Wast e Fee d Profiles 
Report! R7O0B 

DATE: 11/30/05 

ONYX ENVIRONMENT All SERVICES, LLC 

WASTE PROFILE SUMMARY 

BUSINESS: 

DEPT 

ADDRESS 1 

ADDRESS 2 

VST. . 

ACT. . 

ARCHER DANIELS MIDLAND, COVITAMIN E PLANT 

37 OO E. DIVISION STREET 

DECATUR IL 62526 

DAVID BROADHACKER 

WASTE NAME: SOLVENT RECOVERY 

PROCESS GENERATING WASTE: SOLVENT RECOVERY 

SHIP. NAME: WASTE FLAMMABLE LIQUIDS, N.O.S 

ADDL. DESC: (ACETONE, METHANOL) 

Version 06.04 

TWI-028691 

SELLING REGION LAB 

NUMBER : 142-8-7B9 

PHONE : 217/451-4392 

EXPIRES : 01/11/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: ILR000021550 

STATE EPA ID..: 115015534S 

EPA STATUS . . . . : CH2C RESTRICT 

SALES OFFICE..; RPR 

CHEMICAL COMPOSITION 

ACETONE 

HEPTANE 

METHYL ALCOHOI 

WATER 

BENZENE 

NON-TRI CHEMICALS 

EMULSIFIED OIL 15 

UNIT DESCRIPTION 

25 35 % 

25 35 % 

25 35 % 

1 38 % 

1 3B PPM 

25 % 

METALS EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State...; Liquid 

Flash Point > = 200 CL 

pH : 04.0 - 09.0 

Color VARIES 

Odor NONE 

Layers ; Single Layer 

Specific Gravity.: 0.950 - 1.150 

Free Liquids : 99 - 100 

Cyanides < 5 : PPM TOTAL 

Sulfides < 3 PPM TOTAL 

PCB*s : ppm. Regulated by 40 CFR 761: 

Phenolics : < 10 PPM 

% Taxable : DOT UN/NA NBR: UN1993 

Treatment Codes..: T07 

CRQ RPT QTY : Material Class: 

EPA Permit : EXP: 

Hazard Class : 3 

State Codes : 090001 

Benzene 38 NESHAP: Controlled Benzene NESHAP 

Packing Group....: II 

process Codes....: CBC 

Cert o£ Dstrct Rq: 

Federal Codec; DOOl D018 F003 

KEO. GREY GLOVES 

TYPE C RESPIS CONST FLOW 

HANDLING 

H-DEX INNER GLOVE 

INDEX/BLUE NimiLE (INNER GLOVE) 

BENZENE NESHAP CONTROLS REQUIRED; NO CERT 

CANCER SUSPECT AGENT: BENZENE 

Inhalation: 2 

DOT PROPERTIES 

Oral: 2 Flammable: 0 Health: 0 

Waste Type 

Form Code 

B219 

1 

CHARGE CODE: ITS 

BENZENE NESHAP CONTROLS REQUIRED; 

COMMENTS 

REVIEWED FOR MACT METALS 

VES01799 5 
Report: R7008 

DATE: 11/24/09 

ONYX ENVIRONMENTAL SERVICES, 

WASTE PROFILE SUMMARY 

BUSINESSi 

DEPT 

ADDRESS l i 

ADDRESS 2: 

I""" VST. . : 

.CT. . : 

IMPERIAL CLEANERS 

2210 WISCONSIN AVE 

NEK HOLSTEIN 

KEN WALKER 

WASTE NAME: fBTRACHLOROETHYLENE CONTAMINAT ED SOIL 

PROCESS GENERATING WASTE: CLEANUP OF TETRACHLOROETHYLENE SOIL FROM DRY CLEAN 

SKIP. NAME: HAZARDOUS WASTE, SOLID, N.O.S 

ADDL. DESC: EQ (TETRACHLOROETHYLENE) 

Version 06.04 

TWI-096110 

SELLING REGION LAB 

NUMBER : 144-0-059 

PHONE. : 920/898-4800 

EXPIRES 10/01/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: WID981540040 

STATE EPA ID..: 9550019999 

EPA STATUS CHK RESTRICT 

SALES OFFICE. . ; CSH 

CHEMICAL COMPOSITION 

TETRACHLOROETHYLENE 

SOIL 

NON-TRI CHEMICALS 

PAPER, PLASTIC, 

9 - MAX UNIT DESCRIPTION 

0 10000 PPM 

95 100 % 

0 5 % 

METALS EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State...: Solid 

Flash Point : > = 200 CL 

pH : 05.0 - 10.0 

Color ,: BROWN 

Odor : NONE 

Layers : single Layer 

Specific Gravity.: 0.000 

Free Liquids : 0 

Cyanides : < 5 PPM TOTAL 

Sulfides : < 3 PPM TOTAL 

PCB'a : ppm. Regulated by 40 CFR 761: 

Phenolics < 10 PPM 

H Taxable : DOT UN/NA NBR: NA3077 

Treatment Codes..: T07 

CRQ RPT QTY : 100 Material Class: 

EPA Permit : EXP: 

Hazard Class.....: 9 

State Codes......: 090001 

Benzene NESHAP: 

Packing Group....: Il l 

Process Codes..,.: BSL 

Cert of Dstrct Rq: 

Federal Codes: F002 

HANDLING 

NEO. GREY GLOVES N-DEX INNER GLOVE 

TYPE C RESPIR CONST FLOW 

INDEX/BLUE NITBILE (INNER GLOVE) 

Jcapplers chem tape 2 

DOT PROPERTIES 

Inhalation: 2 Dermal: 2 Oral: 2 Flammable: 0 

Waste Type 

Form Code 

B301 

1 

CHARGE CODE: NS 

PE EVENT EXPIRES 12-31-09 

COMMENTS 

REVIEWED FOR MACT METALS 

VES01799 6 
Report! R700 8 

DATE! 11/24/09 

BASF CORP 

. .HANNIBAL PLANT 

315 0 HWY JJ 

ONYX ENVIRONMENTAL SERVICES, LLC 

WASTE PROFILE SUMMARY 

MO £3461 

BUSINESS: 

DEPT 

ADDRESS 1 

ADDRESS 2 : 

«" 'r/ST, . : PALMYRA 

vCT. . : 

WASTE NAME: IMI-2 HERBICIDE ORGANIC WASTE SPILL CLEANUP 

PROCESS GENERATING WASTE: ORGANIC WASTE SPILL CLEANUP 

SHIP. NAME: HAZARDOUS WASTE, SOLID, N.O.S 

ADDL. DESC: (TOLUENE, METHANOL) 

Version 06.04 

TWX-097802 

SELLING REGION LAB 

NUMBER 10S-7-002 

PHONE. : 

EXPIRES ! 10/27/11 

STATUS : APPR FOR SERV 

FEDERAL EPA ID: MOD050226075 

STATE EPA ID..! 9290019999 

EPA STATUS : CHK RESTRICT 

SALES OFFICE..: RPK 

CHEMICAL COMPOSITION 

METHANOL 

TETRAHYDROFuaUJ 

TOLUENE 

WATER 

NON-TRI CHEMICALS 

SOIL AND GRAVEL 

SPILL CLEAN-UP DEBRIS 

HERBICIDE BY-PRODUCTS 

0 

0 

.1 

0 

95 

0 

0 

UNIT DESCRIPTION 

.1 % 

.1 % 

2 % 

1 % 

99 % 

1 % 

.1 % 

METALS EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State...: Solid 

Flash Point N/A CL 

pH : 04 . 0 - 09 . 0 

Color : BROWN 

Odor ; NONE 

Layers . : Single Layer 

Specific Gravity.: 0.000 

Free Liquids : 0 

Cyanides : < 5 PPM 

Sulfides : < 3 PPM 

PCB'S : PP">, Regulated by 40 CFR 761: 

Phenolics ....,...:< 10 PPM 

% Taxable : DOT DN/NA NBR: NA3 077 

Treatment Codes..: T07 

CRQ RPT QTY : Material Class: 

EPA Permit EXP: 

Hazard Class : 9 

State Codes : 090001 

Benzene : NESHAP: 

Packing Group....: III 

Process Codes....: BSL 

Cert of Dstrat Rq: Y 

TOTAL 

TOTAL 

Federal Codess DOOl F003 F005 

HANDLING 

NEO. GREY GLOVES N-DEX INNER GLOVE 

TYPE C RESPIR CONST FLOW 

INDEX/BLUE NITRILE (INNER GLOVE) 

DOT PROPERTIES 

Inhalation: 2 Dermal: 2 Oral: 2 Flammable: 0 Health: 0 

SUMMARY 

Waste Type B3 01 . 

Form Code 1 

COMMENTS 

CHARGE CODE: NS REVIEWED FOR MACT METALS 

PE 10-28-10 REPORT WEIGHT 

VES01799 7 
Report: R7008 ONYX ENVIRONMENTAL SERVICES , LL C 

DATE: 11/30/09 WASTE PROFIL E SUMMARY TWI-TW2519 

SELLIN G REGION 

BUSINESS: VEOLI A ES TECHNICA L SOLUTIONS 110-9-722 

DEPT 

ADDRESS 1 7 MOBILE AV E EXPIRE S 11/30/14 

ADDRESS 2 CONTRACT NOT I N PLAC E 

r "-/st.. 

SAUGET I L 62201 FEDERAL EPA ID : ILD09864242 4 

CT. . 

STATE EPA ID . . : 163121000 9 

E PA STATUS. . . . : CHK RESTRIC T 

WASTE NAME I OW-SITE RAINWATER St ASH WATER SALES OFFICE . . : RPK 

PROCESS GEHERAriNG WASTE: COLLECTION OF ON-SITE STORMWATER & PRECIPITATION; 

SHIP. NAME: HAZARDOUS WASTE, LIQUID, N.O.S 

ADDL. DESC: 

CHEMICAL COMPOSITION 

WATER 

NON-TRI CHEMICALS 

ASHWATER 

MISC SOLIDS, WASTE RESIDUES 

MIN - MAX UNIT DESCRIPTION 

9 9 10 0 % 

50 % 

1 % 

METALS 

Arsenic as As 

Cadmium as Cd 

Lead as Pb 

Mercury as Hg 

Selenium as Se 

Chromium Hex 

Nickel as Ni 

Thallium as Tl 

EP TOX/TCLP 

5.0 

1.0 

5.0 

.2 

1.0 

mg/l 

mg/l 

mg/l 

mg/l 

mg/l 

PHYSICAL CHARACTERISTICS 

Physical State...: Liquid 

Flash Point : > - 200 CL 

pH : 02.0 - 12.5 

Color : VARIES 

Odor NONE 

Layers ...: Single Layer 

Specific Gravity.: 0.950 - 1.150 

Free Liquids : 99 - 100 

Cyanides..; : < 5 PPM TOTAL 

Sulfides : < 3 PPM TOTAL 

PCB'S : ppm. Regulated by 40 CFR 761: 

Phenolics..-. : < 10 PPM 

% Taxable : DOT UN/NA NBR: NA3 0 82 

Treatment Codes..: T07 

CRQ RPT QTY : Material Class: 

EPA Permit EXP: 

Hazard Class.....: 9 

State Codas : 090001 

Benzene : NESHAP: 

Packing Group....: Il l 

process Codes....: 

Cert of Dstrct Rq: 

Federal Codes: D007 D008 D004 D005 D006 D009 DOlO D011 D012 D013 D014 D015 D016 D017 D018 + 

SIT E GENERATED WASTE 

Inhalation: 0 

DOT PROPERTIES 

Dermal: 0 Oral: 0 Flammable: 0 Health: 0 

TWI Signed Addendum 

SITE GENERATED 

VES01799 8 
Report: R7008 

DATE: 11/3 0/09 

ONYX ENVIRONMENTAL SERVICES, 

WASTE PROFILE SUMMARY 

BUSINESS : 

DEPT 

ADDRESS 1 

ADDRESS 2 

f—-Y/ST. . 

ICT. . 

US ARMY FLW 

. .DIRECTOR OF PUBLIC WORKS 

IMWE-LNW- PWE,BLDG 2101, DPW 

133 4 1ST ST 

FORT LEONARD WOOD MO 65473-

SHANNON CAIN 

nASTE NAME: DECON WATER-TREATED VX S GB TO DRINKING WATER STANDARDS 

PROCESS GENERATING WASTE: DECON OF CHEMICAL WEAPONS RECOGNITION TRAINING COM 

SHIP. NAME: NON-REGULATED MATERIAL 

ADDL. DESC: 

Version 06.04 

TWI-076886 

SELLING REGION LAB 

NUMBER : 143-8-393 

PHONE : 573 596 0682 

EXPIRES : 02/19/11 

STATUS APPR FOR SERV 

FEDERAL EPA ID: MO3213720979 

STATE EPA ID..: 9290019999 

EPA STATUS : UNDETERMINABL 

SALES OFFICE..: TWI 

CHEMICAL COMPOSITION 

WATER 

SODIUM HYDROXIDE 

NON-TRI CHEMICALS 

SUPER TROPICAL BLEACH 

COMMENTS 

TRACES OF VX AND GB AGENT ARE NEUTRALIZED WITH BLEACH AND RINSED 

WITH THOUSANDS OF GALLONS OF WATER, THEN COLLECTED FOR 

INCINERATION. ALL WATER IS TESTED PRIOR TO SHIPMENT TO ENSURE 

COMPLIANCE WITH DRINKING WATER STANDRADS. VX AND GB 

CONCENTRATION ARE CERTIFIED TO BE BELOW 20 PPB AND ARE USUALLY 

<2 PPB. (3X LEVEL) 

UNIT DESCRIPTION 

93 

1 

100 % 

2 % 

5 % 

EP TOX/TCLP PHYSICAL CHARACTERISTICS 

Physical State...: Liquid 

Flash Point > =. 200 CL 

pH : 05.0 - 09.0 

Color : VARIES 

Odor : NONE 

Layers. s Single Layer 

Specific Gravity.: 0.950 - 1.150 

Free Liquids : 99 - 100 

Cyanides : < 5 PPM TOTAL 

Sulfides < 3 PPH TOTAL 

PCB's : N/A ppm. Regulated by 40 CFR 761: 

Phenolics : < 10 PPM 

% Taxable : DOT UN/NA NBR: 

Treatment Codes. . : T07 

CRQ RPT QTY,.....: Material Class: 

EPA Permit. EXP: 

Hazard Class.....: 

State Codes : 090002 

Benzene : NESHAP: 

Packing Group....: 

Process Codes....: DI2 

Cert of Dstrct Rq: Y 

Federal Codes: 

NEO. GREY GLOVES 

TYPE C RESPIR CONST FLOW 

HANDLING 

N-DEX INNER GLOVE 

INDEX/BLUE NITRILE (INNER GLOVE) 

DI-WATER WITH DECOMPOSITION PRODUCTS OF GB/VX. 

REACTIVE CATEGORY: A (FOR SCHEDULING ONLY) 

Inhalation: 2 Dermal: 3 

DOT PROPERTIES 

Oral: 2 

Waste Type 

Form Code 

B219 

1 

.CHARGE CODE: NS 

HIVE CATEGORY: A (FOR SCHEDULING ONLY) 

jj-18-10 

"BILLING: TRIP TICK, WT TIC, COD AND COPY OF TAG 

TO RETURN WITH MANIFEST TO GENERATOR ALSO. 

REVIEWED FOR MACT METALS 

COD REQUIRED 

VEOLIA TRANSPORTATION ONLY. 

WITH INVOICE. WHEN COD IS PRINTED, COPY TO CSR 

VES01799 9 
TWI Laboratory Analysis Report 

Receiver #: TK304 Visual Inspection: Glove Box / Hooded Feeder 

# of Drums: 1 

Date: 6/29/2001 

Profile #:2ZZ2ZZ 

Generator TRADE WASTE INCINERATION 

Descript: 

Process Code(s): 

Drum Storage Compatability 

Profiled DOT Hazard Class 9 

P = Pass F = Fail 

8A 8B 4/5 

Sample Number 

Drum Rep / Comp 

303022]_iL00000001j 

1/ IIII 11 

303022 

Free Liquid (%) IIII 11 

303022 

Profile Conform Date Initials 

Pumpable NO 

IIII 11 

303022 wwww v Yes No 11/06/09 MT 

Layers/Phases -% Ea. www w 

Color ^\\\ 

Turbidity www w W W 

Viscosity L X 

Physical State www w 

Water Miscibility WWW W W \ V 

Add. Description 

Water Reactivity www w W W 

Radiation Screen =BKG X 

Flam. Pot. Screen See Flashpoint X 

pH Screen 5 at 100 pent 2-12.5 X 

Oxidizer Screen 

Paint Filter Test WWWN W 

Cyanide Screen WWW W 

Sulfide Screen WWW W 

Incidental Odor www w ^\\\ Specie Gravity 1.01 11/04/09 MT 

BTU/Lb 1570 11/04/09 BD 

% Chloride 1.2 W W i 11/04/09 KD 

Flash Point - Deg F w w 01/01/00 

PCBs By GC - mg/kg <50ppm 11/06/09 

pH by Meter wwww J W W 01/01/00 

Arsenic mg/kg 4.768 0 

Beryllium mg/kg 4.765 0 

Cadmium mg/kg 4.765 0 

Chromium mg/kg 4.805 0 

Lead mg/kg 4.784 0 

Mercury mg/kg 0.056 0 W W 

Profile Review for Appendix WAP-C Consitituenfs by: 

Date: 

Add. Comments: The data in the sample information section(6/29/2001)is date profile 777777 was created. 

VES01800 0 
File Inventory Print Approvals Chemist Receiving Laboratory Tank Farm Process Planning Window Billing Help 

I Laboratory 5ample Analysis 

pie Number 

r Edit Mode Update and 

Submit to Lab 

Manager 

Cancel 

Exit 

Manifest 100000001 

Layers/Phases Y~ 

Sample Status L 

ITesQ \_ 

•Approval— 

Status View Profile 

~ 2 Summary 

r Sample Status Codes -

Comments 

ViewPDW 

Submit 

ReSample = S *i 

PCB suspect = P 

In Laboratory = L 

Metals = E a 

Pending Lab Manager Approval = M 

Discrepant = D ^_ 

Rejected = R 

Conforms/Accepted = A Y 

p Water Reactivity 

T No RXN f" RXN: 

• Radiation Screen 

r =BKG r >BKG: 

Value 

-Flam. Pot Screen 

r Neg r Pos T BOC 

ppH ScreenValue fg " W 100% r 10* 

r Oxidizer SaeenT Neg r Pos 

• Paint Filter Test 

r Pass T Fail H V-Fail T N/A 

Specific Gravity 

BTU/lb 

£ Chloride 

Flash Point (Deg. F) 

PCBs by GC (mg/kg) 

PCB GC Comment 

PCBs-Screen (ppm) 

1.01 

1570 

1.2 

jl/1/1900 

1/1/1900 

p Cyanide Screen 

JTM Negf" PosP N/A j ~ Cyantesmo 

2.4,5 - T (ppm) 

Silvex (ppm) 

(1/1/1900 " | 

-Sulfide Screen 

r Neg r Pos T N/A 

PCP Screen (ppm) 

pH by Meter 

r KIT F SC |W190Q 

r iooxr 10^)1^1/1900 

-Metals-—— 

As j4.7S8 

Pb 14.784 

- Incidental Odor 

r No r Yes: 

Adjust Metals 

Ash %-

VES01800 1 
I Wl Laboratory Analysis Keport 

Receiver #: TK310 Visual Inspection: Glove Box / Hooded Feeder 

# of Drums: 1 

Date: 6/29/2001 

Profile #.7777.7.7 

Generator: TRADE WASTE INCINERATION 

Descript: 

Process Code(s): 

Drum Storage Compatability 

Profiled DOT Hazard Class 9 

P = Pass F=Fai/ 

8A 8B 4/5 

Sample Number 

Drum Rep / Comp 

301556J_IL00000001 

1/ II 111 11 

301556 

Free Liquid (%) II 111 11 

301556 

Profile Conform Date Initials 

Pumpabte NO 

II 111 11 

301556 wwww v Yes No 10/01/09 SL 

Layers/Phases -% Ea. \\\\\\\ w ^\\\ Color wwww v 

Turbidity 

Viscosity L X 

Physical State 

Water Misdbility \\\w\\\ v W W " 

Add. Description 

Water Reactivity wwww v W W 

Radiation Screen =BKG X 

Flam. Pot Screen See Flashpoint X 

pH Screen 3 at 100 pent 2-12.5 X 

Oxidizer Screen wwww v 

Paint Filter Test wwww v 

Cyanide Screen wwww v ^\\\ Sulfide Screen \\\\\\\ w ^\\\ Incidental Odor wwww v ^\\\ Specific Gravity 0.83 

^ 

10/01/09 SL 

BTU/Lb 9600 ^\\\ 10/01/09 MT 

% Chloride <0.S ^\\\ 10/01/09 JF 

Flash Point - Deg F w w ^ 01/01/00 

PCBs ByGC - mg/kg <50ppm 10/01/09 

pH by Meter 01/01/00 

Arsenic mg/kg 0 0 

Beryllium rtig/kg 0 0 

Cadmium mg/kg 0 0 

Chromium mg/kg 0 0 

Lead mg/kg 0 0 

Mercuiy mg/kg 0 0 W W 

Profile Re/iewfor Appendix WAP-C Consitituents by: 

Date: 

Add. Comments: The data in the sample infonnation section(6/29/2001)is date profile 7.77777 was created. 

VES01800 2 
Fie Inventory Print Approvals Chsmist Receiving Laboratory Tank Farm Process Planning Window Biling Help, 

•S1 utipf dlgry Siiiriple Analysis 

Sample PJumberUpdate Cancel 

r Edit Mode Update and Submit to Lab 

Manager 

Manifest ILOQ000001 Sample Status W 

•Approval 

Status 

i 3 . 

