Description T Total/NA



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## 01/03/2013 Page 367 of 383

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/18/12 12:30 12/18/12 10:05 173178 Batch Method: TestAmerica Chicago

1664A Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1 RecTubeWExtract 2 1000 mL 1000 mL 01 2.3690 g 2.3699 g 2.3701 g MB 500-173173/1-A 1664A 1000 mL 1000 mL 02 6.2581 g 6.2973 g 6.2972 g LCS 500-173173/2-A 1664A FC EB 4 1000 mL 1000 mL 12 2.3493 g 2.3497 g 2.3496 g 500-53315-H-6-A 1664A T Lab Sample ID Client Sample IDMethod ChainBasis WeightOne%Diff Residue Residue2 1664 HEM 00060 Pass_0.0005g 0.0008999999999 99679 g 0.0010999999999 9966 g MB 500-173173/1-A 1664A Pass_0.0005g 0.0392000000000 001 g 0.0391000000000 004 g 5 mL LCS 500-173173/2-A 1664A FC EB 4 Pass_0.0005g 0.0003999999999 99956 g 0.0003000000000 00189 g 500-53315-H-6-A 1664A T

Batch Notes Balance ID 1634 Calibration Check After 2nd Weighing 0.0021 / 1.0000 g Calibration Check Before 1st Weighing 0.0020 / 0.9999 g Person's name who did the concentration see analyst name Evaporator Temperature 50 Degrees C Hexane Lot# Hexanes_00012 Methanol Lot Number Methanol_00006 Na2SO4 Lot Number Na2SO4_00006 Silica Gel Lot Number Silica gel_00003 (checked in batch 157954 7/31/12) Speedvap ID# 1563 Weight Set ID C-2495, C-1144
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Boyd, Cheryl L 12/17/12 01:25 12/17/12 00:19 173108 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036 4.89 mL 5 mL 250 mL 250 mL OK MB 500-173108/1 9034 2.73 mL 5 mL 250 mL 250 mL OK 5 mL LCS 500-173108/2 9034 FC EB 4 5.25 mL 5 mL 250 mL 250 mL OK 500-53315-G-6 9034 T
Batch Notes First End time 01:25 Iodine Lot Number 0.25NIODINE00005 Iodine Vendor INHOUSE Normality of Iodine Solution 0.0237 N Sodium Thiosulfate Lot Number NO2S2O300008 Sodium Thiosulfate Vendor INHOUSE Nominal Amount Used 250 mL Perform Calculation (0=No, 1=Yes) 1 Starch Lot Number STARCHIND00004 Starch Vendor VWR First Start time 00:19 Sulfuric Acid Reagent ID Number 6NHCL00006 Normality of first Titrant 0.0246 N Titrant Standardization Date 11/21/12
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 12:55 12/19/12 11:25 173291 Batch Method: TestAmerica Chicago

9030B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount WSTSF1 00036 10.0000 g 10 mL MB 500-173291/1 9030B, 9034 10.0000 g 10 mL 10 mL LCS 500-173291/2 9030B, 9034 FC COMPOSITE 4 10.3275 g 10 mL 500-53315-A-1 9030B, 9034 T FC D COMPOSITE 4 10.4669 g 10 mL 500-53315-A-2 9030B, 9034 T
Batch Notes Batch Comment BAlance ID #2489 Distillation Temperature 70 Degrees C Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014 Sulfuric Acid Reagent ID Number 20% H2SO4_00003 Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Moore, Colleen L 12/19/12 13:40 12/19/12 13:35 173474 Batch Method: TestAmerica Chicago

9034 Lab Sample ID Client Sample IDMethod ChainBasis FinalAmount IodineAmount TitrantVolume1 CalcMsg 10 mL 5 mL 4.65 mL OK MB 500-173291/1-A 9034 10 mL 5 mL 0.44 mL OK LCS 500-173291/2-A 9034 FC COMPOSITE 4 10 mL 10 mL 4.40 mL OK 500-53315-A-1-L 9034 T FC D COMPOSITE 4 10 mL 10 mL 4.02 mL OK 500-53315-A-2-J 9034 T
Batch Notes HCl Concentration 6N Lot # of hydrochloric acid 6NHCL00006 Iodine Lot Number 0.25NIODINE00005 Iodine Vendor INHOUSE Normality of Iodine Solution 0.0232 N Sodium Thiosulfate Reagent ID Number NO2S2O300008 Perform Calculation (0=No, 1=Yes) 1 Starch Lot Number STARCHIND00004 Starch Vendor VWR Normality of first Titrant 0.0246 N Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/19/12 07:35 12/19/12 05:10 173324 Batch Method: TestAmerica Chicago

9071B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount 1664 HEM 00060 10 g 10 mL MB 500-173324/1 9071B, 9071B 10 g 10 mL 5 mL LCS 500-173324/2 9071B, 9071B FC COMPOSITE 4 10.2484 g 10 mL 500-53315-A-1 9071B, 9071B T FC D COMPOSITE 4 10.4122 g 10 mL 500-53315-A-2 9071B, 9071B T
Batch Notes Acid used for pH adjust Lot # J23A13 Balance ID 1634 Concentration End Time See end date / time Concentration Start Time See start date / time Evaporator Temperature 50 DEG. C Filter Paper Lot Number 6711653 Hexane Lot# HEXANES_00012 Na2SO4 Lot Number Na2SO4_00006
Basis Basis Description T Total/NA



