Instructions for filling the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data fro

fuel burning power plants and which test methods were used to do so for cases where the test methods are not 

supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in t

if you do not have access to a lab which performs methods that are in the ERT. Constituents of concern are: Car

Monoxide, Formaldehyde, Methane, Speciated Volatile Hazardous Air Pollutants (HAPs), Speciated Semi

HAPs, Sulfer Dioxide, Oxygen, Carbon Dioxide, Hydrogen Cyanide, Nitrogen Oxides, Total Dissolved Solids (TDS), 

Suspended Solids (TSS). You must complete 3 separate sampling events for each of the requested constituents. 

spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled b

separate copies of this spreadsheet. Fields shaded in yellow are required. All cells that are shaded in light gree

populated using drop-down lists. You do not need to populate cells shaded in gray, as they are automatically po

from the Boiler Information worksheet. Please Do Not modify the structure of this spreadsheet by adding or su

rows, columns, cells. Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information wo

2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family requred for this analysis. 

spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission 

results. There are generally 1 to 3 emission test results records to be entered depending on the constiuent or co

family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter bot

Hg+2, or if the Ontario-Hydro Method was used, you would need to enter Hg0, HgP, and Hg

Specieated Volatile Organic HAP and Speciated Semi-Volatile Organic HAP worksheets allow you to use a drop

provided in the Constituent field to define as many records as needed to record each HAP that you have results f

General instructions follow for these worksheets:

Boiler Operation Information

1. Please determine which units of measure (acfm or dscfm) were used for Exhaust Flow Rate and which units o

(deg C or deg F) were used for Exhaust Temperature. Fill these units of measure into the Units of Measure field.

2. Please provide the values of all requested parameters for each of the 3 sample testing periods in the Sample 

2, and Sample 3 fields.

3. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop-downs in the Fuel Type Selection 

You may enter up to 4 fuel types. Then, enter the input rate of each fuel in the Sample 1, Sample 2, and Sample 

If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of 
If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of 

2. Please enter the unit of measure using the drop down provided.

3. Please enter the test method used to determine the fuel input rate.

4. Please provide any other information that you feel may be important in the Other Supporting Information fie

Emission Data

1. Some constituents ask for the emission rate results of each of the 3 samples in two different units of measure

others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds p

BTU) and ppmvd @ 7% O2(parts per million by volume dry basis at 7 percent oxygen)), you are required to prov

2. Please provide the test method used. This may or may not match the example given in the Test Method Used 

Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010).

3. Please provide any other information that you feel may be important in the Other Supporting Information fie

4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for p

enter these data.
nformation about emission data from fossil 

ses where the test methods are not currently 

nly be used if the method is not in the ERT or 

T. Constituents of concern are: Carbon 

ants (HAPs), Speciated Semi-Volatile Organic 

Oxides, Total Dissolved Solids (TDS), and Total 

each of the requested constituents. This 

multiple boilers should be handled by using 

All cells that are shaded in light green are 

in gray, as they are automatically populated 

 of this spreadsheet by adding or subtracting 

wing naming convention: 

misTestMethods.xls).

boiler on the Boiler Information worksheet. 

ent family requred for this analysis. On each 

fuel input information, and emission test 

d depending on the constiuent or constituent 

Mercury requires that you enter both Hg0 and 

, and Hg+2. However, both the 

orksheets allow you to use a drop-down 

ord each HAP that you have results for. 

xhaust Flow Rate and which units of measure 

ure into the Units of Measure field.

mple testing periods in the Sample 1, Sample 

er Supporting Information field.

downs in the Fuel Type Selection field. 

he Sample 1, Sample 2, and Sample 3 fields. 

samples, then enter an input rate of zero. 
samples, then enter an input rate of zero. 

he Other Supporting Information field.

es in two different units of measure, while 

f measure (ex. lb/MMBtu (Pounds per million 

t oxygen)), you are required to provide both.

mple given in the Test Method Used field. 

ethod (ex. U.S. EPA Method 0010).

he Other Supporting Information field.

 method you are entering data for please also 
EIA Facility Code Facility Name Boiler ID Control Device Configuraton

6042 Manatee PMT2 Listed (by boiler) in Question 16 (page 17) of the questionnaire

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Boiler Information
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/11/2010 5/11/2010