View Profile 

Summaiy 

Comments 

ViewPDW 

Cancel Submit 

• Sample Status Codes - ReSample = S PCB suspect = P 

In Laboratory =1 

Metals = E 

Pending Lab Manage! Approval = M 

Discrepant * D 

Rejected = R 

Conforms/Accepted » A 

Layers/Phases J Ei S 

[-Water Reaotivily 

f~ No RXN F* RXN: 

• Radiation Screen 

P -BKG r >BKG: 

p Ram. Pot Screen 

f" Neg i~ Pos r BOC 

•pH ScreenValue J5 jy 1005 £ r- m 

-Oxidizer Screenr Neo r Pos 

- Paint Filter Test 

r Paw r Fail I~ V-Fail T N/A 

f Cyanide Saeen 

f" Negr" PosT N/A (~ Cyantesmo 

r Sulfide Screen 

T Neg T Pos r N/A 

Value Date 

Specific Gravity 

BTU/lb 

2 Chloride 

Flash Point (Deg. F) 

PCBs by GC [mg/kg] 

PCB GC Comment 

PCBs-Screen (ppm) 

0.85 

[SB10 

j<0.5B 

Initials 

|11/15/2009 |MT 

|li/15/2009 ~ |mT 

(11/15/2009 [MT 

h/1/1900 

2,45-T Ippm) 

Silvex (ppm) 1/1/1900 

PCP Screen (ppm) 

pH by Meter 

r KIT r GC |V1/19C0 

r lOO^r 10*1,1/1/1900 

•Metals 

- Incidental Odor 

r No T Yes: 

•Ash % 

VES01800 3 
I WI LaDoratory Analysis Keport 

Receiver #: 352920 Sample Required 

# of Drums: 1 

Date: 10/22/2009 

Profile #. 076886 

Generator: US ARMY FLW 

Descript: DECON WATER-TREATED VX & GB TO DRINKING WATER STANDARDS 

Process Code(s): DI2 

Drum Storage Compatability 

Profiled DOT Hazard Class 9 

P = Pass F <> Fail 

8A 8B 4/5 

Sample Number 

Drum Rep / Comp 

302522j_005389778JJ 

BULK/1 

Free Liquid (%) 100 

' mi n III Profile Conform Date Initials 

Pumpable YES 302522 www w Yes No 10/22/09 BD 

Layers/Phases -% Ea. 100 WW\W W 

Color colorless wwvw w W W 

Turbidity transparent www w W W 

Viscosity low L X 

Physical State liquid wwww\ > ^ w \ Water ffecibility Misc www w W W 

Add. Description 

Water Reactivity No RXN www w W W 

Radiation Screen -BKG =BKG X 

Flam. Pot. Screen NEGATIVE See Flashpoint X 

pH Screen 7 at 100 pent 2-12.5 X 

Oxidizer Screen NEGATIVE www w \\\ \ 

Paint Filler Test N/A www w ^\\\N 

Cyanide Screen NEGATIVE www w 

Sulfide Screen NEGATIVE ^\\\ wwww ^ ^\\\ Incidental Odor No www w 

Specific Gravity 1.01 0.950-1.150 10/22/09 BD 

BTU/Lb <500 1 -5000 10/22/09 KD 

% Chloride <0.5 2 -0 10/22/09 AJ 

Flash Point - Deg F >140 W W i 01/01/00 

PCBs By GC - mg/kg <50ppm 10/22/09 

pH by Meter www w W W 01/01/00 

Arsenic ing/kg 0 0 W W 

Beryllium mg/kg 0 0 W W 

Cadmium mg/kg 0 0 ^\\\ Chromium mg/kg 0 0 

Lead mg/kg 0 0 W W 

Mercury mg/kg 0 0 W W 

% Ml--3,1! 

Additional Comments: MAY SHOW POS OX SCREEN DUE TO BLEACH-OKAY TO ACCEPT. 

Profile Review for Appendix WAP-C Consitituents by: KMEREDITH 

Date: 3/13/2009 

Add. Comments: DI-WATER W/DECOMPOSITION PRODUCTS OF GB/VX 

VES01800 4 
C M S Performanc e Evaluatio n 

VES01800 5 
TAG 

LOOP 

DESCRIPON 

SERVIC E 

LOCATION 

LP-SH T 

P&ID 

REMARKS 

INSTL-RMKS 

SPEC-RMKS 

S / N 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

QUARTERLY 

WT 

204 

WEIGHT TRANSMITTER 

SPECIALT Y FEEDER 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

CALIBRATIO N NOTES 

TOLEDO 

8140 EXP 

0-4,00 0 # 

0-4,00 0 # 

4-2 0 MADC 

0#-819 Ct S 

200#=983 Ct S 

1#=.819 ct s 

30052 

Chec k scale , digita l Calibratio n per . Toled o instructions . 

The n wit h n o weigh t o n scal e adjus t analo g zero . (NOTE: HMI 

wil l no t displa y number s les s tha n zero) . Nex t ad d weigh t 

= t o 10% ar e mor e o f scale s range , the n adjus t analo g span , 

t o indicat e weigh t o n scale , a s rea d o n HMI screen . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INSTRUMENT READING 

Before Calibration s*\ 

_ is i 

After Calibration 

INPU T VALU E 

Q _ 

ISO 

CALIBRATIO N SOURCE REFERENC E 

Comments 

Performe d by: ^ Date : Time : Z.A M (v\ 

J B Place : 

CALSHEET . WDB /(Field)or Shop) 

VES01800 6 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNIT #2 

QUARTERLY 

WT 

210 

WEIGHT TRANSMITTER 

SOLID CHARG CONV. 

FIEL D 

303 1 

MANLTFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-ODT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

TOLEDO 

8140 

0-40 0 # 

0-40 0 # 

4-2 0 MADC 

0#=819 Ct S 

200#=2457 Ct S 

1#=8.19 Ct S 

I / O NUMBER: 30070 

CALIBRATIO N NOTES 

Chec k scale , digita l Calibratio n per . Toled o instructions . 

The n wit h n o weigh t o n scal e adjus t analo g zero . (NOTE: HMI 

wil l no t displa y number s les s tha n zero ) . Nex t ad d weigh t 

= t o 10% ar e mor e o f scale s range , the n adjus t analo g span , 

t o indicat e weigh t o n scale , a s rea d o n HMI screen . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E 

o 

so 

INSTRUMENT READING 

Before Calibration ^ 

Afte r Calibration 

50.2 -

CALIBRATIO N SOURCE REFERENC E 

Comments : 

Performe d b y : ,fe^ — f • Date : ifi'l 0!-® ! Time : 2-)S" " AMTg p 

J B Place : 

CALSHEET.WDB QFieli^or Shop) 

VES01800 7 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

QUARTERLY 

PDT 

250 

PRESSURE DIFF . TRANSMITTE MANUFACT: YOKOGAWA 

BAGHOUSE INLET/OUTLE T 

FIEL D 

2035 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I/O NUMBER: 

0-1 5 i n wc 

4-2 0 MA 

CALIBRATIO N NOTES 

U SE PNEUMATIC CALIBRATIO N BENCH WITH MANOMETER AND LOOP 

CALIBRATOR . INPU T PNEUMATIC SIGNAL AND READ OUTPUT WITH 

LOOP CALIBRATOR . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPOR T 

INPU T VALU E INSTRUMENT READING 

0 W. c • Befor e Calibratio n ^.OU X 

q After Calibration. (_j q ^ 

2.0,0 ^ACALIBRATIO N SOURCE REFERENC E 

Comments : 

Performe d by : — - _ Date : Time: . M± am(pF ) 

 t - -, • = ^ ^^ ^ 

J B Place ; 

CALSHEET.WDB [Field dr Shop) 

VES01800 8 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

QUARTERLY 

PT 

200 

PRESSURE TRANSMITTER 

LOW CHAMBER 

FIEL D 

203 2 

MANUFACT 

MODEL 

SCALE 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTIO N 

I / O NUMBER 

•7. 5 t o +2. 5 in . 

4-2 0 MA 

wc . 

CALIBRATIO N NOTES 

Connec t transmitte r t o b e calibrate d t o pressur e sourc e an d 

calibrate d referenc e (Manometer) , inpu t appropriat e pressur e 

a n d verif y wit h curren t meter . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E INSTRUMENT READING 

-7. S 

if Before Calibration 

W.C -

-7-S " 

After Calibration 

2S 2.0 . A 

CALIBRATIO N SOURCE REFERENC E 

Comments : 

Performe d bv : -i^* — I • Date JD-Z2-0CJ Time.-Z'fl O AM^T) 

J B Place : ; ^=r>v 

CALSHEET.WDB (Field o^Shop)) 

VES01800 9 
TWI INSTRUMENT CALIBRATIO N RECORD 

UNIT #2 

QUARTERLY 

TAG : PT 

LOOP: 219 

DESCRIPON : PRESSURE TRANSMITTER 

SERVICE : UPPER CHAMBER 

LOCATION : FIEL D 

LP-SHT : 

P&ID : 3033 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

MANUFACT 

MODEL 

SCALE 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTIO N 

I / O NUMBER 

7 . 5 t o +2. 5 in . wc . 

4-2 0 MA 

CALIBRATIO N NOTES 

Connec t transmitte r t o b e calibrate d t o pressur e sourc e an d 

calibrate d referenc e (Manometer) , inpu t appropriat e pressur e 

a n d verif y wit h curren t meter . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

XNPUT VALU E 

—~ .— // . - Before Calibration 

INSTRUMENT READING 

Afte r Calibration 

Z.S ' 2.0. 0 y^ A 

CALIBRATIO N SOURCE REFERENC E 

Comments : 

Performe d by : _ Date : Time : Z'/S ~ AM(P M 

J B Place : 

CALSHEET . WDB (Field oifShop)) 

VES01801 0 
TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

QUARTERLY 

TAG : A T 

LOOP: 28 9 

DESCRIPON : OXYGEN MANUFACT: COSA 

SERVICE : STACK GAS ANALYZE R 

LOCATION : STACK 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

203 5 

MANUFACT 

MODEL 

SCALE 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTIO N 

I / O NUMBER 

0-25% 

0-25% 

4-2 0 MADC 

CALIBRATIO N NOTES 

Flo w calibratio n ga s a t 2- 3 psi g an d 3 scf h 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPOR T 

INPU T VALUE 

3- 0 

INSTRUMENT READING 

Before Calibration 

2\.i s 20- f 

1-Q 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

ZERO GAS CYL ft: CC 111 <T33 

SPAK GAS CY L #:_ SA 

Comments : 

Performe d b y 

J B 

CALSHEET . WDB 

zjhfjJt/ J DatezlMlA l Time : /t ) *'OQt 

Place : 

PM 

((Field'hor Shop) 

VES01801 1 
TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

QUARTERLY 

TAG : 

LOOP: 

DESCRJPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

AT 

288B 

HC 

STACK GAS ANALYZE R 

STACK 

556 

630 On MCS 100 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

Therm o Elec.co . 

5 1C 

0-10 0 PPM 

4-2 0 MADC 

CALIBRATIO N NOTES 

1) Ope n sampl e ga s bottl e valves . 

2) Pres s MENU Butto n 

3) Pres s CALIBRATIO N 

4) Pres s ZERO ADJUST 

5) Pres s SPA N ADJUST afte r 4)finishe d 

6) Pres s RUN afte r 5)finishe d 

7) Clos e sampl e ga s bottles . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/hr . 

CALIBRATIO N REPOR T 

INPUT VALU E 

0 

ISA 

INSTRUMENT READING 

Befor e Calibration 

0 

~?5. 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

G AS CYL #: 

Comments : 

Performe d b 

J B 

CALSHEET.WDB 

Date:i0^d23 _ Time : fg h PM 

Place: . 

(Field br Shop) 

VES01801 2 
TWI INSTRDMENT CALIBRATIO N RECORD 

UNI T #2-

QUARTERLY 

TAG : AT 

LOOP: 288 B 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

OPACITY 

STACK GAS 

STACK 

2.0 0 t o 5.70m a 

MANUFACT 

MODEL 

SCAL E 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTIO N 

I /O NUMBER 

TELEDYNE INST . 

LightHaw k 560D I 

0-100% 

4-2 0 MADC 

CALIBRATIO N NOTES 

Clea n window s 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPUT VALU E INSTRUMENT READING 

Befor e Calibration 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comments 

Performe d by : CKuc k £du]&.Cofs Date : Time : j^AM$)PM 

J B Place : ^ 

CALSHEET.WDB ffield\> r Shop) 

VES01801 3 
TAG : 

LOOP : 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRDMENT CALIBRATIO N RECORD 

UNI T #2 

ANNUAL 

TT 

200A 

P L C THERMOCOUPLE INPUT MANUFACT: 

LOWER CHAMBER MODEL: 

FIEL D SCALE : 

CALIB-IN : 

2032 CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

MODICON 

B883-20 0 

0-250 0 deg . 

TYPE K 

CALIBRATIO N NOTES 

U s e col d junctio n compensate d thermocoupl e calibrato r t o 

inpu t a typ e K temperatur e signa l o f 500 de g F . an d 2,00 0 

deg.F . a t inpu t o f PLC , the n verif y thi s singl e o n th e 

contro l pane l CRT . 

S e e Manufacture s literatur e fo r detaile d instructions , 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E 

S0o ° F 

ZQoQ ° F 

INSTRUMENT READING 

Befor e Calibration 

S O I 

-t> 

ZOOO 

After Calibration 

CALIBRATIO N SOURCE REFERENCE 

Comments : 

Performe d by : Date : Time : .am (miT) 

J B Place : 

CALSHEET.WDB (Fielde r Shop) 

VES01801 4 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNIT #2 

ANNUAL 

TT 

200B 

P L C THERMOCOUPLE INPUT 

LOWER CHAMBER 

FIEL D 

2032 

MANUFACT 

MODEL 

SCALE 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTION 

I / O NUMBER 

MODICON 

B883-20 0 

0-250 0 deg . 

TYPE K 

CALIBRATIO N NOTES 

U s e col d junctio n compensate d thermocoupl e calibrato r t o 

inpu t a typ e K temperatur e signa l o f 500 de g F . an d 2,00 0 

deg.F . a t inpu t o f PLC , the n verif y thi s singl e o n th e 

contro l pane l CRT . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E INSTRUMENT READING 

^dQO° f~ Befor e Calibration ^0O° 

7j00O° F ZQOOc 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comments : )\) o CaUiocg 'T-ic)/ \ n-eedeJ. 

Performe d by : Date : _AM(PM^ ) 

.TB 

CALSHEET.WDB 

Place : 

(Field) or Shop) 

VES01801 5 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRDMENT CALIBRATIO N RECORD 

UNIT #2 

ANNUAL 

TT 

219A 

P L C THERMOCOUPLE INPUT MANUFACT: MODICON 

UPPER CHAMBER 

FIEL D 

2033 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I/O NUMBER: 

0-250 0 

TYP E K 

deg . F . 

CALIBRATIO N NOTES 

U s e col d junctio n compensate d thermocoupl e calibrato r t o 

inpu t a typ e K temperatur e signa l o f 500 de g F . an d 2,00 0 

deg.F . a t inpu t o f PLC , the n verif y thi s singl e o n th e 

contro l pane l CRT . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPUT VALU E INSTRUMENT READING 

5~0<0D F Bef ° r e Calibration ^QQ ® 

X06O ° F Zooo ° 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comments : K)o CfllibcaiiP/ \ needed. 

Performe d by: . Date : Time : _am(pm) 

J B Plac e 

CALSHEET . WDB ((Field)or Shop) 

VES01801 6 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRDMENT CALIBRATIO N RECORD 

UNI T #2 

ANNUAL 

TT 

219B 

P L C THERMOCOUPLE INPUT MANUFACT: MODICON 

UPPER CHAMBER 

FIEL D 

2033 

MANUFACT 

MODEL 

SCAL E 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTIO N 

I/O NUMBER 

0-250 0 

TYPE K 

deg . 

CALIBRATIO N NOTES 

U s e col d junctio n compensate d thermocoupl e calibrato r t o 

inpu t a'typ e K temperatur e signa l o f 50 0 de g F . an d 2,00 0 

deg.F . a t inpu t o f PLC , the n verif y thi s singl e o n th e 

contro l pane l CRT . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPUT VALU E INSTRUMENT READING 

r-/~\ s\° f— Before Calibration —s^/>° 

\^QO tz 6 0 0 

2.006 ° 

Afte r Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comments : 

b y : fe^-TTT &y__^j2 ^ n a te://-/0-O <

Per f orme d 7Time:Z'3 ^ AM <gft 

J B 

CALSHEET.WDB 

Place : 

(FieldSor Shop) 

VES01801 7 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMIARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

ANNUAL 

TT 

223 

P L C THERMOCOUPLE INPU T MANUFACT: MODICON 

SDA INLE T 

FIEL D 

2033 

MANUFACT 

MODEL 

SCALE 

CALIB-I N 

CALIB-OU T 

PROCESS-S P 

INST-S P 

ACTIO N 

I / O NUMBER 

0-250 0 

TYPE K 

deg . 

CALIBRATIO N NOTES 

U s e col d junctio n compensate d thermocoupl e calibrato r t o 

inpu t a typ e K temperatur e signa l o f 500 de g F . an d 2,00 0 

deg.F . a t inpu t o f PLC , the n verif y thi s singl e o n th e 

contro l pane l CRT. 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPOR T 

INSTRUMENT READING 

Befor e Calibration — , o 

ZQQ\ ° 

After Calibration 

INPU T VALU E 

bOO°F 

Zooo e F 

CALIBRATIO N SOURCE REFERENC E 

Comaents : D aalibra'f/ai ^ needed. 

Performe d by: . Date : Time : Z- ^ 

J B Place : / < = av . 

CALSHEET . WDB ((Field) or Shop) 

VES01801 8 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNIT #2 

ANNUAL 

TT 

270 

P L C THERMOCOUPLE INPU T MANUFACT: MODICON 

SDA OUTLET 

FIEL D 

2034 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

0-250 0 deg . 

TYPE K 

CALIBRATIO N NOTES 

U se col d junctio n compensate d thermocoupl e calibrato r t o 

inpu t a typ e K temperatur e signa l o f 50 0 de g F . an d 2,00 0 

deg.F . a t inpu t o f PLC , the n verif y thi s singl e o n th e 

contro l pane l CRT . 

S ee Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E 

SOO ° F 

-zoo o F 

INSTRUMENT READING 

Before Calibration SOO 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comments : K) o CcS lUra-Ko ^ n€eo/ei , 

Performe d by : ( . —Qj?0 Date : M-lO-Cft Time : "2J 3S~AM(PM^ ) 

J B Place : 

CALSHEET.WDB ((Fiel'djor Shop) 

VES01801 9 
TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

ANNUAL 

TAG : FT 

LOOP: 283 

DESCRIPON : STACK 

SERVICE : STACK 

LOCATION : FIEL D 

LP-SHT : 

P&ID : 2035 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

FLOW TRANSMITTER MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

Rosemoun t 

0-20,00 0 ACFM 

0-.5"W C 

4-2 0 MADC 

S e t Damp/po t t o mi d poin t 

CALIBRATIO N NOTES 

U SE PNEUMATIC CALIBRATIO N BENCH WITH INCLIN E MANOMETER AND 

LOOP CALIBRATOR . INPUT PNEUMATIC SIGNAL AND READ OUTPUT 

WITH LOOP CALIBRATOR . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E INSTRUMENT READING 

Q

/f , . _ Before Calibration o o> •> A 

U C . 3 .% 3 * A 

. £ * W. C 1%2L„A -

<•> /' After Calibration , ., _ . 

H HO 

CALIBRATIO N SOURCE REFERENC E 

Comments : 

J^cJT T &j_ J ^ Date : tl - Time : / Cf- ( Performe d by:-J^<L — \ , <J >^ jC^CT Date : Time:/U-v:/S~> (J\M7P ~ (m) ] M 

J B Place : 

CALSHEET.WDB /Field J > r Shop) 

VES01802 0 
TAG : 

LOOP: 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNIT #2 

ANNUAL 

FT 

215 

FLOW TRANSMITTER 

HIGH BT U 

F L D 

203 1 

Change d Rang e 11/12/9 6 

SENSITIVIT Y 5.5 8 

SW 1,2,3,4 , OFF 

97193 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

MICRO MOTION 

D 40S-S S 

0-360 0 lb/h r 

4-2 0 MADC 

CALIBRATIO N NOTES 

Flus h proces s piping , connec t wate r hos e t o upstrea m sid e o f 

flo w meter , se t contro l syste m t o appropriat e rat e control , 

a n d rea d totalizer , flo w wate r int o a containe r an d compar e 

t h e toltalize r readin g t o th e measure d amount i n container . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E INSTRUMENT READING 

i . i , n Before Calibration da/ — w 

10 |k> , pe r mm . W l.l S lbs . 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comment s : M o m(<kr<a f 

Performe d b y 

J B 

CALSHEET.WD B 

Date : //-)*)-O l Time : Z'ZO AM^P*M^ ) 

Place : 

(Field/or Shop) 

VES01802 1 
TAG : 

LOOP : 

DESCRIPON : 

SERVICE : 

LOCATION : 

LP-SHT : 

P&ID : 

REMARKS: 

INSTL-RMKS : 

SPEC-RMKS : 

S/N : 

TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

ANNUAL 

FT 

216 

FLOW TRANSMITTER 

LOW BTU 

FLD 

2031 

Change d Rang e 11/12/9 6 

SENSITIVIT Y 5.1 6 

SW 1,3,4 , OFF 

32936 

MANUFACT: 

MODEL: 

SCALE : 

CALIB-IN : 

CALIB-OUT : 

PROCESS-SP : 

INST-SP : 

ACTION : 

I / O NUMBER: 

MICRO MOTION 

D 40S-S S 

0-360 0 lb/h r 

4-2 0 MADC 

CALIBRATIO N NOTES 

Flus h proces s piping , connec t wate r hos e t o upstrea m sid e o f 

flo w meter , se t contro l syste m t o appropriat e rat e control , 

a n d rea d totalizer , flo w wate r int o a containe r an d compar e 

t h e toltalize r readin g t o th e measure d amount i n container . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPUT VALU E INSTRUMENT READING 

i ~ ,, o Befor e Calibration C\ O, i n 

IO lbs , fe C Wurs. tor I Y~>\n. _ I'l l \&S> • 

After Calibration 

CALIBRATIO N SOURC E REFERENC E 

Comment s 

Performe d b y 

J B 

CALSHEET . WDB 

. Date : ll-\°i-0^ Time : Z-00 AM /PM' 

Place : 

((Fieldjor Shop) 

VES01802 2 
TWI INSTRUMENT CALIBRATIO N RECORD 

UNI T #2 

ANNUAL 

TAG : FT 

LOOP: 288 

DESCRIPON : FLOW TRANSMITTER MANUFACT: E- H 

SERVICE : LIM E SLURRY TO HEAD TANK MODEL 

LOCATION : FIEL D SCALE : 0-2 0 GPM 

LP-SHT : CALIB-I N 

P&ID : 2034 CALIB-OUT : 4-2 0 MADC 

REMARKS: PROCESS-S P 

INSTL-RMKS : INST-S P 

SPEC-RMKS : ACTIO N 

S/N : I/O NUMBER 

CALIBRATIO N NOTES 

Flus h proces s piping , connec t wate r hos e t o upstrea m sid e o f 

flo w meter . Se t contro l syste m t o appropriat e contro l rate , 

a n d rea d totalizer , flo w wate r int o a containe r an d compar e 

t h e toltalize r readin g t o th e measure d amount i n container . 

