### Name:

Title: Company: Sign Date: Name:
Title: Company: Sign Date: Permitted Facility Representative / Date Testing Company Representative / Date



## Information Collection Request Emission Test Program Report Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.



### Monday, November 21, 2011 Page 1 of 35

### Information Collection Request Emission Test Program Report

Facility Information:
Cleco Power, LLC

275 Rodemacher Road

Lena LA 71447
Contact: Paul Turregano

Phone: 318 484-7413

Fax:

Email: paul.turregano@clecl.com Testing Company:

Shaw E & I

4171 Essen Lane

Baton Rouge LA 70809
Contact: Richard Ishikawa

Phone: 225 932-2745

Fax:

Email: richard.ishikawa@shawgrp.com

Air Permit Number: Permitted Source ID/Name:
Cleco Rodemacher Power Station 7446811

Permitted Maximum Process Rate: Max. Normal Operation Process Rate: Target Process Test Rat

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Industry/SCC/NAIS

Sampling Location Information:

Test Parameter Information: AFS #: FRS #:

SCC / Description

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width

Boiler 32 216 4.5 12.5 4 0 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location

Carbon Monoxide Method 10 3 120 0 Boiler 32 2,3,7,8-TCDD Method 23 3 480 0 Boiler 32 1,2,3,7,8-PeCDD Method 23 3 480 0 Boiler 32 1,2,3,4,7,8-HxCDD Method 23 3 480 0 Boiler 32 1,2,3,6,7,8-HxCDD Method 23 3 480 0 Boiler 32 1,2,3,7,8,9-HxCDD Method 23 3 480 0 Boiler 32 Regulation Description Compound Limit Unit EPA's Information Collection Request for electric utility steam generating units 0



### Monday, November 21, 2011 Page 2 of 35

### Information Collection Request Emission Test Program Report

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.

1,2,3,4,6,7,8-HpCDD Method 23 3 480 0 Boiler 32
OCDD Method 23 3 480 0 Boiler 32 2,3,7,8-TCDF Method 23 3 480 0 Boiler 32 1,2,3,7,8-PeCDF Method 23 3 480 0 Boiler 32 2,3,4,7,8-PeCDF Method 23 3 480 0 Boiler 32 1,2,3,4,7,8-HxCDF Method 23 3 480 0 Boiler 32 1,2,3,6,7,8-HxCDF Method 23 3 480 0 Boiler 32 2,3,4,6,7,8-HxCDF Method 23 3 480 0 Boiler 32 1,2,3,7,8,9-HxCDF Method 23 3 480 0 Boiler 32 1,2,3,4,6,7,8-HpCDF Method 23 3 480 0 Boiler 32 1,2,3,4,7,8,9-HpCDF Method 23 3 480 0 Boiler 32
OCDF Method 23 3 480 0 Boiler 32 3,3',4,4'-TCB (PCB77) Method 23 3 480 0 Boiler 32 3,4,4',5-TCB (PCB81) Method 23 3 480 0 Boiler 32 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 0 Boiler 32 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 0 Boiler 32 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 0 Boiler 32 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 0 Boiler 32 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 0 Boiler 32 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 0 Boiler 32

2,3',4,4',5,5'-HxCB (PCB167) Method 23 3 480 0 Boiler 32 3,3',4,4',5,5'-HxCB (PCB169) Method 23 3 480 0 Boiler 32 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 0 Boiler 32

Total organic compounds

(TOC) as Methane Method 25A 3 120 0 Boiler 32

Total PM2.5 OTM - 27/28 3 240 0 Boiler 32 Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 240 0 Boiler 32

Organic Condensible

Particulate OTM - 27/28 3 240 0 Boiler 32

Filterable PM2.5 OTM - 27/28 3 240 0 Boiler 32 Selenium Method 29 3 240 0 Boiler 32 Arsenic Method 29 3 240 0 Boiler 32 Beryllium Method 29 3 240 0 Boiler 32 Cadmium Method 29 3 240 0 Boiler 32 Chromium Method 29 3 240 0 Boiler 32 Cobalt Method 29 3 240 0 Boiler 32 Lead Method 29 3 240 0 Boiler 32 Manganese Method 29 3 240 0 Boiler 32 Nickel Method 29 3 240 0 Boiler 32 Antimony Method 29 3 240 0 Boiler 32
Co2 Method 3A CO2 3 60 0 Boiler 32
O2 Method 3A O2 3 60 0 Boiler 32 Sulfur Dioxide Method 6C 3 120 0 Boiler 32 Nitrogen oxides (NOx) Method 7E 3 120 0 Boiler 32