Steam Output (1000 lb/hr) 5327 5325 5329 1000 lb/hr

Total Heat Input (MMBtu/hr) 7506 7508 7514 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 9.216040761 9.216040761 9.216040761 %

Exhaust Flow Rate (acfm or dscfm) 1469055.512 1474423.975 1481305.477 dscfm

Exhaust Temperature (deg C or deg F) 320 320 320 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 1,001 1,001 1,002 gallon/minute gas fuel meter

Emission Test Results

Formaldehyde 

Emission Rate 

Sample 1 (lb/MMBtu)

Formaldehyde 

Emission Rate 

Sample 1 

(ppmvd @ 7% O2)

Formaldehyde 

Emission Rate 

Sample 2 (lb/MMBtu)

Formaldehyde 

Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

Formaldehyde 

Emission Rate 

Sample 3 (lb/MMBtu)

Formaldehyde 

Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA

Method 320)

Other Supporting 

Information

0 0.00 2.39678E-05 0.02 0 0.00 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Formaldehyde Emission Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/11/2010 5/11/2010

Steam Output (1000 lb/hr) 5327 5325 5329 1000 lb/hr

Total Heat Input (MMBtu/hr) 7506 7508 7514 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 9.216040761 9.216040761 9.216040761 %

Exhaust Flow Rate (acfm or dscfm) 1469055.512 1474423.975 1481305.477 dscfm

Exhaust Temperature (deg C or deg F) 320 320 320 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 1,001 1,001 1,002 gallon/minute gas fuel meter

Emission Test Results

Methane Emission Rate 

Sample 1

 (lb/MMBtu)

Methane Emission Rate 

Sample 1

(ppmvd @ 7% O2)

Methane Emission Rate 

Sample 2 

(lb/MMBtu)

Methane Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

Methane Emission Rate 

Sample 3 

(lb/MMBtu)

Methane Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA

Method 18)

Other Supporting 

Information

0.000517353 0.90 0.000634846 1.11 0.00072351 1.26 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls CH4 Emission Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 8/6/2010 8/6/2010 8/6/2010

Steam Output (1000 lb/hr) 5426 5438 5440 1000 lb/hr

Total Heat Input (MMBtu/hr) 7675 7684 7707 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 6.4 6.2 6.01 %

Exhaust Flow Rate (acfm or dscfm) 0 0 0 dscfm

Exhaust Temperature (deg C or deg F) 332 339 337 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 416900 417400 418600 lb/hour gas fuel meter

Emission Test Results

Total Vapor Phase 

Mercury Emission Rate 

Sample 1

 (lb/MMBtu)

Total Vapor Phase 

Mercury Emission Rate 

Sample 2 

(lb/MMBtu)

Total Vapor Phase 

Mercury Emission Rate 

Sample 3 

(lb/MMBtu)

Test Method Used

(ex. U.S. EPA

Method 30B)

Other Supporting 

Information

6.03E-08 6.04E-08 5.48E-08 U.S. EPA Method 30BADL

Data Sheets and QA/QC Documentation

Total Mass (ng)

trap ID Section 1 Section 2 Sections 1+2 (ng) (ug)

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train A OL 59023 5.83 0.28 6.11 0.00 6.11 0.006110

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train B OL 71904 15.08 0.44 15.52 10.00 5.52 0.005520

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train A OL 59046 5.89 0.43 6.32 0.00 6.32 0.006320

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train B OL 70148 15.56 0.26 15.82 10.00 5.82 0.005820

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train A OL 59010 5.81 0.58 6.39 0.00 6.39 0.006390

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train B OL 71930 15.17 0.13 15.30 10.00 5.30 0.005300

Start Stop per tube per run per tube per run per tube per run

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train A 8/6/2010 8:22 10:22 0.063252992 6.33E-02 0.000485467 4.85E-04 0.002126344 2.13E-03

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train B 8/6/2010 8:22 10:22 0.057357793 5.74E-02 0.000440221 4.40E-04 0.001928168 1.93E-03

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train A 8/6/2010 10:43 12:43 0.062338002 6.23E-02 0.000479005 4.79E-04 0.002098043 2.10E-03

