# Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility Pearl Harbor, Oahu, Hawaii Latitude: 21 o 

# 22’15” N Longitude: 157 o 

# 53’33” W
HDOH Facility ID No. 9-102271 HDOH Release ID No. 99051, 010011, 020028

October 2008

Prepared by:

TEC Inc. 1001 Bishop St. Suite 1400 American Savings Bank Tower Honolulu, Hawaii 96813

Prepared for:

Commander Navy Region Hawaii Environmental Department, Code N45 850 Ticonderoga Street, Suite 110 Pearl Harbor, Hawaii 96860-5101

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## i 

# Table of Contents

Table of Contents

............................................................................................................................. i Executive Summary ......................................................................................................................... 1 1.0 Introduction .......................................................................................................................... 4 1.1 Project Objective ............................................................................................................. . 4 1.2 Previous Reports .............................................................................................................. 4 1.3 Background .................................................................................................................... .. 5 1.3.1 Site Description ......................................................................................................... 5 1.3.2 Facility Information .................................................................................................. 5 1.3.3 UST Information ....................................................................................................... 5 1.4 Previous Environmental Investigations ............................................................................ 5 1.5 Regulatory Updates .......................................................................................................... 7 2.0 Sample Collection and Analyses .......................................................................................... 8 2.1 Monitoring Well Purging ................................................................................................. 8 2.2 Groundwater Sample Collection ...................................................................................... 8 2.3 Groundwater Sample Analyses ........................................................................................ 8 3.0 Groundwater Sample Analytical Results ............................................................................. 9 3.1 July 2008 Sample Analytical Results ............................................................................... 9 3.2 Groundwater Contaminant Trend ................................................................................... 11 3.3 Results of Oil-Water Interface Measurements ............................................................... 11 3.4 Groundwater Status ........................................................................................................ 12 4.0 Summary and Conclusions ................................................................................................. 15 5.0 References .......................................................................................................................... 18

List of Tables Table 1 Analytical Results for Quarterly Gr oundwater Sampling Release Response Report ..10 Table 2 Oil-Water Interface Measurements ..............................................................................12 Table 3 Action Levels fo r Compounds of Concern ..................................................................13 Table 4 Responses to Groundwater Monitoring Results ..........................................................13

List of Figures Figure 1 TPH Trends in Groundw ater, Round 12 (July 29, 2008) .............................................16 Figure 2 PAH Trends in Groundw ater, Round 12 (July 29, 2008) ............................................17 List of Appendices Appendix A – Laboratory Analytical Reports

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 1 

# Executive Summary This Quarterly Groundwater Monitoring Report pr esents the results of groundwater sampling conducted on July 29, 2008 at the United States (U S) Navy Bulk Fuel Storage Facility at Red Hill, Oahu, Hawaii (the Facility). The sampli ng and reporting was conducted by TEC Inc. (TEC) for the Air Force Center for Engineering and th e Environment (AFCEE) a nd the Fleet Industrial Supply Center (FISC) at Pearl Ha rbor, Hawaii. This report is part of a series of quarterly groundwater monitoring reports prov ided by the US Navy to the State of Hawaii Department of Health (HDOH) in accordance with HDOH’s release response requirements. Currently, there are 18 active and 2 inactive, 12.5 million gallon, field- constructed underground storage tanks (USTs) located at the Facility. Background In 2002, the United States (US) Navy installed a groundwater monitoring well (currently named RHMW01) into the basal aquifer, directly down- gradient from the Facility, within the lower access tunnel. Groundwater samples from this well indicated that petroleum from the Facility had migrated to the basal aquifer (AMEC, 2002). In 2005, the US Navy began quarterly monitoring of the aquifer to protect their down-gr adient drinking water re source associated with the US Navy Well 2254-01. The US Navy Well 2254-01 is located approximately 3,000 feet downgradient from the Red Hill Fuel Storage Facility and provides approximately 24 % of the potable water to the Pearl Har bor Water System (PHWS). By September 2005, the US Navy had installe d two more groundwater monitoring wells (RHMW02 and RHMW03) within the Facility lower access tunnel, a background groundwater monitoring well (RHMW04) up-gradient from the Facility at ground surface adjacent to the US Navy Firing Range, and a groundwater monito ring well within the US Navy Well 2254-01 infiltration gallery (RHMW2254-01). All five wells were sampled twice as part of a comprehensive environmental investigation and risk assessment (TEC, 2006). For this investig ation, groundwater samples were analyzed for petroleum constituents and compared agai nst HDOH Drinking Water Environmental Action Levels (EALs) (HDOH, 2005a). In addition, a three-dimensional (3-D) groundwater model was developed to produce site-specific risk-based ac tion levels (SSRBLs) for compounds of concern. The results of this modeling effort indicated th at Jet Propulsion (JP)–5 fuel presented the biggest risk to the US Navy water supply, due to its mob ility and toxicity. Finally, the model indicated that a non-aqueous plume (free product) of JP-5 must migrate to with in 1,100 feet of the US Navy Well 2254-01 infiltration gallery for HDOH EA Ls to be exceeded within the gallery. Based on this, free-product must be observed at RHMW01 for EALs to be exceeded at the US Navy Well 2254-01. During the Summer of 2008, HDOH updated their EA Ls, which resulted in significant changes to the action levels associated with methylnaphth alenes (total 1- and 2 -). The drinking water toxicity EAL for these compounds was previously 240 μ g/L, assuming they were not carcinogens. Evidence that they are carcinogenic to humans ha s now been accepted by the United States Environmental Protection Agency (USEPA), and HDOH adopted a more rigorous

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## 2 EAL of 0.47 μ g/L, corresponding to a residential tap wa ter scenario, and a 1 in a million cancer risk. This equates to lowering the previ ous action level by a factor of 510 (HDOH, 2008).

Groundwater Protection Plan In 2008, the US Navy completed the Red Hill Bulk Fuel Storage Facility Final Groundwater Protection Plan (TEC, 2008), or Plan, which specified SSRBLs for each well, and actions that would occur for the pertinent cases, based on categories for each groundwater monitoring well (Categories 1 through 4). The main object of th e Plan is to protect groundwater quality entering the US Navy Well 2254-01, which provides potable wa ter to the PHWS. Th is is accomplished by comparing petroleum concentrations in the Facility wells (RHMW01, RHMW02, and RHMW03) to the SSRBLs and taking the corr esponding action. A secondary but important objective of the Plan is to identify leaking US Ts by evaluating increasi ng concentration trends, or the sudden and lasting presence of free produc t in one or more groundwater monitoring wells. In the current quarterly groundwater monitoring report, the current water quality is compared to these categories and actions are recommended, based on those specified in the Plan.

Current Results This quarterly groundwater monitoring report pres ents the analytical results from samples collected in July 2008 and compares them to Stat e and site-specific action levels. Concentration trends for chemicals that exceeded HDOH Drinki ng Water EALs are also provided. Four normal samples were collected from RHMW2254- 01, RHMW01, RHMW02 and RHMW03; a duplicate sample was collected at RHMW02; and the labo ratory conducted matrix spike/matrix spike duplicate (MS/MSD) analysis on the sample aliquot from RHMW2254-01. Samples were analyzed for Total Petroleum Hydrocarbons (TPH ) quantified as diesel-range organics (DRO) and gasoline range organics (G RO); volatile organic compounds (VOCs); polynuclear aromatic hydrocarbons (PAHs); and lead. Laboratory analytical results indicate that TPH-DRO and P AHs were detected in the groundwater from beneath the Facility at c oncentrations that exceed HDOH Drinking Water EALs. TPH-DRO was detected at 327 microgr ams per liter (μg/L) in RHMW01, at 4,055 μg/L (average of normal and duplicate sample) in RHMW02, and 199 μg/L in RHMW03. The HDOH Drinking Water EAL for TPH-DRO is 100 μg/L. Th ree PAHs were detected in the normal and duplicate samples associated with RHMW02 at average concentrations above the HDOH Drinking Water EALs: naphthalene at 136 μg/L (HDOH EAL is 6.2 μg/L), 1-methylnaphthalene at 99 μg/L and 2-methylnaphthalene at 36.9 μg/L (HDOH EAL for total methylnaphthalenes [1- and 2-] is 0.47 μg/L). Trend Analysis At RHMW01, concentrations of TPH-DRO have been greater than the HDOH Drinking Water EAL since September 2005 but less than 25 percent of the SSRBL of 4,500 μ g/L. TPH-DRO has been decreasing in concentration over the last three rounds, since January 2008.
At RHMW02, concentrations of TPH-DRO have been greater than the HDOH Drinking Water EAL since September 2005 and greater th an 50 percent of the SSRBL of 4,500 μ g/L over that same period. TPH-DRO has been increasing in co ncentration over the last three rounds, since January 2008, and the average concentrati on from the July 2008 sampling event was

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## 3 approximately 91 percent of the SSRBL (sol ubility limit). Three PAHs (naphthalene, 1- methylnaphthalene, and 2-methyl naphthalene) also have exceeded the EALs since September 2005, and have been increasing in concentra tion since January 2008. There are no SSRBLs set for these PAHs to date.

At RHMW03, concentrations of TPH-DRO have fluctuated around the HDOH EAL since September 2005 and are significantly lower th an at RHMW01 and RHMW02. There are no significant trends observed in the results at RHMW03.

Current Groundwater Status Based on the monitoring event th at occurred in July 2008, no free product was observed at RHMW01, RHMW02, or RHMW03. Results fro m groundwater samples indicate that RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is greater than the HDOH EAL for drinking water (100 μ g/L), but less than half the SSRBL of 4,500 μ g/L (solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires: 1. Quarterly reports to be sent to HDOH; and 2. Initiation of a leak determination progr am to identify if tanks are leaking. Results from groundwater samples indicate that RH M02 is presently in Category 3 status, since TPH-DRO (4,470 μ g/L and 3,640 μ g/L [duplicate]) is greater th an the HDOH EAL for drinking water (100 μ g/L), and greater than half the SSRBL of 4,500 μ g/L (solubility limit of JP-5). Category 3 response at RHMW02 requires: 1. Quarterly reports to be sent to HDOH; 2. Initiation of a leak determination progr am to identify if tanks are leaking; 3. Increase monitoring frequency to once per month if concentrations are increasing; 4. Notify HDOH within 7 days and follow with written notification within 30 days; 5. Measure product with interface probe in wells of concern; 6. Immediately determine if tanks are leaking.

Conclusions and Recommendations There is no indication of an imminent threat to the US Navy Well 2254-01 water resources based on this report, since petroleum concentrations at RHMW01 remain less than half the SSRBLs. It is recommended that RHMW01 and RHMW02 be ev aluated monthly for the presence of fuel on groundwater, in accordance with the Plan. It is also recommended that quarterly groundwater sampling for TPH-DRO, TPH-GRO, VOCs, PAHs , and lead be continued as previously scheduled until new data indicates a different schedule is required.

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## 4 

# 1.0 Introduction This report presents the results of the 12 th 

## groundwater sampling and analysis event, conducted in July 2008 at the Red Hill Fuel Storage Facil ity, Oahu, Hawaii (hereafter referred to as “the Facility”). The Facility consists of 18 activ e and 2 inactive undergr ound storage tanks (USTs) operated by the Fleet Industrial and Supply Ce nter (FISC), Pearl Ha rbor. The groundwater sampling and analysis event is part of a groundw ater monitoring program for the UST site in response to past UST releases, previous envi ronmental investigations, and recommendations from the Hawaii Department of Health (HDOH). 

# 1.1 Project Objective This groundwater sampling and analysis project was performed to evaluate the presence of chemicals of potential concern in groundwater underlying the Facil ity. The project was conducted to ensure the Navy remains in co mpliance with HDOH UST release response requirements as described in Hawaii Administra tive Rules (HAR) 11-281 Subchapter 7, Release Response Action. The groundwater sampling and an alysis procedures generally followed the procedures described in Red Hill Bulk Fuel Storage Faci lity Groundwater Protection Plan (TEC Inc [TEC], 2008) (Also refe rred to as “the Plan”). This groundwater sampling and analysis event was conducted by TEC under Air Force Center for Engineering and the Environment (AFC EE) Contract Number F41624-03-D-8618, Task Order 021. 

# 1.2 Previous Reports The following groundwater monitoring reports we re previously submitted to the HDOH:

1. Groundwater Sampling Report, First Quarter 2005 (submitted April 2005); 2. Groundwater Sampling Report, Second Quarter 2005 (submitted August 2005); 3. Groundwater Sampling Report, Third Quarter 2005 (submitted November 2005); 4. Groundwater Sampling Report, Fourth Quarter 2005 (submitted February 2006); 5. Groundwater Monitoring Results, July 2006 (submitted September 2006); 6. Groundwater Monitoring Results, December 2006 (submitted January 2007); 7. Groundwater Monitoring Results, March 2007 (submitted May 2007); 8. Groundwater Monitoring Results, June 2007 (submitted August 2007); 9. Groundwater Monitoring Results, September 2007 (submitted October 2007); 10. Groundwater Monitoring Results, January 2008 (submitted March 2008); and 11. Groundwater Monitoring Results, April 2008 (submitted May 2008);

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## 5 

# 1.3 Background The following sections provide a description of th e site and information on the Facility and USTs.
1.3.1 Site Description The Facility is located in Hala wa Heights on Oahu, Hawaii. Land adjacent to the north of the Facility is occupied by Halawa Correctional Facility and private businesses. Land to the south and west of the Facility include s the Coast Guard Reservation. Moanalua Valley is located east of the Facility (Dawson, 2006). The Navy Public Works Department operates a po table water infiltration tunnel approximately 1,550 feet hydraulically downgradient from the Facility (Dawson, 2006). The US Navy Well 2254-01 is located approximately 3,000 feet downgrad ient (west) of the Facility and provides approximately 24 % of the potable water to th e Pearl Harbor Water System, which serves approximately 52,200 military consumers (TEC, 2008).
1.3.2 Facility Information The Facility consists of 18 ac tive and 2 inactive USTs operate d by Navy FISC Pearl Harbor. Each UST has a capacity of 12.5 million gallons. Th e Facility is located approximately 100 feet above the basal aquifer (Dawson, 2006).
1.3.3 UST Information The USTs were constructed in the early 1940s. Th e tanks were constructed of steel and currently contain Jet Propulsion (JP)–5 fuel a nd F-76 (diesel marine fuel). Pr eviously, several tanks stored Navy Special Fuel Oil, Navy Distillate, aviati on gasoline, and motor gasoline. Each tank measures approximately 245 feet in height and 100 feet in diameter. The upper domes of the tanks lie at depths varying between approxima tely 100 feet and 200 feet below the existing ground surface (TEC, 2006). 

