ANALYTICAL REPORT

Job Number: 500-53315-1

Job Description: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, SC 29651

Attention: Mr. Robert Stevens

_____________________________________________

Approved for release.

Donna L Ingersoll

Project Manager II

1/3/2013 4:44 PM

Donna L Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

01/03/2013

cc: Mr. David Kirby

Mr. Robert Malcomson

These test results meet all the requirements of NELAC for accredited parameters.

The Lab Certification ID# is 100201.

All questions regarding this test report should be directed to the TestAmerica Project Manager whose signature appears

on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be

reproduced only in its entirety.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.

TestAmerica Laboratories, Inc.

TestAmerica Chicago 2417 Bond Street, University Park, IL 60484

Tel (708) 534-5200 Fax (708) 534-5211 www.testamericainc.com

Page 1 of 383 01/03/2013
Table of Contents

Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13

Method / Analyst Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Sample Datasheets . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

QC Data Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Data Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 60

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68

Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99

Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100

GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100

Method 8260B . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 100

Method 8260B QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101

Method 8260B Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124

Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 130

Method 8260B ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 130

Method 8260B CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 160

Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181

Method 8260B Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 181

Page 2 of 383 01/03/2013
Table of Contents

Method 8260B LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 184

Method 8260B MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187

Method 8260B Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189

Method 8260B Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 195

Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 198

Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 198

Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 199

Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 200

Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 205

Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 205

Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 216

Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 220

Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 234

Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 242

Met Dup/Trip . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 246

Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 248

Met Serial Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 254

Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 255

Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 267

Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 270

Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 276

Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 286

General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 294

Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 295

Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 296

Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 301

Page 3 of 383 01/03/2013
Table of Contents

Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 301

Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305

Gen Chem MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 306

Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 310

Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 312

Gen Chem Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 330

Gen Chem Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 332

Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 340

Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 355

Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 377

Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 382

Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 383

Page 4 of 383 01/03/2013
Job Narrative

500-53315-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/15/2012 9:10 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 2.7o C.

GC/MS VOA 

Method(s) 8260B: Due to the high concentration of Acetone, the matrix spike / matrix spike duplicate (3MS/3MSD) for sample -3 could not 

be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.

Method(s) 8260B: One internal standard response was outside of acceptance limits for the following samples:FC D DISCRETE 4 

(500-53315-4), FC DISCRETE 4 (500-53315-3). The samples were re-analyzed at a dilution for Acetone. All internal standard area 

responses were within limits in the diluted runs. Both sets of data have been provided.

No other analytical or quality issues were noted.

Metals 

Method(s) 6010B: The serial dilution performed for the following sample, 500-53315-1, was outside control limits for Ci,Ni,Pb,V-, and Zn.

Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-53315-1 were outside control limits for 

Zn. The associated laboratory control sample (LCS) recovery met acceptance criteria.

Method(s) 7470A: The matrix spike duplicate (MSD) recovery for sample 500-53315-6 was outside control limits for Hg. The associated 

laboratory control sample (LCS) recovery met acceptance criteria.

No other analytical or quality issues were noted.

General Chemistry 

No analytical or quality issues were noted.

Page 5 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53315-1

Instrument ID: CMS16 Analysis Batch Number: 170196

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD1 500-170196/6 IC

11/19/12 12:14 16I1119A.D GC Column: DB624 ID: 0.2(mm)

Acetone 1.91 Poor chromatography wernerb 11/19/12 13:19

8260B

Page 6 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53315-1

Instrument ID: CMS25 Analysis Batch Number: 169636

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD3 500-169636/4 IC

11/14/12 10:29 25I1114c.D GC Column: ID:

Acetonitrile 2.17 Poor chromatography arndtb 11/14/12 10:48

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD4 500-169636/5 IC

11/14/12 10:53 25I1114d.D GC Column: ID:

Acetone 1.95 Poor chromatography arndtb 11/14/12 11:34

Acetonitrile 2.17 Peak Tail arndtb 11/14/12 11:19

2-Butanone (MEK) 3.03 Poor chromatography arndtb 11/14/12 11:35

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD5 500-169636/6 IC

11/14/12 11:18 25I1114e.D GC Column: ID:

Bromomethane 1.36 Peak Tail arndtb 11/14/12 11:58

Acetonitrile 2.17 Peak Tail arndtb 11/14/12 11:35

8260B

Page 7 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA MANUAL INTEGRATION SUMMARY

TestAmerica Chicago 500-53315-1

Instrument ID: CMS25 Analysis Batch Number: 169637

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD3 500-169637/4 IC

11/14/12 10:29 25I1114c.D GC Column: ID:

Acetonitrile 2.17 Poor chromatography arndtb 11/14/12 10:48

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD4 500-169637/5 IC

11/14/12 10:53 25I1114d.D GC Column: ID:

Acetone 1.95 Poor chromatography arndtb 11/14/12 11:34

Acetonitrile 2.17 Peak Tail arndtb 11/14/12 11:19

2-Butanone (MEK) 3.03 Poor chromatography arndtb 11/14/12 11:35

Lab Sample ID: Client Sample ID:

Date Analyzed: Lab File ID:

COMPOUND NAME RETENTION

TIME

MANUAL INTEGRATION

REASON ANALYST DATE

STD5 500-169637/6 IC

11/14/12 11:18 25I1114e.D GC Column: ID:

Bromomethane 1.36 Peak Tail arndtb 11/14/12 11:58

Acetonitrile 2.17 Peak Tail arndtb 11/14/12 11:35

8260B

Page 8 of 383 01/03/2013
SAMPLE SUMMARY

Client: Project Integration, Inc Job Number: 500-53315-1

Lab Sample ID Client Sample ID Client Matrix Sampled Received

Date/Time Date/Time

500-53315-1 FC COMPOSITE 4 Solid 12/14/2012 1515 12/15/2012 0910

500-53315-2 FC D COMPOSITE 4 Solid 12/14/2012 1515 12/15/2012 0910

500-53315-3 FC DISCRETE 4 Solid 12/14/2012 1445 12/15/2012 0910

500-53315-4 FC D DISCRETE 4 Solid 12/14/2012 1445 12/15/2012 0910

500-53315-5 TRIP BLANK Water 12/14/2012 0000 12/15/2012 0910

500-53315-6 FC EB 4 Water 12/14/2012 1430 12/15/2012 0910

TestAmerica Chicago Page 9 of 383 01/03/2013
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53315-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53315-1 FC COMPOSITE 4

Barium 346 3.70 mg/Kg 6010B

Copper 834 3.70 mg/Kg 6010B

Chromium 14400 V 3.70 mg/Kg 6010B

Nickel 89.8 V 3.70 mg/Kg 6010B

Lead 209 B V 1.85 mg/Kg 6010B

Vanadium 241 V 1.85 mg/Kg 6010B

Zinc 481 V 7.41 mg/Kg 6010B

Mercury 0.543 0.0595 mg/Kg 7471A

Flashpoint >176 40.0 Degrees F 1010

Chromium, hexavalent 3.97 3.85 mg/Kg 7196A

Cyanide, Total 0.745 J B 1.91 mg/Kg 9014

Sulfide 739 93.3 mg/Kg 9034

pH 9.50 0.200 SU 9045C

HEM (Oil & Grease) 11100 1880 mg/Kg 9071B

Percent Moisture 74 0.10 % Moisture

Percent Solids 26 0.10 % Moisture

% Moisture 74.0 0.100 % SM 2540G

Total Solids 26.0 0.100 % SM 2540G

TCLP

Barium 0.0194 J 0.500 mg/L 6010B

Copper 0.0487 0.0250 mg/L 6010B

Nickel 0.0549 0.0250 mg/L 6010B

TestAmerica Chicago Page 10 of 383 01/03/2013
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53315-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53315-2 FC D COMPOSITE 4

Barium 326 3.46 mg/Kg 6010B

Copper 784 3.46 mg/Kg 6010B

Chromium 13200 3.46 mg/Kg 6010B

Nickel 86.4 3.46 mg/Kg 6010B

Lead 188 B 1.73 mg/Kg 6010B

Vanadium 221 1.73 mg/Kg 6010B

Zinc 451 6.92 mg/Kg 6010B

Mercury 0.248 0.0628 mg/Kg 7471A

Flashpoint >176 40.0 Degrees F 1010

Chromium, hexavalent 4.08 3.76 mg/Kg 7196A

Cyanide, Total 0.765 J B 1.66 mg/Kg 9014

Sulfide 774 90.8 mg/Kg 9034

pH 9.58 0.200 SU 9045C

HEM (Oil & Grease) 8910 1830 mg/Kg 9071B

Percent Moisture 74 0.10 % Moisture

Percent Solids 26 0.10 % Moisture

% Moisture 74.0 0.100 % SM 2540G

Total Solids 26.0 0.100 % SM 2540G

TCLP

Copper 0.0483 0.0250 mg/L 6010B

Chromium 0.0120 J 0.0250 mg/L 6010B

Nickel 0.0582 0.0250 mg/L 6010B

500-53315-3 FC DISCRETE 4

Acetone 4220 864 ug/Kg 8260B

2-Butanone (MEK) 145 17.3 ug/Kg 8260B

Percent Moisture 71 0.10 % Moisture

Percent Solids 29 0.10 % Moisture

500-53315-4 FC D DISCRETE 4

Acetone 8710 888 ug/Kg 8260B

2-Butanone (MEK) 191 17.8 ug/Kg 8260B

Percent Moisture 72 0.10 % Moisture

Percent Solids 28 0.10 % Moisture

TestAmerica Chicago Page 11 of 383 01/03/2013
EXECUTIVE SUMMARY - Detections

Client: Project Integration, Inc Job Number: 500-53315-1

Analyte Result

Reporting 

Limit Units Method

Lab Sample ID Client Sample ID

Qualifier

500-53315-6 FC EB 4

2-Butanone (MEK) 13.0 5.00 ug/L 8260B

Barium 0.000580 J B 0.0100 mg/L 6010B

Copper 0.00303 J 0.0100 mg/L 6010B

Chromium 0.00312 J B 0.0100 mg/L 6010B

Lead 0.00214 J B 0.00500 mg/L 6010B

Zinc 0.00724 J 0.0200 mg/L 6010B

Mercury 0.000102 J 0.000200 mg/L 7470A

TestAmerica Chicago Page 12 of 383 01/03/2013
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53315-1

Description Lab Location Method Preparation Method

Matrix: Solid

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Metals TAL CHI SW846 3050B

Metals (ICP) TAL CHI SW846 6010B

TCLP Extraction TAL CHI SW846 1311

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

TCLP Extraction TAL CHI SW846 1311

Preparation, Mercury TAL CHI SW846 7470A

Mercury (CVAA) TAL CHI SW846 7471A

Preparation, Mercury TAL CHI SW846 7471A

Ignitability, Pensky-Martens Closed-Cup Method TAL CHI SW846 1010

Chromium, Hexavalent TAL CHI SW846 7196A

Alkaline Digestion (Chromium, Hexavalent) TAL CHI SW846 3060A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Distillation (Acid Soluble and Insoluble) TAL CHI SW846 9030B

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

pH TAL CHI SW846 9045C

HEM and SGT-HEM TAL CHI SW846 9071B

Preparation, HEM and SGT-HEM TAL CHI SW846 9071B

Percent Moisture TAL CHI EPA Moisture

Total, Fixed, and Volatile Solids TAL CHI SM SM 2540G

Matrix: Water

Volatile Organic Compounds (GC/MS) TAL CHI SW846 8260B

Purge and Trap TAL CHI SW846 5030B

Metals (ICP) TAL CHI SW846 6010B

Preparation, Total Metals TAL CHI SW846 3010A

Mercury (CVAA) TAL CHI SW846 7470A

Preparation, Mercury TAL CHI SW846 7470A

HEM and SGT-HEM TAL CHI 1664A 1664A

HEM and SGT-HEM (SPE) TAL CHI 1664A 1664A

Chromium, Hexavalent TAL CHI SW846 7196A

Cyanide TAL CHI SW846 9014

Cyanide, Distillation TAL CHI SW846 9010B

Sulfide, Acid soluble and Insoluble (Titrimetric) TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 9034

Sulfide, Reactive TAL CHI SW846 7.3.4

TestAmerica Chicago Page 13 of 383 01/03/2013
METHOD SUMMARY

Client: Project Integration, Inc Job Number: 500-53315-1

Description Lab Location Method Preparation Method

Lab References:

TAL CHI = TestAmerica Chicago

Method References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Chicago Page 14 of 383 01/03/2013
METHOD / ANALYST SUMMARY

Client: Project Integration, Inc Job Number: 500-53315-1

Method Analyst Analyst ID

SW846 8260B Arndt, Brett D BDA

SW846 8260B Werner, Brian D BDW

SW846 6010B Smith, Todd D TDS

SW846 7470A Bills, Brandon J BJB

SW846 7471A Bills, Brandon J BJB

SW846 1010 Wasowicz, Andrew P APW

1664A 1664A Brogan, Mary T MTB

SW846 7196A Wasowicz, Andrew P APW

SW846 9014 Treadwell, Eliane A EAT

SW846 9034 Boyd, Cheryl L CLB

SW846 9034 Moore, Colleen L CLM

SW846 9045C Moore, Colleen L CLM

SW846 9071B Brogan, Mary T MTB

EPA Moisture Veldhuizen, Chris M CMV

SM SM 2540G Veldhuizen, Chris M CMV

TestAmerica Chicago

Page 15 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC DISCRETE 4

Client Matrix: % Moisture: 71.1

500-53315-3

Solid

Date Sampled: 12/14/2012 1445

Date Received: 12/15/2012 0910

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/18/2012 0930

12/18/2012 0930

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53315-03.D

5 g

5 mL

5030B

CMS16

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173225

N/A

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

2-Butanone (MEK) 145 6.25 17.3

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 116 70 - 134

Toluene-d8 (Surr) 98 75 - 122

4-Bromofluorobenzene (Surr) 91 70 - 122

Dibromofluoromethane 113 75 - 120

TestAmerica Chicago Page 16 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC DISCRETE 4

Client Matrix: % Moisture: 71.1

500-53315-3

Solid

Date Sampled: 12/14/2012 1445

Date Received: 12/15/2012 0910

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/18/2012 0745

12/20/2012 0216

50

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53315-03.D

5 g

Run Type: DL 5 mL

5030B

CMS25

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173509

500-173238

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

Acetone 4220 225 864

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 109 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 91 75 - 120

Dibromofluoromethane 105 75 - 120

TestAmerica Chicago Page 17 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC D DISCRETE 4

Client Matrix: % Moisture: 71.8

500-53315-4

Solid

Date Sampled: 12/14/2012 1445

Date Received: 12/15/2012 0910

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/18/2012 1040

12/18/2012 1040

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53315-04.D

5 g

5 mL

5030B

CMS16

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173225

N/A

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

2-Butanone (MEK) 191 6.43 17.8

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 117 70 - 134

Toluene-d8 (Surr) 97 75 - 122

4-Bromofluorobenzene (Surr) 85 70 - 122

Dibromofluoromethane 112 75 - 120

TestAmerica Chicago Page 18 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC D DISCRETE 4

Client Matrix: % Moisture: 71.8

500-53315-4

Solid

Date Sampled: 12/14/2012 1445

Date Received: 12/15/2012 0910

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/18/2012 0745

12/20/2012 0240

50

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53315-04.D

5 g

Run Type: DL 5 mL

5030B

CMS25

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173509

500-173238

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL

Acetone 8710 231 888

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 119 75 - 125

Toluene-d8 (Surr) 93 75 - 120

4-Bromofluorobenzene (Surr) 90 75 - 120

Dibromofluoromethane 116 75 - 120

TestAmerica Chicago Page 19 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

TRIP BLANK

Client Matrix:

500-53315-5

Water

Date Sampled: 12/14/2012 0000

Date Received: 12/15/2012 0910

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/20/2012 0108

12/20/2012 0108

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53315-05.D

5 mL

5 mL

5030B

CMS25

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173508

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 105 75 - 125

Toluene-d8 (Surr) 100 75 - 120

4-Bromofluorobenzene (Surr) 97 75 - 120

Dibromofluoromethane 109 75 - 120

TestAmerica Chicago Page 20 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC EB 4

Client Matrix:

500-53315-6

Water

Date Sampled: 12/14/2012 1430

Date Received: 12/15/2012 0910

8260B Volatile Organic Compounds (GC/MS)

Dilution:

12/20/2012 0149

12/20/2012 0149

1.0

8260B

Final Weight/Volume:

Initial Weight/Volume: Lab File ID:

Instrument ID:

53315-06.D

5 mL

5 mL

5030B

CMS25

Analysis Date:

Prep Date:

Analysis Batch:

Prep Batch:

500-173508

N/A

Analysis Method:

Prep Method:

Analyte Result (ug/L) Qualifier MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) 13.0 1.47 5.00

Surrogate %Rec Qualifier Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 107 75 - 125

Toluene-d8 (Surr) 99 75 - 120

4-Bromofluorobenzene (Surr) 94 75 - 120

Dibromofluoromethane 107 75 - 120

TestAmerica Chicago Page 21 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC COMPOSITE 4

Client Matrix: % Moisture: 74.1

500-53315-1

Solid

Date Sampled: 12/14/2012 1515

Date Received: 12/15/2012 0910

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51217B

Dilution: 1.0 Initial Weight/Volume: 1.0407 g

12/17/2012 2246 Final Weight/Volume: 100 mL

12/17/2012 0850

3050B

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173224

Prep Batch: 500-173139

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Barium 346 0.441 3.70

Copper 834 1.00 3.70

Chromium 14400 V 0.618 3.70

Nickel 89.8 V 0.811 3.70

Lead 209 B V 0.637 1.85

Vanadium 241 V 0.281 1.85

Zinc 481 V 2.54 7.41

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: P51219B

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/19/2012 2229 Final Weight/Volume: 50 mL

12/19/2012 0820

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173518

500-173406

500-173187

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/17/2012 1245

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Barium 0.0194 J 0.0100 0.500

Copper 0.0487 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel 0.0549 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: 121912RB.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/19/2012 1024 Final Weight/Volume: 25 mL

12/18/2012 1300

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173438

500-173264

500-173187

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/17/2012 1245

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000200 0.000200

7471A Mercury (CVAA)

TestAmerica Chicago Page 22 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC COMPOSITE 4

Client Matrix: % Moisture: 74.1

500-53315-1

Solid

Date Sampled: 12/14/2012 1515

Date Received: 12/15/2012 0910

7471A Mercury (CVAA)

7471A Instrument ID:

Lab File ID: 121812C.PRN

Dilution: 1.0 Initial Weight/Volume: 0.6494 g

12/18/2012 1400 Final Weight/Volume: 50 mL

12/17/2012 1400

7471A

HG5

Analysis Date:

Prep Date:

Analysis Batch: 500-173328

Prep Batch: 500-173153

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Mercury 0.543 0.0227 0.0595

TestAmerica Chicago Page 23 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC D COMPOSITE 4

Client Matrix: % Moisture: 73.7

500-53315-2

Solid

Date Sampled: 12/14/2012 1515

Date Received: 12/15/2012 0910

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51217B

Dilution: 1.0 Initial Weight/Volume: 1.0994 g

12/17/2012 2317 Final Weight/Volume: 100 mL

12/17/2012 0850

3050B

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173224

Prep Batch: 500-173139

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Barium 326 0.411 3.46

Copper 784 0.937 3.46

Chromium 13200 0.577 3.46

Nickel 86.4 0.757 3.46

Lead 188 B 0.595 1.73

Vanadium 221 0.262 1.73

Zinc 451 2.37 6.92

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: P51219B

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/19/2012 2235 Final Weight/Volume: 50 mL

12/19/2012 0820

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173518

500-173406

500-173187

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/17/2012 1245

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Barium <0.500 0.0100 0.500

Copper 0.0483 0.0100 0.0250

Chromium 0.0120 J 0.0100 0.0250

Nickel 0.0582 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: 121912RB.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/19/2012 1029 Final Weight/Volume: 25 mL

12/18/2012 1300

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173438

500-173264

500-173187

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

Leach Date: 12/17/2012 1245

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL RL

Mercury <0.000200 0.0000200 0.000200

7471A Mercury (CVAA)

TestAmerica Chicago Page 24 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC D COMPOSITE 4

Client Matrix: % Moisture: 73.7

500-53315-2

Solid

Date Sampled: 12/14/2012 1515

Date Received: 12/15/2012 0910

7471A Mercury (CVAA)

7471A Instrument ID:

Lab File ID: 121812C.PRN

Dilution: 1.0 Initial Weight/Volume: 0.6068 g

12/18/2012 1401 Final Weight/Volume: 50 mL

12/17/2012 1400

7471A

HG5

Analysis Date:

Prep Date:

Analysis Batch: 500-173328

Prep Batch: 500-173153

Analysis Method:

Prep Method:

Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL

Mercury 0.248 0.0239 0.0628

TestAmerica Chicago Page 25 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

Client Sample ID:

Lab Sample ID:

FC EB 4

Client Matrix:

500-53315-6

Water

Date Sampled: 12/14/2012 1430

Date Received: 12/15/2012 0910

6010B Metals (ICP)

6010B Instrument ID:

Lab File ID: P51219A

Dilution: 1.0 Initial Weight/Volume: 50 mL

12/19/2012 1457 Final Weight/Volume: 50 mL

12/18/2012 1530

3010A

ICP5

Analysis Date:

Prep Date:

Analysis Batch: 500-173517

Prep Batch: 500-173349

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Barium 0.000580 J B 0.000440 0.0100

Copper 0.00303 J 0.00106 0.0100

Chromium 0.00312 J B 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead 0.00214 J B 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc 0.00724 J 0.00472 0.0200

7470A Mercury (CVAA)

7470A Instrument ID:

Lab File ID: 121812RB.CSV

Dilution: 1.0 Initial Weight/Volume: 25 mL

12/18/2012 0949 Final Weight/Volume: 25 mL

12/17/2012 1300

7470A

HG6

Analysis Date:

Prep Date:

Analysis Batch: 500-173280

Prep Batch: 500-173172

Analysis Method:

Prep Method:

Analyte Result (mg/L) Qualifier MDL RL

Mercury 0.000102 J 0.0000710 0.000200

TestAmerica Chicago Page 26 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC COMPOSITE 4

Client Matrix:

500-53315-1

Solid

Date Sampled: 12/14/2012 1515

Date Received: 12/15/2012 0910

Analyte Result Qual Units MDL RL Dil Method

Flashpoint >176 Degrees F 40.0 40.0 1.0 1010

Analysis Batch: 500-173558 Analysis Date (Start): 12/19/2012 1721 (End) 12/19/2012 1800 DryWt Corrected: N

Chromium, hexavalent 3.97 mg/Kg 1.50 3.85 1.0 7196A

Analysis Batch: 500-173341 Analysis Date (Start): 12/18/2012 1549 (End) 12/18/2012 1550 DryWt Corrected: Y

Prep Batch: 500-173258 Prep Date: 12/18/2012 1000

Cyanide, Total 0.745 J B mg/Kg 0.630 1.91 1.0 9014

Analysis Batch: 500-173386 Analysis Date (Start): 12/18/2012 1424 (End) 12/18/2012 1424 DryWt Corrected: Y

Prep Batch: 500-173250 Prep Date: 12/18/2012 1035

Sulfide 739 mg/Kg 14.9 93.3 1.0 9034

Analysis Batch: 500-173474 Analysis Date: 12/19/2012 1336 DryWt Corrected: Y

Prep Batch: 500-173291 Prep Date: 12/19/2012 1125

Sulfide, Reactive <48.6 mg/Kg 3.79 48.6 1.0 9034

Analysis Batch: 500-173472 Analysis Date: 12/19/2012 1218 DryWt Corrected: N

Prep Batch: 500-173290 Prep Date: 12/19/2012 1040

pH 9.50 SU 0.200 0.200 1.0 9045C

Analysis Batch: 500-173479 Analysis Date (Start): 12/20/2012 1512 (End) 12/20/2012 1611 DryWt Corrected: N

HEM (Oil & Grease) 11100 mg/Kg 835 1880 1.0 9071B

Analysis Batch: 500-173330 Analysis Date: 12/19/2012 1101 DryWt Corrected: Y

Prep Batch: 500-173324 Prep Date: 12/19/2012 0510

Percent Moisture 74 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173077 Analysis Date: 12/15/2012 1243 DryWt Corrected: N

Percent Solids 26 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173077 Analysis Date: 12/15/2012 1243 DryWt Corrected: N

% Moisture 74.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173236 Analysis Date: 12/18/2012 0734 DryWt Corrected: N

Total Solids 26.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173236 Analysis Date: 12/18/2012 0734 DryWt Corrected: N

TestAmerica Chicago Page 27 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC D COMPOSITE 4

Client Matrix:

500-53315-2

Solid

Date Sampled: 12/14/2012 1515

Date Received: 12/15/2012 0910

Analyte Result Qual Units MDL RL Dil Method

Flashpoint >176 Degrees F 40.0 40.0 1.0 1010

Analysis Batch: 500-173558 Analysis Date (Start): 12/19/2012 1800 (End) 12/19/2012 1840 DryWt Corrected: N

Chromium, hexavalent 4.08 mg/Kg 1.46 3.76 1.0 7196A

Analysis Batch: 500-173341 Analysis Date (Start): 12/18/2012 1550 (End) 12/18/2012 1550 DryWt Corrected: Y

Prep Batch: 500-173258 Prep Date: 12/18/2012 1000

Cyanide, Total 0.765 J B mg/Kg 0.549 1.66 1.0 9014

Analysis Batch: 500-173386 Analysis Date (Start): 12/18/2012 1424 (End) 12/18/2012 1425 DryWt Corrected: Y

Prep Batch: 500-173250 Prep Date: 12/18/2012 1035

Sulfide 774 mg/Kg 14.5 90.8 1.0 9034

Analysis Batch: 500-173474 Analysis Date: 12/19/2012 1337 DryWt Corrected: Y

Prep Batch: 500-173291 Prep Date: 12/19/2012 1125

Sulfide, Reactive <49.3 mg/Kg 3.85 49.3 1.0 9034

Analysis Batch: 500-173472 Analysis Date: 12/19/2012 1219 DryWt Corrected: N

Prep Batch: 500-173290 Prep Date: 12/19/2012 1045

pH 9.58 SU 0.200 0.200 1.0 9045C

Analysis Batch: 500-173479 Analysis Date (Start): 12/20/2012 1611 (End) 12/20/2012 1710 DryWt Corrected: N

HEM (Oil & Grease) 8910 mg/Kg 811 1830 1.0 9071B

Analysis Batch: 500-173330 Analysis Date: 12/19/2012 1112 DryWt Corrected: Y

Prep Batch: 500-173324 Prep Date: 12/19/2012 0510

Percent Moisture 74 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173077 Analysis Date: 12/15/2012 1243 DryWt Corrected: N

Percent Solids 26 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173077 Analysis Date: 12/15/2012 1243 DryWt Corrected: N

% Moisture 74.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173236 Analysis Date: 12/18/2012 0734 DryWt Corrected: N

Total Solids 26.0 % 0.100 0.100 1.0 SM 2540G

Analysis Batch: 500-173236 Analysis Date: 12/18/2012 0734 DryWt Corrected: N

TestAmerica Chicago Page 28 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC DISCRETE 4

Client Matrix:

500-53315-3

Solid

Date Sampled: 12/14/2012 1445

Date Received: 12/15/2012 0910

Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 71 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173311 Analysis Date: 12/18/2012 1359 DryWt Corrected: N

Percent Solids 29 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173311 Analysis Date: 12/18/2012 1359 DryWt Corrected: N

TestAmerica Chicago Page 29 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC D DISCRETE 4

Client Matrix:

500-53315-4

Solid

Date Sampled: 12/14/2012 1445

Date Received: 12/15/2012 0910

Analyte Result Qual Units MDL RL Dil Method

Percent Moisture 72 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173311 Analysis Date: 12/18/2012 1359 DryWt Corrected: N

Percent Solids 28 % 0.10 0.10 1.0 Moisture

Analysis Batch: 500-173311 Analysis Date: 12/18/2012 1359 DryWt Corrected: N

TestAmerica Chicago Page 30 of 383 01/03/2013
Analytical Data

Client: Project Integration, Inc Job Number: 500-53315-1

General Chemistry

Client Sample ID:

Lab Sample ID:

FC EB 4

Client Matrix:

500-53315-6

Water

Date Sampled: 12/14/2012 1430

Date Received: 12/15/2012 0910

Analyte Result Qual Units MDL RL Dil Method

HEM (Oil & Grease) <5.20 mg/L 1.51 5.20 1.0 1664A

Analysis Batch: 500-173178 Analysis Date: 12/18/2012 1114

Prep Batch: 500-173173 Prep Date: 12/18/2012 0724

Chromium, hexavalent <0.0100 mg/L 0.00325 0.0100 1.0 7196A

Analysis Batch: 500-173079 Analysis Date (Start): 12/15/2012 1322 (End) 12/15/2012 1322

Cyanide, Total <0.0100 mg/L 0.00331 0.0100 1.0 9014

Analysis Batch: 500-173387 Analysis Date (Start): 12/18/2012 1354 (End) 12/18/2012 1354

Prep Batch: 500-173245 Prep Date: 12/18/2012 0830

Sulfide <1.00 mg/L 0.230 1.00 1.0 9034

Analysis Batch: 500-173108 Analysis Date (Start): 12/17/2012 0111 (End) 12/17/2012 0114

Sulfide, Reactive <1.00 mg/L 1.00 1.00 1.0 9034

Analysis Batch: 500-173107 Analysis Date: 12/17/2012 0108

Prep Batch: 500-173106 Prep Date: 12/17/2012 0013

TestAmerica Chicago Page 31 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53315-3 FC DISCRETE 4 113 116 98 91

500-53315-4 FC D DISCRETE 4 112 117 97 85

MB 500-173225/4 106 106 113 104

LCS 500-173225/5 105 104 111 103

500-53315-3 MS FC DISCRETE 4 MS 118 117 95 85

500-53315-3 MSD FC DISCRETE 4 MSD 116 119 96 84

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

TestAmerica Chicago

Page 32 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Solid

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53315-3 DL FC DISCRETE 4 DL 105 109 97 91

500-53315-4 DL FC D DISCRETE 4 

DL

116 119 93 90

MB 500-173509/6 96 101 95 94

LCS 500-173509/4 98 102 97 99

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 33 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Surrogate Recovery Report

8260B Volatile Organic Compounds (GC/MS)

Client Matrix: Water

Lab Sample ID Client Sample ID

DBFM DCA TOL BFB

%Rec %Rec %Rec %Rec

500-53315-5 TRIP BLANK 109 105 100 97

500-53315-6 FC EB 4 107 107 99 94

MB 500-173508/6 96 101 95 94

LCS 500-173508/4 98 102 97 99

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

TestAmerica Chicago

Page 34 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173225

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 16M1218.D5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

MB 500-173225/4 CMS16

Analysis Date: 12/18/2012 0830

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173225

Prep Date:

Leach Date:

12/18/2012 0830

N/A

Analyte Result Qual MDL RL

Acetone <5.00 2.16 5.00

2-Butanone (MEK) <5.00 1.81 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 106 70 - 134

Toluene-d8 (Surr) 113 75 - 122

4-Bromofluorobenzene (Surr) 104 70 - 122

Dibromofluoromethane 106 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-173225

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 16S1218.D5 g

Units: ug/Kg 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-173225/5 CMS16

Analysis Date: 12/18/2012 0853

Analysis Batch:

Prep Batch:

Leach Batch:

500-173225

N/A

N/A

Prep Date:

Leach Date:

12/18/2012 0853

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 45.56 91 50 - 138

2-Butanone (MEK) 50.0 52.85 106 58 - 133

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 104 70 - 134

Toluene-d8 (Surr) 111 75 - 122

4-Bromofluorobenzene (Surr) 103 70 - 122

Dibromofluoromethane 105 75 - 120

TestAmerica Chicago Page 35 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Dilution:

Dilution:

Solid

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

53315-03s.D

5 g

5 mL

53315-03t.D

5 g

5 mL

Method: 8260B

Preparation: 5030B

CMS16

CMS16

500-53315-3

500-53315-3

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173225

12/18/2012 0954

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173225

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 1017

12/18/2012 1017

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173225

N/A

N/A

12/18/2012 0954

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Acetone 104 399 50 - 138 7 30 E 4 E 4

2-Butanone (MEK) 106 91 58 - 133 8 30

Surrogate MS % Rec MSD % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 117 119 70 - 134

Toluene-d8 (Surr) 95 96 75 - 122

4-Bromofluorobenzene (Surr) 85 84 70 - 122

Dibromofluoromethane 118 116 75 - 120

Solid

12/18/2012 0954 12/18/2012 1017

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Solid

Method: 8260B

Preparation: 5030B

MS Lab Sample ID: 500-53315-3 Units: ug/Kg MSD Lab Sample ID: 500-53315-3

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173225

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 0954

N/A

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 1017

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Acetone 6940 173 173 7120 E 4 7629 E 4

2-Butanone (MEK) 145 173 173 329.3 303.4

TestAmerica Chicago Page 36 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173508

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 25M1219p.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

MB 500-173508/6 CMS25

Analysis Date: 12/20/2012 0043

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173508

Prep Date:

Leach Date:

12/20/2012 0043

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.29 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 101 75 - 125

Toluene-d8 (Surr) 95 75 - 120

4-Bromofluorobenzene (Surr) 94 75 - 120

Dibromofluoromethane 96 75 - 120

Water

1.0

Lab Control Sample - Batch: 500-173508

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 25S1219p.D5 mL

Units: ug/L 5 mL

Method: 8260B

Preparation: 5030B

LCS 500-173508/4 CMS25

Analysis Date: 12/19/2012 2354

Analysis Batch:

Prep Batch:

Leach Batch:

500-173508

N/A

N/A

Prep Date:

Leach Date:

12/19/2012 2354

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 52.35 105 46 - 153

2-Butanone (MEK) 50.0 53.39 107 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 102 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 99 75 - 120

Dibromofluoromethane 98 75 - 120

TestAmerica Chicago Page 37 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173509

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 25M1219p.D

Units: ug/Kg

Method: 8260B

Preparation: N/A

MB 500-173509/6 CMS25

Analysis Date: 12/20/2012 0043

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173509

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Acetone <5.00 1.30 5.00

2-Butanone (MEK) <5.00 1.47 5.00

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 101 75 - 125

Toluene-d8 (Surr) 95 75 - 120

4-Bromofluorobenzene (Surr) 94 75 - 120

Dibromofluoromethane 96 75 - 120

Solid

1.0

Lab Control Sample - Batch: 500-173509

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 25S1219p.D

Units: ug/Kg

Method: 8260B

Preparation: N/A

LCS 500-173509/4 CMS25

Analysis Date: 12/19/2012 2354

Analysis Batch:

Prep Batch:

Leach Batch:

500-173509

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Acetone 50.0 52.35 105 46 - 153

2-Butanone (MEK) 50.0 53.39 107 54 - 138

Surrogate % Rec Acceptance Limits

1,2-Dichloroethane-d4 (Surr) 102 75 - 125

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 99 75 - 120

Dibromofluoromethane 98 75 - 120

TestAmerica Chicago Page 38 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173139

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51217B1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

MB 500-173139/1-A ICP5

Analysis Date: 12/17/2012 2104

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173224

500-173139

Prep Date:

Leach Date:

12/17/2012 0850

N/A

Analyte Result Qual MDL RL

Barium <1.00 0.119 1.00

Copper <1.00 0.271 1.00

Chromium <1.00 0.167 1.00

Nickel <1.00 0.219 1.00

Lead 0.2420 J 0.172 0.500

Vanadium <0.500 0.0759 0.500

Zinc <2.00 0.686 2.00

Solid

1.0

Lab Control Sample - Batch: 500-173139

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51217B1 g

Units: mg/Kg 100 mL

Method: 6010B

Preparation: 3050B

LCS 500-173139/2-A ICP5

Analysis Date: 12/17/2012 2110

Analysis Batch:

Prep Batch:

Leach Batch:

500-173224

500-173139

N/A

Prep Date:

Leach Date:

12/17/2012 0850

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 200 197.2 99 80 - 120

Copper 25.0 24.95 100 80 - 120

Chromium 20.0 19.91 100 80 - 120

Nickel 50.0 49.11 98 80 - 120

Lead 10.0 10.07 101 80 - 120

Vanadium 50.0 49.74 99 80 - 120

Zinc 50.0 48.83 98 80 - 120

TestAmerica Chicago Page 39 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Dilution:

Dilution:

Solid

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

P51217B

1.0117 g

100 mL

P51217B

1.0566 g

100 mL

Method: 6010B

Preparation: 3050B

ICP5

ICP5

500-53315-1

500-53315-1

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173139

12/17/2012 2304

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173224

500-173139

N/A

Analysis Date:

Prep Date:

Leach Date:

12/17/2012 2310

12/17/2012 0850

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173224

500-173139

N/A

12/17/2012 0850

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Barium 84 82 75 - 125 4 20

Copper 2 -38 75 - 125 4 20 4 4

Chromium -1125 -1577 75 - 125 2 20 4 4

Nickel 82 81 75 - 125 4 20

Lead 116 12 75 - 125 17 20 4 4

Vanadium 79 76 75 - 125 3 20

Zinc 65 65 75 - 125 1 20 F F

Solid

12/17/2012 2304 12/17/2012 2310

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Solid

Method: 6010B

Preparation: 3050B

MS Lab Sample ID: 500-53315-1 Units: mg/Kg MSD Lab Sample ID: 500-53315-1

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173139

Analysis Date:

Prep Date:

Leach Date:

12/17/2012 0850

N/A

Analysis Date:

Prep Date:

Leach Date:

12/17/2012 0850

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Barium 346 762 729 987.2 943.9

Copper 834 95.2 91.2 836.2 4 799.8 4

Chromium 14400 76.2 72.9 13510 4 13220 4

Nickel 89.8 190 182 246.8 237.5

Lead 209 38.1 36.5 253.1 4 213.5 4

Vanadium 241 190 182 391.8 379.3

Zinc 481 190 182 605.1 F 600.3 F

TestAmerica Chicago Page 40 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Units: mg/Kg

Solid

Dilution: 5.0

Serial Dilution - Batch: 500-173139

Lab Sample ID:

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51217B1.0407 g

100 mL

Method: 6010B

Preparation: 3050B

500-53315-1 ICP5

Analysis Date: 12/17/2012 2252

Analysis Batch:

Prep Batch:

Leach Batch:

500-173224

500-173139

N/A

Prep Date:

Leach Date:

12/17/2012 0850

N/A

Analyte Sample Result/Qual Result %Diff Limit Qual

Barium 346 377.6 9.2 10

Copper 834 868.4 4.1 10

Chromium 14400 16720 16 10 V

Nickel 89.8 102.4 14 10 V

Lead 209 239.4 15 10 V

Vanadium 241 281.4 17 10 V

Zinc 481 576.2 20 10 V

Units: mg/Kg

Solid

Dilution: 1.0

Duplicate - Batch: 500-173139

Lab Sample ID:

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51217B1.0334 g

100 mL

Method: 6010B

Preparation: 3050B

500-53315-1 ICP5

Analysis Date: 12/17/2012 2258

Analysis Batch:

Prep Batch:

Leach Batch:

500-173224

500-173139

N/A

Prep Date:

Leach Date:

12/17/2012 0850

N/A

Analyte Sample Result/Qual Result RPD Limit Qual

Barium 346 335.3 3 20

Copper 834 804.0 4 20

Chromium 14400 13970 3 20

Nickel 89.8 88.38 2 20

Lead 209 201.3 4 20

Vanadium 241 234.5 3 20

Zinc 481 468.4 3 20

TestAmerica Chicago Page 41 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173349

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219A50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

MB 500-173349/1-A ICP5

Analysis Date: 12/19/2012 1352

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173517

500-173349

Prep Date:

Leach Date:

12/18/2012 1530

N/A

Analyte Result Qual MDL RL

Barium 0.002710 J 0.000440 0.0100

Copper <0.0100 0.00106 0.0100

Chromium 0.001210 J 0.000960 0.0100

Nickel <0.0100 0.00190 0.0100

Lead 0.002720 J 0.00158 0.00500

Vanadium <0.00500 0.000620 0.00500

Zinc <0.0200 0.00472 0.0200

Water

1.0

Lab Control Sample - Batch: 500-173349

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219A50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-173349/2-A ICP5

Analysis Date: 12/19/2012 1358

Analysis Batch:

Prep Batch:

Leach Batch:

500-173517

500-173349

N/A

Prep Date:

Leach Date:

12/18/2012 1530

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.955 98 80 - 120

Copper 0.250 0.2524 101 80 - 120

Chromium 0.200 0.1989 99 80 - 120

Nickel 0.500 0.4934 99 80 - 120

Lead 0.100 0.1010 101 80 - 120

Vanadium 0.500 0.4993 100 80 - 120

Zinc 0.500 0.4858 97 80 - 120

TestAmerica Chicago Page 42 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPE Leachate Blank - Batch: 500-173406

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

TCLP

LB 500-173187/1-D ICP5

Analysis Date: 12/19/2012 2107

Analysis Batch:

Prep Batch:

Leach Batch: 500-173187

500-173518

500-173406

Prep Date:

Leach Date:

12/19/2012 0820

12/17/2012 1245

Analyte Result Qual MDL RL

Barium <0.500 0.0100 0.500

Copper <0.0250 0.0100 0.0250

Chromium <0.0250 0.0100 0.0250

Nickel <0.0250 0.0100 0.0250

Lead <0.0500 0.00500 0.0500

Vanadium <0.0250 0.00500 0.0250

Zinc <0.100 0.0200 0.100

Water

1.0

Lab Control Sample - Batch: 500-173406

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: P51219B50 mL

Units: mg/L 50 mL

Method: 6010B

Preparation: 3010A

LCS 500-173406/3-A ICP5

Analysis Date: 12/19/2012 2120

Analysis Batch:

Prep Batch:

Leach Batch:

500-173518

500-173406

N/A

Prep Date:

Leach Date:

12/19/2012 0820

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Barium 2.00 1.975 99 80 - 120

Copper 0.250 0.2464 99 80 - 120

Chromium 0.200 0.1969 98 80 - 120

Nickel 0.500 0.4873 97 80 - 120

Lead 0.100 0.09785 98 80 - 120

Vanadium 0.500 0.4959 99 80 - 120

Zinc 0.500 0.4782 96 80 - 120

TestAmerica Chicago Page 43 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173172

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121812RB.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-173172/7-A HG6

Analysis Date: 12/18/2012 0909

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173280

500-173172

Prep Date:

Leach Date:

12/17/2012 1300

N/A

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000710 0.000200

Water

1.0

Lab Control Sample - Batch: 500-173172

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121812RB.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-173172/8-A HG6

Analysis Date: 12/18/2012 0911

Analysis Batch:

Prep Batch:

Leach Batch:

500-173280

500-173172

N/A

Prep Date:

Leach Date:

12/17/2012 1300

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002027 101 80 - 120

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

121812RB.CSV

25 mL

25 mL

121812RB.CSV

25 mL

25 mL

Method: 7470A

Preparation: 7470A

HG6

HG6

500-53315-6

500-53315-6

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173172

12/18/2012 0957

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173280

500-173172

N/A

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 0959

12/17/2012 1300

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173280

500-173172

N/A

12/17/2012 1300

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Mercury 86 69 75 - 125 20 20 F

TestAmerica Chicago Page 44 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Water

12/18/2012 0957 12/18/2012 0959

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Water

Method: 7470A

Preparation: 7470A

MS Lab Sample ID: 500-53315-6 Units: mg/L MSD Lab Sample ID: 500-53315-6

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173172

Analysis Date:

Prep Date:

Leach Date:

12/17/2012 1300

N/A

Analysis Date:

Prep Date:

Leach Date:

12/17/2012 1300

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Mercury 0.000102 J 0.00100 0.00100 0.000960 0.000789 F

Units: mg/L

Water

Dilution: 1.0

Duplicate - Batch: 500-173172

Lab Sample ID:

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121812RB.CSV25 mL

25 mL

Method: 7470A

Preparation: 7470A

500-53315-6 HG6

Analysis Date: 12/18/2012 0955

Analysis Batch:

Prep Batch:

Leach Batch:

500-173280

500-173172

N/A

Prep Date:

Leach Date:

12/17/2012 1300

N/A

Analyte Sample Result/Qual Result RPD Limit Qual

Mercury 0.000102 J 0.0001082 6 20 J

TestAmerica Chicago Page 45 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173264

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121912RB.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

MB 500-173264/7-A HG6

Analysis Date: 12/19/2012 1008

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173438

500-173264

Prep Date:

Leach Date:

12/18/2012 1300

N/A

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000200 0.000200

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

TCLP SPLPE Leachate Blank - Batch: 500-173264

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121912RB.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

TCLP

LB 500-173187/1-B HG6

Analysis Date: 12/19/2012 1012

Analysis Batch:

Prep Batch:

Leach Batch: 500-173187

500-173438

500-173264

Prep Date:

Leach Date:

12/18/2012 1300

12/17/2012 1245

Analyte Result Qual MDL RL

Mercury <0.000200 0.0000200 0.000200

Water

1.0

Lab Control Sample - Batch: 500-173264

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121912RB.CSV25 mL

Units: mg/L 25 mL

Method: 7470A

Preparation: 7470A

LCS 500-173264/8-A HG6

Analysis Date: 12/19/2012 1010

Analysis Batch:

Prep Batch:

Leach Batch:

500-173438

500-173264

N/A

Prep Date:

Leach Date:

12/18/2012 1300

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.00200 0.002002 100 80 - 120

TestAmerica Chicago Page 46 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173153

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121812C.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

MB 500-173153/7-A HG5

Analysis Date: 12/18/2012 1304

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173328

500-173153

Prep Date:

Leach Date:

12/17/2012 1400

N/A

Analyte Result Qual MDL RL

Mercury <0.0167 0.00637 0.0167

Solid

1.0

Lab Control Sample - Batch: 500-173153

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 121812C.PRN0.6 g

Units: mg/Kg 50 mL

Method: 7471A

Preparation: 7471A

LCS 500-173153/8-A HG5

Analysis Date: 12/18/2012 1310

Analysis Batch:

Prep Batch:

Leach Batch:

500-173328

500-173153

N/A

Prep Date:

Leach Date:

12/17/2012 1400

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Mercury 0.167 0.1717 103 80 - 120

TestAmerica Chicago Page 47 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173173

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

MB 500-173173/1-A No Equipment 

Analysis Date: 12/18/2012 1005

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173178

500-173173

Prep Date:

Leach Date:

12/18/2012 0525

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <5.00 1.45 5.00

Water

1.0

Lab Control Sample - Batch: 500-173173

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1000 mL

Units: mg/L 1000 mL

Method: 1664A

Preparation: 1664A

N/A

LCS 500-173173/2-A No Equipment 

Analysis Date: 12/18/2012 1011

Analysis Batch:

Prep Batch:

Leach Batch:

500-173178

500-173173

N/A

Prep Date:

Leach Date:

12/18/2012 0535

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 40.0 39.10 98 78 - 114

TestAmerica Chicago Page 48 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173079

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 7196A

Preparation: N/A

N/A

MB 500-173079/3 SPEC5

Analysis Date: 12/15/2012 1321

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173079

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <0.0100 0.00325 0.0100

Water

1.0

Lab Control Sample - Batch: 500-173079

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 7196A

Preparation: N/A

N/A

LCS 500-173079/4 SPEC5

Analysis Date: 12/15/2012 1321

Analysis Batch:

Prep Batch:

Leach Batch:

500-173079

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 0.250 0.2497 100 85 - 115

Dilution:

Dilution:

Water

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Water

Method: 7196A

Preparation: N/A

N/A

N/A

SPEC5

SPEC5

500-53315-6

500-53315-6

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173079

12/15/2012 1322

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173079

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

12/15/2012 1323

N/A

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173079

N/A

N/A

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Chromium, hexavalent 100 100 85 - 115 0 20

TestAmerica Chicago Page 49 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Water

12/15/2012 1322 12/15/2012 1323

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Water

Method: 7196A

Preparation: N/A

MS Lab Sample ID: 500-53315-6 Units: mg/L MSD Lab Sample ID: 500-53315-6

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173079

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Analysis Date:

Prep Date:

Leach Date:

N/A

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Chromium, hexavalent <0.0100 0.250 0.250 0.2500 0.2500

TestAmerica Chicago Page 50 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173258

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

MB 500-173258/1-A SPEC5

Analysis Date: 12/18/2012 1546

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173341

500-173258

Prep Date:

Leach Date:

12/18/2012 1000

N/A

Analyte Result Qual MDL RL

Chromium, hexavalent <1.00 0.389 1.00

Solid

1.0

Lab Control Sample - Batch: 500-173258

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173258/2-A SPEC5

Analysis Date: 12/18/2012 1546

Analysis Batch:

Prep Batch:

Leach Batch:

500-173341

500-173258

N/A

Prep Date:

Leach Date:

12/18/2012 1000

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 10.0 8.252 83 80 - 120

Solid

50

Lab Control Sample - Batch: 500-173258

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 2.5 g

Units: mg/Kg 100 mL

Method: 7196A

Preparation: 3060A

N/A

LCS 500-173258/3-A SPEC5

Analysis Date: 12/18/2012 1547

Analysis Batch:

Prep Batch:

Leach Batch:

500-173341

500-173258

N/A

Prep Date:

Leach Date:

12/18/2012 1000

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Chromium, hexavalent 1550 1601 104 80 - 120

TestAmerica Chicago Page 51 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173245

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-173245/1-A SPEC5

Analysis Date: 12/18/2012 1345

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173387

500-173245

Prep Date:

Leach Date:

12/18/2012 0830

N/A

Analyte Result Qual MDL RL

Cyanide, Total <0.0100 0.00331 0.0100

Water

1.0

Lab Control Sample - Batch: 500-173245

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 50 mL

Units: mg/L 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-173245/2-A SPEC5

Analysis Date: 12/18/2012 1345

Analysis Batch:

Prep Batch:

Leach Batch:

500-173387

500-173245

N/A

Prep Date:

Leach Date:

12/18/2012 0830

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 0.100 0.1057 106 80 - 120

TestAmerica Chicago Page 52 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173250

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

MB 500-173250/1-A SPEC5

Analysis Date: 12/18/2012 1423

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173386

500-173250

Prep Date:

Leach Date:

12/18/2012 1035

N/A

Analyte Result Qual MDL RL

Cyanide, Total 0.1850 J 0.165 0.500

Solid

1.0

Lab Control Sample - Batch: 500-173250

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 1.0000 g

Units: mg/Kg 50 mL

Method: 9014

Preparation: 9010B

N/A

LCS 500-173250/2-A SPEC5

Analysis Date: 12/18/2012 1423

Analysis Batch:

Prep Batch:

Leach Batch:

500-173386

500-173250

N/A

Prep Date:

Leach Date:

12/18/2012 1035

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Cyanide, Total 5.00 5.235 105 80 - 120

Dilution:

Dilution:

Solid

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: Client Matrix: Solid

1.1473 g

50 mL

1.1489 g

50 mL

Method: 9014

Preparation: 9010B

N/A

N/A

SPEC5

SPEC5

500-53315-2

500-53315-2

MS Lab Sample ID:

MSD Lab Sample ID:

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173250

12/18/2012 1425

N/A

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

500-173386

500-173250

N/A

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 1425

12/18/2012 1035

N/A

Analysis Batch:

Prep Batch:

Leach Batch:

500-173386

500-173250

N/A

12/18/2012 1035

Analyte Limit RPD RPD Limit

% Rec.

MS MSD MS Qual MSD Qual

Cyanide, Total 81 89 75 - 125 8 20

TestAmerica Chicago Page 53 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Solid

12/18/2012 1425 12/18/2012 1425

Dilution: 1.0 Dilution: 1.0

Client Matrix: Client Matrix: Solid

Method: 9014

Preparation: 9010B

MS Lab Sample ID: 500-53315-2 Units: mg/Kg MSD Lab Sample ID: 500-53315-2

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 500-173250

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 1035

N/A

Analysis Date:

Prep Date:

Leach Date:

12/18/2012 1035

N/A

Amount

Sample

Analyte Result/Qual Amount Result/Qual Result/Qual

MS Spike MSD Spike MS MSD

Cyanide, Total 0.765 J 6.63 6.62 6.130 6.651

TestAmerica Chicago Page 54 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173106

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-173106/1-A No Equipment 

Analysis Date: 12/17/2012 0019

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173107

500-173106

Prep Date:

Leach Date:

12/17/2012 0001

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <1.00 1.00 1.00

Water

1.0

Lab Control Sample - Batch: 500-173106

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 250 mL

Units: mg/L 250 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-173106/2-A No Equipment 

Analysis Date: 12/17/2012 0035

Analysis Batch:

Prep Batch:

Leach Batch:

500-173107

500-173106

N/A

Prep Date:

Leach Date:

12/17/2012 0005

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 3.60 3.292 91 80 - 120

TestAmerica Chicago Page 55 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Water

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173108

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 9034

Preparation: N/A

N/A

MB 500-173108/1 No Equipment 

Analysis Date: 12/17/2012 0019

Analysis Batch:

Prep Batch:

Leach Batch:

N/A

N/A

500-173108

Prep Date:

Leach Date:

N/A

N/A

Analyte Result Qual MDL RL

Sulfide <1.00 0.230 1.00

Water

1.0

Lab Control Sample - Batch: 500-173108

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Units: mg/L Final Weight/Volume:

Method: 9034

Preparation: N/A

N/A

LCS 500-173108/2 No Equipment 

Analysis Date: 12/17/2012 0021

Analysis Batch:

Prep Batch:

Leach Batch:

500-173108

N/A

N/A

Prep Date:

Leach Date:

N/A

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 3.60 3.286 91 80 - 120

TestAmerica Chicago Page 56 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173290

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

MB 500-173290/1-A No Equipment 

Analysis Date: 12/19/2012 1215

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173472

500-173290

Prep Date:

Leach Date:

12/19/2012 1005

N/A

Analyte Result Qual MDL RL

Sulfide, Reactive <50.0 3.90 50.0

Solid

1.0

Lab Control Sample - Batch: 500-173290

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 7.3.4

N/A

LCS 500-173290/2-A No Equipment 

Analysis Date: 12/19/2012 1215

Analysis Batch:

Prep Batch:

Leach Batch:

500-173472

500-173290

N/A

Prep Date:

Leach Date:

12/19/2012 1010

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide, Reactive 180 168.6 94 80 - 120

TestAmerica Chicago Page 57 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173291

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

MB 500-173291/1-A No Equipment 

Analysis Date: 12/19/2012 1335

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173474

500-173291

Prep Date:

Leach Date:

12/19/2012 1125

N/A

Analyte Result Qual MDL RL

Sulfide <25.0 4.00 25.0

Solid

1.0

Lab Control Sample - Batch: 500-173291

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10.0000 g

Units: mg/Kg 10 mL

Method: 9034

Preparation: 9030B

N/A

LCS 500-173291/2-A No Equipment 

Analysis Date: 12/19/2012 1335

Analysis Batch:

Prep Batch:

Leach Batch:

500-173474

500-173291

N/A

Prep Date:

Leach Date:

12/19/2012 1125

N/A

Analyte Spike Amount Result % Rec. Limit Qual

Sulfide 180 168.3 93 80 - 120

TestAmerica Chicago Page 58 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Client Matrix: Solid

Dilution: 1.0

Lab Sample ID:

Method Blank - Batch: 500-173324

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

MB 500-173324/1-A No Equipment 

Analysis Date: 12/19/2012 0920

Analysis Batch:

Prep Batch:

Leach Batch: N/A

500-173330

500-173324

Prep Date:

Leach Date:

12/19/2012 0510

N/A

Analyte Result Qual MDL RL

HEM (Oil & Grease) <500 222 500

Solid

1.0

Lab Control Sample - Batch: 500-173324

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume: Final Weight/Volume: 10 g

Units: mg/Kg 10 mL

Method: 9071B

Preparation: 9071B

N/A

LCS 500-173324/2-A No Equipment 

Analysis Date: 12/19/2012 0931

Analysis Batch:

Prep Batch:

Leach Batch:

500-173330

500-173324

N/A

Prep Date:

Leach Date:

12/19/2012 0510

N/A

Analyte Spike Amount Result % Rec. Limit Qual

HEM (Oil & Grease) 4000 4090 102 80 - 120

TestAmerica Chicago Page 59 of 383 01/03/2013
DATA REPORTING QUALIFIERS

Client: Project Integration, Inc Job Number: 500-53315-1

Lab Section Qualifier Description

GC/MS VOA

MS, MSD: The analyte present in the original sample is 4 times greater 

than the matrix spike concentration; therefore, control limits are not 

applicable.

4

E Result exceeded calibration range.

Metals

B Compound was found in the blank and sample.

F MS or MSD exceeds the control limits

MS, MSD: The analyte present in the original sample is 4 times greater 

than the matrix spike concentration; therefore, control limits are not 

applicable.

4

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

V Serial Dilution exceeds the control limits

General Chemistry

B Compound was found in the blank and sample.

Result is less than the RL but greater than or equal to the MDL and the 

concentration is an approximate value.

