### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs**  AZCatalystPaperSnowflake Power Boiler #2 Coal ICR Phase I Organic HAP and CO Coal PC 3/24/2006 Sample #1 On/Before May 2008 100 90 98.7 28.9 0.3 98.74.009212953 4.0 AZCatalystPaperSnowflake Power Boiler #2 Coal ICR Phase I Organic HAP and CO Coal PC 3/24/2006 Sample #2 On/Before May 2008 100 90 98.7 28.7 0.1 98.74.009212953 4.0 AZCatalystPaperSnowflake Power Boiler #2 Coal ICR Phase I Organic HAP and CO Coal PC 3/24/2006 Sample #3 On/Before May 2008 100 90 98.7 29 0.1 98.74.009212953 4.0 FLSmurfit-Stone 7PB ICR Phase I Organic HAP and CO (2) Coal PC 6/20/2008 Sample #1 After May 2008 99.76 49.94 0.12 99.764.052270356 4.1 FLSmurfit-Stone 7PB ICR Phase I Organic HAP and CO (2) Coal PC 6/20/2008 Sample #2 After May 2008 99.76 49.94 0.12 99.764.052270356 4.1 FLSmurfit-Stone 7PB ICR Phase I Organic HAP and CO (2) Coal PC 6/20/2008 Sample #3 After May 2008 99.76 50.31 0.12 99.764.052270356 4.1 HIPuuneneSugarMill Boiler 3 ICR Phase II - Voluntary Additional CO data (2)

Coal Stoker/SlopedGrate/Other 5/24/2006 Sample #1 On/Before May 2008 89.06 58.86 30.44 89.063.617634302 3.6 HIPuuneneSugarMill Boiler 3 ICR Phase II - Voluntary Additional CO data (2)

Coal Stoker/SlopedGrate/Other 5/24/2006 Sample #2 On/Before May 2008 89.06 58.86 30.44 89.063.617634302 3.6 HIPuuneneSugarMill Boiler 3 ICR Phase II - Voluntary Additional CO data (2)

Coal Stoker/SlopedGrate/Other 5/25/2006 Sample #3 On/Before May 2008 89.06 58.86 30.44 89.063.617634302 3.6 IAADMCornProcessingCR EU-501A ICR Phase I Organic HAP and CO (3) Coal FB 5/25/1989 Sample #1 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-501A ICR Phase I Organic HAP and CO (3) Coal FB 5/25/1989 Sample #2 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-501A ICR Phase I Organic HAP and CO (3) Coal FB 5/26/1989 Sample #3 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-501B ICR Phase I Organic HAP and CO (4) Coal FB 5/15/1989 Sample #1 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-501B ICR Phase I Organic HAP and CO (4) Coal FB 5/15/1989 Sample #2 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-501B ICR Phase I Organic HAP and CO (4) Coal FB 5/15/1989 Sample #3 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-502A ICR Phase I Organic HAP and CO (2) Coal FB 5/19/1989 Sample #1 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-502A ICR Phase I Organic HAP and CO (2) Coal FB 5/19/1989 Sample #2 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-502A ICR Phase I Organic HAP and CO (2) Coal FB 5/19/1989 Sample #3 On/Before May 2008 500 450 45018.27908641 18.0 IAADMCornProcessingCR EU-530 ICR Phase I Organic HAP and CO Coal FB 11/20/2002Sample #1 On/Before May 2008 110 99 111.2 50.9 0 111.24.516965353 4.5 IAADMCornProcessingCR EU-530 ICR Phase I Organic HAP and CO Coal FB 11/20/2002Sample #2 On/Before May 2008 110 99 111.2 50.9 0 111.24.516965353 4.5 IAADMCornProcessingCR EU-530 ICR Phase I Organic HAP and CO Coal FB 11/20/2002Sample #3 On/Before May 2008 110 99 111.1 51.1 0.2 111.14.512903334 4.5 IAArchersDanielsMidlandDesMoines Asea Boiler #1 ICR Phase II - Templates CO Coal FB 8/24/2009 Sample #1 After May 2008 104.3 93.87 93.873.813017425 3.8 IAArchersDanielsMidlandDesMoines Asea Boiler #1 ICR Phase II - Templates CO Coal FB 8/24/2009 Sample #2 After May 2008 104.3 93.87 93.873.813017425 3.8 IAArchersDanielsMidlandDesMoines Asea Boiler #1 ICR Phase II - Templates CO Coal FB 8/25/2009 Sample #3 After May 2008 104.3 93.87 93.873.813017425 3.8 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 4/22/2004 Sample #1 On/Before May 2008 89 59.3 0.3 89 3.61519709 3.6 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 4/22/2004 Sample #2 On/Before May 2008 89 59 0.2 89 3.61519709 3.6 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 4/22/2004 Sample #3 On/Before May 2008 89 59.2 0.4 89 3.61519709 3.6 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO (2) Coal Stoker/SlopedGrate/Other 12/12/2006Sample #1 On/Before May 2008 51.5 28.9 0 51.52.091939889 2.1 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO (2) Coal Stoker/SlopedGrate/Other 12/12/2006Sample #2 On/Before May 2008 51.5 28.9 0 51.52.091939889 2.1 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO (2) Coal Stoker/SlopedGrate/Other 12/12/2006Sample #3 On/Before May 2008 51.5 28.9 0 51.52.091939889 2.1 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO (3) Coal Stoker/SlopedGrate/Other 3/15/2005 Sample #1 On/Before May 2008 88.67 58.96 0 88.673.601792427 3.6 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO (3) Coal Stoker/SlopedGrate/Other 3/15/2005 Sample #2 On/Before May 2008 88.67 58.96 0 88.673.601792427 3.6 IAMuscatinePowerandWater Unit 7 ICR Phase I Organic HAP and CO (3) Coal Stoker/SlopedGrate/Other 3/15/2005 Sample #3 On/Before May 2008 88.67 58.96 0 88.673.601792427 3.6 IAUofNorthernIowa Boiler #3 ICR Phase I Organic HAP and CO B3 Coal PC 8/3/2007 Sample #1 On/Before May 2008 151.4 69.6 1.8 151.46.149897072 6.1 IAUofNorthernIowa Boiler #3 ICR Phase I Organic HAP and CO B3 Coal PC 8/3/2007 Sample #2 On/Before May 2008 149 70.1 1.9 1496.052408611 6.1 IAUofNorthernIowa Boiler #3 ICR Phase I Organic HAP and CO B3 Coal PC 8/3/2007 Sample #3 On/Before May 2008 149 69.9 2 1496.052408611 6.1 IAUofNorthernIowa Boiler #3 ICR Phase II - Templates CO Coal PC 10/6/2009 Sample #1 After May 2008 149 134.1 149 71.2 0 1496.052408611 6.1 IAUofNorthernIowa Boiler #3 ICR Phase II - Templates CO Coal PC 10/6/2009 Sample #2 After May 2008 149 134.1 149 71.2 1.2 1496.052408611 6.1 IAUofNorthernIowa Boiler #3 ICR Phase II - Templates CO Coal PC 10/6/2009 Sample #3 After May 2008 149 134.1 149 71.5 2 1496.052408611 6.1 ILCornProductsInt B10 ICR Phase II - Voluntary CO Coal FB 1/23/2007 Sample #1 On/Before May 2008 96.96 49.5 0 96.963.938533819 3.9 ILCornProductsInt B10 ICR Phase II - Voluntary CO Coal FB 1/23/2007 Sample #2 On/Before May 2008 96.96 49.5 0 96.963.938533819 3.9 ILCornProductsInt B10 ICR Phase II - Voluntary CO Coal FB 1/23/2007 Sample #3 On/Before May 2008 96.96 49.5 0 96.963.938533819 3.9 ILPolyOne B1 ICR Phase II - ERT ERT Coal FB 9/10/2009 1 After May 2008 90.24 81.216 90.41 44.74 0 90.413.672471561 3.7 ILPolyOne B1 ICR Phase II - ERT ERT Coal FB 9/11/2009 2 After May 2008 90.24 81.216 90.24 44.85 0 90.243.665566128 3.7 ILPolyOne B1 ICR Phase II - ERT ERT Coal FB 9/11/2009 3 After May 2008 90.24 81.216 90.24 44.64 -0.06 90.243.665566128 3.7

INNotreDame B-4 ICR Phase II - Templates CO Coal Stoker/SlopedGrate/Other 8/25/2009 Sample #1 After May 2008 60 54 59.9 29.6 0.5 59.92.433149502 2.4

INNotreDame B-4 ICR Phase II - Templates CO Coal Stoker/SlopedGrate/Other 8/25/2009 Sample #2 After May 2008 60 54 59.9 29.4 0.5 59.92.433149502 2.4

INNotreDame B-4 ICR Phase II - Templates CO Coal Stoker/SlopedGrate/Other 8/25/2009 Sample #3 After May 2008 60 54 59.9 29.5 0.5 59.92.433149502 2.4 KYISPChemicals 0AA (Riley) ICR Phase II - Templates CO Coal Stoker/SlopedGrate/Other 11/17/2009Sample #1 After May 2008 414.3 372.87 413.9 201.3 0.4 413.916.81269748 17.0 KYISPChemicals 0AA (Riley) ICR Phase II - Templates CO Coal Stoker/SlopedGrate/Other 11/17/2009Sample #2 After May 2008 414.3 372.87 413.9 201.3 0.4 413.916.81269748 17.0 KYISPChemicals 0AA (Riley) ICR Phase II - Templates CO Coal Stoker/SlopedGrate/Other 11/17/2009Sample #3 After May 2008 414.3 372.87 413.9 201.3 0.4 413.916.81269748 17.0 NCBlueRidgePaper G11039 ICR Phase I CO (RC) Coal PC 11/7/2002 Sample #1 On/Before May 2008 1000 900 90036.55817282 37.0 NCBlueRidgePaper G11039 ICR Phase I CO (RC) Coal PC 11/7/2002 Sample #2 On/Before May 2008 1000 900 90036.55817282 37.0 NCBlueRidgePaper G11039 ICR Phase I CO (RC) Coal PC 11/7/2002 Sample #3 On/Before May 2008 1000 900 90036.55817282 37.0 NCBlueRidgePaper G11040 ICR Phase I CO (N4) Coal PC 11/6/2002 Sample #1 On/Before May 2008 1000 900 920 90036.55817282 37.0 NCBlueRidgePaper G11040 ICR Phase I CO (N4) Coal PC 11/6/2002 Sample #2 On/Before May 2008 1000 900 920 90036.55817282 37.0 NCBlueRidgePaper G11040 ICR Phase I CO (N4) Coal PC 11/6/2002 Sample #3 On/Before May 2008 1000 900 920 90036.55817282 37.0 NCUNCCogen ES-001 ICR Phase II - ERT ERT Coal FB 8/12/2009 U6-CEM-1 After May 2008 49.2 44.28 44.281.798662103 1.8 NCUNCCogen ES-001 ICR Phase II - ERT ERT Coal FB 8/13/2009 U6-CEM-2 After May 2008 49.2 44.28 44.281.798662103 1.8 NCUNCCogen ES-001 ICR Phase II - ERT ERT Coal FB 8/13/2009 U6-CEM-3 After May 2008 49.2 44.28 44.281.798662103 1.8 NEADMLincoln EU26 Coal Boiler ICR Phase I Organic HAP and CO Coal FB 2/15/1989 Sample #1 On/Before May 2008 496.8 496 249 0 49620.14761524 20.0 NEADMLincoln EU26 Coal Boiler ICR Phase I Organic HAP and CO Coal FB 2/15/1989 Sample #2 On/Before May 2008 496.8 496 249 0 49620.14761524 20.0 NEADMLincoln EU26 Coal Boiler ICR Phase I Organic HAP and CO Coal FB 2/15/1989 Sample #3 On/Before May 2008 496.8 496 249 0 49620.14761524 20.0 OHAppletonIdeas Boiler 4 (B003) ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 1/29/2003 Sample #1 On/Before May 2008 902.8 812.52 812.5233.00471842 33.0 OHAppletonIdeas Boiler 4 (B003) ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 1/29/2003 Sample #2 On/Before May 2008 902.8 812.52 812.5233.00471842 33.0 OHAppletonIdeas Boiler 4 (B003) ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 1/29/2003 Sample #3 On/Before May 2008 902.8 812.52 812.5233.00471842 33.0 OHMortonSaltRittman B002 - Coal-Fired Boiler #2 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 8/25/2009 1 After May 2008 400.6 360.54 401 202.1 0.3 401 16.288697 16.0 OHMortonSaltRittman B002 - Coal-Fired Boiler #2 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 8/26/2009 2 After May 2008 400.6 360.54 401 201.6 0.3 401 16.288697 16.0 OHMortonSaltRittman B002 - Coal-Fired Boiler #2 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 8/27/2009 3 After May 2008 400.6 360.54 401 201.6 0.2 401 16.288697 16.0 OHMortonSaltRittman B002 - Coal-Fired Boiler #2 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 8/25/2009 1 After May 2008 400.6 360.54 360.5414.64520403 15.0 OHMortonSaltRittman B002 - Coal-Fired Boiler #2 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 8/26/2009 2 After May 2008 400.6 360.54 360.5414.64520403 15.0 OHMortonSaltRittman B002 - Coal-Fired Boiler #2 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 8/27/2009 3 After May 2008 400.6 360.54 360.5414.64520403 15.0 OKGPMuskogeeMill B-3 ICR Phase I Organic HAP and CO (B-3) Coal PC 5/21/2003 Sample #1 On/Before May 2008 869 782.1 782.131.76905218 32.0 OKGPMuskogeeMill B-3 ICR Phase I Organic HAP and CO (B-3) Coal PC 5/21/2003 Sample #2 On/Before May 2008 869 782.1 782.131.76905218 32.0 OKGPMuskogeeMill B-3 ICR Phase I Organic HAP and CO (B-3) Coal PC 5/21/2003 Sample #3 On/Before May 2008 869 782.1 782.131.76905218 32.0