### Page 1 of 1 9071B 

## 01/03/2013 Page 372 of 383

### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Brogan, Mary T 12/19/12 11:35 12/19/12 09:20 173330 Batch Method: TestAmerica Chicago

9071B Lab Sample ID Client Sample IDMethod ChainBasis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1 RecTubeWExtract 2 10 mL 10 mL 24 2.3781 g 2.3790 g 2.3791 g MB 500-173324/1-A 9071B 10 mL 10 mL 25 2.3332 g 2.3745 g 2.3741 g LCS 500-173324/2-A 9071B FC COMPOSITE 4 10 mL 10 mL 33 2.2879 g 2.3174 g 2.3174 g 500-53315-A-1-M 9071B T FC D COMPOSITE 4 10 mL 10 mL 34 2.3277 g 2.3522 g 2.3521 g 500-53315-A-2-K 9071B T Lab Sample ID Client Sample IDMethod ChainBasis WeightOne%Diff Residue Residue2 Pass_0.0005g 0.0009000000000 00123 g 0.0010000000000 0033 g MB 500-173324/1-A 9071B Pass_0.0005g 0.0412999999999 997 g 0.0408999999999 997 g LCS 500-173324/2-A 9071B FC COMPOSITE 4 Pass_0.0005g 0.0295000000000 001 g 0.0295000000000 001 g 500-53315-A-1-M 9071B T FC D COMPOSITE 4 Pass_0.0005g 0.0244999999999 997 g 0.0244 g 500-53315-A-2-K 9071B T

Batch Notes Balance ID 1634 Calibration Check After 2nd Weighing 0.0019 / 0.9999 Calibration Check Before 1st Weighing 0.0019 / 0.9999 Evaporator Temperature 50 Celsius Filter Paper Lot # 6711653
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/15/12 12:43 173077 Batch Method: TestAmerica Chicago

Moisture Lab Sample ID Client Sample IDMethod ChainBasis DISH# DishWeight SampleMassWet SampleMassDry FC COMPOSITE 4 13 33.86 g 44.15 g 36.53 g 500-53315-A-1 Moisture T FC D COMPOSITE 4 14 41.36 g 51.51 g 44.03 g 500-53315-A-2 Moisture T
Batch Notes Balance ID 971 No Unit Date samples were placed in the oven 12/15/12 Oven Temp when samples are put in oven 105 Degrees C Time samples were place in the oven 1300 Date samples were removed from oven 12/17/12 Oven Temp when samples removed from oven 105 Degrees C Time Samples were removed from oven 1450 Oven ID 776 ID number of the thermometer c-1966
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/18/12 12:44 173311 Batch Method: TestAmerica Chicago

Moisture Lab Sample ID Client Sample IDMethod ChainBasis DISH# DishWeight SampleMassWet SampleMassDry FC DISCRETE 4 39 1.27 g 11.43 g 4.21 g 500-53315-A-3 Moisture T FC D DISCRETE 4 40 1.27 g 11.57 g 4.17 g 500-53315-A-4 Moisture T
Batch Notes Balance ID 971 No Unit Date samples were placed in the oven 12/18/12 Oven Temp when samples are put in oven 105 Degrees C Time samples were place in the oven 1330 Date samples were removed from oven 12/19/12 Oven Temp when samples removed from oven 105 Degrees C Time Samples were removed from oven 0700 Oven ID 776 ID number of the thermometer c-1966
Basis Basis Description T Total/NA



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### Lab Name: Job No.: SDG No.: GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Analyst: Batch Start Date: Batch End Date: Veldhuizen, Chris M 12/18/12 07:34 173236 Batch Method: TestAmerica Chicago

SM 2540G Lab Sample ID Client Sample IDMethod ChainBasis CalcMsg FC COMPOSITE 4 Not Calculated. RunCalculation is NULL 500-53315-A-1 SM 2540G T
FC D COMPOSITE 4 Not Calculated. RunCalculation is NULL 500-53315-A-2 SM 2540G T

Batch Notes

Basis Basis Description T Total/NA



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## Login Sample Receipt Checklist
Client: Project Integration, Inc Job Number: 500-53315-1 Login Number: 53315

Question Answer Comment Creator: Lunt, Jeff T List Source:TestAmerica Chicago List Number: 1



### True Radioactivity wasn't checked or is </= background as measured by a survey meter. True The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or tampered with. True Samples were received on ice. 2.7 True Cooler Temperature is acceptable

. True Cooler Temperature is recorded

. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within HoldingTime

. True Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample PreservationVerified

. True There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True Containers requiring zero headspace have no headspace or bubble is <6mm (1/4"). True Multiphasic samples are not present. True Samples do not require splitting or compositing. N/A Residual Chlorine Checked.

TestAmerica Chicago 

## 01/03/2013 Page 383 of 383

# ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Tel:(708)534-5200 TestAmerica Job ID: 500-53315-1 Client Project/Site: John Deere Des Moines Works (JDDMW) For: Project Integration, Inc 1097 Highway 101 South Suite D-16 Greer, South Carolina 29651 Attn: Mr. Robert Stevens
Authorized for release by: 1/3/2013 4:42:16 PM Donna Ingersoll Project Manager II donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 

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# Table of Contents Client: Project Integration, Inc Project/Site: John Deere Des Moines Works (JDDMW) TestAmerica Job ID: 500-53315-1



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## 1/3/2013 

# Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 

# Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 

# Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 

# Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 

# Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 

# Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 

# Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8 

# Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14 

# QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .15 

# Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21 

# QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22 

# Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32 

# Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35 

# Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 

# Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .37 

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