# 1.4 Previous Environmental Investigations 1998 to 2001: From 1998 to 2001, the Navy conducted an in vestigation at the Facility to assess potential releases from the fuel storage USTs and piping systems. In February 2001, the Navy installed a one-inch diameter sentinel we ll RHMW01 (previously known as MW-V1D) to monitor for contamination of the basal aquifer underlying the Facility. The well was installed and completed at approximately 100 feet below grade within the underground access tunnel. At the time of well completion, depth to water in RHMW01 was measured at 86 feet below grade (Dawson, 2006). In February 2001, groundwater samples collected from sentinel well RHMW01 contained total petroleum hydrocarbons (TPH) concentrati ons ranging from 883 micrograms per liter ( μ g/L) to 1,050 μ g/L and total lead ranging from 10.4 μ g/L to 15 μ g/L. The maximum total lead concentration in the samples was equal to the primary drinking water standard of 15 μ g/L for lead and exceeded the HDOH Tier 1 groundwater action level of 5.6 μ g/L (Dawson, 2006).

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## 6 2005 – Groundwater Sampling: The Navy began quarterly groundwater sampling at existing monitoring wells in 2005. Dawson Group, Inc. collected groundwater samples from RHMW01 and the Red Hill Navy Pump Sta tion (US Navy Well 2254-01) in February, June, September, and December 2005. Samples collected in February and June 2005 were not filtered in the field prior to analysis for lead. Analytical results for samples collected from RHMW01 indicated concentrations of total lead were above the HDOH Ti er 1 action level of 5.6 μ g/L. The results were not considered appropriate for risk assessment since the sample had not been filtered. In addition, lead was not a component of fuels from the tanks near RHMW01. Lead may have been part of the Facility construction material (TEC, 2007). Samples were filtered in September and Decembe r 2005, and dissolved lead concentrations were below the HDOH Tier 1 action level. Concentrat ions of all other cont aminants of potential concern were below HDOH Tier 1 action levels. 2005 – Site Investigation: As part of a site investiga tion, TEC installed three groundwater monitoring wells at the Faci lity between June and September 2005. Well RHMW02 was installed in the lower access tunnel near Tanks 5 and 6. Well RHMW03 was installed in the lower access tunnel near Tanks 13 and 14. Well RHMW04 was inst alled hydraulically upgradient of the USTs to provide geochemist ry for water moving through the basal aquifer beneath the Facility. Wells RHMW02 and RHMW03 were completed to depths of approximately 125 feet below the tunnel floor, and well RHMW04 was completed to a depth of approximately 300 feet below ground surface outsi de the tunnel. Groundwater samples were collected from the three newly installed well s and two existing wells (RHMW01 and US Navy Well 2254-01) in September 2005. Naphthalene and trichloroethylene were detect ed in samples collected from RHMW02 at concentrations greater than the HDOH Tier 1 acti on levels. Lead was detected in the sample collected from RHMW01 at a concentration greater than the HDOH Tier 1 action level; however, the sample was not filtered in the field pr ior to analysis. Analytical results for filtered samples obtained by Dawson during the same period indicated concentrations of dissolved lead were below the HDOH Tier 1 action level. 2006 – Site Investigation: Dedicated sampling pumps were in stalled in five wells (RHMW01, RHMW02, RHMW03, RHMW04, and US Navy Well 2254-01). TEC collected groundwater samples from the wells in July 2006. The gr oundwater samples were analyzed for petroleum constituents. Naphthalene was detected in sa mples collected from RHMW02 at concentrations above the HDOH Tier 1 action level. In September 2005, with concurrence from th e HDOH, the Navy decided to use the newer HDOH Environmental Action Levels (EALs) for the Red Hill Site Investigation and Risk Assessment project. The EALs are current and pr ovide action levels for more chemicals, and are much more useful for conducting screening risk assessments. Since the HDOH June 2005 Policy Letter stated that the two sets of action levels should not be mixed, the Tier 1 screening levels

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## 7 presented in HAR Section 11-281-78 would no longer be used to evaluate environmental impact at the Facility. 2006 – Groundwater Sampling: Groundwater samples were collected in December 2006. Analytical results indicated the following:

• No chemicals were detected in groundwat er from US Navy Well 2254-01 or RHMW03;

• TPH as diesel range organics (TPH-DRO) was detected in groundwater above the HDOH Drinking Water EALs in RHMW01; and

• TPH as gasoline range organics (TPH-GRO), TPH-DRO, and naphthalene were detected in groundwater above the HDOH Dri nking Water EALs in RHMW02. 2007 – Groundwater Sampling: Groundwater samples were co llected in March, June, and September 2007. Analytical resu lts indicated the following:

• No chemicals were detected above H DOH Drinking Water EALs at US Navy Well 2254-01;

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01 during all three sampling events;

• TPH-GRO exceeded HDOH Drinking Wate r EALs at RHMW02 in March;

• TPH-DRO and naphthalene exceeded HDOH Drinking Water EALs at RHMW02 during all three sampling events;

• 1-methylnaphthalene and 2-methylnapht halene exceeded HDOH Drinking Water EAL for taste and odor at RHMW02 duri ng all three sampling events; and

• TPH-DRO exceeded HDOH Drinking Wate r EALs at RHMW03 in June. 2008 – Groundwater Sampling: Groundwater samples were collected in January and April 2008. Analytical results indicated the following:

• No chemicals were detected above H DOH Drinking Water EALs at US Navy Well 2254-01;

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW01;

• TPH-GRO did not exceed HDOH Dr inking Water EALs at RHMW02;

• TPH-DRO and naphthalene exceeded HDO H Drinking Water EALs at RHMW02;

• 1-methylnaphthalene and 2-methylnapht halene exceeded HDOH Drinking Water EAL for taste and odor at RHMW02; and

• TPH-DRO exceeded HDOH Drinking Water EALs at RHMW03.


# 1.5 Regulatory Updates During the Summer of 2008, HDOH updated their EA Ls, which resulted in significant changes to the action levels associated with methylnaphth alenes (total 1- and 2 -). The drinking water toxicity EAL for these compounds was previously 240 μ g/L, assuming they were not carcinogens. Evidence that they are carcinoge nic to humans has now been accepted by the United States Environmental Protection Agency (USEPA), and HDOH adopted a more rigorous EAL of 0.47 μ g/L, corresponding to a residential tap wa ter scenario, and a 1 in a million cancer risk. This equates to lowering the pr evious action level by a factor of 510.

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## 8 

# 2.0 Sample Collection and Analyses Field activities relating to groundwater samp le collection were conducted on July 29, 2008. Groundwater samples were collected from three monitoring wells located inside the Facility lower access tunnel and one monitoring well loca ted at the Red Hill Navy Pump Station. Sampling and analysis were conducted according to Red Hill Bulk Fuel Storage Facility Groundwater Protection Plan (TEC, 2008). A total of seven samples were collected; one normal sample from monitoring wells US Navy Well 2254-01, RHMW01, RHMW02 and RHMW03, one duplicate sample from RHMW02 (Sampl ed as RHMWA01 and reported as RHMW02- WG11D), and one matrix spike and matr ix spike duplicate from US Navy Well 2254-01. 

# 2.1 Monitoring Well Purging The groundwater monitoring wells were purged a nd sampled using a dedicated pump system. Well purging was considered complete when no less than three successive water quality parameter measurements had stabili zed within approximately 10 per cent. Field parameters were measured at regular intervals during well purgi ng and included pH, te mperature, specific conductivity, dissolved oxygen, and turbidity. Purge water was disposed in the Facility oil/water separator system. 

# 2.2 Groundwater Sample Collection Each monitoring well was sampled immediatel y following purging. All wells were sampled directly from their dedicated bladder pump sy stem. Samples were placed into sampling containers with appropriate preservatives (i.e ., hydrochloric acid [H Cl] for volatile organic analysis, nitric acid [HNO 3 

## ] for dissolved lead). Dissolved lead samples were filtered in the field and placed in preserved bottles. Sample cont ainers were labeled with the date, sample identification number, type of analysis, and samp ler’s name. The containers were placed on ice in sample coolers and transported under chain-of -custody procedures to the certified laboratory for analysis. 

# 2.3 Groundwater Sample Analyses Groundwater samples were analyzed by SGS Environm ental Service, Inc. in Anchorage, Alaska for TPH-DRO and TPH-GRO by EPA Method 8015B , volatile organic compounds (VOCs) by EPA Method 8260B, polynuclear aromatic hydr ocarbons (PAHs) by EPA Method 8270C SIMS, and dissolved lead by EPA Method 6020.

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## 9 

# 3.0 Groundwater Sample Analytical Results This section provides a summary of analytical results for grou ndwater samples collected from three monitoring wells located in the lower access tunnel of the F acility and one monitoring well located at the Red Hill Navy Pump Station. D uplicate sample results from monitoring well RHMW02 are reported in this document as RH MW02D. A summary of groundwater analytical results is included in Table 1. Complete analyt ical laboratory reports are provided in Appendix A. 

# 3.1 July 2008 Sample Analytical Results All groundwater samples were analyzed for TP H-DRO, TPH-GRO, VOCs, PAHs, and dissolved lead. Bromomethane was detected at US Na vy Well 2254-01 at 1.26F μg/L, which is below the HDOH Drinking Water EAL of 8.5 μg/L. Data qualif ier “F” indicates the re sult is between the method detection limit (MDL) and the reporting limit (RL) and considered an estimated value. TPH-DRO was detected at RHMW01 at 327 μg/L , which is above the HDOH Drinking Water EAL of 100 μg/L. All other chemicals of pot ential concern were be low HDOH Drinking Water EALs at RHMW01.

TPH-DRO was detected at RHMW02 and duplicate sample at 4,470 and 3,640 μg/L, respectively (HDOH EAL is 100 μg/L). Napht halene was analyzed by EPA Method 8270 SIM and EPA Method 8260B and detected by bot h methods at RHMW02. EPA Method 8260B produced the highest naphthalene concentratio ns, which were 320 and 309 μg/L for the normal and duplicate sample, respectiv ely (HDOH EAL is 6.2 μg/L). The concentrations of 1-methylnaphthalene and 2-met hylnapthalene were above the new HDOH Drinking Water EALs toxicity of 0.47 μ g/L. All other chemicals of potent ial concern were below HDOH Drinking Water EALs at RHMW02. Only three compounds were detected at RHMW03: TPH-DRO, naphthalene, and 1- methylnaphthylene. TPH-DRO was detected at RHMW03 at 199 μg/L, (HDOH EAL is 100 μg/L). All other chemicals of potential co ncern were below HDOH Dr inking Water EALs at RHMW03.Table 1. Analytical Results for Quarterly Groundwater Monitoring Release Response Report (July 29, 2008)Red Hill Fuel Storage Facility, Pearl Harbor, HawaiiResult Q MDL RL Result Q MDL RL ResultQ MDL RL Result Q MDL RL Result Q MDL RLTPH (middle distillates)208 100327F 80 400447083.3 417364080 400199F 82.5 412 ND U 83.3 417TPH (gasolines)100 100 ND U 10 100 61.7 F 10 100 61.2 F 10 100 ND U 10 100 ND U 10 100METHYLNAPHTHALENE,1-0.47 10 ND U 0.015 0.051020.773 2.5896.00.773 2.58 0.0294 F 0.0156 0.0521 ND U 0.0156 0.0521METHYLNAPHTHALENE,2-0.47 10 ND U 0.015 0.0531.50.773 2.5842.20.773 2.58 ND U 0.0156 0.0521 ND U 0.0156 0.0521METHYLNAPHTHALENE (total 1- & 2-)0.47 10 ND133.5 138.20.0294 NDACENAPHTHENE365 20 ND U 0.015 0.05 0.470 F 0.155 0.515 0.45 F 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521ACENAPHTHYLENE243 1965 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521ANTHRACENE1825 21.7 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521BENZO(a)ANTHRACENE0.094.7NDU0.0150.05NDU0.1550.515NDU0.1550.515NDU0.01560.0521NDU0.01560.0521MethodHDOH ResidentialDrinking Water EALs1UG/LHDOH DrinkingWater CeilingEALs2UG/LChemicalRHMW01UG/LSW8015B(Petroleum)RHMW2254UG/LRHMW02UG/LRHMW02DUG/LRHMW03UG/LJuly 29, 2008July 29, 2008 July 29, 2008 July 29, 2008 July 29, 2008BENZO(a)ANTHRACENE0.094.7NDU0.0150.05NDU0.1550.515NDU0.1550.515NDU0.01560.0521NDU0.01560.0521BENZO(a)PYRENE0.2 0.81 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521BENZO(b)FLUORANTHENE0.09 0.75 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521BENZO(g,h,i)PERYLENE1460 0.13 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521BENZO(k)FLUORANTHENE0.92 0.4 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521CHRYSENE9.2 1 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521DIBENZO(a,h)ANTHTRACENE0.01 0.515 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521FLUORANTHENE1460 130 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521FLUORENE243 945 0.0206 F 0.015 0.05 0.324 F 0.155 0.515 0.304 F 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521INDENO(1,2,3-cd)PYRENE0.09 0.095 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521NAPHTHALENE6.2 21 0.114 0.031 0.11403.2 10.31323.2 10.3 0.0689 F 0.0323 0.104 ND U 0.0323 0.104PHENANTHRENE243 408 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521PYRENE182.5 67.5 ND U 0.015 0.05 ND U 0.155 0.515 ND U 0.155 0.515 ND U 0.0156 0.0521 ND U 0.0156 0.0521TETRACHLOROETHANE, 1,1,1,2-0.52 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5TRICHLOROETHANE, 1,1,1-200 970 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TETRACHLOROETHANE, 1,1,2,2-0.07 500 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5TRICHLOROETHANE, 1,1,2-5 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TRICHLOROBENZENE, 1,2,4-70 3000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DIBROMO,1,2- CHLOROPROPANE,3-0.04 10 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2DICHLOROPROPANE, 1,2-5 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DICHLOROBENZENE, 1,3-183 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1SW8270SIM(PAHs)DICHLOROPROPENE, 1,3-0.43 50000 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4DICHLOROBENZENE, 1,4-75 5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5ACETONE21783 20000 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10BENZENE5 170 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4 ND U 0.12 0.4BROMODICHLOROMETHANE0.22 50000 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5BROMOFORM100 510 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1BROMOMETHANE8.7 50000 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 ND U 0.94 3 1.26 F 0.94 3CARBON TETRACHLORIDE5 520 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROBENZENE100 50 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5 ND U 0.15 0.5CHLOROETHANE8588 16 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1CHLOROFORM70 2400 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1 ND U 0.3 1CHLOROMETHANE1.8 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DICHLOROETHYLENE, Cis 1,2-70 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DIBROMOETHANE, 1,2-0.0065 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1ETHYLBENZENE700 30 ND U 0.31 1 0.580 F 0.31 1 0.560 F 0.31 1 ND U 0.31 1 ND U 0.31 1HEXACHLOROBUTADIENE0.86 6 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1XYLENES10000 20 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2 ND U 0.62 2METHYL ETHYL KETONE7065 8400 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYL ISOBUTYL KETONE1991 1300 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10 ND U 3.1 10METHYLENE CHLORIDE4.8 9100 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5 ND U 1 5NAPHTHALENE6 221NDU0 6223206 2203096 220NDU0 622NDU0 622SW8260(VOCs)NAPHTHALENE6.221NDU0.6223206.2203096.220NDU0.622NDU0.622STYRENE100 10 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TETRACHLOROETHYLENE5 170 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TOLUENE1000 40 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1DICHLOROETHYLENE, Trans 1,2-100 260 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1TRICHLOROETHYLENE5 310 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1VINYL CHLORIDE2 3400 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1SW6020LEAD15 50000 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1 ND U 0.31 1PAHs - Polynuclear aromatic hydrocarbonsMDL - Method detection limitVOCs - Volatile organic compoundsRL - Reporting limitUG/L - Micrograms per LiterTPH - Total petroleum hydrocarbonsQ - Data qualifierND - Indicates that the compound was not detected above the stated method detection limitU - Indicates that the compound was analyzed for but not detected at or above the stated limitF - Indicates that the compound was identified but the concentration was above the MDL and below the RL-Result exceeds one or both HDOH EAL's12Toxicity-based environmental action levels, Table D-1b,Screening For Environmental Hazards At Sites WithContaminated Soil and Groundwater,HDOH, 2008Taste, odor and solubilitythresholds,Table D-1b,Screening For Environmental Hazards At Sites With ContaminatedSoil and Groundwater, HDOH, 2008200Page 1 of 1

