, " 

## il

. i 

### 712192 SPA 10 RCRA REVISION CHECKLIST 81

Petroleum Refinery Primary andSecondary 

# •

Oil/Water/Solids Separation Sludge Listings (F037 and F038) 55

### fR46354-46397 November 2, 1990

as 

### amended onDecember 17, 1990, at 55

### fR51707 (RCRA Cluster I, HSWA)

Following the promulgationof the tworules addressed by 

### this checklist, an interim final rule <56 FR 21955;May 13, 1991; Revision Checklist 89) revised the definition of wastes subject to the F037 and F038 listings. That rule also clarified that, with regard to F038, floats generated in aggressive biological treatment units are not included in the listing description,ofthat waste stream. Because these changes narrowthe scope of the F037 and F038 listings, they are considered**optional~** 

### States wishing to adopt the optional changes addressed by 

### Revision Checklist 89 are strongly encouraged to adopt!'themat the same time the Revision Checklist 81provisions are adopted.

STATE ANALOG IS: 

# if FEDERAL ANALOGOUS MORE 

### BROAD.. RCRA FEDERAL STATE EQUIV­ STRIN­ ER IN REQUIREMENT CITATION CITATION ALENT GENT SCOPE

PART 261

- IDENTIFICATION AND LISTING OF HAZARDOUS WASTE WAC 173-303 

# • SUBPART D - LISTS OF HAZARDOUS WASTES

HAZARDOUS WASTES FROM NON-SPECIFIC SOURCES 1,2 add the waste codes IF037" and "F038" to list in alphanumeric order as shown below; redesignate the introductoryparagraph and the table as paragraph (a) 261.31(a) 9904 

### x

Industry andEPA hazardous Hazard waste No. Hazardous.·waste code



### * * * * 

## * * 

### * * F037 Petroleum refineryprimary oil/water/solids separation sludge--Any sludge (T) generated from the gravitational separation of oil/water/solidsduring the storage or treatment of process wastewaters and oily cooling wastewaters frompetroleum refineries. Suchsludges include, but are not limited to, those generated in:' oil/water/solids separators; tanks and impoundments; ditches and other conveyances; sumps; and stormwater 

# .' units receiving dry weather flow. Sludges generated in stormwater units that dQ not receive dry weather flow, sludges generated in aggressive biological treatment units as defined in §261.31(b)(2) (including sludges generated in one or moreadditional units

November 2, 1990 - Page 1 of 47/2/92 SPA RCRAREVISION CHECKLIST 81: Petroleum Refinery Primary and Secondary Oil/Water/Solids Separation Sludge Listings (F037 and F038) (Cont'd)

STATE ANALOG IS: FEDERAL ANALOGOUS MORE BROADFEDERAL RCRA STATE EQUIV- STRIN- ER IN REQUIREMENT CITATION CITATION' ALENT GENT SCOPE

after wastewaters have been treated in aggressive biological treatment units) and K051 wastes are not(!inCluded in this listing. F038 Petroleum refinery secondary (emulsified) oil/water/solids separation sludge-­ (T) Any sludge and/or float generated from the physical and/or chemical separation of oil/water/solids in process wastewaters and oilycooling wastewaters frompetroleum refineries. Such wastes include, but are not limited to, all sludges and floats generated in: ,induced ai,r flotation OAF) units, tanks and**i~undments,** and all sludges generated in DAF units. Sludges generated in stonmwater units that do not receivedry weather flow, sludges generated in aggressivebiological treatment units as defined in, §261.31(b)(2) (including sludges generated in one or moreadditional units after wastewaters have been treated in aggressive biological treatment units) and F037, K048, and K051 wastes are not included in this listing.