J

TestAmerica Chicago Page 60 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

GC/MS VOA

Analysis Batch:500-173225

LCS 500-173225/5 Lab Control Sample T Solid 8260B

MB 500-173225/4 Method Blank T Solid 8260B

500-53315-3 FC DISCRETE 4 T Solid 8260B

500-53315-3MS Matrix Spike T Solid 8260B

500-53315-3MSD Matrix Spike Duplicate T Solid 8260B

500-53315-4 FC D DISCRETE 4 T Solid 8260B

Prep Batch: 500-173238

500-53315-3DL FC DISCRETE 4 T Solid 5030B

500-53315-4DL FC D DISCRETE 4 T Solid 5030B

Analysis Batch:500-173508

LCS 500-173508/4 Lab Control Sample T Water 8260B

MB 500-173508/6 Method Blank T Water 8260B

500-53315-5 TRIP BLANK T Water 8260B

500-53315-6 FC EB 4 T Water 8260B

Analysis Batch:500-173509

LCS 500-173509/4 Lab Control Sample T Solid 8260B

MB 500-173509/6 Method Blank T Solid 8260B

500-53315-3DL FC DISCRETE 4 T Solid 8260B 500-173238

500-53315-4DL FC D DISCRETE 4 T Solid 8260B 500-173238

Report Basis

T = Total

TestAmerica Chicago

Page 61 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Prep Batch: 500-173139

LCS 500-173139/2-A Lab Control Sample T Solid 3050B

MB 500-173139/1-A Method Blank T Solid 3050B

500-53315-1 FC COMPOSITE 4 T Solid 3050B

500-53315-1DU Duplicate T Solid 3050B

500-53315-1MS Matrix Spike T Solid 3050B

500-53315-1MSD Matrix Spike Duplicate T Solid 3050B

500-53315-2 FC D COMPOSITE 4 T Solid 3050B

Prep Batch: 500-173153

LCS 500-173153/8-A Lab Control Sample T Solid 7471A

MB 500-173153/7-A Method Blank T Solid 7471A

500-53315-1 FC COMPOSITE 4 T Solid 7471A

500-53315-2 FC D COMPOSITE 4 T Solid 7471A

Prep Batch: 500-173172

LCS 500-173172/8-A Lab Control Sample T Water 7470A

MB 500-173172/7-A Method Blank T Water 7470A

500-53315-6 FC EB 4 T Water 7470A

500-53315-6DU Duplicate T Water 7470A

500-53315-6MS Matrix Spike T Water 7470A

500-53315-6MSD Matrix Spike Duplicate T Water 7470A

Prep Batch: 500-173187

LB 500-173187/1-B TCLP SPLPE Leachate Blank P Solid 1311

LB 500-173187/1-D TCLP SPLPE Leachate Blank P Solid 1311

500-53315-1 FC COMPOSITE 4 P Solid 1311

500-53315-2 FC D COMPOSITE 4 P Solid 1311

Analysis Batch:500-173224

LCS 500-173139/2-A Lab Control Sample T Solid 6010B 500-173139

MB 500-173139/1-A Method Blank T Solid 6010B 500-173139

500-53315-1 FC COMPOSITE 4 T Solid 6010B 500-173139

500-53315-1DU Duplicate T Solid 6010B 500-173139

500-53315-1MS Matrix Spike T Solid 6010B 500-173139

500-53315-1MSD Matrix Spike Duplicate T Solid 6010B 500-173139

500-53315-2 FC D COMPOSITE 4 T Solid 6010B 500-173139

Prep Batch: 500-173264

LCS 500-173264/8-A Lab Control Sample T Water 7470A

MB 500-173264/7-A Method Blank T Water 7470A

LB 500-173187/1-B TCLP SPLPE Leachate Blank P Solid 7470A 500-173187

500-53315-1 FC COMPOSITE 4 P Solid 7470A 500-173187

500-53315-2 FC D COMPOSITE 4 P Solid 7470A 500-173187

TestAmerica Chicago

Page 62 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Analysis Batch:500-173280

LCS 500-173172/8-A Lab Control Sample T Water 7470A 500-173172

MB 500-173172/7-A Method Blank T Water 7470A 500-173172

500-53315-6 FC EB 4 T Water 7470A 500-173172

500-53315-6DU Duplicate T Water 7470A 500-173172

500-53315-6MS Matrix Spike T Water 7470A 500-173172

500-53315-6MSD Matrix Spike Duplicate T Water 7470A 500-173172

Analysis Batch:500-173328

LCS 500-173153/8-A Lab Control Sample T Solid 7471A 500-173153

MB 500-173153/7-A Method Blank T Solid 7471A 500-173153

500-53315-1 FC COMPOSITE 4 T Solid 7471A 500-173153

500-53315-2 FC D COMPOSITE 4 T Solid 7471A 500-173153

Prep Batch: 500-173349

LCS 500-173349/2-A Lab Control Sample T Water 3010A

MB 500-173349/1-A Method Blank T Water 3010A

500-53315-6 FC EB 4 T Water 3010A

Prep Batch: 500-173406

LCS 500-173406/3-A Lab Control Sample T Water 3010A

LB 500-173187/1-D TCLP SPLPE Leachate Blank P Solid 3010A 500-173187

500-53315-1 FC COMPOSITE 4 P Solid 3010A 500-173187

500-53315-2 FC D COMPOSITE 4 P Solid 3010A 500-173187

Analysis Batch:500-173438

LB 500-173187/1-B TCLP SPLPE Leachate Blank P Solid 7470A 500-173264

LCS 500-173264/8-A Lab Control Sample T Water 7470A 500-173264

MB 500-173264/7-A Method Blank T Water 7470A 500-173264

500-53315-1 FC COMPOSITE 4 P Solid 7470A 500-173264

500-53315-2 FC D COMPOSITE 4 P Solid 7470A 500-173264

Analysis Batch:500-173517

LCS 500-173349/2-A Lab Control Sample T Water 6010B 500-173349

MB 500-173349/1-A Method Blank T Water 6010B 500-173349

500-53315-6 FC EB 4 T Water 6010B 500-173349

Analysis Batch:500-173518

LB 500-173187/1-D TCLP SPLPE Leachate Blank P Solid 6010B 500-173406

LCS 500-173406/3-A Lab Control Sample T Water 6010B 500-173406

500-53315-1 FC COMPOSITE 4 P Solid 6010B 500-173406

500-53315-2 FC D COMPOSITE 4 P Solid 6010B 500-173406

TestAmerica Chicago

Page 63 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Report Basis

P = TCLP

T = Total

TestAmerica Chicago

Page 64 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-173077

500-53315-1 FC COMPOSITE 4 T Solid Moisture

500-53315-2 FC D COMPOSITE 4 T Solid Moisture

Analysis Batch:500-173079

LCS 500-173079/4 Lab Control Sample T Water 7196A

MB 500-173079/3 Method Blank T Water 7196A

500-53315-6 FC EB 4 T Water 7196A

500-53315-6MS Matrix Spike T Water 7196A

500-53315-6MSD Matrix Spike Duplicate T Water 7196A

Prep Batch: 500-173106

LCS 500-173106/2-A Lab Control Sample T Water 7.3.4

MB 500-173106/1-A Method Blank T Water 7.3.4

500-53315-6 FC EB 4 T Water 7.3.4

Analysis Batch:500-173107

LCS 500-173106/2-A Lab Control Sample T Water 9034 500-173106

MB 500-173106/1-A Method Blank T Water 9034 500-173106

500-53315-6 FC EB 4 T Water 9034 500-173106

Analysis Batch:500-173108

LCS 500-173108/2 Lab Control Sample T Water 9034

MB 500-173108/1 Method Blank T Water 9034

500-53315-6 FC EB 4 T Water 9034

Prep Batch: 500-173173

LCS 500-173173/2-A Lab Control Sample T Water 1664A

MB 500-173173/1-A Method Blank T Water 1664A

500-53315-6 FC EB 4 T Water 1664A

Analysis Batch:500-173178

LCS 500-173173/2-A Lab Control Sample T Water 1664A 500-173173

MB 500-173173/1-A Method Blank T Water 1664A 500-173173

500-53315-6 FC EB 4 T Water 1664A 500-173173

Analysis Batch:500-173236

500-53315-1 FC COMPOSITE 4 T Solid SM 2540G

500-53315-2 FC D COMPOSITE 4 T Solid SM 2540G

Prep Batch: 500-173245

LCS 500-173245/2-A Lab Control Sample T Water 9010B

MB 500-173245/1-A Method Blank T Water 9010B

500-53315-6 FC EB 4 T Water 9010B

TestAmerica Chicago

Page 65 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Prep Batch: 500-173250

LCS 500-173250/2-A Lab Control Sample T Solid 9010B

MB 500-173250/1-A Method Blank T Solid 9010B

500-53315-1 FC COMPOSITE 4 T Solid 9010B

500-53315-2 FC D COMPOSITE 4 T Solid 9010B

500-53315-2MS Matrix Spike T Solid 9010B

500-53315-2MSD Matrix Spike Duplicate T Solid 9010B

Prep Batch: 500-173258

LCS 500-173258/2-A Lab Control Sample T Solid 3060A

LCS 500-173258/3-A Lab Control Sample T Solid 3060A

MB 500-173258/1-A Method Blank T Solid 3060A

500-53315-1 FC COMPOSITE 4 T Solid 3060A

500-53315-2 FC D COMPOSITE 4 T Solid 3060A

Prep Batch: 500-173290

LCS 500-173290/2-A Lab Control Sample T Solid 7.3.4

MB 500-173290/1-A Method Blank T Solid 7.3.4

500-53315-1 FC COMPOSITE 4 T Solid 7.3.4

500-53315-2 FC D COMPOSITE 4 T Solid 7.3.4

Prep Batch: 500-173291

LCS 500-173291/2-A Lab Control Sample T Solid 9030B

MB 500-173291/1-A Method Blank T Solid 9030B

500-53315-1 FC COMPOSITE 4 T Solid 9030B

500-53315-2 FC D COMPOSITE 4 T Solid 9030B

Analysis Batch:500-173311

500-53315-3 FC DISCRETE 4 T Solid Moisture

500-53315-4 FC D DISCRETE 4 T Solid Moisture

Prep Batch: 500-173324

LCS 500-173324/2-A Lab Control Sample T Solid 9071B

MB 500-173324/1-A Method Blank T Solid 9071B

500-53315-1 FC COMPOSITE 4 T Solid 9071B

500-53315-2 FC D COMPOSITE 4 T Solid 9071B

Analysis Batch:500-173330

LCS 500-173324/2-A Lab Control Sample T Solid 9071B 500-173324

MB 500-173324/1-A Method Blank T Solid 9071B 500-173324

500-53315-1 FC COMPOSITE 4 T Solid 9071B 500-173324

500-53315-2 FC D COMPOSITE 4 T Solid 9071B 500-173324

TestAmerica Chicago

Page 66 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

General Chemistry

Analysis Batch:500-173341

LCS 500-173258/2-A Lab Control Sample T Solid 7196A 500-173258

LCS 500-173258/3-A Lab Control Sample T Solid 7196A 500-173258

MB 500-173258/1-A Method Blank T Solid 7196A 500-173258

500-53315-1 FC COMPOSITE 4 T Solid 7196A 500-173258

500-53315-2 FC D COMPOSITE 4 T Solid 7196A 500-173258

Analysis Batch:500-173386

LCS 500-173250/2-A Lab Control Sample T Solid 9014 500-173250

MB 500-173250/1-A Method Blank T Solid 9014 500-173250

500-53315-1 FC COMPOSITE 4 T Solid 9014 500-173250

500-53315-2 FC D COMPOSITE 4 T Solid 9014 500-173250

500-53315-2MS Matrix Spike T Solid 9014 500-173250

500-53315-2MSD Matrix Spike Duplicate T Solid 9014 500-173250

Analysis Batch:500-173387

LCS 500-173245/2-A Lab Control Sample T Water 9014 500-173245

MB 500-173245/1-A Method Blank T Water 9014 500-173245

500-53315-6 FC EB 4 T Water 9014 500-173245

Analysis Batch:500-173472

LCS 500-173290/2-A Lab Control Sample T Solid 9034 500-173290

MB 500-173290/1-A Method Blank T Solid 9034 500-173290

500-53315-1 FC COMPOSITE 4 T Solid 9034 500-173290

500-53315-2 FC D COMPOSITE 4 T Solid 9034 500-173290

Analysis Batch:500-173474

LCS 500-173291/2-A Lab Control Sample T Solid 9034 500-173291

MB 500-173291/1-A Method Blank T Solid 9034 500-173291

500-53315-1 FC COMPOSITE 4 T Solid 9034 500-173291

500-53315-2 FC D COMPOSITE 4 T Solid 9034 500-173291

Analysis Batch:500-173479

500-53315-1 FC COMPOSITE 4 T Solid 9045C

500-53315-2 FC D COMPOSITE 4 T Solid 9045C

Analysis Batch:500-173558

500-53315-1 FC COMPOSITE 4 T Solid 1010

500-53315-2 FC D COMPOSITE 4 T Solid 1010

Report Basis

T = Total

TestAmerica Chicago

Page 67 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-1 FC COMPOSITE 4

P:3050B 500-53315-A-1-A 500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B 500-53315-A-1-A 500-173224 500-173139 12/17/2012 22:46 1 TAL CHI TDS

P:3010A 500-53315-A-1-N 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B 500-53315-A-1-N 500-173518 500-173406 12/19/2012 22:29 1 TAL CHI TDS

P:7470A 500-53315-A-1-J 500-173438 500-173264 12/18/2012 13:00 1 TAL CHI BJB

A:7470A 500-53315-A-1-J 500-173438 500-173264 12/19/2012 10:24 1 TAL CHI BJB

P:7471A 500-53315-A-1-F 500-173328 500-173153 12/17/2012 14:00 1 TAL CHI BJB

A:7471A 500-53315-A-1-F 500-173328 500-173153 12/18/2012 14:00 1 TAL CHI BJB

A:1010 500-53315-A-1 500-173558 12/19/2012 17:21 1 TAL CHI APW

P:3060A 500-53315-A-1-I 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A 500-53315-A-1-I 500-173341 500-173258 12/18/2012 15:49 1 TAL CHI APW

P:9010B 500-53315-A-1-H 500-173386 500-173250 12/18/2012 10:35 1 TAL CHI EAT

A:9014 500-53315-A-1-H 500-173386 500-173250 12/18/2012 14:24 1 TAL CHI EAT

P:7.3.4 500-53315-A-1-K 500-173472 500-173290 12/19/2012 10:40 1 TAL CHI CLM

A:9034 500-53315-A-1-K 500-173472 500-173290 12/19/2012 12:18 1 TAL CHI CLM

P:9030B 500-53315-A-1-L 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 500-53315-A-1-L 500-173474 500-173291 12/19/2012 13:36 1 TAL CHI CLM

A:9045C 500-53315-A-1 500-173479 12/20/2012 15:12 1 TAL CHI CLM

P:9071B 500-53315-A-1-M 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B 500-53315-A-1-M 500-173330 500-173324 12/19/2012 11:01 1 TAL CHI MTB

A:Moisture 500-53315-A-1 500-173077 12/15/2012 12:43 1 TAL CHI CMV

A:SM 2540G 500-53315-A-1 500-173236 12/18/2012 07:34 1 TAL CHI CMV

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-1 MS FC COMPOSITE 4

P:3050B 500-53315-A-1-C MS 500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B 500-53315-A-1-C MS 500-173224 500-173139 12/17/2012 23:04 1 TAL CHI TDS

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-1 MSD FC COMPOSITE 4

P:3050B 500-53315-A-1-D 

MSD

500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B 500-53315-A-1-D 

MSD

500-173224 500-173139 12/17/2012 23:10 1 TAL CHI TDS

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 68 of 383 01/03/2013
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Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-1 DU FC COMPOSITE 4

P:3050B 500-53315-A-1-B DU 500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B 500-53315-A-1-B DU 500-173224 500-173139 12/17/2012 22:58 1 TAL CHI TDS

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-1 SD FC COMPOSITE 4

P:3050B 500-53315-A-1-A SD 

^5

500-173224 500-173139 12/17/2012 08:50 5 TAL CHI LAH

A:6010B 500-53315-A-1-A SD 

^5

500-173224 500-173139 12/17/2012 22:52 5 TAL CHI TDS

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-2 FC D COMPOSITE 4

P:3050B 500-53315-A-2-A 500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B 500-53315-A-2-A 500-173224 500-173139 12/17/2012 23:17 1 TAL CHI TDS

P:3010A 500-53315-A-2-L 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B 500-53315-A-2-L 500-173518 500-173406 12/19/2012 22:35 1 TAL CHI TDS

P:7470A 500-53315-A-2-H 500-173438 500-173264 12/18/2012 13:00 1 TAL CHI BJB

A:7470A 500-53315-A-2-H 500-173438 500-173264 12/19/2012 10:29 1 TAL CHI BJB

P:7471A 500-53315-A-2-B 500-173328 500-173153 12/17/2012 14:00 1 TAL CHI BJB

A:7471A 500-53315-A-2-B 500-173328 500-173153 12/18/2012 14:01 1 TAL CHI BJB

A:1010 500-53315-A-2 500-173558 12/19/2012 18:00 1 TAL CHI APW

P:3060A 500-53315-A-2-G 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A 500-53315-A-2-G 500-173341 500-173258 12/18/2012 15:50 1 TAL CHI APW

P:9010B 500-53315-A-2-D 500-173386 500-173250 12/18/2012 10:35 1 TAL CHI EAT

A:9014 500-53315-A-2-D 500-173386 500-173250 12/18/2012 14:24 1 TAL CHI EAT

P:7.3.4 500-53315-A-2-I 500-173472 500-173290 12/19/2012 10:45 1 TAL CHI CLM

A:9034 500-53315-A-2-I 500-173472 500-173290 12/19/2012 12:19 1 TAL CHI CLM

P:9030B 500-53315-A-2-J 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 500-53315-A-2-J 500-173474 500-173291 12/19/2012 13:37 1 TAL CHI CLM

A:9045C 500-53315-A-2 500-173479 12/20/2012 16:11 1 TAL CHI CLM

P:9071B 500-53315-A-2-K 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B 500-53315-A-2-K 500-173330 500-173324 12/19/2012 11:12 1 TAL CHI MTB

A:Moisture 500-53315-A-2 500-173077 12/15/2012 12:43 1 TAL CHI CMV

A:SM 2540G 500-53315-A-2 500-173236 12/18/2012 07:34 1 TAL CHI CMV

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 69 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-2 MS FC D COMPOSITE 4

P:9010B 500-53315-A-2-E MS 500-173386 500-173250 12/18/2012 10:35 1 TAL CHI EAT

A:9014 500-53315-A-2-E MS 500-173386 500-173250 12/18/2012 14:25 1 TAL CHI EAT

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 15:15 Received Date/Time: 500-53315-2 MSD FC D COMPOSITE 4

P:9010B 500-53315-A-2-F 

MSD

500-173386 500-173250 12/18/2012 10:35 1 TAL CHI EAT

A:9014 500-53315-A-2-F 

MSD

500-173386 500-173250 12/18/2012 14:25 1 TAL CHI EAT

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:45 Received Date/Time: 500-53315-3 FC DISCRETE 4

P:5030B 500-53315-A-3 500-173225 12/18/2012 09:30 1 TAL CHI BDW

A:8260B 500-53315-A-3 500-173225 12/18/2012 09:30 1 TAL CHI BDW

P:5030B 500-53315-A-3-A DL 500-173509 500-173238 12/18/2012 07:45 50 TAL CHI BDW

A:8260B 500-53315-A-3-A DL 500-173509 500-173238 12/20/2012 02:16 50 TAL CHI BDA

A:Moisture 500-53315-A-3 500-173311 12/18/2012 13:59 1 TAL CHI CMV

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:45 Received Date/Time: 500-53315-3 MS FC DISCRETE 4

P:5030B 500-53315-A-3 MS 500-173225 12/18/2012 09:54 1 TAL CHI BDW

A:8260B 500-53315-A-3 MS 500-173225 12/18/2012 09:54 1 TAL CHI BDW

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:45 Received Date/Time: 500-53315-3 MSD FC DISCRETE 4

P:5030B 500-53315-A-3 MSD 500-173225 12/18/2012 10:17 1 TAL CHI BDW

A:8260B 500-53315-A-3 MSD 500-173225 12/18/2012 10:17 1 TAL CHI BDW

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 70 of 383 01/03/2013
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Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:45 Received Date/Time: 500-53315-4 FC D DISCRETE 4

P:5030B 500-53315-A-4 500-173225 12/18/2012 10:40 1 TAL CHI BDW

A:8260B 500-53315-A-4 500-173225 12/18/2012 10:40 1 TAL CHI BDW

P:5030B 500-53315-A-4-A DL 500-173509 500-173238 12/18/2012 07:45 50 TAL CHI BDW

A:8260B 500-53315-A-4-A DL 500-173509 500-173238 12/20/2012 02:40 50 TAL CHI BDA

A:Moisture 500-53315-A-4 500-173311 12/18/2012 13:59 1 TAL CHI CMV

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 00:00 Received Date/Time: 500-53315-5 TRIP BLANK

P:5030B 500-53315-B-5 500-173508 12/20/2012 01:08 1 TAL CHI BDA

A:8260B 500-53315-B-5 500-173508 12/20/2012 01:08 1 TAL CHI BDA

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:30 Received Date/Time: 500-53315-6 FC EB 4

P:5030B 500-53315-B-6 500-173508 12/20/2012 01:49 1 TAL CHI BDA

A:8260B 500-53315-B-6 500-173508 12/20/2012 01:49 1 TAL CHI BDA

P:3010A 500-53315-E-6-E 500-173517 500-173349 12/18/2012 15:30 1 TAL CHI RL

A:6010B 500-53315-E-6-E 500-173517 500-173349 12/19/2012 14:57 1 TAL CHI TDS

P:7470A 500-53315-E-6-A 500-173280 500-173172 12/17/2012 13:00 1 TAL CHI BJB

A:7470A 500-53315-E-6-A 500-173280 500-173172 12/18/2012 09:49 1 TAL CHI BJB

P:1664A 500-53315-H-6-A 500-173178 500-173173 12/18/2012 07:24 1 TAL CHI MTB

A:1664A 500-53315-H-6-A 500-173178 500-173173 12/18/2012 11:14 1 TAL CHI MTB

A:7196A 500-53315-F-6 500-173079 12/15/2012 13:22 1 TAL CHI APW

P:9010B 500-53315-D-6-A 500-173387 500-173245 12/18/2012 08:30 1 TAL CHI EAT

A:9014 500-53315-D-6-A 500-173387 500-173245 12/18/2012 13:54 1 TAL CHI EAT

P:7.3.4 500-53315-G-6-A 500-173107 500-173106 12/17/2012 00:13 1 TAL CHI CLB

A:9034 500-53315-G-6-A 500-173107 500-173106 12/17/2012 01:08 1 TAL CHI CLB

A:9034 500-53315-G-6 500-173108 12/17/2012 01:11 1 TAL CHI CLB

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:30 Received Date/Time: 500-53315-6 MS FC EB 4

P:7470A 500-53315-E-6-C MS 500-173280 500-173172 12/17/2012 13:00 1 TAL CHI BJB

A:7470A 500-53315-E-6-C MS 500-173280 500-173172 12/18/2012 09:57 1 TAL CHI BJB

A:7196A 500-53315-F-6 MS 500-173079 12/15/2012 13:22 1 TAL CHI APW

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 71 of 383 01/03/2013
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Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:30 Received Date/Time: 500-53315-6 MSD FC EB 4

P:7470A 500-53315-E-6-D 

MSD

500-173280 500-173172 12/17/2012 13:00 1 TAL CHI BJB

A:7470A 500-53315-E-6-D 

MSD

500-173280 500-173172 12/18/2012 09:59 1 TAL CHI BJB

A:7196A 500-53315-F-6 MSD 500-173079 12/15/2012 13:23 1 TAL CHI APW

12/15/2012 09:10

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: 12/14/2012 14:30 Received Date/Time: 500-53315-6 DU FC EB 4

P:7470A 500-53315-E-6-B DU 500-173280 500-173172 12/17/2012 13:00 1 TAL CHI BJB

A:7470A 500-53315-E-6-B DU 500-173280 500-173172 12/18/2012 09:55 1 TAL CHI BJB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 72 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

MB N/A

P:5030B MB 500-173225/4 500-173225 12/18/2012 08:30 1 TAL CHI BDW

A:8260B MB 500-173225/4 500-173225 12/18/2012 08:30 1 TAL CHI BDW

P:5030B MB 500-173508/6 500-173508 12/20/2012 00:43 1 TAL CHI BDA

A:8260B MB 500-173508/6 500-173508 12/20/2012 00:43 1 TAL CHI BDA

A:8260B MB 500-173509/6 500-173509 12/20/2012 00:43 1 TAL CHI BDA

P:3050B MB 500-173139/1-A 500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B MB 500-173139/1-A 500-173224 500-173139 12/17/2012 21:04 1 TAL CHI TDS

P:3010A MB 500-173349/1-A 500-173517 500-173349 12/18/2012 15:30 1 TAL CHI RL

A:6010B MB 500-173349/1-A 500-173517 500-173349 12/19/2012 13:52 1 TAL CHI TDS

P:7470A MB 500-173172/7-A 500-173280 500-173172 12/17/2012 13:00 1 TAL CHI BJB

A:7470A MB 500-173172/7-A 500-173280 500-173172 12/18/2012 09:09 1 TAL CHI BJB

P:7470A MB 500-173264/7-A 500-173438 500-173264 12/18/2012 13:00 1 TAL CHI BJB

A:7470A MB 500-173264/7-A 500-173438 500-173264 12/19/2012 10:08 1 TAL CHI BJB

P:7471A MB 500-173153/7-A 500-173328 500-173153 12/17/2012 14:00 1 TAL CHI BJB

A:7471A MB 500-173153/7-A 500-173328 500-173153 12/18/2012 13:04 1 TAL CHI BJB

P:1664A MB 500-173173/1-A 500-173178 500-173173 12/18/2012 05:25 1 TAL CHI MTB

A:1664A MB 500-173173/1-A 500-173178 500-173173 12/18/2012 10:05 1 TAL CHI MTB

A:7196A MB 500-173079/3 500-173079 12/15/2012 13:21 1 TAL CHI APW

P:3060A MB 500-173258/1-A 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A MB 500-173258/1-A 500-173341 500-173258 12/18/2012 15:46 1 TAL CHI APW

P:9010B MB 500-173245/1-A 500-173387 500-173245 12/18/2012 08:30 1 TAL CHI EAT

A:9014 MB 500-173245/1-A 500-173387 500-173245 12/18/2012 13:45 1 TAL CHI EAT

P:9010B MB 500-173250/1-A 500-173386 500-173250 12/18/2012 10:35 1 TAL CHI EAT

A:9014 MB 500-173250/1-A 500-173386 500-173250 12/18/2012 14:23 1 TAL CHI EAT

P:7.3.4 MB 500-173106/1-A 500-173107 500-173106 12/17/2012 00:01 1 TAL CHI CLB

A:9034 MB 500-173106/1-A 500-173107 500-173106 12/17/2012 00:19 1 TAL CHI CLB

A:9034 MB 500-173108/1 500-173108 12/17/2012 00:19 1 TAL CHI CLB

P:7.3.4 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 10:05 1 TAL CHI CLM

A:9034 MB 500-173290/1-A 500-173472 500-173290 12/19/2012 12:15 1 TAL CHI CLM

P:9030B MB 500-173291/1-A 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 MB 500-173291/1-A 500-173474 500-173291 12/19/2012 13:35 1 TAL CHI CLM

P:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B MB 500-173324/1-A 500-173330 500-173324 12/19/2012 09:20 1 TAL CHI MTB

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LB N/A

P:3010A LB 500-173187/1-D 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B LB 500-173187/1-D 500-173518 500-173406 12/19/2012 21:07 1 TAL CHI TDS

P:7470A LB 500-173187/1-B 500-173438 500-173264 12/18/2012 13:00 1 TAL CHI BJB

A:7470A LB 500-173187/1-B 500-173438 500-173264 12/19/2012 10:12 1 TAL CHI BJB

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 73 of 383 01/03/2013
Quality Control Results

Client: Project Integration, Inc Job Number: 500-53315-1

Laboratory Chronicle

Lab ID:

Method Bottle ID Run

Analysis 

Batch Prep Batch

Date Prepared / 

Analyzed Dil Lab Analyst

Client ID:

Sample Date/Time: N/A Received Date/Time: N/A

LCS N/A

P:5030B LCS 500-173225/5 500-173225 12/18/2012 08:53 1 TAL CHI BDW

A:8260B LCS 500-173225/5 500-173225 12/18/2012 08:53 1 TAL CHI BDW

P:5030B LCS 500-173508/4 500-173508 12/19/2012 23:54 1 TAL CHI BDA

A:8260B LCS 500-173508/4 500-173508 12/19/2012 23:54 1 TAL CHI BDA

A:8260B LCS 500-173509/4 500-173509 12/19/2012 23:54 1 TAL CHI BDA

P:3050B LCS 500-173139/2-A 500-173224 500-173139 12/17/2012 08:50 1 TAL CHI LAH

A:6010B LCS 500-173139/2-A 500-173224 500-173139 12/17/2012 21:10 1 TAL CHI TDS

P:3010A LCS 500-173349/2-A 500-173517 500-173349 12/18/2012 15:30 1 TAL CHI RL

A:6010B LCS 500-173349/2-A 500-173517 500-173349 12/19/2012 13:58 1 TAL CHI TDS

P:3010A LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 08:20 1 TAL CHI LAH

A:6010B LCS 500-173406/3-A 500-173518 500-173406 12/19/2012 21:20 1 TAL CHI TDS

P:7470A LCS 500-173172/8-A 500-173280 500-173172 12/17/2012 13:00 1 TAL CHI BJB

A:7470A LCS 500-173172/8-A 500-173280 500-173172 12/18/2012 09:11 1 TAL CHI BJB

P:7470A LCS 500-173264/8-A 500-173438 500-173264 12/18/2012 13:00 1 TAL CHI BJB

A:7470A LCS 500-173264/8-A 500-173438 500-173264 12/19/2012 10:10 1 TAL CHI BJB

P:7471A LCS 500-173153/8-A 500-173328 500-173153 12/17/2012 14:00 1 TAL CHI BJB

A:7471A LCS 500-173153/8-A 500-173328 500-173153 12/18/2012 13:10 1 TAL CHI BJB

P:1664A LCS 500-173173/2-A 500-173178 500-173173 12/18/2012 05:35 1 TAL CHI MTB

A:1664A LCS 500-173173/2-A 500-173178 500-173173 12/18/2012 10:11 1 TAL CHI MTB

A:7196A LCS 500-173079/4 500-173079 12/15/2012 13:21 1 TAL CHI APW

P:3060A LCS 500-173258/2-A 500-173341 500-173258 12/18/2012 10:00 1 TAL CHI APW

A:7196A LCS 500-173258/2-A 500-173341 500-173258 12/18/2012 15:46 1 TAL CHI APW

P:3060A LCS 500-173258/3-A 500-173341 500-173258 12/18/2012 10:00 50 TAL CHI APW

A:7196A LCS 500-173258/3-A 500-173341 500-173258 12/18/2012 15:47 50 TAL CHI APW

P:9010B LCS 500-173245/2-A 500-173387 500-173245 12/18/2012 08:30 1 TAL CHI EAT

A:9014 LCS 500-173245/2-A 500-173387 500-173245 12/18/2012 13:45 1 TAL CHI EAT

P:9010B LCS 500-173250/2-A 500-173386 500-173250 12/18/2012 10:35 1 TAL CHI EAT

A:9014 LCS 500-173250/2-A 500-173386 500-173250 12/18/2012 14:23 1 TAL CHI EAT

A:9034 LCS 500-173108/2 500-173108 12/17/2012 00:21 1 TAL CHI CLB

P:7.3.4 LCS 500-173106/2-A 500-173107 500-173106 12/17/2012 00:05 1 TAL CHI CLB

A:9034 LCS 500-173106/2-A 500-173107 500-173106 12/17/2012 00:35 1 TAL CHI CLB

P:7.3.4 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 10:10 1 TAL CHI CLM

A:9034 LCS 500-173290/2-A 500-173472 500-173290 12/19/2012 12:15 1 TAL CHI CLM

P:9030B LCS 500-173291/2-A 500-173474 500-173291 12/19/2012 11:25 1 TAL CHI CLM

A:9034 LCS 500-173291/2-A 500-173474 500-173291 12/19/2012 13:35 1 TAL CHI CLM

P:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 05:10 1 TAL CHI MTB

A:9071B LCS 500-173324/2-A 500-173330 500-173324 12/19/2012 09:31 1 TAL CHI MTB

Lab References:

TAL CHI = TestAmerica Chicago

TestAmerica Chicago A = Analytical Method P = Prep Method 

Page 74 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1664 HEM_00060 04/26/13 Mallin / JTBaker, Lot E50600 / K19H00 (Purchased Reagent) HEM (Oil & Grease) 8000 mg/L

SGT-HEM 4000 mg/L

8260 IS WK_00381 12/03/12 11/19/12 1, Lot NA 5 mL 8260 IS SK_00026 5 mL 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

.8260 IS SK_00026 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW IS_00102 11/20/12 11/06/12 MEOH, Lot DA946 20 mL 8260 IS SK_00026 4000 uL 1,4-Dichlorobenzene-d4 50 ug/mL

1,4-Difluorobenzene 50 ug/mL

Chlorobenzene-d5 50 ug/mL

Pentafluorobenzene 50 ug/mL

.8260 IS SK_00026 08/31/14 RESTEK, Lot AO88671 (Purchased Reagent) 1,4-Dichlorobenzene-d4 250 ug/mL

1,4-Difluorobenzene 250 ug/mL

Chlorobenzene-d5 250 ug/mL

Pentafluorobenzene 250 ug/mL

8260 LOW SS_00104 11/20/12 11/06/12 MEOH, Lot DA946 20 mL 8260 SS SK_00031 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 LOW SS_00107 12/27/12 12/13/12 MEOH, Lot DA946 20 mL 8260 SS SK_00032 4000 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 SS WK_00378 12/03/12 11/19/12 1, Lot NA 5 mL 8260 SS SK_00031 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

.8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

8260 STD WK_00211 11/28/12 11/14/12 METHANOL, Lot NA 2 mL 8260 STD STK_00032 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

Page 75 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

Page 76 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00032 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Page 77 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Page 78 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

Page 79 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

ACR/NITRSTDWK_00204 11/21/12 11/14/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Page 80 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

.ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

GAS STD WK RE_00243 11/21/12 11/14/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

GAS STD WK RE_00244 11/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

5 mL 8260 SS WK_00385 0.8656 1,2-Dichloroethane-d4 (Surr) 43.28 ug/L

uL

INST16 IS/SS_00223 01/01/13 12/18/12 1, Lot NA

4-Bromofluorobenzene (Surr) 43.28 ug/L

Dibromofluoromethane 43.28 ug/L

Toluene-d8 (Surr) 43.28 ug/L

.8260 SS WK_00385 01/01/13 12/18/12 1, Lot NA 5 mL 8260 SS SK_00032 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00032 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

KET/CS2 STDWK_00179 11/28/12 11/14/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

Page 81 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

KET/CS2 STDWK_00184 12/25/12 12/11/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00014 2 mL 2-Butanone (MEK) 100 ug/mL

Acetone 100 ug/mL

.KET/CS2 SK_00014 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

Acetone 100 ug/mL

level 1_00011 12/31/16 03/20/12 1, Lot CY647 1 mL level1std5ppm_00006 100 uL Benzene 0.5 ug/mL

Ethylbenzene 0.5 ug/mL

m-Xylene & p-Xylene 1 ug/mL

o-Xylene 0.5 ug/mL

Toluene 0.5 ug/mL

Trichloroethene 0.5 ug/mL

Vinyl chloride 0.5 ug/mL

.level1std5ppm_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level18260wk_00006 100 uL Benzene 5 ug/mL

Ethylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

o-Xylene 5 ug/mL

Toluene 5 ug/mL

Trichloroethene 5 ug/mL

level1gaswk_00006 100 uL Vinyl chloride 5 ug/mL

..level18260wk_00006 06/30/12 03/22/11 1, Lot NA 1 mL level18260sk_00001 1 mL Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Trichloroethene 100 ug/mL

...level18260sk_00001 06/30/12 Restek, Lot AO67921 (Purchased Reagent) Benzene 100 ug/mL

Ethylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

o-Xylene 100 ug/mL

Toluene 100 ug/mL

Page 82 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Trichloroethene 100 ug/mL

..level1gaswk_00006 02/28/12 03/22/11 1, Lot CY647 2 mL level1gaspt_00005 100 uL Vinyl chloride 100 ug/mL

...level1gaspt_00005 02/28/12 03/22/11 MEOH, Lot NA 1 mL level1gassk_00001 1 mL Vinyl chloride 2000 ug/mL

....level1gassk_00001 02/28/12 SUPELCO, Lot LB65254 (Purchased Reagent) Vinyl chloride 2000 ug/mL

LOW8260SS WK_00042 12/03/12 11/19/12 1, Lot DA057 1 mL 8260 SS WK_00378 200 uL 1,2-Dichloroethane-d4 (Surr) 50 ug/mL

4-Bromofluorobenzene (Surr) 50 ug/mL

Dibromofluoromethane 50 ug/mL

Toluene-d8 (Surr) 50 ug/mL

.8260 SS WK_00378 12/03/12 11/19/12 1, Lot NA 5 mL 8260 SS SK_00031 5 mL 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

..8260 SS SK_00031 07/31/14 RESTEK, Lot A088175 (Purchased Reagent) 1,2-Dichloroethane-d4 (Surr) 250 ug/mL

4-Bromofluorobenzene (Surr) 250 ug/mL

Dibromofluoromethane 250 ug/mL

Toluene-d8 (Surr) 250 ug/mL

LOW8260STD WK_00208 11/21/12 11/14/12 METHANOL, Lot DG596 1 mL 8260 STD WK_00211 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Page 83 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00243 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Dichlorofluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00179 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00174 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00211 11/28/12 11/14/12 METHANOL, Lot NA 2 mL 8260 STD STK_00032 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

Page 84 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

Page 85 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00032 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

Page 86 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00243 11/21/12 11/14/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Dichlorofluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00179 11/28/12 11/14/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00174 11/21/12 11/14/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOW8260STD WK_00209 11/26/12 11/19/12 1, Lot DG596 1 mL 8260 STD WK_00212 50 uL 1,1,1,2-Tetrachloroethane 5 ug/mL

1,1,1-Trichloroethane 5 ug/mL

1,1,2,2-Tetrachloroethane 5 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

5 ug/mL

Page 87 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,1,2-Trichloroethane 5 ug/mL

1,1-Dichloroethane 5 ug/mL

1,1-Dichloroethene 5 ug/mL

1,1-Dichloropropene 5 ug/mL

1,2,3-Trichlorobenzene 5 ug/mL

1,2,3-Trichloropropane 5 ug/mL

1,2,4-Trichlorobenzene 5 ug/mL

1,2,4-Trimethylbenzene 5 ug/mL

1,2-Dibromo-3-Chloropropane 5 ug/mL

1,2-Dichlorobenzene 5 ug/mL

1,2-Dichloroethane 5 ug/mL

1,2-Dichloropropane 5 ug/mL

1,3,5-Trimethylbenzene 5 ug/mL

1,3-Dichlorobenzene 5 ug/mL

1,3-Dichloropropane 5 ug/mL

1,4-Dichlorobenzene 5 ug/mL

1-Chlorohexane 5 ug/mL

2,2-Dichloropropane 5 ug/mL

2-Chlorotoluene 5 ug/mL

4-Chlorotoluene 5 ug/mL

4-Isopropyltoluene 5 ug/mL

Benzene 5 ug/mL

Bromobenzene 5 ug/mL

Bromoform 5 ug/mL

Carbon tetrachloride 5 ug/mL

Chlorobenzene 5 ug/mL

Chlorobromomethane 5 ug/mL

Chlorodibromomethane 5 ug/mL

Chloroform 5 ug/mL

cis-1,2-Dichloroethene 5 ug/mL

cis-1,3-Dichloropropene 5 ug/mL

Dibromomethane 5 ug/mL

Dichlorobromomethane 5 ug/mL

Ethylbenzene 5 ug/mL

Ethylene Dibromide 5 ug/mL

Hexachlorobutadiene 5 ug/mL

Isopropylbenzene 5 ug/mL

m-Xylene & p-Xylene 10 ug/mL

Methyl tert-butyl ether 5 ug/mL

Methylene Chloride 5 ug/mL

n-Butylbenzene 5 ug/mL

N-Propylbenzene 5 ug/mL

Naphthalene 5 ug/mL

o-Xylene 5 ug/mL

sec-Butylbenzene 5 ug/mL

Styrene 5 ug/mL

tert-Butylbenzene 5 ug/mL

Tetrachloroethene 5 ug/mL

Page 88 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Tetrahydrofuran 5 ug/mL

Toluene 5 ug/mL

trans-1,2-Dichloroethene 5 ug/mL

trans-1,3-Dichloropropene 5 ug/mL

Trichloroethene 5 ug/mL

GAS STD WK RE_00244 50 uL Bromomethane 5 ug/mL

Chloroethane 5 ug/mL

Chloromethane 5 ug/mL

Dichlorodifluoromethane 5 ug/mL

Trichlorofluoromethane 5 ug/mL

Vinyl chloride 5 ug/mL

KET/CS2 STDWK_00180 50 uL 2-Butanone (MEK) 5 ug/mL

2-Hexanone 5 ug/mL

4-Methyl-2-pentanone (MIBK) 5 ug/mL

Acetone 5 ug/mL

Carbon disulfide 5 ug/mL

VA/2CEVESTDWK_00175 50 uL 2-Chloroethyl vinyl ether 5 ug/mL

Vinyl acetate 5 ug/mL

.8260 STD WK_00212 12/03/12 11/19/12 METHANOL, Lot NA 2 mL 8260 STD STK_00033 2 mL 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Page 89 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

..8260 STD STK_00033 08/31/14 Restek, Lot A088677 (Purchased Reagent) 1,1,1,2-Tetrachloroethane 100 ug/mL

1,1,1-Trichloroethane 100 ug/mL

1,1,2,2-Tetrachloroethane 100 ug/mL

1,1,2-Trichloro-1,2,2-trifluor

oethane

100 ug/mL

1,1,2-Trichloroethane 100 ug/mL

1,1-Dichloroethane 100 ug/mL

1,1-Dichloroethene 100 ug/mL

1,1-Dichloropropene 100 ug/mL

1,2,3-Trichlorobenzene 100 ug/mL

1,2,3-Trichloropropane 100 ug/mL

1,2,4-Trichlorobenzene 100 ug/mL

1,2,4-Trimethylbenzene 100 ug/mL

1,2-Dibromo-3-Chloropropane 100 ug/mL

1,2-Dichlorobenzene 100 ug/mL

1,2-Dichloroethane 100 ug/mL

1,2-Dichloropropane 100 ug/mL

1,3,5-Trimethylbenzene 100 ug/mL

1,3-Dichlorobenzene 100 ug/mL

1,3-Dichloropropane 100 ug/mL

Page 90 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

1,4-Dichlorobenzene 100 ug/mL

1-Chlorohexane 100 ug/mL

2,2-Dichloropropane 100 ug/mL

2-Chlorotoluene 100 ug/mL

4-Chlorotoluene 100 ug/mL

4-Isopropyltoluene 100 ug/mL

Benzene 100 ug/mL

Bromobenzene 100 ug/mL

Bromoform 100 ug/mL

Carbon tetrachloride 100 ug/mL

Chlorobenzene 100 ug/mL

Chlorobromomethane 100 ug/mL

Chlorodibromomethane 100 ug/mL

Chloroform 100 ug/mL

cis-1,2-Dichloroethene 100 ug/mL

cis-1,3-Dichloropropene 100 ug/mL

Dibromomethane 100 ug/mL

Dichlorobromomethane 100 ug/mL

Ethylbenzene 100 ug/mL

Ethylene Dibromide 100 ug/mL

Hexachlorobutadiene 100 ug/mL

Isopropylbenzene 100 ug/mL

m-Xylene & p-Xylene 200 ug/mL

Methyl tert-butyl ether 100 ug/mL

Methylene Chloride 100 ug/mL

n-Butylbenzene 100 ug/mL

N-Propylbenzene 100 ug/mL

Naphthalene 100 ug/mL

o-Xylene 100 ug/mL

sec-Butylbenzene 100 ug/mL

Styrene 100 ug/mL

tert-Butylbenzene 100 ug/mL

Tetrachloroethene 100 ug/mL

Tetrahydrofuran 100 ug/mL

Toluene 100 ug/mL

trans-1,2-Dichloroethene 100 ug/mL

trans-1,3-Dichloropropene 100 ug/mL

Trichloroethene 100 ug/mL

.GAS STD WK RE_00244 11/26/12 11/19/12 METHANOL, Lot NA 2 mL GAS STD SK_00027 2 mL Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

..GAS STD SK_00027 08/31/14 RESTEK, Lot A088739 (Purchased Reagent) Bromomethane 100 ug/mL

Chloroethane 100 ug/mL

Chloromethane 100 ug/mL

Dichlorodifluoromethane 100 ug/mL

Page 91 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Trichlorofluoromethane 100 ug/mL

Vinyl chloride 100 ug/mL

.KET/CS2 STDWK_00180 12/03/12 11/19/12 METHANOL, Lot NA 2 mL KET/CS2 SK_00013 2 mL 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

..KET/CS2 SK_00013 11/30/13 Restek, Lot A088681 (Purchased Reagent) 2-Butanone (MEK) 100 ug/mL

2-Hexanone 100 ug/mL

4-Methyl-2-pentanone (MIBK) 100 ug/mL

Acetone 100 ug/mL

Carbon disulfide 100 ug/mL

.VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

..2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

...2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

..VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

...VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

LOWACRSTD WK_00188 11/21/12 11/14/12 MEOH, Lot DG596 1 mL ACR/NITRSTDWK_00204 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00204 11/21/12 11/14/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

LOWACRSTD WK_00189 11/26/12 11/19/12 MEOH, Lot DG596 1 mL ACR/NITRSTDWK_00205 100 uL Acetonitrile 80 ug/mL

Acrolein 400 ug/mL

Acrylonitrile 80 ug/mL

Propionitrile 80 ug/mL

.ACR/NITRSTDWK_00205 11/26/12 11/19/12 METHANOL, Lot NA 2 mL ACRNITSTDSK_00032 2 mL Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

..ACRNITSTDSK_00032 12/31/12 Restek, Lot A090686 (Purchased Reagent) Acetonitrile 800 ug/mL

Acrolein 4000 ug/mL

Acrylonitrile 800 ug/mL

Propionitrile 800 ug/mL

M11FSTKHG_00001 05/31/17 ULTRA, Lot L00365 (Purchased Reagent) Mercury 1000 ug/mL

M12ASTKHG_00001 01/01/13 Inorganic Ventures, Lot E2-HG02091 (Purchased Reagent) Mercury 1000 ug/mL

M12JSPKIC_00002 05/23/13 10/04/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

Page 92 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Page 93 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12KSPKIC_00001 05/23/13 11/20/12 1, Lot N\A 500 mL M12ESTKIC_00003 3 mL As 10 ug/mL

M12ESTKIC_00006 4 mL Lead 10 ug/mL

M12ESTKIC_00010 2.5 mL Tl 10 ug/mL

M12ESTKIC_00011 50 mL Al 200 ug/mL

Barium 200 ug/mL

Ca 1000 ug/mL

K 1000 ug/mL

Mg 1000 ug/mL

Na 1000 ug/mL

M12ESTKIC_00012 50 mL As 10 ug/mL

B 100 ug/mL

Be 5 ug/mL

Bi 50 ug/mL

Cd 5 ug/mL

Chromium 20 ug/mL

Co 50 ug/mL

Copper 25 ug/mL

Fe 100 ug/mL

Lead 10 ug/mL

Li 50 ug/mL

Mn 50 ug/mL

Nickel 50 ug/mL

Se 10 ug/mL

Sr 100 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 50 ug/mL

M12ESTKIC_00013 50 mL Ag 5 ug/mL

Mo 100 ug/mL

Page 94 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Sb 50 ug/mL

Si 500 ug/mL

Sn 100 ug/mL

Ti 100 ug/mL

M12ISTKIC_00004 4.5 mL Se 10 ug/mL

.M12ESTKIC_00003 06/01/13 IV, Lot F2-AS02083 (Purchased Reagent) As 1000 ug/mL

.M12ESTKIC_00006 06/01/13 IV, Lot F2-PB03035 (Purchased Reagent) Lead 1000 ug/mL

.M12ESTKIC_00010 06/01/13 IV, Lot E2-TL01124 (Purchased Reagent) Tl 1000 ug/mL

.M12ESTKIC_00011 05/23/13 EE, Lot 1214205 (Purchased Reagent) Al 2000 ug/mL

Barium 2000 ug/mL

Ca 10000 ug/mL

K 10000 ug/mL

Mg 10000 ug/mL

Na 10000 ug/mL

.M12ESTKIC_00012 05/23/13 EE, Lot 1214206 (Purchased Reagent) As 40 ug/mL

B 1000 ug/mL

Be 50 ug/mL

Bi 500 ug/mL

Cd 50 ug/mL

Chromium 200 ug/mL

Co 500 ug/mL

Copper 250 ug/mL

Fe 1000 ug/mL

Lead 20 ug/mL

Li 500 ug/mL

Mn 500 ug/mL

Nickel 500 ug/mL

Se 10 ug/mL

Sr 1000 ug/mL

Tl 50 ug/mL

Vanadium 500 ug/mL

Zinc 500 ug/mL

.M12ESTKIC_00013 05/23/13 EE, Lot 1214331 (Purchased Reagent) Ag 50 ug/mL

Mo 1000 ug/mL

Sb 500 ug/mL

Si 5000 ug/mL

Sn 1000 ug/mL

Ti 1000 ug/mL

.M12ISTKIC_00004 09/01/13 IV, Lot E2-SE02033 (Purchased Reagent) Se 1000 ug/mL

M12LCCVIC_00001 07/10/13 12/10/12 1, Lot N/A 1000 mL M12GSTKIC_00002 10 mL Barium 0.5 ug/mL

Chromium 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.5 ug/mL

Nickel 0.5 ug/mL

Vanadium 5 ug/mL

Zinc 0.5 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Page 95 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12LCRIIC_00001 06/01/13 12/03/12 1, Lot NA 1000 mL M12ESTKIC_00002 2 mL Barium 20 ug/L

Chromium 20 ug/L

Copper 20 ug/L

Lead 10 ug/L

Nickel 20 ug/L

Vanadium 10 ug/L

Zinc 40 ug/L

.M12ESTKIC_00002 06/01/13 IV, Lot F2-MEB423074 (Purchased Reagent) Barium 10 ug/mL

Chromium 10 ug/mL

Copper 10 ug/mL

Lead 5 ug/mL

Nickel 10 ug/mL

Vanadium 5 ug/mL

Zinc 20 ug/mL

M12LICVIC_00001 07/10/13 12/06/12 1, Lot N/A 1000 mL M12GSTKIC_00002 8 mL Barium 0.4 ug/mL

Chromium 0.4 ug/mL

Copper 0.4 ug/mL

Lead 0.4 ug/mL

Nickel 0.4 ug/mL

Vanadium 4 ug/mL

Zinc 0.4 ug/mL

.M12GSTKIC_00002 07/10/13 HP, Lot 1219103 (Purchased Reagent) Barium 50 ug/mL

Chromium 50 ug/mL

Copper 50 ug/mL

Lead 50 ug/mL

Nickel 50 ug/mL

Vanadium 500 ug/mL

Zinc 50 ug/mL

M12LISAIC_00001 12/01/13 12/03/12 1, Lot na 1000 mL M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

M12LISBIC_00001 09/01/13 12/03/12 1, Lot B51037 1000 mL M12ISTKIC_00003 10 mL Ag 0.2 ug/mL

As 0.1 ug/mL

Barium 0.5 ug/mL

Be 0.5 ug/mL

Page 96 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

Cd 1 ug/mL

Chromium 0.5 ug/mL

Co 0.5 ug/mL

Copper 0.5 ug/mL

Lead 0.05 ug/mL

Mn 0.5 ug/mL

Nickel 1 ug/mL

Sb 0.6 ug/mL

Se 0.05 ug/mL

Tl 0.1 ug/mL

Vanadium 0.5 ug/mL

Zinc 1 ug/mL

M12KSTKIC_00003 100 mL Al 500 ug/mL

Ca 500 ug/mL

Fe 200 ug/mL

Mg 500 ug/mL

.M12ISTKIC_00003 09/01/13 IV, Lot E2-MEB399019 (Purchased Reagent) Ag 20 ug/mL

As 10 ug/mL

Barium 50 ug/mL

Be 50 ug/mL

Cd 100 ug/mL

Chromium 50 ug/mL

Co 50 ug/mL

Copper 50 ug/mL

Lead 5 ug/mL

Mn 50 ug/mL

Nickel 100 ug/mL

Sb 60 ug/mL

Se 5 ug/mL

Tl 10 ug/mL

Vanadium 50 ug/mL

Zinc 100 ug/mL

.M12KSTKIC_00003 12/01/13 IV, Lot F2-meb414132 (Purchased Reagent) Al 5000 ug/mL

Ca 5000 ug/mL

Fe 2000 ug/mL

Mg 5000 ug/mL

VA/2CEVESTDWK_00174 11/21/12 11/14/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VA/2CEVESTDWK_00175 11/26/12 11/19/12 METHANOL, Lot DG860 2 mL 2-CEVE STD PT_00023 100 uL 2-Chloroethyl vinyl ether 100 ug/mL

VA STD PT_00024 100 uL Vinyl acetate 100 ug/mL

.2-CEVE STD PT_00023 01/08/13 10/08/12 METHANOL, Lot NA 1 mL 2-CEVESTDSK_00005 1 mL 2-Chloroethyl vinyl ether 2000 ug/mL

..2-CEVESTDSK_00005 11/30/16 Restek, Lot A085117 (Purchased Reagent) 2-Chloroethyl vinyl ether 2000 ug/mL

.VA STD PT_00024 01/10/13 10/11/12 METHANOL, Lot NA 1 mL VA STD SK_00007 1 mL Vinyl acetate 2000 ug/mL

Page 97 of 383 01/03/2013
REAGENT TRACEABILITY SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Reagent ID

Exp

Date Date

Prep Dilutant

Used

Reagent

Final

Volume

Parent Reagent

Reagent ID

Volume

Added Analyte Concentration

..VA STD SK_00007 03/31/14 RESTEK, Lot A090525 (Purchased Reagent) Vinyl acetate 2000 ug/mL

VOC/THF SPK_00122 11/19/12 11/13/12 1, Lot DG596 2 mL 8260ADDSPKPT_00024 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00024 11/19/12 10/08/12 1, Lot NA 1 mL 8260ADDSPKSK_00014 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00014 11/19/12 ACCUSTD, Lot 212071076 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00124 12/03/12 11/19/12 1, Lot DG596 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

VOC/THF SPK_00127 12/25/12 12/11/12 1, Lot DG860 2 mL 8260ADDSPKPT_00025 50 uL 2-Butanone (MEK) 50 mg/L

Acetone 50 mg/L

.8260ADDSPKPT_00025 01/19/13 11/19/12 1, Lot NA 1 mL 8260ADDSPKSK_00015 1 mL 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

..8260ADDSPKSK_00015 01/19/13 ACCUSTD, Lot 212091219 (Purchased Reagent) 2-Butanone (MEK) 2000 mg/L

Acetone 2000 mg/L

WSTCR1_00008 04/30/15 ERA, Lot 160412 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTCR13_00623 12/25/12 STL, Lot Lead(II)Chrom_00001 (Purchased Reagent) Chromium, hexavalent 38.64 mg/L

WSTCR2_00008 05/31/17 Ultra Scientific, Lot L00439 (Purchased Reagent) Chromium, hexavalent 1000 mg/L

WSTINCN1_00567 12/18/12 12/18/12 DI WATER, Lot NA 100 mL WSTCN1_00011 1 mL Cyanide, Total 10 mg/L

.WSTCN1_00011 01/31/14 ERA, Lot 060112 (Purchased Reagent) Cyanide, Total 1000 mg/L

WSTINCN2_00559 12/18/12 12/18/12 DI WATER, Lot NA 100 mL WSTCN2_00028 1 mL Cyanide, Amenable 10 mg/L

Cyanide, Free 10 mg/L

Cyanide, Reactive 10 mg/L

Cyanide, Total 10 mg/L

Cyanide, Weak Acid Dissociable 10 mg/L

.WSTCN2_00028 03/31/13 RICCA, Lot 4204518 (Purchased Reagent) Cyanide, Amenable 1000 mg/L

Cyanide, Free 1000 mg/L

Cyanide, Reactive 1000 mg/L

Cyanide, Total 1000 mg/L

Cyanide, Weak Acid Dissociable 1000 mg/L

WSTSF1_00036 11/15/13 NaS/1.5g/JTB/Y39592, Lot Zn0.5n/20mL (Purchased Reagent) Sulfide 180 mg/L

Sulfide as H2S 209.1 mg/L

Sulfide, Reactive 180 mg/L

Page 98 of 383 01/03/2013
Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory Authority Program EPA Region Certification ID

TestAmerica Chicago Alabama State Program 4 40461

TestAmerica Chicago California NELAP 9 01132CA

TestAmerica Chicago Georgia State Program 4 939

TestAmerica Chicago Georgia State Program 4 N/A

TestAmerica Chicago Hawaii State Program 9 N/A

TestAmerica Chicago Illinois NELAP 5 100201

TestAmerica Chicago Indiana State Program 5 C-IL-02

TestAmerica Chicago Iowa State Program 7 82

TestAmerica Chicago Kansas NELAP 7 E-10161

TestAmerica Chicago Kentucky State Program 4 90023

TestAmerica Chicago Kentucky (UST) State Program 4 66

TestAmerica Chicago L-A-B DoD ELAP L2304

TestAmerica Chicago L-A-B ISO/IEC 17025 L2304

TestAmerica Chicago Louisiana NELAP 6 30720

TestAmerica Chicago Massachusetts State Program 1 M-IL035

TestAmerica Chicago Mississippi State Program 4 N/A

TestAmerica Chicago North Carolina DENR State Program 4 291

TestAmerica Chicago North Dakota State Program 8 R-194

TestAmerica Chicago Oklahoma State Program 6 8908

TestAmerica Chicago South Carolina State Program 4 77001

TestAmerica Chicago Texas NELAP 6 T104704252-09-TX

TestAmerica Chicago USDA Federal P330-12-00038

TestAmerica Chicago Virginia NELAP 3 460142

TestAmerica Chicago Wisconsin State Program 5 999580010

TestAmerica Chicago Wyoming State Program 8 8TMS-Q

Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s 

current list of certified methods and analytes.