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 11 

# 3.2 Groundwater Contaminant Trend Groundwater samples have been collected and analyzed by TEC since September 2005. Figure 1 shows TPH trends in groundwater at the Facility. Fi gure 2 shows PAH trends in groundwater at the Facility. In these figures, open icons (wit hout fill) represent the method detection limit for chemicals that were not detected.

RHMW01 TPH-GRO has only been detected in Apr il 2008 at 13.6F μg/L, which is below the HDOH Drinking Water EAL of 100 μg/L. In July 2008, TPH-GRO was not dete cted. TPH-DRO was detected above the HDOH Drinking Water EAL of 100 μg/L during all groundwater sampling events and had shown a decreasing trend until th e January 2008 sampling event. Concentration of TPH-DRO observed during the July 2008 sampli ng event was lower than the concentrations observed in January and April 2008, but hi gher than the previous four rounds.

RHMW02 TPH-GRO was detected in eigh t of nine sampling events since September 2005, and exceeded the HDOH Drinking Water EAL three tim es during 2006 and 2007. The maximum concentration detected was 148 μg/L, which is slightly above the EAL of 100 μg/L. The concentration of TPH-DRO was relatively stab le at RHMW02 until January 2008, ranging from 2,250 to 3,180 μg/L. However, since January 20 08 it has shown an increasing trend with concentrations up to 4,470 μg/L, well above the HDOH Drinking Water EAL of 100 μg/L. PAHs at RHMW02 remain above the HDOH Dri nking Water EALs, and concentrations have also been increasi ng since January 2008.

RHMW03 TPH-GRO has never been detect ed. TPH-DRO had shown a decr easing trend until the January 2008 sampling event. Concentrations of TP H-DRO observed during the July 2008 sampling event were lower than the concentrations obser ved in January 2008, but hi gher than the previous rounds. In general, concentrations of petrol eum-related compounds at RHMW03 have been the lowest of the three wells located within the Facility. 

# 3.3 Results of Oil-Water Interface Measurements The presence and thickness of light-non aque ous phased liquids (LNAPL), otherwise known as free product, released from the USTs were meas ured during this sampling event using a 100 ft Heron Oil/Water Interface Meter. The static water levels were m easured to a precision of ± 0.01 ft and fuel thickness was measured to a pr ecision of ± 0.01 ft with this equipment. In January 2008, fuel was measured in monito ring wells RHMW01 and RHMW02 at a thickness of < 0.01 ft, but has not been observed in other monitoring wells to date. Measurements to determine the presence and thickness of fuel were conducted at RHMW01, RHMW02, and RHMW03 during the cu rrent sampling round. No fuel product was observed in any of these wells during this event (see Table 2).

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 12 Table 2. Oil-Water Interface Measurements

Date RHMW01 RHMW02 RHMW03 SWL

(ft) LNAPL (ft) SWL (ft) LNAPL (ft) SWL (ft) LNAPL (ft) January 2008 17.74 < 0.01 18.78 < 0.01 NT NT April 2008 NT NT NT NT NT NT July 2008 19.04 0.00 18.91 0.00 18.86 0.00

SWL Static water level, elevation above mean sea level LNAPL Light Non-Aqueous Phased Liquid, fuel product on groundwater ft Feet NT Not Taken 

# 3.4 Groundwater Status Compounds of concern are defined as those petroleum-related chem icals that have been observed in the groundwater samples above th e HDOH EALs. In accordance with the Red Hill Bulk Fuel Storage Facility Final Groundwater Protection Plan (TEC, 2008), the following categories may be applicable based on the concentration of a co mpound at a specific well re lated to site-specific risk-based action levels (SSRBL) and EALs (see Table 3) and groundwater concentration trends.

Table 3. Action Levels for Compounds of Concern

Chemical EAL (μg/L) SSRBL (μg/L) Petroleum Mixtures TPH-DRO 100 4,500 TPH-GRO 100 4,500 Semi-Volatile Compounds 1-Methylnaphthalene 0.47 NA 2-Methylnaphthalene 0.47 NA Naphthalene 6.22 NA NA – Not applicable or not determined SSRBLs are applicable at RHMW01, RHMW02, and RHMW03 EALs are applicable at US Navy Well 2254-01



## Based on the monitoring event th at occurred in July 2008, no free product was observed at RHMW01, RHMW02, or RHMW03. Results fro m groundwater samples indicate that RHMW01 and RHMW03 are presently in Category 2 status, since TPH-DRO is greater than the HDOH EAL for drinking water (100 μ g/L), but less than half the SSRBL of 4,500 μ g/L (solubility limit of JP-5). Category 2 response at RHMW01 and RHMW03 requires: 1. Quarterly reports to be sent to HDOH; and

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 13 2. Initiation of a leak determination progr am to identify if tanks are leaking. Results from groundwater samples indicate that RH M02 is presently in Category 3 status, since TPH-DRO (4,470 μ g/L and 3,640 μ g/L [duplicate]) is greater th an the HDOH EAL for drinking water (100 μ g/L), and greater than half the SSRBL of 4,500 μ g/L (solubility limit of JP-5). Category 3 response at RHMW02 requires:

1. Quarterly reports to be sent to HDOH; 2. Initiation of a leak determination progr am to identify if tanks are leaking; 3. Increase monitoring frequency to once per month if concentrations are increasing; 4. Notify HDOH within 7 days and follow with written notification within 30 days; 5. Measure product with interface probe in wells of concern; 6. Immediately determine if tanks are leaking. Table 4 describes each category a nd identifies response actions to be taken in accordance with the Plan.

Table 4. Responses to Groundwater Monitoring Results

Results Category RHMW02 or RHMW03 RHMW01 U.S. Navy Pumping Well 2254-01 Results Category 1: Result above detection limit but below drinking water EAL and trend for all compounds stable or decreasing A A A,D,M,E,P

Results Category 2: Trend for any compound increasing or drinking water EAL exceeded A, B A, B A,B,C,D,E,F,G,K, L,O
Results Category 3: Result Between 1/10X SSRBL and SSRBL for benzene, or between 1/2X SSRBL and SSRBL for TPH A,B,G,H,I,J A,B,E,G,H,I,J A,B,C,D,E,F,G,I,J, K,L,O

Results Category 4: Result Exceeding any SSRBL or petroleum product measured or observed A,C,D,E,F,I,J, K,M,N A,C,D,E,F,I, J,K,M,N,O A,C,D,E,F,G,I,J,K, L,O

Specific Responses: A. Send quarterly reports to HDOH B. Begin program to determine the source of leak C. Notify HDOH verbally within 1 day and fo llow with written notification in 30 days D. Notify FISC Chain of Command within 1 day E. Send Type 1 Report (see box below) to HDOH F. Send Type 2 Report (see box below) to HDOH

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 14 G. Increase monitoring frequ ency to once per month (if concentrations increasing) H. Notify HDOH verbally within 7 days and follow with written notification in 30 days I. Remove sampling pumps (see Appendix C), measur e product in pertinent wells with interface probe, re-install pumps if product is not detected. J. Immediately determine leaking tank K. Collect samples from nearby Halawa D eep Monitoring Well (2253-03) and OWDF MW01 For permission to sample 2253-03, call DLNR Commission on Water Resource Management (808) 587-0214, DLNR.CWRM@Hawaii.gov L. Provide alternative water source at 2254-01 M. Prepare for alternative water source at US Navy Well 2254-01 N. Re-measure for product every month with reports to HDOH O. Install additional monitoring well downgradient 

## Report Types HDOH Type 1 Report

• Re-evaluate Tier 3 Risk Asse ssment/groundwater model results

• Proposal to HDOH on a course of action HDOH Type 2 Report

• Proposal for groundwater treatment

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 15 

# 4.0 Summary and Conclusions TPH-DRO and PAHs are present in the groundwater beneath the Facility at concentrations that exceed HDOH Drinking Water EALs. There is no i ndication of an imminen t threat to the US Navy Well 2254-01 water resources, since petroleu m concentrations at RHMW01 remain less than half the SSRBLs.

It is recommended that RHMW01 and RHMW02 be evaluated mont hly for the presence of fuel on groundwater, in accordance with the Plan. It is also recommended that quarterly groundwater sampling for TPH-DR O, TPH-GRO, VOCs, PAHs, and lead be continued as previously scheduled until new data indicates a different schedule is required. The quarterly collection and analysis of groundw ater samples will continue to monitor the quality of the groundwater located beneath the Facility. Groundw ater monitoring reports will be submitted to the HDOH upon receipt and evaluation of laboratory analy tical results.Figure1TPHTrendsinGroundwaterRound12(July29,2008)RedHillFuelStorageFacilityOahu,Hawaii* The HDOH EAL was updated in the Summer of 2008, basedon the US EPA Evaluation of 1and 2methylnaphthalene as aontheUSEPAEvaluationof1--methylnaphthaleneasacarcinogen, Residential Tap Water Scenario , and 1 in a millioncancer risk (HDOH, 2008).Figure2PAHTrendsinGroundwaterRound12(July29,2008)RedHillFuelStorageFacilityOahu,Hawaii

### Quarterly Groundwater Monitoring Report Red Hill Fuel Storage Facility October 2008

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## 18 

# 5.0 References AMEC. 2002. Red Hill Bulk Fuel Storage Facility Investigation Report , Prepared for NAVFAC Pacific, August 2002.
Dawson Group, Inc. 2006. Fourth Quarter 2005 Groundwater Sam pling Report, Red Hill Fuel Storage Facility, Hawaii. February 2006.
Hawaii Administrative Rules, Titl e 11, Chapter 281, Subchapter 7. State of Hawaii Department of Health (HDOH). 2005. Screening for Envir onmental Concerns at Sites with Contaminated Soil and Groundwater, Volume 1: Summary Tier 1 Lookup Tables. Interim Final. May 2005.

HDOH. 2008. Screening for Environmental Hazards at Sites With Contaminated Soil and Groundwater . Summer 2008. State of Hawaii Department of Health. 2005b. Use of May 2005 Environmental Action Levels (“EALs”) at Leaking Underg round Storage Tank Sites . Memo. 15 July. The Environmental Company, Inc. and AMEC. 2005. Red Hill Bulk Fuel Storage Facility Work Plan, Pearl Harbor, Hawaii. June.

TEC Inc. 2006. Red Hill Bulk Fuel Storage Facility , Final – Addendum Planning Documents, Pearl Harbor, Hawaii. May.

TEC Inc. 2007. Red Hill Bulk Fuel Storage Facility, Final Technical Report, Pearl Harbor, Hawaii . August.

TEC Inc. 2008. Red Hill Bulk Fuel Storage Facility, Final Groundwater Protection Plan, Pearl Harbor, Hawaii. January.

# Appendix A Laboratory Analytical Reports

## SGS Work Order:

Contents:
Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS Environmental Services Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 9121-003 Red Hill BFSF The Environmental Company, Inc. (TEC) 1083866

## CASE NARRATIVE Print Date: 9/9/2008

Workorder No.: 1083866 Project Name: 9121-003 Red Hill BFSF Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID 

## Sample Comments

Sample Type Client Sample ID Refer to the sample receipt form for information on sample condition.

1083866002 AK102 - The pattern is consistent with a weathered gasoline.

PS RHMWA01-WG-12

1083866003 AK102 - The pattern is consistent with a weathered gasoline.

PS RHMW02-WG-12

1083866006 AK101 - BMS recovery for GRO does not meet QC goals. The associated LCS/LCSD meet all QC goals.

BMS RHMW2254-WG-12 MS

1083866007 AK101 - BMS/BMSD recoveries do not meet RPD goals. The associated LCS/LCSD meet all QC goals.

BMSD RHMW2254-WG-12 MSD

847977 8260B - Initial calibration verification (ICV) recovery for several analytes did not meet QC goals (biased high). These

analytes were not detected above the PQL in the associated samples. CCV CCV for HBN 204112 [VMS/9995]

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# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1083866

Certification:
I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1001 Bishop Street Ste 1400 ASB Tower Honolulu, HI 96813
Attn: Jeff Hart T: (808)528-1445 F:(808)528-0768 jshart@tecinc.com

Barbara Hager Barbara.Hager@sgs.com Project Manager 

### 9121-003 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

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. 5301 w w w . us. sgs.com M em ber of S G S G roupEnclosed are the analytical results associated with this workorder.
As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request.
The laboratory certification numbers are AK971-05 (DW), UST-005 (CS) and AK00971 (Micro) for ADEC and 001992 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A,7471A,9040B,9045C, 9056, 9060, 9065, 8015B, 8021B, 8081A/8082, 8260B, 8270C).
Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.
If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 907-562-2343.