### Page 1 of 7

### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs**  OKGPMuskogeeMill B-4 ICR Phase I Organic HAP and CO (B-4) Coal PC 4/16/2003 Sample #1 On/Before May 2008 150.1 135.09 50.38 14.59 0.48 50.382.046445274 2.0 OKGPMuskogeeMill B-4 ICR Phase I Organic HAP and CO (B-4) Coal PC 4/16/2003 Sample #2 On/Before May 2008 150.1 135.09 50.38 15.41 0.53 50.382.046445274 2.0 OKGPMuskogeeMill B-4 ICR Phase I Organic HAP and CO (B-4) Coal PC 4/16/2003 Sample #3 On/Before May 2008 150.1 135.09 50.38 15.52 0.4 50.382.046445274 2.0 TNEastman_NO_CBIDATA Boiler 30 ICR Phase II - ERT ERT Coal PC 8/25/2009 1 After May 2008 50 45 50 25 0 502.031009601 2.0 TNEastman_NO_CBIDATA Boiler 30 ICR Phase II - ERT ERT Coal PC 8/25/2009 2 After May 2008 50 45 50 25 0 502.031009601 2.0 TNEastman_NO_CBIDATA Boiler 30 ICR Phase II - ERT ERT Coal PC 8/26/2009 3 After May 2008 50 45 50 25 0 502.031009601 2.0 VAINVISTAWaynesboro 2-205 (B#2) Boiler #2 ICR Phase II - Templates CO Coal PC 8/4/2009 Sample #1 After May 2008 49.9 44.91 50.1 25.21 0.74 50.1 2.03507162 2.0 VAINVISTAWaynesboro 2-205 (B#2) Boiler #2 ICR Phase II - Templates CO Coal PC 8/4/2009 Sample #2 After May 2008 49.9 44.91 50.1 25.15 0.78 50.1 2.03507162 2.0 VAINVISTAWaynesboro 2-205 (B#2) Boiler #2 ICR Phase II - Templates CO Coal PC 8/5/2009 Sample #3 After May 2008 49.9 44.91 50.2 25.17 0.06 50.2 2.03913364 2.0 VAPhilipMorrisPark500 B2 ICR Phase I Organic HAP and CO (Unit B2) Coal PC 9/21/2005 Sample #1 On/Before May 2008 906 815.4 815.433.12170458 33.0 VAPhilipMorrisPark500 B2 ICR Phase I Organic HAP and CO (Unit B2) Coal PC 9/21/2005 Sample #2 On/Before May 2008 906 815.4 815.433.12170458 33.0 VAPhilipMorrisPark500 B2 ICR Phase I Organic HAP and CO (Unit B2) Coal PC 9/21/2005 Sample #3 On/Before May 2008 906 815.4 815.433.12170458 33.0 VAPhilipMorrisPark500 B3 ICR Phase I Organic HAP and CO (Unit B3) Coal PC 9/22/2005 Sample #1 On/Before May 2008 906 815.4 815.433.12170458 33.0 VAPhilipMorrisPark500 B3 ICR Phase I Organic HAP and CO (Unit B3) Coal PC 9/22/2005 Sample #2 On/Before May 2008 906 815.4 815.433.12170458 33.0 VAPhilipMorrisPark500 B3 ICR Phase I Organic HAP and CO (Unit B3) Coal PC 9/22/2005 Sample #3 On/Before May 2008 906 815.4 815.433.12170458 33.0 VAUniversityofVirginia 7103-1-01R ICR Phase I Organic HAP and CO (2) Coal Stoker/SlopedGrate/Other 12/6/2007 Sample #1 On/Before May 2008 97.3 87.57 98.2 50.08 0.01 98.23.988902857 4.0 VAUniversityofVirginia 7103-1-01R ICR Phase I Organic HAP and CO (2) Coal Stoker/SlopedGrate/Other 12/6/2007 Sample #2 On/Before May 2008 97.3 87.57 98.2 50.82 0.85 98.23.988902857 4.0 VAUniversityofVirginia 7103-1-01R ICR Phase I Organic HAP and CO (2) Coal Stoker/SlopedGrate/Other 12/6/2007 Sample #3 On/Before May 2008 97.3 87.57 98.2 50.71 -0.07 98.23.988902857 4.0 VAUniversityofVirginia 7103-1-01R ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 9/15/2009 1 After May 2008 506.1 248.99 0.66 506.120.55787918 21.0 VAUniversityofVirginia 7103-1-01R ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 9/16/2009 2 After May 2008 505.1 248.82 0.02 505.120.51725899 21.0 VAUniversityofVirginia 7103-1-01R ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 9/16/2009 3 After May 2008 505.1 248.83 0.11 505.120.51725899 21.0 WVDuPontWashingtonWorks P05 ICR Phase I Organic HAP and CO P05 11.02.05 Coal Stoker/SlopedGrate/Other 11/2/2005 Sample #1 On/Before May 2008 90.96 81.864 90.77 60.22 30.63 90.77 3.68709483 3.7 WVDuPontWashingtonWorks P05 ICR Phase I Organic HAP and CO P05 11.02.05 Coal Stoker/SlopedGrate/Other 11/2/2005 Sample #2 On/Before May 2008 90.96 81.864 90.77 60.22 30.63 90.77 3.68709483 3.7 WVDuPontWashingtonWorks P05 ICR Phase I Organic HAP and CO P05 11.02.05 Coal Stoker/SlopedGrate/Other 11/3/2005 Sample #3 On/Before May 2008 90.96 81.864 90.77 60.22 30.63 90.77 3.68709483 3.7 CTElectric Boat EMU 17 ICR Phase II - ERT ERT Liquid N/A 8/20/2009 1 After May 2008 189.4 170.46 170.466.924117932 6.9 CTElectric Boat EMU 17 ICR Phase II - ERT ERT Liquid N/A 8/20/2009 2 After May 2008 189.4 170.46 170.466.924117932 6.9 CTElectric Boat EMU 17 ICR Phase II - ERT ERT Liquid N/A 8/20/2009 3 After May 2008 189.4 170.46 170.466.924117932 6.9

HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (1)

Non-Continental Liquid

N/A 10/7/2010 Sample #1 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (1)

Non-Continental Liquid

N/A 10/8/2010 Sample #2 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (1)

Non-Continental Liquid

N/A 10/8/2010 Sample #3 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (2)

Non-Continental Liquid

N/A 10/9/2010 Sample #1 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (2)

Non-Continental Liquid

N/A 10/9/2010 Sample #2 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (2)

Non-Continental Liquid

N/A 10/9/2010 Sample #3 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5 INUSSteelGaryWorks O4B10459 ICR Phase II - ERT ERT Liquid N/A 9/9/2009 M10-2A After May 2008 90.1 81.09 81.093.293891371 3.3 INUSSteelGaryWorks O4B10459 ICR Phase II - ERT ERT Liquid N/A 9/9/2009 M10-2B After May 2008 90.1 81.09 81.093.293891371 3.3

MAUMass EU#7 ICR Phase I Organic HAP and COEU#7Oil Liquid N/A 3/1/1995 Sample #1 On/Before May 2008 89.5 80.55 89.5 0 89.53.635507186 3.6

MAUMass EU#7 ICR Phase I Organic HAP and COEU#7Oil Liquid N/A 3/1/1995 Sample #2 On/Before May 2008 89.5 80.55 89.5 0 89.53.635507186 3.6

MAUMass EU#7 ICR Phase I Organic HAP and COEU#7Oil Liquid N/A 3/1/1995 Sample #3 On/Before May 2008 89.5 80.55 89.5 0 89.53.635507186 3.6 MIConsumerEnergyCo-CampbellEUAUXBLR12 ICR Phase II - Templates CO Liquid N/A 9/1/2009 Sample #1 After May 2008 104.1 93.69 93.693.805705791 3.8 MIConsumerEnergyCo-CampbellEUAUXBLR12 ICR Phase II - Templates CO Liquid N/A 9/1/2009 Sample #2 After May 2008 104.1 93.69 93.693.805705791 3.8 MIConsumerEnergyCo-CampbellEUAUXBLR12 ICR Phase II - Templates CO Liquid N/A 9/1/2009 Sample #3 After May 2008 104.1 93.69 93.693.805705791 3.8 MNGPDuluth EU33 Boiler #3 ICR Phase II - ERT ERT Liquid N/A 8/4/2009 1 After May 2008 51.2 46.08 50 22.3 0 502.031009601 2.0 MNGPDuluth EU33 Boiler #3 ICR Phase II - ERT ERT Liquid N/A 8/4/2009 2 After May 2008 51.2 46.08 50 22.3 0 502.031009601 2.0 MNGPDuluth EU33 Boiler #3 ICR Phase II - ERT ERT Liquid N/A 8/5/2009 3 After May 2008 51.2 46.08 50 22.3 0 502.031009601 2.0 NCCampLejeuneMCB C-CG-650-84B ICR Phase I Organic HAP and CO C-CG-650-84B Liquid N/A 3/18/2008 Sample #1 On/Before May 2008 484 435.6 435.617.69415565 18.0 NCCampLejeuneMCB C-CG-650-84B ICR Phase I Organic HAP and CO C-CG-650-84B Liquid N/A 3/18/2008 Sample #2 On/Before May 2008 484 435.6 435.617.69415565 18.0 NCCampLejeuneMCB C-CG-650-84B ICR Phase I Organic HAP and CO C-CG-650-84B Liquid N/A 3/18/2008 Sample #3 On/Before May 2008 484 435.6 435.617.69415565 18.0 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Liquid N/A 8/25/2009 1 After May 2008 484 435.6 435.617.69415565 18.0 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Liquid N/A 8/25/2009 2 After May 2008 484 435.6 435.617.69415565 18.0 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Liquid N/A 8/26/2009 3 After May 2008 484 435.6 435.617.69415565 18.0 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Liquid N/A 8/26/2009 4 After May 2008 484 435.6 435.617.69415565 18.0 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Liquid N/A 8/27/2009 5 After May 2008 484 435.6 435.617.69415565 18.0 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Liquid N/A 8/27/2009 6 After May 2008 484 435.6 435.617.69415565 18.0 NDGreatPlainsSynfuels BF-5002A ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #1 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5002A ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #2 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5002A ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #3 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5002B ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #1 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5002B ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #2 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5002B ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #3 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101A ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #1 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101A ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #2 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101A ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #3 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101B ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #1 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101B ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #2 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101B ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #3 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101S ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #1 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101S ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #2 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NDGreatPlainsSynfuels BF-5101S ICR Phase II - Voluntary Additional CO from Test Report