S e e Manufacture s literatur e fo r detaile d instructions . 

Fil l ou t an d affi x a new calibratio n sticker . 

0 . 1 lb/h r 

CALIBRATIO N REPORT 

INPU T VALU E 

^ o r one . ryj'muL'he.' 

INSTRUMENT READING 

Before Calibration 

After Calibration 

CALIBRATIO N SOURCE REFERENC E 

Comments : jvJo Calikca4 ^ A Ylecr^J. 

b^A^TTi 2

Performe d ^ S>J2> Date : XL-UCft Time:iH2_AM(g ) 

J B 

CALSHEET . WDB 

Place: . 

(Field)or Shop) 

VES01802 3 
5404 Jedmed Ct. - St. Louis, MO E3129 

Business: (314) 845-7778 - Fax: (314) 845-7779 

Scale Inspection Report 

C V-4- y<~-n<-^ 

Customer: ONYX ENVIRONMENTAL 

#7 MOBILE AVENUE 

SAUGET, IL 62201 

Location: Direct Injection 

MFG/Model: WI130 

Scale Type: VEHICLE 

Capacity: 60000LB 

escription: Class III L 

Serial No: 011150 

Scale No: 2 

Divisions: 5LB 

Scale was found in Tolerance: X yes 

Shift Test 

Sides/Corners/ 

Sections 

Weights 

Applied 

Scale Reading 

(As found) 

Error (+/-) Tolerance 

Maintenance 

Scale Reading After 

Adjustment (As Left) 

Accept/ 

Reject 

Section 1 21,000 lb 21,000 lb +0 lb +/- 45 lb ACCEPT 

Section 2 21,000 lb 21,000 lb +0 lb +/- 45 lb ACCEPT 

Section 3 21,000 lb 21,000 lb + 0 lb +/- 45 lb ACCEPT 

Section 4 21,000 lb 21,000 lb +0 lb +/- 45 ib ACCEPT 

Section 5 21,000 lb 21,000 lb +0 lb +/- 45 lb . ACCEPT 

Section 6 21,000 lb 21,005 lb +5 lb +/-.4S lb ACCEPT 

Buildup Weight Weights Applied Scale Reading 

(As found) 

Error (+/-) Tolerance 

Maintenance 

Scale Reading After 

Adjustment (As Left) 

Accept/ 

Reject 

Section 4 3,000 lb 3,000 lb +0 lb +/- 10 lb ACCEPT 

6,000 lb 6,000 lb +o lb +/- 15 lb ACCEPT 

9,000 lb 9,000 ib " +0 lb +/- 20 lb ACCEPT 

12,000 lb 12,000 ib +0 lb +/- 25 lb ACCEPT 

15,000 lb ' 15,000 lb +0 lb +/- 30 lb ACCEPT 

18,000 lb 18,000 lb +0 lb +/- 40 lb ACCEPT 

Section 4 21,000 lb 21,005 lb +5 lb +/- 45 lb ACCEPT 

Test Procedure follows QSPOO9-O01/O02 NISTifc MO: 259883/253250 39598 OBS04-0268/03-0450 274998 

Rice Lake: 822/266926-02 822/272801-06 822/274081-06 ^ „ / r 

_ ^ p, jOjctftCn . 

- a Or /HAP***** 

CalDate: 11/09/2009 Next Cal due: 90 Days 

Service Technician Registration #: 0524-M 

Calibrated By Service Technician: Jim Koerkenmeier 

Calibration Dates: JAN APR JUL OCT 

Job Queue*: LT217651 Report ID: 68963385 

Uncertainty of Measurement provided on request 

FOR CUSTOMER USE ONLY £ 

Reviewed By Date Reviewed 

This document shal not be reproduced, except in full, without the approval ol Accurate Superior Scale Company.. 

page 1 0f i Form 030, Rev 15,08/19/09 

VES01802 4 
BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 1 OF 2 

OPERATING PARAMETERS PLC COIL BW COIL 

1 OCL TRV POSITION (OPEN) 01602 00401 

2 OCL UPPER CHAMBER TEMP. 1 min avg. 01603 00402 

3 OCL HI BTU Ibs/hr Max 01604 00403 

4 OCL LOWER CHAMBER TEMP. 1 min avg. 01605 00404 

5 OCL LO BTU Ibs/hr Max 01606 00405 

6 OCL FLUE GAS HCL, 1 hr. rolling avg. 01607 00406 

T OCL FLUE GAS CO, 1 hr. rolling avg. 01608 00407 

8 OCL FLUE GAS OPACITY, high for 480 sec/hr. avg. 01609 00408 

9 OCL FLUE GAS OPACITY, high instantaneous 01610 00409 

10 OCL FLUE GAS FLOW RATE, high 1 min. avg 01611 00410 

11 OCL HEAT INPUT high mbtu/hr 01613 00411 

12 OCL CHLORINE INPUT, high Ibs/hr 01614 00412 

13 OCL SOLID FEED, high Ibs/hr Max. 01526 00413 

14 OCL UPPER CHAMBER TEMP, low 1 hr rolling avg. 01538 00414 

15 OCL SPECIALITY FEEDED high Ibs/hr Max. 01516 00415 

17 AWFC SDA OUTLET TEMP, highl min. avg. 01591 00417 

18 AWFC BAG HOUSE DIFF.PR. DROP. Low 1 min. avg. 01593 00418 

19 AWFC FLUE GAS CO, high 1 min. avg. 01594 00419 

20 AWFC FLUE GAS 02, low 1 min. avg. 01596 00420 

21 AWFC FLUE GAS HC, high 1 min. avg. 01597 00421 

22 AWFC FLUE GAS HCL, high 1 min. avg. 01598 00422 

23 AWFC FLUE GAS FLOW RATE, high irist. 01599 00423 

24 AWFC FLUE GAS OPACITY, high 1 min. avg. 01601 00424 

',) AWFC LOW CHAMBER TEMP., low 1 hr. avg. 01586 00425 

_6 AWFC LOWER CHAMBER PRESS, high for 5 sees. 01588 00426 

27 AWFC UPPER CHAMBER PRESS, high for 5 sees. 01589 00427 

28 AWFC FAILER OF PROCESS MONITOR 01527 00428 

29 AWFC ID FAN FAILURE or high high vibration for 5 min. 01625 00429 

30 AWFC Upper or Lower Chamber Temp, high 01600 00430 

32 MWFC ALL WASTE FEED OFF FROM FIX (manually shut off) 01740 00432 

35 MWFC FLUE GAS HCL, high 1 min. avg. 01592 00435 

36 MWFC HEAT INPUT high anticipated 01622 00436 

37 MWFC CHLORINE INPUT, high Ibs/hr 01623 00437 

38 MWFC E-STOPS orT/C MODULE inactive 01615 00438 

39 MWFC FLUE GAS CO, high 1 hr. avg. 01595 00439 

40 MWFC ATOMIZER high high vibration for 5 sec. 01624 00440 

41 SWFC SPEC. FEED Ibs/hr high 01576 00441 

PASS 

y 

~ Z 2 

FAIL 

ZZL 

1ZL 

5 

VES01802 5 
1

 BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task 1C4039) PAGE 2 OF 2 

OPERATING PARAMETERS PLC COIL BW COIL 

42 SWFC HIBTU Ibs/hr high 01578 00442 

43 SWFC LOBTU Ibs/hr high 01580 00443 

45 SWFC HIBTU loss of signal 03019 00445 

46 SWFC LOBTU loss of signal 03020 00446 

47 SWFC SPECIALITY FEED/COMPRESSED GAS FEED loss of signal 03021 00447 

48 MWFC NORTH & SOUTH IPS ALARMS FAILED 05703 00448 

49 SWFC UPPER CHAMBER SECONDARY FUEL loss of signal 03022 00449 

50 MWFC NORTH & SOUTH IPS SERVERSFAILED 05705 00450 

51 SWFC DIRECT INJECT (common alarm) 03132 00451 

52 OPL Bag Leak Detection System (Tribo) 

65 OPL Pumpable 1 Hour Rolling Total OPL 08205 04113 

66 OPL Non-Pumpable 1 Hour Rolling Total OPL 08206 04114 

67 OPL Total waste 1 Hour Rolling Total OPL 08208 04115 

68 OPL CL 12 Hour Rolling Total OPL 08211 04116 

69 OPL Low Volatile 12 Hour Rolling Total OPL 08214 04117 

70 OPL Semi Volatile 12 Hour Rolling Total OPL 08216 04118 

71 OPL Mercury 12 Hour Rolling Total OPL 08218 04119 

72 OPL Ash 12 Hour Rolling Total OPL 08220 04120 

73 OPL PCC Temperature 1 Hour Rolling Average Low OPL 08222 04121 

74 OPL SCC Temperature 1 Hour Rolling Average Low OPL 08224 04122 

75 OPL SDA Outlet Temperature 1 Hour Rolling Average High OPL 08226 04123 

76 OPL Baghouse Differential Pressure 1 Minute Average Low OPL 08227 04124 

77 OPL Baghouse Differential Pressure 1 Minute Average High OPL 08228 04125 

OPL Stack HCL Corrected 1 Hour Rolling Average High OPL 08232 04126 

OPL Stack CO Corrected i Hour Rolling Average High OPL 08236 04127 

80 OPL Stack Flow 1 Hour Rolling Average High OPL 08244 04128 

81 OPL BTU 1 Hour Total OPL 08209 04129 

82 OPL Hrt Cl/Hra Lime Flow 1 Minute Average High OPL 08251 04130 

83 AWFC Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 

84 WILL NOT ACCEPT SOUD CHARGES >750 KBTU/CHARGE 

85 Hi/DI Atomizing Air Low pressure alarm (Manual Check) 

86 Lo/DI Atomizing Air Low pressure alarm (Manual Check) 

87 Specialty Feeder Atomizing Air Low Pressure alarm (Manual check) 

OCL =CONDITION LIMIT 

AWFC =AUTOMATIC WASTE FEED CUTOFF 

MWFC =MISC WASTE FEED CUTOFF 

SWFC =SPECIFlC WASTE FEED CUTOFF 

PASS FAIL 

~7~ 

~ Z 1 

~ZL 

z z 

~ Z 7 

ZZL 

z z 

z 

Comments 

CHECKED BY: DATE:/l%/^O l TIME: /^< T AM<g ^ 

APPROVED: j/t%&L-/J*. /<^'M' PLACE: Control Room 

,EEKLY_2 

4/4/07 HK 

VES01802 6 
J

 BIWEEKLY UNIT #2 

COMPLIANCE CHfCK SHEET 

(CMS Task IC4039) PAGE 1 OF 2 

OPERATING PARAMETERS PLC COIL BW COIL 

1 OCL TRV POSITION (OPEN) 01602 00401 

2 OCL UPPER CHAMBER TEMP. 1 min avg. 01603 00402 

3 OCL HI BTU Ibs/hr Max 01604 00403 

4 OCL LOWER CHAMBER TEMP. 1 min avg. 01605 00404 

5 OCL LOBTU Ibs/hr Max 01606 00405 

6 OCL . FLUE GAS HCL, 1 hr. rolling avg. 01607 00406 

7 OCL FLUE GAS CO, 1 hr. rolling avg. 01608 00407 

8 OCL FLUE GAS OPACITY, high for 480 sec/hr. avg. 01609 00408 

9 OCL FLUE GAS OPACITY, high instantaneous 01610 00409 

10 OCL FLUE GAS FLOW RATE, high 1 min. avg 01611 00410 

11 OCL HEAT INPUT high mbtu/hr 01613 00411 

12 OCL CHLORINE INPUT, high Ibs/hr 01614 00412 

13 OCL SOLID FEED, high Ibs/hr Max. 01526 00413 

14 OCL UPPER CHAMBER TEMP, low 1 hr rolling avg. 01538 00414 

15 OCL SPECIALITY FEEDED high Ibs/hr Max. 01516 00415 

17 AWFC SDA OUTLET TEMP, highl min. avg. 01591 00417 

18 AWFC BAG HOUSE DIFF.PR. DROP. Low 1 min. avg. 01593 00418 

19 AWFC FLUE GAS CO, high 1 min. avg. 01594 00419 

20 AWFC FLUE GAS 02, low 1 min. avg. 01596 00420 

21 AWFC FLUE GAS HC, high 1 min. avg. 01597 . 00421 

22 AWFC FLUE GAS HCL, high 1 min. avg. 01598 00422 

23 AWFC FLUE GAS FLOW RATE, high irtst. 01599 00423 

24 AWFC FLUE GAS OPACITY, high 1 min. avg. 01601 00424 

/5 AWFC LOW CHAMBER TEMP., low 1 hr. avg. 01586 00425 

16 AWFC LOWER CHAMBER PRESS, high for 5 sees. 01588 00426 

27 AWFC UPPER CHAMBER PRESS, high for 5 sees. 01589 00427 

28 AWFC FAILER OF PROCESS MONITOR 01527 00428 

29 AWFC ID FAN FAILURE or high high vibration for 5 min. 01625 00429 

30 AWFC Upper or Lower Chamber Temp, high 01600 00430 

32 MWFC ALL WASTE FEED OFF FROM FIX (manually shut off) 01740 00432 

35 MWFC FLUE GAS HCL, high 1 min. avg. 01592 00435 

36 MWFC HEAT INPUT high anticipated 01622 00436 

37 MWFC CHLORINE INPUT, high Ibs/hr 01623 00437 

38 MWFC E-STOPS orT/C MODULE inactive 01615 00438 

39 MWFC FLUE GAS CO, high 1 hr. avg. 01595 00439 

40 MWFC ATOMIZER high high vibration for 5 sec. 01624 00440 

41 SWFC SPEC. FEED Ibs/hr high 01576 00441 

PASS 

/ 

z z : 

/ 

Z7Z 

~ r 

z z . 

J 

T 

/ 

FAIL 

VES01802 7 
" BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 2 OF 2 

OPERATING PARAMETERS PLC COIL BW COIL PASS 

/ 

42 SWFC HIBTU Ibs/hr high 01578 00442 

43 SWFC LOBTU Ibs/hr high 01580 00443 J. 

45 SWFC HIBTU loss of signal 03019 00445 J 

46 SWFC LOBTU loss of signal 03020 00446 

47 SWFC SPECIALITY FEED/COMPRESSED GAS FEED loss of signal 03021 00447 :/, 

48 MWFC NORTH & SOUTH IPS ALARMS FAILED 05703 00448 h 

49 SWFC UPPER CHAMBER SECONDARY FUEL loss of signal 03022 00449 J 

50 MWFC NORTH & SOUTH IPS SERVERSFAILED 05705 00450 J 

51 SWFC DIRECT INJECT (common alarm) 03132 00451 J 

52 OPL Bag Leak Detection System (Tribo) / 65 OPL Pumpable 1 Hour Rolling Total OPL 08205 04113 / 66 OPL Non-Pumpable 1 Hour Rolling Total OPL 08206 04114 j 

67 OPL Total waste 1 Hour Rolling Total OPL 08208 04115 / 

68 OPL CL 12 Hour Rolling Total OPL 08211 04116 

69 OPL Low Volatile 12 Hour Rolling Total OPL 08214 04117 

70 OPL Semi Volatile 12 Hour Rolling Total OPL 08216 04118 

-

J

r -

71 OPL Mercury 12 Hour Rolling Total OPL 08218 04119 

-

J

r -

72 OPL Ash 12 Hour Rolling Total OPL 08220 04120 

73 OPL PCC Temperature 1 Hour Rolling Average Low OPL 08222 04121 — f -

74 OPL SCC Temperature 1 Hour Rolling Average Low OPL 08224 04122 /' 75 OPL SDA Outlet Temperature 1 Hour Rolling Average High OPL 08226 04123 

76 OP - 7 - L Baghouse Differential Pressure 1 Minute Average Low OPL 08227 04124 - 7 -

77 OPL Baghouse Differential Pressure 1 Minute Average High OPL 08228 04125 / 

OPL Stack HCL Corrected 1 Hour Rolling Average High OPL 08232 04126 

) OPL Stack CO Corrected 1 Hour Rolling Average High OPL 08236 04127 v/ 

80 OPL Stack Flow 1 Hour Rolling Average High OPL 08244 04128 / 81 OPL BTU 1 Hour Total OPL 08209 04129 y. 

82 OPL Hit Cl/Hra Lime Flow 1 Minute Average High OPL 08251 04130 y 

83 AWFC Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 / 

84 WILL NOT ACCEPT SOLID CHARGES >750 KBTU/CHARGE 

./ 

85 Hi/DI Atomizing Air Low pressure alarm (Manual Check) y. 

86 Lo/DI Atomizing Air Low pressure alarm (Manual Check) / 

87 Specialty Feeder Atomizing Air Low Pressure alarm (Manual check) / 

OCL CONDITION LIMIT 

AWFC =AUTOMATIC WASTE FEED CUTOFF 

MWFC =MISC WASTE FEED CUTOFF 

SWFC =SPECIFIC WASTE FEED CUTOFF 

Comments 

CHECKED BY: A.& ^ IM DATE: /& - /Q -6 f TIME: / 0 J & AM (ti p 

APPROVED: PLACE: Control Room 

,EEKLY_2 

4/4/07 HK 

VES01802 8 
• BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 1 OF 2 

OPERATING PARAMETERS PLC COIL BWCOIL PASS FAIL 

1 OCL TRV POSITION (OPEN) 01602 00401 

2 OCL UPPER CHAMBER TEMP. 1 min avg. 01603 00402 

3 OCL HIBTU Ibs/hr Max 01604 00403 

4 OCL LOWER CHAMBER TEMP. 1 min avg. 01605 00404 

5 OCL LO BTU lbs/hr Max 01606 00405 

6 OCL FLUE GAS HCL, 1 hr. rolling avg. 01607 00406 

7 OCL FLUE GAS CO, 1 hr. rolling avg. 01608 00407 

8 OCL FLUE GAS OPACITY, high for 480 sec/hr. avg. 01609 00408 

9 OCL FLUE GAS OPACITY, high instantaneous 01610 00409 

10 OCL FLUE GAS FLOW RATE, high 1 min. avg 01611 00410 

11 OCL HEAT INPUT high mbtu/hr 01613 00411 

12 OCL CHLORINE INPUT, high Ibs/hr 01614 00412 

13 OCL SOLID FEED, high Ibs/hr Max. 01526 00413 

14 OCL UPPER CHAMBER TEMP, low 1 hr rolling avg. 01538 00414 

15 OCL SPECIALITY FEEDED high Ibs/hr Max. 01516 00415 

17 AWFC SDA OUTLET TEMP, highl min. avg. 01591 00417 

18 AWFC BAG HOUSE DIFF.PR. DROP. Low 1 min. avg. 01593 00418 

19 AWFC FLUE GAS CO, high 1 min. avg. 01594 00419 

20 AWFC FLUE GAS 02, low 1 min. avg. 01596 00420 

21 AWFC FLUE GAS HC, high 1 min. avg. 01597 00421 

22 AWFC FLUE GAS HCL, high 1 min. avg. 01598 00422 

23 AWFC FLUE GAS FLOW RATE, high inst. 01599 00423 

24 AWFC FLUE GAS OPACITY, high 1 min. avg. 01601 00424 

;5 AWFC LOW CHAMBER TEMP., low 1 hr. avg. 01586 00425 

z6 AWFC LOWER CHAMBER PRESS, high for 5 sees. 01588 00426 

27 AWFC UPPER CHAMBER PRESS, high for 5 sees. 01589 00427 

28 AWFC FAILER OF PROCESS MONITOR 01527 00428 

29 AWFC ID FAN FAILURE or high high vibration for 5 min. 01625 00429 

30 AWFC Upper or Lower Chamber Temp, high 01600 00430 

32 MWFC ALL WASTE FEED OFF FROM FIX (manually shut off) 01740 00432 

35 MWFC FLUE GAS HCL, high 1 min. avg. 01592 00435 

36 MWFC HEAT INPUT high anticipated 01622 00436 

37 MWFC CHLORINE INPUT, high Ibs/hr 01623 00437 

38 MWFC E-STOPS orT/C MODULE inactive 01615 00438 

39 MWFC FLUE GAS CO, high 1 hr. avg. 01595 00439 

40 MWFC ATOMIZER high high vibration for 5 sec. 01624 00440 

41 SWFC SPEC. FEED Ibs/hr high 01576 00441 

5 

1ZL 

5 

z 

z 

± 

z : 

z 

2 " 