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit PQL Practical Quantitation Limit (reporting limit). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indicates value that is greater than or equal to the MDL. J The quantitation is an estimation. ND Indicates the analyte is not detected B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits. D The analyte concentration is the result of dilution. GT Greater Than LT Less Than Q QC parameter out of acceptance range. M A matrix effect was present. E The analyte result is above the calibrated range. R Rejected DF Analytical Dilution Factor JL The analyte was positively identified, but the quantitation is a low estimation. <Surr> Surrogate QC spiked standard <Surr/IS> Surrogate / Internal Standard QC spiked standard QC Quality Control QA Quality Assurance MB Method Blank LCS (D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) BMS(D) Site Specific Matrix Spike RPD Relative Percent Difference ICV Initial Calibration Verification CCV Continuous Calibration Verification MSA Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified Print Date: 9/9/2008

Notes: All DRO/RRO analysese are integrated per SOP.

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## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 9121-003 Red Hill BFSF Workorder No.: 1083866 

## Analytical Methods

Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS AFCEE 3.1 8260 (W) SW8260B Dissolved Metals by ICP-MS SW6020 DRO by 8015B (W) SW8015C GRO (W) SW8015C Print Date: 9/9/2008



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1083866001 RHMW03-WG-12
1083866002 RHMWA01-WG-12
1083866003 RHMW02-WG-12
1083866004 RHMW01-WG-12
1083866005 RHMW2254-WG-12
1083866006 RHMW2254-WG-12 MS
1083866007 RHMW2254-WG-12 MSD
1083866008 TB01

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage Alaska 99518 t ( 907 ) 562

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### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW03-WG-12 SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5551 MXX20608 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5551 Analytical Method: SW6020 Analysis Date/Time: 08/05/08 19:24 Prep Batch: MXX20608 Prep Method: SW3010A Prep Date/Time: 08/04/08 16:00 Container ID:1083866001-G Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

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### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW03-WG-12 SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 ug/L VFC9090 VXX18484 10.0 1 4-Bromofluorobenzene <surr> 105 50-150 % VFC9090 VXX18484 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9090 Analytical Method: SW8015C Analysis Date/Time: 08/05/08 11:15 Prep Batch: VXX18484 Prep Method: SW5030B Prep Date/Time: 08/05/08 10:00 Container ID:1083866001-A Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

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### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW03-WG-12 SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.199 J 0.412 mg/L XFC8106 XXX19765 0.0825 1 5a Androstane <surr> 98 50-150 % XFC8106 XXX19765 1

Batch Information Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8106 Analytical Method: SW8015C Analysis Date/Time: 08/11/08 16:31 Prep Batch: XXX19765 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:40 Container ID:1083866001-J Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW03-WG-12 SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS9995 VXX18532 0.120 1 Toluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Ethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Styrene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromomethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Acetone ND 10.0 ug/L VMS9995 VXX18532 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS9995 VXX18532 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS9995 VXX18532 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 Chloroform ND 1.00 ug/L VMS9995 VXX18532 0.300 1 Bromobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromomethane ND 3.00 ug/L VMS9995 VXX18532 0.940 1 Bromochloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Vinyl chloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW03-WG-12 SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 Methylene chloride ND 5.00 ug/L VMS9995 VXX18532 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 P & M -Xylene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Naphthalene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 o-Xylene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromoform ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Trichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS9995 VXX18532 1 Toluene-d8 <surr> 100 80-120 % VMS9995 VXX18532 1 4-Bromofluorobenzene <surr> 99.6 76-120 % VMS9995 VXX18532 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS9995 Analytical Method: SW8260B Analysis Date/Time: 08/09/08 13:16 Prep Batch: VXX18532 Prep Method: SW5030B Prep Date/Time: 08/09/08 05:28 Container ID:1083866001-D Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW03-WG-12 SGS Ref. #: 1083866001 Collection Date/Time: 07/29/08 11:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Acenaphthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Fluorene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Phenanthrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Anthracene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Fluoranthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Pyrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo(a)Anthracene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Chrysene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[b]Fluoranthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[k]fluoranthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[a]pyrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Indeno[1,2,3-c,d] pyrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Dibenzo[a,h]anthracene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[g,h,i]perylene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Naphthalene 0.0689 J 0.104 ug/L XMS4671 XXX19761 0.0323 1 1-Methylnaphthalene 0.0294 J 0.0521 ug/L XMS4671 XXX19761 0.0156 1 2-Methylnaphthalene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Terphenyl-d14 <surr> 89.9 50-135 % XMS4671 XXX19761 1

Batch Information Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4671 Analytical Method: 8270D SIMS Analysis Date/Time: 08/26/08 14:25 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866001-H Dilution Factor: 1 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5551 MXX20608 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5551 Analytical Method: SW6020 Analysis Date/Time: 08/05/08 19:31 Prep Batch: MXX20608 Prep Method: SW3010A Prep Date/Time: 08/04/08 16:00 Container ID:1083866002-G Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics 61.2 J 100 ug/L VFC9090 VXX18484 10.0 1 4-Bromofluorobenzene <surr> 142 50-150 % VFC9090 VXX18484 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9090 Analytical Method: SW8015C Analysis Date/Time: 08/05/08 11:33 Prep Batch: VXX18484 Prep Method: SW5030B Prep Date/Time: 08/05/08 10:00 Container ID:1083866002-A Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 3.64 0.400 mg/L XFC8106 XXX19765 0.0800 1 5a Androstane <surr> 83.3 50-150 % XFC8106 XXX19765 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8106 Analytical Method: SW8015C Analysis Date/Time: 08/11/08 16:41 Prep Batch: XXX19765 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:40 Container ID:1083866002-J Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene 0.120 J 0.400 ug/L VMS9995 VXX18532 0.120 1 Toluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Ethylbenzene 0.560 J 1.00 ug/L VMS9995 VXX18532 0.310 1 n-Butylbenzene 9.10 1.00 ug/L VMS9995 VXX18532 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 n-Propylbenzene 12.1 1.00 ug/L VMS9995 VXX18532 0.310 1 Styrene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromomethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Acetone ND 10.0 ug/L VMS9995 VXX18532 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS9995 VXX18532 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS9995 VXX18532 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 Chloroform ND 1.00 ug/L VMS9995 VXX18532 0.300 1 Bromobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromomethane ND 3.00 ug/L VMS9995 VXX18532 0.940 1 Bromochloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Vinyl chloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 sec-Butylbenzene 8.34 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 Methylene chloride ND 5.00 ug/L VMS9995 VXX18532 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 P & M -Xylene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Naphthalene 309 20.0 ug/L VMS10000 VXX18539 6.20 10 o-Xylene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromoform ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 tert-Butylbenzene 1.33 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Trichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Isopropylbenzene (Cumene) 7.24 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS9995 VXX18532 1 Toluene-d8 <surr> 99.4 80-120 % VMS9995 VXX18532 1 4-Bromofluorobenzene <surr> 92.1 76-120 % VMS9995 VXX18532 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10000 Analytical Method: SW8260B Analysis Date/Time: 08/11/08 19:33 Prep Batch: VXX18539 Prep Method: SW5030B Prep Date/Time: 08/11/08 15:11 Container ID:1083866002-E Dilution Factor: 10 Analyst: DSH Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS9995 Analytical Method: SW8260B Analysis Date/Time: 08/09/08 13:50 Prep Batch: VXX18532 Prep Method: SW5030B Prep Date/Time: 08/09/08 05:28 Container ID:1083866002-D Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMWA01-WG-12 SGS Ref. #: 1083866002 Collection Date/Time: 07/29/08 12:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Acenaphthene 0.450 J 0.515 ug/L XMS4677 XXX19761 0.155 10 Fluorene 0.304 J 0.515 ug/L XMS4677 XXX19761 0.155 10 Phenanthrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Anthracene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Fluoranthene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Pyrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo(a)Anthracene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Chrysene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[b]Fluoranthene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[k]fluoranthene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[a]pyrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Indeno[1,2,3-c,d] pyrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Dibenzo[a,h]anthracene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[g,h,i]perylene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Naphthalene 132 10.3 ug/L XMS4683 XXX19761 3.20 100 1-Methylnaphthalene 96.0 2.58 ug/L XMS4682 XXX19761 0.773 50 2-Methylnaphthalene 42.2 2.58 ug/L XMS4682 XXX19761 0.773 50 Terphenyl-d14 <surr> 78.7 50-135 % XMS4677 XXX19761 10

Batch Information Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4677 Analytical Method: 8270D SIMS Analysis Date/Time: 08/29/08 02:45 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866002-H Dilution Factor: 10 Analyst: JDH Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4682 Analytical Method: 8270D SIMS Analysis Date/Time: 09/04/08 04:46 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866002-H Dilution Factor: 50 Analyst: JDH Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4683 Analytical Method: 8270D SIMS Analysis Date/Time: 09/05/08 14:22 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866002-H Dilution Factor: 100 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5551 MXX20608 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5551 Analytical Method: SW6020 Analysis Date/Time: 08/05/08 20:06 Prep Batch: MXX20608 Prep Method: SW3010A Prep Date/Time: 08/04/08 16:00 Container ID:1083866003-G Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics 61.7 J 100 ug/L VFC9090 VXX18484 10.0 1 4-Bromofluorobenzene <surr> 145 50-150 % VFC9090 VXX18484 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9090 Analytical Method: SW8015C Analysis Date/Time: 08/05/08 11:51 Prep Batch: VXX18484 Prep Method: SW5030B Prep Date/Time: 08/05/08 10:00 Container ID:1083866003-A Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 4.47 0.417 mg/L XFC8106 XXX19765 0.0833 1 5a Androstane <surr> 94.2 50-150 % XFC8106 XXX19765 1

Batch Information Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8106 Analytical Method: SW8015C Analysis Date/Time: 08/11/08 16:50 Prep Batch: XXX19765 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:40 Container ID:1083866003-J Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS9995 VXX18532 0.120 1 Toluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Ethylbenzene 0.580 J 1.00 ug/L VMS9995 VXX18532 0.310 1 n-Butylbenzene 9.52 1.00 ug/L VMS9995 VXX18532 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 n-Propylbenzene 12.3 1.00 ug/L VMS9995 VXX18532 0.310 1 Styrene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromomethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Acetone ND 10.0 ug/L VMS9995 VXX18532 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS9995 VXX18532 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS9995 VXX18532 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 Chloroform ND 1.00 ug/L VMS9995 VXX18532 0.300 1 Bromobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromomethane ND 3.00 ug/L VMS9995 VXX18532 0.940 1 Bromochloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Vinyl chloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 sec-Butylbenzene 8.55 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 Methylene chloride ND 5.00 ug/L VMS9995 VXX18532 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 P & M -Xylene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Naphthalene 320 20.0 ug/L VMS10000 VXX18539 6.20 10 o-Xylene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromoform ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 tert-Butylbenzene 1.31 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Trichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Isopropylbenzene (Cumene) 7.22 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloroethane-D4 <surr> 102 73-120 % VMS9995 VXX18532 1 Toluene-d8 <surr> 99 80-120 % VMS9995 VXX18532 1 4-Bromofluorobenzene <surr> 90.9 76-120 % VMS9995 VXX18532 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10000 Analytical Method: SW8260B Analysis Date/Time: 08/11/08 20:07 Prep Batch: VXX18539 Prep Method: SW5030B Prep Date/Time: 08/11/08 15:11 Container ID:1083866003-E Dilution Factor: 10 Analyst: DSH Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS9995 Analytical Method: SW8260B Analysis Date/Time: 08/09/08 14:24 Prep Batch: VXX18532 Prep Method: SW5030B Prep Date/Time: 08/09/08 05:28 Container ID:1083866003-D Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW02-WG-12 SGS Ref. #: 1083866003 Collection Date/Time: 07/29/08 12:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Acenaphthene 0.470 J 0.515 ug/L XMS4677 XXX19761 0.155 10 Fluorene 0.324 J 0.515 ug/L XMS4677 XXX19761 0.155 10 Phenanthrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Anthracene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Fluoranthene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Pyrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo(a)Anthracene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Chrysene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[b]Fluoranthene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[k]fluoranthene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[a]pyrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Indeno[1,2,3-c,d] pyrene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Dibenzo[a,h]anthracene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Benzo[g,h,i]perylene ND 0.515 ug/L XMS4677 XXX19761 0.155 10 Naphthalene 140 10.3 ug/L XMS4683 XXX19761 3.20 100 1-Methylnaphthalene 102 2.58 ug/L XMS4682 XXX19761 0.773 50 2-Methylnaphthalene 31.5 2.58 ug/L XMS4682 XXX19761 0.773 50 Terphenyl-d14 <surr> 80.5 50-135 % XMS4677 XXX19761 10