Liquid N/A 9/13/2010 Sample #3 After May 2008 1000 900 247.3 136.9 0 247.310.04537349 10.0 NJMerckRahway E750010 - Boiler #10 ICR Phase I Organic HAP and CO (8) Liquid N/A 10/28/2003Sample #1 On/Before May 2008 45.8 41.22 45.8 30.9 14.79 45.81.860404795 1.9 NJMerckRahway E750010 - Boiler #10 ICR Phase I Organic HAP and CO (8) Liquid N/A 10/29/2003Sample #2 On/Before May 2008 45.8 41.22 45.8 30.9 14.79 45.81.860404795 1.9 NJMerckRahway E750010 - Boiler #10 ICR Phase I Organic HAP and CO (8) Liquid N/A 10/29/2003Sample #3 On/Before May 2008 45.8 41.22 45.8 30.9 14.79 45.81.860404795 1.9 NJMerckRahway E750011 - Boiler #11 ICR Phase I Organic HAP and CO (10) Liquid N/A 3/5/2008 Sample #1 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750011 - Boiler #11 ICR Phase I Organic HAP and CO (10) Liquid N/A 3/5/2008 Sample #2 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750011 - Boiler #11 ICR Phase I Organic HAP and CO (10) Liquid N/A 3/5/2008 Sample #3 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750012 - Boiler #12 ICR Phase I Organic HAP and CO (12) Liquid N/A 3/7/2008 Sample #1 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0



### Page 2 of 7

### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs**  NJMerckRahway E750012 - Boiler #12 ICR Phase I Organic HAP and CO (12) Liquid N/A 3/7/2008 Sample #2 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750012 - Boiler #12 ICR Phase I Organic HAP and CO (12) Liquid N/A 3/7/2008 Sample #3 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750009 - Boiler #9 ICR Phase I Organic HAP and CO (6) Liquid N/A 3/14/2008 Sample #1 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750009 - Boiler #9 ICR Phase I Organic HAP and CO (6) Liquid N/A 3/14/2008 Sample #2 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750009 - Boiler #9 ICR Phase I Organic HAP and CO (6) Liquid N/A 3/14/2008 Sample #3 On/Before May 2008 25.8 23.22 25.8 12.5 25.81.048000954 1.0 NJMerckRahway E750003 - Boiler #3 ICR Phase I Organic HAP and CO (2) Liquid N/A 3/12/2008 Sample #1 On/Before May 2008 25.8 23.22 23.220.943200859 0.9 NJMerckRahway E750003 - Boiler #3 ICR Phase I Organic HAP and CO (2) Liquid N/A 3/12/2008 Sample #2 On/Before May 2008 25.8 23.22 23.220.943200859 0.9 NJMerckRahway E750003 - Boiler #3 ICR Phase I Organic HAP and CO (2) Liquid N/A 3/12/2008 Sample #3 On/Before May 2008 25.8 23.22 23.220.943200859 0.9 NJMerckRahway E750005 - Boiler #5 ICR Phase I Organic HAP and CO (4) Liquid N/A 3/18/2008 Sample #1 On/Before May 2008 25.8 23.22 23.220.943200859 0.9 NJMerckRahway E750005 - Boiler #5 ICR Phase I Organic HAP and CO (4) Liquid N/A 3/18/2008 Sample #2 On/Before May 2008 25.8 23.22 23.220.943200859 0.9 NJMerckRahway E750005 - Boiler #5 ICR Phase I Organic HAP and CO (4) Liquid N/A 3/18/2008 Sample #3 On/Before May 2008 25.8 23.22 23.220.943200859 0.9 NJPolyOne E200 Boiler #2 ICR Phase II - Voluntary CO (2) Liquid N/A 6/10/2010 Sample #1 After May 2008 26 23.4 26 13 0 261.056124993 1.1 NJPolyOne E200 Boiler #2 ICR Phase II - Voluntary CO (2) Liquid N/A 6/10/2010 Sample #2 After May 2008 26 23.4 26 13 0 261.056124993 1.1 NJPolyOne E200 Boiler #2 ICR Phase II - Voluntary CO (2) Liquid N/A 6/10/2010 Sample #3 After May 2008 26 23.4 26 13 0 261.056124993 1.1 NJPolyOne E200 Boiler #2 ICR Phase II - Voluntary CO Liquid N/A 6/9/2010 Sample #1 After May 2008 26 23.4 26 13 0 261.056124993 1.1 NJPolyOne E200 Boiler #2 ICR Phase II - Voluntary CO Liquid N/A 6/9/2010 Sample #2 After May 2008 26 23.4 26 13 0 261.056124993 1.1 NJPolyOne E200 Boiler #2 ICR Phase II - Voluntary CO Liquid N/A 6/9/2010 Sample #3 After May 2008 26 23.4 26 13 0 261.056124993 1.1 NJVinelandMuniElectric-HowardDown Unit 9 ICR Phase II - ERT ERT Liquid N/A 7/21/2009 1 After May 2008 45.4 40.86 40.861.659741046 1.7 NJVinelandMuniElectric-HowardDown Unit 9 ICR Phase II - ERT ERT Liquid N/A 7/22/2009 2 After May 2008 45.4 40.86 40.861.659741046 1.7 NJVinelandMuniElectric-HowardDown Unit 9 ICR Phase II - ERT ERT Liquid N/A 7/22/2009 3 After May 2008 45.4 40.86 40.861.659741046 1.7 OHOSUColumbus B140 ICR Phase I Organic HAP and CO Liquid N/A 2/2/2005 Sample #1 On/Before May 2008 100 90 84.9 903.655817282 3.7 OHOSUColumbus B140 ICR Phase I Organic HAP and CO Liquid N/A 2/2/2005 Sample #2 On/Before May 2008 100 90 84.9 903.655817282 3.7 OHOSUColumbus B140 ICR Phase I Organic HAP and CO Liquid N/A 2/2/2005 Sample #3 On/Before May 2008 100 90 84.9 903.655817282 3.7 ORGeorgiaPacificWaunaMill EU33 - Power Boiler ICR Phase I Org HAP & CO Pwr Blr EU-33 Oil Liquid N/A 3/14/2007 Sample #1 On/Before May 2008 100 90 1000 903.655817282 3.7 ORGeorgiaPacificWaunaMill EU33 - Power Boiler ICR Phase I Org HAP & CO Pwr Blr EU-33 Oil Liquid N/A 3/14/2007 Sample #2 On/Before May 2008 100 90 1000 903.655817282 3.7 ORGeorgiaPacificWaunaMill EU33 - Power Boiler ICR Phase I Org HAP & CO Pwr Blr EU-33 Oil Liquid N/A 3/14/2007 Sample #3 On/Before May 2008 100 90 1000 903.655817282 3.7 PABoeingRidleyPark 033 ICR Phase II - ERT ERT Liquid N/A 9/22/2009 ITM-1 After May 2008 100 90 903.655817282 3.7 PABoeingRidleyPark 033 ICR Phase II - ERT ERT Liquid N/A 9/23/2009 ITM-2 After May 2008 100 90 903.655817282 3.7 PABoeingRidleyPark 033 ICR Phase II - ERT ERT Liquid N/A 9/24/2009 ITM-3 After May 2008 100 90 903.655817282 3.7 PAConemaughPowerPlantNewFlorence Aux Boiler B ICR Phase I Additional CO from Test Report Liquid N/A 10/17/2006Sample #1 On/Before May 2008 176.2 158.58 158.586.441550051 6.4 PAConemaughPowerPlantNewFlorence Aux Boiler B ICR Phase I Additional CO from Test Report Liquid N/A 10/17/2006Sample #2 On/Before May 2008 176.2 158.58 158.586.441550051 6.4 PAConemaughPowerPlantNewFlorence Aux Boiler B ICR Phase I Additional CO from Test Report Liquid N/A 10/17/2006Sample #3 On/Before May 2008 176.2 158.58 158.586.441550051 6.4 PAKeystonePowerPlantSheloctaAux Boiler A ICR Phase I Organic HAP and CO Liquid N/A 6/22/1993 Sample #1 On/Before May 2008 299 269.1 269.110.93089367 11.0 PAKeystonePowerPlantSheloctaAux Boiler A ICR Phase I Organic HAP and CO Liquid N/A 6/22/1993 Sample #2 On/Before May 2008 299 269.1 269.110.93089367 11.0 PAKeystonePowerPlantSheloctaAux Boiler B ICR Phase I Organic HAP and CO (2) Liquid N/A 6/22/1993 Sample #1 On/Before May 2008 299 269.1 269.110.93089367 11.0 PAKeystonePowerPlantSheloctaAux Boiler B ICR Phase I Organic HAP and CO (2) Liquid N/A 6/22/1993 Sample #2 On/Before May 2008 299 269.1 269.110.93089367 11.0 SCMilliken-Dewey D30 ICR Phase II - Templates CO Liquid N/A 8/11/2009 Sample #1 After May 2008 2244 2019.6 2244 1119 895.6 2244 91.1517109 91.0 SCMilliken-Dewey D30 ICR Phase II - Templates CO Liquid N/A 8/11/2009 Sample #2 After May 2008 2244 2019.6 2244 1119 895.6 2244 91.1517109 91.0 SCMilliken-Dewey D30 ICR Phase II - Templates CO Liquid N/A 8/11/2009 Sample #3 After May 2008 2244 2019.6 2244 1119 895.6 2244 91.1517109 91.0 TNInvistaChattanooga EU003 - Vaporizer #2 ICR Phase II - Templates CO Liquid N/A 7/28/2009 Sample #1 After May 2008 49.9 44.91 44.911.824252824 1.8 TNInvistaChattanooga EU003 - Vaporizer #2 ICR Phase II - Templates CO Liquid N/A 7/28/2009 Sample #2 After May 2008 49.9 44.91 44.911.824252824 1.8 TNInvistaChattanooga EU003 - Vaporizer #2 ICR Phase II - Templates CO Liquid N/A 7/29/2009 Sample #3 After May 2008 49.9 44.91 44.911.824252824 1.8 TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86 ICR Phase II - Templates CO Liquid N/A 11/18/2009Sample #1 After May 2008 25 22.5 501 25 10 0 251.015504801 1.0 TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86 ICR Phase II - Templates CO Liquid N/A 11/18/2009Sample #2 After May 2008 25 22.5 501 25 10 0 251.015504801 1.0 TNMilanArmyAmmunitionPlantD88L-1, Source #27-0010-86 ICR Phase II - Templates CO Liquid N/A 11/19/2009Sample #3 After May 2008 25 22.5 501 25 10 0 251.015504801 1.0 VANewportNewsShipbuildingDryDock 78-E1 ICR Phase II - ERT ERT Liquid N/A 11/17/2009CO-1 After May 2008 89.8 80.82 80.823.282923919 3.3 VANewportNewsShipbuildingDryDock 78-E1 ICR Phase II - ERT ERT Liquid N/A 11/18/2009CO-2 After May 2008 89.8 80.82 80.823.282923919 3.3 VANewportNewsShipbuildingDryDock 78-E1 ICR Phase II - ERT ERT Liquid N/A 11/18/2009CO-3 After May 2008 89.8 80.82 80.823.282923919 3.3 WVMountainStateCarbonFollansbee S1 ICR Phase I Organic HAP and CO Process GasN/A 9/5/2007 Sample #1 On/Before May 2008 17 9.217 0.113 170.756637298 0.8 WVMountainStateCarbonFollansbee S1 ICR Phase I Organic HAP and CO Process GasN/A 9/5/2007 Sample #2 On/Before May 2008 17 9.13 0.092 170.756637298 0.8 WVMountainStateCarbonFollansbee S1 ICR Phase I Organic HAP and CO Process GasN/A 9/5/2007 Sample #3 On/Before May 2008 17 9.315 0.12 170.756637298 0.8 WVMountainStateCarbonFollansbee S1 ICR Phase II - Test Report Phase II CO From Test Report

Process GasN/A 10/20/2009Sample #1 After May 2008 17 9.2 0.2 170.756637298 0.8 WVMountainStateCarbonFollansbee S1 ICR Phase II - Test Report Phase II CO From Test Report

Process GasN/A 10/21/2009Sample #2 After May 2008 17 9.2 0.2 170.756637298 0.8 WVMountainStateCarbonFollansbee S1 ICR Phase II - Test Report Phase II CO From Test Report

Process GasN/A 10/21/2009Sample #3 After May 2008 17.2 8.8 -0.2 17.20.756637298 0.8 ALIPCourtland No. 3 Combination Boier / 11CU301 ICR Phase II - Templates

CO Biomass FB 7/8/2009 Sample #1 After May 2008 1500 1350 1002.4 724 3 135054.83725923 55.0 ALIPCourtland No. 3 Combination Boier / 11CU301 ICR Phase II - Templates

CO Biomass FB 7/9/2009 Sample #2 After May 2008 1500 1350 1002.4 297 5 135054.83725923 55.0 ALIPCourtland No. 3 Combination Boier / 11CU301 ICR Phase II - Templates