^ 1 

VES01802 9 
BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 2 OF 2 

OPERATING PARAMETERS PLC COIL BW COIL PASS 

42 SWFC HIBTU Ibs/hr high 01578 00442 

43 SWFC LOBTU Ibs/hr high 01580 00443 y 

45 SWFC HIBTU loss of signal 03019 00445 <> 46 SWFC LOBTU loss of signal 03020 00446 y 

47 SWFC SPECIALITY FEED/COMPRESSED GAS FEED loss of signal 03021 00447 

48 MWFC NORTH & SOUTH IPS ALARMS FAILED 05703 00448 y 

49 SWFC UPPER CHAMBER SECONDARY FUEL loss of signal 03022 00449 

50 MWFC NORTH & SOUTH IPS SERVERSFAILED 05705 00450 y 

51 SWFC DIRECT INJECT (common alarm) 03132 00451 y 

52 OPL Bag Leak Detection System (Tribo) y 

65 OPL Pumpable 1 Hour Rolling Total OPL 08205 04113 y 

66 OPL Non-Pumpable 1 Hour Rolling Total OPL 08206 04114 y 

67 OPL Total waste 1 Hour Rolling Total OPL 08208 04115 y 

68 OPL CL 12 Hour Rolling Total OPL 08211 04116 

69 OPL Low Volatile 12 Hour Rolling Total OPL 08214 04117 y 

70 OPL Semi Volatile 12 Hour Roiling Total OPL 08216 04118 \y^<-

71 OPL Mercury 12 Hour Rolling Total OPL 08218 04119 

72 OPL Ash 12 Hour Rolling Total OPL 08220 04120 y 

73 OPL PCC Temperature 1 Hour Rolling Average Low OPL 08222 04121 y 

74 OPL SCC Temperature 1 Hour Rolling Average Low OPL 08224 04122 y 

75 OPL SDA Outlet Temperature 1 Hour Rolling Average High OPL 08226 04123 

76 OPL Baghouse Differential Pressure 1 Minute Average Low OPL 08227 04124 y 

77 OPL Baghouse Differential Pressure 1 Minute Average High OPL 08228 04125 

OPL Stack HCL Corrected 1 Hour Rolling Average High OPL 08232 04126 y 

t» OPL Stack CO Corrected 1 Hour Rolling Average High OPL 08236 04127 y 

80 OPL Stack Flow 1 Hour Rolling Average High OPL 08244 04128 y 

81 OPL BTU 1 Hour Total OPL 08209 04129 

82 OPL Hrt CI/Hra Lime Flow 1 Minute Average High OPL 08251 04130 y 

83 AWFC Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 y 

84 WILL NOT ACCEPT SOLID CHARGES >750 KBTU/CHARGE s 

85 Hi/DI Atomizing Air Low pressure alarm (Manual Check) 

86 Lo/DI Atomizing Air Low pressure alarm (Manual Check) y 

87 Specialty Feeder Atomizing Air Low Pressure alarm (Manual check) y 

OCL CONDITION LIMIT 

AWFC =AUTOMATIC WASTE FEED CUTOFF 

MWFC =MISC WASTE FEED CUTOFF 

SWFC =SPECIFIC WASTE FEED CUTOFF 

Comments 

CHECKED BY: ^^TT^^ ^ DATE ://-//-£ ) TIME: (am)pM 

A

n

°ROVED: ^//(Z^/^jc^ Jj' ^ PLACE: Control Room 

L-..vT£EKLY_2 

4/4/07 HK 

VES01803 0 
BIWEEKLY UNIT#2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 1 OF 2 

OPERATING PARAMETERS 

1 OCL TRV POSITION (OPEN) 

2 OCL UPPER CHAMBER TEMP. 1 min avg. 

3 OCL HI BTU lbs/hr Max 

4 OCL LOWER CHAMBER TEMP. 1 min avg. 

5 OCL LOBTU Ibs/hr Max 

6 OCL FLUE GAS HCL, 1 hr. rolling avg. 

7 OCL FLUE GAS CO, 1 hr. rolling avg. 

8 OCL FLUE GAS OPACITY, high for 480 sec/hr. avg. 

9 OCL FLUE GAS OPACITY, high instantaneous 

10 OCL FLUE GAS FLOW RATE, high 1 min. avg 

11 OCL HEAT INPUT high mbtu/hr 

12 OCL CHLORINE INPUT, high Ibs/hr 

13 OCL SOLID FEED, high Ibs/hr Max. 

14 OCL UPPER CHAMBER TEMP, low 1 hr rolling avg. 

15 OCL SPECIALITY FEEDED high Ibs/hr Max. 

17 AWFC SDA OUTLET TEMP, highl min. avg. 

18 AWFC BAG HOUSE DIFF.PR. DROP. Low 1 min. avg. 

19 AWFC FLUE GAS CO, high 1 min. avg. 

20 AWFC FLUE GAS 02, low 1 min. avg. 

21 AWFC FLUE GAS HC, high 1 min. avg. 

22 AWFC FLUE GAS HCL, high 1 min. avg. 

23 AWFC FLUE GAS FLOW RATE, high inst. 

24 AWFC FLUE GAS OPACITY, high 1 min. avg. 

'5 AWFC LOW CHAMBER TEMP., low 1 hr. avg. 

Js AWFC LOWER CHAMBER PRESS, high for 5 sees. 

27 AWFC UPPER CHAMBER PRESS, high for 5 sees. 

28 AWFC FAILER OF PROCESS MONITOR 

29 AWFC ID FAN FAILURE or high high vibration for 5 min. 

30 AWFC Upper or Lower Chamber Temp, high 

32 MWFC ALL WASTE FEED OFF FROM FIX (manually shut off) 

35 MWFC FLUE GAS HCL, high 1 min. avg. 

36 MWFC HEAT INPUT high anticipated 

37 MWFC CHLORINE INPUT, high Ibs/hr 

38 MWFC E-STOPS or T/C MODULE inactive 

39 MWFC FLUE GAS CO, high 1 hr. avg. 

40 MWFC ATOMIZER high high vibration for 5 sec. 

41 SWFC SPEC. FEED Ibs/hr high 

PLC COIL BWCOIL PASS FAIL 

01602 00401 / 

01603 00402 

01604 00403 - y 

01605 00404 

01606 00405 

01607 00406 

01608 00407 

01609 00408 s/ 

01610 00409 

01611 00410

 s 

y 

01613 00411 v / 

01614 00412 y 

01526 00413 

01538 00414 

01516 00415 y 

01591 00417 y 

01593 00418 y 

01594 00419 y 

01596 00420 y 

01597 00421 y 

01598 00422 y 01599 00423 

01601 00424 y 01586 00425 y 

01588 00426 y 

01589 00427 y 

01527 00428 

01625 00429 

01600 00430 y 

01740 00432 y 

01592 00435 y 01622 00436 y 

01623 00437 y 

01615 00438 y 

01595 00439 y 

01624 00440 y 

01576 00441 V 

VES01803 1 
BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 2 OF 2 

OPERATING PARAMETERS PLC COIL BWCOIL PASS FAIL 

42 SWFC HIBTU Ibs/hr high 01578 00442 

43 SWFC LOBTU Ibs/hr high 01580 00443 

45 SWFC HIBTU loss of signal 03019 00445 

46 SWFC LOBTU loss of signal 03020 00446 

47 SWFC SPECIALITY FEED/COMPRESSED GAS FEED loss of signal 03021 00447 

48 MWFC NORTH & SOUTH IPS ALARMS FAILED 05703 00448 

49 SWFC UPPER CHAMBER SECONDARY FUEL loss of signal 03022 00449 

50 MWFC NORTH & SOUTH IPS SERVERSFAILED 05705 00450 

51 SWFC DIRECT INJECT (common alarm) 03132 00451 

52 OPL Bag Leak Detection System (Tribo) 

65 OPL Pumpable 1 Hour Rolling Total OPL 08205 04113 

66 OPL Non-Pumpabte 1 Hour Rolling Total OPL 08206 04114 

67 OPL Total waste 1 Hour Rolling Total OPL 08208 04115 

68 OPL CL 12 Hour Rolling Total OPL 08211 04116 

69 OPL Low Volatile 12 Hour Rolling Total OPL 08214 04117 

70 OPL Semi Volatile 12 Hour Rolling Total OPL 08216 04118 

71 OPL Mercury 12 Hour Rolling Total OPL 08218 04119 

72 OPL Ash 12 Hour Rolling Total OPL 08220 04120 

73 OPL PCC Temperature 1 Hour Rolling Average Low OPL 08222 04121 

74 OPL SCC Temperature 1 Hour Rolling Average Low OPL 08224 04122 

75 OPL SDA Outlet Temperature 1 Hour Rolling Average High OPL 08226 04123 

76 OPL Baghouse Differential Pressure 1 Minute Average Low OPL 08227 04124 

77 OPL Baghouse Differential Pressure 1 Minute Average High OPL 08228 04125 

OPL Stack HCL Corrected 1 Hour Rolling Average High OPL 08232 04126 

OPL Stack CO Corrected 1 Hour Rolling Average High OPL 08236 04127 

80 OPL Stack Flow 1 Hour Rolling Average High OPL 08244 04128 

81 OPL BTU 1 Hour Total OPL 08209 04129 

82 OPL Hrt Cl/Hra Lime Flow 1 Minute Average High OPL 08251 04130 

83 AWFC Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 

84 WILL NOT ACCEPT SOLID CHARGES >750 KBTU/CHARGE 

85 Hi/DI Atomizing Air Low pressure alarm (Manual Check) 

86 Lo/DI Atomizing Air Low pressure alarm (Manual Check) 

87 Specialty Feeder Atomizing Air Low Pressure alarm (Manual check) 

OCL =CONDITION LIMIT 

AWFC =AUTOMATIC WASTE FEED CUTOFF 

MWFC =MISC WASTE FEED CUTOFF 

SWFC =SPECIFIC WASTE FEED CUTOFF 

./ 

_ z z 

_^X _ 

- X 

1 

_ x _ 

:£ 

i 

Comments 

CHECKED BY: J-S^- . 1 .^A-M ? 0ATE jD~Z<Z-d1 TIME: j^g> M 

APPROVED: /^^^Z-/^ ^ /^V W PLACE: Control Room 

L, ., cEKLY_2 

4/4/07 HK 

VES01803 2 
BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 1 OF 2 

OPERATING PARAMETERS PLC COIL BWCOIL 

1 OCL TRV POSITION (OPEN) 01602 00401 

2 OCL UPPER CHAMBER TEMP. 1 min avg. 01603 00402 

3 OCL HI BTU Ibs/hr Max 01604 00403 

4 OCL LOWER CHAMBER TEMP. 1 min avg. 01605 00404 

5 OCL LO BTU lbs/hr Max 01606 00405 

6 OCL FLUE GAS HCL, 1 hr. rolling avg. 01607 00406 

7 OCL FLUE GAS CO, 1 hr. rolling avg. 01608 00407 

8 OCL FLUE GAS OPACITY, high for 480 sec/hr. avg. 01609 00408 

9 OCL FLUE GAS OPACITY, high instantaneous 01610 00409 

10 OCL FLUE GAS FLOW RATE, high 1 min. avg 01611 00410 

11 OCL HEAT INPUT high mbtu/hr 01613 00411 

12 OCL CHLORINE INPUT, high Ibs/hr 01614 00412 

13 OCL SOLID FEED, high Ibs/hr Max. 01526 00413 

14 OCL UPPER CHAMBER TEMP, low 1 hr rolling avg. 01538 00414 

15 OCL SPECIALITY FEEDED high Ibs/hr Max. 01516 00415 

17 AWFC SDA OUTLET TEMP, highl min. avg. 01591 00417 

18 AWFC BAG HOUSE DIFF.PR. DROP. Low 1 min. avg. 01593 00418 

19 AWFC FLUE GAS CO, high 1 min. avg. 01594 00419 

20 AWFC FLUE GAS 02, low 1 min. avg. 01596 00420 

21 AWFC FLUE GAS HC, high 1 min. avg. 01597 00421 

22 AWFC FLUE GAS HCU high 1 min. avg. 01598 00422 

23 AWFC FLUE GAS FLOW RATE, high iiist. 01599 00423 

24 AWFC FLUE GAS OPACITY, high 1 min. avg. 01601 00424 

'•>5 AWFC LOW CHAMBER TEMP., low 1 hr. avg. 01586 00425 

26 AWFC LOWER CHAMBER PRESS, high for 5 sees. 01588 00426 

27 AWFC UPPER CHAMBER PRESS, high for 5 sees. 01589 00427 

28 AWFC FAILER OF PROCESS MONITOR 01527 00428 

29 AWFC ID FAN FAILURE or high high vibration for 5 min. 01625 00429 

30 AWFC Upper or Lower Chamber Temp, high 01600 00430 

32 MWFC ALL WASTE FEED OFF FROM FIX (manually shut off) 01740 00432 

35 MWFC FLUE GAS HCL, high 1 min. avg. 01592 00435 

36 MWFC HEAT INPUT high anticipated 01622 00436 

37 MWFC CHLORINE INPUT, high Ibs/hr 01623 00437 

38 MWFC E-STOPS orT/C MODULE inactive 01615 00438 

39 MWFC FLUE GAS CO, high 1 hr. avg. 01595 00439 

40 MWFC ATOMIZER high high vibration for 5 sec. 01624 00440 

41 SWFC SPEC. FEED Ibs/hr high 01576 00441 

PASS 

ZZLZ 

I 

r z : 

zlz i 

FAIL 

VES01803 3 
BIWEEKLY UNIT #2 

COMPLIANCE CHECK SHEET 

(CMS Task IC4039) PAGE 2 OF 2 

OPERATING PARAMETERS PLC COIL BWCOIL PASS 

42 SWFC HIBTU Ibs/hr high 01578 00442 / 

43 SWFC LOBTU Ibs/hr high 01580 00443 y 

45 SWFC HIBTU loss of signal 03019 00445 y 

46 SWFC LOBTU loss of signal 03020 00446 y 

47 SWFC SPECIALITY FEED/COMPRESSED GAS FEED loss of signal 03021 00447 y 

48 MWFC NORTH & SOUTH IPS ALARMS FAILED 05703 00448 y 49 SWFC UPPER CHAMBER SECONDARY FUEL ioss of signal 03022 00449 y 

50 MWFC NORTH & SOUTH IPS SERVERSFAILED 05705 00450 y 

51 SWFC DIRECT INJECT (common alann) 03132 00451 y 

52 OPL Bag Leak Detection System (Tribo) y 

65 OPL Pumpable 1 Hour Rolling Total OPL 08205 04113 y 

66 OPL Non-Pumpable 1 Hour Rolling Total OPL 08206 04114 y 

67 OPL Total waste 1 Hour Rolling Total OPL 08208 04115 y 

68 OPL CL 12 Hour Rolling Total OPL 08211 04116 

69 OPL Low Volatile 12 Hour Rolling Total OPL 08214 04117 <y 

70 OPL Semi Volatile 12 Hour Rolling Total OPL 08216 04118 y 

71 OPL Mercury 12 Hour Rolling Total OPL 08218 04119 y 

72 OPL Ash 12 Hour Rolling Total OPL 08220 04120 

73 OPL PCC Temperature 1 Hour Rolling Average Low OPL 08222 04121 y\ 

74 OPL SCC Temperature 1 Hour Rolling Average Low OPL 08224 04122 y 

y 

75 OPL SDA Outlet Temperature 1 Hour Rolling Average High OPL 08226 04123 

y 

y 76 OPL Baghouse Differential Pressure 1 Minute Average Low OPL 08227 04124 

77 OPL Baghouse Differential Pressure 1 Minute Average High OPL 08228 04125 

/8 OPL Stack HCL Corrected 1 Hour Rolling Average High OPL 08232 04126 y 79 OPL Stack CO Corrected 1 Hour Rolling Average High OPL 08236 04127 

80 OPL Stack - y Flow 1 Hour Rolling Average High OPL 08244 04128 

- y 

81 OPL BTU 1 Hour Total OPL 08209 04129 y. 

82 OPL Hrt Cl/Hra Lime Flow 1 Minute Average High OPL 08251 04130 y 

83 AWFC Lime Slurry Density 1 Hour Rolling Average Low 08156 04132 y 

84 WILL NOT ACCEPT SOLID CHARGES >750 KBTU/CHARGE y 

85 Hi/DI Atomizing Air Low pressure alarm (Manual Check) y 

86 Lo/DI Atomizing Air Low pressure alarm (Manual Check) 

87 Specialty Feeder Atomizing Air Low Pressure alarm (Manual check) y 

OCL =CONDITION LIMIT 

AWFC =AUTOMATIC WASTE FEED CUTOFF 

MWFC =MISC WASTE FEED CUTOFF 

SWFC =SPECIFIC WASTE FEED CUTOFF 

Comments 

DATE: PM 

PLACE: Control Room 

CHECKED BY: A^-T T A „ ^1/ 

"PROVED: ^/<SL& L/^ c /<ft'i^ 

t$IWEEKLY_2 

4/4/07 HK 

VES01803 4 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit#

 2 Serial # 

Parameter NIST Traceable Calibration Standards 

> 0 2 25 % G a s Concentration 

r CO-lo w range 200pp m Low (Zero) 0 + 0.5 

r CO-high range 3000ppm Mid 8.93 ± 0.5 

r HCI 1000pp m High 15 ± 0.5 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0 0 — — 

2-Mid 8.93 9.1 — -0.17 — 

3-High . 15 15.1 — • — -0.1 

4-Low 0 0 0 — — 

5-Mid 8.93 9 — -0.07 — 

6-High 15 15.3 — — -0.3 

7-I nw n n n 

8-Mid 8.93 9.1 — -0.17 — 

9-High 15 • 15.2 — — -0.2 

Mean Difference = 0.00 -0.14 -0.20 

Calibration Error = 0.00% -0.55% -0.80% 

Calibration Error = = Mean Difference / Span Value * 100 

Brian Bunfill E/J Tech 

Name Title 

9/25/2009 

Signature 

2/4/2010 

Date 

VES01803 5 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit# Serial # 346 

Parameter 

r 0 2 25 % 

'<* CO-lo w range 200pp m 

r CO-high range 3000ppm 

r HCI 1000pp m 

Parameter NIST Traceable Calibration Standards 

r 0 2 25 % 

'<* CO-lo w range 200pp m 

r CO-high range 3000ppm 

r HCI 1000pp m 

G a s Concentration 

Parameter 

r 0 2 25 % 

'<* CO-lo w range 200pp m 

r CO-high range 3000ppm 

r HCI 1000pp m 

Low (Zero) 0 ± 10 

Parameter 

r 0 2 25 % 

'<* CO-lo w range 200pp m 

r CO-high range 3000ppm 

r HCI 1000pp m 

Mid 68.9 ± 10 

Parameter 

r 0 2 25 % 

'<* CO-lo w range 200pp m 

r CO-high range 3000ppm 

r HCI 1000pp m High 153 ± 10 • 

Calibration Error = Mean Difference / Span Value * 100 

Brian Bunfill E/l Tech 

Name 

Signature 

Title 

9/25/2009 

2/4/2010 

Date 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0.1 -0.1 — — 

2-Mid 68.9 71.7 — -2.8 — 

3-High 153 152.7 — — 0.3 

4-Low 0 0.4 -0.4 — — 

5-Mid 68.9 71.9 — -3 — 

6-High 153 152.8 — — 0.2 

0 0.6 ,0.6 — — « 

8-Mid 68.9 71,6 — -2.7 — 

9-High 153 152.6 . — — 0.4 

Mean Difference = -0.37 -2.83 0.30 

Calibration Error = -0.18% -1.42% 0.15% 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit# Serial # 346 

Parameter 

r 0 2 25 % 

f"' CO-low range 200pp m 

CO-high range 3000ppm 

r HCI 1000pp m 

Parameter NIST Traceable Calibration Standards 

r 0 2 25 % 

f"' CO-low range 200pp m 

CO-high range 3000ppm 

r HCI 1000pp m 

G a s Concentration 

Parameter 

r 0 2 25 % 

f"' CO-low range 200pp m 

CO-high range 3000ppm 

r HCI 1000pp m 

Low (Zero) 0 ± 150 

Parameter 

r 0 2 25 % 

f"' CO-low range 200pp m 

CO-high range 3000ppm 

r HCI 1000pp m 

Mid 1079.1 ± 150 

Parameter 

r 0 2 25 % 

f"' CO-low range 200pp m 

CO-high range 3000ppm 

r HCI 1000pp m High 2220 + 150 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0.1 -0.1 — — 

2-Mid 1079.1 1151.9 — -72.8 — 

3-High 2220 2217.4 — — 2.6 

4-Low 0 0.4 -0.4 . — — 

5-Mid 1079.1 1095.3 — -16.2 — 

6-High 2220 2182.5 — — 37.5. 

7-Low . _ 0 —0J 3 . _,0.6... — r— 

8-Mid 1079.1 10912 — -12.1 — 

9-High 2220 2178.4 — — 41.6 

Mean Difference = -0.37 -33.70 27.23 

Calibration Error = -0.01% -1.12% 0.91% 

Calibration Error = Mean Difference / Span Value * 100 

Brian Bunfill E/ITech 

Name 

U S 

Signature 

Title 

9/25/2009 

2/4/2010 

Date 
ABSOLUTE CALIBRATION AUDIT (ACA) DATA SHEET 

Unit#

 2 Serial # 

Parameter NIST Traceable Calibration Standards 

r 0 2 25 % G a s Concentration 

r CO-lo w range 200ppm Low (Zero) 0 + 50 

r CO-high range 3000ppm Mid 318 + 50 

HCI 1000pp m High 743 ± 50 

Run Number Concentration Difference 

Reference Analyzer Low Mid High 

1-Low 0 0 0 — — 

2-Mid 318 276.5 — 41.5 — 

3-High .743 741.1 • — — 1.9 

4-Low 0 0 0 — — 

5-Mid 318 312.4 — 5.6 — 

6-High 743 738.1 — — 4.9 

7-Low 0 0 . . . . 0 — .... ... 