Batch Information Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4677 Analytical Method: 8270D SIMS Analysis Date/Time: 08/29/08 03:18 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866003-H Dilution Factor: 10 Analyst: JDH Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4682 Analytical Method: 8270D SIMS Analysis Date/Time: 09/04/08 05:18 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866003-H Dilution Factor: 50 Analyst: JDH Initial Prep Wt./Vol.: 970 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4683 Analytical Method: 8270D SIMS Analysis Date/Time: 09/05/08 14:55 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866003-H Dilution Factor: 100 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5551 MXX20608 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5551 Analytical Method: SW6020 Analysis Date/Time: 08/05/08 20:13 Prep Batch: MXX20608 Prep Method: SW3010A Prep Date/Time: 08/04/08 16:00 Container ID:1083866004-G Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 ug/L VFC9090 VXX18484 10.0 1 4-Bromofluorobenzene <surr> 109 50-150 % VFC9090 VXX18484 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9090 Analytical Method: SW8015C Analysis Date/Time: 08/05/08 12:10 Prep Batch: VXX18484 Prep Method: SW5030B Prep Date/Time: 08/05/08 10:00 Container ID:1083866004-A Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics 0.327 J 0.400 mg/L XFC8106 XXX19765 0.0800 1 5a Androstane <surr> 94.7 50-150 % XFC8106 XXX19765 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8106 Analytical Method: SW8015C Analysis Date/Time: 08/11/08 16:59 Prep Batch: XXX19765 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:40 Container ID:1083866004-J Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS9995 VXX18532 0.120 1 Toluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Ethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Isopropyltoluene 0.400 J 1.00 ug/L VMS9995 VXX18532 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Styrene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromomethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Acetone ND 10.0 ug/L VMS9995 VXX18532 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS9995 VXX18532 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS9995 VXX18532 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 Chloroform ND 1.00 ug/L VMS9995 VXX18532 0.300 1 Bromobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromomethane ND 3.00 ug/L VMS9995 VXX18532 0.940 1 Bromochloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Vinyl chloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 Methylene chloride ND 5.00 ug/L VMS9995 VXX18532 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 P & M -Xylene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Naphthalene ND 2.00 ug/L VMS10000 VXX18539 0.620 1 o-Xylene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromoform ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Trichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS9995 VXX18532 1 Toluene-d8 <surr> 100 80-120 % VMS9995 VXX18532 1 4-Bromofluorobenzene <surr> 95.8 76-120 % VMS9995 VXX18532 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10000 Analytical Method: SW8260B Analysis Date/Time: 08/11/08 19:00 Prep Batch: VXX18539 Prep Method: SW5030B Prep Date/Time: 08/11/08 15:11 Container ID:1083866004-E Dilution Factor: 1 Analyst: DSH Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS9995 Analytical Method: SW8260B Analysis Date/Time: 08/09/08 14:58 Prep Batch: VXX18532 Prep Method: SW5030B Prep Date/Time: 08/09/08 05:28 Container ID:1083866004-D Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW01-WG-12 SGS Ref. #: 1083866004 Collection Date/Time: 07/29/08 14:30 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Acenaphthene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Fluorene 0.0206 J 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Phenanthrene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Anthracene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Fluoranthene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Pyrene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Benzo(a)Anthracene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Chrysene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Benzo[b]Fluoranthene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Benzo[k]fluoranthene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Benzo[a]pyrene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Dibenzo[a,h]anthracene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Benzo[g,h,i]perylene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Naphthalene 0.114 0.100 ug/L XMS4671 XXX19761 0.0310 1 1-Methylnaphthalene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 2-Methylnaphthalene ND 0.0500 ug/L XMS4671 XXX19761 0.0150 1 Terphenyl-d14 <surr> 84.9 50-135 % XMS4671 XXX19761 1

Batch Information Initial Prep Wt./Vol.: 1000 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4671 Analytical Method: 8270D SIMS Analysis Date/Time: 08/26/08 16:06 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866004-H Dilution Factor: 1 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW2254-WG-12 SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS5551 MXX20608 0.310 5

Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS5551 Analytical Method: SW6020 Analysis Date/Time: 08/05/08 17:30 Prep Batch: MXX20608 Prep Method: SW3010A Prep Date/Time: 08/04/08 16:00 Container ID:1083866005-G Dilution Factor: 5 Analyst: MH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW2254-WG-12 SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 ug/L VFC9090 VXX18484 10.0 1 4-Bromofluorobenzene <surr> 109 50-150 % VFC9090 VXX18484 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9090 Analytical Method: SW8015C Analysis Date/Time: 08/05/08 12:28 Prep Batch: VXX18484 Prep Method: SW5030B Prep Date/Time: 08/05/08 10:00 Container ID:1083866005-A Dilution Factor: 1 Analyst: HM

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW2254-WG-12 SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.417 mg/L XFC8106 XXX19765 0.0833 1 5a Androstane <surr> 94.1 50-150 % XFC8106 XXX19765 1

Batch Information Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8106 Analytical Method: SW8015C Analysis Date/Time: 08/11/08 17:09 Prep Batch: XXX19765 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:40 Container ID:1083866005-J Dilution Factor: 1 Analyst: HKG

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW2254-WG-12 SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS9995 VXX18532 0.120 1 Toluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Ethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Styrene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromomethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Acetone ND 10.0 ug/L VMS9995 VXX18532 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS9995 VXX18532 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS9995 VXX18532 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 Chloroform ND 1.00 ug/L VMS9995 VXX18532 0.300 1 Bromobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromomethane 1.26 J 3.00 ug/L VMS9995 VXX18532 0.940 1 Bromochloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Vinyl chloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW2254-WG-12 SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 Methylene chloride ND 5.00 ug/L VMS9995 VXX18532 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 P & M -Xylene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Naphthalene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 o-Xylene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromoform ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Trichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloroethane-D4 <surr> 102 73-120 % VMS9995 VXX18532 1 Toluene-d8 <surr> 99.2 80-120 % VMS9995 VXX18532 1 4-Bromofluorobenzene <surr> 100 76-120 % VMS9995 VXX18532 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS9995 Analytical Method: SW8260B Analysis Date/Time: 08/09/08 12:42 Prep Batch: VXX18532 Prep Method: SW5030B Prep Date/Time: 08/09/08 05:28 Container ID:1083866005-D Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### RHMW2254-WG-12 SGS Ref. #: 1083866005 Collection Date/Time: 07/29/08 09:45 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Acenaphthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Fluorene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Phenanthrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Anthracene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Fluoranthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Pyrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo(a)Anthracene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Chrysene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[b]Fluoranthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[k]fluoranthene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[a]pyrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Indeno[1,2,3-c,d] pyrene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Dibenzo[a,h]anthracene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Benzo[g,h,i]perylene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Naphthalene ND 0.104 ug/L XMS4671 XXX19761 0.0323 1 1-Methylnaphthalene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 2-Methylnaphthalene ND 0.0521 ug/L XMS4671 XXX19761 0.0156 1 Terphenyl-d14 <surr> 97 50-135 % XMS4671 XXX19761 1

Batch Information Initial Prep Wt./Vol.: 960 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS4671 Analytical Method: 8270D SIMS Analysis Date/Time: 08/26/08 16:39 Prep Batch: XXX19761 Prep Method: SW3520C Prep Date/Time: 08/05/08 09:15 Container ID:1083866005-H Dilution Factor: 1 Analyst: JDH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### TB01 SGS Ref. #: 1083866008 Collection Date/Time: 07/29/08 08:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS9995 VXX18532 0.120 1 Toluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Ethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chlorobenzene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS9995 VXX18532 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Styrene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromomethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Acetone ND 10.0 ug/L VMS9995 VXX18532 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS9995 VXX18532 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS9995 VXX18532 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 Chloroform ND 1.00 ug/L VMS9995 VXX18532 0.300 1 Bromobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Chloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromomethane 1.36 J 3.00 ug/L VMS9995 VXX18532 0.940 1 Bromochloromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Vinyl chloride ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 9/9/2008

Client Sample ID: 

### TB01 SGS Ref. #: 1083866008 Collection Date/Time: 07/29/08 08:05 Receipt Date/Time: 07/31/08 11:00 Project ID: 9121-003 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS9995 VXX18532 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS9995 VXX18532 3.10 1 Methylene chloride ND 5.00 ug/L VMS9995 VXX18532 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 P & M -Xylene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 Naphthalene ND 2.00 ug/L VMS9995 VXX18532 0.620 1 o-Xylene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Bromoform ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Trichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS9995 VXX18532 0.310 1 1,2-Dichloroethane-D4 <surr> 102 73-120 % VMS9995 VXX18532 1 Toluene-d8 <surr> 100 80-120 % VMS9995 VXX18532 1 4-Bromofluorobenzene <surr> 99.5 76-120 % VMS9995 VXX18532 1

Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS9995 Analytical Method: SW8260B Analysis Date/Time: 08/09/08 12:08 Prep Batch: VXX18532 Prep Method: SW5030B Prep Date/Time: 08/09/08 05:28 Container ID:1083866008-A Dilution Factor: 1 Analyst: DSH

S G S E nvironm ental S ervices Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518 t ( 907 ) 562

. 2343 f ( 907 ) 561

. 5301 w w w . us. sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 846324 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX20608 SW3010A 08/04/2008 QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Metals by ICP/MS



### Lead ND 1.00 ug/L 08/05/08 

### 0.310

Instrument Method Batch MMS5551

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 846350 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX19761 SW3520C 08/05/2008 QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Polynuclear Aromatics GC/MS


### Acenaphthylene ND 0.0500 ug/L 08/27/08 

### 0.0150 Acenaphthene ND 0.0500 ug/L 08/27/08 

### 0.0150 Fluorene ND 0.0500 ug/L 08/27/08 

### 0.0150 Phenanthrene ND 0.0500 ug/L 08/27/08 

### 0.0150 Anthracene ND 0.0500 ug/L 08/27/08 

### 0.0150 Fluoranthene ND 0.0500 ug/L 08/27/08 

### 0.0150 Pyrene ND 0.0500 ug/L 08/27/08 

### 0.0150 Benzo(a)Anthracene ND 0.0500 ug/L 08/27/08 

### 0.0150 Chrysene ND 0.0500 ug/L 08/27/08 

### 0.0150 Benzo[b]Fluoranthene ND 0.0500 ug/L 08/27/08 

### 0.0150 Benzo[k]fluoranthene ND 0.0500 ug/L 08/27/08 

### 0.0150 Benzo[a]pyrene ND 0.0500 ug/L 08/27/08 

### 0.0150 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L 08/27/08 

### 0.0150 Dibenzo[a,h]anthracene ND 0.0500 ug/L 08/27/08 

### 0.0150 Benzo[g,h,i]perylene ND 0.0500 ug/L 08/27/08 

### 0.0150 Naphthalene ND 0.100 ug/L 08/27/08 

### 0.0310 1-Methylnaphthalene ND 0.0500 ug/L 08/27/08 

### 0.0150 2-Methylnaphthalene ND 0.0500 ug/L 08/27/08 

### 0.0150
Surrogates 

### Terphenyl-d14 <surr> 122 50-135 % 08/27/08

Instrument Method Batch XMS4673

8270D SIMS HP 5890 Series II MS2 SVOAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 846380 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX19765 SW3520C 08/05/2008 QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results Reporting/Control Limit Units Analysis Date MDL



### Semivolatile Organic Fuels Department


### Diesel Range Organics ND 0.400 mg/L 08/11/08 

### 0.0800
Surrogates


### 5a Androstane <surr> 100 60-120 % 08/11/08

Instrument Method Batch XFC8106

SW8015C HP 5890 Series II FID SV D RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 846453 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18484 SW5030B 08/05/2008 QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter Results Reporting/Control Limit Units Analysis Date MDL



### Volatile Fuels Department


### Gasoline Range Organics ND 100 ug/L 08/05/08 

### 10.0
Surrogates


### 4-Bromofluorobenzene <surr> 99.4 50-150 % 08/05/08

Instrument Method Batch VFC9090

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 847971 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008 QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005, 1083866008

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 847971 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene ND 0.400 ug/L 08/09/08 

### 0.120 Toluene ND 1.00 ug/L 08/09/08 

### 0.310 Ethylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 n-Butylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 1,4-Dichlorobenzene ND 0.500 ug/L 08/09/08 

### 0.150 1,2-Dichloroethane ND 0.500 ug/L 08/09/08 

### 0.150 1,3,5-Trimethylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 4-Chlorotoluene ND 1.00 ug/L 08/09/08 

### 0.310 Chlorobenzene ND 0.500 ug/L 08/09/08 

### 0.150 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 08/09/08 

### 3.10 cis-1,2-Dichloroethene ND 1.00 ug/L 08/09/08 

### 0.310 4-Isopropyltoluene ND 1.00 ug/L 08/09/08 

### 0.310 cis-1,3-Dichloropropene ND 0.500 ug/L 08/09/08 

### 0.150 n-Propylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 Styrene ND 1.00 ug/L 08/09/08 

### 0.310 Dibromomethane ND 1.00 ug/L 08/09/08 

### 0.310 trans-1,3-Dichloropropene ND 1.00 ug/L 08/09/08 

### 0.310 1,2,4-Trichlorobenzene ND 1.00 ug/L 08/09/08 

### 0.310 Acetone ND 10.0 ug/L 08/09/08 

### 3.10 1,1,2,2-Tetrachloroethane ND 0.500 ug/L 08/09/08 

### 0.150 1,2-Dibromo-3-chloropropane ND 2.00 ug/L 08/09/08 

### 0.620 Methyl-t-butyl ether ND 5.00 ug/L 08/09/08 

### 1.50 Tetrachloroethene ND 1.00 ug/L 08/09/08 

### 0.310 Dibromochloromethane ND 0.500 ug/L 08/09/08 

### 0.150 1,3-Dichloropropane ND 0.400 ug/L 08/09/08 

### 0.120 1,2-Dibromoethane ND 1.00 ug/L 08/09/08 

### 0.310 Carbon tetrachloride ND 1.00 ug/L 08/09/08 

### 0.310 1,1,1,2-Tetrachloroethane ND 0.500 ug/L 08/09/08 

### 0.150 Chloroform ND 1.00 ug/L 08/09/08 

### 0.300 Bromobenzene ND 1.00 ug/L 08/09/08 

### 0.310 Chloromethane ND 1.00 ug/L 08/09/08 

### 0.310 1,2,3-Trichloropropane ND 1.00 ug/L 08/09/08 

### 0.310 Bromomethane ND 3.00 ug/L 08/09/08 

### 0.940 Bromochloromethane ND 1.00 ug/L 08/09/08 

### 0.310 Vinyl chloride ND 1.00 ug/L 08/09/08 

### 0.310 Dichlorodifluoromethane ND 1.00 ug/L 08/09/08 

### 0.310 Chloroethane ND 1.00 ug/L 08/09/08 

### 0.310 sec-Butylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 Bromodichloromethane ND 0.500 ug/L 08/09/08 

### 0.150Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 847971 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1-Dichloroethene ND 1.00 ug/L 08/09/08 