### Monday, November 21, 2011 Page 3 of 35

### Information Collection Request Emission Test Program Report



### Monday, November 21, 2011 Page 4 of 35

### Information Collection Request Emission Test Program Report

Sampling / Stack Data Results Summary

Location Boiler 32 - Method 10
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Boiler 32 - Method 10 3
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 5 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 10 3 6
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Boiler 32 - Method 10 3 6 9 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 6 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 23
Average
Run Number 1 2 3

Test Date 2/17/2011 2/18/2011 2/19/2011

Run Start Time 4:42:00 AM 8:20:00 AM 8:25:00 AM

Run Finish Time 8:15:00 AM 4:39:00 PM 4:36:00 PM
Net Run Time, minutes 480 480 480 Dry Gas Meter Volume Sampled, dscf 253.699 259.440 259.359 257.499
Moisture Content of Stack Gas, % 9.99 9.37 9.47 9.610 Moisture Saturation at Stack Gas Temperature, % 49.98 48.85 51.94 50.257
Carbon Dioxide, % 14.7 14.7 15.1 14.833 Oxygen, % 5 5 4.5 4.833 Average Stack Gas Temperature, °F 178.92 178.00 180.83 179.250 Dry Volumetric Flow Rate, dry scfm 648,138.4 666,629.3 654,834.6 656,534.100
Actual Wet Volumetric Flue Gas Flow Rate, acfm 874,559.1 889,979.9 877,612.7 880,717.233 Percent Isokinetic of Sampling Rate, % 104.3 103.7 105.5 104.500
F-Factor, dscfm/MMBtu @ %O2 9968 9854 10036 9,952.667

Fw

Fc



### Location Boiler 32 - Method 25A
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 7 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 29
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Boiler 32 - Method 3A CO2
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 8 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A CO2 3
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Boiler 32 - Method 3A CO2 3 6 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 9 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A CO2 3 6 9
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Boiler 32 - Method 3A O2 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 10 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A O2 3
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Boiler 32 - Method 3A O2 3 6 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, November 21, 2011 Page 11 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A O2 3 6 9
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Boiler 32 - OTM - 27/28 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Monday, November 21, 2011 Page 12 of 35

### Information Collection Request Emission Test Program Report

Emissions Summary

Location: Boiler 32 - Method 10 Compound: Carbon Monoxide Average
Run 1 2 2/17-1 Elb/hr 2.97E+01 2.96E+01 2.61E+01 28.467 lb/mmBtuO2 9.97E-02 1.01E-02 8.72E-03 0.040
ppm 1.02E+01 1.05E+01 9.22E+00 9.973 ppm@7%O2 9.21E+00 9.39E+00 8.01E+00 8.870



### Location: Boiler 32 - Method 10 3 Compound: Carbon Monoxide Average
Run 2/17-2 2/17-3 2/18-1 Elb/hr 2.81E+01 3.31E+01 2.49E+01 28.700 lb/mmBtuO2 9.40E-03 1.17E-02 8.03E-03 0.010
ppm 9.93E+00 1.17E+01 8.58E+00 10.070 ppm@7%O2 8.63E+00 1.08E+01 7.45E+00 8.960



### Location: Boiler 32 - Method 10 3 6 Compound: Carbon Monoxide Average
Run 2/18-2 2/18-3 2/19-1 Elb/hr 2.48E+01 2.64E+01 2.50E+01 25.400 lb/mmBtuO2 7.98E-03 8.56E-03 8.14E-03 0.008
ppm 8.53E+00 9.09E+00 8.75E+00 8.790 ppm@7%O2 7.41E+00 7.95E+00 7.42E+00 7.593



### Location: Boiler 32 - Method 10 3 6 9 Compound: Carbon Monoxide Average
Run 2/19-2 2/19-3 3 Elb/hr 2.12E+01 2.19E+01 5.78E+01 33.633 lb/mmBtuO2 6.94E-03 7.23E-03 1.92E-02 0.011
ppm 7.42E+00 7.68E+00 2.01E+01 11.733 ppm@7%O2 6.33E+00 6.59E+00 1.78E+01 10.240