CO Biomass FB 7/10/2009 Sample #3 After May 2008 1500 1350 1002.4 298 -1 135054.83725923 55.0 ARWestFraserHuttig SN-24 ICR Phase I Organic HAP and CO (2) Biomass Stoker/SlopedGrate/Other 3/1/2005 Sample #1 On/Before May 2008 2000 1800 1510 1524.45 665.55 0.81 1524.4561.92345173 62.0 ARWestFraserHuttig SN-24 ICR Phase I Organic HAP and CO (2) Biomass Stoker/SlopedGrate/Other 3/1/2005 Sample #2 On/Before May 2008 2000 1800 1510 1524.45 665.55 0.81 1524.4561.92345173 62.0 ARWestFraserHuttig SN-24 ICR Phase I Organic HAP and CO (2) Biomass Stoker/SlopedGrate/Other 3/1/2005 Sample #3 On/Before May 2008 2000 1800 1510 1524.45 665.55 0.81 1524.4561.92345173 62.0 ARWestFraserHuttig SN-24 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 8/6/2009 Sample #1 After May 2008 1717 1720.56 968.17 0.5 1720.5669.88947759 70.0 ARWestFraserHuttig SN-24 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 8/6/2009 Sample #2 After May 2008 1717 1720.56 968.17 0.5 1720.5669.88947759 70.0 ARWestFraserHuttig SN-24 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 8/6/2009 Sample #3 After May 2008 1717 1720.56 968.17 0.5 1720.5669.88947759 70.0 ARWestFraserHuttig SN-24 ICR Phase II - Voluntary Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/18/2010 Sample #1 After May 2008 915 915.03 403.05 0.09 915.0337.16869431 37.0 ARWestFraserHuttig SN-24 ICR Phase II - Voluntary Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/18/2010 Sample #2 After May 2008 915 915.03 403.05 0.09 915.0337.16869431 37.0 ARWestFraserHuttig SN-24 ICR Phase II - Voluntary Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/18/2010 Sample #3 After May 2008 915 915.03 403.05 0.09 915.0337.16869431 37.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase I Organic HAP and CO SN-45 (2) Biomass Fuel Cell 12/3/2003 Sample #1 On/Before May 2008 5967.74 2931.6 -0.26 5967.74242.4107447 240.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase I Organic HAP and CO SN-45 (2) Biomass Fuel Cell 12/3/2003 Sample #2 On/Before May 2008 5967.74 2931.6 -0.26 5967.74242.4107447 240.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase I Organic HAP and CO SN-45 (2) Biomass Fuel Cell 12/3/2003 Sample #3 On/Before May 2008 5967.74 2931.6 -0.26 5967.74242.4107447 240.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase I Organic HAP and CO SN-45 Biomass Fuel Cell 9/28/2004 Sample #1 On/Before May 2008 10000 9000 7008.49 3579.56 1.26 7008.49284.6862096 280.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase I Organic HAP and CO SN-45 Biomass Fuel Cell 9/28/2004 Sample #2 On/Before May 2008 10000 9000 7008.49 3579.56 1.26 7008.49284.6862096 280.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase I Organic HAP and CO SN-45 Biomass Fuel Cell 9/28/2004 Sample #3 On/Before May 2008 10000 9000 7008.49 3579.56 1.26 7008.49284.6862096 280.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates CO - D&F Results

Biomass Fuel Cell 7/17/2009 Sample #1 After May 2008 347.19 184.82 0.38 347.1914.10292447 14.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates CO - D&F Results

Biomass Fuel Cell 7/17/2009 Sample #2 After May 2008 347.19 184.82 0.38 347.1914.10292447 14.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates CO - D&F Results

Biomass Fuel Cell 7/20/2009 Sample #3 After May 2008 347.19 184.82 0.38 347.1914.10292447 14.0



### Page 3 of 7

### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs**  GATempleInlandRome WF ICR Phase II - Templates CO Biomass FB 7/29/2009 Sample #1 After May 2008 400 360 499 300 150.8 2.7 30012.18605761 12.0 GATempleInlandRome WF ICR Phase II - Templates CO Biomass FB 7/29/2009 Sample #2 After May 2008 400 360 499 300 150.8 4.3 30012.18605761 12.0 GATempleInlandRome WF ICR Phase II - Templates CO Biomass FB 7/30/2009 Sample #3 After May 2008 400 360 499 300 150.8 5 30012.18605761 12.0 GATempleInlandThomson BW-B001 ICR Phase I Organic HAP and CO Biomass Suspension Burner 1/30/2003 Sample #1 On/Before May 2008 299 269.1 280.1 297 -1 29712.06419703 12.0 GATempleInlandThomson BW-B001 ICR Phase I Organic HAP and CO Biomass Suspension Burner 1/30/2003 Sample #2 On/Before May 2008 299 269.1 280.1 297 1 29712.06419703 12.0 GATempleInlandThomson BW-B001 ICR Phase I Organic HAP and CO Biomass Suspension Burner 1/30/2003 Sample #3 On/Before May 2008 299 269.1 280.1 297 1 29712.06419703 12.0 GATempleInlandThomson BW-B001 ICR Phase II - Voluntary Additional CO Data

Biomass Suspension Burner 12/3/2008 Sample #1 On/Before May 2008 100 50 1 1004.062019202 4.1 GATempleInlandThomson BW-B001 ICR Phase II - Voluntary Additional CO Data

Biomass Suspension Burner 12/3/2008 Sample #3 On/Before May 2008 100 49 0 1004.062019202 4.1 GATempleInlandThomson BW-B001 ICR Phase II - Voluntary Additional CO Data

Biomass Suspension Burner 12/3/2008 Sample #3 On/Before May 2008 100 49 1 1004.062019202 4.1 IDChilcoLakeSawmill HFB1 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 7/29/2009 Sample #1 After May 2008 1110 508 111045.08841315 45.0 IDChilcoLakeSawmill HFB1 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 7/29/2009 Sample #2 After May 2008 1110 508 111045.08841315 45.0 IDChilcoLakeSawmill HFB1 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 7/29/2009 Sample #3 After May 2008 1110 508 111045.08841315 45.0 INConsolidatedGrainandBargeP17B ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/5/2008 Sample #1 On/Before May 2008 104.1 93.69 104.1 104.1 52.5 0.2 104.1 4.22856199 4.2 INConsolidatedGrainandBargeP17B ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/5/2008 Sample #2 On/Before May 2008 104.1 93.69 104.1 104.1 52.5 0.2 104.1 4.22856199 4.2 INConsolidatedGrainandBargeP17B ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/5/2008 Sample #3 On/Before May 2008 104.1 93.69 104.1 104.1 52.5 0.2 104.1 4.22856199 4.2 INConsolidatedGrainandBargeP17C ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/5/2008 Sample #1 On/Before May 2008 104.1 93.69 104.1 104.1 52.5 0.2 104.1 4.22856199 4.2 INConsolidatedGrainandBargeP17C ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/5/2008 Sample #2 On/Before May 2008 104.1 93.69 104.1 104.1 52.5 0.2 104.1 4.22856199 4.2 INConsolidatedGrainandBargeP17C ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/5/2008 Sample #3 On/Before May 2008 104.1 93.69 104.1 104.1 52.5 0.2 104.1 4.22856199 4.2 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (5)

Biomass Stoker/SlopedGrate/Other 2/5/1997 Sample #1 On/Before May 2008 140 126 290 135 2 29011.77985569 12.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (5)

Biomass Stoker/SlopedGrate/Other 2/5/1997 Sample #2 On/Before May 2008 140 126 290 135 2 29011.77985569 12.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (5)

Biomass Stoker/SlopedGrate/Other 2/5/1997 Sample #3 On/Before May 2008 140 126 290 135 2 29011.77985569 12.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (4)

Biomass Stoker/SlopedGrate/Other 4/4/2000 Sample #1 On/Before May 2008 1000 900 552.61 294.56 0.2 552.6122.44712431 22.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (4)

Biomass Stoker/SlopedGrate/Other 4/4/2000 Sample #2 On/Before May 2008 1000 900 552.61 294.56 0.2 552.6122.44712431 22.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (4)

Biomass Stoker/SlopedGrate/Other 4/4/2000 Sample #3 On/Before May 2008 1000 900 552.61 294.56 0.2 552.6122.44712431 22.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (3)

Biomass Stoker/SlopedGrate/Other 5/8/2002 Sample #1 On/Before May 2008 293.44 264.096 293.44 149.74 0.27 293.4411.91958915 12.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (3)

Biomass Stoker/SlopedGrate/Other 5/8/2002 Sample #2 On/Before May 2008 293.44 264.096 293.44 149.74 0.27 293.4411.91958915 12.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (3)

Biomass Stoker/SlopedGrate/Other 5/8/2002 Sample #3 On/Before May 2008 293.44 264.096 293.44 149.74 0.27 293.4411.91958915 12.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/2/2005 Sample #1 On/Before May 2008 593.36 534.024 593.36 310.77 0.78 593.3624.10239714 24.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/2/2005 Sample #2 On/Before May 2008 593.36 534.024 593.36 310.77 0.78 593.3624.10239714 24.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/3/2005 Sample #3 On/Before May 2008 593.36 534.024 593.36 310.77 0.78 593.3624.10239714 24.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/3/2005 Sample #4 On/Before May 2008 593.36 534.024 593.36 310.77 0.78 593.3624.10239714 24.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/3/2005 Sample #5 On/Before May 2008 593.36 534.024 593.36 310.77 0.78 593.3624.10239714 24.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (2)

Biomass Stoker/SlopedGrate/Other 3/3/2005 Sample #6 On/Before May 2008 593.36 534.024 593.36 310.77 0.78 593.3624.10239714 24.0 MILPCSagola TOH-Wood ICR Phase I Organic HAP and CO-TOH Wood Biomass Stoker/SlopedGrate/Other 3/12/2008 Sample #1 On/Before May 2008 239 215.1 238.76 111.81 0.4 238.769.698477047 9.7 MILPCSagola TOH-Wood ICR Phase I Organic HAP and CO-TOH Wood Biomass Stoker/SlopedGrate/Other 3/12/2008 Sample #2 On/Before May 2008 239 215.1 238.76 111.81 0.4 238.769.698477047 9.7 MILPCSagola TOH-Wood ICR Phase I Organic HAP and CO-TOH Wood Biomass Stoker/SlopedGrate/Other 3/12/2008 Sample #3 On/Before May 2008 239 215.1 238.76 111.81 0.4 238.769.698477047 9.7 MILPCSagola TOH-Wood ICR Phase I Organic HAP and CO-TOH Wood Biomass Stoker/SlopedGrate/Other 3/12/2008 Sample #1 On/Before May 2008 238.76 214.884 238.76 111.81 0.4 238.769.698477047 9.7 MILPCSagola TOH-Wood ICR Phase I Organic HAP and CO-TOH Wood Biomass Stoker/SlopedGrate/Other 3/12/2008 Sample #2 On/Before May 2008 238.76 214.884 238.76 111.81 0.4 238.769.698477047 9.7 MILPCSagola TOH-Wood ICR Phase I Organic HAP and CO-TOH Wood Biomass Stoker/SlopedGrate/Other 3/12/2008 Sample #3 On/Before May 2008 238.76 214.884 238.76 111.81 0.4 238.769.698477047 9.7 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (1)

Biomass Stoker/SlopedGrate/Other 3/30/2011 Sample #1 After May 2008 511 459.9 511 251.2 0.12 51120.75691812 21.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (1)

Biomass Stoker/SlopedGrate/Other 3/30/2011 Sample #2 After May 2008 511 459.9 511 251.2 0.12 51120.75691812 21.0 MILPCSagola TOH-Wood ICR Phase II - Test Report Additional CO from Test Report (1)