### 0.310 2-Butanone (MEK) ND 10.0 ug/L 08/09/08 

### 3.10 Methylene chloride ND 5.00 ug/L 08/09/08 

### 1.00 Trichlorofluoromethane ND 1.00 ug/L 08/09/08 

### 0.310 P & M -Xylene ND 2.00 ug/L 08/09/08 

### 0.620 Naphthalene ND 2.00 ug/L 08/09/08 

### 0.620 o-Xylene ND 1.00 ug/L 08/09/08 

### 0.310 Bromoform ND 1.00 ug/L 08/09/08 

### 0.310 1-Chlorohexane ND 1.00 ug/L 08/09/08 

### 0.310 1,2,4-Trimethylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 tert-Butylbenzene ND 1.00 ug/L 08/09/08 

### 0.310 1,1,1-Trichloroethane ND 1.00 ug/L 08/09/08 

### 0.310 1,1-Dichloroethane ND 1.00 ug/L 08/09/08 

### 0.310 2-Chlorotoluene ND 1.00 ug/L 08/09/08 

### 0.310 Trichloroethene ND 1.00 ug/L 08/09/08 

### 0.310 trans-1,2-Dichloroethene ND 1.00 ug/L 08/09/08 

### 0.310 1,2-Dichlorobenzene ND 1.00 ug/L 08/09/08 

### 0.310 2,2-Dichloropropane ND 1.00 ug/L 08/09/08 

### 0.310 Hexachlorobutadiene ND 1.00 ug/L 08/09/08 

### 0.310 Isopropylbenzene (Cumene) ND 1.00 ug/L 08/09/08 

### 0.310 1,2-Dichloropropane ND 1.00 ug/L 08/09/08 

### 0.310 1,1-Dichloropropene ND 1.00 ug/L 08/09/08 

### 0.310 1,1,2-Trichloroethane ND 1.00 ug/L 08/09/08 

### 0.310 1,3-Dichlorobenzene ND 1.00 ug/L 08/09/08 

### 0.310 1,2,3-Trichlorobenzene ND 1.00 ug/L 08/09/08 

### 0.310
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 102 73-120 % 08/09/08 

### Toluene-d8 <surr> 101 80-120 % 08/09/08 

### 4-Bromofluorobenzene <surr> 97.4 76-120 % 08/09/08

Instrument Method Batch VMS9995

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Prep 

### 848185 Method Blank The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18539 SW5030B 08/11/2008 QC results affect the following production samples: 

### 1083866002, 1083866003, 1083866004

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy


### Naphthalene ND 2.00 ug/L 08/11/08 

### 0.620
Surrogates 

### 1,2-Dichloroethane-D4 <surr> 108 73-120 % 08/11/08 

### Toluene-d8 <surr> 102 80-120 % 08/11/08

Instrument Method Batch VMS10000

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 846325 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) MXX20608 SW3010A 08/04/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS



### Lead LCS 1080 108 ( 80-120 ) 1000 ug/L 08/05/2008

Batch Method Instrument 

### MMS5551

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 846351 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX19761 SW3520C 08/05/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MSMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 846351 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX19761 SW3520C 08/05/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Acenaphthylene LCS 0.315 63 ( 50-105 ) 0.5 ug/L 08/26/2008
Acenaphthene LCS 0.317 63 ( 45-110 ) 0.5 ug/L 08/26/2008

Fluorene LCS 0.324 65 ( 50-110 ) 0.5 ug/L 08/26/2008

Phenanthrene LCS 0.334 67 ( 50-115 ) 0.5 ug/L 08/26/2008

Anthracene LCS 0.327 66 ( 55-110 ) 0.5 ug/L 08/26/2008

Fluoranthene LCS 0.378 76 ( 55-125 ) 0.5 ug/L 08/26/2008

Pyrene LCS 0.365 73 ( 50-130 ) 0.5 ug/L 08/26/2008
Benzo(a)Anthracene LCS 0.399 80 ( 55-120 ) 0.5 ug/L 08/26/2008
Chrysene LCS 0.368 74 ( 55-120 ) 0.5 ug/L 08/26/2008
Benzo[b]Fluoranthene LCS 0.380 76 ( 46-130 ) 0.5 ug/L 08/26/2008
Benzo[k]fluoranthene LCS 0.381 76 ( 60-125 ) 0.5 ug/L 08/26/2008
Benzo[a]pyrene LCS 0.423 85 ( 55-120 ) 0.5 ug/L 08/26/2008
Indeno[1,2,3-c,d] pyrene LCS 0.393 79 ( 45-125 ) 0.5 ug/L 08/26/2008
Dibenzo[a,h]anthracene LCS 0.405 81 ( 41-140 ) 0.5 ug/L 08/26/2008
Benzo[g,h,i]perylene LCS 0.391 78 ( 46-125 ) 0.5 ug/L 08/26/2008
Naphthalene LCS 0.344 69 ( 42-100 ) 0.5 ug/L 08/26/2008
1-Methylnaphthalene LCS 0.328 66 ( 46-115 ) 0.5 ug/L 08/26/2008
2-Methylnaphthalene LCS 0.311 62 ( 45-105 ) 0.5 ug/L 08/26/2008

Surrogates 

### Terphenyl-d14 <surr> LCS 120 ( 50-135 ) 08/26/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 846351 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX19761 SW3520C 08/05/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS4671

8270D SIMS HP 5890 Series II MS2 SVOAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 846381 Lab Control Sample 846382 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) XXX19765 SW3520C 08/05/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.61 92 ( 75-125 ) 5 mg/L 08/11/2008 LCSD 4.97 99 8 (< 20 ) 5 mg/L 08/11/2008

Surrogates 

### 5a Androstane <surr> LCS 106 ( 60-120 ) 08/11/2008 LCSD 117 9 08/11/2008

Batch Method Instrument 

### XFC8106

SW8015C HP 5890 Series II FID SV D RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 846454 Lab Control Sample 846455 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18484 SW5030B 08/05/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits



### Volatile Fuels Department 

### Gasoline Range Organics LCS 191 95 ( 79-108 ) 200 ug/L 08/05/2008 LCSD 192 96 1 (< 20 ) 200 ug/L 08/05/2008

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 109 ( 50-150 ) 08/05/2008 LCSD 110 1 08/05/2008

Batch Method Instrument 

### VFC9090

SW8015C HP 5890 Series II PID+FID VCAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 847972 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005, 1083866008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 847972 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene LCS 28.4 95 ( 80-120 ) 30 ug/L 08/09/2008

Toluene LCS 29.2 97 ( 77-120 ) 30 ug/L 08/09/2008
Ethylbenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 08/09/2008
n-Butylbenzene LCS 27.6 92 ( 80-124 ) 30 ug/L 08/09/2008

1,4-Dichlorobenzene LCS 30.8 103 ( 80-120 ) 30 ug/L 08/09/2008

1,2-Dichloroethane LCS 31.9 106 ( 80-129 ) 30 ug/L 08/09/2008
1,3,5-Trimethylbenzene LCS 29.1 97 ( 80-128 ) 30 ug/L 08/09/2008

4-Chlorotoluene LCS 28.3 94 ( 79-128 ) 30 ug/L 08/09/2008

Chlorobenzene LCS 31.7 106 ( 80-120 ) 30 ug/L 08/09/2008
4-Methyl-2-pentanone (MIBK) LCS 91.0 101 ( 69-134 ) 90 ug/L 08/09/2008

cis-1,2-Dichloroethene LCS 30.2 101 ( 80-125 ) 30 ug/L 08/09/2008
4-Isopropyltoluene LCS 29.1 97 ( 80-125 ) 30 ug/L 08/09/2008
cis-1,3-Dichloropropene LCS 25.6 85 ( 80-120 ) 30 ug/L 08/09/2008
n-Propylbenzene LCS 29.9 100 ( 80-129 ) 30 ug/L 08/09/2008
Styrene LCS 31.8 106 ( 80-120 ) 30 ug/L 08/09/2008

Dibromomethane LCS 31.6 105 ( 80-120 ) 30 ug/L 08/09/2008
trans-1,3-Dichloropropene LCS 27.4 91 ( 80-124 ) 30 ug/L 08/09/2008

1,2,4-Trichlorobenzene LCS 30.6 102 ( 80-120 ) 30 ug/L 08/09/2008

Acetone LCS 81.6 91 ( 50-135 ) 90 ug/L 08/09/2008

1,1,2,2-Tetrachloroethane LCS 29.8 99 ( 76-123 ) 30 ug/L 08/09/2008
1,2-Dibromo-3-chloropropane LCS 26.9 90 ( 73-130 ) 30 ug/L 08/09/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 847972 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Methyl-t-butyl ether LCS 40.9 91 ( 80-120 ) 45 ug/L 08/09/2008

Tetrachloroethene LCS 30.6 102 ( 79-122 ) 30 ug/L 08/09/2008

Dibromochloromethane LCS 30.5 102 ( 80-120 ) 30 ug/L 08/09/2008
1,3-Dichloropropane LCS 29.2 97 ( 80-121 ) 30 ug/L 08/09/2008

1,2-Dibromoethane LCS 31.7 106 ( 80-120 ) 30 ug/L 08/09/2008

Carbon tetrachloride LCS 29.0 97 ( 80-126 ) 30 ug/L 08/09/2008

1,1,1,2-Tetrachloroethane LCS 30.4 101 ( 80-120 ) 30 ug/L 08/09/2008

Chloroform LCS 30.7 102 ( 80-124 ) 30 ug/L 08/09/2008

Bromobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 08/09/2008

Chloromethane LCS 26.4 88 ( 67-125 ) 30 ug/L 08/09/2008
1,2,3-Trichloropropane LCS 29.4 98 ( 80-120 ) 30 ug/L 08/09/2008

Bromomethane LCS 26.2 87 ( 30-140 ) 30 ug/L 08/09/2008

Bromochloromethane LCS 31.9 106 ( 77-129 ) 30 ug/L 08/09/2008
Vinyl chloride LCS 26.5 88 ( 72-145 ) 30 ug/L 08/09/2008

Dichlorodifluoromethane LCS 24.8 83 ( 62-153 ) 30 ug/L 08/09/2008

Chloroethane LCS 26.0 87 ( 67-133 ) 30 ug/L 08/09/2008
sec-Butylbenzene LCS 29.3 98 ( 80-120 ) 30 ug/L 08/09/2008

Bromodichloromethane LCS 28.9 96 ( 80-120 ) 30 ug/L 08/09/2008

1,1-Dichloroethene LCS 29.9 100 ( 76-130 ) 30 ug/L 08/09/2008
2-Butanone (MEK) LCS 87.7 97 ( 66-136 ) 90 ug/L 08/09/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 847972 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Methylene chloride LCS 28.7 96 ( 63-131 ) 30 ug/L 08/09/2008

Trichlorofluoromethane LCS 31.6 105 ( 68-145 ) 30 ug/L 08/09/2008
P & M -Xylene LCS 61.9 103 ( 80-120 ) 60 ug/L 08/09/2008
Naphthalene LCS 30.2 101 ( 75-120 ) 30 ug/L 08/09/2008
o-Xylene LCS 31.4 105 ( 80-120 ) 30 ug/L 08/09/2008

Bromoform LCS 31.8 106 ( 80-120 ) 30 ug/L 08/09/2008

1-Chlorohexane LCS 40.8 91 ( 70-125 ) 45 ug/L 08/09/2008
1,2,4-Trimethylbenzene LCS 29.8 99 ( 80-125 ) 30 ug/L 08/09/2008
tert-Butylbenzene LCS 28.8 96 ( 80-122 ) 30 ug/L 08/09/2008

1,1,1-Trichloroethane LCS 27.8 93 ( 80-122 ) 30 ug/L 08/09/2008

1,1-Dichloroethane LCS 29.6 99 ( 80-120 ) 30 ug/L 08/09/2008

2-Chlorotoluene LCS 28.4 95 ( 80-125 ) 30 ug/L 08/09/2008

Trichloroethene LCS 30.0 100 ( 80-125 ) 30 ug/L 08/09/2008

trans-1,2-Dichloroethene LCS 28.7 96 ( 79-132 ) 30 ug/L 08/09/2008

1,2-Dichlorobenzene LCS 30.7 102 ( 80-120 ) 30 ug/L 08/09/2008
2,2-Dichloropropane LCS 27.3 91 ( 80-132 ) 30 ug/L 08/09/2008

Hexachlorobutadiene LCS 28.5 95 ( 77-125 ) 30 ug/L 08/09/2008
Isopropylbenzene (Cumene) LCS 31.3 104 ( 80-121 ) 30 ug/L 08/09/2008
1,2-Dichloropropane LCS 30.2 101 ( 80-121 ) 30 ug/L 08/09/2008
1,1-Dichloropropene LCS 28.9 96 ( 80-122 ) 30 ug/L 08/09/2008

1,1,2-Trichloroethane LCS 29.2 97 ( 77-120 ) 30 ug/L 08/09/2008Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 847972 Lab Control Sample

The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18532 SW5030B 08/09/2008

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,3-Dichlorobenzene LCS 30.4 101 ( 80-120 ) 30 ug/L 08/09/2008

1,2,3-Trichlorobenzene LCS 31.8 106 ( 77-120 ) 30 ug/L 08/09/2008

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 103 ( 73-120 ) 08/09/2008

Toluene-d8 <surr> LCS 99 ( 80-120 ) 08/09/2008

4-Bromofluorobenzene <surr> LCS 91 ( 76-120 ) 08/09/2008

Batch Method Instrument 

### VMS9995

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 09/09/2008 8:32
Batch Method Date Prep 

### 848186 Lab Control Sample 848187 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 9121-003 Red Hill BFSF Water (Surface, Eff., Ground) VXX18539 SW5030B 08/11/2008

QC results affect the following production samples: 

### 1083866002, 1083866003, 1083866004

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Naphthalene LCS 32.7 109 ( 75-120 ) 30 ug/L 08/11/2008 LCSD 32.9 110 1 (< 20 ) 30 ug/L 08/11/2008

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 106 ( 73-120 ) 08/11/2008 LCSD 103 3 08/11/2008

Toluene-d8 <surr> LCS 100 ( 80-120 ) 08/11/2008 LCSD 99 0 08/11/2008

4-Bromofluorobenzene <surr> LCS 90 ( 76-120 ) 08/11/2008 LCSD 94 4 08/11/2008

Batch Method Instrument 

### VMS10000

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 846326 Matrix Spike 846327 Matrix Spike Duplicate

1083829004 Water (Surface, Eff., Ground) MXX20608 3010 H20 Digest for Metals ICP-MS 08/04/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Metals by ICP/MS


### Lead MS 128 1210 108 ( 80-120 ) 1000 ug/L 08/05/2008 MSD 1180 105 2 (< 15 ) 1000 ug/L 08/05/2008

Batch Method Instrument 

### MMS5551

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 846328 Bench Spike DIGESTED

1083829004 Water (Surface, Eff., Ground) MXX20608 3010 H20 Digest for Metals ICP-MS 08/04/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Metals by ICP/MS


### Lead BND 128 1440 105 ( 75-125 ) 1250 ug/L 08/05/2008

Batch Method Instrument 

### MMS5551

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 846397 Bench Spike DIGESTED

1083866005 Water (Surface, Eff., Ground) MXX20608 3010 H20 Digest for Metals ICP-MS 08/04/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Metals by ICP/MS


### Lead BND ND 1200 96 ( 75-125 ) 1250 ug/L 08/05/2008

Batch Method Instrument 

### MMS5551

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 847974 Matrix Spike 847975 Matrix Spike Duplicate