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train B 8/6/2010 10:43 12:43 0.058370103 5.84E-02 0.000448516 4.49E-04 0.001964500 1.96E-03

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train A 8/6/2010 13:03 15:03 0.059389100 5.94E-02 0.000457712 4.58E-04 0.002004778 2.00E-03

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train B 8/6/2010 13:03 15:03 0.050297488 5.03E-02 0.000387643 3.88E-04 0.001697875 1.70E-03

Averages 0.058500913 0.000449761 0.001969951

Average R Vol. diff (%) Limit Abs. diff. (μg/dscm) % Limit

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train A 0.080

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train B 0.080 0.370831136

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train A 0.083

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train B 0.081 1.651368660

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train A 0.087

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train B 0.085 2.065557229

% Limit Crec R (%) by Run R (%) by program Limit

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train A 4.802744425

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-1-Train B 8.661417323

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train A 7.300509338

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-2-Train B 4.676258993

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train A 9.982788296

fpl-10-pmt.fl-icr#1-Hg30B-PMT2-1-3-Train B 2.51450677 0.106558438 90.41989107

0.009091612 8.288717686

Run ID Sorbent Trap Breakthrough (B) Measured Spike Recovery ( R )

≤ 10% of Section 1 Hg 

mass for Hg conc. >1 

μg/dscm: or ≤ 20% of 

Section 1 for Hg conc.≤1 

μg/dscm

0.118526151 94.32657782

93.5967113

Average Recovery, 

between 85 and 

115% 0.11808977 96.04366499

≤20% of field recovery 

test

0.005895199 4.887787462 ≤10 % RD mass for 

Hg conc. >1 

μg/dscm: or ≤20% 

RD or ≤0.2 μg/dscm 

abs.diff. for Hg conc. 

≤1 μg/dscm

0.003967898 3.287184681

Hg Emissions(lb/Tbtu) Hg Emissions (lb/hr)

Paired Trap Agreement (RD)

Summary of M30B Quality Assurance Checks

Run ID Volume Sampled (dscm)

Hg Emissions (lb/yr)*

Summary of Hg Collected on Sorbent Traps via Method 30B

Run ID

Appartioned Mass (ng) Initial Spike (ng) Total Non-spike

Individual Sorbent Tube Emission Summary, Method 30B

Run ID Test Date Run Time

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Hg Emission Data-30B
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/13/2010 5/13/2010

Steam Output (1000 lb/hr) 5326 5318 5324 1000 lb/hr

Total Heat Input (MMBtu/hr) 7489 7502 7510 MMBtu/hr

Basis (Wet/Dry) Wet Wet Wet N/A

Exhaust Steam % Moisture 4.99 5.04 5.11 %

Exhaust Flow Rate (acfm or dscfm) 1587453.955 1740618.358 1646575.965 dscfm

Exhaust Temperature (deg C or deg F) 314.50 318.25 319.17 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 409300 410000 410400 lb/hour gas fuel meter

Compound 

(use drop down to define for as many

rows as needed)

Volatile Organic HAP 

Emission Rate Sample 

1 

(lb/MMBtu)

Volatile Organic HAP 

Emission Rate Sample 

1 

(μg @ 7% O2)

Volatile Organic 

HAP Emission Rate 

Sample 2 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 2

(μg @ 7% O2)

Volatile Organic 

HAP Emission 

Rate Sample 3 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 3

(μg @ 7% O2) Test Method Used Other Supporting Information

Dichlorodifluoromethane [<2.44E-06] [<2.83] [<2.67E-06] [<3.09] [<3.83E-06] [<4.44] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]

Chloromethane [<2.47E-06] [<2.86] [<1.63E-06] [<1.89] [<1.64E-06] [<1.9] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.03+[<0.02]; 0.03+[<0.