Biomass Stoker/SlopedGrate/Other 3/30/2011 Sample #3 After May 2008 511 459.9 511 251.2 0.12 51120.75691812 21.0 MNAndersonCorpBayport Boiler 11 EU620 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 4/22/2008 Sample #1 On/Before May 2008 299 269.1 298.28 150.73 0.25 298.2812.11619088 12.0 MNAndersonCorpBayport Boiler 11 EU620 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 4/22/2008 Sample #2 On/Before May 2008 299 269.1 298.28 150.73 0.25 298.2812.11619088 12.0 MNAndersonCorpBayport Boiler 11 EU620 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 4/22/2008 Sample #3 On/Before May 2008 299 269.1 298.28 150.73 0.25 298.2812.11619088 12.0 MNAndersonCorpBayport Boiler 11 EU620 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 4/22/2008 Sample #1 On/Before May 2008 299 150.73 0.25 29912.14543741 12.0 MNAndersonCorpBayport Boiler 11 EU620 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 4/22/2008 Sample #2 On/Before May 2008 299 150.73 0.25 29912.14543741 12.0 MNAndersonCorpBayport Boiler 11 EU620 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 4/22/2008 Sample #3 On/Before May 2008 299 150.73 0.25 29912.14543741 12.0 MNAndersonCorpBayport Boiler 12 EU621 ICR Phase I Organic HAP and CO (8) Biomass Suspension Burner 4/22/2008 Sample #1 On/Before May 2008 299 269.1 298.28 150.73 0.25 298.2812.11619088 12.0 MNAndersonCorpBayport Boiler 12 EU621 ICR Phase I Organic HAP and CO (8) Biomass Suspension Burner 4/22/2008 Sample #2 On/Before May 2008 299 269.1 298.28 150.73 0.25 298.2812.11619088 12.0 MNAndersonCorpBayport Boiler 12 EU621 ICR Phase I Organic HAP and CO (8) Biomass Suspension Burner 4/22/2008 Sample #3 On/Before May 2008 299 269.1 298.28 150.73 0.25 298.2812.11619088 12.0 MNAndersonCorpBayport Boiler 12 EU621 ICR Phase I Organic HAP and CO (8) Biomass Suspension Burner 4/22/2008 Sample #1 On/Before May 2008 299 150.73 0.25 29912.14543741 12.0 MNAndersonCorpBayport Boiler 12 EU621 ICR Phase I Organic HAP and CO (8) Biomass Suspension Burner 4/22/2008 Sample #2 On/Before May 2008 299 150.73 0.25 29912.14543741 12.0 MNAndersonCorpBayport Boiler 12 EU621 ICR Phase I Organic HAP and CO (8) Biomass Suspension Burner 4/22/2008 Sample #3 On/Before May 2008 299 150.73 0.25 29912.14543741 12.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 9/12/2007 Sample #1 On/Before May 2008 872 784.8 860 0 86034.93336514 35.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 9/12/2007 Sample #2 On/Before May 2008 872 784.8 860 1 86034.93336514 35.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 9/12/2007 Sample #3 On/Before May 2008 872 784.8 860 6 86034.93336514 35.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -3) Biomass Stoker/SlopedGrate/Other 3/29/2004 Sample #1 On/Before May 2008 1987 709 397 216 70928.79971614 29.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -3) Biomass Stoker/SlopedGrate/Other 3/29/2004 Sample #2 On/Before May 2008 1987 709 397 216 70928.79971614 29.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -3) Biomass Stoker/SlopedGrate/Other 3/29/2004 Sample #3 On/Before May 2008 1987 709 397 216 70928.79971614 29.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -5 ) Biomass Stoker/SlopedGrate/Other 11/18/2005Sample #1 On/Before May 2008 500 450 197 0 45018.27908641 18.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -5 ) Biomass Stoker/SlopedGrate/Other 11/18/2005Sample #2 On/Before May 2008 500 450 197 0 45018.27908641 18.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -5 ) Biomass Stoker/SlopedGrate/Other 11/18/2005Sample #3 On/Before May 2008 500 450 197 0 45018.27908641 18.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -1) Biomass Stoker/SlopedGrate/Other 3/27/2006 Sample #1 On/Before May 2008 2017 722 402 204 72229.32777864 29.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -1) Biomass Stoker/SlopedGrate/Other 3/27/2006 Sample #2 On/Before May 2008 2017 722 402 204 72229.32777864 29.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -1) Biomass Stoker/SlopedGrate/Other 3/27/2006 Sample #3 On/Before May 2008 2017 722 402 204 72229.32777864 29.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -2) Biomass Stoker/SlopedGrate/Other 9/27/2007 Sample #1 On/Before May 2008 614 595 303 156 59524.16901425 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -2) Biomass Stoker/SlopedGrate/Other 9/27/2007 Sample #2 On/Before May 2008 614 595 303 156 59524.16901425 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase I Organic HAP and CO (AA-006 -2) Biomass Stoker/SlopedGrate/Other 9/27/2007 Sample #3 On/Before May 2008 614 595 303 156 59524.16901425 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (4)

Biomass Stoker/SlopedGrate/Other 1/20/2011 Sample #1 After May 2008 603 603 60324.49397579 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (4)

Biomass Stoker/SlopedGrate/Other 1/20/2011 Sample #2 After May 2008 603 603 60324.49397579 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (4)

Biomass Stoker/SlopedGrate/Other 1/20/2011 Sample #3 After May 2008 603 603 60324.49397579 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (2)

Biomass Stoker/SlopedGrate/Other 1/26/2010 Sample #1 After May 2008 353 317.7 705 353 178 0 35314.33892778 14.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (2)

Biomass Stoker/SlopedGrate/Other 1/26/2010 Sample #2 After May 2008 353 317.7 705 353 178 0 35314.33892778 14.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (2)

Biomass Stoker/SlopedGrate/Other 1/26/2010 Sample #3 After May 2008 353 317.7 705 353 178 0 35314.33892778 14.0



### Page 4 of 7

### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs**  MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (1)

Biomass Stoker/SlopedGrate/Other 1/27/2009 Sample #1 After May 2008 700 630 2003 581 294 0 58123.60033157 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (1)

Biomass Stoker/SlopedGrate/Other 1/27/2009 Sample #2 After May 2008 700 630 2003 581 294 0 58123.60033157 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (1)

Biomass Stoker/SlopedGrate/Other 1/27/2009 Sample #3 After May 2008 700 630 2003 581 294 0 58123.60033157 24.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (3)

Biomass Stoker/SlopedGrate/Other 7/20/2010 Sample #1 After May 2008 533 479.7 533 267 0 53321.65056235 22.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (3)

Biomass Stoker/SlopedGrate/Other 7/20/2010 Sample #2 After May 2008 533 479.7 533 267 0 53321.65056235 22.0 MSIPVicksburg Power Boiler-AA-006 ICR Phase II - Comments Additional CO from Comments (3)

Biomass Stoker/SlopedGrate/Other 7/20/2010 Sample #3 After May 2008 533 479.7 533 267 0 53321.65056235 22.0 MSWeyerhaeuserBruce AA-002 No. 2 Boiler ICR Phase II - Templates CO Biomass Fuel Cell 8/4/2009 Sample #1 After May 2008 998 488 3 99840.53895164 41.0 MSWeyerhaeuserBruce AA-002 No. 2 Boiler ICR Phase II - Templates CO Biomass Fuel Cell 8/4/2009 Sample #2 After May 2008 998 494 3 99840.53895164 41.0 MSWeyerhaeuserBruce AA-002 No. 2 Boiler ICR Phase II - Templates CO Biomass Fuel Cell 8/4/2009 Sample #3 After May 2008 998 508 0 99840.53895164 41.0 TNBowaterNewsprint Bubbling Fluidized Bed Boiler ICR Phase II - ERT ERT Biomass FB 8/5/2009 1 After May 2008 500 450 499 300 147 0 30012.18605761 12.0 TNBowaterNewsprint Bubbling Fluidized Bed Boiler ICR Phase II - ERT ERT Biomass FB 8/5/2009 2 After May 2008 500 450 499 300 147 0.3 30012.18605761 12.0 TNBowaterNewsprint Bubbling Fluidized Bed Boiler ICR Phase II - ERT ERT Biomass FB 8/6/2009 3 After May 2008 500 450 499 300 147 1 30012.18605761 12.0
TNDomtar2384 HFB1-1 ICR Phase II - ERT ERT Biomass FB 9/16/2009 1 After May 2008 325 292.5 501 252.4 125.4 0 252.410.25253647 10.0
TNDomtar2384 HFB1-1 ICR Phase II - ERT ERT Biomass FB 9/16/2009 2 After May 2008 325 292.5 501 252.4 125.8 0 252.410.25253647 10.0
TNDomtar2384 HFB1-1 ICR Phase II - ERT ERT Biomass FB 9/17/2009 3 After May 2008 325 292.5 501 252.4 125.4 0 252.410.25253647 10.0 TXDibollTemple-Inland PB-44 ICR Phase I Organic HAP and CO Biomass Suspension Burner 6/29/2007 Sample #1 On/Before May 2008 100 90 100 1004.062019202 4.1 TXDibollTemple-Inland PB-44 ICR Phase I Organic HAP and CO Biomass Suspension Burner 6/29/2007 Sample #2 On/Before May 2008 100 90 100 1004.062019202 4.1 TXDibollTemple-Inland PB-44 ICR Phase I Organic HAP and CO Biomass Suspension Burner 6/29/2007 Sample #3 On/Before May 2008 100 90 100 1004.062019202 4.1 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO (3) Biomass Stoker/SlopedGrate/Other 10/26/2005Sample #1 On/Before May 2008 469 236.3 116.9 46919.05087006 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO (3) Biomass Stoker/SlopedGrate/Other 10/26/2005Sample #2 On/Before May 2008 472.9 236.9 113.9 472.919.20928881 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO (3) Biomass Stoker/SlopedGrate/Other 10/26/2005Sample #3 On/Before May 2008 465 237.8 121.5 46518.88838929 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 8/22/2007 Sample #1 On/Before May 2008 473.4 242.6 -3.61 473.4 19.2295989 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 8/22/2007 Sample #2 On/Before May 2008 473.4 242.8 -3.68 473.4 19.2295989 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 8/22/2007 Sample #3 On/Before May 2008 473.4 242.3 -3.86 473.4 19.2295989 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO (2) Biomass Stoker/SlopedGrate/Other 8/22/2007 Sample #4 On/Before May 2008 473.4 241.6 -3.55 473.4 19.2295989 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO (2) Biomass Stoker/SlopedGrate/Other 8/22/2007 Sample #5 On/Before May 2008 473.4 242.6 -3.27 473.4 19.2295989 19.0 WIFlambeauRiverPaper B24 ICR Phase I Organic HAP and CO (2) Biomass Stoker/SlopedGrate/Other 8/22/2007 Sample #6 On/Before May 2008 473.4 245.6 -2.27 473.4 19.2295989 19.0 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase I Organic HAP and CO B10 Biomass FB 1/14/1999 Sample #1 On/Before May 2008 271.4 271.4 271.411.02432012 11.0 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase I Organic HAP and CO B10 Biomass FB 1/14/1999 Sample #2 On/Before May 2008 271.4 271.4 271.411.02432012 11.0 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase I Organic HAP and CO B10 Biomass FB 1/14/1999 Sample #3 On/Before May 2008 271.4 271.4 271.411.02432012 11.0 WVAmericanWoodmark B1 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 3/23/2005 Sample #1 On/Before May 2008 2280 1510 750 228092.61403781 93.0 WVAmericanWoodmark B1 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 3/23/2005 Sample #2 On/Before May 2008 2280 1510 750 228092.61403781 93.0 WVAmericanWoodmark B1 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 3/23/2005 Sample #3 On/Before May 2008 2280 1510 750 228092.61403781 93.0 WVWeyerhaeuserBuckhannon001-01 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 8/23/2005 Sample #1 On/Before May 2008 1000 900 998.23 497.1 249.8 998.2340.54829428 41.0 WVWeyerhaeuserBuckhannon001-01 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 8/23/2005 Sample #2 On/Before May 2008 1000 900 998.23 497.1 249.8 998.2340.54829428 41.0 WVWeyerhaeuserBuckhannon001-01 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 8/23/2005 Sample #3 On/Before May 2008 1000 900 998.23 497.1 249.8 998.2340.54829428 41.0 WVWeyerhaeuserBuckhannon001-01 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 8/24/2010 Sample #1 After May 2008 1000 900 5880 1002.79 500.61 0.04 1002.7940.73352236 41.0 WVWeyerhaeuserBuckhannon001-01 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 8/24/2010 Sample #2 After May 2008 1000 900 5880 1002.79 500.61 0.04 1002.7940.73352236 41.0 WVWeyerhaeuserBuckhannon001-01 ICR Phase II - Voluntary Additional CO from Test Report