8-Mid 318 323.1 — -5.1 — 

9-High 743 739 — — 4 

Mean Difference = 0.00 14.00 3.60 

Calibration Error = 0.00% 1.40% 0.36% 

Calibration Error = Mean Difference / Span Value * 100 

Brian Bunfill 

Name 

Signature 

VES01803 8 

E/l Tech 

Title 

9/26/2009 

Date 

2/4/2010 
Table 1 

Summary of Relative Accuracy Test Audit Results 

Veolia ES Technical Solutions 

Sauget, Illinois 

June 22,23 and 24,2009 

CEM S Parameter Units Measured R A Criteria Pass/Fail 

Unit 2 CO ppm @ 7% 0 2 0.004 ppma Uni Pass t 2 

0 2 , dry % o 2 0.09%a 1.0

 a 'c Pass 

Unit 2 

Oi, wet % o 2 0.13%a 1.0

 a 'c Pass 

Unit 3 CO ppm @ 7% 0 2 0.063 ppma 

5a.b Uni Pass t 3 

0 2 , dry % o 2 0.02%a 1.0

 a

-

c Pass 

Unit 3 

Oi, wet % o 2 0.31%a 1.0

 a 'c Pass 

Unit 4 CO ppm @ 7% 0 2 1.146 ppm1 5a.b Uni Pass t 4 

Oz , dry % 0 2 0.15%a 1.0

 a 'c Pass 

Unit 4 

02 , wet % o 2 > 0.46%a 1.0

 a 'c Pass 

a

 Percent of emission standard or absolute average difference (ppm or %). 

b PS4B . 

c

 PS 3. 

/ 

JULY 7, 2009 

CEC Project 090-861 

INCINERATOR CEMS RATA 

VEOLIA ES 

VES01803 9 
Incinerator 

Data Point 

"Veolia 

Environmental Services 

Sauget Illinois 

Created 

Period Start 

Period En 

1/1/2010 6:00 AM 

1/1/2010 6:00 AM 

1/1/2010 6:00 AM 

Page 1 of7 

IMin 

AVG 

Warn 

1 Min 

AVG 

Shut 

IMin 1 Hr Roll 1 Hr Roll 1 Hr Roll I Hr Roll 1 Hr Roll 1 Hr Roll 12 Hr 12 Hr 12 Hr lHrTot lHrTot lHrTot 

AVG Warn Shut OPL Tot Tot Shut Tot OPL Roll Tot Roll Tot Roll Tot Warn Shut OPL 

OPL Warn Warn Shut OPL 

Thermodynamic BTU 

HCLtoLime 

Stack CO Corrected 

LimeSlurryDensity 

Stack HCL Corrected 

Stack HCL RCRA 

Stack 02 Corrected 

Stack 02 Raw 

Stack Opacity 

Stack Flow 

SDA Outlet Temp 

Baghouse Diff Press Low 

Baghouse Diff Press High 9.000000 10.00000 

25.00000 28.00000 33.50000 

450.0000 500.0000 

67.50000 0.000000 

450.0000 500.0000 

450.0000 500.0000 

4.000000 

4.000000 3.000000 

8.000000 10.00000 

15000.00 . . 

430.0000 500.0000 

3.000000 2.000000 

30.00000 75.00000 100.0000 

67.50000 67.30000 67.00000 

25.00000 32.00000 

20.00000 25.00000 100.0000 

14600.00 14950.00 15147.00 

417.0000 418.0000 420.0000 

15.00000 15.50000 16.00000 

VES01804 0 
Stack THC 

Low BTU Weight 

Special Feed Weight 

High BTU Weight 

Solids Weight 

PCC Temp 

SCC Temp 

Stack CO RCRA 

Liquid Weight 

Weight 

Chlonne 

Mercury 

Ash 

Low Volatile 

Semi Volatile 

8.000000 10.00000 

1750.000 1590.000 

1860.000 1794.000 

450.0000 500.0000 

Veolia 

Environmental Services 

Sauget Illinois 

1000.000 1020.000 1053.000 

1775.000 1742.000 1734.000 

1880.000 1854.000 1849.000 

50.00000 90.00000 100.0000 

2850.000 2950.000 3107.000 

3750.000 3850.000 4017.000 

200.0000 218.0000 

0.003000 0.003400 

625.0000 673.0000 

Created 

Period Start 

Period En 

1/1/2010 6:00 AM 

1/1/2010 6:00 AM 

1/1/2010 6:00 AM 

Page 2 of7 

. 1900.000 1933.000 1993.000 

. 600.0000 664.0000 724.0000 

. 1900.000 1952.000 2012.000 

. 1000.000 1020.000 1053.000 

40.00000 46.00000 

56.00000 63.00000 

. 2400.000 2500.000 2616.000 200.0000 217.0000 233.0000 

. 0.030000 0.034000 0.040800 

. 7500.000 8000.000 8076.000 

. 500.0000 530.0000 552.0000 

. 700.0000 730.0000 756.0000 

VES01804 1 
Facility Oxygen Data 

VES01804 2 
December, 2009 Average Oxyge n Concentrations for Units 2, 3, and 4 

Unit 2 Method 5/26 Method 0023A 

Date Wet 02 Dry 02 Wet 02 Dry 02 

(%) {%) (%) (%) 

12/8/2009 5.6 10.3 4.8 9.1 

12/9/2009 5.8 10.4 5.1 9.3 

12/10/2009 5.1 9.3 4.3 8.2 

Unit 3 Method 5/26 Method 0023A 

Date Wet 02 Dry 02 Wet 02 Dry 02 

(%) (%) (%) (%) 

12/1/2009 5.7 9.5 4.0 7.3 

12/2/2009 4.5 7.8 4.1 7.3 

12/3/2009 6.2 10.4 5.6 9.5 

Unit 4 Method 5/26 Method 0023A 

Date Wet 02 Dry 02 Wet 02 Dry 02 

(%) (%) (%) (%) 

12/16/2009 8.6 12.7 7.7 12.6 

12/17/2009 7.9 12.5 8.0 12.4 

12/18/2009 7.3 12.6 6.9 12.3 
CD 

VES01804 4 
AECOM 

Appendix B 

Reference Method Field Data and Calculations 

VES01804 5 
Metho d 5/26 A 

VES01804 6 
Particulate Results Summary 

Unit 2 

Veolia ES Technical Solutions 

Sauget, IL 

Test Results: Run 1 Run 2 Run 3 Average 

Particulate Emission Concentration: 

grains/dscf 0.00096 0.00130 0.00067 0.00098 

grains/dscf@7% 02 0.00126 0.00172 0.00080 0.00126 

Where: 

Particulate Emission CoricentFatiorr 

VES01804 7 
Parameter: Molecular 

Weight 

Run 1 

(Total mg)'mg/dscm; (ppm® (IWhr) 

7%02) 

Results Summary 

Unit 2 

Veolia ES Technical Solutions 

Sauget, IL 

Run 2 

(Total mg)'mg/dscm't (ppm@ (Ib/hr) 

7%02) 

Run 3 

(Total mgymg/dscm) (ppm@ (Ib/hr) 

7%02) 

Averaqe 

(mg/dscm) (ppm@ (Ib/hr) 

7%02) 

HCI 

CL2 

Total 

I 38.46 | I 16.7 

OS | 0.4 

13.2 

0.2 

13,4 

0.31 

0.01 

2.0 | 18.2 

I 0.5 I 0.4 

15.9 

0.2 

16.0 

0.41 

0.01 

I 32.4 | 27.6 21.8 0.61 20.4 17.0 044 

I 4.9 | 4.2 1.7 0.09 1.7 0.7 0.04 

23.5 17.7 

Where: 

pprtwd @ 7%Q? * part? per million « 7ViOxyaett=^maiHssltl'24 04 [it$tS/mo(Jftnol Svfn*«ao 8-?}r(2D S-QS'MS j 

VES01804 8 
Calculations Summary 

Unit 2 

Veolia ES Technical Solutions 

Sauget, IL 

Vw(std), scf = 

Vm(std), dscf = 

Bws= 

Md= 

Ms= 

Vs, ft/sec = 

Qs, acfm = 

Qs(std), dscfm = 

Isokinetic Sampling Rate, % 

Run 1 

30.784 

38.510 

0.444 

29.79 

24.55 

31.0 

15,453 

5,352 

98.2 

Run 2 

32.139 

42.729 

0.429 

29.73 

24.69 

33.4 

16,634 

5,963 

97.8 

Run 3 

31.523 

41.447 

0.432 

29.67 

24.63 

33.5 

16,661 

5,921 

95.6 

Averaqe 

31.482 

40.895 

0.435 

29.73 

24.62 

32.6 

16,250 

5,745 

97.2 

Where: 

Vwfstd^ =, volume of water vapor in gas, standard renditions; = 0.O4707'*Vlc 

Md >= nttteeular weight of stadias, dry basts = (Q 44 x%CQ2) + (0.32 x%02) + [&28 X (%N2+ %CO)J 

|Vs= Stack gas velocity = 85.4-9 x Cp X Sq Rf. dP) xfSq.Rf. (Ts(R»Ws X PS)] 

QS(S«) *-stackgas flowrate, standard eondilwns *Q s x t>Bws) x$287{rs{Rft.x (Ps/2S.92> 
Test Data Summary 

Unit 2 

Veolia ES Technical Solutions 

Sauget, IL 

Parameter 

Run Date 

Start Time 

Stop Time 

Duration of Run, Minutes 

Ave. Nozzle Diameter, inches 

Pitot Calibration Factor, CF 

Meter Gamma 

Meter Delta H, inches of H20 

Stack Diameter, inches 

Rectangular Width, inches 

Rectangular Length, inches 

Stack Area, sq.ft. 

Barometric Pressure, inches of Hg 

Static Pressure, inches of H20 

Drv Gas Meter Sample Volume. rVM)ft3 

Initial 

Final 

Difference 

Ave. Stack Temperature, Ts(F) 

Ave. Meter Temperature, Tm(F) 

Ave. Run Delta H, inches of H20 

Ave. Square Root of Delta P 

Run 1 

12/08/09 

10:05 

11:11 

60 

0.431 

0.84 

0.991 

1.801 

39 

8.30 

29.6 

-0.07 

55.894 

93.807 

37.913 

378.0 

51.3 

1.35 

0.4026 

Run 2 

12/09/09 

9:46 

10:49 

60 

0.431 

0.84 

0.991 

1.801 

39 

8.30 

29.3 

-0.07 

204.08 

245.112 

41.032 

363.1 

34.0 

1.61 

0.4363 

Run 3 

12/10/09 

11:00 

12:03 

60 

0.431 

0.84 

0.991 

1.801 

39 

8.30 

29.8 

-0.06 

373.656 

414.056 

40.4 

380.4 

50.0 

1.57 

0.4356 

Moisture Data 

Volume of water collected, mis 

Silica Gel, grams 

Total Collected, mis 

646 I 

8 

654 

675 

7.8 

682.8 

654 

15.7 

669.7 

ORSAT Data 

%02 

%C02 

%CO 

10.3 

8.6 

10.4 

8.2 

9.3 

8.1 

VES01805 0 
Field Data Summary 

Unit 2 

Veolia ES Technical Solutions 

Sauget, IL 

Stack 

TempJF) 

Delta 

P 

Do/M 

W SQRr Delta? 

Slack Tempff) Delta 

P 

Delta 

H 

TmtF) SQRT 

Delta P 

Stack 

Tempfff 

Delta 

P 

Delta 

H 

TmF) SQRT 

Delta P 

Stack 

TempJF) 

Delta 

P 

Do/M 

W In out 

SQRr 

Delta? 

Slack Tempff) Delta 

P 

Delta 

H in out 

SQRT 

Delta P 

Stack 

Tempfff 

Delta 

P 

Delta 

H In out 

SQRT 

Delta P 

379 0.18 1.5 43 46 0.4243 354 0.21 1.75 29 34 0.4583 i: •i 377 0.21 1.70 30 38 0.4583 

380 0.19 1.6 43 48 0.4359 3S4 0.23 1.S0 30 37 0.4796 378 0.21 1.70 34 46 0.4683 

360 0.19 1.6 44 52 0.4359 364 0.22 1.80 30 38 0.4690 :• j: 379 0.20 1.65 37 52 0.4472 

379 0.19 1.6 45 54 0,4359 366 0.20 1.70 30 39 0.4472 [: :| 379 0.22 1.80 39 56 0.4690 

376 0.14 1.2 45 55 0,3742 364 0.15 1.25 30 39 0.3B73 !: 378 0.18 1.50 42 58 0.4243 

375 0.09 0.75 46 55 0.3000 352 0.10 0.83 30 38 0.3162 i; I: 372 0.10 0.82 43 59 0.3162 

376 0.19 1.8 40 55 0.4359 363 0.21 1.75 29 37 0.4563 i: 383 0.22 1.80 49 59 0.4690 

379 0.18 1.5 4S SS 0.4243 363 0.20 1.70 30 38 0.4472 il 384 0.22 1.80 47 61 0.4690 

377 0.18 1.5 49 50 0.4243 364 0.23 i.90 30 39 0.4796 •; 385 0.20 1.65 48 62 0.4472 

379 0.18 1.5 50 61 0.4243 364 0.21 1.75 30 40 0.4583 i: 385 0.21 1.70 49 63 0.4683 

379 0,16 1.3 51 62 0.4000 365 0.20 1.70 30 40 0.4472 ;i !; 384 0.19 1.60 51 63 0.4359 

378 0.10 0,8 52 62 0.3162 364 0.1S 1.25 30 40 0.3873 :• il 381 0.14 1.15 52 64 0.3742 

378.0 0.164 1.35 47 '56 0.4026 363.1 0.19 1.61 30 38 0.4363 380.4 0.19 1.57 43 57 0.4356 

Traversa Paint 

A1 

2 

3 

4 

5 

6 

81 

2 

3 

4 

5 

Average 

laboratory Results 

Fuel F-factor,dscf/MMBtu 

FlterlD 

Font Half Residues: 

Fiterwt.g 

Acetone rinse volume, ml 

Acetone wt, g 

F.H. Total, g 

flick Half Residues: 

BH.Total.g 

Acetone Blank Residues: 

Acetone blank volume, mt 

Acetone Blank vwight, g 

Acetone weight galn.g 

Acetone Blank concentration 

,0>1% of Acetone Blank Weight 

Weiqht of Residue in Acetone Wash, a 

Corrected Acetone Blank Value, g 

(f.H, Total+B.H. Total-Blank): 

Run 1 

I 0.0006 

J L" J L" 

I 0.0019 I 

0.0025 

I 0.0026 I 

3 I 

1 Z 1 

153.8992 I I 153.8992 ~1 

I 0.0016 I 

0.0019 

I 196 

I 0.00000 I 

I 0.0015 | 

I 0.0001 1 

I 0.0003 1 fj 

I 0.00000 I Ca = Ma/VaPa 

I 0.0015 I 

Wa = CaVawPa 

0.0001 I I 0,000039 ~l I 0,0001 

Total, g 

VES01805 1 
Dry Ga s Meter Calibration Data Summary 

Unit 2 

Veolia ES Technical Solutions 

Sauget, IL 

Parameter 

Run ID 

Run Date 

Meter Box ID 

Duration of Run, Minutes 

Meter Gamma 

Delta H@, inches of H20 

Barometric Pressure, inches of Hg 

Sample Volume, dcf (Vm) 

Ave. Meter Temperature, F (Tm) 

Dry Molecular Weight (Md) 

Ave. Delta H, inches of H20 

Ave. SQRT Delta H, inches of H20 

Yqa (calculated calibration factor) 

% Difference 

12/8/2009 

002 

60 

0.991 

1.801 

29.6 

37.913 

51.33 

29.79 

1.35 

1.15 

0.995 

0.4 

12/9/2009 

002 

60 

0.991 

1.801 

29.3 

41.032 

34.04 

29.73 

1.61 

1.26 

0.993 

0.2 

12/10/2009 

002 

60 

0.991 

1.801 

29.8 

40.400 

49.96 

29.67 

1.57 

1.25 

1.007 

1.6 

Averaqe 

0.7 

Yqa = (test duration/Vm) x (SQRT(0.0319*TmR)/(Delta H@ x (Pbar + Ave. Delta H/13.6)) x (SQRT(29/Md)) x Ave.(SQRT Delta 

% Difference = (Yqa - Meter Gamma)/Meter Gamma 

Three run Average % Difference must be <= 5% 

VES01805 2 
AECO M 

Sampling Train 

Run Number 

Client 

E P A ISOKINETI C SAMPLIN G 

Barometric Pressure 

FIEL D DAT A SHEE T 

Veolia ES Technical Solutions 

Facility Location 

Source 

Date 

Operator 

Stack Dia. - iii. 

Start Time 

Stop Time 

Sauget eU, I L 

Static Pressure (+/-) "Oi O"/ 

Probe/Pilot Number S/HjT". */-P~ 

Pitot Coefficient 

LEAK CHECKS in "Hg 

INITIAL VAC IS" 

MID VAC. —-

FINAL VAC. ts) 

Filter Box No. 

Meter Box No. 

Orifice Coefficient (Y) 

Delta H@ _ 

Nozzle Size/No. 

cfm _ods\ 

CFM 

CFM &,0£>M 

INIT. PITOT FINAL PITOT 

FILTER DATA 

z 

ioz<r H,(t~ XAD Thermocouple ID: /?),<?7&~cXS 

1ARI 

o < Hi -*7 

..IMPINGER VOL'S. 

|gEWAB> 

3E 

&nt>rif 

3? 

I 

LM 

F 

IF IH O 

1 sH 

K 

w *VOLUME

 A 

TEMPERATURE READINGS °F I -PUMP 

VAflHIM 

I 

LM 

F 

IF IH O 

1 sH 

K 

w *VOLUME

 A 

• A K PU t 1 11 1 N 

Ml II l> 

-PUMP 

VAflHIM 

I 

LM 

F 

IF IH O 

1 sH 

K 

w *VOLUME

 A 

• A K PU t 1 11 1 N IN Oil 1 . i 

-PUMP 

VAflHIM 

(3 $ 055. ST * 2>p? M i lb? 

2- r ,<? /»«M,/7 W > '2S& 2-7* XT 13 +8 

3 i0 r f Obis * U~'l 2<f i M- f.SY So? 

<T TO %C Bilk- l,/ < 2-6 f. 2 %. -rl8 IU ? r V 

vr 50 0,Of •r/.r 2^5 J-7? 3^ n> . r r H 

#•(9 5 

> A<r 0764 — ,1L 

* s & 

1 / — • 

UO UK f)dt> c$i % ?77 'H (an 

war Sb 0,18 / .<r 374 ifb \ ( 4 & CS' 0.1 to am*} lo 37# O p - <r ^ /// / 

|t>5 

RINSE: 

'TO 

Orsat 

C02 ,02. 

VES01805 3 
E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

Sampling Train 

Run Number 

Client 

Barometric Pressure 

Static Pressure (+/-) 

3 

Veolia ES Technical Solutions Probe/Pitot Number Sf^S~~^ C> 

Facility Location 

Source 

D:'.!iOperator 

Stack Dia. - in. 

Start Time 

Stop Time 

Sauget,, IL 

QH'tt # 3 -

2 f l 

Pitot Coefficient 

Filter Box No. 

Meter Box No. 

Orifice Coefficient (V) 

Delta H@ 

Nozzle Size/No. 

XAD Thermocouple IDi 

Imp Outlet TC ID: 

O. & 

LEAK CHECKS in "Hg,. 

INITIAL VAC. / > 

MID VAC. •> 

FINAL VAC. jO 

CFM 

CFM 

CFM 

INIT. PITOT FINAL PITOT 

FILTER DATA 

MJ-M 

mmmmm 

160 

^MM 1 

IIIIMn 

1 1 IK-KJ ' MKH itlj ' 

iiii\orp 

BDeiullitln wc® 

* l.\s\1l IIII ' 1 TEMPERATURE READINGS, °F 1 

&a|int rCOMMENTS 

J; _ 

^MM 1 

IIIIMn 

1 1 IK-KJ ' MKH itlj ' 

iiii\orp 

BDeiullitln wc® I' '\tii 1 \n' A &a|int rCOMMENTS 

J; _ 

At f / 1W / a?, 7-^' 6 

3- r *> 3 a-/ ^0 V7 7 

'{..BO 7 z/«r c'4 Z.70 3-1/ 3d 30 

2<S> i< Xb{ 3x. 

1-15 7-«?? £6 7.<7 (a 

0- VL7. bh l& 4« <o 

l.q 111 .4, ?R ^0 ?? •7 

a, 1/75 "toy >D "7 

f 155 ^2^ 40 

in OR MO & 

' 

SRJNSEj 

(06 

Final Purge Hate Jft \ft 

Final PH 

7JL 

Orsat 

i.02 : 

JO.'/ 

VES01805 4 
A3CO M

 EP A

 ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

r IMPINGER VOL'S. Orsat 

Sampling Train Barometric Pressure w^f •<S ' * ? • LEAK CHECKS in "Hg 

INITIAL VAC. /5 ^ 

^mir,.-

'RINSE. G02? 

Run Number Static Pressure (+/-) 

LEAK CHECKS in "Hg 

INITIAL VAC. /5 ^ in. CFM CS.O/S 

Client Veolia ES Technical Solutions Probe/Pitot Number MID VAC. — in. CFM S.( 1 3 — i o o 

" 

S.( 1 3 

Facility Location Sausct, IL Pitot Coefficient FINAL VAC. /CS in. CFMtf.«t7 7 f C o 1=17 

Source Filter Box No. m k +

 y y a sDate Meter Box No. •mm INIT. PITOT *^ " FINAL PITOT I tj Ci 1 O G 

Operator «/- Orifice Coefficient (Y) '••'W&VQf FILTER DATA f 0 b I bO 

Stack Dia.-in. 2<? Delta H@ liPpjBiBjfg 

Stare Time Nozzle Size/No. 

Stop Time II !BO XAD Thermocouple ID: fVG»T~C i L SSSSSSII2IC A^EIiSfcs.iis« nnal Pur gettate M A 

Imp Outlet TC ID: K - 2f*- 7 Final PH . 

*\MPI t ( 1 ()( K \H0C1IV orih< l \SMI II 1 TEMPERATUR E READING S F PUMP 

1IIIM IIMI m \ o ' ML IIK VOL NOI 1 MF OIK *M f VA( HUM •COMMENTS 

_ ... Ueltall, in.vii,iJk, ft SI it Iv 1 UOII OM N MODI LI _I%HINrFR„ IN 

A\ 0 <" irf b 3 7 3 r b-?& 0 7 7 Z<W t u t 3 3 s r -

' 2- ((? 2:>? 

ts* 

s / r f>**> •5ft£>.73— 2(, 0 3 7 ft 

t W 3 7 9 

to %< O.t b ?»7 ^ Z<?c* S7 CP 

V 2T M> 0,1 0 o.8>- I S ? 5Tf 5 " 

r <2|.^ 

>» A * o ZUo T f . . ..v... 