Page 99 of 383 TestAmerica Chicago 01/03/2013
Method 8260B

Volatile Organic Compounds (GC/MS) 

by Method 8260B

Page 100 of 383 01/03/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53315-1

SDG No.:

Matrix: Solid Level: Low

TestAmerica Chicago

GC Column (1): DB624 ID: 0.2 (mm)

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC DISCRETE 4 500-53315-3 113 116 98 91

FC D DISCRETE 4 500-53315-4 112 117 97 85

MB 500-173225/4 106 106 113 104

LCS 500-173225/5 105 104 111 103

FC DISCRETE 4 MS 500-53315-3 MS 118 117 95 85

FC DISCRETE 4 MSD 500-53315-3 MSD 116 119 96 84

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 70-134

TOL = Toluene-d8 (Surr) 75-122

BFB = 4-Bromofluorobenzene (Surr) 70-122

FORM II 8260B

# Column to be used to flag recovery values

Page 101 of 383 01/03/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53315-1

SDG No.:

Matrix: Solid Level: Medium

TestAmerica Chicago

GC Column (1): ID:

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

FC DISCRETE 4 DL 500-53315-3 DL 105 109 97 91

FC D DISCRETE 4 DL 500-53315-4 DL 116 119 93 90

MB 500-173509/6 96 101 95 94

LCS 500-173509/4 98 102 97 99

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 102 of 383 01/03/2013
FORM II

GC/MS VOA SURROGATE RECOVERY

Lab Name: Job No.: 500-53315-1

SDG No.:

Matrix: Water Level: Low

TestAmerica Chicago

GC Column (1): ID:

Client Sample ID Lab Sample ID DBFM # DCA # TOL # BFB #

TRIP BLANK 500-53315-5 109 105 100 97

FC EB 4 500-53315-6 107 107 99 94

MB 500-173508/6 96 101 95 94

LCS 500-173508/4 98 102 97 99

QC LIMITS

DBFM = Dibromofluoromethane QC LIMITS 75-120

DCA = 1,2-Dichloroethane-d4 (Surr) 75-125

TOL = Toluene-d8 (Surr) 75-120

BFB = 4-Bromofluorobenzene (Surr) 75-120

FORM II 8260B

# Column to be used to flag recovery values

Page 103 of 383 01/03/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53315-1

Solid Lab File ID: 16S1218.D

Lab ID: LCS 500-173225/5 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 45.56 91 50-138

2-Butanone (MEK) 50.0 52.85 106 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 104 of 383 01/03/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53315-1

Water Lab File ID: 25S1219p.D

Lab ID: LCS 500-173508/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/L)

SPIKE

ADDED

(ug/L)

#

LCS LCS

COMPOUND

Acetone 50.0 52.35 105 46-153

2-Butanone (MEK) 50.0 53.39 107 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 105 of 383 01/03/2013
GC/MS VOA LAB CONTROL SAMPLE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Medium

500-53315-1

Solid Lab File ID: 25S1219p.D

Lab ID: LCS 500-173509/4 Client ID:

TestAmerica Chicago

REC 

%

REC

QC

CONCENTRATION LIMITS

(ug/Kg)

SPIKE

ADDED

(ug/Kg)

#

LCS LCS

COMPOUND

Acetone 50.0 52.35 105 46-153

2-Butanone (MEK) 50.0 53.39 107 54-138

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 106 of 383 01/03/2013
GC/MS VOA MATRIX SPIKE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53315-1

Solid Lab File ID: 53315-03s.D

Lab ID: 500-53315-3 MS Client ID: FC DISCRETE 4 MS

TestAmerica Chicago

LIMITS

COMPOUND

CONCENTRATION %

REC

QC

REC

SAMPLE

CONCENTRATION

SPIKE

ADDED

(ug/Kg) (ug/Kg) (ug/Kg)

#

MS MS

Acetone 173 6940 7120 104 50-138 E 4

2-Butanone (MEK) 173 145 329.3 106 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 107 of 383 01/03/2013
GC/MS VOA MATRIX SPIKE DUPLICATE RECOVERY

FORM III

Lab Name: Job No.:

SDG No.:

Matrix: Level:

Matrix:

Low

500-53315-1

Solid Lab File ID: 53315-03t.D

Lab ID: 500-53315-3 MSD Client ID: FC DISCRETE 4 MSD

TestAmerica Chicago

COMPOUND

SPIKE

ADDED CONCENTRATION %

REC

%

RPD

QC LIMITS

(ug/Kg) (ug/Kg) RPD REC 

#

MSD MSD

Acetone 173 7629 399 7 30 50-138 E 4

2-Butanone (MEK) 173 303.4 91 8 30 58-133

FORM III 8260B

# Column to be used to flag recovery and RPD values

Page 108 of 383 01/03/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/20/2012 00:43

Heated Purge:(Y/N) N

CMS25

Lab File ID: 25M1219p.D Lab Sample ID: MB 500-173509/6

Matrix: Solid

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173509/4 25S1219p.D 12/19/2012 23:54

FC DISCRETE 4 DL 500-53315-3 DL 53315-03.D 12/20/2012 02:16

FC D DISCRETE 4 DL 500-53315-4 DL 53315-04.D 12/20/2012 02:40

FORM IV 8260B

Page 109 of 383 01/03/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/18/2012 08:30

DB624

Heated Purge:(Y/N) Y

CMS16

Lab File ID: 16M1218.D Lab Sample ID: MB 500-173225/4

Matrix: Solid

0.2(mm)

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173225/5 16S1218.D 12/18/2012 08:53

FC DISCRETE 4 500-53315-3 53315-03.D 12/18/2012 09:30

FC DISCRETE 4 MS 500-53315-3 MS 53315-03s.D 12/18/2012 09:54

FC DISCRETE 4 MSD 500-53315-3 MSD 53315-03t.D 12/18/2012 10:17

FC D DISCRETE 4 500-53315-4 53315-04.D 12/18/2012 10:40

FORM IV 8260B

Page 110 of 383 01/03/2013
FORM IV

GC/MS VOA METHOD BLANK SUMMARY

Lab Name:

SDG No.:

TestAmerica Chicago Job No.: 500-53315-1

Date Analyzed:

GC Column: ID:

Instrument ID: 12/20/2012 00:43

Heated Purge:(Y/N) N

CMS25

Lab File ID: 25M1219p.D Lab Sample ID: MB 500-173508/6

Matrix: Water

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:

LAB SAMPLE ID

LAB

CLIENT SAMPLE ID FILE ID DATE ANALYZED

LCS 500-173508/4 25S1219p.D 12/19/2012 23:54

TRIP BLANK 500-53315-5 53315-05.D 12/20/2012 01:08

FC EB 4 500-53315-6 53315-06.D 12/20/2012 01:49

FORM IV 8260B

Page 111 of 383 01/03/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53315-1

Lab File ID:

Instrument ID:

16B1119c.D

CMS16

11/19/2012

11:14

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 170196

50 15.0 - 40.0 % of mass 95 19.7 

75 30.0 - 60.0 % of mass 95 53.5 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.5 

173 Less than 2.0 % of mass 174 0.7 (1.0)1

174 50.0 - 120.00 % of mass 95 75.9 

175 5.0 - 9.0 % of mass 174 5.3 (6.9)1

176 95.0 - 101.0 % of mass 174 74.4 (98.0)1

177 5.0 - 9.0 % of mass 176 5.8 (7.8)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-170196/6 16I1119A.D 11/19/2012 12:14

STD2 500-170196/7 16I1119B.D 11/19/2012 12:37

STD3 500-170196/8 16I1119C.D 11/19/2012 13:00

STD4 500-170196/9 16I1119D.D 11/19/2012 13:23

STD5 500-170196/10 16I1119E.D 11/19/2012 13:46

STD6 500-170196/11 16I1119F.D 11/19/2012 14:09

ICV 500-170196/19 16S1119.D 11/19/2012 17:14

FORM V 8260B Page 112 of 383 01/03/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53315-1

Lab File ID:

Instrument ID:

16B1218.D

CMS16

12/18/2012

07:09

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173225

50 15.0 - 40.0 % of mass 95 19.8 

75 30.0 - 60.0 % of mass 95 50.0 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 7.8 

173 Less than 2.0 % of mass 174 0.2 (0.3)1

174 50.0 - 120.00 % of mass 95 74.6 

175 5.0 - 9.0 % of mass 174 6.4 (8.6)1

176 95.0 - 101.0 % of mass 174 71.2 (95.4)1

177 5.0 - 9.0 % of mass 176 3.9 (5.4)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173225/2 16C1218.D 12/18/2012 07:43

CCV 500-173225/3 16D1218.D 12/18/2012 08:07

MB 500-173225/4 16M1218.D 12/18/2012 08:30

LCS 500-173225/5 16S1218.D 12/18/2012 08:53

FC DISCRETE 4 500-53315-3 53315-03.D 12/18/2012 09:30

FC DISCRETE 4 MS 53315-03s.

D

500-53315-3 MS 12/18/2012 09:54

FC DISCRETE 4 MSD 53315-03t.

D

500-53315-3 MSD 12/18/2012 10:17

FC D DISCRETE 4 500-53315-4 53315-04.D 12/18/2012 10:40

FORM V 8260B Page 113 of 383 01/03/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53315-1

Lab File ID:

Instrument ID:

25B1114.D

CMS25

11/14/2012

09:17

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 169636

50 15.0 - 40.0 % of mass 95 26.1 

75 30.0 - 60.0 % of mass 95 46.8 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.8 

173 Less than 2.0 % of mass 174 0.8 (1.0)1

174 50.0 - 120.00 % of mass 95 78.1 

175 5.0 - 9.0 % of mass 174 5.6 (7.2)1

176 95.0 - 101.0 % of mass 174 77.7 (99.5)1

177 5.0 - 9.0 % of mass 176 5.0 (6.4)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-169636/2 25I1114a.D 11/14/2012 09:41

STD2 500-169636/3 25I1114b.D 11/14/2012 10:05

STD3 500-169636/4 25I1114c.D 11/14/2012 10:29

STD4 500-169636/5 25I1114d.D 11/14/2012 10:53

STD5 500-169636/6 25I1114e.D 11/14/2012 11:18

STD6 500-169636/7 25I1114f.D 11/14/2012 11:42

STD7 500-169636/8 25I1114g.D 11/14/2012 12:06

STD8 500-169636/9 25I1114h.D 11/14/2012 12:30

STD9 500-169636/10 25I1114i.D 11/14/2012 12:54

ICV 500-169636/20 25S1114.D 11/14/2012 16:57

FORM V 8260B Page 114 of 383 01/03/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53315-1

Lab File ID:

Instrument ID:

25B1114.D

CMS25

11/14/2012

09:17

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 169637

50 15.0 - 40.0 % of mass 95 26.1 

75 30.0 - 60.0 % of mass 95 46.8 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 6.8 

173 Less than 2.0 % of mass 174 0.8 (1.0)1

174 50.0 - 120.00 % of mass 95 78.1 

175 5.0 - 9.0 % of mass 174 5.6 (7.2)1

176 95.0 - 101.0 % of mass 174 77.7 (99.5)1

177 5.0 - 9.0 % of mass 176 5.0 (6.4)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

STD1 500-169637/2 25I1114a.D 11/14/2012 09:41

STD2 500-169637/3 25I1114b.D 11/14/2012 10:05

STD3 500-169637/4 25I1114c.D 11/14/2012 10:29

STD4 500-169637/5 25I1114d.D 11/14/2012 10:53

STD5 500-169637/6 25I1114e.D 11/14/2012 11:18

STD6 500-169637/7 25I1114f.D 11/14/2012 11:42

STD7 500-169637/8 25I1114g.D 11/14/2012 12:06

STD8 500-169637/9 25I1114h.D 11/14/2012 12:30

STD9 500-169637/10 25I1114i.D 11/14/2012 12:54

ICV 500-169637/20 25S1114.D 11/14/2012 16:57

FORM V 8260B Page 115 of 383 01/03/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53315-1

Lab File ID:

Instrument ID:

25B1219p.D

CMS25

12/19/2012

22:40

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173508

50 15.0 - 40.0 % of mass 95 20.1 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 5.6 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 112.8 

175 5.0 - 9.0 % of mass 174 7.3 (6.4)1

176 95.0 - 101.0 % of mass 174 109.9 (97.5)1

177 5.0 - 9.0 % of mass 176 6.9 (6.2)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173508/2 25C1219p.D 12/19/2012 23:06

CCV 500-173508/3 25D1219p.D 12/19/2012 23:30

LCS 500-173508/4 25S1219p.D 12/19/2012 23:54

MB 500-173508/6 25M1219p.D 12/20/2012 00:43

TRIP BLANK 500-53315-5 53315-05.D 12/20/2012 01:08

FC EB 4 500-53315-6 53315-06.D 12/20/2012 01:49

FORM V 8260B Page 116 of 383 01/03/2013
FORM V

BROMOFLUOROBENZENE (BFB)

Lab Name:

SDG No.:

Job No.: 500-53315-1

Lab File ID:

Instrument ID:

25B1219p.D

CMS25

12/19/2012

22:40

BFB Injection Date:

BFB Injection Time:

M/E ION ABUNDANCE CRITERIA

% RELATIVE

ABUNDANCE

Analysis Batch No.: 173509

50 15.0 - 40.0 % of mass 95 20.1 

75 30.0 - 60.0 % of mass 95 45.2 

95 Base Peak, 100% relative abundance 100.0 

96 5.0 - 9.0 % of mass 95 5.6 

173 Less than 2.0 % of mass 174 0.0 (0.0)1

174 50.0 - 120.00 % of mass 95 112.8 

175 5.0 - 9.0 % of mass 174 7.3 (6.4)1

176 95.0 - 101.0 % of mass 174 109.9 (97.5)1

177 5.0 - 9.0 % of mass 176 6.9 (6.2)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:

GC/MS VOA INSTRUMENT PERFORMANCE CHECK

TestAmerica Chicago

CLIENT SAMPLE ID

LAB

FILE ID LAB SAMPLE ID

DATE

ANALYZED

TIME

ANALYZED

CCV 500-173509/2 25C1219p.D 12/19/2012 23:06

CCV 500-173509/3 25D1219p.D 12/19/2012 23:30

LCS 500-173509/4 25S1219p.D 12/19/2012 23:54

MB 500-173509/6 25M1219p.D 12/20/2012 00:43

FC DISCRETE 4 DL 500-53315-3 DL 53315-03.D 12/20/2012 02:16

FC D DISCRETE 4 DL 500-53315-4 DL 53315-04.D 12/20/2012 02:40

FORM V 8260B Page 117 of 383 01/03/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53315-1

Sample No.: STD3 500-170196/8 Date Analyzed: 11/19/2012 13:00

Lab File ID (Standard): 16I1119C.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10620

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

464716

116179 170040

680160

134826

539304

INITIAL CALIBRATION MID-POINT 3.42 3.99 6.38

3.92

2.92

4.49

3.49

6.88

5.88

232358 340080 269652

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170196/19 258949 3.42 378895 3.99 285510 6.38

CCV 500-173225/2 300281 3.41 435506 3.99 330057 6.38

CCV 500-173225/3 292123 3.42 413832 3.99 322880 6.38

MB 500-173225/4 272848 3.42 399265 3.99 312018 6.38

LCS 500-173225/5 290208 3.42 418105 3.99 323317 6.38

500-53315-3 FC DISCRETE 4 227570 3.42 339047 3.99 220989 6.38

500-53315-3 MS FC DISCRETE 4 MS 213499 3.42 331660 3.99 210155 6.38

500-53315-3 MSD FC DISCRETE 4 MSD 222386 3.42 342573 3.99 213812 6.38

500-53315-4 FC D DISCRETE 4 234392 3.42 348797 3.99 222533 6.38

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 118 of 383 01/03/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53315-1

Sample No.: STD3 500-170196/8 Date Analyzed: 11/19/2012 13:00

Lab File ID (Standard): 16I1119C.D

Instrument ID: CMS16 GC Column: DB624 ID: 0.2(mm)

Heated Purge: (Y/N) Y

Calibration ID: 10620

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

283260

70815

INITIAL CALIBRATION MID-POINT 8.21

8.71

7.71

141630

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-170196/19 139276 8.21

CCV 500-173225/2 157799 8.21

CCV 500-173225/3 156710 8.21

MB 500-173225/4 155307 8.21

LCS 500-173225/5 156529 8.22

500-53315-3 FC DISCRETE 4 65296* 8.22

500-53315-3 MS FC DISCRETE 4 MS 58501* 8.21

500-53315-3 MSD FC DISCRETE 4 MSD 57059* 8.21

500-53315-4 FC D DISCRETE 4 59961* 8.21

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 119 of 383 01/03/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53315-1

Sample No.: STD6 500-169636/7 Date Analyzed: 11/14/2012 11:42

Lab File ID (Standard): 25I1114f.D

Instrument ID: CMS25 GC Column: ID: ()

Heated Purge: (Y/N) N

Calibration ID: 10605

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

957684

239421 344275

1377100

275429

1101714

INITIAL CALIBRATION MID-POINT 3.40 4.05 6.49

3.90

2.90

4.55

3.55

6.99

5.99

478842 688550 550857

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-169636/20 466984 3.40 692259 4.05 555803 6.49

CCV 500-173509/2 480196 3.40 684781 4.05 547136 6.49

CCV 500-173509/3 505330 3.40 709189 4.05 565358 6.49

LCS 500-173509/4 497255 3.40 699991 4.05 565828 6.49

MB 500-173509/6 498155 3.40 711732 4.05 565897 6.49

500-53315-3 DL FC DISCRETE 4 DL 476846 3.40 702694 4.05 561857 6.49

500-53315-4 DL FC D DISCRETE 4 DL 428304 3.40 644386 4.05 482292 6.49

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 120 of 383 01/03/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53315-1

Sample No.: STD6 500-169636/7 Date Analyzed: 11/14/2012 11:42

Lab File ID (Standard): 25I1114f.D

Instrument ID: CMS25 GC Column: ID: ()

Heated Purge: (Y/N) N

Calibration ID: 10605

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

491836

122959

INITIAL CALIBRATION MID-POINT 8.35

8.85

7.85

245918

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-169636/20 239626 8.35

CCV 500-173509/2 250328 8.35

CCV 500-173509/3 267460 8.35

LCS 500-173509/4 265281 8.35

MB 500-173509/6 255019 8.35

500-53315-3 DL FC DISCRETE 4 DL 234564 8.35

500-53315-4 DL FC D DISCRETE 4 DL 181036 8.35

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 121 of 383 01/03/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53315-1

Sample No.: STD6 500-169637/7 Date Analyzed: 11/14/2012 11:42

Lab File ID (Standard): 25I1114f.D

Instrument ID: CMS25 GC Column: ID: ()

Heated Purge: (Y/N) N

Calibration ID: 10606

AREA # RT # AREA # RT # AREA # RT #

PFB DFB CBZ

UPPER LIMIT

LOWER LIMIT

957684

239421 344275

1377100

275429

1101714

INITIAL CALIBRATION MID-POINT 3.40 4.05 6.49

3.90

2.90

4.55

3.55

6.99

5.99

478842 688550 550857

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-169637/20 466984 3.40 692259 4.05 555803 6.49

CCV 500-173508/2 480196 3.40 684781 4.05 547136 6.49

CCV 500-173508/3 505330 3.40 709189 4.05 565358 6.49

LCS 500-173508/4 497255 3.40 699991 4.05 565828 6.49

MB 500-173508/6 498155 3.40 711732 4.05 565897 6.49

500-53315-5 TRIP BLANK 488133 3.40 739413 4.05 586574 6.49

500-53315-6 FC EB 4 499196 3.40 746245 4.05 595648 6.49

PFB = Pentafluorobenzene

DFB = 1,4-Difluorobenzene

CBZ = Chlorobenzene-d5

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 122 of 383 01/03/2013
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY

Lab Name: Job No.:

SDG No.:

FORM VIII

TestAmerica Chicago 500-53315-1

Sample No.: STD6 500-169637/7 Date Analyzed: 11/14/2012 11:42

Lab File ID (Standard): 25I1114f.D

Instrument ID: CMS25 GC Column: ID: ()

Heated Purge: (Y/N) N

Calibration ID: 10606

AREA # RT # AREA # RT # AREA # RT #

DCB

UPPER LIMIT

LOWER LIMIT

491836

122959

INITIAL CALIBRATION MID-POINT 8.35

8.85

7.85

245918

LAB SAMPLE ID CLIENT SAMPLE ID

ICV 500-169637/20 239626 8.35

CCV 500-173508/2 250328 8.35

CCV 500-173508/3 267460 8.35

LCS 500-173508/4 265281 8.35

MB 500-173508/6 255019 8.35

500-53315-5 TRIP BLANK 252464 8.35

500-53315-6 FC EB 4 252293 8.35

DCB = 1,4-Dichlorobenzene-d4

Area Limit = 50%-200% of internal standard area

RT Limit = ± 0.5 minutes of internal standard RT

# Column used to flag values outside QC limits

FORM VIII 8260B

Page 123 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC DISCRETE 4

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-3

Matrix: Lab File ID: 53315-03.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/14/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.1

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/18/2012 09:30

DB624 ID:

Analysis Batch No.: 173225 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

78-93-3 2-Butanone (MEK) 145 17.3 6.25

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 116 70-134

2037-26-5 Toluene-d8 (Surr) 98 75-122

460-00-4 4-Bromofluorobenzene (Surr) 91 70-122

1868-53-7 Dibromofluoromethane 113 75-120

FORM I 8260B

Page 124 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC DISCRETE 4 DL

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-3 DL

Matrix: Lab File ID: 53315-03.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/14/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.1

50

Level: (low/med) Medium

5(g)

5 (mL)

5(mL)

Date Analyzed: 12/20/2012 02:16

ID:

Analysis Batch No.: 173509 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 4220 864 225

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 109 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 91 75-120

1868-53-7 Dibromofluoromethane 105 75-120

FORM I 8260B

Page 125 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC D DISCRETE 4

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-4

Matrix: Lab File ID: 53315-04.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/14/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.8

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/18/2012 10:40

DB624 ID:

Analysis Batch No.: 173225 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

78-93-3 2-Butanone (MEK) 191 17.8 6.43

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 117 70-134

2037-26-5 Toluene-d8 (Surr) 97 75-122

460-00-4 4-Bromofluorobenzene (Surr) 85 70-122

1868-53-7 Dibromofluoromethane 112 75-120

FORM I 8260B

Page 126 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC D DISCRETE 4 DL

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-4 DL

Matrix: Lab File ID: 53315-04.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/14/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.8

50

Level: (low/med) Medium

5(g)

5 (mL)

5(mL)

Date Analyzed: 12/20/2012 02:40

ID:

Analysis Batch No.: 173509 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 8710 888 231

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 119 75-125

2037-26-5 Toluene-d8 (Surr) 93 75-120

460-00-4 4-Bromofluorobenzene (Surr) 90 75-120

1868-53-7 Dibromofluoromethane 116 75-120

FORM I 8260B

Page 127 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

TRIP BLANK

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-5

Matrix: Lab File ID: 53315-05.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/14/2012 00:00

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL) Date Analyzed: 12/20/2012 01:08

ID:

Analysis Batch No.: 173508 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 105 75-125

2037-26-5 Toluene-d8 (Surr) 100 75-120

460-00-4 4-Bromofluorobenzene (Surr) 97 75-120

1868-53-7 Dibromofluoromethane 109 75-120

FORM I 8260B

Page 128 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC EB 4

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-6

Matrix: Lab File ID: 53315-06.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

12/14/2012 14:30

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL) Date Analyzed: 12/20/2012 01:49

ID:

Analysis Batch No.: 173508 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) 13.0 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 107 75-125

2037-26-5 Toluene-d8 (Surr) 99 75-120

460-00-4 4-Bromofluorobenzene (Surr) 94 75-120

1868-53-7 Dibromofluoromethane 107 75-120

FORM I 8260B

Page 129 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170196/6 16I1119A.D

Level 2 STD2 500-170196/7 16I1119B.D

Level 3 STD3 500-170196/8 16I1119C.D

Level 4 STD4 500-170196/9 16I1119D.D

Level 5 STD5 500-170196/10 16I1119E.D

Level 6 STD6 500-170196/11 16I1119F.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Dichlorodifluoromethane 0.5101 0.4328 0.4745 0.4472 0.4791 Ave 5.9

0.4553

0.4665 0.0100 15.0

Chloromethane 0.6409 0.5486 0.6042 0.5514 0.5726 Ave 6.2

0.5611

0.5798 0.1000 15.0

Vinyl chloride 0.5489 0.4879 0.5232 0.4889 0.5055 Ave 4.9

0.4889

0.5072 0.0100 15.0

Bromomethane 0.2173 0.1622 0.1619 0.1577 0.1599 Lin2 0.9990

0.1594

0.3023 0.1550 0.0100 0.9900

Chloroethane 0.2848 0.2512 0.2658 0.2550 0.2653 Ave 4.4

0.2627

0.2641 0.0100 15.0

Trichlorofluoromethane 0.6410 0.5479 0.5898 0.5813 0.5855 Ave 5.1

0.5792

0.5875 0.0100 15.0

Acrolein 0.0833 0.0649 0.0739 0.0632 0.0635 Lin2 0.9920

0.0576

4.1129 0.0627 0.0010 0.9900

1,1-Dichloroethene 0.3883 0.3810 0.3940 0.3681 0.3657 Ave 4.2

0.3520

0.3748 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.4271 0.3940 0.4076 0.3784 0.3788 Ave 6.6

0.3531

0.3898 0.0100 15.0

Acetone 0.2177 0.1065 0.1169 0.1078 0.1047 Lin1 0.9950

0.0952

0.5599 0.0976 0.0100 0.9900

Carbon disulfide 1.2281 1.2015 1.3462 1.3937 1.2778 Ave 5.7

1.2592

1.2844 0.0100 15.0

Acetonitrile 0.0349 0.0327 0.0349 0.0328 0.0329 Ave 6.1

0.0294

0.0330 0.0010 15.0

Methylene Chloride 0.4402 0.4262 0.4539 0.4254 0.4228 Ave 4.4

0.3973

0.4276 0.0100 15.0

Acrylonitrile 0.1608 0.1223 0.1370 0.1213 0.1263 Lin2 0.9950

0.1142

1.5562 0.1209 0.0010 0.9900

trans-1,2-Dichloroethene 0.4687 0.4410 0.4603 0.4325 0.4314 Ave 4.6

0.4139

0.4413 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 130 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

Methyl tert-butyl ether 1.2409 1.0967 1.2053 1.0887 1.1030 Ave 7.6

1.0084

1.1238 0.0100 15.0

1,1-Dichloroethane 0.9158 0.8754 0.8985 0.8573 0.8580 Ave 4.0

0.8171

0.8704 0.1000 15.0

Vinyl acetate 0.7794 0.7899 0.8439 0.8848 0.9027 Ave 6.1

0.8075

0.8347 0.0100 15.0

2,2-Dichloropropane 0.5123 0.4762 0.4910 0.4760 0.4692 Ave 5.5

0.4333

0.4764 0.0100 15.0

cis-1,2-Dichloroethene 0.5178 0.4752 0.4900 0.4699 0.4727 Ave 4.9

0.4468

0.4787 0.0100 15.0

2-Butanone (MEK) 0.1907 0.1661 0.1744 0.1666 0.1738 Ave 7.0

0.1547

0.1710 0.0100 15.0

Propionitrile 0.0377 0.0303 0.0325 0.0300 0.0310 Ave 10.0

0.0283

0.0316 0.0010 15.0

Bromochloromethane 0.2134 0.1810 0.1955 0.1835 0.1826 Ave 7.7

0.1724

0.1881 0.0100 15.0

Tetrahydrofuran 0.1362 0.1110 0.1157 0.1060 0.1101 Lin2 0.9970

0.0981

0.1550 0.1053 0.0100 0.9900

Chloroform 0.8071 0.7676 0.7909 0.7569 0.7592 Ave 3.9

0.7200

0.7669 0.0100 15.0

1,1,1-Trichloroethane 0.6379 0.6227 0.6514 0.6248 0.6266 Ave 3.7

0.5828

0.6244 0.0100 15.0

Carbon tetrachloride 0.3601 0.3514 0.3626 0.3590 0.3620 Ave 1.9

0.3457

0.3568 0.0100 15.0

1,1-Dichloropropene 0.6628 0.6440 0.6397 0.6320 0.6326 Ave 3.2

0.6014

0.6354 0.0100 15.0

Benzene 1.2960 1.2332 1.2212 1.1893 1.1679 Ave 5.2

1.1124

1.2033 0.0100 15.0

1,2-Dichloroethane 0.4036 0.3828 0.3925 0.3773 0.3822 Ave 3.7

0.3615

0.3833 0.0100 15.0

Trichloroethene 0.3071 0.2871 0.2880 0.2787 0.2819 Ave 4.3

0.2706

0.2856 0.0100 15.0

1,2-Dichloropropane 0.2945 0.3110 0.2983 0.3002 0.3013 Ave 2.3

0.2903

0.2993 0.0100 15.0

Dibromomethane 0.1499 0.1401 0.1448 0.1410 0.1445 Ave 3.6

0.1346

0.1425 0.0100 15.0

Bromodichloromethane 0.3131 0.3276 0.3492 0.3570 0.3677 Ave 5.9

0.3548

0.3449 0.0100 15.0

2-Chloroethyl vinyl ether 0.1275 0.1289 0.1333 0.1400 0.1446 Ave 5.1

0.1302

0.1341 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 131 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

cis-1,3-Dichloropropene 0.3823 0.3878 0.3955 0.4081 0.4277 Ave 4.1

0.4075

0.4015 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.2134 0.2212 0.2438 0.2360 0.2310 Ave 5.2

0.2176

0.2272 0.0100 15.0

Toluene 0.7563 0.7457 0.7103 0.7065 0.7016 Ave 4.3

0.6724

0.7155 0.0100 15.0

trans-1,3-Dichloropropene 0.3019 0.3263 0.3366 0.3455 0.3644 Ave 6.4

0.3505

0.3375 0.0100 15.0

1,1,2-Trichloroethane 0.2720 0.2647 0.2830 0.2757 0.2832 Ave 2.6

0.2710

0.2749 0.0100 15.0

Tetrachloroethene 0.3877 0.3857 0.3641 0.3770 0.3714 Ave 3.1

0.3585

0.3741 0.0100 15.0

1,3-Dichloropropane 0.4386 0.4678 0.4537 0.4585 0.4651 Ave 2.7

0.4404

0.4540 0.0100 15.0

2-Hexanone 0.1953 0.1931 0.1955 0.2045 0.1961 Ave 2.7

0.1880

0.1954 0.0100 15.0

Dibromochloromethane 0.2040 0.2329 0.2507 0.2602 0.2677 Ave 9.7

0.2616

0.2462 0.0100 15.0

1,2-Dibromoethane 0.1811 0.1775 0.1848 0.1786 0.1848 Ave 2.7

0.1720

0.1798 0.0100 15.0

1-Chlorohexane 0.6093 0.5831 0.5505 0.5582 0.5737 Ave 4.3

0.5435

0.5697 0.0100 15.0

Chlorobenzene 0.9184 0.9225 0.9033 0.9116 0.9054 Ave 2.2

0.8681

0.9049 0.3000 15.0

1,1,1,2-Tetrachloroethane 0.2930 0.2979 0.3101 0.3188 0.3208 Ave 3.6

0.3132

0.3090 0.0100 15.0

Ethylbenzene 0.5544 0.5503 0.5126 0.5352 0.5171 Ave 4.1

0.5009

0.5284 0.0100 15.0

m&p-Xylene 1.3686 1.3827 1.3012 1.2861 1.2289 Ave 6.9

1.1453

1.2855 0.0100 15.0

o-Xylene 1.3495 1.4372 1.3698 1.3557 1.3252 Ave 4.5

1.2528

1.3484 0.0100 15.0

Styrene 0.9608 1.0612 1.0145 1.0388 1.0303 Ave 3.6

0.9843

1.0150 0.0100 15.0

Bromoform 0.1125 0.1362 0.1408 0.1514 0.1643 Ave 13.0

0.1539

0.1432 0.1000 15.0

Isopropylbenzene 3.1539 3.6540 3.1572 3.3315 3.1688 Ave 6.7

3.0455

3.2518 0.0100 15.0

Bromobenzene 0.6695 0.7563 0.7093 0.7420 0.7361 Ave 4.2

0.7199

0.7222 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 132 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

1,1,2,2-Tetrachloroethane 0.5452 0.5696 0.5597 0.5706 0.5758 Ave 3.0

0.5328

0.5589 0.3000 15.0

1,2,3-Trichloropropane 0.1912 0.1794 0.1660 0.1701 0.1701 Ave 6.1

0.1622

0.1732 0.0100 15.0

N-Propylbenzene 3.9287 4.2993 3.7879 3.9367 3.7362 Ave 6.3

3.5832

3.8787 0.0100 15.0

2-Chlorotoluene 2.3554 2.5038 2.2305 2.3361 2.2656 Ave 4.9

2.1830

2.3124 0.0100 15.0

1,3,5-Trimethylbenzene 2.6219 2.9360 2.6333 2.7109 2.6361 Ave 5.3

2.5201

2.6764 0.0100 15.0

4-Chlorotoluene 2.6491 2.9401 2.6216 2.7188 2.6440 Ave 5.1

2.5353

2.6848 0.0100 15.0

tert-Butylbenzene 2.2801 2.5455 2.2199 2.2982 2.2247 Ave 6.1

2.1418

2.2850 0.0100 15.0

1,2,4-Trimethylbenzene 2.7631 3.0061 2.6438 2.7255 2.6458 Ave 5.8

2.5511

2.7226 0.0100 15.0

sec-Butylbenzene 3.5331 3.8935 3.3623 3.4462 3.3180 Ave 7.1

3.1870

3.4567 0.0100 15.0

1,3-Dichlorobenzene 1.4471 1.5053 1.3813 1.4255 1.3778 Ave 4.0

1.3501

1.4145 0.0100 15.0

p-Isopropyltoluene 2.9586 3.2474 2.8310 2.8845 2.8017 Ave 6.6

2.6869

2.9017 0.0100 15.0

1,4-Dichlorobenzene 1.3977 1.4878 1.3669 1.4117 1.3954 Ave 3.8

1.3295

1.3982 0.0100 15.0

n-Butylbenzene 2.8602 3.1543 2.7994 2.7899 2.7599 Ave 6.2

2.6239

2.8313 0.0100 15.0

1,2-Dichlorobenzene 1.2797 1.3306 1.2155 1.2573 1.2376 Ave 3.9

1.1916

1.2521 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0873 0.0832 0.0794 0.0812 0.0900 Ave 4.7

0.0826

0.0839 0.0100 15.0

1,2,4-Trichlorobenzene 0.9789 0.9823 0.8678 0.7520 0.7794 Ave 13.0

0.7396

0.8500 0.0100 15.0

Hexachlorobutadiene 0.6292 0.6291 0.5100 0.4198 0.4138 Qua1 0.9940

+++++

0.7417 0.5403 -0.001 0.0100 0.9900

Naphthalene 1.6968 1.5945 1.4268 1.3407 1.4423 Lin2 0.9970

1.3291

1.6628 1.3908 0.0100 0.9900

1,2,3-Trichlorobenzene 0.7531 0.7667 0.6080 0.5315 0.5708 Qua2 0.9900

0.5407

0.4654 0.6784 -0.001 0.0100 0.9900

Dibromofluoromethane 0.4012 0.4120 0.3878 0.4079 Ave 4.3

0.3703

0.3958 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 133 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

DB624 ID: 0.2(mm)

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6

1,2-Dichloroethane-d4 (Surr) 0.3252 0.3396 0.3092 0.3325 Ave 6.0

0.2918

0.3196 0.0100 15.0

Toluene-d8 (Surr) 1.0538 1.0512 0.9999 1.0425 Ave 4.8

0.9393

1.0174 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5024 0.5042 0.4741 0.5018 Ave 5.3

0.4456

0.4856 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 134 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-170196/6 16I1119A.D

Level 2 STD2 500-170196/7 16I1119B.D

Level 3 STD3 500-170196/8 16I1119C.D

Level 4 STD4 500-170196/9 16I1119D.D

Level 5 STD5 500-170196/10 16I1119E.D

Level 6 STD6 500-170196/11 16I1119F.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Dichlorodifluoromethane PFB Ave 12902 50070 127370 264568 422626

553924

5.00 20.0 50.0 100 150

200

Chloromethane PFB Ave 16213 63463 162200 326211 505093

682571

5.00 20.0 50.0 100 150

200

Vinyl chloride PFB Ave 13885 56436 140448 289222 445896

594740

5.00 20.0 50.0 100 150

200

Bromomethane PFB Lin2 5496 18758 43458 93314 141095

193922

5.00 20.0 50.0 100 150

200

Chloroethane PFB Ave 7205 29060 71345 150837 234006

319655

5.00 20.0 50.0 100 150

200

Trichlorofluoromethane PFB Ave 16215 63387 158331 343881 516513

704692

5.00 20.0 50.0 100 150

200

Acrolein PFB Lin2 84258 300252 793200 1494545 2240120

2801943

200 800 2000 4000 6000

8000

1,1-Dichloroethene PFB Ave 9821 44072 105755 217759 322621

428198

5.00 20.0 50.0 100 150

200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 10804 45578 109401 223828 334178

429549

5.00 20.0 50.0 100 150

200

Acetone PFB Lin1 5507 12315 31383 63749 92368

115814

5.00 20.0 50.0 100 150

200

Carbon disulfide PFB Ave 31066 138989 361364 824494 1127201

1531938

5.00 20.0 50.0 100 150

200

Acetonitrile PFB Ave 7059 30299 75012 155141 232468

286410

40.0 160 400 800 1200

1600

Methylene Chloride PFB Ave 11136 49301 121856 251650 373003

483310

5.00 20.0 50.0 100 150

200

Acrylonitrile PFB Lin2 32531 113188 294241 574185 891617

1111839

40.0 160 400 800 1200

1600

trans-1,2-Dichloroethene PFB Ave 11855 51013 123566 255847 380526

503496

5.00 20.0 50.0 100 150

200

Methyl tert-butyl ether PFB Ave 31388 126868 323557 644017 972967

1226790

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 135 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

1,1-Dichloroethane PFB Ave 23166 101272 241193 507139 756847

994036

5.00 20.0 50.0 100 150

200

Vinyl acetate PFB Ave 19714 91380 226543 523396 796266

982422

5.00 20.0 50.0 100 150

200

2,2-Dichloropropane PFB Ave 12960 55088 131791 281610 413914

527180

5.00 20.0 50.0 100 150

200

cis-1,2-Dichloroethene PFB Ave 13099 54969 131526 277962 416945

543539

5.00 20.0 50.0 100 150

200

2-Butanone (MEK) PFB Ave 4823 19213 46819 98580 153328

188153

5.00 20.0 50.0 100 150

200

Propionitrile DFB Ave 11092 40835 102296 208849 323908

406897

40.0 160 400 800 1200

1600

Bromochloromethane PFB Ave 5399 20944 52481 108571 161097

209785

5.00 20.0 50.0 100 150

200

Tetrahydrofuran PFB Lin2 3446 12837 31053 62700 97150

119315

5.00 20.0 50.0 100 150

200

Chloroform PFB Ave 20416 88794 212306 447767 669705

875928

5.00 20.0 50.0 100 150

200

1,1,1-Trichloroethane PFB Ave 16137 72040 174862 369627 552754

709015

5.00 20.0 50.0 100 150

200

Carbon tetrachloride DFB Ave 13245 59272 142459 312633 472055

620557

5.00 20.0 50.0 100 150

200

1,1-Dichloropropene PFB Ave 16767 74498 171713 373900 558058

731603

5.00 20.0 50.0 100 150

200

Benzene DFB Ave 47671 208006 479794 1035802 1523052

1996925

5.00 20.0 50.0 100 150

200

1,2-Dichloroethane DFB Ave 14847 64572 154226 328584 498369

649012

5.00 20.0 50.0 100 150

200

Trichloroethene DFB Ave 11297 48428 113149 242684 367651

485784

5.00 20.0 50.0 100 150

200

1,2-Dichloropropane DFB Ave 10834 52448 117184 261424 392941

521104

5.00 20.0 50.0 100 150

200

Dibromomethane DFB Ave 5515 23635 56895 122814 188390

241667

5.00 20.0 50.0 100 150

200

Bromodichloromethane DFB Ave 11517 55249 137199 310916 479512

636972

5.00 20.0 50.0 100 150

200

2-Chloroethyl vinyl ether DFB Ave 4691 21736 52381 121903 188565

233764

5.00 20.0 50.0 100 150

200

cis-1,3-Dichloropropene DFB Ave 14063 65411 155392 355410 557705

731626

5.00 20.0 50.0 100 150

200

4-Methyl-2-pentanone (MIBK) DFB Ave 7850 37307 95785 205560 301187

390574

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 136 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

Toluene DFB Ave 27820 125770 279057 615277 914875

1207131

5.00 20.0 50.0 100 150

200

trans-1,3-Dichloropropene DFB Ave 11105 55044 132225 300866 475199

629293

5.00 20.0 50.0 100 150

200

1,1,2-Trichloroethane PFB Ave 6881 30616 75972 163072 249804

329645

5.00 20.0 50.0 100 150

200

Tetrachloroethene CBZ Ave 11739 49681 113412 247302 371178

488872

5.00 20.0 50.0 100 150

200

1,3-Dichloropropane CBZ Ave 13281 60253 141339 300730 464793

600568

5.00 20.0 50.0 100 150

200

2-Hexanone CBZ Ave 5913 24867 60900 134127 195945

256358

5.00 20.0 50.0 100 150

200

Dibromochloromethane CBZ Ave 6176 29991 78104 170673 267577

356811

5.00 20.0 50.0 100 150

200

1,2-Dibromoethane DFB Ave 6662 29944 72598 155572 240952

308703

5.00 20.0 50.0 100 150

200

1-Chlorohexane PFB Ave 15413 67451 147771 330227 506094

661180

5.00 20.0 50.0 100 150

200

Chlorobenzene CBZ Ave 27808 118815 281396 597934 904889

1183858

5.00 20.0 50.0 100 150

200

1,1,1,2-Tetrachloroethane CBZ Ave 8870 38367 96602 209122 320615

427140

5.00 20.0 50.0 100 150

200

Ethylbenzene CBZ Ave 16785 70876 159684 351002 516773

683074

5.00 20.0 50.0 100 150

200

m&p-Xylene CBZ Ave 82877 356156 810673 1687130 2456378

3123829

10.0 40.0 100 200 300

400

o-Xylene CBZ Ave 40858 185102 426723 889192 1324449

1708514

5.00 20.0 50.0 100 150

200

Styrene CBZ Ave 29090 136679 316041 681314 1029721

1342275

5.00 20.0 50.0 100 150

200

Bromoform CBZ Ave 3407 17540 43862 99282 164184

209852

5.00 20.0 50.0 100 150

200

Isopropylbenzene DCB Ave 51019 228406 516591 1065124 1575324

2017775

5.00 20.0 50.0 100 150

200

Bromobenzene DCB Ave 10830 47272 116055 237235 365963

476962

5.00 20.0 50.0 100 150

200

1,1,2,2-Tetrachloroethane DCB Ave 8819 35605 91578 182439 286268

352978

5.00 20.0 50.0 100 150

200

1,2,3-Trichloropropane DCB Ave 3093 11214 27159 54392 84576

107459

5.00 20.0 50.0 100 150

200

N-Propylbenzene DCB Ave 63553 268743 619776 1258627 1857403

2373990

5.00 20.0 50.0 100 150

200

FORM VI 8260B Page 137 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 6

2-Chlorotoluene DCB Ave 38102 156509 364951 746878 1126306

1446295

5.00 20.0 50.0 100 150

200

1,3,5-Trimethylbenzene DCB Ave 42413 183522 430864 866728 1310538

1669636

5.00 20.0 50.0 100 150

200

4-Chlorotoluene DCB Ave 42853 183778 428943 869237 1314457

1679760

5.00 20.0 50.0 100 150

200

tert-Butylbenzene DCB Ave 36885 159113 363220 734777 1106000

1419051

5.00 20.0 50.0 100 150

200

1,2,4-Trimethylbenzene DCB Ave 44697 187908 432579 871394 1315353

1690213

5.00 20.0 50.0 100 150

200

sec-Butylbenzene DCB Ave 57153 243374 550146 1101803 1649521

2111505

5.00 20.0 50.0 100 150

200

1,3-Dichlorobenzene DCB Ave 23410 94092 226011 455769 684977

894523

5.00 20.0 50.0 100 150

200

p-Isopropyltoluene DCB Ave 47861 202992 463212 922211 1392838

1780196

5.00 20.0 50.0 100 150

200

1,4-Dichlorobenzene DCB Ave 22610 92998 223660 451341 693731

880833

5.00 20.0 50.0 100 150

200

n-Butylbenzene DCB Ave 46268 197168 458033 891981 1372078

1738419

5.00 20.0 50.0 100 150

200

1,2-Dichlorobenzene DCB Ave 20701 83175 198883 401981 615248

789503

5.00 20.0 50.0 100 150

200

1,2-Dibromo-3-Chloropropane DCB Ave 1412 5199 12985 25946 44755

54754

5.00 20.0 50.0 100 150

200

1,2,4-Trichlorobenzene DCB Ave 15835 61405 141991 240412 387497

490028

5.00 20.0 50.0 100 150

200

Hexachlorobutadiene DCB Qua1 10179 39324 83450 134222 205730

+++++

5.00 20.0 50.0 100 150

+++++

Naphthalene DCB Lin2 27448 99668 233455 428628 717029

880550

5.00 20.0 50.0 100 150

200

1,2,3-Trichlorobenzene DCB Qua2 12182 47927 99479 169921 283755

358235

5.00 20.0 50.0 100 150

200

Dibromofluoromethane PFB Ave 46408 110602 229403 359839

450525

20.0 50.0 100 150

200

1,2-Dichloroethane-d4 (Surr) DFB Ave 54848 133405 269262 433613

523883

20.0 50.0 100 150

200

Toluene-d8 (Surr) DFB Ave 177743 413010 870860 1359449

1686334

20.0 50.0 100 150

200

4-Bromofluorobenzene (Surr) CBZ Ave 64705 157084 310979 501486

607718

20.0 50.0 100 150

200

FORM VI 8260B Page 138 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS16

Analy Batch No.: 170196

Calibration Start Date: 11/19/2012 12:14 Calibration End Date: 10620

Y

11/19/2012 14:09

GC Column: DB624 ID: 0.2(mm)

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Curve Type Legend:

Ave = Average ISTD

Lin1 = Linear 1/conc ISTD

Lin2 = Linear 1/conc^2 ISTD

Qua1 = Quadratic 1/conc ISTD

Qua2 = Quadratic 1/conc^2 ISTD

FORM VI 8260B Page 139 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-169636/2 25I1114a.D

Level 2 STD2 500-169636/3 25I1114b.D

Level 3 STD3 500-169636/4 25I1114c.D

Level 4 STD4 500-169636/5 25I1114d.D

Level 5 STD5 500-169636/6 25I1114e.D

Level 6 STD6 500-169636/7 25I1114f.D

Level 7 STD7 500-169636/8 25I1114g.D

Level 8 STD8 500-169636/9 25I1114h.D

Level 9 STD9 500-169636/10 25I1114i.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6267 0.6059 0.5583 0.5593 Ave 11.0

0.7116 0.7140 0.6992 0.7051

0.6475 0.0100 15.0

Chloromethane 1.3015 1.0453 0.9025 0.8641 Ave 13.0

0.9958 0.9920 0.9583 0.9520

1.0014 0.1000 15.0

Vinyl chloride 0.7381 0.7395 0.7007 0.7169 0.7202 Ave 8.2

0.8411 0.8539 0.8325 0.8376

0.7756 0.0100 15.0

Bromomethane 0.0930 0.0874 0.1319 0.0939 Qua1 0.9980

0.1431 0.1678 0.1774 0.1911

-0.054 0.1250 0.0003 0.0100 0.9900

Chloroethane 0.3725 0.3490 0.3073 0.2815 Ave 8.8

0.3535 0.3570 0.3479 0.3478

0.3396 0.0100 15.0

Trichlorofluoromethane 0.7867 0.7170 0.7355 0.7044 Ave 5.7

0.8073 0.8108 0.7973 0.7996

0.7698 0.0100 15.0

Dichlorofluoromethane 0.9181 0.8585 0.8326 0.8292 Ave 6.3

0.9602 0.9591 0.9448 0.9451

0.9059 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5594 0.5039 0.5013 0.5075 Ave 4.0

0.5451 0.5404 0.5331 0.5266

0.5272 0.0100 15.0

Acrolein 0.0653 0.0508 0.0519 0.0506 Ave 9.3

0.0513 0.0528 0.0510 0.0514

0.0531 0.0010 15.0

1,1-Dichloroethene 0.4814 0.4114 0.4116 0.4186 Ave 5.6

0.4529 0.4536 0.4471 0.4401

0.4396 0.0100 15.0

Acetone 0.0862 0.0669 Lin1 0.9990

0.0603 0.0638 0.0605 0.0585

0.1396 0.0593 0.0100 0.9900

Carbon disulfide 1.6120 1.5896 Ave 3.6

1.7255 1.7217 1.7163 1.6755

1.6734 0.0100 15.0

Acetonitrile 0.0417 0.0334 0.0357 0.0342 Ave 10.0

0.0308 0.0320 0.0316 0.0319

0.0339 0.0010 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 140 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Methylene Chloride 0.4134 0.3950 Ave 2.4

0.4162 0.4214 0.4201 0.4205

0.4144 0.0100 15.0

Methyl tert-butyl ether 0.5873 0.5558 0.5767 0.5751 Ave 4.8

0.5964 0.6288 0.6193 0.6376

0.5971 0.0100 15.0

trans-1,2-Dichloroethene 0.4969 0.4714 0.4802 0.4690 Ave 2.8

0.4994 0.5012 0.4981 0.5021

0.4898 0.0100 15.0

Acrylonitrile 0.1233 0.0964 0.0989 0.0964 Ave 9.1

0.0964 0.1003 0.0974 0.0986

0.1009 0.0010 15.0

1,1-Dichloroethane 1.1443 1.0662 1.0334 1.0546 Ave 3.4

1.1127 1.1107 1.1090 1.1012

1.0915 0.1000 15.0

Vinyl acetate 0.6064 0.5706 0.5890 0.6136 Ave 4.3

0.6078 0.6455 0.6277 0.6463

0.6134 0.0100 15.0

2,2-Dichloropropane 0.6725 0.6011 0.6452 0.6474 Ave 5.7

0.6930 0.7023 0.7076 0.7102

0.6724 0.0100 15.0

cis-1,2-Dichloroethene 0.4779 0.4805 0.4654 0.4786 Ave 3.4

0.4977 0.5122 0.5050 0.5029

0.4900 0.0100 15.0

2-Butanone (MEK) 0.0855 0.0852 Ave 2.0

0.0835 0.0880 0.0857 0.0876

0.0859 0.0100 15.0

Propionitrile 0.0258 0.0211 0.0203 0.0239 Ave 7.3

0.0234 0.0234 0.0227 0.0228

0.0229 0.0010 15.0

Bromochloromethane 0.1759 0.1659 0.1645 0.1732 Ave 5.1

0.1800 0.1876 0.1852 0.1869

0.1774 0.0100 15.0

Tetrahydrofuran 0.0608 0.0559 Ave 4.1

0.0598 0.0632 0.0600 0.0616

0.0602 0.0100 15.0

Chloroform 0.7642 0.7420 0.7427 0.7512 Ave 2.7

0.7819 0.7901 0.7886 0.7819

0.7678 0.0100 15.0

1,1,1-Trichloroethane 0.8037 0.6853 0.7017 0.7217 Ave 5.3

0.7638 0.7628 0.7655 0.7624

0.7459 0.0100 15.0

Carbon tetrachloride 0.5656 0.4815 0.4809 0.4715 Ave 6.0

0.5066 0.5007 0.4941 0.4813

0.4978 0.0100 15.0

1,1-Dichloropropene 0.8371 0.6861 0.6672 0.6998 Ave 7.1

0.7343 0.7197 0.7159 0.7187

0.7224 0.0100 15.0

Benzene 1.3416 1.3682 1.2676 1.2584 1.2711 Ave 3.1

1.3139 1.3047 1.2916 1.2506

1.2964 0.0100 15.0

1,2-Dichloroethane 0.3620 0.3300 0.3466 0.3363 Ave 2.9

0.3488 0.3529 0.3482 0.3416

0.3458 0.0100 15.0

Trichloroethene 0.2999 0.3740 0.3420 0.3534 0.3550 Ave 6.2

0.3698 0.3628 0.3591 0.3525

0.3521 0.0100 15.0

1,2-Dichloropropane 0.4011 0.3552 0.3669 0.3810 Ave 4.0

0.3930 0.3945 0.3896 0.3817

0.3829 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 141 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane 0.1339 0.1208 0.1203 0.1225 Ave 3.5

0.1265 0.1272 0.1238 0.1230

0.1248 0.0100 15.0

Bromodichloromethane 0.3886 0.3333 0.3435 0.3500 Ave 4.7

0.3658 0.3672 0.3638 0.3596

0.3590 0.0100 15.0

2-Chloroethyl vinyl ether 0.1009 0.1066 0.1211 Ave 9.8

0.1214 0.1319 0.1282 0.1282

0.1198 0.0100 15.0

cis-1,3-Dichloropropene 0.3681 0.3335 0.3673 0.3812 Ave 6.9

0.4024 0.4120 0.4061 0.3997

0.3838 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.1174 0.1312 Ave 6.9

0.1296 0.1461 0.1321 0.1310

0.1313 0.0100 15.0

Toluene 0.7622 0.8254 0.7315 0.7621 0.8038 Ave 4.3

0.8309 0.8194 0.8076 0.7815

0.7916 0.0100 15.0

trans-1,3-Dichloropropene 0.2661 0.2721 0.2745 0.2910 Ave 7.1

0.3072 0.3166 0.3129 0.3138

0.2943 0.0100 15.0

1,1,2-Trichloroethane 0.2405 0.2127 0.2226 0.2354 Ave 5.3

0.2434 0.2491 0.2432 0.2459

0.2366 0.0100 15.0

Tetrachloroethene 0.4912 0.4634 0.4661 0.4689 Ave 2.0

0.4810 0.4775 0.4709 0.4639

0.4729 0.0100 15.0

1,3-Dichloropropane 0.3521 0.3430 0.3631 0.3655 Ave 3.4

0.3768 0.3815 0.3700 0.3681

0.3650 0.0100 15.0

2-Hexanone 0.0898 0.0958 Ave 7.8

0.1054 0.1085 0.1086 0.1081

0.1027 0.0100 15.0

Dibromochloromethane 0.2353 0.2499 0.2582 0.2578 Ave 6.0

0.2748 0.2829 0.2742 0.2741

0.2634 0.0100 15.0

1,2-Dibromoethane 0.1484 0.1529 0.1471 0.1529 Ave 3.2

0.1580 0.1623 0.1566 0.1551

0.1542 0.0100 15.0

1-Chlorohexane 0.8430 0.7044 0.6586 0.6853 Ave 7.5

0.7341 0.7299 0.7197 0.7224

0.7247 0.0100 15.0

Chlorobenzene 1.0912 1.0617 1.0296 1.0316 Ave 2.7

1.0644 1.0581 1.0326 0.9989

1.0460 0.3000 15.0

Ethylbenzene 0.6126 0.6262 0.5910 0.6046 0.6108 Ave 2.3

0.6314 0.6272 0.6147 0.5959

0.6127 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3598 0.3180 0.3265 0.3245 Ave 4.2