Biomass Stoker/SlopedGrate/Other 8/24/2010 Sample #3 After May 2008 1000 900 5880 1002.79 500.61 0.04 1002.7940.73352236 41.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 121799 Bagasse Suspension/Grate 12/17/1999Sample #1 On/Before May 2008 645.7 358.5 2.8 645.726.22845799 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 121799 Bagasse Suspension/Grate 12/17/1999Sample #2 On/Before May 2008 645.7 358.5 2.8 645.726.22845799 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 121799 Bagasse Suspension/Grate 12/17/1999Sample #3 On/Before May 2008 645.7 358.5 2.8 645.726.22845799 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 013100 Bagasse Suspension/Grate 1/31/2000 Sample #1 On/Before May 2008 649.2 348.8 6 649.226.37062866 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 013100 Bagasse Suspension/Grate 1/31/2000 Sample #2 On/Before May 2008 639 341.3 8.5 639 25.9563027 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 013100 Bagasse Suspension/Grate 1/31/2000 Sample #3 On/Before May 2008 639 341.3 8.5 639 25.9563027 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010501 Bagasse Suspension/Grate 1/5/2001 Sample #1 On/Before May 2008 5000 4500 3000 2998.9 401 4.5 2998.9121.8158939 120.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010501 Bagasse Suspension/Grate 1/5/2001 Sample #2 On/Before May 2008 5000 4500 3000 2998.9 401 3.8 2998.9121.8158939 120.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010501 Bagasse Suspension/Grate 1/6/2001 Sample #3 On/Before May 2008 5000 4500 3000 2998.9 401 3.8 2998.9121.8158939 120.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010902 Bagasse Suspension/Grate 1/9/2002 Sample #1 On/Before May 2008 674.86 0.33 674.8627.41294279 27.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010902 Bagasse Suspension/Grate 1/9/2002 Sample #2 On/Before May 2008 654.62 -2.85 654.62 26.5907901 27.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010902 Bagasse Suspension/Grate 1/9/2002 Sample #3 On/Before May 2008 655.74 1.17 655.7426.63628472 27.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 111502 Bagasse Suspension/Grate 11/15/2002Sample #1 On/Before May 2008 3562 781can't read 3562 144.689124 140.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 111502 Bagasse Suspension/Grate 11/15/2002Sample #2 On/Before May 2008 3562 781can't read 3562 144.689124 140.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 111502 Bagasse Suspension/Grate 11/15/2002Sample #3 On/Before May 2008 3562 781can't read 3562 144.689124 140.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 123003 Bagasse Suspension/Grate 12/30/2003Sample #1 On/Before May 2008 812.35 0.38 812.3532.99781299 33.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 123003 Bagasse Suspension/Grate 12/30/2003Sample #2 On/Before May 2008 802.52 1.29 802.52 32.5985165 33.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 123003 Bagasse Suspension/Grate 12/30/2003Sample #3 On/Before May 2008 813.72 1.17 813.7233.05346265 33.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 020405 Bagasse Suspension/Grate 2/4/2005 Sample #1 On/Before May 2008 646.19 21.89 646.1926.24836188 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 020405 Bagasse Suspension/Grate 2/4/2005 Sample #2 On/Before May 2008 646.19 22.82 646.1926.24836188 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 020405 Bagasse Suspension/Grate 2/4/2005 Sample #3 On/Before May 2008 646.84 20 646.8426.27476501 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP andCO 050305-050505 Bagasse Suspension/Grate 5/3/2005 Sample #1 On/Before May 2008 636.34 291.51 0.25 636.3425.84825299 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP andCO 050305-050505 Bagasse Suspension/Grate 5/3/2005 Sample #2 On/Before May 2008 636.34 291.51 0.25 636.3425.84825299 26.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010506 Bagasse Suspension/Grate 1/5/2006 Sample #1 On/Before May 2008 621.41 8.85 621.4125.24179353 25.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010506 Bagasse Suspension/Grate 1/5/2006 Sample #2 On/Before May 2008 623.51 6.35 623.5125.32709593 25.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 010506 Bagasse Suspension/Grate 1/5/2006 Sample #3 On/Before May 2008 626.27 9.34 626.2725.43920766 25.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 012507 Bagasse Suspension/Grate 1/25/2007 Sample #1 On/Before May 2008 608.1 547.29 6500 608.1 608.124.70113877 25.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 012507 Bagasse Suspension/Grate 1/25/2007 Sample #2 On/Before May 2008 608.1 547.29 6500 608.1 608.124.70113877 25.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 012507 Bagasse Suspension/Grate 1/25/2007 Sample #3 On/Before May 2008 608.1 547.29 6500 608.1 608.124.70113877 25.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 012408 Bagasse Suspension/Grate 1/24/2008 Sample #1 On/Before May 2008 8991.2 907.8 2.51 8991.2365.2242705 370.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 012408 Bagasse Suspension/Grate 1/24/2008 Sample #2 On/Before May 2008 8991.2 907.8 2.51 8991.2365.2242705 370.0 FLUSSugarCorp Boiler No. 7 ICR Phase I Organic HAP and CO 012408 Bagasse Suspension/Grate 1/24/2008 Sample #3 On/Before May 2008 8991.2 907.8 2.51 8991.2365.2242705 370.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 032405 Bagasse Suspension/Grate 3/24/2005 Sample #1 On/Before May 2008 643.18 354.25 15.15 643.1826.12609511 26.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 032405 Bagasse Suspension/Grate 3/24/2005 Sample #2 On/Before May 2008 643.18 347.96 11.13 643.1826.12609511 26.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 032405 Bagasse Suspension/Grate 3/24/2005 Sample #3 On/Before May 2008 626.34 336.81 3.53 626.3425.44205107 25.0 FLUSSugarCorp Boiler No. 8 Bagasse Suspension/Grate 1/11/2006 Sample #5 On/Before May 2008 1000 900 649 616.6 -6.34 90036.55817282 37.0



### Page 5 of 7

### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs**  FLUSSugarCorp Boiler No. 8 Bagasse Suspension/Grate 1/11/2006 Sample #6 On/Before May 2008 1000 900 649 613.81 -4.1 90036.55817282 37.0 FLUSSugarCorp Boiler No. 8 Bagasse Suspension/Grate 1/11/2006 Sample #7 On/Before May 2008 1000 900 649 613.97 -3.63 90036.55817282 37.0 FLUSSugarCorp Boiler No. 8 Bagasse Suspension/Grate 1/11/2006 Sample #8 On/Before May 2008 1000 900 649 614.76 -2.95 90036.55817282 37.0 FLUSSugarCorp Boiler No. 8 Bagasse Suspension/Grate 1/11/2006 Sample #9 On/Before May 2008 1000 900 649 614.75 -3.1 90036.55817282 37.0 FLUSSugarCorp Boiler No. 8 Bagasse Suspension/Grate 1/11/2006 Sample #10On/Before May 2008 1000 900 649 614.38 -3.39 90036.55817282 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 010507 Bagasse Suspension/Grate 1/5/2007 Sample #1 On/Before May 2008 908.32 598.2 2.78 908.3236.89613282 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 010507 Bagasse Suspension/Grate 1/5/2007 Sample #2 On/Before May 2008 908.32 593.6 0.75 908.3236.89613282 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 010507 Bagasse Suspension/Grate 1/5/2007 Sample #3 On/Before May 2008 908.32 592.31 2.09 908.3236.89613282 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 010507 Bagasse Suspension/Grate 1/5/2007 Sample #3 On/Before May 2008 908.32 591.06 2.85 908.3236.89613282 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 112907 Bagasse Suspension/Grate 11/29/2007Sample #1 On/Before May 2008 906.44 447.63 1.76 906.4436.81976686 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 112907 Bagasse Suspension/Grate 11/29/2007Sample #2 On/Before May 2008 906.44 441.85 1.55 906.4436.81976686 37.0 FLUSSugarCorp Boiler No. 8 ICR Phase I Organic HAP and CO 112907 Bagasse Suspension/Grate 11/29/2007Sample #3 On/Before May 2008 906.44 450.46 1.54 906.4436.81976686 37.0 HIPuuneneSugarMill Boiler 3 ICR Phase II - Voluntary Additional CO data (2)

Bagasse Suspension/Grate 5/24/2006 Sample #1 On/Before May 2008 90.3 81.27 90.3 90.3 3.66800334 3.7 HIPuuneneSugarMill Boiler 3 ICR Phase II - Voluntary Additional CO data (2)

Bagasse Suspension/Grate 5/24/2006 Sample #2 On/Before May 2008 90.3 81.27 90.3 90.3 3.66800334 3.7 HIPuuneneSugarMill Boiler 3 ICR Phase II - Voluntary Additional CO data (2)

Bagasse Suspension/Grate 5/25/2006 Sample #3 On/Before May 2008 90.3 81.27 90.3 90.3 3.66800334 3.7 ARAnthonyForestProducts SN-12 ICR Phase II - ERT ERT Biomass Fuel Cell 9/2/2009 1 After May 2008 1000 900 ? 501.1 0.2 90036.55817282 37.0 ARAnthonyForestProducts SN-12 ICR Phase II - ERT ERT Biomass Fuel Cell 9/2/2009 2 After May 2008 1000 900 ? 503.4 1.3 90036.55817282 37.0 ARAnthonyForestProducts SN-12 ICR Phase II - ERT ERT Biomass Fuel Cell 9/3/2009 3 After May 2008 1000 900 ? 498.2 0.4 90036.55817282 37.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates CO Biomass Fuel Cell 8/11/2009 Sample #1 After May 2008 348.17 180.64 0.72 348.1714.14273226 14.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates CO Biomass Fuel Cell 8/12/2009 Sample #2 After May 2008 349.21 178.64 0.32 349.2114.18497726 14.0 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates CO Biomass Fuel Cell 8/12/2009 Sample #3 After May 2008 349.21 178.64 0.32 349.2114.18497726 14.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 011905 Bagasse Suspension/Grate 1/19/2005 Sample #1 On/Before May 2008 5000 4500 ? 1478.5 -0.65 4500182.7908641 180.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 011905 Bagasse Suspension/Grate 1/19/2005 Sample #2 On/Before May 2008 5000 4500 ? 1487 2.25 4500182.7908641 180.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 011905 Bagasse Suspension/Grate 1/19/2005 Sample #3 On/Before May 2008 5000 4500 ? 1429.9 3 4500182.7908641 180.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 012006 Bagasse Suspension/Grate 1/20/2006 Sample #1 On/Before May 2008 5000 4500 ? 1466 2.65 4500182.7908641 180.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 012006 Bagasse Suspension/Grate 1/20/2006 Sample #2 On/Before May 2008 5000 4500 ? 1478.5 2.25 4500182.7908641 180.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 012006 Bagasse Suspension/Grate 1/20/2006 Sample #3 On/Before May 2008 5000 4500 ? 1475.5 3 4500182.7908641 180.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 012298 Bagasse Suspension/Grate 1/22/1998 Sample #1 On/Before May 2008 6271 3526 0 6271254.7292242 250.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 012298 Bagasse Suspension/Grate 1/22/1998 Sample #2 On/Before May 2008 6271 3526 0 6271254.7292242 250.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 012298 Bagasse Suspension/Grate 1/22/1998 Sample #3 On/Before May 2008 6271 3526 0 6271254.7292242 250.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121007 Bagasse Suspension/Grate 12/10/2007Sample #1 On/Before May 2008 9085? 1.24 9085369.0344445 370.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121007 Bagasse Suspension/Grate 12/10/2007Sample #2 On/Before May 2008 9085? 1.24 9085369.0344445 370.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121007 Bagasse Suspension/Grate 12/10/2007Sample #3 On/Before May 2008 9085? 1.24 9085369.0344445 370.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121304 Bagasse Suspension/Grate 12/13/2004Sample #1 On/Before May 2008 1376.5? -0.65 1376.555.91369432 56.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121304 Bagasse Suspension/Grate 12/13/2004Sample #2 On/Before May 2008 1367.9? 2.25 1367.955.56436067 56.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121304 Bagasse Suspension/Grate 12/13/2004Sample #3 On/Before May 2008 1370.3? 3 1370.355.66184913 56.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121702 Bagasse Suspension/Grate 12/17/2002Sample #1 On/Before May 2008 2933.7 795.26 435.6 2933.7119.1674573 120.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121702 Bagasse Suspension/Grate 12/17/2002Sample #2 On/Before May 2008 2933.7 795.26 435.6 2933.7119.1674573 120.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 121702 Bagasse Suspension/Grate 12/17/2002Sample #3 On/Before May 2008 2933.7 795.26 435.6 2933.7119.1674573 120.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase II - Voluntary Additional CO Data