1- ?

r a . 7.0- i.SO .Z£.o IS-9 oft G "7 

T> 2.S7 3 / 1 S 7 7 

6.2- / t .70 / b 

O.t l l-LO z<w J l O r l ft 

0 . 1 + 1.19- I C O 

\J " TT 

VES01805 5 
AZCOM 

, , r _ SAMPL E TRAI N MOISTUR E RECOVER Y DAT A SHEE T 

Reference Method / Sampling Trai n : 00,5 \ d-bft 

Recovered by : ^ MOftfaS Recovered by : <J. • f*VO <tf Recovered by : >T |T^ S 

Run No. U3 --(^ l Date: IJ -l^I& l Run No. U3l — i ^-Dat e : RunNo .UJ^J ^ J Date : 

X A D Module No. : fsj|A- X A D Module No. : N | rV X A D Module No. : f"i | fir 

FilterNo. : Tl8 "9" ^ ©.^3 7 FilterNo.:^! !

 0 "Ifi 71 Filtur No. : 

Im pinge r No. sn d Volum e Im pinge r No. and Volum e Im pinger No. and Volum e 

No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) 

1 1 1 

2 tot> 2 l o o 2 

3 (" ^ 

\ 

3 3 \ox>. I f / 

\ J 

4 o 

r 

4 0 > 4 

0 f 

11 

5 / D O 5 ) o o 5 

i 

6 / O o /ot> 6 ( 0 0 6 t o o 

7 7 7 

DIFF : DIFF : 

7 

DIFF : 

Totals f £ 5 0 Total s HSO H a s 6 7 5 Totals 

Initial 

(g) 

Final 

(g) 

tin Initial 

(g) 

Final 

(g) / 

\ Initial 

(g) 

Final 

(g) 

Initial 

(g) 

Final 

(g) DIFF : 

tin Initial 

(g) 

Final 

(g) DIFF : / 

\ Initial 

(g) 

Final 

(g) DIFF : 

Silica 

Gel y . o 

Silica 

G el 

Silica

 1 

Gel 

Silica 

Gel y . o 

Silica 

G el 

Silica

 1 

Gel 

Final Net Moistur e Gain : Final Net Moisture Gain : Final Net Moisture Gain : 

C:\Oocuments and SettlngMrnlos10estoop\[Molsture Recovery.xls]A 

VES01805 6 
Method 0023A 

VES01805 7 
PCDD / 

Veoli a 

PCD F Emi s 

Metho d 0 

Run No. 

Date 

Start Time 

E S Technica l Sc 

sio n Result s - T l 

023 A Samplin g I 

1 

08-Dec-09 

12:30 

)lution s 

EQ Basi s - Fron i 

3

arameter s 

2 

09-Dec-09 

12:59 

Hal f 

3 

10-Dec-09 

13:00 

Sample Volume 

Stop Time 

Units 

dscf 

15:36 

107.857 

16:54 

121.809 

16:06. 

121.529 

Sample Volume m

3 3.05 3.45 3.44 

Moisture Content % v/v 47.3 43.9 46.1 

0 2 Concentration % v/v (dry) 9.10 9.30 8.20 

C 0 2 Concentration % v/v (dry) 8.43 8.14 7.90 

Isokinetics % 98 95 97 

Stack Flowrate dscfm 4,987 5,840 5,682 

PCDD/PCD F 

Parameters TEF (a) 

pg ng/m3 

TEQ 

pg ng/m3 

TEQ 

pg ng/m3 

TEQ 

2,3,7,8-TCDD 1.00 2.87 9.4E-04 2.27 6.6E-04 2.37 6.9E-04 

1,2,3,7,8-PeCDD 0.50 4.13 6.8E-04 3.34 4.8E-04 3.70 5.4E-04 

1,2,3,4,7,8-HxCDD 0.10 5.22 1.7E-04 7.68 2.2E-04 4.98 1.4E-04 

1,2,3,6,7,8-HxCDD 0.10 4.11 1.3E-04 6.04 1.8E-04 3.92 1.1 E-04 

1,2,3,7,8,9-HxCDD 0.10 4.3 1.4E-04 6.34 1.8E-04 4.11 1.2E-04 

1,2,3,4,6,7,8-HpCDD 0.01 8.03 2.6E-05 5.41 i.6E-05 8.70 2.5E-05 

OCDD 0.001 8.89 2.9E-06 17.6 5.1 E-06 14.2 4.1 E-06 

2,3,7,8-TCDF 0.10 2.58 8.4E-05 3.84 1.1 E-04 3.02 8.8E-05 

1,2,3,7,8-PeCDF 0.05 3.92 6.4E-05 4.33 6.3E-05 3.52 5.1 E-05 

2,3,4,7,8-PeCDF 0.50 4.15 6.8E-04 4.58 6.6E-04 3.73 5.4E-04 

1,2,3,4,7,8-HxCDF 0.10 3.93 1.3E-04 3.11 9.0E-05 2.61 7.6E-05 

1,2,3,6,7,8-HxCDF 0.10 4.60 1.5E-04 2.48 7.2E-05 1.57 4.6E-05 

2,3,4,6,7,8-HxCDF 0.10 1.68 5.5E-05 3.13 9.1 E-05 1.98 5.8E-05 

1,2,3,7,8,9-HxCDF 0.10 1.89 6.2E-05 1.85 5.4E-05 2.22 6.5E-05 

1,2,3,4,6,7,8-HpCDF 0.01 3.11 1.0E-05 9.35 2.7E-05 6.49 1.9E-05 

1,2,3,4,7,8,9-HpCDF 6.6i 4.10 1.3E-05 3.56 1.0E-05 2.28 6.6E-06 

OCDF 0.001 6.33 2.1 E-06 5.75 1.7E-06 7.44 2.2E-06 

TOTAL TEQs (ng/m3) = 3.3E-03 

i qp 

2.9E-03 

i £P n** 

2.6E-03 

O OP f\1 

1U1 AJ-i i s (ng/m (gj 7 yo SJi) — 

TOTAL TEQs (g/s) 7.9E-12 8.1E-12 6.9E-12 

(a) U.S. EPA (1989) Toxic Equivalency Factor 

S:\_JOB\2009Weolia\Test DataVUnit 2\(unil2_M0023A.xlsx]TEQS-FH 

VES01805 8 
Veoli a E S Technica l Solution s 

PCD D / PCD F Emissio n Result s - TE Q Basi s - Bac k 

Metho d 0023 A Samplin g Parameter s 

Hal f 

Run No. 1 2 3 

Date 08-Dec-09 09-Deo-09 10-Dec-09 

Start Time . 12:30 12:59 13:00 

Stop Time 

1 Initc 

15:36 16:54 16:06 

Sample Volume dscf 107.857 121.809 121.529 

Sample Volume , m

3 3.05 3.45 3.44 

Moisture Content % v/v 47.3 43.9 46.1 

0 2 Concentration % v/v (dry) 9.50 9.50 9.50 

C 0 2 Concentration % v/v (dry) 9.20 9.20 9.20 

Isokinetics % 98 95 97 

Stack Flowrate dscfm 4,987 5,840 5,682 

PCDD/PCD F P9 ng/m3 

pg ng/m3 

pg ng/m3 

Parameters TEF (a) TEQ TEQ TEQ 

2,3,7,8-TCDD 1.00 4.14 1.4E-03 3.34 9.7E-04 4.80 1.4E-03 

1,2,3,7,8-PeCDD 0.50 21.1 3.5E-03 18.6 2.7E-03 17.1 2.5E-03 

1,2,3,4,7,8-HxCDD 0.10 27.0 8.8E-04 21.9 6.3E-04 17.7 5.1 E-04 

1,2,3,6,7,8-HxCDD 0.10 49.0 1.6E-03 43.2 1.3E-03 32.2 9.4E-04 

1,2,3,7,8,9-HxCDD 0.10 31.0 1.0E-03 24.7 7.2E-04 23.7 6.9E-04 

1,2,3,4,6,7,8-HpCDD 0.01 203 6.6E-04 194 5.6E-04 149 4.3E-04 

OCDD 0.001 167 5.5E-05 182 5.3E-05 117 3.4E-05 

2,3,7,8-TCDF 0.10 22.5 7.4E-04 15.0 4.3E-04 14.1 4.1 E-04 

1,2,3,7,8-PeCDF 0.05 32.5 5.3E-04 218 3.2E-04 16.6 2.4E-04 

2,3,4,7,8-PeCDF 0.50 104 1.7E-02 56.3 8.2E-03 50.1 7.3E-03 

1,2,3,4,7,8-HxCDF L 0.10 55.1 1.8E-03 46.1 1.3E-03 25.9 7.5E-04 

1,2,3,6,7,8-HxCDF L 0.10 47.0 1.5E-03 32.8 9.5E-04 23.7 6.9E-04 

2,3,4,6,7,8-HxCDF 0.10 96.0 3.1E-03 55.0 1.6E-03 44.0 1.3E-03 

1,2,3,7,8,9-HxCDF 0.10 24.8 8.1E-04 15.3 4.4E-04 11.2 3.3E-04 

1,2,3,4,6,7,8-HpCDF 0.01 114 3.7E-04 133 3.9E-04 63.5 1.8E-04 

1,2,3,4,7,8,9-HpCDF 0.01 22.5 7.4E-05 19.2 5.6E-05 11.6 3.4E-05 

OCDF r

 6.6o'i 42.5 1.4E-05 73.0 2.1 E-05 21.0 6.1 E-06 

TOTAL TEQs (ng/m3) 0.035 0.021 0.018 

TOTAL TEQs (ng/m3 @ 7 % 02 ) 0.043 0.025 0.022 

TOTAL TEQs (g/s) = 8.3E-11 5.7E-11 4.7E-11 

(a) U.S.EPA (1989) Toxic Equivalency Factor 

S:\_JOB\2009\Veolla\Test DataUJnit 2Munit2_M0023A.xlsx]T£QS-FH 

VES01805 9 
Veoli a E S Technica l Solution s - Uni t 2 

Fixe d Heart h Kil n #2 

Metho d 0023 A Samplin g Parameter s 

Run No. 1 

08-Dec-09 

12:30 

15:36 

2 

09-Dec-09 

12:59 

16:54 

3 

10-Dec-09 

13:00 

16:06 AVGS 

Date 

1 

08-Dec-09 

12:30 

15:36 

2 

09-Dec-09 

12:59 

16:54 

3 

10-Dec-09 

13:00 

16:06 AVGS 

Start Time Units 

1 

08-Dec-09 

12:30 

15:36 

2 

09-Dec-09 

12:59 

16:54 

3 

10-Dec-09 

13:00 

Stop Time 16:06 AVGS 

1 

08-Dec-09 

12:30 

15:36 

2 

09-Dec-09 

12:59 

16:54 

3 

10-Dec-09 

13:00 

16:06 AVGS 

Nozzle Diameter inches • 0.431 

29.40 

180.0 

109.422 

0.431 

29.50 

180.0 

119.067 

0.431 

29.80 

180.0 

121.773 

0.431 

Barometric Pressure iri. Hg 

• 0.431 

29.40 

180.0 

109.422 

0.431 

29.50 

180.0 

119.067 

0.431 

29.80 

180.0 

121.773 

29.57 

Net Sampling Time min. 

• 0.431 

29.40 

180.0 

109.422 

0.431 

29.50 

180.0 

119.067 

0.431 

29.80 

180.0 

121.773 

180.0 

Volume Metered dcf 

• 0.431 

29.40 

180.0 

109.422 

0.431 

29.50 

180.0 

119.067 

0.431 

29.80 

180.0 

121.773 116.754 

Avg. DGM Temp. °F 63.2 46.1 64.1 57.8 

Avg Delta H in H 2 0 1.20 1.46 1.51 1.39 

Avg Delta H in. Hg \ 0.0885 0.1074 0.1114 0.1024 

DGM Calibration Factor — 0.9910 0.9910 0.9910 0.9910 

Gas Sample Volume dscf 107.857 121.809 121.529 117.065 

Total Water Collected mL 2051.9 2021.5 2205.3 2092.9 

Volume of Water Vapor scf 96.747 95.314 103.980 98.680 

Moisture ^measured) % v/v i 47.3 43.9 . 46.1 45.8 

Moisture (@ saturation) % v/v 101.8 101.4 100.4 101.2 

Dry Mole Fraction, 100-%M — 0.5271 0.5610 0.5389 0.5424 

C 0 2 at Stack %dry 8.43 

9.10 

8.14 

9.30 

7.90 

8.20 

8.16 

O z at Stack % dry 

8.43 

9.10 

8.14 

9.30 

7.90 

8.20 8.87 

CO + N2 %dry 82.47 82.56 83.90 82.98 

Dry Molecular Weight Ib/lb-mole 29.71 29.67 29.59 i 29.66 

Wet Molecular Weight Ib/lb-mole 24.17 24.55 24.25 24.32 

Excess Air at Stack % 71.8 74.4 58.8 68.3 

Stack Diameter inches 39.0 39.0 39.0 39.0 

Stack Area sq. in. 1194.6 1194.6 1194.6 1194.6 

Static Pressure in HaO -0.04 -0.08 -0.06 -0.06 

Stack Pressure in. Hg 29.40 29.49 29.80 29.56 

Avg. Stack Temp. °F 379.3 373.2 386.0 379.5 

Avg. Sqroot of Delta P -- 0.3945 0.4354 0.4398 0.4233 

SDE Average — 11.430 12.569 12.793 12.264 

Pitot Coefficient — 0.84 0.84 0.84 0.84 

Stack Gas Velocity afpm 1,848 2,013 2,051 1,970 

Stack Flowrate wet acfm 15,328 16,698 I 17,014 16,347 

Stack Flowrate wet scfm 9,474 10,431 i6,575 10,160 

Stack Flowrate dscfm 4,994 5,852 5,699 5,515 

Isokinetics % 98 95 97 97 

Meter Box No. — 2 

1.8010 

2 

1.8010 

2 

1.8010 

— 

Delta H @ ....Ln

-..

H

9.... 

2 

1.8010 

2 

1.8010 

2 

1.8010 -

Field QA Yqc — 1.000 0.994 1.003 0.999 

[Deviation] Pre-Y % 0.9% 0.3% 1.2% 0.8% 

S:\_JOB\2009\Veolia\Test DataUJnit 2\[unit2_M0023A_nsw data.xlsx]DATA 

VES01806 0 
Method 0023A Sampling Parameters 

PT 

RUN 1 AVGS - PCDDs/PCDFs RUN 2 AVGS - PCDDs/ PCDFs RUN 3 AVGS - PCDDs/PCDFs 

PT DP SQRT 

DP 

DGM 

IN 

DGM 

OUT 

DH STACK 

TEMP 

DP SQRT 

DP 

DGM 

IN 

DGM 

OUT 

DH STACK 

TEMP 

DP SQRT 

DP 

DGM 

IN 

DGM 

OUT 

DH STACK 

TEMP 

a1 0.19 0.4359 56 59 1.60 378 0.23 0.4796 23 25 1.70 374 0.22 0.4690 53 56 1.80 388 

1 0.19 0.4359 56 60 1.60 380 0.23 0.4796 27 32 1.70 374 0.24 0.4899 53 59 2.00 389 

a2 0.18 0.4243 57 64 1.50 379 0.23 0.4796 27 32 1.70 375 0.23 0.4796 54 61 1.90 390 

2 0.18 0.4243 57 65 1.50 380 0.23 0.4796 27 33 1.70 377 0.23 0.4796 55 65 1.90 390 

a3 0.18 0.4243 57 65 1.50 383 0.21 0.4583 27 33 1.60 379 0.20 0.4472 57 68 1.65 390 

3 0.17 0.4123 58 66 1.30 381 0.21 0.4583 27 34 1.60 378 0.21 0.4583 58 68 1.70 391 

a4 0.17 0.4123 58 66 1.30 380 0.22 0.4690 27 34 1.70 378 0.21 0.4583 59 68 1.70 390 

4 0.17 0.4123 58 67 1.30 380 0.22 0.4690 28 35 1.70 376 0.22 0.4690 59 68 1.80 389 

a5 0.13 0.3606 59 67 1.00 380 0.20 0.4472 29 40 1,50 375 0.19 0.4359 60 67 1.40 388 

5 0.14 0.3742 59 67 1.00 380 0.20 0.4472 36 52 1.50 374 0.19 0.4359 60 66 1.40 387 

a6 0.10 0.3162 60 67 0.75 377 0.10 0.3162 40 60 0.75 370 0.10 0.3162 60 67 0.75 385 

6 0.10 0.3162 60 67 0.75 377 0.10 0.3162 45 63 0.75 370 0.10 0.3162 62 70 0.75 385 

b1 0.17 0.4123 61 66 1.30 380 0.23 0.4796 50 63 1.70 371 0.21 0.4583 63 70 1.60 385 

1 0.17 0.4123 61 68 1.30 382 0.23 0.4796 51 • 63 1.50 371 0.21 0.4583 64 72 1.60 385 

b2 0.17 0.4123 61 68 1.30 380 0.18 0.4243 52 63 1.35 370 0.20 0.4472 65 72 1.50 384 

2 0.17 0.4123 62 69 1.30 380 0.18 0.4243 52 63 1.35 369 0.21 0.4583 65 72 1.60 384 

1)3 0.16 0.4000 62 69 1.20 381 0.20 0.4472 54 64 1.50 370 0.22 0.4690 63 68 1.65 385 

3 0.16 0.4000 62 69 1.20 380 0.18 0,4243 55 64 1.35 370 0.20 0.4472 62 68 1.50 385 

t>4 0.15 0.3873 62 68 1.10 381 0.18 0.4243 55 62 1.50 372 0.22 0.4690' 61 68 1.50 384 

4 0.15 0.3873 62 68 1.10 381 0.18 0.4243 55 61 1.50 372 0.20 0.4472 62 71 1.50 384 

bS 0.14 0.3742 62 68 1.00 380 0.18 0.4243 55 60 1.50 372 0.20 0.4472 62 71 1.50 383 

5 0.14 0.3742 62 68 1.00 379 0.18 0.4243 54 58 1.50 373 0.18 0.4243 63 72 1.35 383 

be 0.14 0.3742 62 68 1.00 377 0.15 0.3873 53 58 1.20 373 0.15 0.3873 63 72 1.15 380 

e 0.14 0.3742 62 68 1.00 367 0.15 0.3873 53 60 1.20 373 0.15 0.3873 64 73 1.15 380 

AVG 0.16 0.3945 63.2 1.20 379 0.19 0.4354 46.1 1.46 373 0.20 0.4398 64.1 1.51 386 

VES01806 1 
A-COM E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

Sampling Train 

Run Number 

Client 

X 

Barometric Pressure 

Static Pressure (+/-) 

Veolia ES Technical Solutions 

Facility Location 

Source 

Date 

Operator 

Stuck Dia. - in. 

Start Time 

Stop Time 

sauget, JL. 

Probe/Pilot Number iS/Wj"' 

Pitot Coefficient G 1$ 

Filter Box NoMeter Box No. 

Orifice Coefficient (V) 

Delta H@ 

Nozzle Size/No. 

f t -

LEAK CHECKS In ^Hg 

INITIAL VAC. ' ' 

MID VAC._ 

FINAL VAC. 

:KS In ''Hg 

7W 

CFM ^CYP 

CFM 

INIT 

FINAL PITOT 

FILTER DATA 

%5E> XAD Thermocouple ID: 

Imp Outlet TC ID: L£. — <^3— 

•••>n.um'bf.rv:: 

. — 

IMPINGFH VOL'S. 

FINAL 

Iff?** 

9<r 

5r.;>^lWCA--PELi.,»- ..- • 

35X4 I 3&r-3 

MA 

Orsat 

C02, 

1.1 

Final Purge Bate ti j fi, 

Final PH _____ 

SVMI 1 I 

I'tllN 1 

( 1 (X k 

IIMI 

\ i n n u t 

hi- \ n 

DriMP in we 

ORIFirt 

MIlrK \OI 

IM1»I1 inwc 

• \S Ml II II TEMPERATURE READINGS, °F | 1IIMP 

v \ru i m 

in.Hf 

COMMENTS 

SVMI 1 I 

I'tllN 1 

( 1 (X k 

IIMI 

\ i n n u t 

hi- \ n 

DriMP in we 

ORIFirt 

MIlrK \OI 

IM1»I1 inwc 

Mil 1 Ml 

MM h PRjBB^Ii 

llll.VMi 

MOBULL-' 

» T GAS METER 

1IIMP 

v \ru i m 

in.Hf 

COMMENTS 

SVMI 1 I 

I'tllN 1 

( 1 (X k 

IIMI 

\ i n n u t 

hi- \ n 

DriMP in we 

ORIFirt 

MIlrK \OI 

IM1»I1 inwc 

Mil 1 Ml 

MM h PRjBB^Ii 

llll.VMi 

MOBULL-' #IN ^ our -

1IIMP 

v \ru i m 

in.Hf 

COMMENTS 

f ) l<? a s ? 3 

? £ / r A •/? a r t 2vQ St. CO /o 

}$~ %IS ' D.fS c

~l /O 

®- US ZD z.rr to 

f>r*r 3D 7*5 I O.ltf /,s~ UH.U M$ *xu>o 3 . 9 s

i 

Sfc" ft ' o.n A 3 ^6/ f -S"S> - to 

.Off a n ZS(o ^! 9 

£ K " 60 f . 3 u,t r ? s& 1 

AS Or\h h° />£ & 

0 - i + 1.5 ft 7 6 

OAO 0-7S ~ MX* A r n 2 SI is-) i 

i4>Q £ a 7 _3«^e, /<+&o 

1

 V 

HO 3&0 34 ^/ 1 re-^J*v4- /^(?^> 

tig- D, n • — 3 7 ib 

ac !l%t " -U 7 1 . 3 IO 

\n 

" (0 , i(p 1-3-. 1

c

f <r? ^7 (a 

eo.c m 

' 0 Vc 3X0 •2-r'f (cl IO 

i-l nff- r — •u4 so (fk 10 

/<& IA m 7Se 5 S Si (*& 

e r ISD fi.l l \JO 360 7J>c

j ?<^- ^ 

T 

' n.llr LO i l l 2u1 £»£> i 

• OAUc f.r> 311 > r 6 6 6 

ro<r /so Hd>l •xsrft 

m 

3oo| 

VES01806 2 
E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

iHSZoX> 

•uC] 

^IMPINCEB VOL S Orsat 

Sampling Train l*i<H> Barometric Pressure At • \ LEAK CHECKS in "Ug 'INIT,*'," FINAL RINSE CC02- 02 

Run Number Static Pressure INITIAL VAC. In. CFM £> 

Clien t( u t Veolia ES Technical Solutions Probe/Pitot Number MID VAC. in. CFM dr*f*~H >• .T | 

1 t( u 

Facility Location Sauget, IL Pitot Coefficient FINAL VAC. / % in. CFM £>. d> /iQ 

Source Filter Boi No. + - •• + 

Date 13.- Meter Box No. INIT. PITOT «/ FINAL PITOT 

Operator Orifice Coefficient (Y) (3.. KH/ FILTER DATA 

Stack Dia. - in ? Delta II @ ISHbM'bIrIII 

Start Time ty /2L/

<

4- Si^ozzle Size/No. 