### Location: Boiler 32 - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber 1 2 3 Mass_mg 0.0000000495 0.0000000181 0.0000000244 0.000 lb/mmBtuO2 5.64E-12 1.99E-12 2.65E-12 0.000



### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000158 0.00000000766 0.00000000326 0.000 lb/mmBtuO2 1.80E-12 8.43E-13 3.54E-13 0.000



### Monday, November 21, 2011 Page 13 of 35

### Information Collection Request Emission Test Program Report

Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000318 0.00000000398 0.00000000375 0.000 lb/mmBtuO2 3.62E-12 4.38E-13 4.08E-13 0.000



### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000244 0.00000000626 0.0000000061 0.000 lb/mmBtuO2 2.78E-12 6.89E-13 6.63E-13 0.000



### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000252 0.00000000503 0.00000000438 0.000 lb/mmBtuO2 2.87E-12 5.54E-13 4.76E-13 0.000



### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.000000021 0.0000000054 0.00000000525 0.000 lb/mmBtuO2 2.39E-12 5.94E-13 5.71E-13 0.000



### Compound: 1,2,3,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000216 0.00000000432 0.00000000377 0.000 lb/mmBtuO2 2.46E-12 4.75E-13 4.10E-13 0.000



### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000227 0.00000000583 0.00000000567 0.000 lb/mmBtuO2 2.58E-12 6.42E-13 6.16E-13 0.000



### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000266 0.00000000531 0.00000000463 0.000 lb/mmBtuO2 3.03E-12 5.84E-13 5.03E-13 0.000



### Compound: 1,2,3,7,8-PeCDD Average RunNumber 1 2 3 Mass_mg 0.00000001181 0.00000000395 0.00000000395 0.000 lb/mmBtuO2 1.34E-12 4.35E-13 4.29E-13 0.000



### Compound: 1,2,3,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000161 0.00000000271 0.00000000314 0.000 lb/mmBtuO2 1.83E-12 2.98E-13 3.41E-13 0.000



### Monday, November 21, 2011 Page 14 of 35

### Information Collection Request Emission Test Program Report

Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber 1 2 3 Mass_mg 0.00000153 0.0000000309 0.0000000264 0.000 lb/mmBtuO2 1.74E-10 3.40E-12 2.87E-12 0.000



### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber 1 2 3 Mass_mg 0.0000305 0.000021 0.0000255 0.000 lb/mmBtuO2 3.47E-09 2.31E-09 2.77E-09 0.000



### Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber 1 2 3 Mass_mg 0.000123 0.0000182 0.0000251 0.000 lb/mmBtuO2 1.40E-08 2.00E-09 2.73E-09 0.000



### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber 1 2 3 Mass_mg 0.0000596 0.0000288 0.0000222 0.000 lb/mmBtuO2 6.79E-09 3.17E-09 2.41E-09 0.000



### Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber 1 2 3 Mass_mg 0.00000449 0.0000039 0.00000304 0.000 lb/mmBtuO2 5.11E-10 4.29E-10 3.30E-10 0.000



### Compound: 2,3',4,4',5-PeCB (PCB118) Average RunNumber 1 2 3 Mass_mg 0.000194 0.000558 0.0000942 0.000 lb/mmBtuO2 2.21E-08 6.14E-08 1.02E-08 0.000



### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber 1 2 3 Mass_mg 0.000148 0.000101 0.0000575 0.000 lb/mmBtuO2 1.69E-08 1.11E-08 6.25E-09 0.000



### Compound: 2,3,4,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000239 0.00000000478 0.00000000417 0.000 lb/mmBtuO2 2.72E-12 5.26E-13 4.53E-13 0.000



### Compound: 2,3,4,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000159 0.00000000268 0.0000000031 0.000 lb/mmBtuO2 1.81E-12 2.95E-13 3.37E-13 0.000



### Monday, November 21, 2011 Page 15 of 35

### Information Collection Request Emission Test Program Report

Compound: 2,3,7,8-TCDD Average RunNumber 1 2 3 Mass_mg 0.00000001127 0.00000000303 0.00000000271 0.000 lb/mmBtuO2 1.28E-12 3.34E-13 2.95E-13 0.000



### Compound: 2,3,7,8-TCDF Average RunNumber 1 2 3 Mass_mg 0.0000000101 0.0000000104 0.00000000279 0.000 lb/mmBtuO2 1.15E-12 1.14E-12 3.03E-13 0.000



### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber 1 2 3 Mass_mg 0.000000983 0.000000234 0.0000000976 0.000 lb/mmBtuO2 1.12E-10 2.58E-11 1.06E-11 0.000



### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber 1 2 3 Mass_mg 0.00000107 0.000000533 0.0000000668 0.000 lb/mmBtuO2 1.22E-10 5.87E-11 7.26E-12 0.000



### Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber 1 2 3 Mass_mg 0.00000861 0.00000704 0.00000011 0.000 lb/mmBtuO2 9.80E-10 7.75E-10 1.20E-11 0.000



### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber 1 2 3 Mass_mg 0.0000231 0.0000151 0.000000121 0.000 lb/mmBtuO2 2.63E-09 1.66E-09 1.32E-11 0.000



### Compound: OCDD Average RunNumber 1 2 3 Mass_mg 0.0000000242 0.000000136 0.000000158 0.000 lb/mmBtuO2 2.76E-12 1.50E-11 1.72E-11 0.000



### Compound: OCDF Average RunNumber 1 2 3 Mass_mg 0.0000000254 0.00000000468 0.00000000526 0.000 lb/mmBtuO2 2.89E-12 5.15E-13 5.72E-13 0.000



### Location: Boiler 32 - Method 25A Compound: Total organic compounds (TOC) as Average
Run 1 2 3 Elb/hr 5.57E-01 9.57E-01 4.49E-01 0.654



### Monday, November 21, 2011 Page 16 of 35

### Information Collection Request Emission Test Program Report

lb/mmBtuO2 1.88E-04 3.22E-04 1.60E-04 0.000
ppm 3.44E-01 5.91E-01 2.77E-01 0.404 ppm@7%O2 3.01E-01 5.17E-01 2.57E-01 0.358



### Location: Boiler 32 - Method 29 Compound: Antimony Average RunNumber 1 2 3 Mass_mg 0.0011 0.0011 0.0011 0.001 lb/mmBtuO2 2.43E-07 2.43E-07 2.35E-07 0.000



### Compound: Arsenic Average RunNumber 1 2 3 Mass_mg 0.0013 0.001 0.001 0.001 lb/mmBtuO2 2.87E-07 2.21E-07 2.14E-07 0.000



### Compound: Beryllium Average RunNumber 1 2 3 Mass_mg 0.00002 0.00003 0.00002 0.000 lb/mmBtuO2 4.42E-09 6.63E-09 4.28E-09 0.000



### Compound: Cadmium Average RunNumber 1 2 3 Mass_mg 0.0004 0.0009 0.0002 0.001 lb/mmBtuO2 8.83E-08 1.99E-07 4.28E-08 0.000



### Compound: Chromium Average RunNumber 1 2 3 Mass_mg 0.0047 0.0024 0.0028 0.003 lb/mmBtuO2 1.04E-06 5.31E-07 5.99E-07 0.000



### Compound: Cobalt Average RunNumber 1 2 3 Mass_mg 0.002 0.001 0.0019 0.002 lb/mmBtuO2 4.42E-07 2.21E-07 4.06E-07 0.000



### Compound: Lead Average RunNumber 1 2 3 Mass_mg 0.0015 0.0022 0.0019 0.002 lb/mmBtuO2 3.31E-07 4.86E-07 4.06E-07 0.000



### Compound: Manganese Average RunNumber 1 2 3 Mass_mg 0.0098 0.0118 0.0044 0.009 lb/mmBtuO2 2.16E-06 2.61E-06 9.41E-07 0.000



### Monday, November 21, 2011 Page 17 of 35

### Information Collection Request Emission Test Program Report

Compound: Nickel Average RunNumber 1 2 3 Mass_mg 0.0145 0.0234 0.0117 0.017 lb/mmBtuO2 3.20E-06 5.17E-06 2.50E-06 0.000



### Compound: Selenium Average RunNumber 1 2 3 Mass_mg 0.0038 0.001 0.0022 0.002 lb/mmBtuO2 8.39E-07 2.21E-07 4.71E-07 0.000



### Location: Boiler 32 - OTM - 27/28 Compound: Filterable PM2.5 Average RunNumber 1 2 3 Mass_mg 0.7 0.3 1.3 0.767 lb/mmBtuO2 1.69E-04 7.06E-05 3.07E-04 0.000



### Compound: Inorganic (Aqueous) Condensible P Average RunNumber 1 2 3 Mass_mg 0.8 13.7 34.2 16.233 lb/mmBtuO2 1.94E-04 3.22E-03 8.07E-03 0.004