Bgasse Suspension/Grate 12/28/2009Sample #1 After May 2008 9070 4612 0.03 9070368.4251417 370.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase II - Voluntary Additional CO Data

Bgasse Suspension/Grate 12/28/2009Sample #2 After May 2008 9070 4612 0.03 9070368.4251417 370.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase II - Voluntary Additional CO Data

Bgasse Suspension/Grate 12/28/2009Sample #3 After May 2008 9070 4612 0.03 9070368.4251417 370.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 120399 Bagasse Suspension/Grate 12/3/1999 Sample #1 On/Before May 2008 6297 3554 0 6297255.7853492 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 120399 Bagasse Suspension/Grate 12/3/1999 Sample #2 On/Before May 2008 6297 3554 0 6297255.7853492 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 120399 Bagasse Suspension/Grate 12/3/1999 Sample #3 On/Before May 2008 6297 3554 0 6297255.7853492 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 120498 Bagasse Suspension/Grate 12/4/1998 Sample #1 On/Before May 2008 6480 3575 0 6480263.2188443 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 120498 Bagasse Suspension/Grate 12/4/1998 Sample #2 On/Before May 2008 6480 3575 0 6480263.2188443 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 120498 Bagasse Suspension/Grate 12/4/1998 Sample #3 On/Before May 2008 6480 3575 0 6480263.2188443 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 022499 Bagasse Suspension/Grate 2/24/1999 Sample #1 On/Before May 2008 6494 3618 0 6494 263.787527 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 022499 Bagasse Suspension/Grate 2/24/1999 Sample #2 On/Before May 2008 6494 3618 0 6494 263.787527 260.0 FLSugarCaneGrowersCoop Boiler No. 8 ICR Phase I Organic HAP and CO 022499 Bagasse Suspension/Grate 2/24/1999 Sample #3 On/Before May 2008 6494 3618 0 6494 263.787527 260.0 GAADMLocation551 630- Wellons ICR Phase I Organic HAP and CO-630 Biomass Fuel Cell 7/29/2008 Sample #1 After May 2008 884.46 459.97 0.95 884.4635.92693504 36.0 GAADMLocation551 630- Wellons ICR Phase I Organic HAP and CO-630 Biomass Fuel Cell 7/29/2008 Sample #2 After May 2008 884.46 459.97 0.95 884.4635.92693504 36.0 GAADMLocation551 630- Wellons ICR Phase I Organic HAP and CO-630 Biomass Fuel Cell 7/29/2008 Sample #3 After May 2008 884.46 459.97 0.95 884.4635.92693504 36.0 IDChilcoLakeSawmill HFB1 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/30/2005 Sample #1 On/Before May 2008 4572.5 2286.25? 4572.5 185.735828 190.0 IDChilcoLakeSawmill HFB1 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/30/2005 Sample #2 On/Before May 2008 4572.5 2286.25? 4572.5 185.735828 190.0 IDChilcoLakeSawmill HFB1 ICR Phase I Organic HAP and CO Biomass Stoker/SlopedGrate/Other 3/30/2005 Sample #3 On/Before May 2008 4572.5 2286.25? 4572.5 185.735828 190.0 IDPotlatch PB-1 CE ICR Phase I Organic HAP and CO Biomass Fuel Cell 4/30/2008 Sample #1 On/Before May 2008 458.07 264.16 0.03 458.0718.60689136 19.0 IDPotlatch PB-1 CE ICR Phase I Organic HAP and CO Biomass Fuel Cell 4/30/2008 Sample #2 On/Before May 2008 458.07 264.16 0.03 458.0718.60689136 19.0 IDPotlatch PB-1 CE ICR Phase I Organic HAP and CO Biomass Fuel Cell 4/30/2008 Sample #3 On/Before May 2008 458.07 264.16 0.03 458.0718.60689136 19.0 IDPotlatch PB-1 CE ICR Phase II - ERT ERT Biomass Fuel Cell 7/29/2009 1 After May 2008 461.1 273.8 -0.2 461.118.72997054 19.0 IDPotlatch PB-1 CE ICR Phase II - ERT ERT Biomass Fuel Cell 7/30/2009 2 After May 2008 462.3 273.7 -0.05 462.318.77871477 19.0 IDPotlatch PB-1 CE ICR Phase II - ERT ERT Biomass Fuel Cell 7/30/2009 3 After May 2008 462.3 273.7 -0.05 462.318.77871477 19.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase II - Voluntary Additional CO Data from Test Report - Condition 1

Biomass Stoker/SlopedGrate/Other 9/22/2010 Sample #1 After May 2008 1000 900 ? 442? 90036.55817282 37.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase II - Voluntary Additional CO Data from Test Report - Condition 1

Biomass Stoker/SlopedGrate/Other 9/23/2010 Sample #2 After May 2008 1000 900 ? 445? 90036.55817282 37.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase II - Voluntary Additional CO Data from Test Report - Condition 1

Biomass Stoker/SlopedGrate/Other 9/23/2010 Sample #3 After May 2008 1000 900 ? 443? 90036.55817282 37.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase II - Voluntary Additional CO Data from Test Report - Condition 2

Biomass Stoker/SlopedGrate/Other 9/28/2010 Sample #1 After May 2008 1000 900 ? 438? 90036.55817282 37.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase II - Voluntary Additional CO Data from Test Report - Condition 2

Biomass Stoker/SlopedGrate/Other 9/29/2010 Sample #2 After May 2008 1000 900 ? 445? 90036.55817282 37.0 MSGPNewAugusta AA-015 Power Boiler ICR Phase II - Voluntary Additional CO Data from Test Report - Condition 2

Biomass Stoker/SlopedGrate/Other 9/30/2010 Sample #3 After May 2008 1000 900 ? 442? 90036.55817282 37.0
TXRGVSG Boiler No. 6 ICR Phase II - Comments Additional CO data from comments

Bagasse Suspension/Grate 1/13/2009 Sample #1 After May 2008 1000 900 ? ? ? 90036.55817282 37.0
TXRGVSG Boiler No. 6 ICR Phase II - Comments Additional CO data from comments

Bagasse Suspension/Grate 1/13/2009 Sample #2 After May 2008 1000 900 ? ? ? 90036.55817282 37.0
TXRGVSG Boiler No. 6 ICR Phase II - Comments Additional CO data from comments

Bagasse Suspension/Grate 1/13/2009 Sample #3 After May 2008 1000 900 ? ? ? 90036.55817282 37.0

HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (1)

Non-Continental Liquid

N/A 10/8/2010 Sample #2 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (1)

Non-Continental Liquid

N/A 10/8/2010 Sample #3 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (2)

Non-Continental Liquid

N/A 10/9/2010 Sample #1 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5



### Page 6 of 7

### Appendix A-1: Summary of Test Reports Reviewed for CO Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Test Date Category**  **Instrument Range (ppm)**  **90% of Span Max Calibration** 

**Gas Concentration (ppm)**  **Cal High**

**(ppm) Cal mid** 

**(ppm) Cal low** 

**(ppm) S**  **RDL RDL - 2 Sig Figs** 

HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (2)

Non-Continental Liquid

N/A 10/9/2010 Sample #2 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5
HITesoro SG1102 ICR Phase II - Voluntary Additional CO Data from Test Report (2)

Non-Continental Liquid

N/A 10/9/2010 Sample #3 After May 2008 188 169.2 185 96 0.81 1857.514735524 7.5 NENebraskaCityStation Auxiliary Boiler 2 ICR Phase I Organic HAP and CO Liquid N/A 39239Sample #1 On/Before May 2008 1000 5.95 0 100040.62019202 41.0 NENebraskaCityStation Auxiliary Boiler 2 ICR Phase I Organic HAP and CO Liquid N/A 39239Sample #2 On/Before May 2008 1000 5.95 0 100040.62019202 41.0 NENebraskaCityStation Auxiliary Boiler 2 ICR Phase I Organic HAP and CO Liquid N/A 39239Sample #3 On/Before May 2008 1000 5.95 0 100040.62019202 41.0 GATempleInlandThomson BW-B001 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 12/7/2004 Sample #1 On/Before May 2008 1847.1 1103.4 552 1847.175.02955669 75.0 GATempleInlandThomson BW-B001 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 12/7/2004 Sample #2 On/Before May 2008 1847.1 1103.4 552 1847.175.02955669 75.0 GATempleInlandThomson BW-B001 ICR Phase I Organic HAP and CO (2) Biomass Suspension Burner 12/7/2004 Sample #3 On/Before May 2008 1847.1 1103.4 552 1847.175.02955669 75.0



### Page 7 of 7

## Appendix A-2: Summary of Test Reports Reviewed for THC Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Instrument Range**  **(ppm) 90% of Span**  **Max Calibration**

**Gas Concentration (ppm)**  **S RDL**  **RDL - 2 Sig Figs** ILPolyOne B1 ICR Phase II - ERT ERT Coal FB 9/10/2009 10-100 ppm 90 100 905.547972603 5.5 ILPolyOne B1 ICR Phase II - ERT ERT Coal FB 9/11/2009 20-100 ppm 90 100 905.547972603 5.5 ILPolyOne B1 ICR Phase II - ERT ERT Coal FB 9/11/2009 30-100 ppm 90 100 905.547972603 5.5 IAArchersDanielsMidlandDesMoines Asea Boiler #1 ICR Phase II - Templates THC Coal FB 8/24/2009Sample #1 0-100 ppm 90 97.7 905.547972603 5.5 IAArchersDanielsMidlandDesMoines Asea Boiler #1 ICR Phase II - Templates THC Coal FB 8/24/2009Sample #2 0-100 ppm 90 97.7 905.547972603 5.5 IAArchersDanielsMidlandDesMoines Asea Boiler #1 ICR Phase II - Templates THC Coal FB 8/25/2009Sample #3 0-100 ppm 90 97.7 905.547972603 5.5 IAUofNorthernIowa Boiler #3 ICR Phase II - Templates THC Coal PC 10/6/2009Sample #1 0-84.1 ppm 75.69 84.1 75.694.665844959 4.7 IAUofNorthernIowa Boiler #3 ICR Phase II - Templates THC Coal PC 10/6/2009Sample #2 0-84.1 ppm 75.69 84.1 75.694.665844959 4.7 IAUofNorthernIowa Boiler #3 ICR Phase II - Templates THC Coal PC 10/6/2009Sample #3 0-84.1 ppm 75.69 84.1 75.694.665844959 4.7 TNEastman_NO_CBIDATA Boiler 30 ICR Phase II - ERT ERT Coal PC 8/25/2009 10-10 ppm 9 9 0.55479726 0.55 TNEastman_NO_CBIDATA Boiler 30 ICR Phase II - ERT ERT Coal PC 8/25/2009 20-10 ppm 9 9 0.55479726 0.55 TNEastman_NO_CBIDATA Boiler 30 ICR Phase II - ERT ERT Coal PC 8/26/2009 30-10 ppm 9 9 0.55479726 0.55 WINewPageBiron B24 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 9/24/2009 10-88.9 ppm 80.01 80.014.932147644 4.9 WINewPageBiron B24 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 9/24/2009 20-88.9 ppm 80.01 80.014.932147644 4.9 WINewPageBiron B24 ICR Phase II - ERT ERT Coal Stoker/SlopedGrate/Other 9/24/2009 30-88.9 ppm 80.01 80.014.932147644 4.9 OHAppletonIdeas Boiler 4 (B003) ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 1/29/2003Sample #1 45.972 51.08 45.972 2.833904405 2.8 OHAppletonIdeas Boiler 4 (B003) ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 1/29/2003Sample #2 45.972 51.08 45.972 2.833904405 2.8 OHAppletonIdeas Boiler 4 (B003) ICR Phase I Organic HAP and CO Coal Stoker/SlopedGrate/Other 1/29/2003Sample #3 45.972 51.08 45.972 2.833904405 2.8 WVATKRocketCenter NB2766 W-17479-W (Boiler 17)ICR Phase II - Templates THC Coal Stoker/SlopedGrate/Other 10/21/2009Sample #1 14.148 15.72 14.1480.872141293 0.87 WVATKRocketCenter NB2766 W-17479-W (Boiler 17)ICR Phase II - Templates THC Coal Stoker/SlopedGrate/Other 10/21/2009Sample #2 14.148 15.72 14.1480.872141293 0.87 WVATKRocketCenter NB2766 W-17479-W (Boiler 17)ICR Phase II - Templates THC Coal Stoker/SlopedGrate/Other 10/22/2009Sample #3 14.148 15.72 14.1480.872141293 0.87 ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler ICR Phase II - Test Report Phase II THC From Test Report