Stop Time /Jf¥f o 5f°&AD Thermocouple ID: Y^AP -1p (••.'..«vS;SILlC*OEl..-- ;•• ^ ;Fina C l Purge Rate J-l { A" 

Imp Outlet TC ID: k « Final PH 

•V PI 1 ICb r*S\h FR TEMPERATURE READINGS, °F | MIMP 

P IN H AD \OL Ml IIKl.\Ml \ U IIIIM onfMer <TS: ' 

1 aP n <v D 1 IROBF .Monm l " - our m 111! 

Arl 7 J ±f~i*-e—>* . / - 7 ••2 5 - "i- ^ • - I S 

/ , ? ? r ^ ^ aV 

t r 27< - o a. 3 A " / fat**- CMiC^ V i> .t 

2.i„c ?<> i w , - — 1 7 7 n 0 -'7 ,01s J

 \ v5W -

A3 <3<D ITi-oX. ,yt' 

? / r ^ \ n-z-l HO ? j r | f tJfffi^- \ 

#<~ £?.< ' 0-13- 1 . 7 ^7r ? 3 7 '2.7 1 3 

— 1 © 2-2-- 51 fCs, 1 3 

A<T • G-lO 140 1 3 • . .— 

7M>4 . 7 7 ; 3 

0 -7fT 3 7 0 •z-57?- - tt€> Ho 7 

KL^T— rt.. i © 7 

Ae&< P»f-!r-cA«n 

)?\ tJ7 K7( / f 

U* \ m/r ro c 1.3 :v7/ t i 

ft?- Otto w , — S 7 0 Hi 

}I2.C (30 Or iK t,3<r -Z6 T I P , 12—-

/20 au \,S W . 5 7 HQ bHr 1 3- ^ 

.pr & -0.1% 1 * 5 . 270 / S 3 SL 

VXs 

- o, 1$ iJSD •Zd> i Wis ^ 7 f r OX IX 

\f..~f—— Is* , 0 . If) ixo 37 O 1 

t<Tb - Q> \h /\<5b 21 &~ 

(SIS tu* 0.(8 t & 140 M - [Is 

flu /.X L 

ITLC (6O 0 -if 3"fcflr — 37> - p <r 

riAWtUs'ii;^ ^ 

VES01806 3 
ASCOM E P A ISOKINETI C SAMPLIN G - FIEL D DAT A SHEE T 

Al 

A t 

M 

<2tS o 

WglMPINCf R\<II'S Orsat 

Sampling Train Barometric Pressure <2tS o LEAK CHECKS in "Hg 

INITIAL VAC. If/? 

i^INIT, . ^ tlNAI. RINSE C02': 02 : 

Run Number 3 Static Pressure (+/-) - 0 , 

LEAK CHECKS in "Hg 

INITIAL VAC. If/? in. CFM z^?^?/ / 

Client Veolia ES Technical Solufions Probe/Pitot Number ayte-s c MID VAC. 0 1.9 in. CFM O'-'dlT- 1 1.9 

Facility Location Sauget, IL Pitot Coefficient FINAL VAC. /t / in. CFM r> Source Filter Box No. Aft"? - /- / / 

Date Meter Box No. <?t>PINIT. PITOT * ^ FINAL PITOT 

Operator 

Wt u tHUAV T - VatiSOUPi/ Orifice Coefficient (V) 0. t} <J I 

FILTER DATA u 

Stack Dia. - in Delta K @ 

1. 8o( w e ,;

""Vv. -*tiStart Time Nozzle Size/No. 

Stop Time XAD Thermocouple ID; ^fiKI — jt> ;SrLICA:CEL:4 -:;r Final Pur geRate | J A -

Imp Outlet TC ID: lO: ^ 7- 5 2>S~?r7 Final PH — . 

\MI 1 1 I 1 III k M i ni i n 1 IIII II1 l *. Ml II l< TEMPERATUR E READINGS , ° F | PUMP 

1 (UN 1 rum HF AD MFIIKVOI VOI UMl -ORq&NKT 

TMPDSGFRJ 

^a^GA^iMETER^v, V \< lliM • COMMENTS' • 

LHItil in wc DellaH In wc 

^l \t k 

PROBI 

-ORq&NKT 

TMPDSGFRJ <- OUT t in^Hg 

A, D 7.5 ,r, ? 

7S X if) 2<fL S o-

' /o 

15 M D 1 0 . 

3 ^ fe>l. 

10 37-C 0.7 0 fro 17 * T 7 Q 

15 0,2. / i.n HH*. Hr ^ l 

A t 0.2. / 1-1 Z$rf IF? 3 7 u>/o 4 

0 .2-2 -

i-& 5 ? 3«S > 

H9 oa O . f ? IM zSq 7Sfi> 6 0 T 

/ . 4 1 ^ 7 ^ 1 IpL 

a<r • « 8l-< 0.7^ M O 

O

to 7 

 -75 " 3 0 r 

7 ^ / 2£f / ^ > & 

^75" , 92 / ' Pari ckotr^ e 

& <b f ? D T7.5 • 0.2. / hip no 

0 L( Ufa. 01 2(p0 <tl t o 

* fox •OS /,i<r 0.2.Q h.r ?$4 £9 IX *? 

/ft.?" /2o O.ZI f.U 2 6 0 2(11 . bl M.X to 

/3f) il?- 1 5 7 3 f t IT) 

G P S AST i . r 2 2 5 6 2 - l o 

ffa r 's o f « s hL Lf\ / o 

M-f f¥ft <S7-' 5 7 4 . O K 7o 

f M i.f , w> ^ 7 7 / 10 

* i/— 1ST ,724 - t), IS M 5 

i -t S ^>7-<S"2 - 3 5 0 7-UL 0 3 • 7 ^ 

l-IS - S 7 b 0 

S ^ k 40 7 

VES018064 
AECOM 

_ ^ SAMPLE TRAIN MOISTURE RECOVERY DATA SHEET 

Reference Method / Sampling Trai n : (A, o a d~ 3 f\ 

Recovered by: ^^fiYllS Recovered by: ZT- Recovered by: <£• kH«> I^-K-U 

RunNo.tU'Rt Date: ixjflo i Run No. U3L-rt-2-Date : Run No.U/J^tf-3 Date: 

XAJD Module No.: C<jWs.^rV>1 UMT XAD Module No.: (kV<A ^OfO°l l U (f XAD Module No.: A o ^ / / ^ 

Filter No.: <£f= - Pci~o\IK*4 Filter No.: fdL-'cA««Oo Filter No.: fipL-cj>*~~~JIm pinger No. and Volume Im pinger No. and Volume lm pinger No. and Volume 

No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) No. 

Initial 

(mL) 

Final 

(mL) 

Rinse 

(mL) 

1 

0 

1 0 1 d 

2 2 pro 2 IP* 

3 0 °[( / 3 0 

\ 

3 0 

3 •N / 

4 4 

1 

4 

5 A f t - 0 

6 i As**/' 

< r ^ 

6 ' 

7 7 7 

DIFF: DIFF : 

7 

DIFF: 

Totals 3.0 \<° Totals Totals 

Initial 

• (g) 

Final 

(g) 

Initial 

(g) 

Final 

(g) 

i Initial 

(g) 

Final 

(g) 

Initial 

• (g) 

Final 

(g) DIFF 

Initial 

(g) 

Final 

(g) DIFF 

i Initial 

(g) 

Final 

(g) DIFF: 

Silica 

Gel . 3 ^ m i 35.H 

Silica 

Gel 

Silica 

Gel 

Final Net Moisture Gain: •205I. *! Final Net Moisture Gain: Final Net Moisture Gain: 

ft IKr ; L*;i/" /WcM j 

VES018065 

C:\Documents and SeKings\milos\Oesktop\[lvloisture Recovery.xls] A 
Method 25A 

VES018066 
AVERAGE

D CEM DATA Jo

b Nurnber: 6013 

Run ID: R1B 

Date Time THC 

12/8/2009 12:32:00 0.58 

12/8/2009 12:34:00 0.55 

12/8/2009 12:36:00 0.52 

12/8/2009 12:38:00 0.45 

12/8/2009 12:40:00 0.38 

12/8/2009 12:42:00 0.46 

12/8/2009 12:44:00 0.41 

12/8/2009 12:46:00 0.46 

12/8/2009 12:48:00 0:5 

12/8/2009 12:50:00 0.42 

12/8/2009 12:52:00 0.39 

12/8/2009 12:54:00 0.46 

12/8/2009 12:56:00 0.41 

12/8/2009 12:58:00 

j 0.49 

12/8/2009 13:00:00 

j 0.52 

12/8/2009 13:02:00 

I 0.5 

12/8/2009 13:04:00 | 0.52 

12/8/2009 13:06:00 

; 0.46 

12/8/2009 13:08:00 0.52 

12/8/2009 13:10:00 0.51 

12/8/2009 13:12:00 0.54 

12/8/2009 13:14:00 0.54 

12/8/2009 13:16:00 0.55 

12/8/2009 13:18:00 0.54 

12/8/2009 13:20:00 0.5 

12/8/2009 13:22:00 0.54 

12/8/2009 13:24:00 0.53 

12/8/2009 13:26:00 0.51 

12/8/2009 13:28:00 0.52 

12/8/2009 13:30:00 0.51 

Average Value: 0.49 

Corrected Average: .35 

Start Time: 12:30:00 

Start Date: 12/08/09 

VES018067 
AVERAGE

D CEM DATA

 Job Number: 6013321 6 

Run ID: R2B 

Start Time: 13:49:00 

Start Date: 12/09/09 

Date Time THC 

12/9/2009 13:51:00 0.29 

12/9/2009 13:53:00 0.27 

12/9/2009 13:55:00 0.28 

12/9/2009 13:57:00 0.24 

12/9/2009 13:59:00 0.31 

12/9/2009 14:01:00 0.29 

12/9/2009 14:03:00 0.27 

12/9/2009 14:05:00 0.27 

12/9/2009 14:07:00 0.2 

12/9/2009 14:09:00 0.27 

12/9/2009 14:11:00 0.32 

12/9/2009 14:13:00 0.29 

12/9/2009 14:15:00 0.29 

12/9/2009 14:17:00 0.21 

12/9/2009 14:19:00 0.23 

-12/9/2009 14:21:00 0.25 

12/9/2009 ' 14:23:00 0.22 

12/9/2009 14:25:00 0.21 

12/9/2009 14:27:00 0.22 

12/9/2009 14:29:00 0.21 

12/9/2009 14:31:00 0.23 

12/9/2009 14:33:00 0.2 

12/9/2009 14:35:00 0.3 

12/9/2009 14:37:00 0.35 

12/9/2009 14:39:00 0.23 

12/9/2009 14:41:00 0.28 

12/9/2009 14:43:00 0.33 

12/9/2009 14:45:00 0.34 

12/9/2009 14:47:00 0.28 

12/9/2009 14:49:00 0.27 

Average Value: 0.27 

Corrected Average: .16 

VES018068 
AVERAGE D CE M DATA Job Number: 60133216 Start Time: 14:00:00 

Run ID: R3B Start Date: 12/10/09 

Date Time THC 

.12/10/2009 14:02:00 0.46 

12/10/2009 14:04:00 0.51 

12/10/2009 14:06:00 0.43 

12/10/2009 14:08:00 0.43 

12/10/2009 14:10:00 0.39 

12/10/2009 14:12:00 0.48 

12/10/2009 14:14:00 0.38 

12/10/2009 14:16:00 0.41 

12/10/2009 14:18:00 0.38 

12/10/2009 14:20:00 0.39 

12/10/2009 14:22:00 0.39 

12/10/2009 14:24:00 0.43 

12/10/2009 14:26:00 0.42 

12/10/2009 1.4:28:00 0.35 

12/10/2009 14:30:00 0.45 

12/10/2009 14:32:00 0.4 

12/10/2009 14:34:00 0.37 

12/10/2009 14:36:00 0.31 

12/10/2009 14:38:00. 0.38 

12/10/2009 14:40:00 0.35 

12/10/2009 14:42:00 0.35 

12/10/2009 14:44:00 0.34 

12/10/2009 14:46:00 0.37 

12/10/2009 14:48:00 0.36 

12/10/2009 14:50:00 0.31 

12/10/2009 14:52:00 0.29 

12/10/2009 14:54:00 0.3 

12/10/2009 14:56:00 0.28 

12/10/2009 14:58:00 0.29 

12/10/2009 15:00:00 0.35 

Average Value: 0.38 

Corrected Average: .09 

VES018069 
I 

i 

I 

o 

VES018070 
AECOM 

5 

Appendix C 

Reference Method Calibrations, Verifications, and Certifications 

VES018071 
Calibrator: Mike O'toole Reference Thermometer: SYR-CAL-1 

Filter Box Calibration 

Hot Box #5 HotBox#8D 

Manufacturer: 

Serial No.: 

Date received/placed in servic 

Anderson NUTECH 

N/A 

Pre 1995 

Manufacturer: 

Serial No.: 

Date received/placed in servic 

Anderson NUTECH 

N/A 

Pre 1995 

Calibration Date: 8-Jan-09 Calibration Date: 8-Jan-09 

Ambient Hot Ambient Hot 

Reference Temperatures 67 250 Reference Temperatures 69 250 

Actual Temperatures 66 249 Actual Temperatures 69 249 

Temp Difference (tol. = +-2) 1 1 Temp Difference (tol. = +-2) 0 1 

Hot Box #6 Hot Box #9 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: N/A Serial No.: N/A 

Date received/placed in servic Pre 1995 Date received/placed in servia Pre 1995 

Calibration Date: 8-Jan-09 Calibration Date: 8-Jan-09 

Ambient Hot Ambient Hot 

Reference Temperatures 69 250 Reference Temperatures 68 251 

Actual Temperatures 69 250 Actual Temperatures 66 250 

Temp Difference (tol. = +-2) 0 0 Temp Difference (tol. = +-2) 0 1 

Hot Box #7 Hot Box #10 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: N/A Serial No.: N/A 

Date received/placed in servic Pre 1995 Date received/placed in servio Pre 1995 

Calibration Date: 8-Jan-09 Calibration Date: 8-Jan-09 

Ambient Hot Ambient Hot 

Reference Temperatures 68 250 Reference Temperatures 71 250 

Actual Temperatures 69 249 Actual Temperatures 71 250 

Temp Difference (tol. = +-2) -1 1 Temp Difference (tol. = +-2) 0 0 

Hot Box #7A Hot Box #11 

Mianufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: 

Date received/placed in servic 

N/A 

Pre 1995 

Serial No.: 

Date received/placed in servic 

N/A 

Pre 1995 

Calibration Date: 8-Jan-09 Calibration Date: 7-Jan-09 

Ambient Hot Ambient Hot 

Reference Temperatures 69 250 Reference Temperatures 70 251 

Actual Temperatures 69 249 Actual Temperatures 69 250 

Temp Difference (tol. = +-2) 0 1 Temp Difference (tol. = +-2) 1 1 

Hot Box #8 

Manufacturer: 

Serial No.: 

Date received/placed in servic 

Anderson NUTECH 

N/A 

Pre 1995 

Calibration Date: 8-Jan-09 

Ambient Hot 

Reference Temperatures 69 250 

Actual Temperatures 69 248 

Temp Difference (tol. = +-2) 0 2 

Checked amph connector, t-couple and plugs 

QC checked by S Milo 2/9/09 

VES018072 
AZCOM 

Calibrator: 

Date: 

Steven Milo Reference Thremometer ID: CL-1000 

12/16/2008 

Last Impinger Thermocouple Calibration 2007 

Thermocouple Reference Difference (+/-2"> Thermocouple Reference Difference (+/-2°) 

LI-1 Hot 210 212 -2 LI-18 Hot 210 212 -2 LI-1 

Cold 32 33 -1 

LI-18 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 T-couple 2006 Date received/placed in service: Pre 1990 

LI-3 Hot 211 213 -2 LI-20 Hot 211 212 -1 LI-3 

Cold 32 32 0 

LI-20 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

LI-4 Hot 212 213 -1 LI-22 Hot 213 212 1 LI-4 

Cold 32 32 0 

LI-22 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 T-couple 2006 Date received/placed in service: Pre 1990 

LI-8 Hot 212 213 -1 LI-22A Hot 210 212 -2 LI-8 

Cold 32 32 0 

LI-22A 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

Hot 0 LI-24 Hot 210 212 -2 

Cold 0 

LI-24 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

Hot 0 LI-2S Hot 212 212 O 

Cold 0 

LI-2S 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No,: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

LI-13 Hot 210 212 -2 LI-28 Hot 213 212 1 LI-13 

Cold 33 32 1 

LI-28 

Cold 32 32 0 

Manufacturer: Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

LI-15 Hot 210 212 -2 LI-15 

Cold 32 32 0 

Manufacturer Anderson NUTECH 

Serial No.: 

Date received/placed in service: Pre 1990 

After calibration shower heads were cleaned and leak checked 

QC check S. Milo 

VES018073 
Calibrator: 

Date: 

Bill Hardy 

1/18/2010 

Reference Thremometer ID: CL-1000 

Last Impinqer Thermocouple Calibration 2007 

Thermocouple Reference Difference (+/-2°) Thermocouple Reference Difference (+/- 2°) 

LI-1 Hot 210 212 -2 LI-20 Hot 211 212 -1 LI-1 

Cold 32 32 0 

LI-20 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 T-couple 2006 Date received/placed in service: Pre 1990 

Li-3 Hot 212 212 0 LI-22 Hot 211 212 -1 Li-3 

Cold 32 32 0 

LI-22 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

LI-4 Hot 210 212 -2 LI-22A Hot 211 212 -1 LI-4 

Cold 32 32 0 

LI-22A 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 T-couple 2006 Date received/placed in service: Pre 1990 

LI-13 Hot 212 212 0 LI-24 Hot 211 212 -1 LI-13 

Cold 33 32 1 

LI-24 

Cold 33 32 1 

Manufacturer: Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date receivedfolaced in service: Pre 1990 

LM5 Hot 211 212 -1 LI-25 Hot 210 212 -2 LM5 

Cold 33 32 1 

LI-25 

Cold 33 32 1 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

LI-18 Hot 210 212 -2 LI-28 Hot 211 212 -1 LI-18 

Cold 33 32 1 

LI-28 

Cold 32 32 0 

Manufacturer: Anderson NUTECH Manufacturer: Anderson NUTECH 

Serial No.: Serial No.: 

Date received/placed in service: Pre 1990 Date received/placed in service: Pre 1990 

After calibration shower heads were cleaned and leak checked 

QC check S. Milo 

VES018074 
M5 Thermocouple Calibrations - 2009 

Date: 12/16/08 Calibrator: Steven Milo 

BP: 30.08 Ambient Temp (F): 65 

Reference Thermometer ID#: CL-1000 Fluke Digital RTD 2131035 

Manufacture: Fluke 

Date placed in Service: Pre 1980 

Ice Bath Boiling Water 

Thermocouple 

ID# 

Reference 

Temp 

' XA D 

Temp 

Temp 

Difference 

Tol = +-2 F 

Reference 

Temp 

X AD 

Temp 

Temp 

Difference 

Tol = +- 2 F 

M5-TC1 212 212 0 32 33 1 

M5-TC2 212 211 -1 32 33 1 

XAD-6 32 32 0 213 212 -1 

XAD-7 32 32 0 213 212 -1 

Q C check S. Milo 

VES018075 
AsCOM 

M5 Thermocouple Calibrations - 2010 

Date: 1/17/2010 

BP: 30.08 

Reference Thermometer ID#: 

Manufacture: 

Date placed in Service: 

Calibrator: Bill Hardy 

Ambient Temp (F): 65 

CL-1000 Fluke Digital RTD 2131035 

Fluke 

Pre 1980 

Ice Bath Boiling Water 

Thermocouple 

ID# 

Reference 

Temp 

X A D 

Temp 

Temp 

Difference 

Tol = +- 2 F 

Reference 

Temp 

X A D 

Temp 

Temp 

Difference 

Tol = +- 2 F 

M5-TC1 32 33 1 212 212 0 

M5-TC2 32 33 1 212 211 -1 

XAD-6 32 32 0 213 212 -1 

XAD-7 32 32 0 212 212 0 

Q C check S. Milo 

VES018076 
AZCOM 

DRY GAS METER CALIBRATION 

Meter Box No.: 2 

Chack one: 

Annua) Calibration Recalibration 

bate: 7/10/2009 

Operator: S. Milo 

Barometric Pressure: 29.81 (in Hq) 

Theoretical Critical Vacuum: 14.06 (in Hg) 

Manufacturer. Environmental Supply 

Date Received/Placed in service: 2002 

Serial No.: 2 

Pretest Leak Checks 

Allowable Actual 

Positive 0 0.00 

(at 5-7in. H;0) in. H20 per min. 