0.3471 0.3481 0.3435 0.3360

0.3379 0.0100 15.0

m&p-Xylene 1.4172 1.5184 1.3883 1.4484 1.4772 Ave 3.7

1.5193 1.4949 1.4390 1.3765

1.4532 0.0100 15.0

o-Xylene 1.2710 1.4168 1.3402 1.3803 1.4253 Ave 4.9

1.4830 1.4858 1.4466 1.4030

1.4058 0.0100 15.0

Styrene 1.0367 0.9413 1.0331 1.0877 Ave 6.0

1.1364 1.1327 1.1029 1.0651

1.0670 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 142 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1342 0.1290 0.1300 0.1378 Ave 5.5

0.1457 0.1487 0.1442 0.1448

0.1393 0.1000 15.0

Isopropylbenzene 4.0836 3.8956 4.0253 4.3396 Ave 4.7

4.4728 4.3280 4.2696 4.0726

4.1859 0.0100 15.0

Bromobenzene 0.8418 0.7730 0.8017 0.8435 Ave 4.2

0.8804 0.8655 0.8558 0.8324

0.8368 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.4992 0.4183 0.4339 0.4409 Ave 5.5

0.4564 0.4527 0.4413 0.4280

0.4463 0.3000 15.0

N-Propylbenzene 4.8751 4.7238 4.8139 5.1431 Ave 4.3

5.3576 5.1063 5.0181 4.7949

4.9791 0.0100 15.0

1,2,3-Trichloropropane 0.3705 0.3219 0.3365 0.3427 Ave 4.5

0.3594 0.3570 0.3470 0.3367

0.3465 0.0100 15.0

2-Chlorotoluene 2.8872 2.5986 2.6727 2.7903 Ave 3.8

2.8784 2.7818 2.7435 2.6466

2.7499 0.0100 15.0

1,3,5-Trimethylbenzene 3.0596 2.9605 3.1481 3.3739 Ave 5.8

3.5164 3.4113 3.3441 3.2179

3.2540 0.0100 15.0

4-Chlorotoluene 2.9487 2.6742 2.8692 2.9235 Ave 4.2

3.0173 2.9214 2.8681 2.6996

2.8652 0.0100 15.0

tert-Butylbenzene 2.9337 2.7766 2.7908 3.0593 Ave 4.7

3.1788 3.0617 3.0246 2.9064

2.9665 0.0100 15.0

1,2,4-Trimethylbenzene 3.0577 2.8570 3.0570 3.2743 Ave 5.5

3.3951 3.3096 3.2537 3.1107

3.1644 0.0100 15.0

sec-Butylbenzene 4.5072 4.2877 4.5644 4.7518 Ave 4.4

4.9370 4.7434 4.6299 4.4303

4.6065 0.0100 15.0

1,3-Dichlorobenzene 1.7557 1.6307 1.6126 1.6403 Ave 3.8

1.6868 1.6471 1.5962 1.5498

1.6399 0.0100 15.0

p-Isopropyltoluene 3.6787 3.3647 3.6682 3.8530 Ave 5.1

3.9915 3.8347 3.7475 3.6085

3.7184 0.0100 15.0

1,4-Dichlorobenzene 1.8501 1.5676 1.5917 1.6102 Ave 6.4

1.6205 1.5924 1.5568 1.5065

1.6120 0.0100 15.0

n-Butylbenzene 3.7246 3.5101 3.5034 3.7147 Ave 3.5

3.8020 3.7046 3.5925 3.4543

3.6258 0.0100 15.0

1,2-Dichlorobenzene 1.5125 1.3182 1.3353 1.3471 Ave 5.0

1.3736 1.3441 1.3224 1.2938

1.3559 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0640 0.0557 0.0607 Ave 4.2

0.0613 0.0622 0.0619 0.0622

0.0611 0.0100 15.0

1,2,4-Trichlorobenzene 1.0559 1.0114 0.9472 0.9754 Ave 3.3

0.9959 1.0112 0.9823 0.9714

0.9938 0.0100 15.0

Hexachlorobutadiene 0.9048 0.7841 0.7828 0.8164 Ave 5.0

0.8362 0.8060 0.8013 0.7837

0.8144 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 143 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.1523 1.0892 1.1043 1.2375 Ave 8.4

1.3088 1.3385 1.3265 1.3042

1.2326 0.0100 15.0

1,2,3-Trichlorobenzene 0.8054 0.7453 0.7397 0.7760 Ave 3.1

0.8024 0.7863 0.7665 0.7673

0.7736 0.0100 15.0

Dibromofluoromethane 0.4286 Ave 3.4

0.3921 0.4016 0.4001 0.4056

0.4056 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2801 Ave 3.9

0.2563 0.2610 0.2563 0.2563

0.2620 0.0100 15.0

Toluene-d8 (Surr) 1.2583 Ave 5.3

1.1460 1.1369 1.1272 1.1002

1.1537 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5135 Ave 6.4

0.4530 0.4548 0.4445 0.4423

0.4616 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 144 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-169636/2 25I1114a.D

Level 2 STD2 500-169636/3 25I1114b.D

Level 3 STD3 500-169636/4 25I1114c.D

Level 4 STD4 500-169636/5 25I1114d.D

Level 5 STD5 500-169636/6 25I1114e.D

Level 6 STD6 500-169636/7 25I1114f.D

Level 7 STD7 500-169636/8 25I1114g.D

Level 8 STD8 500-169636/9 25I1114h.D

Level 9 STD9 500-169636/10 25I1114i.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 5925 11401 26997 105234

340727 680574 999908 1334171

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 12304 19668 43637 162579

476834 945596 1370421 1801235

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 1792 6991 13184 34662 135512

402756 813940 1190617 1584805

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Qua1 879 1644 6380 17675

68531 159903 253688 361489

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 3522 6566 14857 52973

169260 340269 497534 658073

1.00 2.00 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 7437 13491 35562 132537

386583 772790 1140271 1512970

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 8680 16153 40257 156008

459802 914190 1351103 1788177

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 5289 9481 24240 95490

261022 515069 762341 996359

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 24682 38238 100342 380499

983163 2013878 2919532 3889511

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 4551 7740 19901 78752

216853 432374 639336 832639

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Lin1 4169 12583

28863 60844 86556 110714

5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 77944 299089

826236 1641126 2454485 3170249

5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3153 5029 13796 51503

118119 244233 361545 482815

8.00 16.0 40.0 160

400 800 1200 1600

Methylene Chloride PFB Ave 19989 74311

199298 401716 600718 795639

5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 145 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Methyl tert-butyl ether PFB Ave 5552 10458 27883 108208

285591 599368 885704 1206318

1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,2-Dichloroethene PFB Ave 4698 8869 23219 88248

239156 477780 712403 950052

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrylonitrile PFB Ave 9328 14508 38240 145047

369309 764494 1113946 1491801

8.00 16.0 40.0 160

400 800 1200 1600

1,1-Dichloroethane PFB Ave 10818 20062 49965 198420

532819 1058676 1586028 2083577

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave 5733 10737 28478 115450

291043 615281 897688 1222863

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 6358 11310 31195 121815

331849 669389 1011997 1343669

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 4518 9041 22503 90050

238305 488203 722208 951477

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave 4135 16024

39966 83903 122589 165782

5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 2803 4571 11330 51048

128688 261136 380813 514481

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 1663 3122 7953 32593

86204 178800 264811 353545

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave 2940 10518

28655 60287 85848 116463

5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 7225 13962 35909 141343

374395 753081 1127839 1479445

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 7598 12895 33927 135798

365728 727123 1094771 1442540

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 7696 13009 33599 126143

348829 697542 1036343 1360424

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 7914 12910 32262 131672

351635 685994 1023811 1359894

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 4675 18616 34246 87925 340025

904704 1817615 2709239 3534956

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 4925 8914 24218 89957

240180 491653 730359 965547

1.00 2.00 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1045 5088 9239 24694 94975

254660 505411 753283 996319

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 5457 9597 25633 101917

270576 549582 817263 1078941

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromomethane DFB Ave 1822 3264 8408 32759

87117 177217 259724 347677

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 5287 9005 24000 93640

251902 511588 763207 1016509

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 146 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

2-Chloroethyl vinyl ether DFB Ave 2725 7449 32403

83592 183720 268867 362477

2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 5008 9009 25666 101987

277068 573893 851744 1129853

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave 8206 35107

89269 203592 277039 370296

5.00 20.0

50.0 100 150 200

Toluene DFB Ave 2656 11230 19763 53245 215017

572099 1141442 1694075 2209045

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 3620 7351 19177 77839

211555 441063 656430 886925

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane PFB Ave 2274 4002 10765 44295

116554 237405 347788 465322

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 5346 10002 25680 101199

264948 529023 785866 1043336

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 3832 7403 20002 78881

207573 422657 617363 827757

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave 4945 20677

58037 120168 181279 243107

5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 2561 5394 14227 55644

151370 313439 457571 616524

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 2019 4131 10278 40903

108765 226089 328523 438293

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 7970 13254 31843 128940

351499 695727 1029228 1366789

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 11876 22914 56723 222644

586311 1172309 1723186 2246503

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 1668 6815 12754 33309 131824

347791 694878 1025850 1340093

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 3916 6863 17989 70044

191190 385705 573138 755649

1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 7718 33049 59926 159589 637599

1673870 3312548 4802496 6191326

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 3461 15419 28925 76044 307606

816927 1646151 2414005 3155235

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 11282 20316 56914 234746

626017 1254918 1840518 2395297

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 1460 2785 7164 29735

80261 164803 240639 325699

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 20214 38535 102851 424056

1099936 2200629 3227532 4168680

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 4167 7647 20483 82422

216512 440051 646947 852077

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 147 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 2471 4138 11086 43083

112230 230162 333588 438075

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 24132 46728 123000 502575

1317540 2596340 3793324 4908027

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 1834 3184 8599 33490

88390 181542 262321 344689

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 14292 25705 68289 272668

707862 1414432 2073876 2709003

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 15145 29285 80436 329695

864754 1734520 2527907 3293833

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 14596 26453 73310 285677

742016 1485407 2168057 2763304

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 14522 27466 71308 298955

781727 1556746 2286383 2974995

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 15136 28261 78110 319956

834910 1682789 2459601 3184071

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 22311 42414 116625 464344

1214094 2411809 3499921 4534829

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 8691 16131 41203 160290

414806 837508 1206617 1586342

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 18210 33284 93726 376512

981590 1949768 2832864 3693602

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 9158 15507 40669 157342

398505 809665 1176872 1542031

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 18437 34722 89516 362997

934982 1883655 2715730 3535815

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 7487 13040 34119 131641

337786 683433 999636 1324326

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 633 1424 5930

15066 31633 46778 63674

2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 5227 10005 24201 95311

244912 514149 742574 994295

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 4479 7756 20002 79780

205629 409810 605699 802196

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 5704 10774 28215 120923

321854 680580 1002739 1334973

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 3987 7373 18899 75826

197329 399786 579399 785372

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 80643

187757 382786 572130 767393

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 74925

176491 363647 537534 724583

20.0

50.0 100 150 200

FORM VI 8260B Page 148 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169636

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10605

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 336603

789050 1583796 2364398 3109931

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 110828

249531 503840 741720 994763

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

Lin1 = Linear 1/conc ISTD

Qua1 = Quadratic 1/conc ISTD

FORM VI 8260B Page 149 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-169637/2 25I1114a.D

Level 2 STD2 500-169637/3 25I1114b.D

Level 3 STD3 500-169637/4 25I1114c.D

Level 4 STD4 500-169637/5 25I1114d.D

Level 5 STD5 500-169637/6 25I1114e.D

Level 6 STD6 500-169637/7 25I1114f.D

Level 7 STD7 500-169637/8 25I1114g.D

Level 8 STD8 500-169637/9 25I1114h.D

Level 9 STD9 500-169637/10 25I1114i.D

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane 0.6267 0.6059 0.5583 0.5593 Ave 11.0

0.7116 0.7140 0.6992 0.7051

0.6475 0.0100 15.0

Chloromethane 1.3015 1.0453 0.9025 0.8641 Ave 13.0

0.9958 0.9920 0.9583 0.9520

1.0014 0.1000 15.0

Vinyl chloride 0.7381 0.7395 0.7007 0.7169 0.7202 Ave 8.2

0.8411 0.8539 0.8325 0.8376

0.7756 0.0100 15.0

Bromomethane 0.0930 0.0874 0.1319 0.0939 Qua1 0.9980

0.1431 0.1678 0.1774 0.1911

-0.054 0.1250 0.0003 0.0100 0.9900

Chloroethane 0.3725 0.3490 0.3073 0.2815 Ave 8.8

0.3535 0.3570 0.3479 0.3478

0.3396 0.0100 15.0

Trichlorofluoromethane 0.7867 0.7170 0.7355 0.7044 Ave 5.7

0.8073 0.8108 0.7973 0.7996

0.7698 0.0100 15.0

Dichlorofluoromethane 0.9181 0.8585 0.8326 0.8292 Ave 6.3

0.9602 0.9591 0.9448 0.9451

0.9059 0.0100 15.0

1,1,2-Trichloro-1,2,2-trifluoroethane 0.5594 0.5039 0.5013 0.5075 Ave 4.0

0.5451 0.5404 0.5331 0.5266

0.5272 0.0100 15.0

Acrolein 0.0653 0.0508 0.0519 0.0506 Ave 9.3

0.0513 0.0528 0.0510 0.0514

0.0531 0.0010 15.0

1,1-Dichloroethene 0.4814 0.4114 0.4116 0.4186 Ave 5.6

0.4529 0.4536 0.4471 0.4401

0.4396 0.0100 15.0

Acetone 0.0862 0.0669 Lin1 0.9990

0.0603 0.0638 0.0605 0.0585

0.1396 0.0593 0.0100 0.9900

Carbon disulfide 1.6120 1.5896 Ave 3.6

1.7255 1.7217 1.7163 1.6755

1.6734 0.0100 15.0

Acetonitrile 0.0417 0.0334 0.0357 0.0342 Ave 10.0

0.0308 0.0320 0.0316 0.0319

0.0339 0.0010 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 150 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Methylene Chloride 0.4134 0.3950 Ave 2.4

0.4162 0.4214 0.4201 0.4205

0.4144 0.0100 15.0

Methyl tert-butyl ether 0.5873 0.5558 0.5767 0.5751 Ave 4.8

0.5964 0.6288 0.6193 0.6376

0.5971 0.0100 15.0

trans-1,2-Dichloroethene 0.4969 0.4714 0.4802 0.4690 Ave 2.8

0.4994 0.5012 0.4981 0.5021

0.4898 0.0100 15.0

Acrylonitrile 0.1233 0.0964 0.0989 0.0964 Ave 9.1

0.0964 0.1003 0.0974 0.0986

0.1009 0.0010 15.0

1,1-Dichloroethane 1.1443 1.0662 1.0334 1.0546 Ave 3.4

1.1127 1.1107 1.1090 1.1012

1.0915 0.1000 15.0

Vinyl acetate 0.6064 0.5706 0.5890 0.6136 Ave 4.3

0.6078 0.6455 0.6277 0.6463

0.6134 0.0100 15.0

2,2-Dichloropropane 0.6725 0.6011 0.6452 0.6474 Ave 5.7

0.6930 0.7023 0.7076 0.7102

0.6724 0.0100 15.0

cis-1,2-Dichloroethene 0.4779 0.4805 0.4654 0.4786 Ave 3.4

0.4977 0.5122 0.5050 0.5029

0.4900 0.0100 15.0

2-Butanone (MEK) 0.0855 0.0852 Ave 2.0

0.0835 0.0880 0.0857 0.0876

0.0859 0.0100 15.0

Propionitrile 0.0258 0.0211 0.0203 0.0239 Ave 7.3

0.0234 0.0234 0.0227 0.0228

0.0229 0.0010 15.0

Bromochloromethane 0.1759 0.1659 0.1645 0.1732 Ave 5.1

0.1800 0.1876 0.1852 0.1869

0.1774 0.0100 15.0

Tetrahydrofuran 0.0608 0.0559 Ave 4.1

0.0598 0.0632 0.0600 0.0616

0.0602 0.0100 15.0

Chloroform 0.7642 0.7420 0.7427 0.7512 Ave 2.7

0.7819 0.7901 0.7886 0.7819

0.7678 0.0100 15.0

1,1,1-Trichloroethane 0.8037 0.6853 0.7017 0.7217 Ave 5.3

0.7638 0.7628 0.7655 0.7624

0.7459 0.0100 15.0

Carbon tetrachloride 0.5656 0.4815 0.4809 0.4715 Ave 6.0

0.5066 0.5007 0.4941 0.4813

0.4978 0.0100 15.0

1,1-Dichloropropene 0.8371 0.6861 0.6672 0.6998 Ave 7.1

0.7343 0.7197 0.7159 0.7187

0.7224 0.0100 15.0

Benzene 1.3416 1.3682 1.2676 1.2584 1.2711 Ave 3.1

1.3139 1.3047 1.2916 1.2506

1.2964 0.0100 15.0

1,2-Dichloroethane 0.3620 0.3300 0.3466 0.3363 Ave 2.9

0.3488 0.3529 0.3482 0.3416

0.3458 0.0100 15.0

Trichloroethene 0.2999 0.3740 0.3420 0.3534 0.3550 Ave 6.2

0.3698 0.3628 0.3591 0.3525

0.3521 0.0100 15.0

1,2-Dichloropropane 0.4011 0.3552 0.3669 0.3810 Ave 4.0

0.3930 0.3945 0.3896 0.3817

0.3829 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 151 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Dibromomethane 0.1339 0.1208 0.1203 0.1225 Ave 3.5

0.1265 0.1272 0.1238 0.1230

0.1248 0.0100 15.0

Bromodichloromethane 0.3886 0.3333 0.3435 0.3500 Ave 4.7

0.3658 0.3672 0.3638 0.3596

0.3590 0.0100 15.0

2-Chloroethyl vinyl ether 0.1009 0.1066 0.1211 Ave 9.8

0.1214 0.1319 0.1282 0.1282

0.1198 0.0100 15.0

cis-1,3-Dichloropropene 0.3681 0.3335 0.3673 0.3812 Ave 6.9

0.4024 0.4120 0.4061 0.3997

0.3838 0.0100 15.0

4-Methyl-2-pentanone (MIBK) 0.1174 0.1312 Ave 6.9

0.1296 0.1461 0.1321 0.1310

0.1313 0.0100 15.0

Toluene 0.7622 0.8254 0.7315 0.7621 0.8038 Ave 4.3

0.8309 0.8194 0.8076 0.7815

0.7916 0.0100 15.0

trans-1,3-Dichloropropene 0.2661 0.2721 0.2745 0.2910 Ave 7.1

0.3072 0.3166 0.3129 0.3138

0.2943 0.0100 15.0

1,1,2-Trichloroethane 0.2405 0.2127 0.2226 0.2354 Ave 5.3

0.2434 0.2491 0.2432 0.2459

0.2366 0.0100 15.0

Tetrachloroethene 0.4912 0.4634 0.4661 0.4689 Ave 2.0

0.4810 0.4775 0.4709 0.4639

0.4729 0.0100 15.0

1,3-Dichloropropane 0.3521 0.3430 0.3631 0.3655 Ave 3.4

0.3768 0.3815 0.3700 0.3681

0.3650 0.0100 15.0

2-Hexanone 0.0898 0.0958 Ave 7.8

0.1054 0.1085 0.1086 0.1081

0.1027 0.0100 15.0

Dibromochloromethane 0.2353 0.2499 0.2582 0.2578 Ave 6.0

0.2748 0.2829 0.2742 0.2741

0.2634 0.0100 15.0

1,2-Dibromoethane 0.1484 0.1529 0.1471 0.1529 Ave 3.2

0.1580 0.1623 0.1566 0.1551

0.1542 0.0100 15.0

1-Chlorohexane 0.8430 0.7044 0.6586 0.6853 Ave 7.5

0.7341 0.7299 0.7197 0.7224

0.7247 0.0100 15.0

Chlorobenzene 1.0912 1.0617 1.0296 1.0316 Ave 2.7

1.0644 1.0581 1.0326 0.9989

1.0460 0.3000 15.0

Ethylbenzene 0.6126 0.6262 0.5910 0.6046 0.6108 Ave 2.3

0.6314 0.6272 0.6147 0.5959

0.6127 0.0100 15.0

1,1,1,2-Tetrachloroethane 0.3598 0.3180 0.3265 0.3245 Ave 4.2

0.3471 0.3481 0.3435 0.3360

0.3379 0.0100 15.0

m&p-Xylene 1.4172 1.5184 1.3883 1.4484 1.4772 Ave 3.7

1.5193 1.4949 1.4390 1.3765

1.4532 0.0100 15.0

o-Xylene 1.2710 1.4168 1.3402 1.3803 1.4253 Ave 4.9

1.4830 1.4858 1.4466 1.4030

1.4058 0.0100 15.0

Styrene 1.0367 0.9413 1.0331 1.0877 Ave 6.0

1.1364 1.1327 1.1029 1.0651

1.0670 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 152 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Bromoform 0.1342 0.1290 0.1300 0.1378 Ave 5.5

0.1457 0.1487 0.1442 0.1448

0.1393 0.1000 15.0

Isopropylbenzene 4.0836 3.8956 4.0253 4.3396 Ave 4.7

4.4728 4.3280 4.2696 4.0726

4.1859 0.0100 15.0

Bromobenzene 0.8418 0.7730 0.8017 0.8435 Ave 4.2

0.8804 0.8655 0.8558 0.8324

0.8368 0.0100 15.0

1,1,2,2-Tetrachloroethane 0.4992 0.4183 0.4339 0.4409 Ave 5.5

0.4564 0.4527 0.4413 0.4280

0.4463 0.3000 15.0

N-Propylbenzene 4.8751 4.7238 4.8139 5.1431 Ave 4.3

5.3576 5.1063 5.0181 4.7949

4.9791 0.0100 15.0

1,2,3-Trichloropropane 0.3705 0.3219 0.3365 0.3427 Ave 4.5

0.3594 0.3570 0.3470 0.3367

0.3465 0.0100 15.0

2-Chlorotoluene 2.8872 2.5986 2.6727 2.7903 Ave 3.8

2.8784 2.7818 2.7435 2.6466

2.7499 0.0100 15.0

1,3,5-Trimethylbenzene 3.0596 2.9605 3.1481 3.3739 Ave 5.8

3.5164 3.4113 3.3441 3.2179

3.2540 0.0100 15.0

4-Chlorotoluene 2.9487 2.6742 2.8692 2.9235 Ave 4.2

3.0173 2.9214 2.8681 2.6996

2.8652 0.0100 15.0

tert-Butylbenzene 2.9337 2.7766 2.7908 3.0593 Ave 4.7

3.1788 3.0617 3.0246 2.9064

2.9665 0.0100 15.0

1,2,4-Trimethylbenzene 3.0577 2.8570 3.0570 3.2743 Ave 5.5

3.3951 3.3096 3.2537 3.1107

3.1644 0.0100 15.0

sec-Butylbenzene 4.5072 4.2877 4.5644 4.7518 Ave 4.4

4.9370 4.7434 4.6299 4.4303

4.6065 0.0100 15.0

1,3-Dichlorobenzene 1.7557 1.6307 1.6126 1.6403 Ave 3.8

1.6868 1.6471 1.5962 1.5498

1.6399 0.0100 15.0

p-Isopropyltoluene 3.6787 3.3647 3.6682 3.8530 Ave 5.1

3.9915 3.8347 3.7475 3.6085

3.7184 0.0100 15.0

1,4-Dichlorobenzene 1.8501 1.5676 1.5917 1.6102 Ave 6.4

1.6205 1.5924 1.5568 1.5065

1.6120 0.0100 15.0

n-Butylbenzene 3.7246 3.5101 3.5034 3.7147 Ave 3.5

3.8020 3.7046 3.5925 3.4543

3.6258 0.0100 15.0

1,2-Dichlorobenzene 1.5125 1.3182 1.3353 1.3471 Ave 5.0

1.3736 1.3441 1.3224 1.2938

1.3559 0.0100 15.0

1,2-Dibromo-3-Chloropropane 0.0640 0.0557 0.0607 Ave 4.2

0.0613 0.0622 0.0619 0.0622

0.0611 0.0100 15.0

1,2,4-Trichlorobenzene 1.0559 1.0114 0.9472 0.9754 Ave 3.3

0.9959 1.0112 0.9823 0.9714

0.9938 0.0100 15.0

Hexachlorobutadiene 0.9048 0.7841 0.7828 0.8164 Ave 5.0

0.8362 0.8060 0.8013 0.7837

0.8144 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 153 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: GC Column: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

ID:

INTERNAL STANDARD CURVE EVALUATION

ANALYTE RRF

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CURVE

TYPE

COEFFICIENT

B M1 M2

# %RSD # MAX

%RSD

R^2

OR COD

# MIN R^2

OR COD

MIN RRF

LVL 6 LVL 7 LVL 8 LVL 9

Naphthalene 1.1523 1.0892 1.1043 1.2375 Ave 8.4

1.3088 1.3385 1.3265 1.3042

1.2326 0.0100 15.0

1,2,3-Trichlorobenzene 0.8054 0.7453 0.7397 0.7760 Ave 3.1

0.8024 0.7863 0.7665 0.7673

0.7736 0.0100 15.0

Dibromofluoromethane 0.4286 Ave 3.4

0.3921 0.4016 0.4001 0.4056

0.4056 0.0100 15.0

1,2-Dichloroethane-d4 (Surr) 0.2801 Ave 3.9

0.2563 0.2610 0.2563 0.2563

0.2620 0.0100 15.0

Toluene-d8 (Surr) 1.2583 Ave 5.3

1.1460 1.1369 1.1272 1.1002

1.1537 0.0100 15.0

4-Bromofluorobenzene (Surr) 0.5135 Ave 6.4

0.4530 0.4548 0.4445 0.4423

0.4616 0.0100 15.0

FORM VI 8260B

Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.

Page 154 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 STD1 500-169637/2 25I1114a.D

Level 2 STD2 500-169637/3 25I1114b.D

Level 3 STD3 500-169637/4 25I1114c.D

Level 4 STD4 500-169637/5 25I1114d.D

Level 5 STD5 500-169637/6 25I1114e.D

Level 6 STD6 500-169637/7 25I1114f.D

Level 7 STD7 500-169637/8 25I1114g.D

Level 8 STD8 500-169637/9 25I1114h.D

Level 9 STD9 500-169637/10 25I1114i.D

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Dichlorodifluoromethane PFB Ave 5925 11401 26997 105234

340727 680574 999908 1334171

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloromethane PFB Ave 12304 19668 43637 162579

476834 945596 1370421 1801235

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl chloride PFB Ave 1792 6991 13184 34662 135512

402756 813940 1190617 1584805

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Bromomethane PFB Qua1 879 1644 6380 17675

68531 159903 253688 361489

1.00 2.00 5.00 20.0

50.0 100 150 200

Chloroethane PFB Ave 3522 6566 14857 52973

169260 340269 497534 658073

1.00 2.00 5.00 20.0

50.0 100 150 200

Trichlorofluoromethane PFB Ave 7437 13491 35562 132537

386583 772790 1140271 1512970

1.00 2.00 5.00 20.0

50.0 100 150 200

Dichlorofluoromethane PFB Ave 8680 16153 40257 156008

459802 914190 1351103 1788177

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

PFB Ave 5289 9481 24240 95490

261022 515069 762341 996359

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrolein PFB Ave 24682 38238 100342 380499

983163 2013878 2919532 3889511

40.0 80.0 200 800

2000 4000 6000 8000

1,1-Dichloroethene PFB Ave 4551 7740 19901 78752

216853 432374 639336 832639

1.00 2.00 5.00 20.0

50.0 100 150 200

Acetone PFB Lin1 4169 12583

28863 60844 86556 110714

5.00 20.0

50.0 100 150 200

Carbon disulfide PFB Ave 77944 299089

826236 1641126 2454485 3170249

5.00 20.0

50.0 100 150 200

Acetonitrile PFB Ave 3153 5029 13796 51503

118119 244233 361545 482815

8.00 16.0 40.0 160

400 800 1200 1600

Methylene Chloride PFB Ave 19989 74311

199298 401716 600718 795639

5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 155 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Methyl tert-butyl ether PFB Ave 5552 10458 27883 108208

285591 599368 885704 1206318

1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,2-Dichloroethene PFB Ave 4698 8869 23219 88248

239156 477780 712403 950052

1.00 2.00 5.00 20.0

50.0 100 150 200

Acrylonitrile PFB Ave 9328 14508 38240 145047

369309 764494 1113946 1491801

8.00 16.0 40.0 160

400 800 1200 1600

1,1-Dichloroethane PFB Ave 10818 20062 49965 198420

532819 1058676 1586028 2083577

1.00 2.00 5.00 20.0

50.0 100 150 200

Vinyl acetate PFB Ave 5733 10737 28478 115450

291043 615281 897688 1222863

1.00 2.00 5.00 20.0

50.0 100 150 200

2,2-Dichloropropane PFB Ave 6358 11310 31195 121815

331849 669389 1011997 1343669

1.00 2.00 5.00 20.0

50.0 100 150 200

cis-1,2-Dichloroethene PFB Ave 4518 9041 22503 90050

238305 488203 722208 951477

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Butanone (MEK) PFB Ave 4135 16024

39966 83903 122589 165782

5.00 20.0

50.0 100 150 200

Propionitrile DFB Ave 2803 4571 11330 51048

128688 261136 380813 514481

8.00 16.0 40.0 160

400 800 1200 1600

Bromochloromethane PFB Ave 1663 3122 7953 32593

86204 178800 264811 353545

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrahydrofuran PFB Ave 2940 10518

28655 60287 85848 116463

5.00 20.0

50.0 100 150 200

Chloroform PFB Ave 7225 13962 35909 141343

374395 753081 1127839 1479445

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1-Trichloroethane PFB Ave 7598 12895 33927 135798

365728 727123 1094771 1442540

1.00 2.00 5.00 20.0

50.0 100 150 200

Carbon tetrachloride DFB Ave 7696 13009 33599 126143

348829 697542 1036343 1360424

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1-Dichloropropene PFB Ave 7914 12910 32262 131672

351635 685994 1023811 1359894

1.00 2.00 5.00 20.0

50.0 100 150 200

Benzene DFB Ave 4675 18616 34246 87925 340025

904704 1817615 2709239 3534956

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloroethane DFB Ave 4925 8914 24218 89957

240180 491653 730359 965547

1.00 2.00 5.00 20.0

50.0 100 150 200

Trichloroethene DFB Ave 1045 5088 9239 24694 94975

254660 505411 753283 996319

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichloropropane DFB Ave 5457 9597 25633 101917

270576 549582 817263 1078941

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromomethane DFB Ave 1822 3264 8408 32759

87117 177217 259724 347677

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromodichloromethane DFB Ave 5287 9005 24000 93640

251902 511588 763207 1016509

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 156 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

2-Chloroethyl vinyl ether DFB Ave 2725 7449 32403

83592 183720 268867 362477

2.00 5.00 20.0

50.0 100 150 200

cis-1,3-Dichloropropene DFB Ave 5008 9009 25666 101987

277068 573893 851744 1129853

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Methyl-2-pentanone (MIBK) DFB Ave 8206 35107

89269 203592 277039 370296

5.00 20.0

50.0 100 150 200

Toluene DFB Ave 2656 11230 19763 53245 215017

572099 1141442 1694075 2209045

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

trans-1,3-Dichloropropene DFB Ave 3620 7351 19177 77839

211555 441063 656430 886925

1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,2-Trichloroethane PFB Ave 2274 4002 10765 44295

116554 237405 347788 465322

1.00 2.00 5.00 20.0

50.0 100 150 200

Tetrachloroethene CBZ Ave 5346 10002 25680 101199

264948 529023 785866 1043336

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichloropropane CBZ Ave 3832 7403 20002 78881

207573 422657 617363 827757

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Hexanone CBZ Ave 4945 20677

58037 120168 181279 243107

5.00 20.0

50.0 100 150 200

Dibromochloromethane CBZ Ave 2561 5394 14227 55644

151370 313439 457571 616524

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromoethane DFB Ave 2019 4131 10278 40903

108765 226089 328523 438293

1.00 2.00 5.00 20.0

50.0 100 150 200

1-Chlorohexane PFB Ave 7970 13254 31843 128940

351499 695727 1029228 1366789

1.00 2.00 5.00 20.0

50.0 100 150 200

Chlorobenzene CBZ Ave 11876 22914 56723 222644

586311 1172309 1723186 2246503

1.00 2.00 5.00 20.0

50.0 100 150 200

Ethylbenzene CBZ Ave 1668 6815 12754 33309 131824

347791 694878 1025850 1340093

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

1,1,1,2-Tetrachloroethane CBZ Ave 3916 6863 17989 70044

191190 385705 573138 755649

1.00 2.00 5.00 20.0

50.0 100 150 200

m&p-Xylene CBZ Ave 7718 33049 59926 159589 637599

1673870 3312548 4802496 6191326

0.500 2.00 4.00 10.0 40.0

100 200 300 400

o-Xylene CBZ Ave 3461 15419 28925 76044 307606

816927 1646151 2414005 3155235

0.250 1.00 2.00 5.00 20.0

50.0 100 150 200

Styrene CBZ Ave 11282 20316 56914 234746

626017 1254918 1840518 2395297

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromoform CBZ Ave 1460 2785 7164 29735

80261 164803 240639 325699

1.00 2.00 5.00 20.0

50.0 100 150 200

Isopropylbenzene DCB Ave 20214 38535 102851 424056

1099936 2200629 3227532 4168680

1.00 2.00 5.00 20.0

50.0 100 150 200

Bromobenzene DCB Ave 4167 7647 20483 82422

216512 440051 646947 852077

1.00 2.00 5.00 20.0

50.0 100 150 200

FORM VI 8260B Page 157 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

1,1,2,2-Tetrachloroethane DCB Ave 2471 4138 11086 43083

112230 230162 333588 438075

1.00 2.00 5.00 20.0

50.0 100 150 200

N-Propylbenzene DCB Ave 24132 46728 123000 502575

1317540 2596340 3793324 4908027

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichloropropane DCB Ave 1834 3184 8599 33490

88390 181542 262321 344689

1.00 2.00 5.00 20.0

50.0 100 150 200

2-Chlorotoluene DCB Ave 14292 25705 68289 272668

707862 1414432 2073876 2709003

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3,5-Trimethylbenzene DCB Ave 15145 29285 80436 329695

864754 1734520 2527907 3293833

1.00 2.00 5.00 20.0

50.0 100 150 200

4-Chlorotoluene DCB Ave 14596 26453 73310 285677

742016 1485407 2168057 2763304

1.00 2.00 5.00 20.0

50.0 100 150 200

tert-Butylbenzene DCB Ave 14522 27466 71308 298955

781727 1556746 2286383 2974995

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trimethylbenzene DCB Ave 15136 28261 78110 319956

834910 1682789 2459601 3184071

1.00 2.00 5.00 20.0

50.0 100 150 200

sec-Butylbenzene DCB Ave 22311 42414 116625 464344

1214094 2411809 3499921 4534829

1.00 2.00 5.00 20.0

50.0 100 150 200

1,3-Dichlorobenzene DCB Ave 8691 16131 41203 160290

414806 837508 1206617 1586342

1.00 2.00 5.00 20.0

50.0 100 150 200

p-Isopropyltoluene DCB Ave 18210 33284 93726 376512

981590 1949768 2832864 3693602

1.00 2.00 5.00 20.0

50.0 100 150 200

1,4-Dichlorobenzene DCB Ave 9158 15507 40669 157342

398505 809665 1176872 1542031

1.00 2.00 5.00 20.0

50.0 100 150 200

n-Butylbenzene DCB Ave 18437 34722 89516 362997

934982 1883655 2715730 3535815

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dichlorobenzene DCB Ave 7487 13040 34119 131641

337786 683433 999636 1324326

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2-Dibromo-3-Chloropropane DCB Ave 633 1424 5930

15066 31633 46778 63674

2.00 5.00 20.0

50.0 100 150 200

1,2,4-Trichlorobenzene DCB Ave 5227 10005 24201 95311

244912 514149 742574 994295

1.00 2.00 5.00 20.0

50.0 100 150 200

Hexachlorobutadiene DCB Ave 4479 7756 20002 79780

205629 409810 605699 802196

1.00 2.00 5.00 20.0

50.0 100 150 200

Naphthalene DCB Ave 5704 10774 28215 120923

321854 680580 1002739 1334973

1.00 2.00 5.00 20.0

50.0 100 150 200

1,2,3-Trichlorobenzene DCB Ave 3987 7373 18899 75826

197329 399786 579399 785372

1.00 2.00 5.00 20.0

50.0 100 150 200

Dibromofluoromethane PFB Ave 80643

187757 382786 572130 767393

20.0

50.0 100 150 200

1,2-Dichloroethane-d4 (Surr) DFB Ave 74925

176491 363647 537534 724583

20.0

50.0 100 150 200

FORM VI 8260B Page 158 of 383 01/03/2013
FORM VI

Lab Name: Job No.:

Calibration ID:

SDG No.:

Instrument ID: Heated Purge: (Y/N)

GC/MS VOA INITIAL CALIBRATION DATA

TestAmerica Chicago 500-53315-1

CMS25

Analy Batch No.: 169637

Calibration Start Date: 11/14/2012 09:41 Calibration End Date: 10606

N

11/14/2012 12:54

GC Column: ID:

INTERNAL STANDARD RESPONSE AND CONCENTRATION

ANALYTE CURVE

TYPE

IS

REF

RESPONSE

LVL 1 LVL 2 LVL 3 LVL 4 LVL 5

CONCENTRATION (UG/L)

LVL 2 LVL 3 LVL 4 LVL 5

LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9

Toluene-d8 (Surr) DFB Ave 336603

789050 1583796 2364398 3109931

20.0

50.0 100 150 200

4-Bromofluorobenzene (Surr) CBZ Ave 110828

249531 503840 741720 994763

20.0

50.0 100 150 200

Curve Type Legend:

Ave = Average ISTD

Lin1 = Linear 1/conc ISTD

Qua1 = Quadratic 1/conc ISTD

FORM VI 8260B Page 159 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

11/19/2012 17:14

11/19/2012 12:14

11/19/2012 14:09

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.4665 0.4279 0.0100 45.9 50.0 -8.3 25.0

Chloromethane Ave 0.5798 0.5246 0.1000 45.2 50.0 -9.5 25.0

Vinyl chloride Ave 0.5072 0.5248 0.0100 51.7 50.0 3.5 25.0

Bromomethane Lin2 0.1523 0.0100 47.2 50.0 -5.7 25.0

Chloroethane Ave 0.2641 0.2426 0.0100 45.9 50.0 -8.2 25.0

Trichlorofluoromethane Ave 0.5875 0.5702 0.0100 48.5 50.0 -2.9 25.0

Acrolein Lin2 0.0673 0.0010 2080 2000 4.0 25.0

1,1-Dichloroethene Ave 0.3748 0.3758 0.0100 50.1 50.0 0.2 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.3898 0.3311 0.0100 42.5 50.0 -15.1 25.0

Acetone Lin1 0.1027 0.0100 46.9 50.0 -6.2 25.0

Carbon disulfide Ave 1.284 1.296 0.0100 50.4 50.0 0.9 25.0

Acetonitrile Ave 0.0330 0.0367 0.0010 446 400 11.4 25.0

Methylene Chloride Ave 0.4276 0.4290 0.0100 50.2 50.0 0.3 25.0

Acrylonitrile Lin2 0.1268 0.0010 407 400 1.7 25.0

trans-1,2-Dichloroethene Ave 0.4413 0.4669 0.0100 52.9 50.0 5.8 25.0

Methyl tert-butyl ether Ave 1.124 1.023 0.0100 45.5 50.0 -9.0 25.0

1,1-Dichloroethane Ave 0.8704 0.8721 0.1000 50.1 50.0 0.2 25.0

Vinyl acetate Ave 0.8347 0.8804 0.0100 52.7 50.0 5.5 25.0

2,2-Dichloropropane Ave 0.4764 0.4986 0.0100 52.3 50.0 4.7 25.0

cis-1,2-Dichloroethene Ave 0.4787 0.4840 0.0100 50.6 50.0 1.1 25.0

2-Butanone (MEK) Ave 0.1710 0.1524 0.0100 44.6 50.0 -10.9 25.0

Propionitrile Ave 0.0316 0.0316 0.0010 399 400 -0.2 25.0

Bromochloromethane Ave 0.1881 0.1702 0.0100 45.2 50.0 -9.5 25.0

Tetrahydrofuran Lin2 0.1042 0.0100 48.0 50.0 -4.0 25.0

Chloroform Ave 0.7669 0.7748 0.0100 50.5 50.0 1.0 25.0

1,1,1-Trichloroethane Ave 0.6244 0.6555 0.0100 52.5 50.0 5.0 25.0

Carbon tetrachloride Ave 0.3568 0.3724 0.0100 52.2 50.0 4.4 25.0

1,1-Dichloropropene Ave 0.6354 0.6306 0.0100 49.6 50.0 -0.8 25.0

Benzene Ave 1.203 1.216 0.0100 50.5 50.0 1.1 25.0

1,2-Dichloroethane Ave 0.3833 0.3697 0.0100 48.2 50.0 -3.5 25.0

Trichloroethene Ave 0.2856 0.2917 0.0100 51.1 50.0 2.1 25.0

1,2-Dichloropropane Ave 0.2993 0.2959 0.0100 49.4 50.0 -1.1 25.0

Dibromomethane Ave 0.1425 0.1397 0.0100 49.0 50.0 -2.0 25.0

Bromodichloromethane Ave 0.3449 0.3379 0.0100 49.0 50.0 -2.0 25.0

2-Chloroethyl vinyl ether Ave 0.1341 0.1258 0.0100 46.9 50.0 -6.2 25.0

cis-1,3-Dichloropropene Ave 0.4015 0.4011 0.0100 53.7 53.8 -0.1 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.2272 0.2120 0.0100 46.7 50.0 -6.7 25.0

Toluene Ave 0.7155 0.7132 0.0100 49.8 50.0 -0.3 25.0

trans-1,3-Dichloropropene Ave 0.3375 0.3348 0.0100 48.2 48.6 -0.8 25.0

1,1,2-Trichloroethane Ave 0.2749 0.2675 0.0100 48.6 50.0 -2.7 25.0

FORM VII 8260B

Page 160 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

11/19/2012 17:14

11/19/2012 12:14

11/19/2012 14:09

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Tetrachloroethene Ave 0.3741 0.3914 0.0100 52.3 50.0 4.6 25.0

1,3-Dichloropropane Ave 0.4540 0.4541 0.0100 50.0 50.0 0.0 25.0

2-Hexanone Ave 0.1954 0.1831 0.0100 46.9 50.0 -6.3 25.0

Dibromochloromethane Ave 0.2462 0.2483 0.0100 50.4 50.0 0.9 25.0

1,2-Dibromoethane Ave 0.1798 0.1719 0.0100 47.8 50.0 -4.4 25.0

1-Chlorohexane Ave 0.5697 0.5208 0.0100 45.7 50.0 -8.6 25.0

Chlorobenzene Ave 0.9049 0.8647 0.3000 47.8 50.0 -4.4 25.0

1,1,1,2-Tetrachloroethane Ave 0.3090 0.3084 0.0100 49.9 50.0 -0.2 25.0

Ethylbenzene Ave 0.5284 0.5301 0.0100 50.2 50.0 0.3 25.0

m&p-Xylene Ave 1.285 1.283 0.0100 99.8 100 -0.2 25.0

o-Xylene Ave 1.348 1.295 0.0100 48.0 50.0 -4.0 25.0

Styrene Ave 1.015 1.029 0.0100 50.7 50.0 1.4 25.0

Bromoform Ave 0.1432 0.1401 0.1000 48.9 50.0 -2.2 25.0

Isopropylbenzene Ave 3.252 3.211 0.0100 49.4 50.0 -1.3 25.0

Bromobenzene Ave 0.7222 0.7556 0.0100 52.3 50.0 4.6 25.0

1,1,2,2-Tetrachloroethane Ave 0.5589 0.5584 0.3000 50.0 50.0 -0.1 25.0

1,2,3-Trichloropropane Ave 0.1732 0.1680 0.0100 48.5 50.0 -3.0 25.0

N-Propylbenzene Ave 3.879 3.806 0.0100 49.1 50.0 -1.9 25.0

2-Chlorotoluene Ave 2.312 2.300 0.0100 49.7 50.0 -0.6 25.0

1,3,5-Trimethylbenzene Ave 2.676 2.896 0.0100 54.1 50.0 8.2 25.0

4-Chlorotoluene Ave 2.685 2.597 0.0100 48.4 50.0 -3.3 25.0

tert-Butylbenzene Ave 2.285 2.273 0.0100 49.7 50.0 -0.5 25.0

1,2,4-Trimethylbenzene Ave 2.723 2.842 0.0100 52.2 50.0 4.4 25.0

sec-Butylbenzene Ave 3.457 3.410 0.0100 49.3 50.0 -1.4 25.0

1,3-Dichlorobenzene Ave 1.415 1.361 0.0100 48.1 50.0 -3.8 25.0

p-Isopropyltoluene Ave 2.902 2.828 0.0100 48.7 50.0 -2.5 25.0

1,4-Dichlorobenzene Ave 1.398 1.440 0.0100 51.5 50.0 3.0 25.0

n-Butylbenzene Ave 2.831 2.940 0.0100 51.9 50.0 3.8 25.0

1,2-Dichlorobenzene Ave 1.252 1.205 0.0100 48.1 50.0 -3.8 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0839 0.0784 0.0100 46.7 50.0 -6.6 25.0

1,2,4-Trichlorobenzene Ave 0.8500 0.8024 0.0100 47.2 50.0 -5.6 25.0

Hexachlorobutadiene Qua1 0.5223 0.0100 51.7 50.0 3.4 25.0

Naphthalene Lin2 1.356 0.0100 47.5 50.0 -4.9 25.0

1,2,3-Trichlorobenzene Qua2 0.5963 0.0100 45.8 50.0 -8.3 25.0

Dibromofluoromethane Ave 0.3958 0.3997 0.0100 43.7 43.3 1.0 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3112 0.0100 42.1 43.3 -2.6 25.0

Toluene-d8 (Surr) Ave 1.017 1.099 0.0100 46.8 43.3 8.1 25.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.5002 0.0100 44.6 43.3 3.0 25.0

FORM VII 8260B

Page 161 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

11/19/2012 17:14

11/19/2012 14:32

11/19/2012 16:28

ICV 500-170196/19

DB624

TestAmerica Chicago

Lab File ID: 16S1119.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.4262 0.3493 0.0100 41.0 50.0 -18.0 25.0

Iodomethane Ave 0.5737 0.6405 0.0100 55.8 50.0 11.6 25.0

Methyl acetate Ave 0.3675 0.2295 0.0100 31.2 50.0 -37.6* 25.0

Hexane Ave 0.7834 0.6708 0.0100 42.8 50.0 -14.4 25.0

Cyclohexane Lin2 0.8544 0.0100 46.7 50.0 -6.6 25.0

Heptane Ave 0.5932 0.5269 0.0100 44.4 50.0 -11.2 25.0

Methylcyclohexane Ave 0.5531 0.5154 0.0100 46.6 50.0 -6.8 25.0

1,3,5-Trichlorobenzene Ave 1.012 1.063 0.0100 52.5 50.0 5.0 25.0

FORM VII 8260B

Page 162 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

12/18/2012 07:43

11/19/2012 12:14

11/19/2012 14:09

CCV 500-173225/2

DB624

TestAmerica Chicago

Lab File ID: 16C1218.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.4665 0.4528 0.0100 48.5 50.0 -2.9 50.0

Chloromethane Ave 0.5798 0.5416 0.1000 46.7 50.0 -6.6 50.0

Vinyl chloride Ave 0.5072 0.5144 0.0100 50.7 50.0 1.4 20.0

Bromomethane Lin2 0.1435 0.0100 44.3 50.0 -11.4 50.0

Chloroethane Ave 0.2641 0.2551 0.0100 48.3 50.0 -3.4 50.0

Trichlorofluoromethane Ave 0.5875 0.6000 0.0100 51.1 50.0 2.1 50.0

Acrolein Lin2 0.0644 0.0010 1988 2000 -0.6 50.0

1,1-Dichloroethene Ave 0.3748 0.3809 0.0100 50.8 50.0 1.6 20.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.3898 0.3839 0.0100 49.2 50.0 -1.5 50.0

Acetone Lin1 0.0931 0.0100 41.9 50.0 -16.1 50.0

Carbon disulfide Ave 1.284 1.002 0.0100 39.0 50.0 -22.0 50.0

Acetonitrile Ave 0.0330 0.0321 0.0010 389 400 -2.7 50.0

Methylene Chloride Ave 0.4276 0.4215 0.0100 49.3 50.0 -1.4 50.0

Acrylonitrile Lin2 0.1212 0.0010 388 400 -3.0 50.0

trans-1,2-Dichloroethene Ave 0.4413 0.4513 0.0100 51.1 50.0 2.3 50.0

Methyl tert-butyl ether Ave 1.124 1.091 0.0100 48.5 50.0 -2.9 50.0

1,1-Dichloroethane Ave 0.8704 0.8832 0.1000 50.7 50.0 1.5 50.0

Vinyl acetate Ave 0.8347 0.6282 0.0100 37.6 50.0 -24.7 50.0

2,2-Dichloropropane Ave 0.4764 0.4671 0.0100 49.0 50.0 -1.9 50.0

cis-1,2-Dichloroethene Ave 0.4787 0.4935 0.0100 51.5 50.0 3.1 50.0

2-Butanone (MEK) Ave 0.1710 0.1457 0.0100 42.6 50.0 -14.8 50.0

Propionitrile Ave 0.0316 0.0308 0.0010 389 400 -2.6 50.0

Bromochloromethane Ave 0.1881 0.1879 0.0100 50.0 50.0 -0.1 50.0

Tetrahydrofuran Lin2 0.1049 0.0100 48.3 50.0 -3.3 50.0

Chloroform Ave 0.7669 0.7777 0.0100 50.7 50.0 1.4 20.0

1,1,1-Trichloroethane Ave 0.6244 0.6405 0.0100 51.3 50.0 2.6 50.0

Carbon tetrachloride Ave 0.3568 0.3789 0.0100 53.1 50.0 6.2 50.0

1,1-Dichloropropene Ave 0.6354 0.6530 0.0100 51.4 50.0 2.8 50.0

Benzene Ave 1.203 1.248 0.0100 51.9 50.0 3.7 50.0

1,2-Dichloroethane Ave 0.3833 0.3859 0.0100 50.3 50.0 0.7 50.0

Trichloroethene Ave 0.2856 0.3001 0.0100 52.5 50.0 5.1 50.0

1,2-Dichloropropane Ave 0.2993 0.3094 0.0100 51.7 50.0 3.4 20.0

Dibromomethane Ave 0.1425 0.1436 0.0100 50.4 50.0 0.8 50.0

Bromodichloromethane Ave 0.3449 0.3562 0.0100 51.6 50.0 3.3 50.0

2-Chloroethyl vinyl ether Ave 0.1341 0.1255 0.0100 46.8 50.0 -6.4 50.0

cis-1,3-Dichloropropene Ave 0.4015 0.4120 0.0100 51.3 50.0 2.6 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.2272 0.2008 0.0100 44.2 50.0 -11.6 50.0

Toluene Ave 0.7155 0.7440 0.0100 52.0 50.0 4.0 20.0

trans-1,3-Dichloropropene Ave 0.3375 0.3462 0.0100 51.3 50.0 2.6 50.0

1,1,2-Trichloroethane Ave 0.2749 0.2819 0.0100 51.3 50.0 2.5 50.0

FORM VII 8260B

Page 163 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

12/18/2012 07:43

11/19/2012 12:14

11/19/2012 14:09

CCV 500-173225/2

DB624

TestAmerica Chicago

Lab File ID: 16C1218.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Tetrachloroethene Ave 0.3741 0.4095 0.0100 54.7 50.0 9.5 50.0

1,3-Dichloropropane Ave 0.4540 0.4772 0.0100 52.6 50.0 5.1 50.0

2-Hexanone Ave 0.1954 0.1760 0.0100 45.0 50.0 -9.9 50.0

Dibromochloromethane Ave 0.2462 0.2600 0.0100 52.8 50.0 5.6 50.0

1,2-Dibromoethane Ave 0.1798 0.1840 0.0100 51.2 50.0 2.4 50.0

1-Chlorohexane Ave 0.5697 0.5919 0.0100 52.0 50.0 3.9 50.0

Chlorobenzene Ave 0.9049 0.9618 0.3000 53.1 50.0 6.3 50.0

1,1,1,2-Tetrachloroethane Ave 0.3090 0.3251 0.0100 52.6 50.0 5.2 50.0

Ethylbenzene Ave 0.5284 0.5580 0.0100 52.8 50.0 5.6 20.0

m&p-Xylene Ave 1.285 1.371 0.0100 107 100 6.6 50.0

o-Xylene Ave 1.348 1.408 0.0100 52.2 50.0 4.4 50.0

Styrene Ave 1.015 1.072 0.0100 52.8 50.0 5.7 50.0

Bromoform Ave 0.1432 0.1438 0.1000 50.2 50.0 0.4 50.0

Isopropylbenzene Ave 3.252 3.568 0.0100 54.9 50.0 9.7 50.0

Bromobenzene Ave 0.7222 0.7961 0.0100 55.1 50.0 10.2 50.0

1,1,2,2-Tetrachloroethane Ave 0.5589 0.5755 0.3000 51.5 50.0 3.0 50.0

1,2,3-Trichloropropane Ave 0.1732 0.1783 0.0100 51.5 50.0 3.0 50.0

N-Propylbenzene Ave 3.879 4.216 0.0100 54.4 50.0 8.7 50.0

2-Chlorotoluene Ave 2.312 2.440 0.0100 52.8 50.0 5.5 50.0

1,3,5-Trimethylbenzene Ave 2.676 2.871 0.0100 53.6 50.0 7.3 50.0

4-Chlorotoluene Ave 2.685 2.874 0.0100 53.5 50.0 7.0 50.0

tert-Butylbenzene Ave 2.285 2.462 0.0100 53.9 50.0 7.7 50.0

1,2,4-Trimethylbenzene Ave 2.723 2.888 0.0100 53.1 50.0 6.1 50.0

sec-Butylbenzene Ave 3.457 3.724 0.0100 53.9 50.0 7.7 50.0

1,3-Dichlorobenzene Ave 1.415 1.495 0.0100 52.9 50.0 5.7 50.0

p-Isopropyltoluene Ave 2.902 3.112 0.0100 53.6 50.0 7.2 50.0

1,4-Dichlorobenzene Ave 1.398 1.476 0.0100 52.8 50.0 5.5 50.0

n-Butylbenzene Ave 2.831 3.012 0.0100 53.2 50.0 6.4 50.0

1,2-Dichlorobenzene Ave 1.252 1.285 0.0100 51.3 50.0 2.7 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0839 0.0733 0.0100 43.7 50.0 -12.7 50.0

1,2,4-Trichlorobenzene Ave 0.8500 0.7890 0.0100 46.4 50.0 -7.2 50.0

Hexachlorobutadiene Qua1 0.4997 0.0100 49.2 50.0 -1.7 50.0

Naphthalene Lin2 1.201 0.0100 42.0 50.0 -16.1 50.0

1,2,3-Trichlorobenzene Qua2 0.5323 0.0100 40.6 50.0 -18.9 50.0

Dibromofluoromethane Ave 0.3958 0.4098 0.0100 44.8 43.3 3.5 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3114 0.0100 42.2 43.3 -2.6 50.0

Toluene-d8 (Surr) Ave 1.017 1.098 0.0100 46.7 43.3 7.9 50.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.4926 0.0100 43.9 43.3 1.4 50.0

FORM VII 8260B

Page 164 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

12/18/2012 08:07

11/19/2012 12:14

11/19/2012 14:09

CCV 500-173225/3

DB624

TestAmerica Chicago

Lab File ID: 16D1218.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.3958 0.3999 0.0100 43.7 43.3 1.0 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.3196 0.3212 0.0100 43.5 43.3 0.5 50.0

Toluene-d8 (Surr) Ave 1.017 1.127 0.0100 47.9 43.3 10.8 50.0

4-Bromofluorobenzene (Surr) Ave 0.4856 0.5066 0.0100 45.2 43.3 4.3 50.0

FORM VII 8260B

Page 165 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

0.20(mm)