Biomass FB 7/14/2009Sample #1 92.7 103 92.75.714411781 5.7 ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler ICR Phase II - Test Report Phase II THC From Test Report

Biomass FB 7/15/2009Sample #2 92.7 103 92.75.714411781 5.7 ORGeorgiaPacificWaunaMill EU35 - Fluidized Bed Boiler ICR Phase II - Test Report Phase II THC From Test Report

Biomass FB 7/15/2009Sample #3 92.7 103 92.75.714411781 5.7 TNDomtar2384 HFB1-1 ICR Phase II - ERT ERT Biomass FB 9/16/2009 10-10 ppm 9 9 0.55479726 0.55
TNDomtar2384 HFB1-1 ICR Phase II - ERT ERT Biomass FB 9/16/2009 20-10 ppm 9 9 0.55479726 0.55
TNDomtar2384 HFB1-1 ICR Phase II - ERT ERT Biomass FB 9/17/2009 30-10 ppm 9 9 0.55479726 0.55 TNBowaterNewsprint Bubbling Fluidized Bed Boiler ICR Phase II - ERT ERT Biomass FB 8/5/2009 10-10 ppm 9 100 9 0.55479726 0.55 TNBowaterNewsprint Bubbling Fluidized Bed Boiler ICR Phase II - ERT ERT Biomass FB 8/5/2009 20-10 ppm 9 100 9 0.55479726 0.55 TNBowaterNewsprint Bubbling Fluidized Bed Boiler ICR Phase II - ERT ERT Biomass FB 8/6/2009 30-10 ppm 9 100 9 0.55479726 0.55 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/19/2009 27 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/19/2009 28 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/19/2009 29 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/19/2009 30 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/19/2009 31 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/21/2009 32 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/21/2009 33 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/21/2009 34 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/21/2009 35 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/21/2009 36 76.986 85.54 76.9864.745735764 4.7 WIGPGreenBay2818 B10 - Wastepaper Sludge-Fired Boiler 10 ICR Phase II - ERT

ERT Biomass FB 8/21/2009 37 76.986 85.54 76.9864.745735764 4.7 GATempleInlandRome WF ICR Phase II - Templates THC Biomass FB 7/29/2009Sample #1 0-25 ppm 22.5 22.5 1.386993151 1.4 GATempleInlandRome WF ICR Phase II - Templates THC Biomass FB 7/29/2009Sample #2 0-25 ppm 22.5 22.5 1.386993151 1.4 GATempleInlandRome WF ICR Phase II - Templates THC Biomass FB 7/30/2009Sample #3 0-25 ppm 22.5 22.5 1.386993151 1.4 MSWeyerhaeuserBruce AA-002 No. 2 Boiler ICR Phase II - Templates THC Biomass Fuel Cell 8/4/2009Sample #1 0-100 ppm 90 905.547972603 5.5 MSWeyerhaeuserBruce AA-002 No. 2 Boiler ICR Phase II - Templates THC Biomass Fuel Cell 8/4/2009Sample #2 0-100 ppm 90 905.547972603 5.5 MSWeyerhaeuserBruce AA-002 No. 2 Boiler ICR Phase II - Templates THC Biomass Fuel Cell 8/4/2009Sample #3 0-100 ppm 90 905.547972603 5.5 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates THC Biomass Fuel Cell 8/11/2009Sample #1 102.06 113.4 102.066.291400931 6.3 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates THC Biomass Fuel Cell 8/12/2009Sample #2 102.06 113.4 102.066.291400931 6.3 ARWeyerhaeuserDierksMill SN-45 ICR Phase II - Templates THC Biomass Fuel Cell 8/12/2009Sample #3 102.06 113.4 102.066.291400931 6.3 ARAnthonyForestProducts SN-12 ICR Phase II - ERT ERT Biomass Fuel Cell 9/2/2009 10-22 ppm 19.8 19.8 1.220553973 1.2 ARAnthonyForestProducts SN-12 ICR Phase II - ERT ERT Biomass Fuel Cell 9/2/2009 20-22 ppm 19.8 19.8 1.220553973 1.2 ARAnthonyForestProducts SN-12 ICR Phase II - ERT ERT Biomass Fuel Cell 9/3/2009 30-22 ppm 19.8 19.8 1.220553973 1.2 WAGraysHarborPaper No. 6 Boiler (EU2) ICR Phase II - Comments Stack & Duct Combined

Biomass Dutch Oven/Pile Burner 8/11/2009Sample #1 85.68 95.2 85.685.281669918 5.3 WAGraysHarborPaper No. 6 Boiler (EU2) ICR Phase II - Comments Stack & Duct Combined

Biomass Dutch Oven/Pile Burner 8/11/2009Sample #2 85.68 95.2 85.685.281669918 5.3 WAGraysHarborPaper No. 6 Boiler (EU2) ICR Phase II - Comments Stack & Duct Combined

Biomass Dutch Oven/Pile Burner 8/12/2009Sample #3 85.68 95.2 85.685.281669918 5.3 WANipponPaper #8 Hog Fuel Boiler ICR Phase II - Templates THC Wet BiomassStoker/SlopedGrate/Other 7/29/2009Sample #1 85.68 95.2 85.685.281669918 5.3 WANipponPaper #8 Hog Fuel Boiler ICR Phase II - Templates THC Wet BiomassStoker/SlopedGrate/Other 7/29/2009Sample #2 85.68 95.2 85.685.281669918 5.3 WANipponPaper #8 Hog Fuel Boiler ICR Phase II - Templates THC Wet BiomassStoker/SlopedGrate/Other 7/30/2009Sample #3 85.68 95.2 85.685.281669918 5.3 MEBoralexStratton Boiler #1 ICR Phase II - Templates THC Wet BiomassStoker/SlopedGrate/Other 10/21/2009Sample #1 0-87.2 ppm 78.48 85.1 78.48 4.83783211 4.8



## Page 1 of 2

## Appendix A-2: Summary of Test Reports Reviewed for THC Measurement Error

**FacilityID UnitID**  **Data Source Source Tab**  **Fuel Category**  **Combustor**

**Design Test Date**  **Run # Instrument Range**  **(ppm) 90% of Span**  **Max Calibration**

**Gas Concentration (ppm)**  **S RDL**  **RDL - 2 Sig Figs** MEBoralexStratton Boiler #1 ICR Phase II - Templates THC Wet BiomassStoker/SlopedGrate/Other 10/21/2009Sample #2 0-87.2 ppm 78.48 85.1 78.48 4.83783211 4.8 MEBoralexStratton Boiler #1 ICR Phase II - Templates THC Wet BiomassStoker/SlopedGrate/Other 10/21/2009Sample #3 0-87.2 ppm 78.48 85.1 78.48 4.83783211 4.8 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (12)

Biomass Suspension/Grate1/24/2008Sample #1 0-852.08 ppm 766.872 766.87247.27316495 47 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (12)

Biomass Suspension/Grate1/24/2008Sample #2 0-852.08 ppm 766.872 766.87247.27316495 47 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (12)

Biomass Suspension/Grate1/24/2008Sample #3 0-852.08 ppm 766.872 766.87247.27316495 47 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (13)

Biomass Suspension/Grate1/25/2007Sample #1 853.47 948.3 853.4752.61142419 53 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (13)

Biomass Suspension/Grate1/25/2007Sample #2 853.47 948.3 853.4752.61142419 53 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (13)

Biomass Suspension/Grate1/25/2007Sample #3 853.47 948.3 853.4752.61142419 53 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (14)

Biomass Suspension/Grate1/5/2001Sample #1 86.58 96.2 86.585.337149644 5.3 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (14)

Biomass Suspension/Grate1/5/2001Sample #2 86.58 96.2 86.585.337149644 5.3 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (16)

Biomass Suspension/Grate1/6/2001Sample #3 86.58 96.2 86.585.337149644 5.3 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (15)

Biomass Suspension/Grate1/5/2006Sample #1 0-1,000 ppm 900 90055.47972603 55 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (15)

Biomass Suspension/Grate1/5/2006Sample #2 0-1,000 ppm 900 90055.47972603 55 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (15)

Biomass Suspension/Grate1/5/2006Sample #3 0-1,000 ppm 900 90055.47972603 55 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (17)

Biomass Suspension/Grate1/9/2002Sample #1 219.96 244.4 219.96 13.55924504 14 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (17)

Biomass Suspension/Grate1/9/2002Sample #2 219.96 244.4 219.96 13.55924504 14 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (17)

Biomass Suspension/Grate1/9/2002Sample #3 219.96 244.4 219.96 13.55924504 14 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (18)

Biomass Suspension/Grate 11/15/2002Sample #1 760.5 845 760.546.88036849 47 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (18)

Biomass Suspension/Grate 11/15/2002Sample #2 760.5 845 760.546.88036849 47 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (18)

Biomass Suspension/Grate 11/15/2002Sample #3 760.5 845 760.546.88036849 47 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (22)

Biomass Suspension/Grate 12/30/2003Sample #1 264.96 294.4 264.96 16.33323134 16 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (22)

Biomass Suspension/Grate 12/30/2003Sample #2 264.96 294.4 264.96 16.33323134 16 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (22)

Biomass Suspension/Grate 12/30/2003Sample #3 264.96 294.4 264.96 16.33323134 16 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (23)

Biomass Suspension/Grate12/4/2008Sample #1 0-1,000 ppm 900 90055.47972603 55 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (23)

Biomass Suspension/Grate12/4/2008Sample #2 0-1,000 ppm 900 90055.47972603 55 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (24)

Biomass Suspension/Grate2/4/2005Sample #1 0-2,500 ppm 2250 304.3 2250 138.6993151 140 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (24)

Biomass Suspension/Grate2/4/2005Sample #2 0-2,500 ppm 2250 304.3 2250 138.6993151 140 FLUSSugarCorp Boiler No. 7 ICR Phase II - Voluntary Additional THC Data (24)

Biomass Suspension/Grate2/4/2005Sample #3 0-2,500 ppm 2250 304.3 2250 138.6993151 140 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Heavy LiquidN/A 8/25/2009 10-100.5 ppm 90.45 90.45 5.575712466 5.6 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Heavy LiquidN/A 8/25/2009 20-100.5 ppm 90.45 90.45 5.575712466 5.6 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Heavy LiquidN/A 8/26/2009 30-100.5 ppm 90.45 90.45 5.575712466 5.6 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Heavy LiquidN/A 8/26/2009 40-100.5 ppm 90.45 90.45 5.575712466 5.6 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Heavy LiquidN/A 8/27/2009 50-100.5 ppm 90.45 90.45 5.575712466 5.6 NCInvistaHwy421 B7600 ICR Phase II - ERT ERT Heavy LiquidN/A 8/27/2009 60-100.5 ppm 90.45 90.45 5.575712466 5.6 SCDAKAmericas P8F ICR Phase II - ERT ERT Heavy LiquidN/A 7/14/2009 10-50 ppm 45 45 2.773986301 2.8 SCDAKAmericas P8F ICR Phase II - ERT ERT Heavy LiquidN/A 7/14/2009 20-50 ppm 45 45 2.773986301 2.8 SCDAKAmericas P8F ICR Phase II - ERT ERT Heavy LiquidN/A 7/15/2009 30-50 ppm 45 45 2.773986301 2.8 SCDAKAmericas P8F ICR Phase II - ERT ERT Heavy LiquidN/A 7/15/2009 40-50 ppm 45 45 2.773986301 2.8 SCDAKAmericas P8F ICR Phase II - ERT ERT Heavy LiquidN/A 7/15/2009 50-50 ppm 45 45 2.773986301 2.8 SCDAKAmericas P8F ICR Phase II - ERT ERT Heavy LiquidN/A 7/16/2009 60-50 ppm 45 45 2.773986301 2.8 WVMountainStateCarbonFollansbee S1 ICR Phase II - Test Report Phase II THC From Test Report

Process GasN/A 10/20/2009Sample #1 0-13 ppm 11.7 11.70.721236438 0.72 WVMountainStateCarbonFollansbee S1 ICR Phase II - Test Report Phase II THC From Test Report

Process GasN/A 10/21/2009Sample #2 0-13 ppm 11.7 11.70.721236438 0.72 WVMountainStateCarbonFollansbee S1 ICR Phase II - Test Report Phase II THC From Test Report

Process GasN/A 10/21/2009Sample #3 0-13 ppm 11.7 11.70.721236438 0.72



## Page 2 of 2