847973 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

QC results affect the following production samples: 

### 1083866001, 1083866002, 1083866003, 1083866004, 1083866005, 1083866008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 847974 Matrix Spike 847975 Matrix Spike Duplicate

847973 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene MS ND 31.1 104 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 28.0 93 10 (< 20 ) 30.0 ug/L 08/09/2008 Toluene MS ND 31.8 106 ( 77-120 ) 30.0 ug/L 08/09/2008 MSD 29.5 98 7 (< 20 ) 30.0 ug/L 08/09/2008 Ethylbenzene MS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 30.1 100 9 (< 20 ) 30.0 ug/L 08/09/2008 n-Butylbenzene MS ND 29.8 99 ( 80-124 ) 30.0 ug/L 08/09/2008 MSD 26.9 90 10 (< 20 ) 30.0 ug/L 08/09/2008 1,4-Dichlorobenzene MS ND 34 113 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 31.0 103 9 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dichloroethane MS ND 34.1 114 ( 80-129 ) 30.0 ug/L 08/09/2008 MSD 31.6 105 8 (< 20 ) 30.0 ug/L 08/09/2008 1,3,5-Trimethylbenzene MS ND 31.6 105 ( 80-128 ) 30.0 ug/L 08/09/2008 MSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008 4-Chlorotoluene MS ND 30.9 103 ( 79-128 ) 30.0 ug/L 08/09/2008 MSD 28.6 96 8 (< 20 ) 30.0 ug/L 08/09/2008 Chlorobenzene MS ND 33.9 113 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 31.3 104 8 (< 20 ) 30.0 ug/L 08/09/2008 4-Methyl-2-pentanone (MIBK) MS ND 100 111 ( 69-134 ) 90.0 ug/L 08/09/2008 MSD 93.7 104 7 (< 20 ) 90.0 ug/L 08/09/2008 cis-1,2-Dichloroethene MS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008 MSD 30.4 101 7 (< 20 ) 30.0 ug/L 08/09/2008 4-Isopropyltoluene MS ND 31.3 104 ( 80-125 ) 30.0 ug/L 08/09/2008 MSD 28.7 96 9 (< 20 ) 30.0 ug/L 08/09/2008 cis-1,3-Dichloropropene MS ND 28.3 94 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 26.4 88 7 (< 20 ) 30.0 ug/L 08/09/2008 n-Propylbenzene MS ND 32.2 107 ( 80-129 ) 30.0 ug/L 08/09/2008 MSD 29.7 99 8 (< 20 ) 30.0 ug/L 08/09/2008 Styrene MS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 30.6 102 8 (< 20 ) 30.0 ug/L 08/09/2008 Dibromomethane MS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 31.5 105 6 (< 20 ) 30.0 ug/L 08/09/2008 trans-1,3-Dichloropropene MS ND 30 100 ( 80-124 ) 30.0 ug/L 08/09/2008 MSD 28.7 96 5 (< 20 ) 30.0 ug/L 08/09/2008 1,2,4-Trichlorobenzene MS ND 33.4 111 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 30.1 100 10 (< 20 ) 30.0 ug/L 08/09/2008 Acetone MS ND 90.6 101 ( 50-135 ) 90.0 ug/L 08/09/2008 MSD 80.2 89 12 (< 20 ) 90.0 ug/L 08/09/2008 1,1,2,2-Tetrachloroethane MS ND 32.1 107 ( 76-123 ) 30.0 ug/L 08/09/2008 MSD 30.6 102 5 (< 20 ) 30.0 ug/L 08/09/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 847974 Matrix Spike 847975 Matrix Spike Duplicate

847973 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,2-Dibromo-3-chloropropane MS ND 32 107 ( 73-130 ) 30.0 ug/L 08/09/2008 MSD 27.7 93 14 (< 20 ) 30.0 ug/L 08/09/2008 Methyl-t-butyl ether MS ND 44.8 99 ( 80-120 ) 45.0 ug/L 08/09/2008 MSD 41.6 93 7 (< 20 ) 45.0 ug/L 08/09/2008 Tetrachloroethene MS ND 33.3 111 ( 79-122 ) 30.0 ug/L 08/09/2008 MSD 30.7 102 8 (< 20 ) 30.0 ug/L 08/09/2008 Dibromochloromethane MS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 32.8 109 2 (< 20 ) 30.0 ug/L 08/09/2008 1,3-Dichloropropane MS ND 31.1 104 ( 80-121 ) 30.0 ug/L 08/09/2008 MSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dibromoethane MS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 29.4 98 13 (< 20 ) 30.0 ug/L 08/09/2008 Carbon tetrachloride MS ND 32.4 108 ( 80-126 ) 30.0 ug/L 08/09/2008 MSD 31.9 106 2 (< 20 ) 30.0 ug/L 08/09/2008 1,1,1,2-Tetrachloroethane MS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 31.9 106 3 (< 20 ) 30.0 ug/L 08/09/2008 Chloroform MS ND 33.8 113 ( 80-124 ) 30.0 ug/L 08/09/2008 MSD 30.5 102 10 (< 20 ) 30.0 ug/L 08/09/2008 Bromobenzene MS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 30.3 101 8 (< 20 ) 30.0 ug/L 08/09/2008 Chloromethane MS ND 30 100 ( 67-125 ) 30.0 ug/L 08/09/2008 MSD 27.4 91 9 (< 20 ) 30.0 ug/L 08/09/2008 1,2,3-Trichloropropane MS ND 30.7 102 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 29.3 98 5 (< 20 ) 30.0 ug/L 08/09/2008 Bromomethane MS 1.26 J 29.1 93 ( 30-140 ) 30.0 ug/L 08/09/2008 MSD 27.4 87 6 (< 20 ) 30.0 ug/L 08/09/2008 Bromochloromethane MS ND 34.5 115 ( 77-129 ) 30.0 ug/L 08/09/2008 MSD 32.0 107 8 (< 20 ) 30.0 ug/L 08/09/2008 Vinyl chloride MS ND 29.7 99 ( 72-145 ) 30.0 ug/L 08/09/2008 MSD 27.2 91 9 (< 20 ) 30.0 ug/L 08/09/2008 Dichlorodifluoromethane MS ND 28.4 95 ( 62-153 ) 30.0 ug/L 08/09/2008 MSD 25.3 84 12 (< 20 ) 30.0 ug/L 08/09/2008 Chloroethane MS ND 27.7 93 ( 67-133 ) 30.0 ug/L 08/09/2008 MSD 24.4 81 13 (< 20 ) 30.0 ug/L 08/09/2008 sec-Butylbenzene MS ND 30.8 103 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 28.5 95 8 (< 20 ) 30.0 ug/L 08/09/2008 Bromodichloromethane MS ND 30.9 103 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008 1,1-Dichloroethene MS ND 32.6 109 ( 76-130 ) 30.0 ug/L 08/09/2008 MSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 847974 Matrix Spike 847975 Matrix Spike Duplicate

847973 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) MS ND 97.5 108 ( 66-136 ) 90.0 ug/L 08/09/2008 MSD 89.6 100 9 (< 20 ) 90.0 ug/L 08/09/2008 Methylene chloride MS ND 31 103 ( 63-131 ) 30.0 ug/L 08/09/2008 MSD 28.5 95 9 (< 20 ) 30.0 ug/L 08/09/2008 Trichlorofluoromethane MS ND 34.1 114 ( 68-145 ) 30.0 ug/L 08/09/2008 MSD 30.2 101 12 (< 20 ) 30.0 ug/L 08/09/2008 P & M -Xylene MS ND 66.9 112 ( 80-120 ) 60.0 ug/L 08/09/2008 MSD 61.8 103 8 (< 20 ) 60.0 ug/L 08/09/2008 Naphthalene MS ND 33.4 111 ( 75-120 ) 30.0 ug/L 08/09/2008 MSD 30.7 102 9 (< 20 ) 30.0 ug/L 08/09/2008 o-Xylene MS ND 33.3 111 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 31.4 105 6 (< 20 ) 30.0 ug/L 08/09/2008 Bromoform MS ND 34.4 115 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 34.5 115 0 (< 20 ) 30.0 ug/L 08/09/2008 1-Chlorohexane MS ND 44.2 98 ( 70-125 ) 45.0 ug/L 08/09/2008 MSD 40.2 89 10 (< 20 ) 45.0 ug/L 08/09/2008 1,2,4-Trimethylbenzene MS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008 MSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008 tert-Butylbenzene MS ND 31 103 ( 80-122 ) 30.0 ug/L 08/09/2008 MSD 28.6 95 8 (< 20 ) 30.0 ug/L 08/09/2008 1,1,1-Trichloroethane MS ND 30.7 102 ( 80-122 ) 30.0 ug/L 08/09/2008 MSD 28.8 96 7 (< 20 ) 30.0 ug/L 08/09/2008 1,1-Dichloroethane MS ND 32.3 108 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 29.4 98 9 (< 20 ) 30.0 ug/L 08/09/2008 2-Chlorotoluene MS ND 30.2 101 ( 80-125 ) 30.0 ug/L 08/09/2008 MSD 28.1 94 7 (< 20 ) 30.0 ug/L 08/09/2008 Trichloroethene MS ND 32.2 107 ( 80-125 ) 30.0 ug/L 08/09/2008 MSD 29.6 99 9 (< 20 ) 30.0 ug/L 08/09/2008 trans-1,2-Dichloroethene MS ND 30.9 103 ( 79-132 ) 30.0 ug/L 08/09/2008 MSD 28.7 96 7 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dichlorobenzene MS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 30.8 103 9 (< 20 ) 30.0 ug/L 08/09/2008 2,2-Dichloropropane MS ND 29.3 98 ( 80-132 ) 30.0 ug/L 08/09/2008 MSD 27.7 92 6 (< 20 ) 30.0 ug/L 08/09/2008 Hexachlorobutadiene MS ND 31.1 104 ( 77-125 ) 30.0 ug/L 08/09/2008 MSD 27.5 92 13 (< 20 ) 30.0 ug/L 08/09/2008 Isopropylbenzene (Cumene) MS ND 34.2 114 ( 80-121 ) 30.0 ug/L 08/09/2008 MSD 31.5 105 8 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dichloropropane MS ND 32.2 107 ( 80-121 ) 30.0 ug/L 08/09/2008 MSD 29.9 100 7 (< 20 ) 30.0 ug/L 08/09/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 847974 Matrix Spike 847975 Matrix Spike Duplicate

847973 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1-Dichloropropene MS ND 31.9 106 ( 80-122 ) 30.0 ug/L 08/09/2008 MSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008 1,1,2-Trichloroethane MS ND 31.3 104 ( 77-120 ) 30.0 ug/L 08/09/2008 MSD 29.1 97 8 (< 20 ) 30.0 ug/L 08/09/2008 1,3-Dichlorobenzene MS ND 32.5 108 ( 80-120 ) 30.0 ug/L 08/09/2008 MSD 30.2 101 7 (< 20 ) 30.0 ug/L 08/09/2008 1,2,3-Trichlorobenzene MS ND 34.4 115 ( 77-120 ) 30.0 ug/L 08/09/2008 MSD 31.4 105 9 (< 20 ) 30.0 ug/L 08/09/2008 Surrogates 

### 1,2-Dichloroethane-D4 <surr> MS 30.9 103 ( 73-120 ) 08/09/2008 MSD 30.4 101 1 08/09/2008 Toluene-d8 <surr> MS 29.8 99 ( 80-120 ) 08/09/2008 MSD 30.1 100 1 08/09/2008 4-Bromofluorobenzene <surr> MS 27.9 93 ( 76-120 ) 08/09/2008 MSD 27.6 92 1 08/09/2008

Batch Method Instrument 

### VMS9995

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) MXX20608 3010 H20 Digest for Metals ICP-MS 08/04/2008

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS ND 1060 106 ( 80-120 ) 1000 ug/L 08/05/2008 BMSD 1060 106 0 (< 15 ) 1000 ug/L 08/05/2008

Batch Method Instrument 

### MMS5551

SW6020 Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department 

### Gasoline Range Organics BMS ND 515 114 * ( 79-108 ) 450 ug/L 08/05/2008 BMSD 412 92 22 (< 20 ) 450 ug/L 08/05/2008 * Surrogates 

### 4-Bromofluorobenzene <surr> BMS 56.2 112 ( 50-150 ) 08/05/2008 BMSD 55.6 111 1 08/05/2008

Batch Method Instrument 

### VFC9090

SW8015C HP 5890 Series II PID+FID VCA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS ND 4.82 94 ( 75-125 ) 5.15 mg/L 08/11/2008 BMSD 4.78 91 1 (< 30 ) 5.26 mg/L 08/11/2008 Surrogates 

