Laboratory Services ;TANtPA ELECTRIC 5012 Causeway Blvd • Tampa FI. 33619 • Ph (813)630-7490 • Fax (813)630-7360 • DOH #E54272 

Report For: Ray McDarby Report Date: 8/31/2010 

Laboratory 10: AB07088 

Location Code: 

Sample Information 

Description: Big Bend Unit #1 (4/20-4/22) Sampled By: SCOTT GIVEN 

Project Account Code: W4 Date and Time Collected: 4128/201012:00:00 AM 

Sample Collection Method: Date of Sample Receipt: 4128/2010 

Laboratory Results 

Qualifier Test Analysis Lower Upper Violation 

PARAMETER Result Units MDL Code Method Analyst Date & Time Limit Limit Check 

Chloride Duplicate result, Run 1 a 22.769 ug/ml 0,05 Method 26a KASZS 4/26/201012:16:00 PM 

Chloride Duplicate result Run 2a 20.949 ugiml 0.05 Method 26a KASZS 412612010 12:16:00 PM 

Chloride Duplicate result. Run 3a 2.697 ug/ml Method 26a KASZS 41261201012:16:00 PM 

Chloride Duplicate result. Run 4A 2.747 uglml Method 26a KASZS 4/261201012:16:00 PM 

Chloride result. Run 1a 22.945 uglml 0.05 Method 26a KASZS 4126/20101216:00 PM 

Chloride result. Run 2a 21.189 uglml 0.05 Method 26a KASZS 412612010121600 PM 

Chloride result. Run 3a 2.676 uglml 0.05 Method 26a KASZS 4126/201012:16:00 PM 

Chloride result, Run 4A 2.746 uglml 0.05 Method 26a KASZS 4126/201012:1600 PM 

Chloride, Duplicate Blank result < uglmL u EPA Method 26a KASZS 4/26/2010 12:16:00 PM 

Final Sample Volume, Run 1 a 440 mL EPA Method 26a KASZS 4/261201012:16:00 PM 

Final Sample Volume, Run 2a 495 mL EPA Method 26a KASZS 4/26/201012:1600 PM 

Final Sample Volume, Run 3a 488 mL EPA Method 26a KASZS 4126/201012:16:00 PM 

Final Sample Volume, Run 4a 472 mL EPA Method 26a KASZS 4/26/201012:16:00 PM 

Fluoride Duplicate result, Run 1a 0.287 uglmL 0.05 Method 26a KASZS 41261201012:16:00 PM 

Fluoride Duplicate result. Run 2a 0.282 uglmL 0.05 Method 26a KASZS 4/261201012:16:00 PM 

Fluoride Duplicate result, Run 3a 0.168 uglmL 0.05 Method 26a KASZS 4/261201012:16:00 PM 

Fluoride Duplicate result. Run 4A 0205 uglmL 0.05 Method 26a KASZS 41261201012:16:00 PM 

Fluoride. Duplicate Blank result < uglml u EPA Method 26a KASZS 4/2612010 12:1600 PM 

HCl result. Run 1 a 10339 ug Method 26a KASZS 41261201012:16:00 PM 

HCl result. Run 2a 10721 ug Method 26a KASZS 4/261201012:16:00 PM 

HCl result. Run 3a 1347 u9 Method 26a KASZS 41261201012:1600 PM 

HCl result. Run 4A 1332 ug Method 26a KASZS 4/261201012:16:00 PM 

HF result. Run 1 a 131 u9 Method 26a KASZS 4126/201012:16:00 PM 

HF result. Run2a 147 ug Method 26a KASZS 4/2612010 1216:00 PM 

HF result. Run3a 874 u9 Method 26a KASZS 412612010 12:16:00 PM 

Laboratory Services certifies that the test results in this report meet all requirements of the NElAC standards, unless indicated otherwise 

in the body of the report. Unless otherwise noted, all methods followed are per the most current published version of 40 CFR Part 136, Table B. 

Results reported on this report pertain to the above referenced sample only. 

Report Number: AB07088-083110-09 Page I of2 "General Report" 
Laboratory Services TAMPA ELECTRIC 5012 Causeway Blvd • Tampa FI. 33619 • Ph (813)630-7490 • Fax (813)630-7360 • DOH #E54272 

Qualifier Test Analysis Lower Upper Violation 

PARAMETER Result Units MOL Code Method Analyst Date &Time Limit Limit Check 

HF result, Run4A 100 ug Method 26a KASZS 4/26/201012:16:00 PM 

Comments 

All results calculated on a wet to wet basis, unless otherwise indicated. 

Data Qualifier Codes Explanation: 

U - Indicates that the compound was analyzed for but not detected. 


I - The reported value is between the laboratory method detection limit (MOL) and the laboratory practical quantitation limit (POL). POL 4 x MOL. 


Should there be any questions regarding this report, please contact: 

Cheryl Howard, 


Designee for Peggy Penner, 


Manager, Laboratory Services 


(813) 630-7490 

Laboratory Services certifies that the test results in this report meet all reqUirements of the NELAC standards, unless indicated otherwise 

in the body of the report. Unless otherwise noted, all methods followed are per the most current published version of 40 CFR Part 136, Table B. 

Results reported on this report pertain to the above referenced sample only. 

Report Number: "General Report" AB07088-083110-09 Page 2 of2