Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.EIA

Facility Code Facility Name Boiler ID Fuel Type 1

1250 Lawrence Energy Center Boiler 3 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

1250 Lawrence Energy Center Boiler 3 As Received Higher Heating Value 1250 Lawrence Energy Center Boiler 3 As Received % Moisture 1250 Lawrence Energy Center Boiler 3 As Received % Ash 1250 Lawrence Energy Center Boiler 3 As Received % Sulfur 1250 Lawrence Energy Center Boiler 3 Dry

basis Higher Heating Value 1250 Lawrence Energy Center Boiler 3 Dry

basis % Ash 1250 Lawrence Energy Center Boiler 3 Dry

basis % Sulfur 1250 Lawrence Energy Center Boiler 3 Dry

basis Antimony 1250 Lawrence Energy Center Boiler 3 Dry

basis Arsenic 1250 Lawrence Energy Center Boiler 3 Dry

basis Beryllium 1250 Lawrence Energy Center Boiler 3 Dry

basis Cadmium 1250 Lawrence Energy Center Boiler 3 Dry

basis Chlorine 1250 Lawrence Energy Center Boiler 3 Dry

basis Chromium 1250 Lawrence Energy Center Boiler 3 Dry

basis Cobalt 1250 Lawrence Energy Center Boiler 3 Dry

basis Fluorine 1250 Lawrence Energy Center Boiler 3 Dry

basis Lead 1250 Lawrence Energy Center Boiler 3 Dry

basis Manganese 1250 Lawrence Energy Center Boiler 3 Dry

basis Mercury 1250 Lawrence Energy Center Boiler 3 Dry

basis Nickel 1250 Lawrence Energy Center Boiler 3 Dry

basis SeleniumAnalysis Method for each Analyte

(example: ASTM D5865-04)

ASTM D 5865 ASTM D 3302 ASTM D 3174/5142 ASTM D 4239 ASTM D 5865 ASTM D 3174/5142 ASTM D 4239 ASTM D 3683 mod./ICP ASTM D 3684/6357 ASTM D 3683 mod./ICP ASTM D 3683 mod./ICP ASTM D 6721 ASTM D 3683 mod./ICP ASTM D 3683 mod./ICP ASTM D 3761 ASTM D 3683 mod./ICP ASTM D 3683 mod./ICP ASTM D 6722 ASTM D 3683 mod./ICP ASTM D 3684/6357EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1250 Lawrence Energy Center Boiler 3 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 0512A-WL3-0505-1 5/5/2010 5/5/2010 9501.00 Btu/lb 0513A-WL3-0505-2 5/5/2010 5/5/2010 9562.00 Btu/lb 0514A-WL3-0505-3 5/5/2010 5/5/2010 9517.00 Btu/lb 0519A-WL3-0506-1 5/6/2010 5/6/2010 9400.00 Btu/lb 0520A-WL3-0506-2 5/6/2010 5/6/2010 9538.00 Btu/lb 0521A-WL3-0506-3 5/6/2010 5/6/2010 9589.00 Btu/lb 0540A-WL3-0507-1 5/7/2010 5/7/2010 9471.00 Btu/lb 0541A-WL3-0507-2 5/7/2010 5/7/2010 9528.00 Btu/lb 0542A-WL3-0507-3 5/7/2010 5/7/2010 9582.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 21.86 5.46 0.27 12158 Btu/lb 6.98 0.34 21.6 5.31 0.28 12196 Btu/lb 6.77 0.35 21.59 5.66 0.28 12138 Btu/lb 7.22 0.36 21.92 5.96 0.28 12040 Btu/lb 7.63 0.35 20.93 5.91 0.26 12063 Btu/lb 7.48 0.33 20.72 5.67 0.27 12095 Btu/lb 7.15 0.34 21.57 5.77 0.33 12076 Btu/lb 7.36 0.42 21.04 5.86 0.31 12066 Btu/lb 7.43 0.4 20.75 5.83 0.32 12091 Btu/lb 7.35 0.41Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) <10 μg/g 0.08 μg/g <1 μg/g <1 μg/g 0.3 <10 μg/g 0.04 μg/g <1 μg/g 1 μg/g 0.3 10 μg/g 0.09 μg/g <1 μg/g 1 μg/g 0.3 13 μg/g 0.09 μg/g <1 μg/g 1 μg/g 0.3Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g <0.2 μg/g 5 μg/g 2 μg/g 18 μg/g μg/g <0.2 μg/g 4 μg/g 2 μg/g 19 μg/g μg/g <0.2 μg/g 4 μg/g 2 μg/g 17 μg/g μg/g <0.2 μg/g 5 μg/g 3 μg/g 18 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 4 μg/g <1 μg/g 58 μg/g 2 μg/g 21.86 4 μg/g <1 μg/g 62 μg/g 2 μg/g 21.6 5 μg/g <1 μg/g 68 μg/g 2 μg/g 21.59 4 μg/g <1 μg/g 2 μg/g 21.92 20.93 20.72 21.57 21.04 20.75 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 43.27 6.98 49.75 69.94 4.75 0.88 0.34 43.64 6.77 49.59 70.14 4.73 0.85 0.35 43.53 7.22 49.25 69.69 4.74 0.88 0.36 43.32 7.63 49.05 69.21 4.79 0.91 0.35 43.37 7.48 49.15 68.97 4.85 0.88 0.33 43.91 7.15 48.94 69.1 4.89 0.88 0.34 43.02 7.36 49.62 69.54 4.88 0.87 0.42 43 7.43 49.57 69.29 4.92 0.87 0.4 43.21 7.35 49.44 69.31 4.89 0.87 0.41 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