### 5a Androstane <surr> BMS .112 109 ( 50-150 ) 08/11/2008 BMSD 0.110 105 2 08/11/2008

Batch Method Instrument 

### XFC8106

SW8015C HP 5890 Series II FID SV D R

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 28.0 93 10 (< 20 ) 30.0 ug/L 08/09/2008 Toluene BMS ND 31.8 106 ( 77-120 ) 30.0 ug/L 08/09/2008 BMSD 29.5 98 7 (< 20 ) 30.0 ug/L 08/09/2008 Ethylbenzene BMS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 30.1 100 9 (< 20 ) 30.0 ug/L 08/09/2008 n-Butylbenzene BMS ND 29.8 99 ( 80-124 ) 30.0 ug/L 08/09/2008 BMSD 26.9 90 10 (< 20 ) 30.0 ug/L 08/09/2008 1,4-Dichlorobenzene BMS ND 34 113 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 31.0 103 9 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dichloroethane BMS ND 34.1 114 ( 80-129 ) 30.0 ug/L 08/09/2008 BMSD 31.6 105 8 (< 20 ) 30.0 ug/L 08/09/2008 1,3,5-Trimethylbenzene BMS ND 31.6 105 ( 80-128 ) 30.0 ug/L 08/09/2008 BMSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008 4-Chlorotoluene BMS ND 30.9 103 ( 79-128 ) 30.0 ug/L 08/09/2008 BMSD 28.6 96 8 (< 20 ) 30.0 ug/L 08/09/2008 Chlorobenzene BMS ND 33.9 113 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 31.3 104 8 (< 20 ) 30.0 ug/L 08/09/2008 4-Methyl-2-pentanone (MIBK) BMS ND 100 111 ( 69-134 ) 90.0 ug/L 08/09/2008 BMSD 93.7 104 7 (< 20 ) 90.0 ug/L 08/09/2008 cis-1,2-Dichloroethene BMS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008 BMSD 30.4 101 7 (< 20 ) 30.0 ug/L 08/09/2008 4-Isopropyltoluene BMS ND 31.3 104 ( 80-125 ) 30.0 ug/L 08/09/2008 BMSD 28.7 96 9 (< 20 ) 30.0 ug/L 08/09/2008 cis-1,3-Dichloropropene BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 26.4 88 7 (< 20 ) 30.0 ug/L 08/09/2008 n-Propylbenzene BMS ND 32.2 107 ( 80-129 ) 30.0 ug/L 08/09/2008 BMSD 29.7 99 8 (< 20 ) 30.0 ug/L 08/09/2008 Styrene BMS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 30.6 102 8 (< 20 ) 30.0 ug/L 08/09/2008 Dibromomethane BMS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 31.5 105 6 (< 20 ) 30.0 ug/L 08/09/2008 trans-1,3-Dichloropropene BMS ND 30 100 ( 80-124 ) 30.0 ug/L 08/09/2008 BMSD 28.7 96 5 (< 20 ) 30.0 ug/L 08/09/2008 1,2,4-Trichlorobenzene BMS ND 33.4 111 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 30.1 100 10 (< 20 ) 30.0 ug/L 08/09/2008 Acetone BMS ND 90.6 101 ( 50-135 ) 90.0 ug/L 08/09/2008 BMSD 80.2 89 12 (< 20 ) 90.0 ug/L 08/09/2008 1,1,2,2-Tetrachloroethane BMS ND 32.1 107 ( 76-123 ) 30.0 ug/L 08/09/2008 BMSD 30.6 102 5 (< 20 ) 30.0 ug/L 08/09/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,2-Dibromo-3-chloropropane BMS ND 32 107 ( 73-130 ) 30.0 ug/L 08/09/2008 BMSD 27.7 93 14 (< 20 ) 30.0 ug/L 08/09/2008 Methyl-t-butyl ether BMS ND 44.8 99 ( 80-120 ) 45.0 ug/L 08/09/2008 BMSD 41.6 93 7 (< 20 ) 45.0 ug/L 08/09/2008 Tetrachloroethene BMS ND 33.3 111 ( 79-122 ) 30.0 ug/L 08/09/2008 BMSD 30.7 102 8 (< 20 ) 30.0 ug/L 08/09/2008 Dibromochloromethane BMS ND 33.5 112 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 32.8 109 2 (< 20 ) 30.0 ug/L 08/09/2008 1,3-Dichloropropane BMS ND 31.1 104 ( 80-121 ) 30.0 ug/L 08/09/2008 BMSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dibromoethane BMS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 29.4 98 13 (< 20 ) 30.0 ug/L 08/09/2008 Carbon tetrachloride BMS ND 32.4 108 ( 80-126 ) 30.0 ug/L 08/09/2008 BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 08/09/2008 1,1,1,2-Tetrachloroethane BMS ND 33 110 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 31.9 106 3 (< 20 ) 30.0 ug/L 08/09/2008 Chloroform BMS ND 33.8 113 ( 80-124 ) 30.0 ug/L 08/09/2008 BMSD 30.5 102 10 (< 20 ) 30.0 ug/L 08/09/2008 Bromobenzene BMS ND 32.9 110 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 30.3 101 8 (< 20 ) 30.0 ug/L 08/09/2008 Chloromethane BMS ND 30 100 ( 67-125 ) 30.0 ug/L 08/09/2008 BMSD 27.4 91 9 (< 20 ) 30.0 ug/L 08/09/2008 1,2,3-Trichloropropane BMS ND 30.7 102 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 29.3 98 5 (< 20 ) 30.0 ug/L 08/09/2008 Bromomethane BMS 1.26 J 29.1 93 ( 30-140 ) 30.0 ug/L 08/09/2008 BMSD 27.4 87 6 (< 20 ) 30.0 ug/L 08/09/2008 Bromochloromethane BMS ND 34.5 115 ( 77-129 ) 30.0 ug/L 08/09/2008 BMSD 32.0 107 8 (< 20 ) 30.0 ug/L 08/09/2008 Vinyl chloride BMS ND 29.7 99 ( 72-145 ) 30.0 ug/L 08/09/2008 BMSD 27.2 91 9 (< 20 ) 30.0 ug/L 08/09/2008 Dichlorodifluoromethane BMS ND 28.4 95 ( 62-153 ) 30.0 ug/L 08/09/2008 BMSD 25.3 84 12 (< 20 ) 30.0 ug/L 08/09/2008 Chloroethane BMS ND 27.7 93 ( 67-133 ) 30.0 ug/L 08/09/2008 BMSD 24.4 81 13 (< 20 ) 30.0 ug/L 08/09/2008 sec-Butylbenzene BMS ND 30.8 103 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 28.5 95 8 (< 20 ) 30.0 ug/L 08/09/2008 Bromodichloromethane BMS ND 30.9 103 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 29.2 97 6 (< 20 ) 30.0 ug/L 08/09/2008 1,1-Dichloroethene BMS ND 32.6 109 ( 76-130 ) 30.0 ug/L 08/09/2008 BMSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) BMS ND 97.5 108 ( 66-136 ) 90.0 ug/L 08/09/2008 BMSD 89.6 100 9 (< 20 ) 90.0 ug/L 08/09/2008 Methylene chloride BMS ND 31 103 ( 63-131 ) 30.0 ug/L 08/09/2008 BMSD 28.5 95 9 (< 20 ) 30.0 ug/L 08/09/2008 Trichlorofluoromethane BMS ND 34.1 114 ( 68-145 ) 30.0 ug/L 08/09/2008 BMSD 30.2 101 12 (< 20 ) 30.0 ug/L 08/09/2008 P & M -Xylene BMS ND 66.9 112 ( 80-120 ) 60.0 ug/L 08/09/2008 BMSD 61.8 103 8 (< 20 ) 60.0 ug/L 08/09/2008 Naphthalene BMS ND 33.4 111 ( 75-120 ) 30.0 ug/L 08/09/2008 BMSD 30.7 102 9 (< 20 ) 30.0 ug/L 08/09/2008 o-Xylene BMS ND 33.3 111 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 31.4 105 6 (< 20 ) 30.0 ug/L 08/09/2008 Bromoform BMS ND 34.4 115 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 34.5 115 0 (< 20 ) 30.0 ug/L 08/09/2008 1-Chlorohexane BMS ND 44.2 98 ( 70-125 ) 45.0 ug/L 08/09/2008 BMSD 40.2 89 10 (< 20 ) 45.0 ug/L 08/09/2008 1,2,4-Trimethylbenzene BMS ND 32.6 109 ( 80-125 ) 30.0 ug/L 08/09/2008 BMSD 29.7 99 9 (< 20 ) 30.0 ug/L 08/09/2008 tert-Butylbenzene BMS ND 31 103 ( 80-122 ) 30.0 ug/L 08/09/2008 BMSD 28.6 95 8 (< 20 ) 30.0 ug/L 08/09/2008 1,1,1-Trichloroethane BMS ND 30.7 102 ( 80-122 ) 30.0 ug/L 08/09/2008 BMSD 28.8 96 7 (< 20 ) 30.0 ug/L 08/09/2008 1,1-Dichloroethane BMS ND 32.3 108 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 29.4 98 9 (< 20 ) 30.0 ug/L 08/09/2008 2-Chlorotoluene BMS ND 30.2 101 ( 80-125 ) 30.0 ug/L 08/09/2008 BMSD 28.1 94 7 (< 20 ) 30.0 ug/L 08/09/2008 Trichloroethene BMS ND 32.2 107 ( 80-125 ) 30.0 ug/L 08/09/2008 BMSD 29.6 99 9 (< 20 ) 30.0 ug/L 08/09/2008 trans-1,2-Dichloroethene BMS ND 30.9 103 ( 79-132 ) 30.0 ug/L 08/09/2008 BMSD 28.7 96 7 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dichlorobenzene BMS ND 33.6 112 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 30.8 103 9 (< 20 ) 30.0 ug/L 08/09/2008 2,2-Dichloropropane BMS ND 29.3 98 ( 80-132 ) 30.0 ug/L 08/09/2008 BMSD 27.7 92 6 (< 20 ) 30.0 ug/L 08/09/2008 Hexachlorobutadiene BMS ND 31.1 104 ( 77-125 ) 30.0 ug/L 08/09/2008 BMSD 27.5 92 13 (< 20 ) 30.0 ug/L 08/09/2008 Isopropylbenzene (Cumene) BMS ND 34.2 114 ( 80-121 ) 30.0 ug/L 08/09/2008 BMSD 31.5 105 8 (< 20 ) 30.0 ug/L 08/09/2008 1,2-Dichloropropane BMS ND 32.2 107 ( 80-121 ) 30.0 ug/L 08/09/2008 BMSD 29.9 100 7 (< 20 ) 30.0 ug/L 08/09/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) VXX18532 Volatiles Extraction AFCEE 3.1 8260 (W) 08/09/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1-Dichloropropene BMS ND 31.9 106 ( 80-122 ) 30.0 ug/L 08/09/2008 BMSD 29.3 98 8 (< 20 ) 30.0 ug/L 08/09/2008 1,1,2-Trichloroethane BMS ND 31.3 104 ( 77-120 ) 30.0 ug/L 08/09/2008 BMSD 29.1 97 8 (< 20 ) 30.0 ug/L 08/09/2008 1,3-Dichlorobenzene BMS ND 32.5 108 ( 80-120 ) 30.0 ug/L 08/09/2008 BMSD 30.2 101 7 (< 20 ) 30.0 ug/L 08/09/2008 1,2,3-Trichlorobenzene BMS ND 34.4 115 ( 77-120 ) 30.0 ug/L 08/09/2008 BMSD 31.4 105 9 (< 20 ) 30.0 ug/L 08/09/2008 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 30.9 103 ( 73-120 ) 08/09/2008 BMSD 30.4 101 1 08/09/2008 Toluene-d8 <surr> BMS 29.8 99 ( 80-120 ) 08/09/2008 BMSD 30.1 100 1 08/09/2008 4-Bromofluorobenzene <surr> BMS 27.9 93 ( 76-120 ) 08/09/2008 BMSD 27.6 92 1 08/09/2008

Batch Method Instrument 

### VMS9995

SW8260B HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) XXX19761 3520 Liquid/Liquid Ext for 8270 SIM 08/05/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### Acenaphthylene BMS ND .326 63 ( 50-105 ) 0.521 ug/L 08/26/2008 BMSD 0.305 59 7 (< 30 ) 0.521 ug/L 08/26/2008 Acenaphthene BMS ND .321 62 ( 45-110 ) 0.521 ug/L 08/26/2008 BMSD 0.308 59 4 (< 30 ) 0.521 ug/L 08/26/2008 Fluorene BMS ND .331 64 ( 50-110 ) 0.521 ug/L 08/26/2008 BMSD 0.306 59 8 (< 30 ) 0.521 ug/L 08/26/2008 Phenanthrene BMS ND .331 64 ( 50-115 ) 0.521 ug/L 08/26/2008 BMSD 0.302 58 9 (< 30 ) 0.521 ug/L 08/26/2008 Anthracene BMS ND .353 68 ( 55-110 ) 0.521 ug/L 08/26/2008 BMSD 0.321 62 10 (< 30 ) 0.521 ug/L 08/26/2008 Fluoranthene BMS ND .356 68 ( 55-125 ) 0.521 ug/L 08/26/2008 BMSD 0.335 64 6 (< 30 ) 0.521 ug/L 08/26/2008 Pyrene BMS ND .338 65 ( 50-130 ) 0.521 ug/L 08/26/2008 BMSD 0.320 62 6 (< 30 ) 0.521 ug/L 08/26/2008 Benzo(a)Anthracene BMS ND .409 79 ( 55-120 ) 0.521 ug/L 08/26/2008 BMSD 0.382 73 7 (< 30 ) 0.521 ug/L 08/26/2008 Chrysene BMS ND .347 67 ( 55-120 ) 0.521 ug/L 08/26/2008 BMSD 0.329 63 5 (< 30 ) 0.521 ug/L 08/26/2008 Benzo[b]Fluoranthene BMS ND .383 74 ( 46-130 ) 0.521 ug/L 08/26/2008 BMSD 0.340 65 12 (< 30 ) 0.521 ug/L 08/26/2008 Benzo[k]fluoranthene BMS ND .358 69 ( 60-125 ) 0.521 ug/L 08/26/2008 BMSD 0.326 63 9 (< 30 ) 0.521 ug/L 08/26/2008 Benzo[a]pyrene BMS ND .434 83 ( 55-120 ) 0.521 ug/L 08/26/2008 BMSD 0.385 74 12 (< 30 ) 0.521 ug/L 08/26/2008 Indeno[1,2,3-c,d] pyrene BMS ND .379 73 ( 45-125 ) 0.521 ug/L 08/26/2008 BMSD 0.328 63 14 (< 30 ) 0.521 ug/L 08/26/2008 Dibenzo[a,h]anthracene BMS ND .395 76 ( 41-140 ) 0.521 ug/L 08/26/2008 BMSD 0.338 65 15 (< 30 ) 0.521 ug/L 08/26/2008 Benzo[g,h,i]perylene BMS ND .372 71 ( 46-125 ) 0.521 ug/L 08/26/2008 BMSD 0.328 63 13 (< 30 ) 0.521 ug/L 08/26/2008 Naphthalene BMS ND .306 59 ( 42-100 ) 0.521 ug/L 08/26/2008 BMSD 0.305 59 0 (< 30 ) 0.521 ug/L 08/26/2008 1-Methylnaphthalene BMS ND .313 60 ( 46-115 ) 0.521 ug/L 08/26/2008 BMSD 0.306 59 2 (< 30 ) 0.521 ug/L 08/26/2008 2-Methylnaphthalene BMS ND .308 59 ( 45-105 ) 0.521 ug/L 08/26/2008 BMSD 0.298 57 3 (< 30 ) 0.521 ug/L 08/26/2008 Surrogates 

### Terphenyl-d14 <surr> BMS .479 92 ( 50-135 ) 08/26/2008 BMSD 0.386 74 21 08/26/2008Matrix SGS Ref.# Printed Date/Time 

### 09/09/2008 8:32 Batch Method Date Original Prep 

### 1083866006 Billable Matrix Spike 1083866007 Billable Matrix Spike Dup.

1083866005 Water (Surface, Eff., Ground) XXX19761 3520 Liquid/Liquid Ext for 8270 SIM 08/05/2008

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS4671

8270D SIMS HP 5890 Series II MS2 SVOA