500-53315-1

CMS16

12/18/2012 08:07

11/19/2012 14:32

11/19/2012 16:28

CCV 500-173225/3

DB624

TestAmerica Chicago

Lab File ID: 16D1218.D Conc. Units: ug/L Heated Purge: (Y/N) Y

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 0.5997 0.3993 0.0100 33.3 50.0 -33.4 50.0

Ethyl ether Ave 0.4262 0.3686 0.0100 43.2 50.0 -13.5 50.0

Iodomethane Ave 0.5737 0.5127 0.0100 89.4 100 -10.6 50.0

3-Chloropropene Ave 0.2319 0.2090 0.0100 90.1 100 -9.9 50.0

Methyl acetate Ave 0.3675 0.3591 0.0100 48.8 50.0 -2.3 50.0

Hexane Ave 0.7834 0.6754 0.0100 43.1 50.0 -13.8 50.0

Isopropyl ether Ave 1.776 1.573 0.0100 44.3 50.0 -11.4 50.0

2-Chloro-1,3-butadiene Ave 0.8947 0.7886 0.0100 44.1 50.0 -11.9 50.0

Ethyl acetate Ave 0.3031 0.2917 0.0100 481 500 -3.8 50.0

Methacrylonitrile Ave 0.2264 0.2133 0.0100 94.2 100 -5.8 50.0

Cyclohexane Lin2 0.8119 0.0100 44.3 50.0 -11.4 50.0

Isobutyl alcohol Ave 0.0107 0.0103 0.0010 3867 4000 -3.3 50.0

2,2,4-Trimethylpentane Ave 1.405 1.309 0.0100 46.6 50.0 -6.8 50.0

Heptane Ave 0.5932 0.5496 0.0100 46.3 50.0 -7.4 50.0

n-Butyl alcohol Ave 0.0063 0.0063 0.0010 3996 4000 -0.1 50.0

Methylcyclohexane Ave 0.5531 0.5110 0.0100 46.2 50.0 -7.6 50.0

Methyl methacrylate Ave 0.2123 0.2175 0.0100 102 100 2.4 50.0

2-Nitropropane Ave 0.0771 0.0780 0.0100 4048 4000 1.2 50.0

Ethyl methacrylate Ave 0.3579 0.3633 0.0100 102 100 1.5 50.0

Cyclohexanone Lin1 0.0493 0.0100 4009 4000 0.2 50.0

trans-1,4-Dichloro-2-butene Ave 0.0868 0.0828 0.0100 95.4 100 -4.6 50.0

Pentachloroethane Ave 0.2111 0.2096 0.0100 99.3 100 -0.7 50.0

1,3,5-Trichlorobenzene Ave 1.012 1.023 0.0100 50.5 50.0 1.0 50.0

2-Methylnaphthalene Qua2 0.4760 0.0100 35.6 50.0 -28.8 50.0

FORM VII 8260B

Page 166 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

11/14/2012 16:57

11/14/2012 09:41

11/14/2012 12:54

ICV 500-169636/20

TestAmerica Chicago

Lab File ID: 25S1114.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.6475 0.4588 0.0100 35.4 50.0 -29.1* 25.0

Chloromethane Ave 1.001 0.7458 0.1000 37.2 50.0 -25.5* 25.0

Vinyl chloride Ave 0.7756 0.7960 0.0100 51.3 50.0 2.6 25.0

Bromomethane Qua1 0.1019 0.0100 37.4 50.0 -25.3* 25.0

Chloroethane Ave 0.3396 0.3008 0.0100 44.3 50.0 -11.4 25.0

Trichlorofluoromethane Ave 0.7698 0.7439 0.0100 48.3 50.0 -3.4 25.0

Dichlorofluoromethane Ave 0.9059 0.8663 0.0100 47.8 50.0 -4.4 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.5272 0.5075 0.0100 48.1 50.0 -3.7 25.0

Acrolein Ave 0.0531 0.0541 0.0010 2035 2000 1.8 25.0

1,1-Dichloroethene Ave 0.4396 0.4548 0.0100 51.7 50.0 3.5 25.0

Acetone Lin1 0.0598 0.0100 48.1 50.0 -3.9 25.0

Carbon disulfide Ave 1.673 1.384 0.0100 41.4 50.0 -17.3 25.0

Acetonitrile Ave 0.0339 0.0336 0.0010 396 400 -1.0 25.0

Methylene Chloride Ave 0.4144 0.4378 0.0100 52.8 50.0 5.6 25.0

Methyl tert-butyl ether Ave 0.5971 0.6540 0.0100 54.8 50.0 9.5 25.0

trans-1,2-Dichloroethene Ave 0.4898 0.5297 0.0100 54.1 50.0 8.1 25.0

Acrylonitrile Ave 0.1009 0.0983 0.0010 389 400 -2.7 25.0

1,1-Dichloroethane Ave 1.092 1.147 0.1000 52.6 50.0 5.1 25.0

Vinyl acetate Ave 0.6134 0.7013 0.0100 57.2 50.0 14.3 25.0

2,2-Dichloropropane Ave 0.6724 0.7339 0.0100 54.6 50.0 9.1 25.0

cis-1,2-Dichloroethene Ave 0.4900 0.5238 0.0100 53.5 50.0 6.9 25.0

2-Butanone (MEK) Ave 0.0859 0.0921 0.0100 53.6 50.0 7.2 25.0

Propionitrile Ave 0.0229 0.0238 0.0010 415 400 3.8 25.0

Bromochloromethane Ave 0.1774 0.1858 0.0100 52.4 50.0 4.8 25.0

Tetrahydrofuran Ave 0.0602 0.0614 0.0100 51.0 50.0 2.0 25.0

Chloroform Ave 0.7678 0.8241 0.0100 53.7 50.0 7.3 25.0

1,1,1-Trichloroethane Ave 0.7459 0.8093 0.0100 54.3 50.0 8.5 25.0

Carbon tetrachloride Ave 0.4978 0.5159 0.0100 51.8 50.0 3.6 25.0

1,1-Dichloropropene Ave 0.7224 0.7388 0.0100 51.1 50.0 2.3 25.0

Benzene Ave 1.296 1.298 0.0100 50.1 50.0 0.1 25.0

1,2-Dichloroethane Ave 0.3458 0.3449 0.0100 49.9 50.0 -0.3 25.0

Trichloroethene Ave 0.3521 0.3677 0.0100 52.2 50.0 4.5 25.0

1,2-Dichloropropane Ave 0.3829 0.3892 0.0100 50.8 50.0 1.6 25.0

Dibromomethane Ave 0.1248 0.1220 0.0100 48.9 50.0 -2.2 25.0

Bromodichloromethane Ave 0.3590 0.3555 0.0100 49.5 50.0 -1.0 25.0

2-Chloroethyl vinyl ether Ave 0.1198 0.1332 0.0100 55.6 50.0 11.2 25.0

cis-1,3-Dichloropropene Ave 0.3838 0.4012 0.0100 56.2 53.8 4.5 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1313 0.1388 0.0100 52.9 50.0 5.8 25.0

Toluene Ave 0.7916 0.8148 0.0100 51.5 50.0 2.9 25.0

trans-1,3-Dichloropropene Ave 0.2943 0.3017 0.0100 49.8 48.6 2.5 25.0

FORM VII 8260B

Page 167 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

11/14/2012 16:57

11/14/2012 09:41

11/14/2012 12:54

ICV 500-169636/20

TestAmerica Chicago

Lab File ID: 25S1114.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.2366 0.2447 0.0100 51.7 50.0 3.4 25.0

Tetrachloroethene Ave 0.4729 0.4874 0.0100 51.5 50.0 3.1 25.0

1,3-Dichloropropane Ave 0.3650 0.3709 0.0100 50.8 50.0 1.6 25.0

2-Hexanone Ave 0.1027 0.1093 0.0100 53.2 50.0 6.5 25.0

Dibromochloromethane Ave 0.2634 0.2674 0.0100 50.8 50.0 1.5 25.0

1,2-Dibromoethane Ave 0.1542 0.1557 0.0100 50.5 50.0 1.0 25.0

1-Chlorohexane Ave 0.7247 0.7340 0.0100 50.6 50.0 1.3 25.0

Chlorobenzene Ave 1.046 0.9841 0.3000 47.0 50.0 -5.9 25.0

Ethylbenzene Ave 0.6127 0.6167 0.0100 50.3 50.0 0.7 25.0

1,1,1,2-Tetrachloroethane Ave 0.3379 0.3414 0.0100 50.5 50.0 1.0 25.0

m&p-Xylene Ave 1.453 1.430 0.0100 98.4 100 -1.6 25.0

o-Xylene Ave 1.406 1.361 0.0100 48.4 50.0 -3.2 25.0

Styrene Ave 1.067 1.088 0.0100 51.0 50.0 1.9 25.0

Bromoform Ave 0.1393 0.1458 0.1000 52.3 50.0 4.6 25.0

Isopropylbenzene Ave 4.186 4.271 0.0100 51.0 50.0 2.0 25.0

Bromobenzene Ave 0.8368 0.8982 0.0100 53.7 50.0 7.3 25.0

1,1,2,2-Tetrachloroethane Ave 0.4463 0.4729 0.3000 53.0 50.0 6.0 25.0

N-Propylbenzene Ave 4.979 4.914 0.0100 49.4 50.0 -1.3 25.0

1,2,3-Trichloropropane Ave 0.3465 0.3629 0.0100 52.4 50.0 4.7 25.0

2-Chlorotoluene Ave 2.750 2.767 0.0100 50.3 50.0 0.6 25.0

1,3,5-Trimethylbenzene Ave 3.254 3.643 0.0100 56.0 50.0 12.0 25.0

4-Chlorotoluene Ave 2.865 2.758 0.0100 48.1 50.0 -3.7 25.0

tert-Butylbenzene Ave 2.966 3.068 0.0100 51.7 50.0 3.4 25.0

1,2,4-Trimethylbenzene Ave 3.164 3.425 0.0100 54.1 50.0 8.2 25.0

sec-Butylbenzene Ave 4.606 4.675 0.0100 50.7 50.0 1.5 25.0

1,3-Dichlorobenzene Ave 1.640 1.554 0.0100 47.4 50.0 -5.2 25.0

p-Isopropyltoluene Ave 3.718 3.713 0.0100 49.9 50.0 -0.1 25.0

1,4-Dichlorobenzene Ave 1.612 1.618 0.0100 50.2 50.0 0.4 25.0

n-Butylbenzene Ave 3.626 3.588 0.0100 49.5 50.0 -1.1 25.0

1,2-Dichlorobenzene Ave 1.356 1.308 0.0100 48.2 50.0 -3.5 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0611 0.0608 0.0100 49.7 50.0 -0.6 25.0

1,2,4-Trichlorobenzene Ave 0.9938 0.9093 0.0100 45.8 50.0 -8.5 25.0

Hexachlorobutadiene Ave 0.8144 0.8368 0.0100 51.4 50.0 2.8 25.0

Naphthalene Ave 1.233 1.319 0.0100 53.5 50.0 7.0 25.0

1,2,3-Trichlorobenzene Ave 0.7736 0.7753 0.0100 50.1 50.0 0.2 25.0

Dibromofluoromethane Ave 0.4056 0.4174 0.0100 51.5 50.0 2.9 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2620 0.2583 0.0100 49.3 50.0 -1.4 25.0

Toluene-d8 (Surr) Ave 1.154 1.171 0.0100 50.7 50.0 1.5 25.0

4-Bromofluorobenzene (Surr) Ave 0.4616 0.4512 0.0100 48.9 50.0 -2.3 25.0

FORM VII 8260B

Page 168 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

11/14/2012 16:57

11/14/2012 09:41

11/14/2012 12:54

ICV 500-169637/20

TestAmerica Chicago

Lab File ID: 25S1114.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.6475 0.4588 0.0100 35.4 50.0 -29.1* 25.0

Chloromethane Ave 1.001 0.7458 0.1000 37.2 50.0 -25.5* 25.0

Vinyl chloride Ave 0.7756 0.7960 0.0100 51.3 50.0 2.6 25.0

Bromomethane Qua1 0.1019 0.0100 37.4 50.0 -25.3* 25.0

Chloroethane Ave 0.3396 0.3008 0.0100 44.3 50.0 -11.4 25.0

Trichlorofluoromethane Ave 0.7698 0.7439 0.0100 48.3 50.0 -3.4 25.0

Dichlorofluoromethane Ave 0.9059 0.8663 0.0100 47.8 50.0 -4.4 25.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.5272 0.5075 0.0100 48.1 50.0 -3.7 25.0

Acrolein Ave 0.0531 0.0541 0.0010 2035 2000 1.8 25.0

1,1-Dichloroethene Ave 0.4396 0.4548 0.0100 51.7 50.0 3.5 25.0

Acetone Lin1 0.0598 0.0100 48.1 50.0 -3.9 25.0

Carbon disulfide Ave 1.673 1.384 0.0100 41.4 50.0 -17.3 25.0

Acetonitrile Ave 0.0339 0.0336 0.0010 396 400 -1.0 25.0

Methylene Chloride Ave 0.4144 0.4378 0.0100 52.8 50.0 5.6 25.0

Methyl tert-butyl ether Ave 0.5971 0.6540 0.0100 54.8 50.0 9.5 25.0

trans-1,2-Dichloroethene Ave 0.4898 0.5297 0.0100 54.1 50.0 8.1 25.0

Acrylonitrile Ave 0.1009 0.0983 0.0010 389 400 -2.7 25.0

1,1-Dichloroethane Ave 1.092 1.147 0.1000 52.6 50.0 5.1 25.0

Vinyl acetate Ave 0.6134 0.7013 0.0100 57.2 50.0 14.3 25.0

2,2-Dichloropropane Ave 0.6724 0.7339 0.0100 54.6 50.0 9.1 25.0

cis-1,2-Dichloroethene Ave 0.4900 0.5238 0.0100 53.5 50.0 6.9 25.0

2-Butanone (MEK) Ave 0.0859 0.0921 0.0100 53.6 50.0 7.2 25.0

Propionitrile Ave 0.0229 0.0238 0.0010 415 400 3.8 25.0

Bromochloromethane Ave 0.1774 0.1858 0.0100 52.4 50.0 4.8 25.0

Tetrahydrofuran Ave 0.0602 0.0614 0.0100 51.0 50.0 2.0 25.0

Chloroform Ave 0.7678 0.8241 0.0100 53.7 50.0 7.3 25.0

1,1,1-Trichloroethane Ave 0.7459 0.8093 0.0100 54.3 50.0 8.5 25.0

Carbon tetrachloride Ave 0.4978 0.5159 0.0100 51.8 50.0 3.6 25.0

1,1-Dichloropropene Ave 0.7224 0.7388 0.0100 51.1 50.0 2.3 25.0

Benzene Ave 1.296 1.298 0.0100 50.1 50.0 0.1 25.0

1,2-Dichloroethane Ave 0.3458 0.3449 0.0100 49.9 50.0 -0.3 25.0

Trichloroethene Ave 0.3521 0.3677 0.0100 52.2 50.0 4.5 25.0

1,2-Dichloropropane Ave 0.3829 0.3892 0.0100 50.8 50.0 1.6 25.0

Dibromomethane Ave 0.1248 0.1220 0.0100 48.9 50.0 -2.2 25.0

Bromodichloromethane Ave 0.3590 0.3555 0.0100 49.5 50.0 -1.0 25.0

2-Chloroethyl vinyl ether Ave 0.1198 0.1332 0.0100 55.6 50.0 11.2 25.0

cis-1,3-Dichloropropene Ave 0.3838 0.4012 0.0100 56.2 53.8 4.5 25.0

4-Methyl-2-pentanone (MIBK) Ave 0.1313 0.1388 0.0100 52.9 50.0 5.8 25.0

Toluene Ave 0.7916 0.8148 0.0100 51.5 50.0 2.9 25.0

trans-1,3-Dichloropropene Ave 0.2943 0.3017 0.0100 49.8 48.6 2.5 25.0

FORM VII 8260B

Page 169 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

11/14/2012 16:57

11/14/2012 09:41

11/14/2012 12:54

ICV 500-169637/20

TestAmerica Chicago

Lab File ID: 25S1114.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.2366 0.2447 0.0100 51.7 50.0 3.4 25.0

Tetrachloroethene Ave 0.4729 0.4874 0.0100 51.5 50.0 3.1 25.0

1,3-Dichloropropane Ave 0.3650 0.3709 0.0100 50.8 50.0 1.6 25.0

2-Hexanone Ave 0.1027 0.1093 0.0100 53.2 50.0 6.5 25.0

Dibromochloromethane Ave 0.2634 0.2674 0.0100 50.8 50.0 1.5 25.0

1,2-Dibromoethane Ave 0.1542 0.1557 0.0100 50.5 50.0 1.0 25.0

1-Chlorohexane Ave 0.7247 0.7340 0.0100 50.6 50.0 1.3 25.0

Chlorobenzene Ave 1.046 0.9841 0.3000 47.0 50.0 -5.9 25.0

Ethylbenzene Ave 0.6127 0.6167 0.0100 50.3 50.0 0.7 25.0

1,1,1,2-Tetrachloroethane Ave 0.3379 0.3414 0.0100 50.5 50.0 1.0 25.0

m&p-Xylene Ave 1.453 1.430 0.0100 98.4 100 -1.6 25.0

o-Xylene Ave 1.406 1.361 0.0100 48.4 50.0 -3.2 25.0

Styrene Ave 1.067 1.088 0.0100 51.0 50.0 1.9 25.0

Bromoform Ave 0.1393 0.1458 0.1000 52.3 50.0 4.6 25.0

Isopropylbenzene Ave 4.186 4.271 0.0100 51.0 50.0 2.0 25.0

Bromobenzene Ave 0.8368 0.8982 0.0100 53.7 50.0 7.3 25.0

1,1,2,2-Tetrachloroethane Ave 0.4463 0.4729 0.3000 53.0 50.0 6.0 25.0

N-Propylbenzene Ave 4.979 4.914 0.0100 49.4 50.0 -1.3 25.0

1,2,3-Trichloropropane Ave 0.3465 0.3629 0.0100 52.4 50.0 4.7 25.0

2-Chlorotoluene Ave 2.750 2.767 0.0100 50.3 50.0 0.6 25.0

1,3,5-Trimethylbenzene Ave 3.254 3.643 0.0100 56.0 50.0 12.0 25.0

4-Chlorotoluene Ave 2.865 2.758 0.0100 48.1 50.0 -3.7 25.0

tert-Butylbenzene Ave 2.966 3.068 0.0100 51.7 50.0 3.4 25.0

1,2,4-Trimethylbenzene Ave 3.164 3.425 0.0100 54.1 50.0 8.2 25.0

sec-Butylbenzene Ave 4.606 4.675 0.0100 50.7 50.0 1.5 25.0

1,3-Dichlorobenzene Ave 1.640 1.554 0.0100 47.4 50.0 -5.2 25.0

p-Isopropyltoluene Ave 3.718 3.713 0.0100 49.9 50.0 -0.1 25.0

1,4-Dichlorobenzene Ave 1.612 1.618 0.0100 50.2 50.0 0.4 25.0

n-Butylbenzene Ave 3.626 3.588 0.0100 49.5 50.0 -1.1 25.0

1,2-Dichlorobenzene Ave 1.356 1.308 0.0100 48.2 50.0 -3.5 25.0

1,2-Dibromo-3-Chloropropane Ave 0.0611 0.0608 0.0100 49.7 50.0 -0.6 25.0

1,2,4-Trichlorobenzene Ave 0.9938 0.9093 0.0100 45.8 50.0 -8.5 25.0

Hexachlorobutadiene Ave 0.8144 0.8368 0.0100 51.4 50.0 2.8 25.0

Naphthalene Ave 1.233 1.319 0.0100 53.5 50.0 7.0 25.0

1,2,3-Trichlorobenzene Ave 0.7736 0.7753 0.0100 50.1 50.0 0.2 25.0

Dibromofluoromethane Ave 0.4056 0.4174 0.0100 51.5 50.0 2.9 25.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2620 0.2583 0.0100 49.3 50.0 -1.4 25.0

Toluene-d8 (Surr) Ave 1.154 1.171 0.0100 50.7 50.0 1.5 25.0

4-Bromofluorobenzene (Surr) Ave 0.4616 0.4512 0.0100 48.9 50.0 -2.3 25.0

FORM VII 8260B

Page 170 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

11/14/2012 16:57

11/14/2012 13:19

11/14/2012 16:08

ICV 500-169636/20

TestAmerica Chicago

Lab File ID: 25S1114.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.3493 0.3200 0.0100 45.8 50.0 -8.4 25.0

Iodomethane Qua1 0.7644 0.0100 89.2 50.0 78.3* 25.0

Methyl acetate Ave 0.2344 0.1672 0.0100 35.7 50.0 -28.6* 25.0

Hexane Ave 1.324 1.237 0.0100 46.7 50.0 -6.6 25.0

Cyclohexane Ave 1.508 1.502 0.0100 49.8 50.0 -0.4 25.0

Heptane Ave 0.9508 0.8903 0.0100 46.8 50.0 -6.4 25.0

Methylcyclohexane Ave 0.6690 0.6725 0.0100 50.3 50.0 0.5 25.0

1,3,5-Trichlorobenzene Ave 1.274 1.242 0.0100 48.8 50.0 -2.5 25.0

FORM VII 8260B

Page 171 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

11/14/2012 16:57

11/14/2012 13:19

11/14/2012 16:08

ICV 500-169637/20

TestAmerica Chicago

Lab File ID: 25S1114.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Ethyl ether Ave 0.3493 0.3200 0.0100 45.8 50.0 -8.4 25.0

Iodomethane Qua1 0.7644 0.0100 89.2 50.0 78.3* 25.0

Methyl acetate Ave 0.2344 0.1672 0.0100 35.7 50.0 -28.6* 25.0

Hexane Ave 1.324 1.237 0.0100 46.7 50.0 -6.6 25.0

Cyclohexane Ave 1.508 1.502 0.0100 49.8 50.0 -0.4 25.0

Heptane Ave 0.9508 0.8903 0.0100 46.8 50.0 -6.4 25.0

Methylcyclohexane Ave 0.6690 0.6725 0.0100 50.3 50.0 0.5 25.0

1,3,5-Trichlorobenzene Ave 1.274 1.242 0.0100 48.8 50.0 -2.5 25.0

FORM VII 8260B

Page 172 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:06

11/14/2012 09:41

11/14/2012 12:54

CCV 500-173509/2

TestAmerica Chicago

Lab File ID: 25C1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.6475 0.4729 0.0100 36.5 50.0 -27.0 50.0

Chloromethane Ave 1.001 0.9148 0.1000 45.7 50.0 -8.7 50.0

Vinyl chloride Ave 0.7756 0.7427 0.0100 47.9 50.0 -4.2 20.0

Bromomethane Qua1 0.1501 0.0100 52.8 50.0 5.6 50.0

Chloroethane Ave 0.3396 0.3693 0.0100 54.4 50.0 8.8 50.0

Trichlorofluoromethane Ave 0.7698 0.9122 0.0100 59.3 50.0 18.5 50.0

Dichlorofluoromethane Ave 0.9059 1.034 0.0100 57.1 50.0 14.1 50.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.5272 0.5503 0.0100 52.2 50.0 4.4 50.0

Acrolein Ave 0.0531 0.0347 0.0010 1306 2000 -34.7 50.0

1,1-Dichloroethene Ave 0.4396 0.4452 0.0100 50.6 50.0 1.3 20.0

Acetone Lin1 0.0619 0.0100 49.9 50.0 -0.2 50.0

Carbon disulfide Ave 1.673 1.432 0.0100 42.8 50.0 -14.4 50.0

Acetonitrile Ave 0.0339 0.0349 0.0010 412 400 3.0 50.0

Methylene Chloride Ave 0.4144 0.3952 0.0100 47.7 50.0 -4.6 50.0

Methyl tert-butyl ether Ave 0.5971 0.5759 0.0100 48.2 50.0 -3.5 50.0

trans-1,2-Dichloroethene Ave 0.4898 0.4990 0.0100 50.9 50.0 1.9 50.0

Acrylonitrile Ave 0.1009 0.0990 0.0010 392 400 -1.9 50.0

1,1-Dichloroethane Ave 1.092 1.098 0.1000 50.3 50.0 0.6 50.0

Vinyl acetate Ave 0.6134 0.6029 0.0100 49.1 50.0 -1.7 50.0

2,2-Dichloropropane Ave 0.6724 0.7827 0.0100 58.2 50.0 16.4 50.0

cis-1,2-Dichloroethene Ave 0.4900 0.4882 0.0100 49.8 50.0 -0.4 50.0

2-Butanone (MEK) Ave 0.0859 0.0910 0.0100 53.0 50.0 6.0 50.0

Propionitrile Ave 0.0229 0.0241 0.0010 421 400 5.3 50.0

Bromochloromethane Ave 0.1774 0.1806 0.0100 50.9 50.0 1.8 50.0

Tetrahydrofuran Ave 0.0602 0.0614 0.0100 51.0 50.0 1.9 50.0

Chloroform Ave 0.7678 0.8007 0.0100 52.1 50.0 4.3 20.0

1,1,1-Trichloroethane Ave 0.7459 0.8363 0.0100 56.1 50.0 12.1 50.0

Carbon tetrachloride Ave 0.4978 0.5702 0.0100 57.3 50.0 14.5 50.0

1,1-Dichloropropene Ave 0.7224 0.7188 0.0100 49.8 50.0 -0.5 50.0

Benzene Ave 1.296 1.253 0.0100 48.3 50.0 -3.3 50.0

1,2-Dichloroethane Ave 0.3458 0.3615 0.0100 52.3 50.0 4.5 50.0

Trichloroethene Ave 0.3521 0.3757 0.0100 53.4 50.0 6.7 50.0

1,2-Dichloropropane Ave 0.3829 0.3748 0.0100 48.9 50.0 -2.1 20.0

Dibromomethane Ave 0.1248 0.1225 0.0100 49.1 50.0 -1.8 50.0

Bromodichloromethane Ave 0.3590 0.3756 0.0100 52.3 50.0 4.6 50.0

2-Chloroethyl vinyl ether Ave 0.1198 0.1159 0.0100 48.4 50.0 -3.2 50.0

cis-1,3-Dichloropropene Ave 0.3838 0.3948 0.0100 51.4 50.0 2.9 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1313 0.1304 0.0100 49.7 50.0 -0.7 50.0

Toluene Ave 0.7916 0.8138 0.0100 51.4 50.0 2.8 20.0

trans-1,3-Dichloropropene Ave 0.2943 0.3074 0.0100 52.2 50.0 4.4 50.0

FORM VII 8260B

Page 173 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:06

11/14/2012 09:41

11/14/2012 12:54

CCV 500-173509/2

TestAmerica Chicago

Lab File ID: 25C1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.2366 0.2272 0.0100 48.0 50.0 -4.0 50.0

Tetrachloroethene Ave 0.4729 0.5085 0.0100 53.8 50.0 7.5 50.0

1,3-Dichloropropane Ave 0.3650 0.3531 0.0100 48.4 50.0 -3.3 50.0

2-Hexanone Ave 0.1027 0.1051 0.0100 51.2 50.0 2.3 50.0

Dibromochloromethane Ave 0.2634 0.2777 0.0100 52.7 50.0 5.4 50.0

1,2-Dibromoethane Ave 0.1542 0.1520 0.0100 49.3 50.0 -1.4 50.0

1-Chlorohexane Ave 0.7247 0.7315 0.0100 50.5 50.0 0.9 50.0

Chlorobenzene Ave 1.046 1.062 0.3000 50.8 50.0 1.6 50.0

Ethylbenzene Ave 0.6127 0.6405 0.0100 52.3 50.0 4.5 20.0

1,1,1,2-Tetrachloroethane Ave 0.3379 0.3577 0.0100 52.9 50.0 5.8 50.0

m&p-Xylene Ave 1.453 1.549 0.0100 107 100 6.6 50.0

o-Xylene Ave 1.406 1.493 0.0100 53.1 50.0 6.2 50.0

Styrene Ave 1.067 1.104 0.0100 51.7 50.0 3.5 50.0

Bromoform Ave 0.1393 0.1427 0.1000 51.2 50.0 2.4 50.0

Isopropylbenzene Ave 4.186 4.518 0.0100 54.0 50.0 7.9 50.0

Bromobenzene Ave 0.8368 0.8578 0.0100 51.3 50.0 2.5 50.0

1,1,2,2-Tetrachloroethane Ave 0.4463 0.4009 0.3000 44.9 50.0 -10.2 50.0

N-Propylbenzene Ave 4.979 5.379 0.0100 54.0 50.0 8.0 50.0

1,2,3-Trichloropropane Ave 0.3465 0.3321 0.0100 47.9 50.0 -4.2 50.0

2-Chlorotoluene Ave 2.750 2.880 0.0100 52.4 50.0 4.7 50.0

1,3,5-Trimethylbenzene Ave 3.254 3.566 0.0100 54.8 50.0 9.6 50.0

4-Chlorotoluene Ave 2.865 3.008 0.0100 52.5 50.0 5.0 50.0

tert-Butylbenzene Ave 2.966 3.183 0.0100 53.6 50.0 7.3 50.0

1,2,4-Trimethylbenzene Ave 3.164 3.489 0.0100 55.1 50.0 10.3 50.0

sec-Butylbenzene Ave 4.606 5.007 0.0100 54.4 50.0 8.7 50.0

1,3-Dichlorobenzene Ave 1.640 1.686 0.0100 51.4 50.0 2.8 50.0

p-Isopropyltoluene Ave 3.718 4.120 0.0100 55.4 50.0 10.8 50.0

1,4-Dichlorobenzene Ave 1.612 1.654 0.0100 51.3 50.0 2.6 50.0

n-Butylbenzene Ave 3.626 4.016 0.0100 55.4 50.0 10.8 50.0

1,2-Dichlorobenzene Ave 1.356 1.354 0.0100 49.9 50.0 -0.2 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0611 0.0607 0.0100 49.7 50.0 -0.7 50.0

1,2,4-Trichlorobenzene Ave 0.9938 1.041 0.0100 52.4 50.0 4.7 50.0

Hexachlorobutadiene Ave 0.8144 0.8913 0.0100 54.7 50.0 9.4 50.0

Naphthalene Ave 1.233 1.216 0.0100 49.3 50.0 -1.3 50.0

1,2,3-Trichlorobenzene Ave 0.7736 0.7901 0.0100 51.1 50.0 2.1 50.0

Dibromofluoromethane Ave 0.4056 0.3816 0.0100 47.0 50.0 -5.9 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2620 0.2511 0.0100 47.9 50.0 -4.2 50.0

Toluene-d8 (Surr) Ave 1.154 1.089 0.0100 47.2 50.0 -5.6 50.0

4-Bromofluorobenzene (Surr) Ave 0.4616 0.4426 0.0100 47.9 50.0 -4.1 50.0

FORM VII 8260B

Page 174 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:06

11/14/2012 09:41

11/14/2012 12:54

CCV 500-173508/2

TestAmerica Chicago

Lab File ID: 25C1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dichlorodifluoromethane Ave 0.6475 0.4729 0.0100 36.5 50.0 -27.0 50.0

Chloromethane Ave 1.001 0.9148 0.1000 45.7 50.0 -8.7 50.0

Vinyl chloride Ave 0.7756 0.7427 0.0100 47.9 50.0 -4.2 20.0

Bromomethane Qua1 0.1501 0.0100 52.8 50.0 5.6 50.0

Chloroethane Ave 0.3396 0.3693 0.0100 54.4 50.0 8.8 50.0

Trichlorofluoromethane Ave 0.7698 0.9122 0.0100 59.3 50.0 18.5 50.0

Dichlorofluoromethane Ave 0.9059 1.034 0.0100 57.1 50.0 14.1 50.0

1,1,2-Trichloro-1,2,2-triflu

oroethane

Ave 0.5272 0.5503 0.0100 52.2 50.0 4.4 50.0

Acrolein Ave 0.0531 0.0347 0.0010 1306 2000 -34.7 50.0

1,1-Dichloroethene Ave 0.4396 0.4452 0.0100 50.6 50.0 1.3 20.0

Acetone Lin1 0.0619 0.0100 49.9 50.0 -0.2 50.0

Carbon disulfide Ave 1.673 1.432 0.0100 42.8 50.0 -14.4 50.0

Acetonitrile Ave 0.0339 0.0349 0.0010 412 400 3.0 50.0

Methylene Chloride Ave 0.4144 0.3952 0.0100 47.7 50.0 -4.6 50.0

Methyl tert-butyl ether Ave 0.5971 0.5759 0.0100 48.2 50.0 -3.5 50.0

trans-1,2-Dichloroethene Ave 0.4898 0.4990 0.0100 50.9 50.0 1.9 50.0

Acrylonitrile Ave 0.1009 0.0990 0.0010 392 400 -1.9 50.0

1,1-Dichloroethane Ave 1.092 1.098 0.1000 50.3 50.0 0.6 50.0

Vinyl acetate Ave 0.6134 0.6029 0.0100 49.1 50.0 -1.7 50.0

2,2-Dichloropropane Ave 0.6724 0.7827 0.0100 58.2 50.0 16.4 50.0

cis-1,2-Dichloroethene Ave 0.4900 0.4882 0.0100 49.8 50.0 -0.4 50.0

2-Butanone (MEK) Ave 0.0859 0.0910 0.0100 53.0 50.0 6.0 50.0

Propionitrile Ave 0.0229 0.0241 0.0010 421 400 5.3 50.0

Bromochloromethane Ave 0.1774 0.1806 0.0100 50.9 50.0 1.8 50.0

Tetrahydrofuran Ave 0.0602 0.0614 0.0100 51.0 50.0 1.9 50.0

Chloroform Ave 0.7678 0.8007 0.0100 52.1 50.0 4.3 20.0

1,1,1-Trichloroethane Ave 0.7459 0.8363 0.0100 56.1 50.0 12.1 50.0

Carbon tetrachloride Ave 0.4978 0.5702 0.0100 57.3 50.0 14.5 50.0

1,1-Dichloropropene Ave 0.7224 0.7188 0.0100 49.8 50.0 -0.5 50.0

Benzene Ave 1.296 1.253 0.0100 48.3 50.0 -3.3 50.0

1,2-Dichloroethane Ave 0.3458 0.3615 0.0100 52.3 50.0 4.5 50.0

Trichloroethene Ave 0.3521 0.3757 0.0100 53.4 50.0 6.7 50.0

1,2-Dichloropropane Ave 0.3829 0.3748 0.0100 48.9 50.0 -2.1 20.0

Dibromomethane Ave 0.1248 0.1225 0.0100 49.1 50.0 -1.8 50.0

Bromodichloromethane Ave 0.3590 0.3756 0.0100 52.3 50.0 4.6 50.0

2-Chloroethyl vinyl ether Ave 0.1198 0.1159 0.0100 48.4 50.0 -3.2 50.0

cis-1,3-Dichloropropene Ave 0.3838 0.3948 0.0100 51.4 50.0 2.9 50.0

4-Methyl-2-pentanone (MIBK) Ave 0.1313 0.1304 0.0100 49.7 50.0 -0.7 50.0

Toluene Ave 0.7916 0.8138 0.0100 51.4 50.0 2.8 20.0

trans-1,3-Dichloropropene Ave 0.2943 0.3074 0.0100 52.2 50.0 4.4 50.0

FORM VII 8260B

Page 175 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:06

11/14/2012 09:41

11/14/2012 12:54

CCV 500-173508/2

TestAmerica Chicago

Lab File ID: 25C1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

1,1,2-Trichloroethane Ave 0.2366 0.2272 0.0100 48.0 50.0 -4.0 50.0

Tetrachloroethene Ave 0.4729 0.5085 0.0100 53.8 50.0 7.5 50.0

1,3-Dichloropropane Ave 0.3650 0.3531 0.0100 48.4 50.0 -3.3 50.0

2-Hexanone Ave 0.1027 0.1051 0.0100 51.2 50.0 2.3 50.0

Dibromochloromethane Ave 0.2634 0.2777 0.0100 52.7 50.0 5.4 50.0

1,2-Dibromoethane Ave 0.1542 0.1520 0.0100 49.3 50.0 -1.4 50.0

1-Chlorohexane Ave 0.7247 0.7315 0.0100 50.5 50.0 0.9 50.0

Chlorobenzene Ave 1.046 1.062 0.3000 50.8 50.0 1.6 50.0

Ethylbenzene Ave 0.6127 0.6405 0.0100 52.3 50.0 4.5 20.0

1,1,1,2-Tetrachloroethane Ave 0.3379 0.3577 0.0100 52.9 50.0 5.8 50.0

m&p-Xylene Ave 1.453 1.549 0.0100 107 100 6.6 50.0

o-Xylene Ave 1.406 1.493 0.0100 53.1 50.0 6.2 50.0

Styrene Ave 1.067 1.104 0.0100 51.7 50.0 3.5 50.0

Bromoform Ave 0.1393 0.1427 0.1000 51.2 50.0 2.4 50.0

Isopropylbenzene Ave 4.186 4.518 0.0100 54.0 50.0 7.9 50.0

Bromobenzene Ave 0.8368 0.8578 0.0100 51.3 50.0 2.5 50.0

1,1,2,2-Tetrachloroethane Ave 0.4463 0.4009 0.3000 44.9 50.0 -10.2 50.0

N-Propylbenzene Ave 4.979 5.379 0.0100 54.0 50.0 8.0 50.0

1,2,3-Trichloropropane Ave 0.3465 0.3321 0.0100 47.9 50.0 -4.2 50.0

2-Chlorotoluene Ave 2.750 2.880 0.0100 52.4 50.0 4.7 50.0

1,3,5-Trimethylbenzene Ave 3.254 3.566 0.0100 54.8 50.0 9.6 50.0

4-Chlorotoluene Ave 2.865 3.008 0.0100 52.5 50.0 5.0 50.0

tert-Butylbenzene Ave 2.966 3.183 0.0100 53.6 50.0 7.3 50.0

1,2,4-Trimethylbenzene Ave 3.164 3.489 0.0100 55.1 50.0 10.3 50.0

sec-Butylbenzene Ave 4.606 5.007 0.0100 54.4 50.0 8.7 50.0

1,3-Dichlorobenzene Ave 1.640 1.686 0.0100 51.4 50.0 2.8 50.0

p-Isopropyltoluene Ave 3.718 4.120 0.0100 55.4 50.0 10.8 50.0

1,4-Dichlorobenzene Ave 1.612 1.654 0.0100 51.3 50.0 2.6 50.0

n-Butylbenzene Ave 3.626 4.016 0.0100 55.4 50.0 10.8 50.0

1,2-Dichlorobenzene Ave 1.356 1.354 0.0100 49.9 50.0 -0.2 50.0

1,2-Dibromo-3-Chloropropane Ave 0.0611 0.0607 0.0100 49.7 50.0 -0.7 50.0

1,2,4-Trichlorobenzene Ave 0.9938 1.041 0.0100 52.4 50.0 4.7 50.0

Hexachlorobutadiene Ave 0.8144 0.8913 0.0100 54.7 50.0 9.4 50.0

Naphthalene Ave 1.233 1.216 0.0100 49.3 50.0 -1.3 50.0

1,2,3-Trichlorobenzene Ave 0.7736 0.7901 0.0100 51.1 50.0 2.1 50.0

Dibromofluoromethane Ave 0.4056 0.3816 0.0100 47.0 50.0 -5.9 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2620 0.2511 0.0100 47.9 50.0 -4.2 50.0

Toluene-d8 (Surr) Ave 1.154 1.089 0.0100 47.2 50.0 -5.6 50.0

4-Bromofluorobenzene (Surr) Ave 0.4616 0.4426 0.0100 47.9 50.0 -4.1 50.0

FORM VII 8260B

Page 176 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:30

11/14/2012 09:41

11/14/2012 12:54

CCV 500-173509/3

TestAmerica Chicago

Lab File ID: 25D1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.4056 0.3919 0.0100 48.3 50.0 -3.4 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2620 0.2685 0.0100 51.2 50.0 2.5 50.0

Toluene-d8 (Surr) Ave 1.154 1.117 0.0100 48.4 50.0 -3.2 50.0

4-Bromofluorobenzene (Surr) Ave 0.4616 0.4672 0.0100 50.6 50.0 1.2 50.0

FORM VII 8260B

Page 177 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:30

11/14/2012 09:41

11/14/2012 12:54

CCV 500-173508/3

TestAmerica Chicago

Lab File ID: 25D1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Dibromofluoromethane Ave 0.4056 0.3919 0.0100 48.3 50.0 -3.4 50.0

1,2-Dichloroethane-d4 (Surr) Ave 0.2620 0.2685 0.0100 51.2 50.0 2.5 50.0

Toluene-d8 (Surr) Ave 1.154 1.117 0.0100 48.4 50.0 -3.2 50.0

4-Bromofluorobenzene (Surr) Ave 0.4616 0.4672 0.0100 50.6 50.0 1.2 50.0

FORM VII 8260B

Page 178 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:30

11/14/2012 13:19

11/14/2012 16:08

CCV 500-173509/3

TestAmerica Chicago

Lab File ID: 25D1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 0.8678 0.8362 0.0100 48.2 50.0 -3.6 50.0

Ethyl ether Ave 0.3493 0.3065 0.0100 43.9 50.0 -12.3 50.0

Iodomethane Qua1 0.4434 0.0100 102 100 1.8 50.0

3-Chloropropene Ave 0.2207 0.2460 0.0100 112 100 11.5 50.0

Methyl acetate Ave 0.2344 0.2757 0.0100 58.8 50.0 17.7 50.0

Hexane Ave 1.324 1.247 0.0100 47.1 50.0 -5.8 50.0

Isopropyl ether Ave 1.845 1.840 0.0100 49.9 50.0 -0.3 50.0

2-Chloro-1,3-butadiene Ave 1.221 1.252 0.0100 51.3 50.0 2.6 50.0

Ethyl acetate Ave 0.1818 0.2034 0.0100 560 500 11.9 50.0

Methacrylonitrile Ave 0.1326 0.1554 0.0100 117 100 17.2 50.0

Cyclohexane Ave 1.508 1.444 0.0100 47.9 50.0 -4.2 50.0

2,2,4-Trimethylpentane Ave 2.411 2.437 0.0100 50.5 50.0 1.1 50.0

Isobutyl alcohol Ave 0.0090 0.0108 0.0010 4794 4000 19.9 50.0

Heptane Ave 0.9508 1.035 0.0100 54.5 50.0 8.9 50.0

n-Butyl alcohol Lin1 0.0032 0.0010 4486 4000 12.1 50.0

Methylcyclohexane Ave 0.6690 0.6666 0.0100 49.8 50.0 -0.4 50.0

Methyl methacrylate Ave 0.1324 0.1573 0.0100 119 100 18.8 50.0

2-Nitropropane Ave 0.0447 0.0554 0.0100 4957 4000 23.9 50.0

Ethyl methacrylate Lin1 0.2201 0.0100 102 100 2.0 50.0

Cyclohexanone Qua1 0.0519 0.0100 9878 4000 147.0* 50.0

trans-1,4-Dichloro-2-butene Qua1 0.0685 0.0100 115 100 14.9 50.0

Pentachloroethane Ave 0.2187 0.2646 0.0100 121 100 21.0 50.0

1,3,5-Trichlorobenzene Ave 1.274 1.360 0.0100 53.4 50.0 6.8 50.0

2-Methylnaphthalene Qua1 0.6356 0.0100 45.2 50.0 -9.5 50.0

FORM VII 8260B

Page 179 of 383 01/03/2013
FORM VII

Lab Name: Job No.:

SDG No.:

Instrument ID:

Calibration Date:

Calib Start Date:

Lab Sample ID:

GC Column: ID: Calib End Date:

GC/MS VOA CONTINUING CALIBRATION DATA

500-53315-1

CMS25

12/19/2012 23:30

11/14/2012 13:19

11/14/2012 16:08

CCV 500-173508/3

TestAmerica Chicago

Lab File ID: 25D1219p.D Conc. Units: ug/L Heated Purge: (Y/N) N

ANALYTE CURVE CALC SPIKE %D MAX

TYPE AMOUNT AMOUNT %D

AVE RRF RRF MIN RRF

Butadiene Ave 0.8678 0.8362 0.0100 48.2 50.0 -3.6 50.0

Ethyl ether Ave 0.3493 0.3065 0.0100 43.9 50.0 -12.3 50.0

Iodomethane Qua1 0.4434 0.0100 102 100 1.8 50.0

3-Chloropropene Ave 0.2207 0.2460 0.0100 112 100 11.5 50.0

Methyl acetate Ave 0.2344 0.2757 0.0100 58.8 50.0 17.7 50.0

Hexane Ave 1.324 1.247 0.0100 47.1 50.0 -5.8 50.0

Isopropyl ether Ave 1.845 1.840 0.0100 49.9 50.0 -0.3 50.0

2-Chloro-1,3-butadiene Ave 1.221 1.252 0.0100 51.3 50.0 2.6 50.0

Ethyl acetate Ave 0.1818 0.2034 0.0100 560 500 11.9 50.0

Methacrylonitrile Ave 0.1326 0.1554 0.0100 117 100 17.2 50.0

Cyclohexane Ave 1.508 1.444 0.0100 47.9 50.0 -4.2 50.0

2,2,4-Trimethylpentane Ave 2.411 2.437 0.0100 50.5 50.0 1.1 50.0

Isobutyl alcohol Ave 0.0090 0.0108 0.0010 4794 4000 19.9 50.0

Heptane Ave 0.9508 1.035 0.0100 54.5 50.0 8.9 50.0

n-Butyl alcohol Lin1 0.0032 0.0010 4486 4000 12.1 50.0

Methylcyclohexane Ave 0.6690 0.6666 0.0100 49.8 50.0 -0.4 50.0

Methyl methacrylate Ave 0.1324 0.1573 0.0100 119 100 18.8 50.0

2-Nitropropane Ave 0.0447 0.0554 0.0100 4957 4000 23.9 50.0

Ethyl methacrylate Lin1 0.2201 0.0100 102 100 2.0 50.0

Cyclohexanone Qua1 0.0519 0.0100 9878 4000 147.0* 50.0

trans-1,4-Dichloro-2-butene Qua1 0.0685 0.0100 115 100 14.9 50.0

Pentachloroethane Ave 0.2187 0.2646 0.0100 121 100 21.0 50.0

1,3,5-Trichlorobenzene Ave 1.274 1.360 0.0100 53.4 50.0 6.8 50.0

2-Methylnaphthalene Qua1 0.6356 0.0100 45.2 50.0 -9.5 50.0

FORM VII 8260B

Page 180 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53315-1

Lab Sample ID: MB 500-173225/4

Matrix: Lab File ID: 16M1218.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/18/2012 08:30

DB624 ID:

Analysis Batch No.: 173225 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 2.16

78-93-3 2-Butanone (MEK) <5.00 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 106 70-134

2037-26-5 Toluene-d8 (Surr) 113 75-122

460-00-4 4-Bromofluorobenzene (Surr) 104 70-122

1868-53-7 Dibromofluoromethane 106 75-120

FORM I 8260B

Page 181 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53315-1

Lab Sample ID: MB 500-173508/6

Matrix: Lab File ID: 25M1219p.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL) Date Analyzed: 12/20/2012 00:43

ID:

Analysis Batch No.: 173508 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.29

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 101 75-125

2037-26-5 Toluene-d8 (Surr) 95 75-120

460-00-4 4-Bromofluorobenzene (Surr) 94 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 182 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53315-1

Lab Sample ID: MB 500-173509/6

Matrix: Lab File ID: 25M1219p.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5(mL)

5 (mL)

5(mL)

Date Analyzed: 12/20/2012 00:43

ID:

Analysis Batch No.: 173509 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone <5.00 5.00 1.30

78-93-3 2-Butanone (MEK) <5.00 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 101 75-125

2037-26-5 Toluene-d8 (Surr) 95 75-120

460-00-4 4-Bromofluorobenzene (Surr) 94 75-120

1868-53-7 Dibromofluoromethane 96 75-120

FORM I 8260B

Page 183 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53315-1

Lab Sample ID: LCS 500-173225/5

Matrix: Lab File ID: 16S1218.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/18/2012 08:53

DB624 ID:

Analysis Batch No.: 173225 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 45.56 5.00 2.16

78-93-3 2-Butanone (MEK) 52.85 5.00 1.81

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 104 70-134

2037-26-5 Toluene-d8 (Surr) 111 75-122

460-00-4 4-Bromofluorobenzene (Surr) 103 70-122

1868-53-7 Dibromofluoromethane 105 75-120

FORM I 8260B

Page 184 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53315-1

Lab Sample ID: LCS 500-173508/4

Matrix: Lab File ID: 25S1219p.D

Analysis Method: 8260B Date Collected:

Water

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Low

5(mL) Date Analyzed: 12/19/2012 23:54

ID:

Analysis Batch No.: 173508 Units: ug/L

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 52.35 5.00 1.29

78-93-3 2-Butanone (MEK) 53.39 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 102 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 99 75-120

1868-53-7 Dibromofluoromethane 98 75-120

FORM I 8260B

Page 185 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

SDG No.:

500-53315-1

Lab Sample ID: LCS 500-173509/4

Matrix: Lab File ID: 25S1219p.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor: 1

Level: (low/med) Medium

5(mL)

5 (mL)

5(mL)

Date Analyzed: 12/19/2012 23:54

ID:

Analysis Batch No.: 173509 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 52.35 5.00 1.30

78-93-3 2-Butanone (MEK) 53.39 5.00 1.47

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 102 75-125

2037-26-5 Toluene-d8 (Surr) 97 75-120

460-00-4 4-Bromofluorobenzene (Surr) 99 75-120

1868-53-7 Dibromofluoromethane 98 75-120

FORM I 8260B

Page 186 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC DISCRETE 4 MS

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-3 MS

Matrix: Lab File ID: 53315-03s.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/14/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.1

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/18/2012 09:54

DB624 ID:

Analysis Batch No.: 173225 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 7120 17.3 7.46

78-93-3 2-Butanone (MEK) 329.3 17.3 6.25

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 117 70-134

2037-26-5 Toluene-d8 (Surr) 95 75-122

460-00-4 4-Bromofluorobenzene (Surr) 85 70-122

1868-53-7 Dibromofluoromethane 118 75-120

FORM I 8260B

Page 187 of 383 01/03/2013
FORM I

GC/MS VOA ORGANICS ANALYSIS DATA SHEET Form 1

Client Sample ID:

Lab Name: Job No.:

FC DISCRETE 4 MSD

SDG No.:

500-53315-1

Lab Sample ID: 500-53315-3 MSD

Matrix: Lab File ID: 53315-03t.D

Analysis Method: 8260B Date Collected:

Solid

TestAmerica Chicago

12/14/2012 14:45

Sample wt/vol:

% Moisture:

Soil Extract Vol.: GC Column:

Soil Aliquot Vol: Dilution Factor:

71.1

1

Level: (low/med) Low

5(g)

0.2(mm)

Date Analyzed: 12/18/2012 10:17

DB624 ID:

Analysis Batch No.: 173225 Units: ug/Kg

CAS NO. COMPOUND NAME RESULT Q RL MDL

67-64-1 Acetone 7629 17.3 7.46

78-93-3 2-Butanone (MEK) 303.4 17.3 6.25

CAS NO. SURROGATE %REC Q LIMITS

17060-07-0 1,2-Dichloroethane-d4 (Surr) 119 70-134

2037-26-5 Toluene-d8 (Surr) 96 75-122

460-00-4 4-Bromofluorobenzene (Surr) 84 70-122

1868-53-7 Dibromofluoromethane 116 75-120

FORM I 8260B

Page 188 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53315-1

CMS16

170196

Start Date:

End Date: 11/19/2012 17:14

11/19/2012 11:14

BFB 500-170196/5 11/19/2012 11:14 1 16B1119c.D DB624 0.2(mm)

STD1 500-170196/6 IC 11/19/2012 12:14 1 16I1119A.D DB624 0.2(mm)

STD2 500-170196/7 IC 11/19/2012 12:37 1 16I1119B.D DB624 0.2(mm)

STD3 500-170196/8 

ICIS

11/19/2012 13:00 1 16I1119C.D DB624 0.2(mm)

STD4 500-170196/9 IC 11/19/2012 13:23 1 16I1119D.D DB624 0.2(mm)

STD5 500-170196/10 

IC

11/19/2012 13:46 1 16I1119E.D DB624 0.2(mm)

STD6 500-170196/11 

IC

11/19/2012 14:09 1 16I1119F.D DB624 0.2(mm)

STD1AP 500-170196/12 

IC

11/19/2012 14:32 1 DB624 0.2(mm)

STD2AP 500-170196/13 

IC

11/19/2012 14:55 1 DB624 0.2(mm)

STD3AP 500-170196/14 

IC

11/19/2012 15:18 1 DB624 0.2(mm)

STD4AP 500-170196/15 

IC

11/19/2012 15:42 1 DB624 0.2(mm)

STD5AP 500-170196/16 

IC

11/19/2012 16:05 1 DB624 0.2(mm)

STD6AP 500-170196/17 

IC

11/19/2012 16:28 1 DB624 0.2(mm)

ICV 500-170196/19 11/19/2012 17:14 1 16S1119.D DB624 0.2(mm)

8260B

Page 189 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53315-1

CMS16

173225

Start Date:

End Date: 12/18/2012 10:40

12/18/2012 07:09

BFB 500-173225/1 12/18/2012 07:09 1 16B1218.D DB624 0.2(mm)

CCV 500-173225/2 12/18/2012 07:43 1 16C1218.D DB624 0.2(mm)

CCV 500-173225/3 12/18/2012 08:07 1 16D1218.D DB624 0.2(mm)

MB 500-173225/4 12/18/2012 08:30 1 16M1218.D DB624 0.2(mm)

LCS 500-173225/5 12/18/2012 08:53 1 16S1218.D DB624 0.2(mm)

500-53315-3 FC DISCRETE 4 12/18/2012 09:30 1 53315-03.D DB624 0.2(mm)

500-53315-3 MS FC DISCRETE 4 MS 12/18/2012 09:54 1 53315-03s.D DB624 0.2(mm)

500-53315-3 MSD FC DISCRETE 4 MSD 12/18/2012 10:17 1 53315-03t.D DB624 0.2(mm)

500-53315-4 FC D DISCRETE 4 12/18/2012 10:40 1 53315-04.D DB624 0.2(mm)

8260B

Page 190 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53315-1

CMS25

169636

Start Date:

End Date: 11/14/2012 16:57

11/14/2012 09:17

BFB 500-169636/1 11/14/2012 09:17 1 25B1114.D

STD1 500-169636/2 IC 11/14/2012 09:41 1 25I1114a.D

STD2 500-169636/3 IC 11/14/2012 10:05 1 25I1114b.D

STD3 500-169636/4 IC 11/14/2012 10:29 1 25I1114c.D

STD4 500-169636/5 IC 11/14/2012 10:53 1 25I1114d.D

STD5 500-169636/6 IC 11/14/2012 11:18 1 25I1114e.D

STD6 500-169636/7 

ICIS

11/14/2012 11:42 1 25I1114f.D

STD7 500-169636/8 IC 11/14/2012 12:06 1 25I1114g.D

STD8 500-169636/9 IC 11/14/2012 12:30 1 25I1114h.D

STD9 500-169636/10 

IC

11/14/2012 12:54 1 25I1114i.D

STD2AP 500-169636/11 

IC

11/14/2012 13:19 1

STD3AP 500-169636/12 

IC

11/14/2012 13:43 1

STD4AP 500-169636/13 

IC

11/14/2012 14:07 1

STD5AP 500-169636/14 

IC

11/14/2012 14:31 1

STD6AP 500-169636/15 

IC

11/14/2012 14:55 1

STD7AP 500-169636/16 

IC

11/14/2012 15:20 1

STD8AP 500-169636/17 

IC

11/14/2012 15:44 1

STD9AP 500-169636/18 

IC

11/14/2012 16:08 1

ICV 500-169636/20 11/14/2012 16:57 1 25S1114.D

8260B

Page 191 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53315-1

CMS25

169637

Start Date:

End Date: 11/14/2012 16:57

11/14/2012 09:17

BFB 500-169637/1 11/14/2012 09:17 1 25B1114.D

STD1 500-169637/2 IC 11/14/2012 09:41 1 25I1114a.D

STD2 500-169637/3 IC 11/14/2012 10:05 1 25I1114b.D

STD3 500-169637/4 IC 11/14/2012 10:29 1 25I1114c.D

STD4 500-169637/5 IC 11/14/2012 10:53 1 25I1114d.D

STD5 500-169637/6 IC 11/14/2012 11:18 1 25I1114e.D

STD6 500-169637/7 

ICIS

11/14/2012 11:42 1 25I1114f.D

STD7 500-169637/8 IC 11/14/2012 12:06 1 25I1114g.D

STD8 500-169637/9 IC 11/14/2012 12:30 1 25I1114h.D

STD9 500-169637/10 

IC

11/14/2012 12:54 1 25I1114i.D

STD2AP 500-169637/11 

IC

11/14/2012 13:19 1

STD3AP 500-169637/12 

IC

11/14/2012 13:43 1

STD4AP 500-169637/13 

IC

11/14/2012 14:07 1

STD5AP 500-169637/14 

IC

11/14/2012 14:31 1

STD6AP 500-169637/15 

IC

11/14/2012 14:55 1

STD7AP 500-169637/16 

IC

11/14/2012 15:20 1

STD8AP 500-169637/17 

IC

11/14/2012 15:44 1

STD9AP 500-169637/18 

IC

11/14/2012 16:08 1

ICV 500-169637/20 11/14/2012 16:57 1 25S1114.D

8260B

Page 192 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53315-1

CMS25

173508

Start Date:

End Date: 12/20/2012 08:59

12/19/2012 22:40

BFB 500-173508/1 12/19/2012 22:40 1 25B1219p.D

CCV 500-173508/2 12/19/2012 23:06 1 25C1219p.D

CCV 500-173508/3 12/19/2012 23:30 1 25D1219p.D

LCS 500-173508/4 12/19/2012 23:54 1 25S1219p.D

MB 500-173508/6 12/20/2012 00:43 1 25M1219p.D

500-53315-5 TRIP BLANK 12/20/2012 01:08 1 53315-05.D

500-53315-6 FC EB 4 12/20/2012 01:49 1 53315-06.D

ZZZZZ 12/20/2012 04:42 1

ZZZZZ 12/20/2012 05:19 1

ZZZZZ 12/20/2012 05:43 1

ZZZZZ 12/20/2012 06:07 1

ZZZZZ 12/20/2012 06:32 1

ZZZZZ 12/20/2012 06:56 1

ZZZZZ 12/20/2012 07:21 1

ZZZZZ 12/20/2012 07:45 1

ZZZZZ 12/20/2012 08:10 1

ZZZZZ 12/20/2012 08:34 1

ZZZZZ 12/20/2012 08:59 1

8260B

Page 193 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

GC/MS VOA ANALYSIS RUN LOG

DILUTION

FACTOR

LAB SAMPLE ID CLIENT SAMPLE ID DATE ANALYZED LAB FILE ID COLUMN ID

TestAmerica Chicago 500-53315-1

CMS25

173509

Start Date:

End Date: 12/20/2012 04:18

12/19/2012 22:40

BFB 500-173509/1 12/19/2012 22:40 1 25B1219p.D

CCV 500-173509/2 12/19/2012 23:06 1 25C1219p.D

CCV 500-173509/3 12/19/2012 23:30 1 25D1219p.D

LCS 500-173509/4 12/19/2012 23:54 1 25S1219p.D

MB 500-173509/6 12/20/2012 00:43 1 25M1219p.D

500-53315-3 DL FC DISCRETE 4 DL 12/20/2012 02:16 50 53315-03.D

500-53315-4 DL FC D DISCRETE 4 DL 12/20/2012 02:40 50 53315-04.D

ZZZZZ 12/20/2012 03:05 50

ZZZZZ 12/20/2012 03:29 50

ZZZZZ 12/20/2012 03:54 50

ZZZZZ 12/20/2012 04:18 50

8260B

Page 194 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GC/MS VOA BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173238 12/18/12 07:45 Werner, Brian D

Batch Method:

TestAmerica Chicago

5030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount AnalysisComment

500-53315-A-3 FC DISCRETE 4 5030B, 8260B T 5 g 5 mL meoh

500-53315-A-4 FC D DISCRETE 4 5030B, 8260B T 5 g 5 mL meoh

Batch Notes

Balance ID C-0133

Methanol Lot Number DH247

Pipette ID C-2207

Basis Basis Description

T Total/NA

8260B Page 1 of 1

Page 195 of 383 01/03/2013


METALS

Page 198 of 383 01/03/2013
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

METALS

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53315-1

FC COMPOSITE 4 500-53315-1 

FC D COMPOSITE 4 500-53315-2 

FC EB 4 500-53315-6 

Comments:

Page 199 of 383 01/03/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10

500-53315-1

FC COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: DRY

METALS

TestAmerica Chicago

% Solids: 25.9

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 346 3.70 0.441 mg/Kg 1 6010B

7440-50-8 Copper 834 3.70 1.00 mg/Kg 1 6010B

7440-47-3 Chromium 14400 3.70 0.618 mg/Kg V 1 6010B

7440-02-0 Nickel 89.8 3.70 0.811 mg/Kg V 1 6010B

7439-92-1 Lead 209 1.85 0.637 mg/Kg B V 1 6010B

7440-62-2 Vanadium 241 1.85 0.281 mg/Kg V 1 6010B

7440-66-6 Zinc 481 7.41 2.54 mg/Kg V 1 6010B

7439-97-6 Mercury 0.543 0.0595 0.0227 mg/Kg 1 7471A

FORM IA-IN Page 200 of 383 01/03/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10

500-53315-1

FC COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: WET

METALS - TCLP

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 0.0194 0.500 0.0100 mg/L J 1 6010B

7440-50-8 Copper 0.0487 0.0250 0.0100 mg/L 1 6010B

7440-47-3 Chromium <0.0250 0.0250 0.0100 mg/L 1 6010B

7440-02-0 Nickel 0.0549 0.0250 0.0100 mg/L 1 6010B

7439-92-1 Lead <0.0500 0.0500 0.00500 mg/L 1 6010B

7440-62-2 Vanadium <0.0250 0.0250 0.00500 mg/L 1 6010B

7440-66-6 Zinc <0.100 0.100 0.0200 mg/L 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000020 mg/L

0

1 7470A

FORM IA-IN Page 201 of 383 01/03/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10

500-53315-1

FC D COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: DRY

METALS

TestAmerica Chicago

% Solids: 26.3

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 326 3.46 0.411 mg/Kg 1 6010B

7440-50-8 Copper 784 3.46 0.937 mg/Kg 1 6010B

7440-47-3 Chromium 13200 3.46 0.577 mg/Kg 1 6010B

7440-02-0 Nickel 86.4 3.46 0.757 mg/Kg 1 6010B

7439-92-1 Lead 188 1.73 0.595 mg/Kg B 1 6010B

7440-62-2 Vanadium 221 1.73 0.262 mg/Kg 1 6010B

7440-66-6 Zinc 451 6.92 2.37 mg/Kg 1 6010B

7439-97-6 Mercury 0.248 0.0628 0.0239 mg/Kg 1 7471A

FORM IA-IN Page 202 of 383 01/03/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10

500-53315-1

FC D COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: WET

METALS - TCLP

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium <0.500 0.500 0.0100 mg/L 1 6010B

7440-50-8 Copper 0.0483 0.0250 0.0100 mg/L 1 6010B

7440-47-3 Chromium 0.0120 0.0250 0.0100 mg/L J 1 6010B

7440-02-0 Nickel 0.0582 0.0250 0.0100 mg/L 1 6010B

7439-92-1 Lead <0.0500 0.0500 0.00500 mg/L 1 6010B

7440-62-2 Vanadium <0.0250 0.0250 0.00500 mg/L 1 6010B

7440-66-6 Zinc <0.100 0.100 0.0200 mg/L 1 6010B

7439-97-6 Mercury <0.000200 0.000200 0.000020 mg/L

0

1 7470A

FORM IA-IN Page 203 of 383 01/03/2013
1A-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-6

Date Received: 12/15/2012 09:10

500-53315-1

FC EB 4

Water Date Sampled: 12/14/2012 14:30

Reporting Basis: WET

METALS

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

7440-39-3 Barium 0.000580 0.0100 0.000440 mg/L J B 1 6010B

7440-50-8 Copper 0.00303 0.0100 0.00106 mg/L J 1 6010B

7440-47-3 Chromium 0.00312 0.0100 0.000960 mg/L J B 1 6010B

7440-02-0 Nickel <0.0100 0.0100 0.00190 mg/L 1 6010B

7439-92-1 Lead 0.00214 0.00500 0.00158 mg/L J B 1 6010B

7440-62-2 Vanadium <0.00500 0.00500 0.000620 mg/L 1 6010B

7440-66-6 Zinc 0.00724 0.0200 0.00472 mg/L J 1 6010B

7439-97-6 Mercury 0.000102 0.000200 0.000071 mg/L J

0

1 7470A

FORM IA-IN Page 204 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173224/10

12/17/2012 20:16

Found C True %R

CCV 500-173224/15

12/17/2012 20:51

CCV 500-173224/27

12/17/2012 22:08

Found C True %R Found C True %R

Barium 0.4024 0.400 101 0.5143 0.500 103 0.5097 0.500 102

Chromium 0.4131 0.400 103 0.5169 0.500 103 0.5182 0.500 104

Copper 0.4072 0.400 102 0.5205 0.500 104 0.5167 0.500 103

Lead 0.4153 0.400 104 0.5177 0.500 104 0.5172 0.500 103

Nickel 0.4084 0.400 102 0.5133 0.500 103 0.5128 0.500 103

Vanadium 4.073 4.00 102 5.138 5.00 103 5.132 5.00 103

Zinc 0.4113 0.400 103 0.5095 0.500 102 0.5127 0.500 103

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 205 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173224/39

12/17/2012 23:25

Found C True %R Found C True %R Found C True %R

Barium 0.5136 0.500 103

Chromium 0.5134 0.500 103

Copper 0.5217 0.500 104

Lead 0.5147 0.500 103

Nickel 0.5122 0.500 102

Vanadium 5.141 5.00 103

Zinc 0.5079 0.500 102

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 206 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173517/10

12/19/2012 09:45

Found C True %R

CCV 500-173517/39

12/19/2012 13:02

CCV 500-173517/51

12/19/2012 14:26

Found C True %R Found C True %R

Barium 0.4009 0.400 100 0.5058 0.500 101 0.4985 0.500 100

Chromium 0.4092 0.400 102 0.5060 0.500 101 0.5069 0.500 101

Copper 0.4066 0.400 102 0.5141 0.500 103 0.5071 0.500 101

Lead 0.4102 0.400 103 0.5023 0.500 100 0.5049 0.500 101

Nickel 0.4046 0.400 101 0.5009 0.500 100 0.5041 0.500 101

Vanadium 4.040 4.00 101 5.029 5.00 101 5.027 5.00 101

Zinc 0.4049 0.400 101 0.4922 0.500 98 0.5013 0.500 100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 207 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173517/63

12/19/2012 15:47

Found C True %R Found C True %R Found C True %R

Barium 0.5064 0.500 101

Chromium 0.5161 0.500 103

Copper 0.5146 0.500 103

Lead 0.5134 0.500 103

Nickel 0.5121 0.500 102

Vanadium 5.116 5.00 102

Zinc 0.5102 0.500 102

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 208 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

ICV 500-173518/10

12/19/2012 18:41

Found C True %R

CCV 500-173518/27

12/19/2012 20:32

CCV 500-173518/39

12/19/2012 21:57

Found C True %R Found C True %R

Barium 0.4028 0.400 101 0.5103 0.500 102 0.5135 0.500 103

Chromium 0.4072 0.400 102 0.5110 0.500 102 0.5092 0.500 102

Copper 0.4055 0.400 101 0.5154 0.500 103 0.5149 0.500 103

Lead 0.4072 0.400 102 0.5098 0.500 102 0.5055 0.500 101

Nickel 0.4012 0.400 100 0.5034 0.500 101 0.5014 0.500 100

Vanadium 4.032 4.00 101 5.081 5.00 102 5.067 5.00 101

Zinc 0.4013 0.400 100 0.4996 0.500 100 0.4948 0.500 99

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 209 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M12LICVIC_00001 mg/L

M12LCCVIC_00001

Analyte

CCV 500-173518/51

12/19/2012 23:21

Found C True %R Found C True %R Found C True %R

Barium 0.5130 0.500 103

Chromium 0.5100 0.500 102

Copper 0.5146 0.500 103

Lead 0.5098 0.500 102

Nickel 0.5037 0.500 101

Vanadium 5.078 5.00 102

Zinc 0.4979 0.500 100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 210 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173328/8

12/18/2012 12:59

Found C True %R

CCV 500-173328/12

12/18/2012 13:06

CCV 500-173328/24

12/18/2012 13:29

Found C True %R Found C True %R

Mercury 2.050 2.00 103 1.030 1.00 103 1.110 1.00 111

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 211 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-173328/36

12/18/2012 13:52

Found C True %R

CCV 500-173328/42

12/18/2012 14:03

Found C True %R Found C True %R

Mercury 1.070 1.00 107 0.8470 1.00 85

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 212 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173280/7

12/18/2012 09:03

Found C True %R

CCV 500-173280/19

12/18/2012 09:26

CCV 500-173280/31

12/18/2012 09:51

Found C True %R Found C True %R

Mercury 2.167 2.00 108 0.9179 1.00 92 0.9846 1.00 98

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 213 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

CCV 500-173280/38

12/18/2012 10:19

Found C True %R Found C True %R Found C True %R

Mercury 1.063 1.00 106

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 214 of 383 01/03/2013
2A-IN

Lab Name: Job No.:

SDG No.:

Concentration Units:

CALIBRATION VERIFICATIONS

METALS

ICV Source:

CCV Source:

TestAmerica Chicago 500-53315-1

M11FSTKHG_00001 ug/L

M11FSTKHG_00001

Analyte

ICV 500-173438/7

12/19/2012 10:02

Found C True %R

CCV 500-173438/19

12/19/2012 10:26

CCV 500-173438/28

12/19/2012 10:42

Found C True %R Found C True %R

Mercury 1.885 J 2.00 94 1.056 J 1.00 106 1.092 J 1.00 109

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Italicized analytes were not requested for this sequence.

Page 215 of 383 01/03/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173224/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02010 101 50-150

Copper 0.0200 0.02010 101 50-150

Chromium 0.0200 0.02702 135 50-150

Nickel 0.0200 0.02103 105 50-150

Lead 0.0100 0.01151 115 50-150

Vanadium 0.0100 0.01001 100 50-150

Zinc 0.0400 0.04154 104 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173517/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.01990 100 50-150

Copper 0.0200 0.01955 98 50-150

Chromium 0.0200 0.02070 104 50-150

Nickel 0.0200 0.02010 101 50-150

Lead 0.0100 0.01229 123 50-150

Vanadium 0.0100 0.01023 102 50-150

Zinc 0.0400 0.04138 103 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173517/75

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02015 101 50-150

Copper 0.0200 0.01926 96 50-150

Chromium 0.0200 0.02135 107 50-150

Nickel 0.0200 0.02068 103 50-150

Lead 0.0100 0.01158 116 50-150

Vanadium 0.0100 0.01071 107 50-150

Zinc 0.0400 0.04222 106 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 216 of 383 01/03/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

CRQL CHECK STANDARD

METALS

Method: 6010B Instrument ID: ICP5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRI 500-173518/12

CRQL Check Standard

CRQL Check Standard Source: M12LCRIIC_00001

Concentration Units: mg/L

Barium 0.0200 0.02016 101 50-150

Copper 0.0200 0.01972 99 50-150

Chromium 0.0200 0.02105 105 50-150

Nickel 0.0200 0.01981 99 50-150

Lead 0.0100 0.01011 101 50-150

Vanadium 0.0100 0.01023 102 50-150

Zinc 0.0400 0.04064 102 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 217 of 383 01/03/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

CRQL CHECK STANDARD

METALS

Method: 7470A Instrument ID: HG6

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173280/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 0.2957 148 50-150

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173438/9

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 <2.00 93 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 218 of 383 01/03/2013
2B-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

CRQL CHECK STANDARD

METALS

Method: 7471A Instrument ID: HG5

TestAmerica Chicago

Lab Sample ID:

Analyte True Found Qualifiers %R(1) Limits

CRA 500-173328/10

CRQL Check Standard

CRQL Check Standard Source: M12ASTKHG_00001

Concentration Units: ug/L

Mercury 0.200 0.2100 105 50-150

FORM IIB-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 219 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173224/11 CCB 500-173224/16 CCB 500-173224/28 CCB 500-173224/40

12/17/2012 20:24 12/17/2012 20:58 12/17/2012 22:14 12/17/2012 23:31

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 0.002520 J <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 220 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173517/11 CCB 500-173517/40 CCB 500-173517/52 CCB 500-173517/64

12/19/2012 09:53 12/19/2012 13:08 12/19/2012 14:32 12/19/2012 15:53

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 221 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

mg/L

Analyte RL Found C Found C Found C Found C

ICB 500-173518/11 CCB 500-173518/28 CCB 500-173518/40 CCB 500-173518/52

12/19/2012 18:48 12/19/2012 20:38 12/19/2012 22:04 12/19/2012 23:27

3-IN

Barium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Chromium 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Copper 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Lead 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Nickel 0.0100 <0.0100 <0.0100 <0.0100 <0.0100

Vanadium 0.00500 <0.00500 <0.00500 <0.00500 <0.00500

Zinc 0.0200 <0.0200 <0.0200 <0.0200 <0.0200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 222 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173328/9 CCB 500-173328/13 CCB 500-173328/25 CCB 500-173328/37

12/18/2012 13:01 12/18/2012 13:08 12/18/2012 13:31 12/18/2012 13:54

3-IN

Mercury 0.200 <0.200 <0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 223 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

ug/L

Analyte RL Found C Found C Found C Found C

CCB 500-173328/43

12/18/2012 14:05

3-IN

Mercury 0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 224 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173280/8 CCB 500-173280/20 CCB 500-173280/32 CCB 500-173280/39

12/18/2012 09:04 12/18/2012 09:28 12/18/2012 09:53 12/18/2012 10:21

3-IN

Mercury 0.200 <0.200 <0.200 <0.200 <0.200

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 225 of 383 01/03/2013
Lab Name: Job No.:

Concentration Units:

SDG No.:

INSTRUMENT BLANKS

METALS

TestAmerica Chicago 500-53315-1

ug/L

Analyte RL Found C Found C Found C Found C

ICB 500-173438/8 CCB 500-173438/20 CCB 500-173438/29

12/19/2012 10:04 12/19/2012 10:27 12/19/2012 10:44

3-IN

Mercury 2.00 <2.00 <2.00 <2.00

FORM III-IN

Italicized analytes were not requested for this sequence.

Page 226 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-173139/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: ICP5

METHOD BLANK

METALS

 173224

TestAmerica Chicago

7440-39-3 Barium <1.00 6010B

7440-50-8 Copper <1.00 6010B

7440-47-3 Chromium <1.00 6010B

7440-02-0 Nickel <1.00 6010B

7439-92-1 Lead 0.2420 J 6010B

7440-62-2 Vanadium <0.500 6010B

7440-66-6 Zinc <2.00 6010B

FORM III-IN

Page 227 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173349/1-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: ICP5

METHOD BLANK

METALS

 173517

TestAmerica Chicago

7440-39-3 Barium 0.002710 J 6010B

7440-50-8 Copper <0.0100 6010B

7440-47-3 Chromium 0.001210 J 6010B

7440-02-0 Nickel <0.0100 6010B

7439-92-1 Lead 0.002720 J 6010B

7440-62-2 Vanadium <0.00500 6010B

7440-66-6 Zinc <0.0200 6010B

FORM III-IN

Page 228 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB 500-173187/1-D

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: ICP5

METHOD BLANK

METALS - TCLP

 173518

TestAmerica Chicago

7440-39-3 Barium <0.500 6010B

7440-50-8 Copper <0.0250 6010B

7440-47-3 Chromium <0.0250 6010B

7440-02-0 Nickel <0.0250 6010B

7439-92-1 Lead <0.0500 6010B

7440-62-2 Vanadium <0.0250 6010B

7440-66-6 Zinc <0.100 6010B

FORM III-IN

Page 229 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173172/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: HG6

METHOD BLANK

METALS

 173280

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 230 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: MB 500-173264/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: HG6

METHOD BLANK

METALS

 173438

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 231 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/L Lab Sample ID: LB 500-173187/1-B

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: HG6

METHOD BLANK

METALS - TCLP

 173438

TestAmerica Chicago

7439-97-6 Mercury <0.000200 7470A

FORM III-IN

Page 232 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Concentration Units: mg/Kg Lab Sample ID: MB 500-173153/7-A

CAS No. Analyte Concentration C Q Method

3-IN

Batch No.:

500-53315-1

Instrument Code: HG5

METHOD BLANK

METALS

 173328

TestAmerica Chicago

7439-97-6 Mercury <0.0167 7471A

FORM III-IN

Page 233 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSA 500-173224/13

P51217B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0019

Copper -0.0023

Lead 0.0032

Nickel 0.0013

Vanadium 0.0041

Zinc 0.0078

Aluminum 500 511 102

Antimony 0.0001

Arsenic 0.0014

Beryllium -0.0001

Boron 0.0003

Cadmium 0.0039

Calcium 500 483 97

Cobalt 0.0004

Iron 200 191 96

Magnesium 500 526 105

Manganese 0.0032

Molybdenum 0.0103

Potassium -0.0018

Selenium 0.0006

Silicon 0.0089

Silver 0.0000

Sodium 0.0237

Strontium 0.0023

Thallium 0.0004

Tin 0.0026

Titanium 0.0005

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 234 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSAB 500-173224/14

P51217B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.523 105

Chromium 0.500 0.488 98

Copper 0.500 0.564 113

Lead 0.0500 0.0540 108

Nickel 1.00 0.974 97

Vanadium 0.500 0.516 103

Zinc 1.00 0.917 92

Aluminum 500 515 103

Antimony 0.600 0.620 103

Arsenic 0.100 0.103 103

Beryllium 0.500 0.487 97

Boron 0.0004

Cadmium 1.00 0.959 96

Calcium 500 481 96

Cobalt 0.500 0.481 96

Iron 200 192 96

Magnesium 500 528 106

Manganese 0.500 0.507 101

Molybdenum 0.0109

Potassium -0.0110

Selenium 0.0500 0.0497 99

Silicon 0.0121

Silver 0.200 0.223 111

Sodium 0.0226

Strontium 0.0023

Thallium 0.100 0.107 107

Tin 0.0011

Titanium 0.0005

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 235 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSA 500-173517/13

P51219A

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0020

Copper -0.0022

Lead 0.0054

Nickel 0.0008

Vanadium 0.0041

Zinc 0.0081

Aluminum 500 509 102

Antimony -0.0017

Arsenic -0.0012

Beryllium 0.0000

Boron 0.0004

Cadmium 0.0040

Calcium 500 479 96

Cobalt 0.0001

Iron 200 189 95

Magnesium 500 517 103

Manganese 0.0035

Molybdenum 0.0125

Potassium -0.0053

Selenium 0.0002

Silicon 0.0151

Silver 0.0000

Sodium 0.0079

Strontium 0.0023

Thallium 0.0073

Tin 0.0014

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 236 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSAB 500-173517/14

P51219A

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.518 104

Chromium 0.500 0.482 96

Copper 0.500 0.560 112

Lead 0.0500 0.0528 106

Nickel 1.00 0.948 95

Vanadium 0.500 0.508 102

Zinc 1.00 0.902 90

Aluminum 500 511 102

Antimony 0.600 0.617 103

Arsenic 0.100 0.104 104

Beryllium 0.500 0.481 96

Boron 0.0011

Cadmium 1.00 0.941 94

Calcium 500 479 96

Cobalt 0.500 0.472 94

Iron 200 191 95

Magnesium 500 519 104

Manganese 0.500 0.501 100

Molybdenum 0.0124

Potassium -0.0129

Selenium 0.0500 0.0472 94

Silicon 0.0159

Silver 0.200 0.223 111

Sodium 0.0129

Strontium 0.0023

Thallium 0.100 0.104 104

Tin 0.0020

Titanium 0.0009

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 237 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSA 500-173517/76

P51219A

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0003

Chromium 0.0021

Copper -0.0025

Lead 0.0038

Nickel 0.0004

Vanadium 0.0041

Zinc 0.0080

Aluminum 500 507 101

Antimony 0.0003

Arsenic -0.0005

Beryllium -0.0001

Boron 0.0010

Cadmium 0.0035

Calcium 500 488 98

Cobalt 0.0000

Iron 200 193 97

Magnesium 500 522 104

Manganese 0.0045

Molybdenum 0.0127

Potassium -0.0103

Selenium -0.0026

Silicon 0.0155

Silver 0.0002

Sodium 0.0106

Strontium 0.0022

Thallium 0.0042

Tin -0.0011

Titanium 0.0008

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 238 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSAB 500-173517/77

P51219A

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.508 102

Chromium 0.500 0.490 98

Copper 0.500 0.553 111

Lead 0.0500 0.0533 107

Nickel 1.00 0.965 97

Vanadium 0.500 0.513 103

Zinc 1.00 0.935 93

Aluminum 500 509 102

Antimony 0.600 0.623 104

Arsenic 0.100 0.104 104

Beryllium 0.500 0.490 98

Boron 0.0012

Cadmium 1.00 0.965 96

Calcium 500 488 98

Cobalt 0.500 0.479 96

Iron 200 194 97

Magnesium 500 523 105

Manganese 0.500 0.508 102

Molybdenum 0.0145

Potassium -0.0103

Selenium 0.0500 0.0481 96

Silicon 0.0146

Silver 0.200 0.223 111

Sodium 0.0169

Strontium 0.0022

Thallium 0.100 0.108 108

Tin -0.0003

Titanium 0.0009

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 239 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution A Solution A

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSA 500-173518/13

P51219B

mg/L

M12LISAIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.0000

Chromium 0.0019

Copper -0.0021

Lead 0.0018

Nickel 0.0005

Vanadium 0.0039

Zinc 0.0075

Aluminum 500 509 102

Antimony -0.0009

Arsenic 0.0002

Beryllium -0.0001

Boron 0.0007

Cadmium 0.0025

Calcium 500 478 96

Cobalt 0.0000

Iron 200 189 94

Magnesium 500 519 104

Manganese 0.0048

Molybdenum 0.0125

Potassium -0.0137

Selenium -0.0021

Silicon 0.0145

Silver 0.0002

Sodium 0.0138

Strontium 0.0022

Thallium 0.0058

Tin -0.0017

Titanium 0.0008

Total Heavy Metals 0.0025

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 240 of 383 01/03/2013
4A-IN

Lab Name: Job No.:

Instrument ID:

ICS Source:

Concentration Units:

Analyte

True

Percent

Recovery

Found

SDG No.:

Lab File ID:

Solution AB Solution AB

Lab Sample ID:

TestAmerica Chicago 500-53315-1

ICSAB 500-173518/14

P51219B

mg/L

M12LISBIC_00001

ICP5

INTERFERENCE CHECK STANDARD

METALS

Barium 0.500 0.518 104

Chromium 0.500 0.483 97

Copper 0.500 0.556 111

Lead 0.0500 0.0504 101

Nickel 1.00 0.943 94

Vanadium 0.500 0.508 102

Zinc 1.00 0.902 90

Aluminum 500 510 102

Antimony 0.600 0.613 102

Arsenic 0.100 0.107 107

Beryllium 0.500 0.480 96

Boron 0.0009

Cadmium 1.00 0.935 93

Calcium 500 481 96

Cobalt 0.500 0.470 94

Iron 200 190 95

Magnesium 500 522 104

Manganese 0.500 0.501 100

Molybdenum 0.0115

Potassium -0.0099

Selenium 0.0500 0.0483 97

Silicon 0.0130

Silver 0.200 0.222 111

Sodium 0.0206

Strontium 0.0022

Thallium 0.100 0.104 104

Tin 0.0005

Titanium 0.0008

Total Heavy Metals 4.05 3.87 96

FORM IVA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 241 of 383 01/03/2013
MATRIX SPIKE SAMPLE RECOVERY

METALS

5A-IN

FC COMPOSITE 4 MS

Lab Name: Job No.:

SDG No.:

Client ID: Lab ID: 500-53315-1 MS

500-53315-1

Matrix: Solid Concentration Units: mg/Kg

TestAmerica Chicago

% Solids: 25.9

Control

Limit

%R Analyte SSR 

C

Sample

Result (SR) 

C

Spike

Added (SA) %R Q Method

Barium 987.2 346 762 84 75-125 6010B

Copper 836.2 834 95.2 2 75-125 4 6010B

Chromium 13510 14400 76.2 -1125 75-125 4 6010B

Nickel 246.8 89.8 190 82 75-125 6010B

Lead 253.1 209 38.1 116 75-125 4 6010B

Vanadium 391.8 241 190 79 75-125 6010B

Zinc 605.1 481 190 65 75-125 F 6010B

SSR = Spiked Sample Result

FORM VA - IN

Note - Results and Reporting Limits have been adjusted for dry weight.

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 242 of 383 01/03/2013
MATRIX SPIKE SAMPLE RECOVERY

METALS

5A-IN

FC EB 4 MS

Lab Name: Job No.:

SDG No.:

Client ID: Lab ID: 500-53315-6 MS

500-53315-1

Matrix: Water Concentration Units: mg/L

TestAmerica Chicago

% Solids:

Control

Limit

%R Analyte SSR 

C

Sample

Result (SR) 

C

Spike

Added (SA) %R Q Method

Mercury 0.0009604 0.000102 J 0.00100 86 75-125 7470A

SSR = Spiked Sample Result

FORM VA - IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 243 of 383 01/03/2013
MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

METALS

5A-IN

FC COMPOSITE 4 MSD

Lab Name: Job No.:

SDG No.:

Client ID: Lab ID: 500-53315-1 MSD

500-53315-1

Matrix: Solid Concentration Units: mg/Kg

TestAmerica Chicago

% Solids: 25.9

Analyte (SDR)

C

Control

Limit

%R %R RPD

RPD 

Limit Q Method

Spike

Added (SA) 

Barium 943.9 729 82 75-125 4 20 6010B

Copper 799.8 91.2 -38 75-125 4 20 4 6010B

Chromium 13220 72.9 -1577 75-125 2 20 4 6010B

Nickel 237.5 182 81 75-125 4 20 6010B

Lead 213.5 36.5 12 75-125 17 20 4 6010B

Vanadium 379.3 182 76 75-125 3 20 6010B

Zinc 600.3 182 65 75-125 1 20 F 6010B

SDR = Sample Duplicate Result

FORM VD - IN

Note - Results and Reporting Limits have been adjusted for dry weight.

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 244 of 383 01/03/2013
MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

METALS

5A-IN

FC EB 4 MSD

Lab Name: Job No.:

SDG No.:

Client ID: Lab ID: 500-53315-6 MSD

500-53315-1

Matrix: Water Concentration Units: mg/L

TestAmerica Chicago

% Solids:

Analyte (SDR)

C

Control

Limit

%R %R RPD

RPD 

Limit Q Method

Spike

Added (SA) 

Mercury 0.0007896 0.00100 69 75-125 20 20 F 7470A

SDR = Sample Duplicate Result

FORM VD - IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 245 of 383 01/03/2013
6-IN

DUPLICATES

FC COMPOSITE 4 DU

Lab Name: Job No.:

SDG No.:

Matrix: Concentration Units: mg/Kg

Analyte

Control

Limit Sample (S) 

C

Duplicate (D) 

C

RPD Q Method

500-53315-1

Solid

METALS

% Solids for Sample: 25.9 % Solids for Duplicate:

Client ID: Lab ID: 500-53315-1 DU

25.9

TestAmerica Chicago

Barium 3.73 346 335.3 3 6010B

Copper 3.73 834 804.0 4 6010B

Chromium 3.73 14400 13970 3 6010B

Nickel 3.73 89.8 88.38 2 6010B

Lead 1.86 209 201.3 4 6010B

Vanadium 1.86 241 234.5 3 6010B

Zinc 7.46 481 468.4 3 6010B

FORM VI-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 246 of 383 01/03/2013
6-IN

DUPLICATES

FC EB 4 DU

Lab Name: Job No.:

SDG No.:

Matrix: Concentration Units: mg/L

Analyte

Control

Limit Sample (S) 

C

Duplicate (D) 

C

RPD Q Method

500-53315-1

Water

METALS

% Solids for Sample: % Solids for Duplicate:

Client ID: Lab ID: 500-53315-6 DU

TestAmerica Chicago

Mercury 0.000200 0.000102 J 0.0001082 J 6 7470A

FORM VI-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 247 of 383 01/03/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173139/2-A 

Lab Name: Job No.: 500-53315-1

Sample Matrix: Solid LCS Source: M12KSPKIC_00001

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Barium 200 197.2 99 80 120 6010B

Copper 25.0 24.95 100 80 120 6010B

Chromium 20.0 19.91 100 80 120 6010B

Nickel 50.0 49.11 98 80 120 6010B

Lead 10.0 10.07 101 80 120 6010B

Vanadium 50.0 49.74 99 80 120 6010B

Zinc 50.0 48.83 98 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 248 of 383 01/03/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173349/2-A 

Lab Name: Job No.: 500-53315-1

Sample Matrix: Water LCS Source: M12JSPKIC_00002

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.955 98 80 120 6010B

Copper 0.250 0.2524 101 80 120 6010B

Chromium 0.200 0.1989 99 80 120 6010B

Nickel 0.500 0.4934 99 80 120 6010B

Lead 0.100 0.1010 101 80 120 6010B

Vanadium 0.500 0.4993 100 80 120 6010B

Zinc 0.500 0.4858 97 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 249 of 383 01/03/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173406/3-A 

Lab Name: Job No.: 500-53315-1

Sample Matrix: Water LCS Source: M12KSPKIC_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Barium 2.00 1.975 99 80 120 6010B

Copper 0.250 0.2464 99 80 120 6010B

Chromium 0.200 0.1969 98 80 120 6010B

Nickel 0.500 0.4873 97 80 120 6010B

Lead 0.100 0.09785 98 80 120 6010B

Vanadium 0.500 0.4959 99 80 120 6010B

Zinc 0.500 0.4782 96 80 120 6010B

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 250 of 383 01/03/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173172/8-A 

Lab Name: Job No.: 500-53315-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002027 101 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 251 of 383 01/03/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173264/8-A 

Lab Name: Job No.: 500-53315-1

Sample Matrix: Water LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Water(mg/L)

True Found C %R Limits Q Method

Mercury 0.00200 0.002002 100 80 120 7470A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 252 of 383 01/03/2013
7A-IN

LAB CONTROL SAMPLE

METALS

Lab ID: LCS 500-173153/8-A 

Lab Name: Job No.: 500-53315-1

Sample Matrix: Solid LCS Source: M11FSTKHG_00001

TestAmerica Chicago

Analyte

Solid(mg/Kg)

True Found C %R Limits Q Method

Mercury 0.167 0.1717 103 80 120 7471A

Calculations are performed before rounding to avoid round-off errors in calculated results.

FORM VIIA - IN

Page 253 of 383 01/03/2013
8-IN

Lab ID: 500-53315-1

Lab Name: Job No:

Matrix: Concentration Units: mg/Kg

Analyte

Initial Sample

Result (I) C

Serial

Dilution

Result (S) C

%

Difference Q Method

SDG No:

Solid

500-53315-1

ICP-AES AND ICP-MS SERIAL DILUTIONS

METALS

TestAmerica Chicago

Barium 346 377.6 9.2 6010B

Copper 834 868.4 4.1 6010B

Chromium 14400 16720 16 V 6010B

Nickel 89.8 102.4 14 V 6010B

Lead 209 239.4 15 V 6010B

Vanadium 241 281.4 17 V 6010B

Zinc 481 576.2 20 V 6010B

FORM VIII-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 254 of 383 01/03/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:03

Prep Method: 3010A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.01 0.00044

Chromium 0.01 0.00096

Copper 0.01 0.00106

Lead 0.005 0.00158

Nickel 0.01 0.0019

Vanadium 0.005 0.00062

Zinc 0.02 0.00472

FORM IX - IN

Page 255 of 383 01/03/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:07

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 256 of 383 01/03/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 02/20/2012 13:20

Prep Method: 3050B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Barium 1 0.119

Chromium 1 0.167

Copper 1 0.271

Lead 0.5 0.172

Nickel 1 0.219

Vanadium 0.5 0.0759

Zinc 2 0.686

FORM IX - IN

Page 257 of 383 01/03/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 05/25/2006 09:03

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.005

Chromium 0.01 0.005

Copper 0.01 0.005

Lead 0.005 0.0025

Nickel 0.01 0.005

Vanadium 0.005 0.0025

Zinc 0.02 0.01

FORM IX - IN

Page 258 of 383 01/03/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 6010B MDL Date: 11/01/2005 15:36

Prep Method: 3010A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Barium 0.5 0.01

Chromium 0.025 0.01

Copper 0.025 0.01

Lead 0.05 0.005

Nickel 0.025 0.01

Vanadium 0.025 0.005

Zinc 0.1 0.02

FORM IX - IN

Page 259 of 383 01/03/2013
9-IN

Instrument ID: ICP5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 6010B XMDL Date: 01/28/2008 10:37

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Barium 0.01 0.01

Chromium 0.01 0.01

Copper 0.01 0.01

Lead 0.005 0.005

Nickel 0.01 0.01

Vanadium 0.005 0.005

Zinc 0.02 0.02

FORM IX - IN

Page 260 of 383 01/03/2013
9-IN

Instrument ID: HG6

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 08/31/2012 10:08

Prep Method: 7470A

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 261 of 383 01/03/2013
9-IN

Instrument ID: HG6

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 08/31/2012 10:08

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 262 of 383 01/03/2013
9-IN

Instrument ID: HG6

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

DETECTION LIMITS

Method: 7470A MDL Date: 11/01/2005 11:39

Prep Method: 7470A

Leach Method: 1311

Analyte Wavelength/

Mass

RL MDL

(ug/L) (ug/L)

Mercury 2 0.2

FORM IX - IN

Page 263 of 383 01/03/2013
9-IN

Instrument ID: HG6

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS - TCLP

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7470A XMDL Date: 09/16/2006 08:48

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 2 1

FORM IX - IN

Page 264 of 383 01/03/2013
9-IN

Instrument ID: HG5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

DETECTION LIMITS

Method: 7471A MDL Date: 08/31/2012 10:15

Prep Method: 7471A

Analyte Wavelength/

Mass

RL MDL

(ug/Kg) (ug/Kg)

Mercury 16.7 6.37

FORM IX - IN

Page 265 of 383 01/03/2013
9-IN

Instrument ID: HG5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

METALS

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7471A XMDL Date: 08/31/2012 10:16

Analyte Wavelength/

Mass

XRL XMDL

(ug/L) (ug/L)

Mercury 0.2 0.071

FORM IX - IN

Page 266 of 383 01/03/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53315-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

ICP5

SDG No.:

(mg/L)

11/19/2012 14:31

METALS

Barium 20 6010B

Copper 20 6010B

Chromium 50 6010B

Nickel 50 6010B

Lead 50 6010B

Vanadium 100 6010B

Zinc 20 6010B

FORM XI - IN

Page 267 of 383 01/03/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53315-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG5

SDG No.:

(ug/L)

03/01/2008 11:18

METALS

Mercury 5.0 7471A

FORM XI - IN

Page 268 of 383 01/03/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53315-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

HG6

SDG No.:

(ug/L)

11/01/2010 11:39

METALS

Mercury 5.0 7470A

FORM XI - IN

Page 269 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

METALS

TestAmerica Chicago

Prep Method: 3050B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173139/1-A 12/17/2012 08:50 173139 1 100

LCS 500-173139/2-A 12/17/2012 08:50 173139 1 100

500-53315-1 12/17/2012 08:50 173139 1.0407 100

500-53315-1 DU 12/17/2012 08:50 173139 1.0334 100

500-53315-1 MS 12/17/2012 08:50 173139 1.0117 100

500-53315-1 MSD 12/17/2012 08:50 173139 1.0566 100

500-53315-2 12/17/2012 08:50 173139 1.0994 100

FORM XII-IN

Page 270 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173349/1-A 12/18/2012 15:30 173349 50 50

LCS 500-173349/2-A 12/18/2012 15:30 173349 50 50

500-53315-6 12/18/2012 15:30 173349 50 50

FORM XII-IN

Page 271 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

METALS

TestAmerica Chicago

Prep Method: 3010A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

LB 500-173187/1-D 12/19/2012 08:20 173406 50 50

LCS 500-173406/3-A 12/19/2012 08:20 173406 50 50

500-53315-1 12/19/2012 08:20 173406 50 50

500-53315-2 12/19/2012 08:20 173406 50 50

FORM XII-IN

Page 272 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

METALS

TestAmerica Chicago

Prep Method: 7471A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173153/7-A 12/17/2012 14:00 173153 0.6 50

LCS 500-173153/8-A 12/17/2012 14:00 173153 0.6 50

500-53315-1 12/17/2012 14:00 173153 0.6494 50

500-53315-2 12/17/2012 14:00 173153 0.6068 50

FORM XII-IN

Page 273 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173172/7-A 12/17/2012 13:00 173172 25 25

LCS 500-173172/8-A 12/17/2012 13:00 173172 25 25

500-53315-6 12/17/2012 13:00 173172 25 25

500-53315-6 DU 12/17/2012 13:00 173172 25 25

500-53315-6 MS 12/17/2012 13:00 173172 25 25

500-53315-6 MSD 12/17/2012 13:00 173172 25 25

FORM XII-IN

Page 274 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

METALS

TestAmerica Chicago

Prep Method: 7470A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173264/7-A 12/18/2012 13:00 173264 25 25

LCS 500-173264/8-A 12/18/2012 13:00 173264 25 25

LB 500-173187/1-B 12/18/2012 13:00 173264 25 25

500-53315-1 12/18/2012 13:00 173264 25 25

500-53315-2 12/18/2012 13:00 173264 25 25

FORM XII-IN

Page 275 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

ICP5

12/17/2012 19:16 12/18/2012 02:45

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 19:16

ZZZZZZ 19:22

ZZZZZZ 19:29

ZZZZZZ 19:35

ZZZZZZ 19:41

ZZZZZZ 19:46

ZZZZZZ 19:51

ZZZZZZ 19:59

ZZZZZZ 20:07

ICV 500-173224/10 1 20:16 X X X X X X X

ICB 500-173224/11 1 20:24 X X X X X X X

CRI 500-173224/12 1 20:30 X X X X X X X

ICSA 500-173224/13 1 20:37 X X X X X X X

ICSAB 500-173224/14 1 20:43 X X X X X X X

CCV 500-173224/15 1 20:51 X X X X X X X

CCB 500-173224/16 1 20:58 X X X X X X X

MB 500-173139/1-A 1 T 21:04 X X X X X X X

LCS 500-173139/2-A 1 T 21:10 X X X X X X X

ZZZZZZ 21:16

ZZZZZZ 21:22

ZZZZZZ 21:29

ZZZZZZ 21:35

ZZZZZZ 21:41

ZZZZZZ 21:47

ZZZZZZ 21:54

ZZZZZZ 22:00

CCV 500-173224/27 1 22:08 X X X X X X X

CCB 500-173224/28 1 22:14 X X X X X X X

ZZZZZZ 22:21

ZZZZZZ 22:27

ZZZZZZ 22:33

ZZZZZZ 22:39

500-53315-1 1 T 22:46 X X X X X X X

500-53315-1 SD 5 T 22:52 X X X X X X X

500-53315-1 DU 1 T 22:58 X X X X X X X

500-53315-1 MS 1 T 23:04 X X X X X X X

500-53315-1 MSD 1 T 23:10 X X X X X X X

500-53315-2 1 T 23:17 X X X X X X X

CCV 500-173224/39 1 23:25 X X X X X X X

CCB 500-173224/40 1 23:31 X X X X X X X

ZZZZZZ 23:38

ZZZZZZ 23:44

FORM XIII-IN Page 276 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

ICP5

12/17/2012 19:16 12/18/2012 02:45

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 23:50

ZZZZZZ 23:56

ZZZZZZ 00:02

ZZZZZZ 00:09

ZZZZZZ 00:15

ZZZZZZ 00:21

ZZZZZZ 00:27

ZZZZZZ 00:33

CCV 500-173224/51 00:42

CCB 500-173224/52 00:48

ZZZZZZ 00:54

ZZZZZZ 01:01

ZZZZZZ 01:07

ZZZZZZ 01:13

ZZZZZZ 01:19

ZZZZZZ 01:26

ZZZZZZ 01:32

ZZZZZZ 01:38

ZZZZZZ 01:44

ZZZZZZ 01:50

CCV 500-173224/63 01:59

CCB 500-173224/64 02:05

ZZZZZZ 02:11

ZZZZZZ 02:18

ZZZZZZ 02:24

ZZZZZZ 02:30

CCV 500-173224/69 02:39

CCB 500-173224/70 02:45

Prep Types

T = Total/NA

FORM XIII-IN Page 277 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

ICP5

12/19/2012 08:45 12/19/2012 17:31

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 08:45

ZZZZZZ 08:51

ZZZZZZ 08:57

ZZZZZZ 09:04

ZZZZZZ 09:10

ZZZZZZ 09:15

ZZZZZZ 09:20

ZZZZZZ 09:28

ZZZZZZ 09:36

ICV 500-173517/10 1 09:45 X X X X X X X

ICB 500-173517/11 1 09:53 X X X X X X X

CRI 500-173517/12 1 09:59 X X X X X X X

ICSA 500-173517/13 1 10:05 X X X X X X X

ICSAB 500-173517/14 1 10:12 X X X X X X X

CCV 500-173517/15 10:20

CCB 500-173517/16 10:26

ZZZZZZ 10:33

ZZZZZZ 10:39

ZZZZZZ 10:45

ZZZZZZ 10:52

ZZZZZZ 10:58

ZZZZZZ 11:04

ZZZZZZ 11:11

ZZZZZZ 11:17

ZZZZZZ 11:30

ZZZZZZ 11:37

CCV 500-173517/27 11:45

CCB 500-173517/28 11:51

ZZZZZZ 11:57

ZZZZZZ 12:04

ZZZZZZ 12:10

ZZZZZZ 12:16

ZZZZZZ 12:22

ZZZZZZ 12:28

ZZZZZZ 12:35

ZZZZZZ 12:41

ZZZZZZ 12:47

ZZZZZZ 12:53

CCV 500-173517/39 1 13:02 X X X X X X X

CCB 500-173517/40 1 13:08 X X X X X X X

ZZZZZZ 13:14

ZZZZZZ 13:21

FORM XIII-IN Page 278 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

ICP5

12/19/2012 08:45 12/19/2012 17:31

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 13:27

ZZZZZZ 13:33

ZZZZZZ 13:39

MB 500-173349/1-A 1 T 13:52 X X X X X X X

LCS 500-173349/2-A 1 T 13:58 X X X X X X X

ZZZZZZ 14:04

ZZZZZZ 14:11

ZZZZZZ 14:18

CCV 500-173517/51 1 14:26 X X X X X X X

CCB 500-173517/52 1 14:32 X X X X X X X

ZZZZZZ 14:38

ZZZZZZ 14:45

ZZZZZZ 14:51

500-53315-6 1 T 14:57 X X X X X X X

ZZZZZZ 15:03

ZZZZZZ 15:14

ZZZZZZ 15:20

ZZZZZZ 15:26

ZZZZZZ 15:33

ZZZZZZ 15:39

CCV 500-173517/63 1 15:47 X X X X X X X

CCB 500-173517/64 1 15:53 X X X X X X X

ZZZZZZ 16:00

ZZZZZZ 16:06

ZZZZZZ 16:12

ZZZZZZ 16:18

ZZZZZZ 16:25

ZZZZZZ 16:31

ZZZZZZ 16:37

ZZZZZZ 16:43

CCV 500-173517/73 16:52

CCB 500-173517/74 16:58

CRI 500-173517/75 1 17:04 X X X X X X X

ICSA 500-173517/76 1 17:10 X X X X X X X

ICSAB 500-173517/77 1 17:16 X X X X X X X

CCV 500-173517/78 17:25

CCB 500-173517/79 17:31

Prep Types

T = Total/NA

FORM XIII-IN Page 279 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

ICP5

12/19/2012 17:42 12/20/2012 00:26

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 17:42

ZZZZZZ 17:48

ZZZZZZ 17:54

ZZZZZZ 18:01

ZZZZZZ 18:07

ZZZZZZ 18:12

ZZZZZZ 18:17

ZZZZZZ 18:24

ZZZZZZ 18:33

ICV 500-173518/10 1 18:41 X X X X X X X

ICB 500-173518/11 1 18:48 X X X X X X X

CRI 500-173518/12 1 18:54 X X X X X X X

ICSA 500-173518/13 1 19:00 X X X X X X X

ICSAB 500-173518/14 1 19:06 X X X X X X X

CCV 500-173518/15 19:15

CCB 500-173518/16 19:21

ZZZZZZ 19:27

ZZZZZZ 19:33

ZZZZZZ 19:40

ZZZZZZ 19:46

ZZZZZZ 19:52

ZZZZZZ 19:58

ZZZZZZ 20:04

ZZZZZZ 20:11

ZZZZZZ 20:17

ZZZZZZ 20:23

CCV 500-173518/27 1 20:32 X X X X X X X

CCB 500-173518/28 1 20:38 X X X X X X X

ZZZZZZ 20:44

ZZZZZZ 20:50

ZZZZZZ 20:56

LB 500-173187/1-D 1 P 21:07 X X X X X X X

ZZZZZZ 21:13

LCS 500-173406/3-A 1 T 21:20 X X X X X X X

ZZZZZZ 21:26

ZZZZZZ 21:32

ZZZZZZ 21:43

ZZZZZZ 21:49

CCV 500-173518/39 1 21:57 X X X X X X X

CCB 500-173518/40 1 22:04 X X X X X X X

ZZZZZZ 22:10

ZZZZZZ 22:16

FORM XIII-IN Page 280 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

ICP5

12/19/2012 17:42 12/20/2012 00:26

6010B

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

B

a

C

r

C

u

N

i

P

b

V Z

n

T

y

p

e

ZZZZZZ 22:22

500-53315-1 1 P 22:29 X X X X X X X

500-53315-2 1 P 22:35 X X X X X X X

ZZZZZZ 22:41

ZZZZZZ 22:54

ZZZZZZ 23:00

ZZZZZZ 23:06

ZZZZZZ 23:13

CCV 500-173518/51 1 23:21 X X X X X X X

CCB 500-173518/52 1 23:27 X X X X X X X

ZZZZZZ 23:34

ZZZZZZ 23:40

ZZZZZZ 23:46

ZZZZZZ 23:52

ZZZZZZ 23:59

ZZZZZZ 00:05

ZZZZZZ 00:11

CCV 500-173518/60 00:19

CCB 500-173518/61 00:26

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 281 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

HG6

12/18/2012 08:48 12/18/2012 10:21

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

ZZZZZZ 08:48

ZZZZZZ 08:50

ZZZZZZ 08:52

ZZZZZZ 08:54

ZZZZZZ 08:56

ZZZZZZ 08:59

ICV 500-173280/7 1 09:03 X

ICB 500-173280/8 1 09:04 X

CRA 500-173280/9 1 09:07 X

MB 500-173172/7-A 1 T 09:09 X

LCS 500-173172/8-A 1 T 09:11 X

ZZZZZZ 09:13

ZZZZZZ 09:15

ZZZZZZ 09:17

ZZZZZZ 09:19

ZZZZZZ 09:21

ZZZZZZ 09:23

ZZZZZZ 09:25

CCV 500-173280/19 1 09:26 X

CCB 500-173280/20 1 09:28 X

ZZZZZZ 09:31

ZZZZZZ 09:32

ZZZZZZ 09:35

ZZZZZZ 09:37

ZZZZZZ 09:40

ZZZZZZ 09:42

ZZZZZZ 09:44

ZZZZZZ 09:45

ZZZZZZ 09:47

500-53315-6 1 T 09:49 X

CCV 500-173280/31 1 09:51 X

CCB 500-173280/32 1 09:53 X

500-53315-6 DU 1 T 09:55 X

500-53315-6 MS 1 T 09:57 X

500-53315-6 MSD 1 T 09:59 X

CCV 500-173280/36 10:01

CCB 500-173280/37 10:04

CCV 500-173280/38 1 10:19 X

CCB 500-173280/39 1 10:21 X

Prep Types

T = Total/NA

FORM XIII-IN Page 282 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

HG6

12/19/2012 09:50 12/19/2012 10:50

7470A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

ZZZZZZ 09:50

ZZZZZZ 09:52

ZZZZZZ 09:54

ZZZZZZ 09:56

ZZZZZZ 09:58

ZZZZZZ 10:00

ICV 500-173438/7 1 10:02 X

ICB 500-173438/8 1 10:04 X

CRA 500-173438/9 1 10:07 X

MB 500-173264/7-A 1 T 10:08 X

LCS 500-173264/8-A 1 T 10:10 X

LB 500-173187/1-B 1 P 10:12 X

ZZZZZZ 10:14

ZZZZZZ 10:16

ZZZZZZ 10:18

ZZZZZZ 10:20

ZZZZZZ 10:22

500-53315-1 1 P 10:24 X

CCV 500-173438/19 1 10:26 X

CCB 500-173438/20 1 10:27 X

500-53315-2 1 P 10:29 X

ZZZZZZ 10:31

ZZZZZZ 10:33

ZZZZZZ 10:35

ZZZZZZ 10:37

ZZZZZZ 10:39

ZZZZZZ 10:40

CCV 500-173438/28 1 10:42 X

CCB 500-173438/29 1 10:44 X

ZZZZZZ 10:46

CCV 500-173438/31 10:48

CCB 500-173438/32 10:50

Prep Types

P = TCLP

T = Total/NA

FORM XIII-IN Page 283 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

HG5

12/18/2012 12:44 12/18/2012 14:19

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

STD01REP1 12:44 X

500-173328/1 IC 

STD02REP1 12:46 X

500-173328/2 IC 

STD03REP1 12:47 X

500-173328/3 IC 

STD04REP1 12:49 X

500-173328/4 IC 

STD05REP1 12:51 X

500-173328/5 IC 

STD06REP1 12:53 X

500-173328/6 IC 

ICV 500-173328/7 12:55

ICV 500-173328/8 1 12:59 X

ICB 500-173328/9 1 13:01 X

CRA 500-173328/10 1 13:02 X

MB 500-173153/7-A 1 T 13:04 X

CCV 500-173328/12 1 13:06 X

CCB 500-173328/13 1 13:08 X

LCS 500-173153/8-A 1 T 13:10 X

ZZZZZZ 13:12

ZZZZZZ 13:14

ZZZZZZ 13:16

ZZZZZZ 13:18

ZZZZZZ 13:20

ZZZZZZ 13:21

ZZZZZZ 13:24

ZZZZZZ 13:25

ZZZZZZ 13:27

CCV 500-173328/24 1 13:29 X

CCB 500-173328/25 1 13:31 X

ZZZZZZ 13:33

ZZZZZZ 13:35

ZZZZZZ 13:37

ZZZZZZ 13:39

ZZZZZZ 13:41

ZZZZZZ 13:43

ZZZZZZ 13:45

ZZZZZZ 13:47

ZZZZZZ 13:48

ZZZZZZ 13:50

CCV 500-173328/36 1 13:52 X

CCB 500-173328/37 1 13:54 X

ZZZZZZ 13:56

ZZZZZZ 13:58

FORM XIII-IN Page 284 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

HG5

12/18/2012 12:44 12/18/2012 14:19

7471A

METALS

Lab

Sample

ID

D

/

F

Time

Analytes

H

g

T

y

p

e

500-53315-1 1 T 14:00 X

500-53315-2 1 T 14:01 X

CCV 500-173328/42 1 14:03 X

CCB 500-173328/43 1 14:05 X

ZZZZZZ 14:07

ZZZZZZ 14:09

ZZZZZZ 14:11

ZZZZZZ 14:13

ZZZZZZ 14:15

CCV 500-173328/49 14:17

CCB 500-173328/50 14:19

Prep Types

T = Total/NA

FORM XIII-IN Page 285 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Hudson, Lawrence A

12/17/12 09:20

173139 12/17/12 08:50

Batch Method:

TestAmerica Chicago

3050B

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg InitialAmount FinalAmount M12KSPKIC 00001

CALC NOT SET TO 

RUN

MB 500-173139/1 3050B, 6010B 1 g 100 mL

CALC NOT SET TO 

RUN

LCS 1 g 100 mL 1 mL

500-173139/2

3050B, 6010B

FC COMPOSITE 4 CALC NOT SET TO 

RUN

500-53315-A-1 3050B, 6010B T 1.0407 g 100 mL

FC COMPOSITE 4 CALC NOT SET TO 

RUN

500-53315-A-1 1.0334 g 100 mL

DU

3050B, 6010B T

FC COMPOSITE 4 CALC NOT SET TO 

RUN

500-53315-A-1 1.0117 g 100 mL 1 mL

MS

3050B, 6010B T

FC COMPOSITE 4 CALC NOT SET TO 

RUN

500-53315-A-1 1.0566 g 100 mL 1 mL

MSD

3050B, 6010B T

FC D COMPOSITE 4 CALC NOT SET TO 

RUN

500-53315-A-2 3050B, 6010B T 1.0994 g 100 mL

Batch Notes

Analyst LH

Balance ID C-1966

First End time 0920

Hydrogen peroxide lot number L08A06

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hood ID or number 3

Hot Block ID number 8

Oven, Bath or Block Temperature 1 90 Degrees C

Oven, Bath or Block Temperature 2 90 Degrees C

Pipette ID 1628

Person's name who witnessed reagent drop DB

First Start time 0850

ID number of the thermometer J59717

Digestion Tube/Cup Lot # MF06LKK01

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 286 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Laird, Rebecca