### * * 

### * 

### '* * 

### * 

### * *

add new paragraph entitled "Listing Specific Definitions:" definition of oil/water/ solids for the 261.31(b) 9904 ftnote 2 X 

# ()

purposes of F037 and F038listings 261.31CbH 1) 9904 ftnote 2(a) X for the purposes of F037 and F038, aggressive biological
treatment units

are defined as units which employ one of four specified treatment methods; specific requirements for high-rate aeration: 261.31(bH2H1) 9904 ftnote 2(b)(i) X units**~loy** a 'minimum of 6 hp per million gallons of
treatment volume and either: 261.31(b)(2)(i)(A) 9904 ftnote 2(b)(i)(i) X the hydraulic retention time of the unit is no longer than 5 days 261.31(b)(2)(i)(B) 9904 ftnote 2(b)(i)(ii) X the hydraulic retention time is no longer than 30 days and the unit does not generate a sludge that is

November 2, 1990 - Page 2 of 4

# .

,

# •

, 7/2192 SPA 10 RCRA REVISION CHECKLIST 81: PetroleumRefinery Primary and Secondary Oil/Water/Solids Separation Sludge Listings (F037**a~** F038) (Cont'd)

STATE ANALOG IS: FEDERAL ANALOGOUS MORE BROADFEDERAL RCRA STATE EQUIV- STRIN- ER IN REQUIREMENT CITATION CITATION ALENT GENT SCOPE

hazardous waste by the Toxicity Characteristic 261.31(b)(2)(i)(C) 9904ftnote 2(b)(i)(iii)X**generator~** and treatment, storage anddisposal facilities must prove their sludges are exempt from listing

as F037 and F038 wastes; maintenance of documents and data sufficient to prove that: 261.31(b)(2)(ii) 9904ftnote 2(b)(ii) X unit is an aggressive biological treatment 

# • 2 unit as defined in 261.31(b)(2) sludges were.actually generated in the aggressive biological 261.31(b)(2)(ii)(A) 9904 ftnote 2(b)(ii)(i) X

treatment unit 261.3Hb)(2Hi iH8) 9904ftnote 2(b)(ii)(ii)X sludges are considered to 

### be generated at the moment of deposition in the unit for the purposes.of the F037 listing; depositiondefined 261.31(b)(3)(i) 9904 ftnote 2(c)(i) X for the purposes of the F038 listing 261.31(b)(3)(ii) 9904ftnote 2(c)(ii) X sludges.are considered to be generated at the moment of deposition in the unit; deposition defined 261.31(b)(3)(ii)(A) 9904ftnote 2(c)(ii)(A) X floats are considered
to 

### begenerated at the moment they are fonned in the top of the unit 261.31(b)(3)(ii)(B) 9904ftnote 2(c)(ii)(B) X 

# • APPENDIX VII TO PART 261

November 2, 1990 - Page 3 of 47/2192 

# , SPA**10C~\'** 

### RCRAREVISION CHECKLIST 81: Petroleum Refinery Primary and Secondary Oil/Water/Solids 

## .J Separation Sludge Listings (F037 and F038) CCont'd)

FEDERAL REQUIREMENT FEDERAL RCRA CITATION ANALOGOUS STATE CITATION STATE ANALOG IS: MORE EQUIV- STRINALENT GENT BROADER IN SCOPE

BASIS FOR LISTING HAZARDOUS**~ASTE** add 

### the waste codes nF037" and'IF038" in alphanumeric order,to list as shown below: Appendix VII 082(4) 

## x

APPENDIX VII.--BASIS FOR LISTING HAZARDOUS WASTE

EPA hazardous Hazardousconstituents for

waste No. which listed



### * * * * *. 

### * * 

### * • * * 

### *

F037 Benzene, benzoCa)pyrene, chrysene, lead, chromium. F038 Benzene, benzoCa)pyrene chrysene, lead, chromium.



### * * * * * * * * * * * *

Theintroductory paragraph and table wereoriginally introduced into the code as 261.31. Thefinal rule for this checklist has redesignated the old 261.31 as 261.31(a) and added a new paragraph, 261.31Cb).

2 See the technical correction to the rule at 55 FR 51707(December 17, 1990).

November 2, 1990 - Page 4 of 4