### Compound: Organic Condensible Particulate Average RunNumber 1 2 3 Mass_mg 18.2 2.4 1.6 7.400 lb/mmBtuO2 4.41E-03 5.65E-04 3.78E-04 0.002



### Compound: Total PM2.5 Average RunNumber 1 2 3 Mass_mg 19.7 16.4 37.1 24.400 lb/mmBtuO2 4.77E-03 3.86E-03 8.76E-03 0.006



### Monday, November 21, 2011 Page 18 of 35

### Information Collection Request Emission Test Program Report

Process Run Data

APCD Run Data

Process Lab Run Data



### Monday, November 21, 2011 Page 19 of 35

### Information Collection Request Emission Test Program Report

Sampling / Stack Data Results Detail

Location Boiler 32 - Method 10 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 20 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 10 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 21 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 10 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 22 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 10 3 6 9 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 23 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 23 Average Run Number 1 2 3
Test Date 2/17/2011 2/18/2011 2/19/2011 Run Start Time 4:42:00 AM 8:20:00 AM 8:25:00 AM Run Finish Time 8:15:00 AM 4:39:00 PM 4:36:00 PM Net Traversing Points 12 12 12 Net Run Time, minutes 480 480 480 Nozzle Diameter, inches 0.191 0.191 0.191 0.191 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 0.999 0.999 0.999 0.999 Barometric Pressure, inches of Mercury 29.88 29.95 30 29.943 Average Orifice Meter Differential, inches H2O 1.02 1.07 1.04 1.043 Dry Gas Meter Volume Sampled, cubic feet 258.619 266.150 264.710 263.160 Average Dry Gas Meter Temperature, °F 78.33 83.08 81.17 80.860 Dry Gas Meter Volume Sampled, dscf 253.699 259.440 259.359 257.499 Total Moisture Liquid collected, g 598.5 569.8 576.6 581.633 Volume of Water Vapor, standard cubic feet 28.17 26.82 27.14 27.377 Moisture Content of Stack Gas, % 9.99 9.37 9.47 9.610 Moisture Saturation at Stack Gas Temperature, % 49.98 48.85 51.94 50.257 Dry Mole Fraction 0.9001 0.9063 0.9053 0.904 Carbon Dioxide, % 14.7 14.7 15.1 14.833 Oxygen, % 5 5 4.5 4.833 Carbon Monoxide & Nitrogen, % 80.3 80.3 80.4 80.333 Fuel Factor 1.08 1.08 1.09 Dry Molecular Weight, lb/lb-Mole 30.55 30.55 30.60 30.567 Wet Molecular weight, lb/lb-Mole 29.30 29.37 29.41 29.360 Flue Gas Static Pressure, inches of H2O -1 -1 -1 -1.000 Absolute Flue Gas Pressure, inches of Mercury 29.81 29.88 29.93 29.873 Average Stack Gas Temperature, °F 178.92 178.00 180.83 179.250 Average Velocity Head, inches of H2O 0.8698851956 87598 0.906253941

756931 0.8800649097

9658 0.885

Average Stack Gas Velocity, feet/second 57.28 58.29 57.48 57.683 Stack Cross-Sectional Area, square feet 254.469 254.469 254.469 254.469 Dry Volumetric Flow Rate, dry scfm 648,138.4 666,629.3 654,834.6 656,534.100 Actual Wet Volumetric Flue Gas Flow Rate, acfm 874,559.1 889,979.9 877,612.7 880,717.233 Percent Isokinetic of Sampling Rate, % 104.3 103.7 105.5 104.500 Percent Excess Air, % 30.9 26.9 F-Factor, dscfm/MMBtu @ %O2 9968 9854 10036 9,952.667 Round Duct Diameter, inches 216 216 216 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0
Fw
Fc



### Monday, November 21, 2011 Page 24 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 25A Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 25 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 29 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, November 21, 2011 Page 26 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A CO2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 27 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A CO2 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 28 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A CO2 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 29 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A CO2 3 6 9 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 30 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A O2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 31 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A O2 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 32 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A O2 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 33 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - Method 3A O2 3 6 9 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, November 21, 2011 Page 34 of 35

### Information Collection Request Emission Test Program Report

Location Boiler 32 - OTM - 27/28 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, November 21, 2011 Page 35 of 35