12/18/12 16:00

173349 12/18/12 15:30

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12JSPKIC 00002

MB 500-173349/1 3010A, 6010B 50 mL 50 mL

LCS 50 mL 50 mL 0.5 mL

500-173349/2

3010A, 6010B

500-53315-E-6 FC EB 4 3010A, 6010B T 50 mL 50 mL

Batch Notes

First End time 1600

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L08022

Hot Block ID number 4

Pipette ID 1627

First Start time 1530

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

T Total/NA

6010B Page 1 of 1

Page 287 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Hudson, Lawrence A

12/19/12 08:50

173406 12/19/12 08:20

Batch Method:

TestAmerica Chicago

3010A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M12KSPKIC 00001 AnalysisComment

LB 50 mL 50 mL T-744

500-173187/1-A

3010A, 6010B

LCS 50 mL 50 mL 0.5 mL

500-173406/3

3010A, 6010B

500-53315-A-1-G FC COMPOSITE 4 3010A, 6010B P 50 mL 50 mL

500-53315-A-2-C FC D COMPOSITE 4 3010A, 6010B P 50 mL 50 mL

Batch Notes

Batch Comment T-744, T-748

First End time 0850

Lot # of hydrochloric acid 0000013500

Lot # of Nitric Acid L10022

Hot Block ID number 4

Pipette ID 1627

First Start time 0820

ID number of the thermometer J59688

Digestion Tube/Cup Lot # 20313760

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

Basis Basis Description

P TCLP

6010B Page 1 of 1

Page 288 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/17/12 15:00

173172 12/17/12 13:00

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001 M12ASTKHG 00001

MB 500-173172/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-173172/8

7470A, 7470A

500-53315-E-6 FC EB 4 7470A, 7470A T 25 mL 25 mL

500-53315-E-6 FC EB 4 25 mL 25 mL

DU

7470A, 7470A T

500-53315-E-6 FC EB 4 25 mL 25 mL 0.000025 mL

MS

7470A, 7470A T

500-53315-E-6 FC EB 4 25 mL 25 mL 0.000025 mL

MSD

7470A, 7470A T

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK 7470A Page 1 of 2

Page 289 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/17/12 15:00

173172 12/17/12 13:00

Batch Method:

TestAmerica Chicago

7470A

Basis Basis Description

T Total/NA

7470A Page 2 of 2

Page 290 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/18/12 15:00

173264 12/18/12 13:00

Batch Method:

TestAmerica Chicago

7470A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-173264/7 7470A, 7470A 25 mL 25 mL

LCS 25 mL 25 mL 0.00005 mL

500-173264/8

7470A, 7470A

LB 25 mL 25 mL

500-173187/1-A

7470A, 7470A

500-53315-A-1-G FC COMPOSITE 4 7470A, 7470A P 25 mL 25 mL

500-53315-A-2-C FC D COMPOSITE 4 7470A, 7470A P 25 mL 25 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 6

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 88

Oven, Bath or Block Temperature 2 88

Pipette ID 2240

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Temperature 88 Celsius

ID number of the thermometer hb305412

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Visual ck - digestate F.V. consistency OK

Basis Basis Description

P TCLP 7470A Page 1 of 1

Page 291 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/17/12 14:30

173153 12/17/12 14:00

Batch Method:

TestAmerica Chicago

7471A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount M11FSTKHG 00001

MB 500-173153/7 7471A, 7471A 0.6 g 50 mL

LCS 0.6 g 50 mL 0.0001 mL

500-173153/8

7471A, 7471A

500-53315-A-1 FC COMPOSITE 4 7471A, 7471A T 0.6494 g 50 mL

500-53315-A-2 FC D COMPOSITE 4 7471A, 7471A T 0.6068 g 50 mL

Batch Notes

Hydroxylamine Hydrochloride Lot 19333

Balance ID c0975

Batch Comment STOCK ID: m10cstkhg_00001, m12astkhg_00001 

(Curve)

Blank Soil Lot Number teflon strip_00001

Filter Lot # 21782182

Sulfuric Acid Lot Number k20042

Lot # of hydrochloric acid 0000007153

Lot # of Nitric Acid L03021

Hood ID or number c0454

Hot Block ID number 2

Potassium Persulfate Lot Number k43467

Potassium Permanganate Lot Number k35621

NaCL Lot # UF30BZEMS

Oven, Bath or Block Temperature 1 90

Oven, Bath or Block Temperature 2 90

Pipette ID 1631

Repittetor Volume Check OK

Stannous Chloride Lot Number k21597

Syringe Lot # 1292669

ID number of the thermometer j60025

Digestion Tube/Cup Lot # 1207143

Uncorrected Temperature 90 Celsius

Uncorrected Temperature 2 90 Celsius

7471A Page 1 of 2

Page 292 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

METALS BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Bills, Brandon J

12/17/12 14:30

173153 12/17/12 14:00

Batch Method:

TestAmerica Chicago

7471A

Basis Basis Description

T Total/NA

7471A Page 2 of 2

Page 293 of 383 01/03/2013
GENERAL CHEMISTRY

Page 294 of 383 01/03/2013
COVER PAGE

Lab Name: Job Number: 

Client Sample ID Lab Sample ID

GENERAL CHEMISTRY

Project: John Deere Des Moines Works (JDDMW)

SDG No.:

TestAmerica Chicago 500-53315-1

FC COMPOSITE 4 500-53315-1 

FC D COMPOSITE 4 500-53315-2 

FC DISCRETE 4 500-53315-3 

FC D DISCRETE 4 500-53315-4 

FC EB 4 500-53315-6 

Comments:

Page 295 of 383 01/03/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10

500-53315-1

FC COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: DRY

GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 25.9

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent 3.97 3.85 1.50 mg/Kg 1 7196A

57-12-5 Cyanide, Total 0.745 1.91 0.630 mg/Kg J B 1 9014

18496-25-8 Sulfide 739 93.3 14.9 mg/Kg 1 9034

HEM (Oil & Grease) 11100 1880 835 mg/Kg 1 9071B

FORM IB-IN Page 296 of 383 01/03/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-1

Date Received: 12/15/2012 09:10

500-53315-1

FC COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

Sulfide, Reactive <48.6 48.6 3.79 mg/Kg 1 9034

Flashpoint >176 Degrees 

F

40.0 40.0 1 1010

pH 9.50 0.200 0.200 SU 1 9045C

% Moisture 74.0 0.100 0.100 % 1 SM 2540G

Total Solids 26.0 0.100 0.100 % 1 SM 2540G

FORM IB-IN Page 297 of 383 01/03/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10

500-53315-1

FC D COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: DRY

GENERAL CHEMISTRY

TestAmerica Chicago

% Solids: 26.3

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent 4.08 3.76 1.46 mg/Kg 1 7196A

57-12-5 Cyanide, Total 0.765 1.66 0.549 mg/Kg J B 1 9014

18496-25-8 Sulfide 774 90.8 14.5 mg/Kg 1 9034

HEM (Oil & Grease) 8910 1830 811 mg/Kg 1 9071B

FORM IB-IN Page 298 of 383 01/03/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-2

Date Received: 12/15/2012 09:10

500-53315-1

FC D COMPOSITE 4

Solid Date Sampled: 12/14/2012 15:15

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

Sulfide, Reactive <49.3 49.3 3.85 mg/Kg 1 9034

Flashpoint >176 Degrees 

F

40.0 40.0 1 1010

pH 9.58 0.200 0.200 SU 1 9045C

% Moisture 74.0 0.100 0.100 % 1 SM 2540G

Total Solids 26.0 0.100 0.100 % 1 SM 2540G

FORM IB-IN Page 299 of 383 01/03/2013
1B-IN

INORGANIC ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG ID.:

Matrix:

Lab Sample ID: 500-53315-6

Date Received: 12/15/2012 09:10

500-53315-1

FC EB 4

Water Date Sampled: 12/14/2012 14:30

Reporting Basis: WET

GENERAL CHEMISTRY

TestAmerica Chicago

CAS No. Analyte Result RL MDL Units C Q DIL Method

18540-29-9 Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 1 7196A

57-12-5 Cyanide, Total <0.0100 0.0100 0.00331 mg/L 1 9014

Sulfide, Reactive <1.00 1.00 1.00 mg/L 1 9034

HEM (Oil & Grease) <5.20 5.20 1.51 mg/L 1 1664A

18496-25-8 Sulfide <1.00 1.00 0.230 mg/L 1 9034

FORM IB-IN Page 300 of 383 01/03/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

Analyst: APW Batch Start Date: 12/15/2012

Reporting Units: mg/L Analytical Batch No.: 173079

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 13:20 Chromium, hexavalent 0.2500 0.250 100 90-110 WSTCR2_00008

 2 ICB 13:20 Chromium, hexavalent <0.0100

 8 CCV 13:23 Chromium, hexavalent 0.4943 0.500 99 90-110 WSTCR1_00008

 9 CCB 13:24 Chromium, hexavalent <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 301 of 383 01/03/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

Analyst: APW Batch Start Date: 12/18/2012

Reporting Units: mg/L Analytical Batch No.: 173341

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 15:45 Chromium, hexavalent 0.2699 0.250 108 90-110 WSTCR2_00008

 2 ICB 15:45 Chromium, hexavalent <0.0200

 10 CCV 15:50 Chromium, hexavalent 0.5250 0.500 105 90-110 WSTCR1_00008

 11 CCB 15:51 Chromium, hexavalent <0.0200

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 302 of 383 01/03/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

Analyst: EAT Batch Start Date: 12/18/2012

Reporting Units: mg/L Analytical Batch No.: 173386

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 14:23 Cyanide, Total 0.09250 0.100 93 90-110 WSTINCN2_00559

 2 ICB 14:23 Cyanide, Total <0.0100

 13 CCV 14:26 Cyanide, Total 0.1913 0.200 96 90-110 WSTINCN1_00567

 14 CCB 14:27 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 303 of 383 01/03/2013
2-IN

Lab Name: Job No.:

SDG No.:

500-53315-1

Analyst: EAT Batch Start Date: 12/18/2012

Reporting Units: mg/L Analytical Batch No.: 173387

CALIBRATION QUALITY CONTROL

GENERAL CHEMISTRY

Sample

Number

QC 

Type Time Analyte Result

Spike

Amount

(%)

Recovery Limits Qual Reagent

TestAmerica Chicago

 1 ICV 13:45 Cyanide, Total 0.1041 0.100 104 90-110 WSTINCN2_00559

 2 ICB 13:45 Cyanide, Total <0.0100

 13 CCV 13:48 Cyanide, Total 0.1929 0.200 96 90-110 WSTINCN1_00567

 14 CCB 13:49 Cyanide, Total <0.0100

 25 CCV 13:52 Cyanide, Total 0.1927 0.200 96 90-110 WSTINCN1_00567

 26 CCB 13:52 Cyanide, Total <0.0100

 31 CCV 13:54 Cyanide, Total 0.1924 0.200 96 90-110 WSTINCN1_00567

 32 CCB 13:54 Cyanide, Total <0.0100

FORM II-IN

Note! Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 304 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Method Analyte Result Qual Dil

3-IN

500-53315-1

Lab Sample ID Units

TestAmerica Chicago

METHOD BLANK

GENERAL CHEMISTRY

RL

Batch ID: 173178 Date: 12/18/2012 10:05 Prep Batch: 173173 Date: 12/18/2012 05:25

1664A MB 500-173173/1-A HEM (Oil & Grease) <5.00 mg/L 5.00 1

Batch ID: 173079 Date: 12/15/2012 13:21

7196A MB 500-173079/3 Chromium, hexavalent <0.0100 mg/L 0.0100 1

Batch ID: 173341 Date: 12/18/2012 15:46 Prep Batch: 173258 Date: 12/18/2012 10:00

7196A MB 500-173258/1-A Chromium, hexavalent <1.00 mg/Kg 1.00 1

Batch ID: 173387 Date: 12/18/2012 13:45 Prep Batch: 173245 Date: 12/18/2012 08:30

9014 MB 500-173245/1-A Cyanide, Total <0.0100 mg/L 0.0100 1

Batch ID: 173386 Date: 12/18/2012 14:23 Prep Batch: 173250 Date: 12/18/2012 10:35

9014 MB 500-173250/1-A Cyanide, Total 0.1850 J mg/Kg 0.500 1

Batch ID: 173107 Date: 12/17/2012 00:19 Prep Batch: 173106 Date: 12/17/2012 00:01

9034 MB 500-173106/1-A Sulfide, Reactive <1.00 mg/L 1.00 1

Batch ID: 173108 Date: 12/17/2012 00:19

9034 MB 500-173108/1 Sulfide <1.00 mg/L 1.00 1

Batch ID: 173472 Date: 12/19/2012 12:15 Prep Batch: 173290 Date: 12/19/2012 10:05

9034 MB 500-173290/1-A Sulfide, Reactive <50.0 mg/Kg 50.0 1

Batch ID: 173474 Date: 12/19/2012 13:35 Prep Batch: 173291 Date: 12/19/2012 11:25

9034 MB 500-173291/1-A Sulfide <25.0 mg/Kg 25.0 1

Batch ID: 173330 Date: 12/19/2012 09:20 Prep Batch: 173324 Date: 12/19/2012 05:10

9071B MB 500-173324/1-A HEM (Oil & Grease) <500 mg/Kg 500 1

FORM III-IN

Page 305 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53315-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Solid

5-IN

MATRIX SPIKE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173386 Date: 12/18/2012 14:25 Prep Batch: 173250 Date: 12/18/2012 10:35

9014 500-53315-2 Cyanide, Total 0.765 J mg/Kg B

9014 500-53315-2 

MS 

Cyanide, Total 6.130 mg/Kg 6.63 81 75-125

FORM V-IN

Note - Results and Reporting Limits have been adjusted for dry weight.

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 306 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53315-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173079 Date: 12/15/2012 13:22

7196A 500-53315-6 Chromium, hexavalent <0.0100 mg/L

7196A 500-53315-6 

MS 

Chromium, hexavalent 0.2500 mg/L 0.250 100 85-115

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 307 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53315-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Solid

5-IN

MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173386 Date: 12/18/2012 14:25 Prep Batch: 173250 Date: 12/18/2012 10:35

9014 500-53315-2 

MSD 

Cyanide, Total 6.651 mg/Kg 6.62 89 75-125 8 20

FORM V-IN

Note - Results and Reporting Limits have been adjusted for dry weight.

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 308 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

Matrix:

Analyte

500-53315-1

Method Lab Sample ID Result Unit

Spike

Amount

Pct.

Rec. C Limits RPD

RPD

Limit Q

Water

5-IN

MATRIX SPIKE DUPLICATE SAMPLE RECOVERY

GENERAL CHEMISTRY

TestAmerica Chicago

Batch ID: 173079 Date: 12/15/2012 13:23

7196A 500-53315-6 

MSD 

Chromium, hexavalent 0.2500 mg/L 0.250 100 85-115 0 20

FORM V-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 309 of 383 01/03/2013
7A-IN

Job No.: 500-53315-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Solid

TestAmerica Chicago

Batch ID: 173341 Date: 12/18/2012 15:46 Prep Batch: 173258 Date: 12/18/2012 10:00

LCS Source: WSTCR2_00008

7196A LCS 10.0 83

500-173258/2-

A

Chromium, hexavalent 8.252 mg/Kg 80-120

Batch ID: 173341 Date: 12/18/2012 15:47 Prep Batch: 173258 Date: 12/18/2012 10:00

LCS Source: WSTCR13_00623

7196A LCS 1550 104

500-173258/3-

A

Chromium, hexavalent 1601 mg/Kg 80-120

Batch ID: 173386 Date: 12/18/2012 14:23 Prep Batch: 173250 Date: 12/18/2012 10:35

LCS Source: WSTINCN2_00559

9014 LCS 5.00 105

500-173250/2-

A

Cyanide, Total 5.235 mg/Kg 80-120

Batch ID: 173472 Date: 12/19/2012 12:15 Prep Batch: 173290 Date: 12/19/2012 10:10

LCS Source: WSTSF1_00036

9034 LCS 180 94

500-173290/2-

A

Sulfide, Reactive 168.6 mg/Kg 80-120

Batch ID: 173474 Date: 12/19/2012 13:35 Prep Batch: 173291 Date: 12/19/2012 11:25

LCS Source: WSTSF1_00036

9034 LCS 180 93

500-173291/2-

A

Sulfide 168.3 mg/Kg 80-120

Batch ID: 173330 Date: 12/19/2012 09:31 Prep Batch: 173324 Date: 12/19/2012 05:10

LCS Source: 1664 HEM_00060

9071B LCS 4000 102

500-173324/2-

A

HEM (Oil & Grease) 4090 mg/Kg 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 310 of 383 01/03/2013
7A-IN

Job No.: 500-53315-1

LAB CONTROL SAMPLE

GENERAL CHEMISTRY

Lab Name:

SDG No.:

Q

RPD

Limit Limits RPD

Pct.

Rec.

Spike

Amount Method Lab Sample ID Analyte Result C Unit

Matrix: Water

TestAmerica Chicago

Batch ID: 173178 Date: 12/18/2012 10:11 Prep Batch: 173173 Date: 12/18/2012 05:35

LCS Source: 1664 HEM_00060

1664A LCS 40.0 98

500-173173/2-

A

HEM (Oil & Grease) 39.10 mg/L 78-114

Batch ID: 173079 Date: 12/15/2012 13:21

LCS Source: WSTCR2_00008

7196A LCS 0.250 100

500-173079/4

Chromium, hexavalent 0.2497 mg/L 85-115

Batch ID: 173387 Date: 12/18/2012 13:45 Prep Batch: 173245 Date: 12/18/2012 08:30

LCS Source: WSTINCN2_00559

9014 LCS 0.100 106

500-173245/2-

A

Cyanide, Total 0.1057 mg/L 80-120

Batch ID: 173108 Date: 12/17/2012 00:21

LCS Source: WSTSF1_00036

9034 LCS 3.60 91

500-173108/2

Sulfide 3.286 mg/L 80-120

Batch ID: 173107 Date: 12/17/2012 00:35 Prep Batch: 173106 Date: 12/17/2012 00:05

LCS Source: WSTSF1_00036

9034 LCS 3.60 91

500-173106/2-

A

Sulfide, Reactive 3.292 mg/L 80-120

FORM VIIA-IN

Calculations are performed before rounding to avoid round-off errors in calculated results.

Page 311 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 10:43

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 312 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:44

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.01 0.00325

FORM IX - IN

Page 313 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 7196A MDL Date: 05/29/2012 14:44

Prep Method: 3060A

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Chromium, hexavalent 1 0.389

FORM IX - IN

Page 314 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 7196A XMDL Date: 05/29/2012 10:45

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Chromium, hexavalent 0.02 0.00325

FORM IX - IN

Page 315 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:18

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Cyanide, Total 0.5 0.165

FORM IX - IN

Page 316 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:19

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 317 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9014 MDL Date: 06/18/2012 16:22

Prep Method: 9010B

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 318 of 383 01/03/2013
9-IN

Instrument ID: SPEC5

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

CALIBRATION BLANK DETECTION LIMITS

Method: 9014 XMDL Date: 06/18/2012 16:22

Analyte Wavelength/

Mass

XRL XMDL

(mg/L) (mg/L)

Cyanide, Total 0.01 0.00331

FORM IX - IN

Page 319 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 16:25

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide, Reactive 50 3.9

FORM IX - IN

Page 320 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 01/02/2006 09:18

Prep Method: 7.3.4

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide, Reactive 1 1

FORM IX - IN

Page 321 of 383 01/03/2013
9-IN

Instrument ID: FP4

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1010 MDL Date: 11/11/2005 10:25

Analyte Wavelength/

Mass

RL MDL

(Degrees (Degrees F)

Flashpoint 40 40

FORM IX - IN

Page 322 of 383 01/03/2013
9-IN

Instrument ID: NoEquip

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 1664A MDL Date: 05/29/2012 15:22

Prep Method: 1664A

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

HEM (Oil & Grease) 5 1.45

FORM IX - IN

Page 323 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Water

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:57

Analyte Wavelength/

Mass

RL MDL

(mg/L) (mg/L)

Sulfide 1 0.23

FORM IX - IN

Page 324 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9034 MDL Date: 05/29/2012 15:59

Prep Method: 9030B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

Sulfide 25 4

FORM IX - IN

Page 325 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9045C MDL Date: 11/01/2005 06:06

Analyte Wavelength/

Mass

RL MDL

(SU) (SU)

pH 0.2 0.2

FORM IX - IN

Page 326 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: 9071B MDL Date: 05/29/2012 15:24

Prep Method: 9071B

Analyte Wavelength/

Mass

RL MDL

(mg/Kg) (mg/Kg)

HEM (Oil & Grease) 500 222

FORM IX - IN

Page 327 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: Moisture MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

Percent Moisture 0.1 0.1

Percent Solids 0.1 0.1

FORM IX - IN

Page 328 of 383 01/03/2013
9-IN

Instrument ID: NOEQUIP

Job Number: 500-53315-1

Matrix: Solid

SDG Number:

Lab Name:

GENERAL CHEMISTRY

TestAmerica Chicago

DETECTION LIMITS

Method: SM 2540G MDL Date: 11/01/2005 09:02

Analyte Wavelength/

Mass

RL MDL

(%) (%)

% Moisture 0.1 0.1

Total Solids 0.1 0.1

FORM IX - IN

Page 329 of 383 01/03/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53315-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

SPEC5

SDG No.:

(mg/L)

05/03/2010 07:21

GENERAL CHEMISTRY

Chromium, hexavalent 0.5 7196A

Cyanide, Total 0.400 9014

FORM XI - IN

Page 330 of 383 01/03/2013
11-IN

Lab Name: TestAmerica Chicago Job No: 500-53315-1

Instrument ID: Date:

Analyte

Integ.

Time

(Sec.)

Concentration

Method

LINEAR RANGES

SPEC5

SDG No.:

(mg/L)

05/03/2010 07:27

GENERAL CHEMISTRY

Chromium, hexavalent 1.0 7196A

FORM XI - IN

Page 331 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173106/1-A 12/17/2012 00:01 173106 250 250

LCS 500-173106/2-A 12/17/2012 00:05 173106 250 250

500-53315-6 12/17/2012 00:13 173106 250 250

FORM XII-IN

Page 332 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173245/1-A 12/18/2012 08:30 173245 50 50

LCS 500-173245/2-A 12/18/2012 08:30 173245 50 50

500-53315-6 12/18/2012 08:30 173245 50 50

FORM XII-IN

Page 333 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9010B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173250/1-A 12/18/2012 10:35 173250 1.0000 50

LCS 500-173250/2-A 12/18/2012 10:35 173250 1.0000 50

500-53315-1 12/18/2012 10:35 173250 1.0092 50

500-53315-2 12/18/2012 10:35 173250 1.1423 50

500-53315-2 MS 12/18/2012 10:35 173250 1.1473 50

500-53315-2 MSD 12/18/2012 10:35 173250 1.1489 50

FORM XII-IN

Page 334 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 3060A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173258/1-A 12/18/2012 10:00 173258 2.5 100

LCS 500-173258/2-A 12/18/2012 10:00 173258 2.5 100

LCS 500-173258/3-A 12/18/2012 10:00 173258 2.5 100

500-53315-1 12/18/2012 10:00 173258 2.5027 100

500-53315-2 12/18/2012 10:00 173258 2.5245 100

FORM XII-IN

Page 335 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 7.3.4

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173290/1-A 12/19/2012 10:05 173290 10.0000 10

LCS 500-173290/2-A 12/19/2012 10:10 173290 10.0000 10

500-53315-1 12/19/2012 10:40 173290 10.2894 10

500-53315-2 12/19/2012 10:45 173290 10.1413 10

FORM XII-IN

Page 336 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 1664A

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(mL) (mL)

MB 500-173173/1-A 12/18/2012 05:25 173173 1000 1000

LCS 500-173173/2-A 12/18/2012 05:35 173173 1000 1000

500-53315-6 12/18/2012 07:24 173173 961 1000

FORM XII-IN

Page 337 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9030B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173291/1-A 12/19/2012 11:25 173291 10.0000 10

LCS 500-173291/2-A 12/19/2012 11:25 173291 10.0000 10

500-53315-1 12/19/2012 11:25 173291 10.3275 10

500-53315-2 12/19/2012 11:25 173291 10.4669 10

FORM XII-IN

Page 338 of 383 01/03/2013
12-IN

PREPARATION LOG

Lab Name: Job No.:

SDG No.:

500-53315-1

GENERAL CHEMISTRY

TestAmerica Chicago

Prep Method: 9071B

Lab

Sample

ID

Preparation

Date

Initial

Weight

Final 

Volume

Prep

Batch

Initial

Volume

(g) (mL)

MB 500-173324/1-A 12/19/2012 05:10 173324 10 10

LCS 500-173324/2-A 12/19/2012 05:10 173324 10 10

500-53315-1 12/19/2012 05:10 173324 10.2484 10

500-53315-2 12/19/2012 05:10 173324 10.4122 10

FORM XII-IN

Page 339 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

SPEC5

12/15/2012 13:20 12/15/2012 13:24

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-173079/1 1 13:20 X

ICB 500-173079/2 1 13:20 X

MB 500-173079/3 1 T 13:21 X

LCS 500-173079/4 1 T 13:21 X

500-53315-6 1 T 13:22 X

500-53315-6 MS 1 T 13:22 X

500-53315-6 MSD 1 T 13:23 X

CCV 500-173079/8 1 13:23 X

CCB 500-173079/9 1 13:24 X

ZZZZZZ 13:24

Prep Types

T = Total/NA

FORM XIII-IN Page 340 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

SPEC5

12/18/2012 15:45 12/18/2012 15:59

7196A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

r

6 T

y

p

e

ICV 500-173341/1 1 15:45 X

ICB 500-173341/2 1 15:45 X

MB 500-173258/1-A 1 T 15:46 X

LCS 500-173258/2-A 1 T 15:46 X

LCS 500-173258/3-A 50 T 15:47 X

ZZZZZZ 15:48

ZZZZZZ 15:48

500-53315-1 1 T 15:49 X

500-53315-2 1 T 15:50 X

CCV 500-173341/10 1 15:50 X

CCB 500-173341/11 1 15:51 X

ZZZZZZ 15:52

ZZZZZZ 15:52

ZZZZZZ 15:53

ZZZZZZ 15:54

ZZZZZZ 15:54

ZZZZZZ 15:55

ZZZZZZ 15:56

CCV 500-173341/19 15:56

CCB 500-173341/20 15:57

ZZZZZZ 15:58

CCV 500-173341/22 15:58

CCB 500-173341/23 15:59

Prep Types

T = Total/NA

FORM XIII-IN Page 341 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

SPEC5

12/18/2012 13:45 12/18/2012 13:54

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-173387/1 1 13:45 X

ICB 500-173387/2 1 13:45 X

MB 500-173245/1-A 1 T 13:45 X

LCS 500-173245/2-A 1 T 13:45 X

ZZZZZZ 13:46

ZZZZZZ 13:46

ZZZZZZ 13:46

ZZZZZZ 13:47

ZZZZZZ 13:47

ZZZZZZ 13:47

ZZZZZZ 13:48

ZZZZZZ 13:48

CCV 500-173387/13 1 13:48 X

CCB 500-173387/14 1 13:49 X

ZZZZZZ 13:49

ZZZZZZ 13:49

ZZZZZZ 13:50

ZZZZZZ 13:50

ZZZZZZ 13:50

ZZZZZZ 13:50

ZZZZZZ 13:51

ZZZZZZ 13:51

ZZZZZZ 13:51

ZZZZZZ 13:52

CCV 500-173387/25 1 13:52 X

CCB 500-173387/26 1 13:52 X

ZZZZZZ 13:53

ZZZZZZ 13:53

ZZZZZZ 13:53

500-53315-6 1 T 13:54 X

CCV 500-173387/31 1 13:54 X

CCB 500-173387/32 1 13:54 X

Prep Types

T = Total/NA

FORM XIII-IN Page 342 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

SPEC5

12/18/2012 14:23 12/18/2012 14:29

9014

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

C

N

T

y

p

e

ICV 500-173386/1 1 14:23 X

ICB 500-173386/2 1 14:23 X

MB 500-173250/1-A 1 T 14:23 X

LCS 500-173250/2-A 1 T 14:23 X

ZZZZZZ 14:24

500-53315-1 1 T 14:24 X

500-53315-2 1 T 14:24 X

500-53315-2 MS 1 T 14:25 X

500-53315-2 MSD 1 T 14:25 X

ZZZZZZ 14:25

ZZZZZZ 14:26

ZZZZZZ 14:26

CCV 500-173386/13 1 14:26 X

CCB 500-173386/14 1 14:27 X

ZZZZZZ 14:27

ZZZZZZ 14:27

ZZZZZZ 14:28

ZZZZZZ 14:28

ZZZZZZ 14:28

ZZZZZZ 14:29

CCV 500-173386/21 14:29

CCB 500-173386/22 14:29

Prep Types

T = Total/NA

FORM XIII-IN Page 343 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/17/2012 00:19 12/17/2012 01:08

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-173106/1-A 1 T 00:19 X

LCS 500-173106/2-A 1 T 00:35 X

ZZZZZZ 00:52

500-53315-6 1 T 01:08 X

Prep Types

T = Total/NA

FORM XIII-IN Page 344 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/19/2012 12:15 12/19/2012 12:24

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

R

e

a

c

T

y

p

e

MB 500-173290/1-A 1 T 12:15 X

LCS 500-173290/2-A 1 T 12:15 X

ZZZZZZ 12:16

ZZZZZZ 12:17

ZZZZZZ 12:17

500-53315-1 1 T 12:18 X

500-53315-2 1 T 12:19 X

ZZZZZZ 12:19

ZZZZZZ 12:20

ZZZZZZ 12:21

ZZZZZZ 12:22

ZZZZZZ 12:22

ZZZZZZ 12:23

ZZZZZZ 12:24

Prep Types

T = Total/NA

FORM XIII-IN Page 345 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

FP4

12/19/2012 14:45 12/19/2012 18:00

1010

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

F

P

T

y

p

e

ZZZZZZ 14:45

ZZZZZZ 15:24

ZZZZZZ 16:03

ZZZZZZ 16:42

500-53315-1 1 T 17:21 X

500-53315-2 1 T 18:00 X

Prep Types

T = Total/NA

FORM XIII-IN Page 346 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NoEquip

12/18/2012 10:05 12/18/2012 12:23

1664A

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-173173/1-A 1 T 10:05 X

LCS 500-173173/2-A 1 T 10:11 X

ZZZZZZ 10:17

ZZZZZZ 10:23

ZZZZZZ 10:30

ZZZZZZ 10:36

ZZZZZZ 10:42

ZZZZZZ 10:49

ZZZZZZ 10:55

ZZZZZZ 11:01

ZZZZZZ 11:08

500-53315-6 1 T 11:14 X

ZZZZZZ 11:20

ZZZZZZ 11:26

ZZZZZZ 11:33

ZZZZZZ 11:39

ZZZZZZ 11:45

ZZZZZZ 11:52

ZZZZZZ 11:58

ZZZZZZ 12:04

ZZZZZZ 12:11

ZZZZZZ 12:17

ZZZZZZ 12:23

Prep Types

T = Total/NA

FORM XIII-IN Page 347 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/17/2012 00:19 12/17/2012 01:22

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-173108/1 1 T 00:19 X

LCS 500-173108/2 1 T 00:21 X

ZZZZZZ 00:24

ZZZZZZ 00:27

ZZZZZZ 00:30

ZZZZZZ 00:32

ZZZZZZ 00:35

ZZZZZZ 00:38

ZZZZZZ 00:41

ZZZZZZ 00:43

ZZZZZZ 00:46

ZZZZZZ 00:49

ZZZZZZ 00:52

ZZZZZZ 00:54

ZZZZZZ 00:57

ZZZZZZ 01:00

ZZZZZZ 01:03

ZZZZZZ 01:05

ZZZZZZ 01:08

500-53315-6 1 T 01:11 X

ZZZZZZ 01:14

ZZZZZZ 01:16

ZZZZZZ 01:19

ZZZZZZ 01:22

Prep Types

T = Total/NA

FORM XIII-IN Page 348 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/19/2012 13:35 12/19/2012 13:39

9034

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

S

2

T

y

p

e

MB 500-173291/1-A 1 T 13:35 X

LCS 500-173291/2-A 1 T 13:35 X

ZZZZZZ 13:36

500-53315-1 1 T 13:36 X

500-53315-2 1 T 13:37 X

ZZZZZZ 13:38

ZZZZZZ 13:38

ZZZZZZ 13:39

Prep Types

T = Total/NA

FORM XIII-IN Page 349 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/19/2012 13:35 12/20/2012 17:10

9045C

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

p

H

T

y

p

e

ZZZZZZ 13:35

ZZZZZZ 13:41

ZZZZZZ 13:47

ZZZZZZ 13:53

ZZZZZZ 13:59

ZZZZZZ 18:30

ZZZZZZ 19:29

ZZZZZZ 20:28

ZZZZZZ 21:28

ZZZZZZ 22:27

ZZZZZZ 23:26

ZZZZZZ 00:25

ZZZZZZ 01:24

ZZZZZZ 02:23

ZZZZZZ 03:22

ZZZZZZ 04:22

ZZZZZZ 05:21

ZZZZZZ 06:20

ZZZZZZ 07:19

ZZZZZZ 08:18

ZZZZZZ 09:17

ZZZZZZ 10:16

ZZZZZZ 11:16

ZZZZZZ 12:15

ZZZZZZ 13:14

ZZZZZZ 14:13

500-53315-1 1 T 15:12 X

500-53315-2 1 T 16:11 X

ZZZZZZ 17:10

Prep Types

T = Total/NA

FORM XIII-IN Page 350 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/19/2012 09:20 12/19/2012 11:23

9071B

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

H

E

M T

y

p

e

MB 500-173324/1-A 1 T 09:20 X

LCS 500-173324/2-A 1 T 09:31 X

ZZZZZZ 09:42

ZZZZZZ 09:53

ZZZZZZ 10:05

ZZZZZZ 10:16

ZZZZZZ 10:27

ZZZZZZ 10:38

ZZZZZZ 10:50

500-53315-1 1 T 11:01 X

500-53315-2 1 T 11:12 X

ZZZZZZ 11:23

Prep Types

T = Total/NA

FORM XIII-IN Page 351 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/15/2012 12:43 12/15/2012 12:43

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

ZZZZZZ 12:43

500-53315-1 1 T 12:43 X X

500-53315-2 1 T 12:43 X X

Prep Types

T = Total/NA

FORM XIII-IN Page 352 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/18/2012 12:44 12/18/2012 14:38

Moisture

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

%

S

o

l

M

o

i

s

t

T

y

p

e

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

ZZZZZZ 12:44

500-53315-3 1 T 13:59 X X

500-53315-4 1 T 13:59 X X

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:12

ZZZZZZ 14:26

ZZZZZZ 14:26

ZZZZZZ 14:26

ZZZZZZ 14:38

Prep Types

T = Total/NA

FORM XIII-IN Page 353 of 383 01/03/2013
13-IN

ANALYSIS RUN LOG

Lab Name: Job No.:

SDG No.:

Instrument ID: Method:

Start Date: End Date:

TestAmerica Chicago 500-53315-1

NOEQUIP

12/18/2012 07:34 12/18/2012 07:34

SM 2540G

GENERAL CHEMISTRY

Lab

Sample

ID

D

/

F

Time

Analytes

M

o

i

s

t

T

S

T

y

p

e

500-53315-1 1 T 07:34 X X

500-53315-2 1 T 07:34 X X

Prep Types

T = Total/NA

FORM XIII-IN Page 354 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/15/12 13:25

173079 12/15/12 13:20

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL 100 mL Color Resp. is 

Blank

ICV 25 uL

500-173079/1

7196A

Color Resp. is 

Blank

ICB 

500-173079/2

7196A

Color Resp. is 

Blank

MB 500-173079/3 7196A

100 mL 100 mL Color Resp. is 

Blank

LCS 25 uL

500-173079/4

7196A

FC EB 4 Color Resp. is 

Blank

500-53315-F-6 7196A T

FC EB 4 100 mL 100 mL Color Resp. is 

Blank

500-53315-F-6 25 uL

MS

7196A T

FC EB 4 100 mL 100 mL Color Resp. is 

Blank

500-53315-F-6 25 uL

MSD

7196A T

100 mL 100 mL Color Resp. is 

Blank

CCV 50 uL

500-173079/8

7196A

Color Resp. is 

Blank

CCB 

500-173079/9

7196A

Batch Notes

Batch Comment filter paper lot# 100232

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number Hexa Chrome Color Reagent-00007

First End time See Start Date/Time

First Start time See Start Date/Time

Sulfuric Acid Reagent ID Number H2SO4 00007

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 355 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/18/12 11:00

173258 12/18/12 10:00

Batch Method:

TestAmerica Chicago

3060A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount Initial pH Final pH WSTCR13 00623 WSTCR2 00008

MB 500-173258/1 3060A, 7196A 2.5 g 100 mL 13 SU 7.5 SU

LCS 2.5 g 100 mL 13 SU 7.5 SU 25 uL

500-173258/2

3060A, 7196A

LCS 2.5 g 100 mL 13 SU 7.5 SU 100 mL

500-173258/3

3060A, 7196A

500-53315-A-1 FC COMPOSITE 4 3060A, 7196A T 2.5027 g 100 mL 13 SU 7.5 SU

500-53315-A-2 FC D COMPOSITE 4 3060A, 7196A T 2.5245 g 100 mL 13 SU 7.5 SU

Lab Sample ID Client Sample ID Method Chain Basis AnalysisComment

MB 500-173258/1 3060A, 7196A

LCS soluble

500-173258/2

3060A, 7196A

insoluble 

0.0240

LCS 

500-173258/3

3060A, 7196A

500-53315-A-1 FC COMPOSITE 4 3060A, 7196A T

500-53315-A-2 FC D COMPOSITE 4 3060A, 7196A T

Batch Notes

Alkaline Digestion Solution Reagent ID CR6digestion_00028

Batch Comment Filter Paper Lot # 100727

First End time see above

Potassium Chromate Lot # K00741

Potassium Phosphate Buffer Reagent ID Pot PO4_Buff_00002

Lead Chromate Lot # 15813PE

Lead Chromate Vendor ID Lead(II)Chrom_00001

Magnesium Chloride Lot Number J14N64 (MagCl_crystal_00002)

Magnesium Chloride Vendor JT Baker

First Start time see above

Ending Temperature 90 Celsius

Starting Temperature 90 Celsius

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 356 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/18/12 16:00

173341 12/18/12 15:45

Batch Method:

TestAmerica Chicago

7196A

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount CalcMsg WSTCR1 00008 WSTCR2 00008

100 mL Color Resp. is 

Blank

ICV 25 uL

500-173341/1

7196A

Color Resp. is 

Blank

ICB 

500-173341/2

7196A

Color Resp. is 

Blank

MB 

500-173258/1-A

7196A

Color Resp. is 

Blank

LCS 

500-173258/2-A

7196A

Color Resp. is 

Blank

LCS 

500-173258/3-A

7196A

FC COMPOSITE 4 Color Resp. is 

Blank

500-53315-A-1-I 7196A T

FC D COMPOSITE 4 Color Resp. is 

Blank

500-53315-A-2-G 7196A T

100 mL Color Resp. is 

Blank

CCV 50 uL

500-173341/10

7196A

Color Resp. is 

Blank

CCB 

500-173341/11

7196A

Batch Notes

Spectrophotometer Cell Path Length 540NM1CM cm

Color Reagent ID Number CR+6 ColorRGT_00007

Sulfuric Acid Reagent ID Number H2SO4_00007

Basis Basis Description

T Total/NA

7196A Page 1 of 1

Page 357 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/18/12 10:00

173245 12/18/12 08:30

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00559

MB 500-173245/1 9010B, 9014 50 mL 50 mL y

LCS 50 mL 50 mL y 500 uL

500-173245/2

9010B, 9014

500-53315-D-6 FC EB 4 9010B, 9014 T 50 mL 50 mL y

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00017

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

9014 Page 1 of 1

Page 358 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/18/12 12:05

173250 12/18/12 10:35

Batch Method:

TestAmerica Chicago

9010B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SulfideCheck WSTINCN2 00559

MB 500-173250/1 9010B, 9014 1.0000 g 50 mL y

LCS 1.0000 g 50 mL y 500 uL

500-173250/2

9010B, 9014

500-53315-A-1 FC COMPOSITE 4 9010B, 9014 T 1.0092 g 50 mL y

500-53315-A-2 FC D COMPOSITE 4 9010B, 9014 T 1.1423 g 50 mL y

500-53315-A-2 FC D COMPOSITE 4 1.1473 g 50 mL y 200 uL

MS

9010B, 9014 T

500-53315-A-2 FC D COMPOSITE 4 1.1489 g 50 mL y 200 uL

MSD

9010B, 9014 T

Batch Notes

Bismuth Nitrate Lot # BismuthNO3_00017

Ca(OCl)2 Reagent ID Number CaCL2O2_00006

Distillation Temperature REFLUXING Degrees C

KI-Starch Paper Lot # 071409

Lead Acetate Lot # 121109

Methyl Red Indicator Reagent ID Meth_Red_IN_00001

Magnesium Chloride Reagent ID Number MagChloride_00010

NaAsO2 Reagent ID Number AscorbicAcid_00003

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00005

Sulfamic Acid Reagent ID Number SulfamicAcid_00022

Sulfuric Acid Reagent ID Number 50%H2SO4_00007

Zinc Acetate Buffer Reagent ID Number IO8ARCN14

Basis Basis Description

T Total/NA

9014 Page 1 of 1

Page 359 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/18/12 14:30

173386 12/18/12 14:23

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00567 WSTINCN2 00559

ICV 25 mL 25 mL 250 uL

500-173386/1

9014

CCV 25 mL 25 mL 500 uL

500-173386/13

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

9014 Page 1 of 1

Page 360 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Treadwell, Eliane A

12/18/12 13:55

173387 12/18/12 13:45

Batch Method:

TestAmerica Chicago

9014

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTINCN1 00567 WSTINCN2 00559

ICV 25 mL 25 mL 250 uL

500-173387/1

9014

CCV 25 mL 25 mL 500 uL

500-173387/13

9014

CCV 25 mL 25 mL 500 uL

500-173387/25

9014

CCV 25 mL 25 mL 500 uL

500-173387/31

9014

Batch Notes

Buffer Reagent ID Number SPMM Buffer_00044

Chloramine-T Reagent ID Number Chloramine-T_00002

KI-Starch Paper Lot # 110510

NaOH Lot # NaOH_00005

Sodium Hydroxide Reagent ID Number 0.25N_NaOH_00015

Pyridine-Barbituric Acid Reagent ID Pyr_BarbAcid_00022

Scrubber Solution ID NaOH_00005

Sodium Phosphate Solution ID SPMM Buffer_00044

Spectrophotometer Wavelength 578NM

Basis Basis Description

9014 Page 1 of 1

Page 361 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/17/12 00:18

173106 12/17/12 00:01

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount

MB 500-173106/1 7.3.4, 9034 250 mL 250 mL

LCS 250 mL 250 mL

500-173106/2

7.3.4, 9034

500-53315-G-6 FC EB 4 7.3.4, 9034 T 250 mL 250 mL

Batch Notes

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 362 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/17/12 01:25

173107 12/17/12 00:19

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount WSTSF1 00036

MB 250 mL 5 mL 4.89 mL OK 250 mL

500-173106/1-A

9034

LCS 250 mL 5 mL 2.73 mL OK 250 mL 5 mL

500-173106/2-A

9034

500-53315-G-6-A FC EB 4 9034 T 250 mL 5 mL 5.25 mL OK 250 mL

Batch Notes

Normality of Iodine Solution 0.0237 N

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 363 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 11:15

173290 12/19/12 10:05

Batch Method:

TestAmerica Chicago

7.3.4

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-173290/1 7.3.4, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-173290/2

7.3.4, 9034

500-53315-A-1 FC COMPOSITE 4 7.3.4, 9034 T 10.2894 g 10 mL

500-53315-A-2 FC D COMPOSITE 4 7.3.4, 9034 T 10.1413 g 10 mL

Batch Notes

Batch Comment Balance ID # 2489

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 364 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 12:25

173472 12/19/12 12:15

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount IodineAmount TitrantVolume1 CalcMsg FinalAmount

MB 10 mL 5 mL 4.86 mL OK 10 mL

500-173290/1-A

9034

LCS 10 mL 5 mL 0.44 mL OK 10 mL

500-173290/2-A

9034

500-53315-A-1-K FC COMPOSITE 4 9034 T 10 mL 5 mL 4.72 mL OK 10 mL

500-53315-A-2-I FC D COMPOSITE 4 9034 T 10 mL 5 mL 4.68 mL OK 10 mL

Batch Notes

Normality of Iodine Solution 0.0232 N

Nominal Amount Used 10 g

Perform Calculation (0=No, 1=Yes) 1

Normality of first Titrant 0.0246 N

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 365 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Wasowicz, Andrew P

12/19/12 18:40

173558 12/19/12 14:45

Batch Method:

TestAmerica Chicago

1010

Lab Sample ID Client Sample ID Method Chain Basis AnalysisComment

500-53315-A-1 FC COMPOSITE 4 1010 T gray-brown clay

500-53315-A-2 FC D COMPOSITE 4 1010 T gray-brown clay

Batch Notes

Equipment ID HFP 339

Basis Basis Description

T Total/NA

1010 Page 1 of 1

Page 366 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/18/12 09:35

173173 12/18/12 05:25

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis GrossWeight TareWeight InitialAmount FinalAmount

MB 500-173173/1 1664A, 1664A 1390 g 390 g 1000 mL 1000 mL

LCS 1390 g 390 g 1000 mL 1000 mL

500-173173/2

1664A, 1664A

500-53315-H-6 FC EB 4 1664A, 1664A T 1351 g 390 g 961 mL 1000 mL

Batch Notes

Batch Comment phase separating filter lot # 6711653

Concentration End Time See end date/time

Concentration Start Time See start date/time

Person's name who did the concentration See analyst name

Disk Lot Number 47mm-1507111, pf-70610210; 90mm-150381, 

pf-70610210

Evaporator Temperature 50 DEG. Degrees C

Extraction Analyst see analyst name

Sulfuric Acid Lot Number MALG35029

Hexane Lot# HEXANES_00012

Manifold ID 1851

Methanol Lot Number Methanol_00007

Na2SO4 Lot Number Na2SO4_00006

Nominal Amount Used 1000 mL

Sufficient volume for MS/MSD? NO

Basis Basis Description

T Total/NA

1664A Page 1 of 1

Page 367 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/18/12 12:30

173178 12/18/12 10:05

Batch Method:

TestAmerica Chicago

1664A

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 1000 mL 1000 mL 01 2.3690 g 2.3699 g 2.3701 g

500-173173/1-A

1664A

LCS 1000 mL 1000 mL 02 6.2581 g 6.2973 g 6.2972 g

500-173173/2-A

1664A

500-53315-H-6-A FC EB 4 1664A T 1000 mL 1000 mL 12 2.3493 g 2.3497 g 2.3496 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2 1664 HEM 00060

Pass_0.0005g 0.0008999999999

99679 g

0.0010999999999

9966 g

MB 

500-173173/1-A

1664A

Pass_0.0005g 0.0392000000000

001 g

0.0391000000000

004 g

LCS 5 mL

500-173173/2-A

1664A

FC EB 4 Pass_0.0005g 0.0003999999999

99956 g

0.0003000000000

00189 g

500-53315-H-6-A 1664A T

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0021 / 1.0000 g

Calibration Check Before 1st Weighing 0.0020 / 0.9999 g

Person's name who did the concentration see analyst name

Evaporator Temperature 50 Degrees C

Hexane Lot# Hexanes_00012

Methanol Lot Number Methanol_00006

Na2SO4 Lot Number Na2SO4_00006

Silica Gel Lot Number Silica gel_00003 (checked in batch 157954 

7/31/12)

Speedvap ID# 1563

Weight Set ID C-2495, C-1144

Basis Basis Description

T Total/NA

1664A Page 1 of 1

Page 368 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Boyd, Cheryl L

12/17/12 01:25

173108 12/17/12 00:19

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis TitrantVolume1 IodineAmount InitialAmount FinalAmount CalcMsg WSTSF1 00036

MB 500-173108/1 9034 4.89 mL 5 mL 250 mL 250 mL OK

LCS 2.73 mL 5 mL 250 mL 250 mL OK 5 mL

500-173108/2

9034

500-53315-G-6 FC EB 4 9034 T 5.25 mL 5 mL 250 mL 250 mL OK

Batch Notes

First End time 01:25

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0237 N

Sodium Thiosulfate Lot Number NO2S2O300008

Sodium Thiosulfate Vendor INHOUSE

Nominal Amount Used 250 mL

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

First Start time 00:19

Sulfuric Acid Reagent ID Number 6NHCL00006

Normality of first Titrant 0.0246 N

Titrant Standardization Date 11/21/12

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 369 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 12:55

173291 12/19/12 11:25

Batch Method:

TestAmerica Chicago

9030B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount WSTSF1 00036

MB 500-173291/1 9030B, 9034 10.0000 g 10 mL

LCS 10.0000 g 10 mL 10 mL

500-173291/2

9030B, 9034

500-53315-A-1 FC COMPOSITE 4 9030B, 9034 T 10.3275 g 10 mL

500-53315-A-2 FC D COMPOSITE 4 9030B, 9034 T 10.4669 g 10 mL

Batch Notes

Batch Comment BAlance ID #2489

Distillation Temperature 70 Degrees C

Sodium Hydroxide Reagent ID Number 0.25N NaOH_00014

Sulfuric Acid Reagent ID Number 20% H2SO4_00003

Zinc Acetate Buffer Reagent ID Number 0.5M ZnAcetate_00005

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 370 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Moore, Colleen L

12/19/12 13:40

173474 12/19/12 13:35

Batch Method:

TestAmerica Chicago

9034

Lab Sample ID Client Sample ID Method Chain Basis FinalAmount IodineAmount TitrantVolume1 CalcMsg

MB 10 mL 5 mL 4.65 mL OK

500-173291/1-A

9034

LCS 10 mL 5 mL 0.44 mL OK

500-173291/2-A

9034

500-53315-A-1-L FC COMPOSITE 4 9034 T 10 mL 10 mL 4.40 mL OK

500-53315-A-2-J FC D COMPOSITE 4 9034 T 10 mL 10 mL 4.02 mL OK

Batch Notes

HCl Concentration 6N

Lot # of hydrochloric acid 6NHCL00006

Iodine Lot Number 0.25NIODINE00005

Iodine Vendor INHOUSE

Normality of Iodine Solution 0.0232 N

Sodium Thiosulfate Reagent ID Number NO2S2O300008

Perform Calculation (0=No, 1=Yes) 1

Starch Lot Number STARCHIND00004

Starch Vendor VWR

Normality of first Titrant 0.0246 N

Zinc Acetate Buffer Reagent ID Number 0.5MZNACETAT00005

Basis Basis Description

T Total/NA

9034 Page 1 of 1

Page 371 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/19/12 07:35

173324 12/19/12 05:10

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount 1664 HEM 00060

MB 500-173324/1 9071B, 9071B 10 g 10 mL

LCS 10 g 10 mL 5 mL

500-173324/2

9071B, 9071B

500-53315-A-1 FC COMPOSITE 4 9071B, 9071B T 10.2484 g 10 mL

500-53315-A-2 FC D COMPOSITE 4 9071B, 9071B T 10.4122 g 10 mL

Batch Notes

Acid used for pH adjust Lot # J23A13

Balance ID 1634

Concentration End Time See end date / time

Concentration Start Time See start date / time

Evaporator Temperature 50 DEG. C

Filter Paper Lot Number 6711653

Hexane Lot# HEXANES_00012

Na2SO4 Lot Number Na2SO4_00006

Basis Basis Description

T Total/NA

9071B Page 1 of 1

Page 372 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

Brogan, Mary T

12/19/12 11:35

173330 12/19/12 09:20

Batch Method:

TestAmerica Chicago

9071B

Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RECTUBE# ReceiverTube RecTubeWExtract

1

RecTubeWExtract

2

MB 10 mL 10 mL 24 2.3781 g 2.3790 g 2.3791 g

500-173324/1-A

9071B

LCS 10 mL 10 mL 25 2.3332 g 2.3745 g 2.3741 g

500-173324/2-A

9071B

500-53315-A-1-M FC COMPOSITE 4 9071B T 10 mL 10 mL 33 2.2879 g 2.3174 g 2.3174 g

500-53315-A-2-K FC D COMPOSITE 4 9071B T 10 mL 10 mL 34 2.3277 g 2.3522 g 2.3521 g

Lab Sample ID Client Sample ID Method Chain Basis WeightOne%Diff Residue Residue2

Pass_0.0005g 0.0009000000000

00123 g

0.0010000000000

0033 g

MB 

500-173324/1-A

9071B

Pass_0.0005g 0.0412999999999

997 g

0.0408999999999

997 g

LCS 

500-173324/2-A

9071B

FC COMPOSITE 4 Pass_0.0005g 0.0295000000000

001 g

0.0295000000000

001 g

500-53315-A-1-M 9071B T

FC D COMPOSITE 4 Pass_0.0005g 0.0244999999999

997 g

500-53315-A-2-K 9071B T 0.0244 g

Batch Notes

Balance ID 1634

Calibration Check After 2nd Weighing 0.0019 / 0.9999

Calibration Check Before 1st Weighing 0.0019 / 0.9999

Evaporator Temperature 50 Celsius

Filter Paper Lot # 6711653

Basis Basis Description

T Total/NA

9071B Page 1 of 1

Page 373 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173077 12/15/12 12:43 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53315-A-1 FC COMPOSITE 4 Moisture T 13 33.86 g 44.15 g 36.53 g

500-53315-A-2 FC D COMPOSITE 4 Moisture T 14 41.36 g 51.51 g 44.03 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/15/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 1300

Date samples were removed from oven 12/17/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 1450

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

Moisture Page 1 of 1

Page 374 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173311 12/18/12 12:44 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

Moisture

Lab Sample ID Client Sample ID Method Chain Basis DISH# DishWeight SampleMassWet SampleMassDry

500-53315-A-3 FC DISCRETE 4 Moisture T 39 1.27 g 11.43 g 4.21 g

500-53315-A-4 FC D DISCRETE 4 Moisture T 40 1.27 g 11.57 g 4.17 g

Batch Notes

Balance ID 971 No Unit

Date samples were placed in the oven 12/18/12

Oven Temp when samples are put in oven 105 Degrees C

Time samples were place in the oven 1330

Date samples were removed from oven 12/19/12

Oven Temp when samples removed from oven 105 Degrees C

Time Samples were removed from oven 0700

Oven ID 776

ID number of the thermometer c-1966

Basis Basis Description

T Total/NA

Moisture Page 1 of 1

Page 375 of 383 01/03/2013
Lab Name: Job No.:

SDG No.:

GENERAL CHEMISTRY BATCH WORKSHEET

500-53315-1

Batch Number: Batch Start Date: Batch Analyst:

Batch End Date:

173236 12/18/12 07:34 Veldhuizen, Chris M

Batch Method:

TestAmerica Chicago

SM 2540G

Lab Sample ID Client Sample ID Method Chain Basis CalcMsg

FC COMPOSITE 4 Not Calculated. 

RunCalculation 

is NULL

500-53315-A-1 SM 2540G T

FC D COMPOSITE 4 Not Calculated. 

RunCalculation 

is NULL

500-53315-A-2 SM 2540G T

Batch Notes

Basis Basis Description

T Total/NA

SM 2540G Page 1 of 1

Page 376 of 383 01/03/2013






Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53315-1

Login Number: 53315

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True 2.7

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

TestAmerica Chicago Page 383 of 383 01/03/2013
ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Chicago

2417 Bond Street

University Park, IL 60484

Tel: (708)534-5200

TestAmerica Job ID: 500-53315-1

Client Project/Site: John Deere Des Moines Works (JDDMW)

For:

Project Integration, Inc

1097 Highway 101 South

Suite D-16

Greer, South Carolina 29651

Attn: Mr. Robert Stevens

Authorized for release by:

1/3/2013 4:42:16 PM

Donna Ingersoll

Project Manager II

donna.ingersoll@testamericainc.com

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited

parameters, exceptions are noted in this report. This report may not be reproduced except in full,

and with written approval from the laboratory. For questions please contact the Project Manager

at the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature is

intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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5

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15
Table of Contents

Client: Project Integration, Inc

Project/Site: John Deere Des Moines Works (JDDMW)

TestAmerica Job ID: 500-53315-1

Page 2 of 37

TestAmerica Chicago

1/3/2013

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

1

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3

4

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Case Narrative

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Job ID: 500-53315-1

Laboratory: TestAmerica Chicago

Narrative

Job Narrative

500-53315-1

Comments

No additional comments. 

Receipt 

The samples were received on 12/15/2012 9:10 AM; the samples arrived in good condition, properly preserved and, where required, on 

ice. The temperature of the cooler at receipt was 2.7o C.