17.11 17.16 17.11 17.11 17.49 17.64 16.93 17.09 17.17EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 1250 Lawrence Energy Center Boiler 3 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 0512A-WL3-0505-1 5/5/2010 5/5/2010 9501.00 Btu/lb 0512A-WL3-0505-2 5/5/2010 5/5/2010 9562.00 Btu/lb 0512A-WL3-0505-3 5/5/2010 5/5/2010 9517.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 21.86 5.46 0.27 12158 Btu/lb 6.98 0.34 21.6 5.31 0.28 12196 Btu/lb 6.77 0.35 21.59 5.66 0.28 12138 Btu/lb 7.22 0.36Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) <10 μg/g 0.08 μg/g <1 μg/g <1 μg/g 0.3 <10 μg/g 0.04 μg/g <1 μg/g 1 μg/g 0.3 <10 μg/g 0.09 μg/g <1 μg/g 1 μg/g 0.3Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g <0.2 μg/g 5 μg/g 2 μg/g 18 μg/g μg/g <0.2 μg/g 4 μg/g 2 μg/g 19 μg/g μg/g <0.2 μg/g 4 μg/g 2 μg/g 17 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 4 μg/g <1 μg/g 58 μg/g 2 μg/g 4 μg/g <1 μg/g 62 μg/g 2 μg/g 5 μg/g <1 μg/g 68 μg/g 2 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

21.86 43.27 6.98 49.75 69.94 4.75 0.88 0.34 21.6 43.64 6.77 49.59 70.14 4.73 0.85 0.35 21.59 43.53 7.22 49.25 69.69 4.74 0.69 0.36 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 17.11 17.16 17.11EIA

Facility Code Facility

Name Boiler ID 1250 Lawrence Energy Center Boiler 3

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) 0509A-WL3-0504-1 5/4/2010 5/4/2010 9451.00 0510A-WL3-0504-2 5/4/2010 5/4/2010 9549.00 0511A-WL3-0504-3 5/4/2010 5/4/2010 9607.00 0512A-WL3-0505-1 5/5/2010 5/5/2010 9501.00 0513A-WL3-0505-2 5/5/2010 5/5/2010 9562.00 0514A-WL3-0505-3 5/5/2010 5/5/2010 9517.00 0540A-WL3-0507-1 5/7/2010 5/7/2010 9471.00 0541A-WL3-0507-2 5/7/2010 5/7/2010 9528.00 0542A-WL3-0507-3 5/7/2010 5/7/2010 9582.00 Fuel Testing ResultsHAPs Test Group

Non-dioxin/furan organic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) Btu/lb 20.67 6.71 0.26 11914 Btu/lb 20.3 6.28 0.25 11981 Btu/lb 20.56 5.76 0.27 12093 Btu/lb 21.86 5.46 0.27 12158 Btu/lb 21.6 5.31 0.28 12196 Btu/lb 21.59 5.66 0.28 12138 Btu/lb 21.57 5.77 0.33 12076 Btu/lb 21.04 5.86 0.31 12066 Btu/lb 20.75 5.83 0.32 12091HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Btu/lb 8.46 0.33 Btu/lb 7.88 0.32 Btu/lb 7.25 0.34 Btu/lb 6.98 0.34 <10 μg/g 0.08 μg/g Btu/lb 6.77 0.35 <10 μg/g 0.04 μg/g Btu/lb 7.22 0.36 <10 μg/g 0.09 μg/g Btu/lb 7.36 0.42 Btu/lb 7.43 0.4 Btu/lb 7.35 0.41Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis)

<1 μg/g <1 μg/g 0.3 μg/g <0.2 μg/g 5 <1 μg/g 1 μg/g 0.3 μg/g <0.2 μg/g 4 <1 μg/g 1 μg/g 0.3 μg/g <0.2 μg/g 4Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units

μg/g 2 μg/g 18 μg/g 4 μg/g <1 μg/g μg/g 2 μg/g 19 μg/g 4 μg/g <1 μg/g μg/g 2 μg/g 17 μg/g 5 μg/g <1 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon 20.67 43.13 8.46 48.41 68.24 20.3 43.32 7.88 48.8 68.55 20.56 43.84 7.25 48.91 69.33 58 μg/g 2 μg/g 21.86 43.27 6.98 49.75 69.94 62 μg/g 2 μg/g 21.6 43.64 6.77 49.59 70.14 68 μg/g 2 μg/g 21.59 43.53 7.22 49.25 69.69 21.57 43.02 7.36 49.62 69.54 21.04 43 7.43 49.57 69.29 20.75 43.21 7.35 49.44 69.31 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen 4.88 0.8 0.33 17.29 4.82 0.8 0.32 17.63 4.86 0.79 0.34 17.43 4.75 0.88 0.34 17.11 4.73 0.85 0.35 17.16 4.74 0.88 0.36 17.11 4.88 0.87 0.42 16.93 4.92 0.87 0.4 17.09 4.89 0.87 0.41 17.17 Ultimate Analy

ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/g