Negative 0 0,000 -

(at 3 In. H9) cfm _^ cfm 

DRY GAS METER DATA •CRITICAL ORIFICE DATA 

Volume Temp critical K Orifice Actual Ambient Temperature 

4H Time Initial Final Total Initial Rnal Orifice Calibratiot Vacuum Initial Final Average 

(in HjO) (min) (ft!

) (ft5

) (ftJ

) °F °F Serial f Coefficien (In Ha) °F °F °F 

0.29 20 0.050 6.378 6.326 71 73 40 0.240 24 70 71 71 

0.64 15 6.402 13.325 6.923 72 76 48 0.350 22.5 72 72 72 

1.15 15 13.396 22.533 9.137 75 77 55 0.460 21 73 72 73 

1.90 10 22.577 30.451 7.874 77 79 63 0.594 19 73 72 73 

3.70 10 30.507 41.271 10.764 78 82 73 0.809 16 73 74 74 

CORRECTED VOLUME 

OryGas Critical DRY GAS METER DRY GAS METER 

Meter Orifice 'CALIBRATION CALIBRATION 

Vm (std ft3) Ver (std ft1) FACTOR Y FACTOR Um 

6,259 6.212 0.993 0.001 1.691 -0.111 

6.831 6.779 0.992 0.00 1.762 -0.039 

8.989 8.919 0.992 0.00 1.830 0.O28 

7.732 7.668 0,992 0.00 1.818 0.02 

10.582 10.446 0.987 0.00 1.907 0.11 

Avg. Y 0.991 Avg. AH@ 1.801 

1) For valid test results, the Actual Vacuum should be 1 to 2 In. Hg greater than the Theoretical Critical Vacuum shown above. 

2) The Critical Orifice Coefficient, K\ must be entered in English units, (ft)*3*(deg R)*0.5/{(ir>.Hg)*(min)). 

3) The minimum number of sample volume required per orifice is 5 cubic feet 

4) For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, acceptable tolerance of individual values from the average is ±0.02 

5) For Orifice Calibration Factor AH@, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air at 68 F and 28.92 inches of Hg, 

acceptable tolerance of Individual values from the average is ± 0.2. 

Dry Gas Meter Thermocouple Calibration 

Ref.TCIO* REF -SYR -TC2 MetfO*: 002-IN Outlet lot* 002-OUT 

Ref. Source Ref.'F °f 4 °e A 

Amb. Air 65 66 -1 66 1 

Hot Water 118 118 0 117 -1 

Potentiometer Calibration 

Low 100'F 99 

Mid 400 "F 400 

High 900 °F 899 

1) Hot Water to be in the range of 104 -122 °F. 

2) Tolerance allowed for all thermocouple individual readings: ± 5,4 °F 

3) Tolerance allowed for all potentiometer individual readings: ± 2 °F 

= 17 .«<?,)—liA _

 vcr(al) 

' m(Hd) 

.750 

cr[s!d) 
AECOM 

SAMPL E PROB E CALIBRATION DATA FOR M 

TYP E "S" PITOT TUB E ASSEMBL Y AN D NOZZLE 

Thermocouple Calibration 

j PROBE ID: j ENSR RTO #2131035 Omega CI10OO. #06022200 Omega CM COO. W06O222OO 

S-M54D 

•1 Furraeo poo-

 -

S-M54D 

»-—» » TC rTM '7 

rc Z rc 

? 

Date: 1/28(2309 

1 34 274 34 274 0 212 373 212 373 0.0 451 506 450 505 -0 1 

j S-M5-40 34 274 34 274 0 212 373 212 373 00 451 506 450 506 • 0 1 

i"*;;*V;r"

 st° 34 274 34 274 0 212 373 212 373 0.0 451 506 450 505 -0 1 i"*;;*V;r" st° 

34 274 34 274 0 212 373 212 373 0.0 451 506 450 505 .0 1 

Type "S" Pitot Tube Calibration: 

Level and Perpendicular 

Obstruction 

Damaged 

a, (-10° S a, s+ 10") 

a2 (-10° s a 2 ^ + 10°) 

fi, (-5°s a, < +5") 

fi2 (-5°< IJ2< *5') 

Y 

e 

z = ATany(±£ 0.125") 

W = ATana(±s 0.03125") 

D, (3/16 S D,s 3/8") 

A 

A72D, (1.05 s P A /D,s 1.5) 

Pitot Tube to Nozzle Calibration: 

jgg-i^°t>--«." 

} Pilot to nozzle separation 

j2) Therniocatpla lo ptlol separation 

i3) Pilot end to probe union distance 

Probe Information 

Manufacturer 

Date Received and placed In Service: 

Condition of Probe when placed in sen 

QA/QC Check 

Completeness _X _ Legib 

rtjfy that the Type Spitot tube/probe ID#__ 

criteria and/or applicable design features and 

iCertified by; Stevenlylilo 1/26/09 

Apex 

pre-1985 

NEW USED RECONDITIONED (circle one) 

Reasonableness 

meets or exceeds all Specifications 

. hereby assigned a pi to! tube calibration factor CD of 0.84 

Steven Milo 2/18/09 

Personnel (Sign a tore/Dale) Team Leader (Signature/Date) 

|AII construction criteria (or an isolated *S* type pilot are within given tolerances prescribed in 

SQuality Assurance Handbook for Air Pollution Measutement Systems: Volume III. Stationary Source-Specific Methods. 

EPA/6O07R-94/038c, September 1994 

VES018078 
AUCOM 

SAMPLE PROBE CALIBRATION DATA FORM 

TYPE "S" PITOT TUBE ASSEMBLY AND NOZZLE 

Thermocouple Calibration 

PROBE iO: 

ThofrvotncleMD i» 

ENSR RTO #2131035 Omega Cl 1000. #06022200 Omega C110O0. #06032200 

S-M5-5C 

fed Bait, Boiling Walcr Tube F.maco peer • W r, 

S-M5-5C TC 

tr 

TC T" 

'M 

«rn 

Date: U2&72U09 34 274 34 274 0 212 373 211 373 -0.1 450 505 447 504 -0 3 

S-M5-5C 34 274 34 274 0 212 373 211 373 -0 1 450 505 447 604 0 3 

34 274 34 274 0 212 373 211 373 -0.1 450 505 447 504 

---

34 274 34 274 0 212 373 211 373 -0.1

 1 450 505 447 504 -0 3 

Type "S" Pitot Tube Calibration: 

Level and Perpendicular 

Obstruction 

Damaged 

a, (-10°< ct,<* 10") 

(i2 (-10° < et 2 £ + 10°) 

(!, (-5" < R, 5 * 5°) 

B2 (-5° <Ej5t5') 

z = ATany(±£ 0.125") 

W = ATan0(iS 0.03125") 

D, (3/16 < D,s 3/8") 

A 

A/2D, (1.05 s PA/D,s 1.5) 

aetemlnlngT/then calculate z. 

Pitot Tube to Nozzle Calibration: 

ID, Tyw S mt* Tup. ^ | j ^> 

HSU— * in Ml 

1) P tot lo nozzle separalton 

2) Thermacouole lo p.tol be pal a Hun 

3) Pitot end to prabs union distance 

>3ifl"(w'E00 nozztei 

Probe Information 

Manufacturer: 

Date Received and placed In Service: 

Condition of Probe when placed in serv 

QA/QC Check 

Completeness X__ Legibi 

I certify that the Type S pilot tube'pro&e ID#_ 

pre-1.995. 

NEW USED RECONDITIONED (circle one) 

Specifications Reasonableness 

rileria and/or applicable design features and is hereby assigned a pilot tube calibration factor C, of 0.84 

;eeds all Specifications, 

Certified by: Steven Milo 1/29/09 

Personnel (Signature/Date) 

Sieven Milo 2/15/09 

Team Leader (Signature/Date) 

All construction criteria for an isolated "S" type pitot are within given tolerances prescribed in 

Quality Assurance Handbook for Air Pollution Measurement Systems: Volume ill, Stationary Source-Specific Methods. 

EPA/60O/R-94,O38c, September 1994 

VES018079 
DAILY CALIBRATION REPORT 

Date: 12/8/2009 

Start Time: 07:58:49 

End Time: 08:10:09 

Methods: 3A, 6C, 7E and 10 

Job Number: 60133216 

Span 

Param Value 

C02 11 

THC 10 

Calibration Error = 

System Bias = 

Mid-Gas 

Standard 

5.02 

5.10 

Analyzer 

Zero Response 

0.02 

N/A 

Analyzer 

Mid Response 

5.01 

N/A 

Zero 

Cal Error 

0.3% 

1.0% 

Mid 

Cal Error 

-0.1% 

0.2% 

System 

Zero Response 

0.06 

0.1 

System 

Mid Response 

5.06 

5.11 

100% x (Analyzer Response - Cylinder Gas Standard Value) / (Span Value) 

100% x (System Response - Analyzer Response) / (Span Value) 

For THC Measurements: 

Calibration Error = 100% x (System Response - Cylinder Gas Standard Value) / (Cylinder Gas Standard Value) 

System Bias = 100% x (System Response - Cylinder Gas Standard Value) / (Span Value) 

System 

Zero Bias 

0.3% 

1.0% 

System 

Mid Bias 

0.4% 

0.1% 

VES018080 
CALIBRATION CHEC K REPOR T Start Time: 11:16:23 

Run ID: R1B Date: 12/8/2009 End Time: 15:48:57 

EPA Methods: 3A, 6G, 7E and 10 

Job Number: 60133216 

Analyzer Analyzer System System System System System System System System 

Zero Mid Pre-Zero Pre-Mid Pre-Zero Pre-Mid Post-Zero Post-Mid Post-Zero Post-Mid 

Param Response Response Response Response Bias Bias Response Response Bias Bias Zero Drift Mid Drift 

C02 0.02 5.01 0.15 5.11 1.1% 0.8% 0.12 4.98 0.8% -0.3% -0.3% -1.1% 

THC N/A N/A 0.13 5.31 1.3% 2.1% 0.16 5.25 1.6% 1.5% 0.3% -0.6% 

System Blas= 100% x (System Response - Analyzer Response) / (Span Value) 

System Drift9 100% x (System Post Response - System Pre Response) / (Span Value) 

For THC Measurements: 

System Bias= 100% x (System Response - Cylinder Gas Standard Value) I (Span Value) 

System 

Avg-Zero 

Response 

0.14 

0.14 

System 

Avg-Mid 

Response 

5.05 

5.28 

VES018081 
DAILY CALIBRATION REPORT 

Date: 12/9/2009 

Start Time: 08:12:31 

End Time: 08:25:26 

Methods: 3A, 6C, 7E and 10 

Job Number: 60133216 

Span 

Param Value 

C02 11 

THC 10 

Calibration Error = 

System Bias = 

Mid-Gas 

Standard 

5.02 

5.10 

Analyzer 

Zero Response 

0.08 

N/A 

Analyzer 

Mid Response 

5 

N/A 

Zero 

Cal Error 

0.8% 

1.5% 

Mid 

Cal Error 

-0.2% 

1.9% 

System 

Zero Response 

0.14 

0.15 

100% x (Analyzer Response - Cylinder Gas Standard Value) / (Span Value) 

100% x (System Response - Analyzer Response) / (Span Value) 

For THC Measurements: 

Calibration Error = 100% x (System Response - Cylinder Gas Standard Value) / (Cylinder Gas Standard Value) 

System Bias = 100% x (System Response - Cylinder Gas Standard Value) / (Span Value) 

System 

Mid Response 

5.05 

5.19 

System 

Zero Bias 

0.5% 

1.5% 

System 

Mid Bias 

0.5% 

0.9% 

VES018082 
CALIBRATION CHECK REPORT 

Run ID: R2B Date: 12/9/2009 

Start Time: 10:57:03 

End Time: 17:11:27 

EPA Methods: 3A, 6C, 7E and 10 

Job Number: 60133216 

Analyzer Analyzer System System System System System System System System System 

Zero Mid Pre-Zero Pre-Mid Pre-Zero Pre-Mid Post-Zero Post-Mid Post-Zero Post-Mid Avg-Zero 

Param Response Response Response Response Bias Bias Response Response Bias Bias Zero Drift Mid Drift Response 

C02 0.08 5 0.09 4.98 0.0% -0.2% 0.1 5.09 0.2% 0.9% 0.1% 1.1% 0.09 

THC N/A N/A 0.06 5-1 0.6% 0.0% 0.16 5.08 1.6% -0.2% 0.9% -0.2% 0.11 

System Bias= 100% x (System Response - Analyzer Response) / (Span Value) 

System Drifts 100% x (System Post Response - System Pre Response) / (Span Value) 

For.THC Measurements: 

System Bias- 100% x (System Response - Cylinder Gas Standard Value) / (Span Value) 

System 

Avg-Mid 

Response 

5.04 

5.09 

VES018083 
DAILY CALIBRATION REPORT 

Date: 12/10/2009 

Start Time: 09:32:24 

End Time: 09:40:21 

Methods: 3A, 6C, 7E and 10 

Job Number: 60133216 

Span 

Param Value 

C02 11 

THC 10 

Calibration Error = 

System Bias = 

Mid-Gas 

Standard 

5.02 

5.10 

Analyzer 

Zero Response 

0.06 

N/A 

Analyzer 

Mid Response 

5.06 

N/A 

Zero 

Cal Error 

0.6% 

2.7% 

Mid 

Cal Error 

0.4% 

0.4% 

System 

Zero Response 

0.11 

0.27 

100% x (Analyzer Response - Cylinder Gas Standard Value) / (Span Value) 

100% x (System Response - Analyzer Response) / (Span Value) 

For THC Measurements: 

Calibration Error = 100% x (System Response - Cylinder Gas Standard Value) / (Cylinder Gas Standard Value) 

System Bias = 100% x (System Response - Cylinder Gas Standard Value) / (Span Value) 

System 

Mid Response 

5.12 

5.12 

System 

Zero Bias 

0.5% 

2.7% 

System 

Mid Bias 

0.5% 

0.2% 

VES018084 
CALIBRATION CHECK REPORT start Time: 12:12:30 EPA Methods: 3A, 6C, 7E and 10 

Run ID: R3B Date: 12/10/2009 End Time: 16:26:00 Job Number: 60133216 

Analyzer Analyzer System System System System System 

Zero Mid Pre-Zero Pre-Mid Pre-Zero Pre-Mid Post-Zero 

Param Response Response Response Response Bias Bias Response 

C02 0.06 5.06 0.17 5.39 1.0% 2.9% 0.04 

THC N/A N/A 0.39 5.04 3.9% -0.6% 0.19 

System Bias= 100% x (System Response - Analyzer Response) / (Span Value) 

System Drift= 100% x (System Post Response - System Pre Response) / (Span Value) 

For THC Measurements: 

System Bias- 100% x (System Response - Cylinder Gas Standard Value) / (Span Value) 

System System System System System 

Post-Mid Post-Zero Post-Mid Avg^Zero Avg-Mid 

Response Bias Bias Zero Drift Mid Drift Response Response 

5.11 -0.2% 0.4% -1.2% -2.5% 0.11 5.25 

5.29 1.9% 1.9% -2.0% 2.5% 0.29 5.16 

VES018085 
Initial THC Monitor Calibrations 

Plant I.D. 

Comments: Source I.EX 

Pollutant _ 

Date 

Project No. kotv^lk 

Operator J .dorrta^ 

Analyzer I.D. VJ j& - M 

Spa n Value i o 

Analyzer Serial No. 

Initial Calibration (Time ) 

Cylinder Valu e 

(ppm) 

Syste m 

Respons e 

(ppm) 

Predicted 

Valu e 

(ppm) 

System 

Respons e 

(ppm) 

Calibration 

Error 

(% of Span ) 

Zero Ga s O.O Of |Iil|il|lllf 

Low Level Ga s 

i 

2 57 2-ft - o.tf 

Mid Level Ga s liiiSiiillPisiSP 

- / 

High Level Ga s 

Cylinder I D. 

Zero Gas 

Low Level Gas 

Mid Level Gas 

High Level Gas 

Calibration Error (System Respons e - Predicted Value) X 100 

Calibration Ga s 

Predicted Valu e [ (High Respons e - Zero Respo n X Mid or Lo w Level Ga s ] + Zero Respons e 

High Level Ga s 

VES018086 
AZCO M Initial Monitor Calibrations 

Plant I.D. Ufol.d 

Comments: Source I.D. U N> , f 2 

Pollutant 

Date 

Project No. lg D\352 I b 

Operator j . Lar^c^ 

Co i Analyzer I.D. ^ i) 0 u£jc i^^jo 

Span Value (( 

Analyzer Serial No. 

Initial Calibration (Time ) 

Cylinder Value 

(ppm or %) 

Analyzer 

Respons e 

(ppm or %) 

Calibration 

Error 

(% of Span) 

System 

Response 

(ppm or %) 

System 

Bias 

(% of Span ) 

Zero Ga s 0 . 0 0-OT- D-oio 0 - 3 

Low Level Ga s — . — . — . 

Mid Level Ga s -0.1 

* 

High Level Ga s 

ICM G \io i 0-4S — 

- — 

Cylinder I.D. 

Zero Gas 

Low Level Gas 

— 

Mid Level Gas Sir mu5i 3 

High Level Gas 

Calibration Error (Analyzer Response - Cylinder Value) X 100 

Span Value 

System Bias = (System Respons e - Analyzer Response) X 100 

Span Value 

VES018087 
Initial THC Monitor Calibrations 

Plant I.D. VJft • CL 

Cornments: Source I.D^ 

Pollutant _ 

Date 

Project No. & oitfzilo 

Operator & . 6>ar MQ^i 

HC Analyzer I.D. UlV? M-ZO 

Spa n Valu e j p 

Analyzer Serial No. 

Initial Calibration (Time ) 

Cylinder Value 

(ppm) 

Syste m 

Respons e 

(ppm) 

Predicted 

Valu e 

(ppm) 

Syste m 

Respons e 

(ppm) 

Calibration 

Error 

(% of Span) 

Zero Ga s O-o 0 \ S 

Low Level Ga s 

a •> « 

Mid Level Ga s 5-1 5 r. i t 

High Level Ga s M3 

Cylinder I.D. 

Zero Gas Uli P -^ 1 

Low Level Ga s C C 2 \1 47 0 

Mid Level Gas 

High Level Ga s $6 Mrt f 

Calibration Error (System Respons e - Predicted Value) X 100 

Calibration Ga s 

Predicted Valu e [ (High Respons e - Zer o Respo n X Mid or Lo w Level Ga s ] + Zero Respons e 

High Level Ga s 

VES018088 
AECO M Initial Monitor Calibrations 

Plant I.D. 'J60i< a 

Comments: Source I.LT 

Pollutant _ 

Date 

Project No. foQlhlx \G 

Operator j -tor^o ^ 

Co 1 Analyzer I.D. Vr^^ * <vyo 

Span Value \ \ 

Analyzer Serial No. 

Initial Calibration (Time ) 

Cylinder Value 

(ppm or %) 

Analyzer 

Respons e 

(ppm or %) 

Calibration 

Error 

(% of Span) 

System 

Respons e 

(ppm or %) 

System 

Bias 

(% of Span) 

Zero Ga s 0-o% o x 

Low Level Ga s 

- — — — 

Mid Level Ga s S-OCSt C M 

High Level Ga s 10 0-1? — -

— 

Cylinder I.D. 

Zero Gas L» H ?- -0 3_ 

Low Level Gas — 

Mid Level Gas 

High Level Gas 

Calibration Error (Analyzer Respons e - Cylinder Value) X 100 

Span Value 

System Bias = (System Respons e - Analyzer Response) X 100 

Span Value 

VES018089 
AECO M Initial Monitor Calibrations 

Plant I.D. a. 

Comments. Source I.D^ 

Pollutant _ 

Date 

Project No. Lol¥>2/L 

Operator ~J. Lcrrtct^J 

Co 

il- \ Q-oL 

Analyzer I.D. Scryon ?y: n/t/p 

Span Value jo 

Analyzer Serial No. 

Initial Calibration (Time ) 

Cylinder Value 

(ppm or %) 

Analyzer 

Respons e 

(ppm or %) 

Calibration 

Error 

(% of Span) 

System 

Response 

(ppm or %) 

System 

Bias 

(% of Span) 

Zero Ga s 

o n O S 

Low Level Ga s — 

— 

Mid Level Ga s S ".| 2 

High Level Ga s )0M 0 - 5 — — 

Cylinder I.D. 

Zero Gas 

Low Level Gas 

Mid Level Gas 

High Level Gas c c Hosgx 

Calibration Error (Analyzer Respons e - Cylinder Value) X 100 

Spa n Value 

System Bias = (System Respons e - Analyzer Response) X 100 

Spa n Valu e 

VES018090 
AECOM Initial THC Monitor Calibrations 

Plant I.D. o i > a. 

Comments : Source I.D_ U \~ 'X 

Pollutant 

Date 

MC 

Project No. hbil'b'xiL* 

Operator ~Z •WacMo-.-^ 

Analyzer I.D. (1 (6 - aA-IO 

Span Value )Q 

Analyzer Serial No._ 

Initial Calibration (Time ) 

Cylinder Value 

(ppm) 

System 

Response 

(ppm) 

Predicted 

Value 

(PPm) 

System 

Response 

(ppm) 

Calibration 

Error 

(% of Span) 

Zero Gas 0 • 0 

Low Level Gas - 4.24= 

Mid Level Gas 5,13 3 

High Level Gas 

Cylinder I.D. 

Zero Gas U HP-^ riLow Level Gas CC DH mo 

Mid Level Gas Cfr <iiO 11555 

High Level Gas 

Calibration Error (System Response - Predicted Value) X 100 

Calibration Gas 

Predicted Value f (High Response - Zero Respon X Mid or Low Level Gas ] + Zero Response 

High Level Gas 

VES018091 
I 

I 

I 

J 

t 

i 

VES018092