GC/MS VOA 

Method(s) 8260B: Due to the high concentration of Acetone, the matrix spike / matrix spike duplicate (3MS/3MSD) for sample -3 could not 

be evaluated for accuracy and precision. The associated laboratory control sample (LCS) met acceptance criteria.

Method(s) 8260B: One internal standard response was outside of acceptance limits for the following samples:FC D DISCRETE 4 

(500-53315-4), FC DISCRETE 4 (500-53315-3). The samples were re-analyzed at a dilution for Acetone. All internal standard area 

responses were within limits in the diluted runs. Both sets of data have been provided.

No other analytical or quality issues were noted.

Metals 

Method(s) 6010B: The serial dilution performed for the following sample, 500-53315-1, was outside control limits for Ci,Ni,Pb,V-, and Zn.

Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for sample 500-53315-1 were outside control limits for 

Zn. The associated laboratory control sample (LCS) recovery met acceptance criteria.

Method(s) 7470A: The matrix spike duplicate (MSD) recovery for sample 500-53315-6 was outside control limits for Hg. The associated 

laboratory control sample (LCS) recovery met acceptance criteria.

No other analytical or quality issues were noted.

General Chemistry 

No analytical or quality issues were noted.

TestAmerica Chicago Page 3 of 37 1/3/2013

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Detection Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC COMPOSITE 4 Lab Sample ID: 500-53315-1

Barium ☼

RL

3.70 mg/Kg

MDL

0.441

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

346 1 6010B Total/NA

Copper 834 3.70 1.00 mg/Kg 1 ☼ 6010B Total/NA

Chromium 14400 V 3.70 0.618 mg/Kg 1 ☼ 6010B Total/NA

Nickel 89.8 V 3.70 0.811 mg/Kg 1 ☼ 6010B Total/NA

Lead 209 B V 1.85 0.637 mg/Kg 1 ☼ 6010B Total/NA

Vanadium 241 V 1.85 0.281 mg/Kg 1 ☼ 6010B Total/NA

Zinc 481 V 7.41 2.54 mg/Kg 1 ☼ 6010B Total/NA

Barium 0.0194 J 0.500 0.0100 mg/L 1 6010B TCLP

Copper 0.0487 0.0250 0.0100 mg/L 1 6010B TCLP

Nickel 0.0549 0.0250 0.0100 mg/L 1 6010B TCLP

Mercury 0.543 0.0595 0.0227 mg/Kg 1 ☼ 7471A Total/NA

Flashpoint >176 40.0 40.0 Degrees F 1 1010 Total/NA

Chromium, hexavalent 3.97 3.85 1.50 mg/Kg 1 ☼ 7196A Total/NA

Cyanide, Total 0.745 J B 1.91 0.630 mg/Kg 1 ☼ 9014 Total/NA

Sulfide 739 93.3 14.9 mg/Kg 1 ☼ 9034 Total/NA

pH 9.50 0.200 0.200 SU 1 9045C Total/NA

HEM (Oil & Grease) 11100 1880 835 mg/Kg 1 ☼ 9071B Total/NA

Total Solids 26.0 0.100 0.100 % 1 SM 2540G Total/NA

Client Sample ID: FC D COMPOSITE 4 Lab Sample ID: 500-53315-2

Barium ☼

RL

3.46 mg/Kg

MDL

0.411

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

326 1 6010B Total/NA

Copper 784 3.46 0.937 mg/Kg 1 ☼ 6010B Total/NA

Chromium 13200 3.46 0.577 mg/Kg 1 ☼ 6010B Total/NA

Nickel 86.4 3.46 0.757 mg/Kg 1 ☼ 6010B Total/NA

Lead 188 B 1.73 0.595 mg/Kg 1 ☼ 6010B Total/NA

Vanadium 221 1.73 0.262 mg/Kg 1 ☼ 6010B Total/NA

Zinc 451 6.92 2.37 mg/Kg 1 ☼ 6010B Total/NA

Copper 0.0483 0.0250 0.0100 mg/L 1 6010B TCLP

Chromium 0.0120 J 0.0250 0.0100 mg/L 1 6010B TCLP

Nickel 0.0582 0.0250 0.0100 mg/L 1 6010B TCLP

Mercury 0.248 0.0628 0.0239 mg/Kg 1 ☼ 7471A Total/NA

Flashpoint >176 40.0 40.0 Degrees F 1 1010 Total/NA

Chromium, hexavalent 4.08 3.76 1.46 mg/Kg 1 ☼ 7196A Total/NA

Cyanide, Total 0.765 J B 1.66 0.549 mg/Kg 1 ☼ 9014 Total/NA

Sulfide 774 90.8 14.5 mg/Kg 1 ☼ 9034 Total/NA

pH 9.58 0.200 0.200 SU 1 9045C Total/NA

HEM (Oil & Grease) 8910 1830 811 mg/Kg 1 ☼ 9071B Total/NA

Total Solids 26.0 0.100 0.100 % 1 SM 2540G Total/NA

Client Sample ID: FC DISCRETE 4 Lab Sample ID: 500-53315-3

2-Butanone (MEK) ☼

RL

17.3 ug/Kg

MDL

6.25

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

145 1 8260B Total/NA

Acetone - DL 4220 864 225 ug/Kg 50 ☼ 8260B Total/NA

Client Sample ID: FC D DISCRETE 4 Lab Sample ID: 500-53315-4

2-Butanone (MEK) ☼

RL

17.8 ug/Kg

MDL

6.43

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

191 1 8260B Total/NA

Acetone - DL 8710 888 231 ug/Kg 50 ☼ 8260B Total/NA

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Detection Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: TRIP BLANK Lab Sample ID: 500-53315-5

 No Detections

Client Sample ID: FC EB 4 Lab Sample ID: 500-53315-6

2-Butanone (MEK)

RL

5.00 ug/L

MDL

1.47

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

13.0 1 8260B Total/NA

Barium 0.000580 J B 0.0100 0.000440 mg/L 1 6010B Total/NA

Copper 0.00303 J 0.0100 0.00106 mg/L 1 6010B Total/NA

Chromium 0.00312 J B 0.0100 0.000960 mg/L 1 6010B Total/NA

Lead 0.00214 J B 0.00500 0.00158 mg/L 1 6010B Total/NA

Zinc 0.00724 J 0.0200 0.00472 mg/L 1 6010B Total/NA

Mercury 0.000102 J 0.000200 0.0000710 mg/L 1 7470A Total/NA

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Method Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method Method Description Protocol Laboratory

8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI

6010B Metals (ICP) SW846 TAL CHI

7470A Mercury (CVAA) SW846 TAL CHI

7471A Mercury (CVAA) SW846 TAL CHI

1010 Ignitability, Pensky-Martens Closed-Cup Method SW846 TAL CHI

1664A HEM and SGT-HEM 1664A TAL CHI

7196A Chromium, Hexavalent SW846 TAL CHI

9014 Cyanide SW846 TAL CHI

9034 Sulfide, Reactive SW846 TAL CHI

9034 Sulfide, Acid soluble and Insoluble (Titrimetric) SW846 TAL CHI

9045C pH SW846 TAL CHI

9071B HEM and SGT-HEM SW846 TAL CHI

Moisture Percent Moisture EPA TAL CHI

SM 2540G Total, Fixed, and Volatile Solids SM TAL CHI

Protocol References:

1664A = EPA-821-98-002

EPA = US Environmental Protection Agency

SM = "Standard Methods For The Examination Of Water And Wastewater",

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

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Sample Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Lab Sample ID Client Sample ID Matrix Collected Received

500-53315-1 FC COMPOSITE 4 Solid 12/14/12 15:15 12/15/12 09:10

500-53315-2 FC D COMPOSITE 4 Solid 12/14/12 15:15 12/15/12 09:10

500-53315-3 FC DISCRETE 4 Solid 12/14/12 14:45 12/15/12 09:10

500-53315-4 FC D DISCRETE 4 Solid 12/14/12 14:45 12/15/12 09:10

500-53315-5 TRIP BLANK Water 12/14/12 00:00 12/15/12 09:10

500-53315-6 FC EB 4 Water 12/14/12 14:30 12/15/12 09:10

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC COMPOSITE 4 Lab Sample ID: 500-53315-1

Date Collected: 12/14/12 15:15 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 25.9

Method: 6010B - Metals (ICP)

RL MDL

Barium 346 3.70 0.441 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 834 3.70 1.00 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Chromium 14400 V 3.70 0.618 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Nickel 89.8 V 3.70 0.811 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Lead 209 B V 1.85 0.637 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Vanadium 241 V 1.85 0.281 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Zinc 481 V 7.41 2.54 mg/Kg ☼ 12/17/12 08:50 12/17/12 22:46 1

Method: 6010B - Metals (ICP) - TCLP

RL MDL

Barium 0.0194 J 0.500 0.0100 mg/L 12/19/12 08:20 12/19/12 22:29 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.0487 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:29 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:29 1

Nickel 0.0549 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:29 1

Lead <0.0500 0.0500 0.00500 mg/L 12/19/12 08:20 12/19/12 22:29 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/19/12 08:20 12/19/12 22:29 1

Zinc <0.100 0.100 0.0200 mg/L 12/19/12 08:20 12/19/12 22:29 1

Method: 7470A - Mercury (CVAA) - TCLP

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/18/12 13:00 12/19/12 10:24 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.543 0.0595 0.0227 mg/Kg ☼ 12/17/12 14:00 12/18/12 14:00 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

Flashpoint >176 40.0 40.0 Degrees F 12/19/12 17:21 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent 3.97 3.85 1.50 mg/Kg ☼ 12/18/12 10:00 12/18/12 15:49 1

Cyanide, Total 0.745 J B 1.91 0.630 mg/Kg ☼ 12/18/12 10:35 12/18/12 14:24 1

Sulfide 739 93.3 14.9 mg/Kg ☼ 12/19/12 11:25 12/19/12 13:36 1

Sulfide, Reactive <48.6 48.6 3.79 mg/Kg 12/19/12 10:40 12/19/12 12:18 1

pH 9.50 0.200 0.200 SU 12/20/12 15:12 1

HEM (Oil & Grease) 11100 1880 835 mg/Kg ☼ 12/19/12 05:10 12/19/12 11:01 1

Total Solids 26.0 0.100 0.100 % 12/18/12 07:34 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D COMPOSITE 4 Lab Sample ID: 500-53315-2

Date Collected: 12/14/12 15:15 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 26.3

Method: 6010B - Metals (ICP)

RL MDL

Barium 326 3.46 0.411 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 784 3.46 0.937 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Chromium 13200 3.46 0.577 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Nickel 86.4 3.46 0.757 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Lead 188 B 1.73 0.595 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Vanadium 221 1.73 0.262 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Zinc 451 6.92 2.37 mg/Kg ☼ 12/17/12 08:50 12/17/12 23:17 1

Method: 6010B - Metals (ICP) - TCLP

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/19/12 08:20 12/19/12 22:35 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.0483 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:35 1

Chromium 0.0120 J 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:35 1

Nickel 0.0582 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 22:35 1

Lead <0.0500 0.0500 0.00500 mg/L 12/19/12 08:20 12/19/12 22:35 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/19/12 08:20 12/19/12 22:35 1

Zinc <0.100 0.100 0.0200 mg/L 12/19/12 08:20 12/19/12 22:35 1

Method: 7470A - Mercury (CVAA) - TCLP

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/18/12 13:00 12/19/12 10:29 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

RL MDL

Mercury 0.248 0.0628 0.0239 mg/Kg ☼ 12/17/12 14:00 12/18/12 14:01 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

Flashpoint >176 40.0 40.0 Degrees F 12/19/12 18:00 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent 4.08 3.76 1.46 mg/Kg ☼ 12/18/12 10:00 12/18/12 15:50 1

Cyanide, Total 0.765 J B 1.66 0.549 mg/Kg ☼ 12/18/12 10:35 12/18/12 14:24 1

Sulfide 774 90.8 14.5 mg/Kg ☼ 12/19/12 11:25 12/19/12 13:37 1

Sulfide, Reactive <49.3 49.3 3.85 mg/Kg 12/19/12 10:45 12/19/12 12:19 1

pH 9.58 0.200 0.200 SU 12/20/12 16:11 1

HEM (Oil & Grease) 8910 1830 811 mg/Kg ☼ 12/19/12 05:10 12/19/12 11:12 1

Total Solids 26.0 0.100 0.100 % 12/18/12 07:34 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC DISCRETE 4 Lab Sample ID: 500-53315-3

Date Collected: 12/14/12 14:45 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 28.9

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

2-Butanone (MEK) 145 17.3 6.25 ug/Kg ☼ 12/18/12 09:30 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 116 70 - 134 12/18/12 09:30 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 98 75 - 122 12/18/12 09:30 1

4-Bromofluorobenzene (Surr) 91 70 - 122 12/18/12 09:30 1

Dibromofluoromethane 113 75 - 120 12/18/12 09:30 1

Method: 8260B - Volatile Organic Compounds (GC/MS) - DL

RL MDL

Acetone 4220 864 225 ug/Kg ☼ 12/18/12 07:45 12/20/12 02:16 50

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 109 75 - 125 12/18/12 07:45 12/20/12 02:16 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 97 75 - 120 12/18/12 07:45 12/20/12 02:16 50

4-Bromofluorobenzene (Surr) 91 75 - 120 12/18/12 07:45 12/20/12 02:16 50

Dibromofluoromethane 105 75 - 120 12/18/12 07:45 12/20/12 02:16 50

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D DISCRETE 4 Lab Sample ID: 500-53315-4

Date Collected: 12/14/12 14:45 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 28.2

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

2-Butanone (MEK) 191 17.8 6.43 ug/Kg ☼ 12/18/12 10:40 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 117 70 - 134 12/18/12 10:40 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 97 75 - 122 12/18/12 10:40 1

4-Bromofluorobenzene (Surr) 85 70 - 122 12/18/12 10:40 1

Dibromofluoromethane 112 75 - 120 12/18/12 10:40 1

Method: 8260B - Volatile Organic Compounds (GC/MS) - DL

RL MDL

Acetone 8710 888 231 ug/Kg ☼ 12/18/12 07:45 12/20/12 02:40 50

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

1,2-Dichloroethane-d4 (Surr) 119 75 - 125 12/18/12 07:45 12/20/12 02:40 50

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 93 75 - 120 12/18/12 07:45 12/20/12 02:40 50

4-Bromofluorobenzene (Surr) 90 75 - 120 12/18/12 07:45 12/20/12 02:40 50

Dibromofluoromethane 116 75 - 120 12/18/12 07:45 12/20/12 02:40 50

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: TRIP BLANK Lab Sample ID: 500-53315-5

Date Collected: 12/14/12 00:00 Matrix: Water

Date Received: 12/15/12 09:10

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/20/12 01:08 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/20/12 01:08 1

1,2-Dichloroethane-d4 (Surr) 105 75 - 125 12/20/12 01:08 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 100 75 - 120 12/20/12 01:08 1

4-Bromofluorobenzene (Surr) 97 75 - 120 12/20/12 01:08 1

Dibromofluoromethane 109 75 - 120 12/20/12 01:08 1

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Client Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC EB 4 Lab Sample ID: 500-53315-6

Date Collected: 12/14/12 14:30 Matrix: Water

Date Received: 12/15/12 09:10

Method: 8260B - Volatile Organic Compounds (GC/MS)

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/20/12 01:49 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) 13.0 5.00 1.47 ug/L 12/20/12 01:49 1

1,2-Dichloroethane-d4 (Surr) 107 75 - 125 12/20/12 01:49 1

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 99 75 - 120 12/20/12 01:49 1

4-Bromofluorobenzene (Surr) 94 75 - 120 12/20/12 01:49 1

Dibromofluoromethane 107 75 - 120 12/20/12 01:49 1

Method: 6010B - Metals (ICP)

RL MDL

Barium 0.000580 J B 0.0100 0.000440 mg/L 12/18/12 15:30 12/19/12 14:57 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper 0.00303 J 0.0100 0.00106 mg/L 12/18/12 15:30 12/19/12 14:57 1

Chromium 0.00312 J B 0.0100 0.000960 mg/L 12/18/12 15:30 12/19/12 14:57 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/18/12 15:30 12/19/12 14:57 1

Lead 0.00214 J B 0.00500 0.00158 mg/L 12/18/12 15:30 12/19/12 14:57 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/18/12 15:30 12/19/12 14:57 1

Zinc 0.00724 J 0.0200 0.00472 mg/L 12/18/12 15:30 12/19/12 14:57 1

Method: 7470A - Mercury (CVAA)

RL MDL

Mercury 0.000102 J 0.000200 0.0000710 mg/L 12/17/12 13:00 12/18/12 09:49 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

General Chemistry

RL MDL

HEM (Oil & Grease) <5.20 5.20 1.51 mg/L 12/18/12 07:24 12/18/12 11:14 1

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/15/12 13:22 1

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/18/12 08:30 12/18/12 13:54 1

Sulfide <1.00 1.00 0.230 mg/L 12/17/12 01:11 1

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/17/12 00:13 12/17/12 01:08 1

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Definitions/Glossary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Qualifiers

GC/MS VOA

Qualifier Description

4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not 

applicable.

Qualifier

E Result exceeded calibration range.

Metals

Qualifier Description

V Serial Dilution exceeds the control limits

Qualifier

B Compound was found in the blank and sample.

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not 

applicable.

F MS or MSD exceeds the control limits

General Chemistry

Qualifier Description

B Compound was found in the blank and sample.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Glossary

These commonly used abbreviations may or may not be present in this report.

☼ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

DL, RA, RE, IN Indicates a Dilution, Reanalysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

EDL Estimated Detection Limit

EPA United States Environmental Protection Agency

MDA Minimum detectable activity

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

GC/MS VOA

Analysis Batch: 173225

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-3 FC DISCRETE 4 Total/NA Solid 8260B

500-53315-3 MS FC DISCRETE 4 Total/NA Solid 8260B

500-53315-3 MSD FC DISCRETE 4 Total/NA Solid 8260B

500-53315-4 FC D DISCRETE 4 Total/NA Solid 8260B

LCS 500-173225/5 Lab Control Sample Total/NA Solid 8260B

MB 500-173225/4 Method Blank Total/NA Solid 8260B

Prep Batch: 173238

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-3 - DL FC DISCRETE 4 Total/NA Solid 5030B

500-53315-4 - DL FC D DISCRETE 4 Total/NA Solid 5030B

Analysis Batch: 173508

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-5 TRIP BLANK Total/NA Water 8260B

500-53315-6 FC EB 4 Total/NA Water 8260B

LCS 500-173508/4 Lab Control Sample Total/NA Water 8260B

MB 500-173508/6 Method Blank Total/NA Water 8260B

Analysis Batch: 173509

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-3 - DL FC DISCRETE 4 Total/NA Solid 8260B 173238

500-53315-4 - DL FC D DISCRETE 4 Total/NA Solid 8260B 173238

LCS 500-173509/4 Lab Control Sample Total/NA Solid 8260B

MB 500-173509/6 Method Blank Total/NA Solid 8260B

Metals

Prep Batch: 173139

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 3050B

500-53315-1 DU FC COMPOSITE 4 Total/NA Solid 3050B

500-53315-1 MS FC COMPOSITE 4 Total/NA Solid 3050B

500-53315-1 MSD FC COMPOSITE 4 Total/NA Solid 3050B

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 3050B

LCS 500-173139/2-A Lab Control Sample Total/NA Solid 3050B

MB 500-173139/1-A Method Blank Total/NA Solid 3050B

Prep Batch: 173153

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 7471A

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 7471A

LCS 500-173153/8-A Lab Control Sample Total/NA Solid 7471A

MB 500-173153/7-A Method Blank Total/NA Solid 7471A

Prep Batch: 173172

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 7470A

500-53315-6 DU FC EB 4 Total/NA Water 7470A

500-53315-6 MS FC EB 4 Total/NA Water 7470A

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Metals (Continued)

Prep Batch: 173172 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 MSD FC EB 4 Total/NA Water 7470A

LCS 500-173172/8-A Lab Control Sample Total/NA Water 7470A

MB 500-173172/7-A Method Blank Total/NA Water 7470A

Leach Batch: 173187

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 TCLP Solid 1311

500-53315-2 FC D COMPOSITE 4 TCLP Solid 1311

LB 500-173187/1-B LB Method Blank TCLP Solid 1311

LB 500-173187/1-D LB Method Blank TCLP Solid 1311

Analysis Batch: 173224

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 6010B 173139

500-53315-1 DU FC COMPOSITE 4 Total/NA Solid 6010B 173139

500-53315-1 MS FC COMPOSITE 4 Total/NA Solid 6010B 173139

500-53315-1 MSD FC COMPOSITE 4 Total/NA Solid 6010B 173139

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 6010B 173139

LCS 500-173139/2-A Lab Control Sample Total/NA Solid 6010B 173139

MB 500-173139/1-A Method Blank Total/NA Solid 6010B 173139

Prep Batch: 173264

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 TCLP Solid 7470A 173187

500-53315-2 FC D COMPOSITE 4 TCLP Solid 7470A 173187

LB 500-173187/1-B LB Method Blank TCLP Solid 7470A 173187

LCS 500-173264/8-A Lab Control Sample Total/NA Solid 7470A

MB 500-173264/7-A Method Blank Total/NA Solid 7470A

Analysis Batch: 173280

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 7470A 173172

500-53315-6 DU FC EB 4 Total/NA Water 7470A 173172

500-53315-6 MS FC EB 4 Total/NA Water 7470A 173172

500-53315-6 MSD FC EB 4 Total/NA Water 7470A 173172

LCS 500-173172/8-A Lab Control Sample Total/NA Water 7470A 173172

MB 500-173172/7-A Method Blank Total/NA Water 7470A 173172

Analysis Batch: 173328

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 7471A 173153

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 7471A 173153

LCS 500-173153/8-A Lab Control Sample Total/NA Solid 7471A 173153

MB 500-173153/7-A Method Blank Total/NA Solid 7471A 173153

Prep Batch: 173349

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 3010A

LCS 500-173349/2-A Lab Control Sample Total/NA Water 3010A

MB 500-173349/1-A Method Blank Total/NA Water 3010A

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Metals (Continued)

Prep Batch: 173406

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 TCLP Solid 3010A 173187

500-53315-2 FC D COMPOSITE 4 TCLP Solid 3010A 173187

LB 500-173187/1-D LB Method Blank TCLP Solid 3010A 173187

LCS 500-173406/3-A Lab Control Sample Total/NA Solid 3010A

Analysis Batch: 173438

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 TCLP Solid 7470A 173264

500-53315-2 FC D COMPOSITE 4 TCLP Solid 7470A 173264

LB 500-173187/1-B LB Method Blank TCLP Solid 7470A 173264

LCS 500-173264/8-A Lab Control Sample Total/NA Solid 7470A 173264

MB 500-173264/7-A Method Blank Total/NA Solid 7470A 173264

Analysis Batch: 173517

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 6010B 173349

LCS 500-173349/2-A Lab Control Sample Total/NA Water 6010B 173349

MB 500-173349/1-A Method Blank Total/NA Water 6010B 173349

Analysis Batch: 173518

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 TCLP Solid 6010B 173406

500-53315-2 FC D COMPOSITE 4 TCLP Solid 6010B 173406

LB 500-173187/1-D LB Method Blank TCLP Solid 6010B 173406

LCS 500-173406/3-A Lab Control Sample Total/NA Solid 6010B 173406

General Chemistry

Analysis Batch: 173077

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid Moisture

500-53315-2 FC D COMPOSITE 4 Total/NA Solid Moisture

Analysis Batch: 173079

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 7196A

500-53315-6 MS FC EB 4 Total/NA Water 7196A

500-53315-6 MSD FC EB 4 Total/NA Water 7196A

LCS 500-173079/4 Lab Control Sample Total/NA Water 7196A

MB 500-173079/3 Method Blank Total/NA Water 7196A

Prep Batch: 173106

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 7.3.4

LCS 500-173106/2-A Lab Control Sample Total/NA Water 7.3.4

MB 500-173106/1-A Method Blank Total/NA Water 7.3.4

Analysis Batch: 173107

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 9034 173106

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Analysis Batch: 173107 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LCS 500-173106/2-A Lab Control Sample Total/NA Water 9034 173106

MB 500-173106/1-A Method Blank Total/NA Water 9034 173106

Analysis Batch: 173108

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 9034

LCS 500-173108/2 Lab Control Sample Total/NA Water 9034

MB 500-173108/1 Method Blank Total/NA Water 9034

Prep Batch: 173173

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 1664A

LCS 500-173173/2-A Lab Control Sample Total/NA Water 1664A

MB 500-173173/1-A Method Blank Total/NA Water 1664A

Analysis Batch: 173178

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 1664A 173173

LCS 500-173173/2-A Lab Control Sample Total/NA Water 1664A 173173

MB 500-173173/1-A Method Blank Total/NA Water 1664A 173173

Analysis Batch: 173236

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid SM 2540G

500-53315-2 FC D COMPOSITE 4 Total/NA Solid SM 2540G

Prep Batch: 173245

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 9010B

LCS 500-173245/2-A Lab Control Sample Total/NA Water 9010B

MB 500-173245/1-A Method Blank Total/NA Water 9010B

Prep Batch: 173250

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9010B

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9010B

500-53315-2 MS FC D COMPOSITE 4 Total/NA Solid 9010B

500-53315-2 MSD FC D COMPOSITE 4 Total/NA Solid 9010B

LCS 500-173250/2-A Lab Control Sample Total/NA Solid 9010B

MB 500-173250/1-A Method Blank Total/NA Solid 9010B

Prep Batch: 173258

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 3060A

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 3060A

LCS 500-173258/2-A Lab Control Sample Total/NA Solid 3060A

LCS 500-173258/3-A Lab Control Sample Total/NA Solid 3060A

MB 500-173258/1-A Method Blank Total/NA Solid 3060A

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Prep Batch: 173290

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 7.3.4

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 7.3.4

LCS 500-173290/2-A Lab Control Sample Total/NA Solid 7.3.4

MB 500-173290/1-A Method Blank Total/NA Solid 7.3.4

Prep Batch: 173291

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9030B

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9030B

LCS 500-173291/2-A Lab Control Sample Total/NA Solid 9030B

MB 500-173291/1-A Method Blank Total/NA Solid 9030B

Analysis Batch: 173311

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-3 FC DISCRETE 4 Total/NA Solid Moisture

500-53315-4 FC D DISCRETE 4 Total/NA Solid Moisture

Prep Batch: 173324

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9071B

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9071B

LCS 500-173324/2-A Lab Control Sample Total/NA Solid 9071B

MB 500-173324/1-A Method Blank Total/NA Solid 9071B

Analysis Batch: 173330

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9071B 173324

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9071B 173324

LCS 500-173324/2-A Lab Control Sample Total/NA Solid 9071B 173324

MB 500-173324/1-A Method Blank Total/NA Solid 9071B 173324

Analysis Batch: 173341

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 7196A 173258

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 7196A 173258

LCS 500-173258/2-A Lab Control Sample Total/NA Solid 7196A 173258

LCS 500-173258/3-A Lab Control Sample Total/NA Solid 7196A 173258

MB 500-173258/1-A Method Blank Total/NA Solid 7196A 173258

Analysis Batch: 173386

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9014 173250

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9014 173250

500-53315-2 MS FC D COMPOSITE 4 Total/NA Solid 9014 173250

500-53315-2 MSD FC D COMPOSITE 4 Total/NA Solid 9014 173250

LCS 500-173250/2-A Lab Control Sample Total/NA Solid 9014 173250

MB 500-173250/1-A Method Blank Total/NA Solid 9014 173250

Analysis Batch: 173387

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-6 FC EB 4 Total/NA Water 9014 173245

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QC Association Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

General Chemistry (Continued)

Analysis Batch: 173387 (Continued)

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

LCS 500-173245/2-A Lab Control Sample Total/NA Water 9014 173245

MB 500-173245/1-A Method Blank Total/NA Water 9014 173245

Analysis Batch: 173472

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9034 173290

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9034 173290

LCS 500-173290/2-A Lab Control Sample Total/NA Solid 9034 173290

MB 500-173290/1-A Method Blank Total/NA Solid 9034 173290

Analysis Batch: 173474

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9034 173291

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9034 173291

LCS 500-173291/2-A Lab Control Sample Total/NA Solid 9034 173291

MB 500-173291/1-A Method Blank Total/NA Solid 9034 173291

Analysis Batch: 173479

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 9045C

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 9045C

Analysis Batch: 173558

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

500-53315-1 FC COMPOSITE 4 Total/NA Solid 1010

500-53315-2 FC D COMPOSITE 4 Total/NA Solid 1010

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Surrogate Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (70-134) (75-122) (70-122) (75-120)

12DCE TOL BFB DBFM

500-53315-3 116 98 91 113

Percent Surrogate Recovery (Acceptance Limits)

FC DISCRETE 4

500-53315-3 MS FC DISCRETE 4 117 95 85 118

500-53315-3 MSD FC DISCRETE 4 119 96 84 116

500-53315-4 FC D DISCRETE 4 117 97 85 112

LCS 500-173225/5 Lab Control Sample 104 111 103 105

MB 500-173225/4 Method Blank 106 113 104 106

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Solid Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE DBFM TOL BFB

500-53315-3 - DL 109 105 97 91

Percent Surrogate Recovery (Acceptance Limits)

FC DISCRETE 4

500-53315-4 - DL FC D DISCRETE 4 119 116 93 90

LCS 500-173509/4 Lab Control Sample 102 98 97 99

MB 500-173509/6 Method Blank 101 96 95 94

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

DBFM = Dibromofluoromethane

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Matrix: Water Prep Type: Total/NA

Lab Sample ID Client Sample ID (75-125) (75-120) (75-120) (75-120)

12DCE TOL BFB DBFM

500-53315-5 105 100 97 109

Percent Surrogate Recovery (Acceptance Limits)

TRIP BLANK

500-53315-6 FC EB 4 107 99 94 107

LCS 500-173508/4 Lab Control Sample 102 97 99 98

MB 500-173508/6 Method Blank 101 95 94 96

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

TOL = Toluene-d8 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS)

Lab Sample ID: MB 500-173225/4 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173225

RL MDL

Acetone <5.00 5.00 2.16 ug/Kg 12/18/12 08:30 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.81 ug/Kg 12/18/12 08:30 1

1,2-Dichloroethane-d4 (Surr) 106 70 - 134 12/18/12 08:30 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 113 75 - 122 12/18/12 08:30 1

4-Bromofluorobenzene (Surr) 104 70 - 122 12/18/12 08:30 1

Dibromofluoromethane 106 75 - 120 12/18/12 08:30 1

Lab Sample ID: LCS 500-173225/5 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173225

Acetone 50.0 45.56 ug/Kg 91 50 - 138

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 52.85 ug/Kg 106 58 - 133

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

104

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 111 75 - 122

4-Bromofluorobenzene (Surr) 103 70 - 122

Dibromofluoromethane 105 75 - 120

Lab Sample ID: 500-53315-3 MS Client Sample ID: FC DISCRETE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173225

Acetone 6940 173 7120 E 4 ug/Kg ☼ 104 50 - 138

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

2-Butanone (MEK) 145 173 329.3 ug/Kg ☼ 106 58 - 133

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

117

MS MS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 95 75 - 122

4-Bromofluorobenzene (Surr) 85 70 - 122

Dibromofluoromethane 118 75 - 120

Lab Sample ID: 500-53315-3 MSD Client Sample ID: FC DISCRETE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173225

Acetone 6940 173 7629 E 4 ug/Kg ☼ 399 50 - 138 7 30

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

2-Butanone (MEK) 145 173 303.4 ug/Kg ☼ 91 58 - 133 8 30

1,2-Dichloroethane-d4 (Surr) 70 - 134

Surrogate

119

MSD MSD

%Recovery Qualifier Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: 500-53315-3 MSD Client Sample ID: FC DISCRETE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173225

Toluene-d8 (Surr) 75 - 122

Surrogate

96

MSD MSD

%Recovery Qualifier Limits

4-Bromofluorobenzene (Surr) 84 70 - 122

Dibromofluoromethane 116 75 - 120

Lab Sample ID: MB 500-173508/6 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173508

RL MDL

Acetone <5.00 5.00 1.29 ug/L 12/20/12 00:43 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/L 12/20/12 00:43 1

1,2-Dichloroethane-d4 (Surr) 101 75 - 125 12/20/12 00:43 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 95 75 - 120 12/20/12 00:43 1

4-Bromofluorobenzene (Surr) 94 75 - 120 12/20/12 00:43 1

Dibromofluoromethane 96 75 - 120 12/20/12 00:43 1

Lab Sample ID: LCS 500-173508/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173508

Acetone 50.0 52.35 ug/L 105 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 53.39 ug/L 107 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

102

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 99 75 - 120

Dibromofluoromethane 98 75 - 120

Lab Sample ID: MB 500-173509/6 Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173509

RL MDL

Acetone <5.00 5.00 1.30 ug/Kg 12/20/12 00:43 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

2-Butanone (MEK) <5.00 5.00 1.47 ug/Kg 12/20/12 00:43 1

1,2-Dichloroethane-d4 (Surr) 101 75 - 125 12/20/12 00:43 1

MB MB

Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac

Toluene-d8 (Surr) 95 75 - 120 12/20/12 00:43 1

4-Bromofluorobenzene (Surr) 94 75 - 120 12/20/12 00:43 1

Dibromofluoromethane 96 75 - 120 12/20/12 00:43 1

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Lab Sample ID: LCS 500-173509/4 Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173509

Acetone 50.0 52.35 ug/Kg 105 46 - 153

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

2-Butanone (MEK) 50.0 53.39 ug/Kg 107 54 - 138

1,2-Dichloroethane-d4 (Surr) 75 - 125

Surrogate

102

LCS LCS

%Recovery Qualifier Limits

Toluene-d8 (Surr) 97 75 - 120

4-Bromofluorobenzene (Surr) 99 75 - 120

Dibromofluoromethane 98 75 - 120

Method: 6010B - Metals (ICP)

Lab Sample ID: MB 500-173139/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173224 Prep Batch: 173139

RL MDL

Barium <1.00 1.00 0.119 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <1.00 1.00 0.271 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

Chromium <1.00 1.00 0.167 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

Nickel <1.00 1.00 0.219 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

Lead 0.2420 J 0.500 0.172 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

Vanadium <0.500 0.500 0.0759 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

Zinc <2.00 2.00 0.686 mg/Kg 12/17/12 08:50 12/17/12 21:04 1

Lab Sample ID: LCS 500-173139/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173224 Prep Batch: 173139

Barium 200 197.2 mg/Kg 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 25.0 24.95 mg/Kg 100 80 - 120

Chromium 20.0 19.91 mg/Kg 100 80 - 120

Nickel 50.0 49.11 mg/Kg 98 80 - 120

Lead 10.0 10.07 mg/Kg 101 80 - 120

Vanadium 50.0 49.74 mg/Kg 99 80 - 120

Zinc 50.0 48.83 mg/Kg 98 80 - 120

Lab Sample ID: 500-53315-1 MS Client Sample ID: FC COMPOSITE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173224 Prep Batch: 173139

Barium 346 762 987.2 mg/Kg ☼ 84 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Copper 834 95.2 836.2 4 mg/Kg ☼ 2 75 - 125

Chromium 14400 V 76.2 13510 4 mg/Kg ☼ -1125 75 - 125

Nickel 89.8 V 190 246.8 mg/Kg ☼ 82 75 - 125

Lead 209 B V 38.1 253.1 4 mg/Kg ☼ 116 75 - 125

Vanadium 241 V 190 391.8 mg/Kg ☼ 79 75 - 125

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP) (Continued)

Lab Sample ID: 500-53315-1 MS Client Sample ID: FC COMPOSITE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173224 Prep Batch: 173139

Zinc 481 V 190 605.1 F mg/Kg ☼ 65 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53315-1 MSD Client Sample ID: FC COMPOSITE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173224 Prep Batch: 173139

Barium 346 729 943.9 mg/Kg ☼ 82 75 - 125 4 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Copper 834 91.2 799.8 4 mg/Kg ☼ -38 75 - 125 4 20

Chromium 14400 V 72.9 13220 4 mg/Kg ☼ -1577 75 - 125 2 20

Nickel 89.8 V 182 237.5 mg/Kg ☼ 81 75 - 125 4 20

Lead 209 B V 36.5 213.5 4 mg/Kg ☼ 12 75 - 125 17 20

Vanadium 241 V 182 379.3 mg/Kg ☼ 76 75 - 125 3 20

Zinc 481 V 182 600.3 F mg/Kg ☼ 65 75 - 125 1 20

Lab Sample ID: 500-53315-1 DU Client Sample ID: FC COMPOSITE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173224 Prep Batch: 173139

Barium 346 335.3 mg/Kg ☼ 3 20

Analyte

DU DU

Result Qualifier Unit D

Sample

Result

Sample

Qualifier RPD Limit

RPD

Copper 834 804.0 mg/Kg ☼ 4 20

Chromium 14400 V 13970 mg/Kg ☼ 3 20

Nickel 89.8 V 88.38 mg/Kg ☼ 2 20

Lead 209 B V 201.3 mg/Kg ☼ 4 20

Vanadium 241 V 234.5 mg/Kg ☼ 3 20

Zinc 481 V 468.4 mg/Kg ☼ 3 20

Lab Sample ID: MB 500-173349/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173349

RL MDL

Barium 0.002710 J 0.0100 0.000440 mg/L 12/18/12 15:30 12/19/12 13:52 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0100 0.0100 0.00106 mg/L 12/18/12 15:30 12/19/12 13:52 1

Chromium 0.001210 J 0.0100 0.000960 mg/L 12/18/12 15:30 12/19/12 13:52 1

Nickel <0.0100 0.0100 0.00190 mg/L 12/18/12 15:30 12/19/12 13:52 1

Lead 0.002720 J 0.00500 0.00158 mg/L 12/18/12 15:30 12/19/12 13:52 1

Vanadium <0.00500 0.00500 0.000620 mg/L 12/18/12 15:30 12/19/12 13:52 1

Zinc <0.0200 0.0200 0.00472 mg/L 12/18/12 15:30 12/19/12 13:52 1

Lab Sample ID: LCS 500-173349/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173349

Barium 2.00 1.955 mg/L 98 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2524 mg/L 101 80 - 120

Chromium 0.200 0.1989 mg/L 99 80 - 120

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 6010B - Metals (ICP) (Continued)

Lab Sample ID: LCS 500-173349/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173517 Prep Batch: 173349

Nickel 0.500 0.4934 mg/L 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lead 0.100 0.1010 mg/L 101 80 - 120

Vanadium 0.500 0.4993 mg/L 100 80 - 120

Zinc 0.500 0.4858 mg/L 97 80 - 120

Lab Sample ID: LCS 500-173406/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173518 Prep Batch: 173406

Barium 2.00 1.975 mg/L 99 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Copper 0.250 0.2464 mg/L 99 80 - 120

Chromium 0.200 0.1969 mg/L 98 80 - 120

Nickel 0.500 0.4873 mg/L 97 80 - 120

Lead 0.100 0.09785 mg/L 98 80 - 120

Vanadium 0.500 0.4959 mg/L 99 80 - 120

Zinc 0.500 0.4782 mg/L 96 80 - 120

Lab Sample ID: LB 500-173187/1-D LB Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173518 Prep Batch: 173406

RL MDL

Barium <0.500 0.500 0.0100 mg/L 12/19/12 08:20 12/19/12 21:07 1

LB LB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Copper <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 21:07 1

Chromium <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 21:07 1

Nickel <0.0250 0.0250 0.0100 mg/L 12/19/12 08:20 12/19/12 21:07 1

Lead <0.0500 0.0500 0.00500 mg/L 12/19/12 08:20 12/19/12 21:07 1

Vanadium <0.0250 0.0250 0.00500 mg/L 12/19/12 08:20 12/19/12 21:07 1

Zinc <0.100 0.100 0.0200 mg/L 12/19/12 08:20 12/19/12 21:07 1

Method: 7470A - Mercury (CVAA)

Lab Sample ID: MB 500-173172/7-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173280 Prep Batch: 173172

RL MDL

Mercury <0.000200 0.000200 0.0000710 mg/L 12/17/12 13:00 12/18/12 09:09 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173172/8-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173280 Prep Batch: 173172

Mercury 0.00200 0.002027 mg/L 101 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7470A - Mercury (CVAA) (Continued)

Lab Sample ID: 500-53315-6 MS Client Sample ID: FC EB 4

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173280 Prep Batch: 173172

Mercury 0.000102 J 0.00100 0.0009604 mg/L 86 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53315-6 MSD Client Sample ID: FC EB 4

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173280 Prep Batch: 173172

Mercury 0.000102 J 0.00100 0.0007896 F mg/L 69 75 - 125 20 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Lab Sample ID: 500-53315-6 DU Client Sample ID: FC EB 4

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173280 Prep Batch: 173172

Mercury 0.000102 J 0.0001082 J mg/L 6 20

Analyte

DU DU

Result Qualifier Unit D

Sample

Result

Sample

Qualifier RPD Limit

RPD

Lab Sample ID: MB 500-173264/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173438 Prep Batch: 173264

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/18/12 13:00 12/19/12 10:08 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173264/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173438 Prep Batch: 173264

Mercury 0.00200 0.002002 mg/L 100 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LB 500-173187/1-B LB Client Sample ID: Method Blank

Matrix: Solid Prep Type: TCLP

Analysis Batch: 173438 Prep Batch: 173264

RL MDL

Mercury <0.000200 0.000200 0.0000200 mg/L 12/18/12 13:00 12/19/12 10:12 1

LB LB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Method: 7471A - Mercury (CVAA)

Lab Sample ID: MB 500-173153/7-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173328 Prep Batch: 173153

RL MDL

Mercury <0.0167 0.0167 0.00637 mg/Kg 12/17/12 14:00 12/18/12 13:04 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7471A - Mercury (CVAA) (Continued)

Lab Sample ID: LCS 500-173153/8-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173328 Prep Batch: 173153

Mercury 0.167 0.1717 mg/Kg 103 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 1664A - HEM and SGT-HEM

Lab Sample ID: MB 500-173173/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173178 Prep Batch: 173173

RL MDL

HEM (Oil & Grease) <5.00 5.00 1.45 mg/L 12/18/12 05:25 12/18/12 10:05 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173173/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173178 Prep Batch: 173173

HEM (Oil & Grease) 40.0 39.10 mg/L 98 78 - 114

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 7196A - Chromium, Hexavalent

Lab Sample ID: MB 500-173079/3 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173079

RL MDL

Chromium, hexavalent <0.0100 0.0100 0.00325 mg/L 12/15/12 13:21 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173079/4 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173079

Chromium, hexavalent 0.250 0.2497 mg/L 100 85 - 115

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: 500-53315-6 MS Client Sample ID: FC EB 4

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173079

Chromium, hexavalent <0.0100 0.250 0.2500 mg/L 100 85 - 115

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53315-6 MSD Client Sample ID: FC EB 4

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173079

Chromium, hexavalent <0.0100 0.250 0.2500 mg/L 100 85 - 115 0 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 7196A - Chromium, Hexavalent (Continued)

Lab Sample ID: MB 500-173258/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173341 Prep Batch: 173258

RL MDL

Chromium, hexavalent <1.00 1.00 0.389 mg/Kg 12/18/12 10:00 12/18/12 15:46 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173258/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173341 Prep Batch: 173258

Chromium, hexavalent 10.0 8.252 mg/Kg 83 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: LCS 500-173258/3-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173341 Prep Batch: 173258

Chromium, hexavalent 1550 1601 mg/Kg 104 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9014 - Cyanide

Lab Sample ID: MB 500-173245/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173387 Prep Batch: 173245

RL MDL

Cyanide, Total <0.0100 0.0100 0.00331 mg/L 12/18/12 08:30 12/18/12 13:45 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173245/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173387 Prep Batch: 173245

Cyanide, Total 0.100 0.1057 mg/L 106 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173250/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173386 Prep Batch: 173250

RL MDL

Cyanide, Total 0.1850 J 0.500 0.165 mg/Kg 12/18/12 10:35 12/18/12 14:23 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173250/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173386 Prep Batch: 173250

Cyanide, Total 5.00 5.235 mg/Kg 105 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9014 - Cyanide (Continued)

Lab Sample ID: 500-53315-2 MS Client Sample ID: FC D COMPOSITE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173386 Prep Batch: 173250

Cyanide, Total 0.765 J B 6.63 6.130 mg/Kg ☼ 81 75 - 125

Analyte

MS MS

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Lab Sample ID: 500-53315-2 MSD Client Sample ID: FC D COMPOSITE 4

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173386 Prep Batch: 173250

Cyanide, Total 0.765 J B 6.62 6.651 mg/Kg ☼ 89 75 - 125 8 20

Analyte

MSD MSD

Result Qualifier Unit D %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits RPD Limit

RPD

Method: 9034 - Sulfide, Reactive

Lab Sample ID: MB 500-173106/1-A Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173107 Prep Batch: 173106

RL MDL

Sulfide, Reactive <1.00 1.00 1.00 mg/L 12/17/12 00:01 12/17/12 00:19 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173106/2-A Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173107 Prep Batch: 173106

Sulfide, Reactive 3.60 3.292 mg/L 91 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173290/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173472 Prep Batch: 173290

RL MDL

Sulfide, Reactive <50.0 50.0 3.90 mg/Kg 12/19/12 10:05 12/19/12 12:15 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173290/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173472 Prep Batch: 173290

Sulfide, Reactive 180 168.6 mg/Kg 94 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric)

Lab Sample ID: MB 500-173108/1 Client Sample ID: Method Blank

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173108

RL MDL

Sulfide <1.00 1.00 0.230 mg/L 12/17/12 00:19 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

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QC Sample Results

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Method: 9034 - Sulfide, Acid soluble and Insoluble (Titrimetric) (Continued)

Lab Sample ID: LCS 500-173108/2 Client Sample ID: Lab Control Sample

Matrix: Water Prep Type: Total/NA

Analysis Batch: 173108

Sulfide 3.60 3.286 mg/L 91 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Lab Sample ID: MB 500-173291/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173474 Prep Batch: 173291

RL MDL

Sulfide <25.0 25.0 4.00 mg/Kg 12/19/12 11:25 12/19/12 13:35 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173291/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173474 Prep Batch: 173291

Sulfide 180 168.3 mg/Kg 93 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

Method: 9071B - HEM and SGT-HEM

Lab Sample ID: MB 500-173324/1-A Client Sample ID: Method Blank

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173330 Prep Batch: 173324

RL MDL

HEM (Oil & Grease) <500 500 222 mg/Kg 12/19/12 05:10 12/19/12 09:20 1

MB MB

Analyte Result Qualifier Unit D Prepared Analyzed Dil Fac

Lab Sample ID: LCS 500-173324/2-A Client Sample ID: Lab Control Sample

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 173330 Prep Batch: 173324

HEM (Oil & Grease) 4000 4090 mg/Kg 102 80 - 120

Analyte

LCS LCS

Result Qualifier Unit D %Rec

Spike

Added

%Rec.

Limits

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC COMPOSITE 4 Lab Sample ID: 500-53315-1

Date Collected: 12/14/12 15:15 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 25.9

Prep 3050B 173139 12/17/12 08:50 LAH TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Analysis 6010B 1 173224 12/17/12 22:46 TDS TAL CHI

Total/NA Prep 7471A 173153 12/17/12 14:00 BJB TAL CHI

Total/NA Analysis 7471A 1 173328 12/18/12 14:00 BJB TAL CHI

TCLP Leach 1311 173187 12/17/12 12:45 MP TAL CHI

TCLP Prep 7470A 173264 12/18/12 13:00 BJB TAL CHI

TCLP Analysis 7470A 1 173438 12/19/12 10:24 BJB TAL CHI

TCLP Prep 3010A 173406 12/19/12 08:20 LAH TAL CHI

TCLP Analysis 6010B 1 173518 12/19/12 22:29 TDS TAL CHI

Total/NA Analysis Moisture 1 173077 12/15/12 12:43 CMV TAL CHI

Total/NA Analysis SM 2540G 1 173236 12/18/12 07:34 CMV TAL CHI

Total/NA Prep 9071B 173324 12/19/12 05:10 MTB TAL CHI

Total/NA Analysis 9071B 1 173330 12/19/12 11:01 MTB TAL CHI

Total/NA Prep 3060A 173258 12/18/12 10:00 APW TAL CHI

Total/NA Analysis 7196A 1 173341 APW TAL CHI

12/18/12 15:49

12/18/12 15:50

(Start)

(End)

Total/NA Prep 9010B 173250 12/18/12 10:35 EAT TAL CHI

Total/NA Analysis 9014 1 173386 EAT TAL CHI

12/18/12 14:24

12/18/12 14:24

(Start)

(End)

Total/NA Prep 7.3.4 173290 12/19/12 10:40 CLM TAL CHI

Total/NA Analysis 9034 1 173472 12/19/12 12:18 CLM TAL CHI

Total/NA Prep 9030B 173291 12/19/12 11:25 CLM TAL CHI

Total/NA Analysis 9034 1 173474 12/19/12 13:36 CLM TAL CHI

Total/NA Analysis 9045C 1 173479 CLM TAL CHI

12/20/12 15:12

12/20/12 16:11

(Start)

(End)

Total/NA Analysis 1010 1 173558 APW TAL CHI

12/19/12 17:21

12/19/12 18:00

(Start)

(End)

Client Sample ID: FC D COMPOSITE 4 Lab Sample ID: 500-53315-2

Date Collected: 12/14/12 15:15 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 26.3

Prep 3050B 173139 12/17/12 08:50 LAH TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Analysis 6010B 1 173224 12/17/12 23:17 TDS TAL CHI

Total/NA Prep 7471A 173153 12/17/12 14:00 BJB TAL CHI

Total/NA Analysis 7471A 1 173328 12/18/12 14:01 BJB TAL CHI

TCLP Leach 1311 173187 12/17/12 12:45 MP TAL CHI

TCLP Prep 7470A 173264 12/18/12 13:00 BJB TAL CHI

TCLP Analysis 7470A 1 173438 12/19/12 10:29 BJB TAL CHI

TestAmerica Chicago

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D COMPOSITE 4 Lab Sample ID: 500-53315-2

Date Collected: 12/14/12 15:15 Matrix: Solid

Date Received: 12/15/12 09:10

Prep 3010A 173406 12/19/12 08:20 LAH TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

TCLP

TCLP Analysis 6010B 1 173518 12/19/12 22:35 TDS TAL CHI

Total/NA Analysis Moisture 1 173077 12/15/12 12:43 CMV TAL CHI

Total/NA Analysis SM 2540G 1 173236 12/18/12 07:34 CMV TAL CHI

Total/NA Prep 9071B 173324 12/19/12 05:10 MTB TAL CHI

Total/NA Analysis 9071B 1 173330 12/19/12 11:12 MTB TAL CHI

Total/NA Prep 3060A 173258 12/18/12 10:00 APW TAL CHI

Total/NA Analysis 7196A 1 173341 APW TAL CHI

12/18/12 15:50

12/18/12 15:50

(Start)

(End)

Total/NA Prep 9010B 173250 12/18/12 10:35 EAT TAL CHI

Total/NA Analysis 9014 1 173386 EAT TAL CHI

12/18/12 14:24

12/18/12 14:25

(Start)

(End)

Total/NA Prep 7.3.4 173290 12/19/12 10:45 CLM TAL CHI

Total/NA Analysis 9034 1 173472 12/19/12 12:19 CLM TAL CHI

Total/NA Prep 9030B 173291 12/19/12 11:25 CLM TAL CHI

Total/NA Analysis 9034 1 173474 12/19/12 13:37 CLM TAL CHI

Total/NA Analysis 9045C 1 173479 CLM TAL CHI

12/20/12 16:11

12/20/12 17:10

(Start)

(End)

Total/NA Analysis 1010 1 173558 APW TAL CHI

12/19/12 18:00

12/19/12 18:40

(Start)

(End)

Client Sample ID: FC DISCRETE 4 Lab Sample ID: 500-53315-3

Date Collected: 12/14/12 14:45 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 28.9

Analysis 8260B 1 173225 12/18/12 09:30 BDW TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 5030B DL 173238 12/18/12 07:45 BDW TAL CHI

Total/NA Analysis 8260B DL 50 173509 12/20/12 02:16 BDA TAL CHI

Total/NA Analysis Moisture 1 173311 12/18/12 13:59 CMV TAL CHI

Client Sample ID: FC D DISCRETE 4 Lab Sample ID: 500-53315-4

Date Collected: 12/14/12 14:45 Matrix: Solid

Date Received: 12/15/12 09:10 Percent Solids: 28.2

Analysis 8260B 1 173225 12/18/12 10:40 BDW TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 5030B DL 173238 12/18/12 07:45 BDW TAL CHI

Total/NA Analysis 8260B DL 50 173509 12/20/12 02:40 BDA TAL CHI

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Lab Chronicle

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Client Sample ID: FC D DISCRETE 4 Lab Sample ID: 500-53315-4

Date Collected: 12/14/12 14:45 Matrix: Solid

Date Received: 12/15/12 09:10

Analysis Moisture 1 173311 12/18/12 13:59 CMV TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: TRIP BLANK Lab Sample ID: 500-53315-5

Date Collected: 12/14/12 00:00 Matrix: Water

Date Received: 12/15/12 09:10

Analysis 8260B 1 173508 12/20/12 01:08 BDA TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: FC EB 4 Lab Sample ID: 500-53315-6

Date Collected: 12/14/12 14:30 Matrix: Water

Date Received: 12/15/12 09:10

Analysis 8260B 1 173508 12/20/12 01:49 BDA TAL CHI

Type

Batch Batch

Prep Type Method Run Analyst Lab

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Total/NA Prep 7470A 173172 12/17/12 13:00 BJB TAL CHI

Total/NA Analysis 7470A 1 173280 12/18/12 09:49 BJB TAL CHI

Total/NA Prep 3010A 173349 12/18/12 15:30 RL TAL CHI

Total/NA Analysis 6010B 1 173517 12/19/12 14:57 TDS TAL CHI

Total/NA Analysis 7196A 1 173079 APW TAL CHI

12/15/12 13:22

12/15/12 13:22

(Start)

(End)

Total/NA Prep 7.3.4 173106 12/17/12 00:13 CLB TAL CHI

Total/NA Analysis 9034 1 173107 12/17/12 01:08 CLB TAL CHI

Total/NA Analysis 9034 1 173108 CLB TAL CHI

12/17/12 01:11

12/17/12 01:14

(Start)

(End)

Total/NA Prep 1664A 173173 12/18/12 07:24 MTB TAL CHI

Total/NA Analysis 1664A 1 173178 12/18/12 11:14 MTB TAL CHI

Total/NA Prep 9010B 173245 12/18/12 08:30 EAT TAL CHI

Total/NA Analysis 9014 1 173387 EAT TAL CHI

12/18/12 13:54

12/18/12 13:54

(Start)

(End)

Laboratory References:

TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200

TestAmerica Chicago

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Certification Summary

Client: Project Integration, Inc TestAmerica Job ID: 500-53315-1

Project/Site: John Deere Des Moines Works (JDDMW)

Laboratory: TestAmerica Chicago

All certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Alabama State Program 4 40461 04-30-13

California NELAP 9 01132CA 04-30-13

Georgia State Program 4 N/A 04-30-13

Georgia State Program 4 939 04-30-13

Hawaii State Program 9 N/A 04-30-13

Illinois NELAP 5 100201 04-30-13

Indiana State Program 5 C-IL-02 04-30-13

Iowa State Program 7 82 05-01-14

Kansas NELAP 7 E-10161 10-31-13

Kentucky State Program 4 90023 12-31-12

Kentucky (UST) State Program 4 66 04-11-13

L-A-B DoD ELAP L2304 01-06-13

L-A-B ISO/IEC 17025 L2304 01-06-13

Louisiana NELAP 6 30720 06-30-13

Massachusetts State Program 1 M-IL035 06-30-13

Mississippi State Program 4 N/A 04-30-13

North Carolina DENR State Program 4 291 12-31-13

North Dakota State Program 8 R-194 04-30-13

Oklahoma State Program 6 8908 08-31-13

South Carolina State Program 4 77001 04-30-13

Texas NELAP 6 T104704252-09-TX 02-28-13

USDA Federal P330-12-00038 02-06-15

Virginia NELAP 3 460142 06-14-13

Wisconsin State Program 5 999580010 08-31-13

Wyoming State Program 8 8TMS-Q 04-30-13

TestAmerica Chicago

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Login Sample Receipt Checklist

Client: Project Integration, Inc Job Number: 500-53315-1

Login Number: 53315

Question Answer Comment

Creator: Lunt, Jeff T

List Source: TestAmerica Chicago

List Number: 1

Radioactivity wasn't checked or is </= background as measured by a survey True

meter.

The cooler's custody seal, if present, is intact. True

Sample custody seals, if present, are intact. True

The cooler or samples do not appear to have been compromised or True

tampered with.

Samples were received on ice. True 2.7

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

Is the Field Sampler's name present on COC? True

There are no discrepancies between the containers received and the COC. True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

Sample Preservation Verified. True

There is sufficient vol. for all requested analyses, incl. any requested True

MS/MSDs

Containers requiring zero headspace have no headspace or bubble is True

<6mm (1/4").

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

Residual Chlorine Checked. N/A

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