Vinyl Chloride [<1.73E-06] [<2] [<1.58E-06] [<1.84] [<1.59E-06] [<1.84] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]

Bromomethane [<1.93E-06] [<2.24] [<1.63E-06] [<1.89] [<1.64E-06] [<1.9] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]

Chloroethane [<1.92E-06] [<2.22] [<1.63E-06] [<1.89] [<1.64E-06] [<1.9] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]

Trichlorofluoromethane [<1.92E-06] [<2.22] [<1.63E-06] [<1.89] [<1.64E-06] [<1.9] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]

Carbon Disulfide [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Acetone [<1.59E-05] [<18.44] [<6.28E-06] [<7.28] [<6.02E-06] [<6.98] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.12+0.07; 0.12+0.06; 0

1,1-Dichloroethene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Iodomethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Methylene Chloride [<1.22E-05] [<14.19] 1.2E-05 13.95 1.97E-05 22.86 U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.01+0.02; 0.01+0.04; 0

trans,1,2-Dichloroethene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Vinyl Acetate [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,1-Dichloroethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

2-Butanone [<9.63E-06] [<11.17] [<2.69E-06] [<3.12] [<2.75E-06] [<3.19] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.03+[<0.01]; 0.03+[<0.

cis,1,2-Dichloroethene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Chloroform [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,1,1-Trichloroethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Carbon Tetrachloride [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,2-Dichloroethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Benzene [<1.22E-05] [<14.1] [<1.09E-06] [<1.26] [<9.09E-07] [<1.05] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.21+0.02; 0.21+0.03; 0

Trichloroethene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,2-Dichloropropane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Dibromomethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Bromodichloromethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

cis,1,3-Dichloropropene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

trans,1,3-Dichloropropene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

4-Methyl-2-Pentanone [<8.44E-06] [<9.78] [<2.69E-06] [<3.12] [<2.7E-06] [<3.13] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,1,2-Trichloroethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Chlorodibromomethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

2-Hexanone [<8.63E-06] [<10] [<2.69E-06] [<3.12] [<2.7E-06] [<3.13] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Toluene [<1.68E-05] [<19.45] [<4.21E-06] [<4.88] [<6.35E-06] [<7.37] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): 0.33+0.01; 0.33+0.01; 0

Tetrachloroethene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Ethylene Dibromide [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Chlorobenzene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,1,1,2-Tetrachloroethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Ethylbenzene [<1.05E-06] [<1.22] [<1.22E-06] [<1.42] [<1.6E-06] [<1.86] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

M&P-Xylene [<2.69E-06] [<3.11] [<2.4E-06] [<2.78] [<2.41E-06] [<2.79] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.03]+[<0.03]; [<0.03]

O-Xylene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Styrene [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Bromoform [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,1,2,2-Tetrachloroethane [<9.59E-07] [<1.11] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B BDL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

1,2,3-Trichloropropane [<1.29E-06] [<1.49] [<8.16E-07] [<0.95] [<8.2E-07] [<0.95] U.S. EPA Method 0031 with SW-846 Method 8260B DLL: Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]

Run 1 Comments:

Speciated Volatile Organic HAP Emission Data

Note: Acetone and methylene chloride were observed in the laboratory

blank. Laboratory notes indicate the elevated acetone, methylene 

chloride, and toluene levels may be due to contamination in the field.

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Spec Volit Org HAP Emis Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/13/2010 5/13/2010

Steam Output (1000 lb/hr) 5326 5318 5324 1000 lb/hr

Total Heat Input (MMBtu/hr) 7489 7502 7510 MMBtu/hr

Basis (Wet/Dry) Wet Wet Wet N/A

Exhaust Steam % Moisture 4.99 5.04 5.11 %

Exhaust Flow Rate (acfm or dscfm) 1587453.955 1740618.358 1646575.965 dscfm

Exhaust Temperature (deg C or deg F) 314.50 318.25 319.17 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 409300 410000 410400 lb/hour gas fuel meter

Compound 

(use drop down to define for as many

rows as needed)

Volatile Organic HAP 

Emission Rate Sample 

1 

(lb/MMBtu)

Volatile Organic HAP 

Emission Rate Sample 

1 

(μg @ 7% O2)

Volatile Organic 

HAP Emission Rate 

Sample 2 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 2

(μg @ 7% O2)

Volatile Organic 

HAP Emission 

Rate Sample 3 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 3

(μg @ 7% O2) Test Method Used Other Supporting Information

Speciated Volatile Organic HAP Emission Data

Note: Acetone and methylene chloride were observed in the laboratory

blank. Laboratory notes indicate the elevated acetone, methylene 

chloride, and toluene levels may be due to contamination in the field.

Dichlorodifluoromethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.07; plus 1/4 condensate (ug): [<4]

Chloromethane Average of 4 Trials, Run 1 (ug): 0.03+[<0.02]; 0.03+[<0.02]; [<0.02]+0.06; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<4]

Vinyl Chloride Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<2]

Bromomethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+0.04; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<2]

Chloroethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<4]

Trichlorofluoromethane Average of 4 Trials, Run 1 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<4]

Carbon Disulfide Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Acetone Average of 4 Trials, Run 1 (ug): 0.12+0.07; 0.12+0.06; 0.09+0.27; 0.06+0.08; plus 1/4 condensate (ug): [<80]

1,1-Dichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Iodomethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Methylene Chloride Average of 4 Trials, Run 1 (ug): 0.01+0.02; 0.01+0.04; 0.11+0.15; 0.02+0.11; plus 1/4 condensate (ug): [<80]

trans,1,2-Dichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Vinyl Acetate Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,1-Dichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

2-Butanone Average of 4 Trials, Run 1 (ug): 0.03+[<0.01]; 0.03+[<0.01]; 0.07+[<0.01]; 0.04+[<0.01]; plus 1/4 condensate (ug): [<80]

cis,1,2-Dichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Chloroform Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,1,1-Trichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Carbon Tetrachloride Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,2-Dichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Benzene Average of 4 Trials, Run 1 (ug): 0.21+0.02; 0.21+0.03; 0.36+0.2; 0.18+0.04; plus 1/4 condensate (ug): [<2]

Trichloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,2-Dichloropropane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Dibromomethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Bromodichloromethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

cis,1,3-Dichloropropene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

trans,1,3-Dichloropropene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

4-Methyl-2-Pentanone Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<80]

1,1,2-Trichloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Chlorodibromomethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

2-Hexanone Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; 0.03+[<0.01]; plus 1/4 condensate (ug): [<80]

Toluene Average of 4 Trials, Run 1 (ug): 0.33+0.01; 0.33+0.01; 0.6+0.07; 0.36+0.02; plus 1/4 condensate (ug): [<2]

Tetrachloroethene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Ethylene Dibromide Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Chlorobenzene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,1,1,2-Tetrachloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Ethylbenzene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+0.02; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

M&P-Xylene Average of 4 Trials, Run 1 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<4]

O-Xylene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Styrene Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

Bromoform Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,1,2,2-Tetrachloroethane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<2]

1,2,3-Trichloropropane Average of 4 Trials, Run 1 (ug): [<0.01]+[<0.01]; [<0.01]+0.04; [<0.01]+[<0.01]; [<0.01]+0.02; plus 1/4 condensate (ug): [<2]

Run 2 Comments:

Dichlorodifluoromethane Average of 4 Trials, Run 2 (ug): 0.04+[<0.02]; [<0.02]+0.03; [<0.02]+0.1; [<0.02]+0.02; plus 1/4 condensate (ug): [<1.0] EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Spec Volit Org HAP Emis Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/13/2010 5/13/2010

Steam Output (1000 lb/hr) 5326 5318 5324 1000 lb/hr

Total Heat Input (MMBtu/hr) 7489 7502 7510 MMBtu/hr

Basis (Wet/Dry) Wet Wet Wet N/A

Exhaust Steam % Moisture 4.99 5.04 5.11 %

Exhaust Flow Rate (acfm or dscfm) 1587453.955 1740618.358 1646575.965 dscfm

Exhaust Temperature (deg C or deg F) 314.50 318.25 319.17 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 409300 410000 410400 lb/hour gas fuel meter

Compound 

(use drop down to define for as many

rows as needed)

Volatile Organic HAP 

Emission Rate Sample 

1 

(lb/MMBtu)

Volatile Organic HAP 

Emission Rate Sample 

1 

(μg @ 7% O2)

Volatile Organic 

HAP Emission Rate 

Sample 2 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 2

(μg @ 7% O2)

Volatile Organic 

HAP Emission 

Rate Sample 3 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 3

(μg @ 7% O2) Test Method Used Other Supporting Information

Speciated Volatile Organic HAP Emission Data

Note: Acetone and methylene chloride were observed in the laboratory

blank. Laboratory notes indicate the elevated acetone, methylene 

chloride, and toluene levels may be due to contamination in the field.

Chloromethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Vinyl Chloride Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50]

Bromomethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Chloroethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Trichlorofluoromethane Average of 4 Trials, Run 2 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Carbon Disulfide Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Acetone Average of 4 Trials, Run 2 (ug): [<0.05]+[<0.05]; [<0.05]+[<0.05]; [<0.05]+[<0.05]; [<0.05]+0.1; plus 1/4 condensate (ug): [<20]

1,1-Dichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Iodomethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Methylene Chloride Average of 4 Trials, Run 2 (ug): 0.05+0.07; 0.24+0.47; 0.12+0.02; 0.03+0.23; plus 1/4 condensate (ug): 2.29

trans,1,2-Dichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Vinyl Acetate Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1-Dichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

2-Butanone Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20]

cis,1,2-Dichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Chloroform Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1,1-Trichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Carbon Tetrachloride Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,2-Dichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Benzene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; 0.01+0.01; 0.03+0.01; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Trichloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,2-Dichloropropane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Dibromomethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Bromodichloromethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

cis,1,3-Dichloropropene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

trans,1,3-Dichloropropene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

4-Methyl-2-Pentanone Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20]

1,1,2-Trichloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Chlorodibromomethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

2-Hexanone Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20]

Toluene Average of 4 Trials, Run 2 (ug): 0.02+0.02; 0.11+0.15; 0.04+0.01; 0.06+0.04; plus 1/4 condensate (ug): [<0.50]

Tetrachloroethene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Ethylene Dibromide Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Chlorobenzene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1,1,2-Tetrachloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Ethylbenzene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; 0.02+0.04; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

M&P-Xylene Average of 4 Trials, Run 2 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0]

O-Xylene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Styrene Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Bromoform Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1,2,2-Tetrachloroethane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,2,3-Trichloropropane Average of 4 Trials, Run 2 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Run 3 Comments:

Dichlorodifluoromethane Average of 4 Trials, Run 3 (ug): [<0.02]+0.09; [<0.02]+0.05; [<0.02]+0.08; [<0.02]+0.08; plus 1/4 condensate (ug): [<1.0]

Chloromethane Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0] EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Spec Volit Org HAP Emis Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/13/2010 5/13/2010

Steam Output (1000 lb/hr) 5326 5318 5324 1000 lb/hr

Total Heat Input (MMBtu/hr) 7489 7502 7510 MMBtu/hr

Basis (Wet/Dry) Wet Wet Wet N/A

Exhaust Steam % Moisture 4.99 5.04 5.11 %

Exhaust Flow Rate (acfm or dscfm) 1587453.955 1740618.358 1646575.965 dscfm

Exhaust Temperature (deg C or deg F) 314.50 318.25 319.17 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 409300 410000 410400 lb/hour gas fuel meter

Compound 

(use drop down to define for as many

rows as needed)

Volatile Organic HAP 

Emission Rate Sample 

1 

(lb/MMBtu)

Volatile Organic HAP 

Emission Rate Sample 

1 

(μg @ 7% O2)

Volatile Organic 

HAP Emission Rate 

Sample 2 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 2

(μg @ 7% O2)

Volatile Organic 

HAP Emission 

Rate Sample 3 

(lb/MMBtu)

Volatile Organic 

HAP Emission 

Rate Sample 3

(μg @ 7% O2) Test Method Used Other Supporting Information

Speciated Volatile Organic HAP Emission Data

Note: Acetone and methylene chloride were observed in the laboratory

blank. Laboratory notes indicate the elevated acetone, methylene 

chloride, and toluene levels may be due to contamination in the field.

Vinyl Chloride Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<0.50]

Bromomethane Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Chloroethane Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Trichlorofluoromethane Average of 4 Trials, Run 3 (ug): [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; [<0.02]+[<0.02]; plus 1/4 condensate (ug): [<1.0]

Carbon Disulfide Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Acetone Average of 4 Trials, Run 3 (ug): [<0.05]+[<0.05]; [<0.05]+[<0.05]; [<0.05]+[<0.05]; 0.06+0.07; plus 1/4 condensate (ug): [<20]

1,1-Dichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Iodomethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Methylene Chloride Average of 4 Trials, Run 3 (ug): 0.05+0.03; 1.14+0.63; 0.03+0.05; 0.04+0.05; plus 1/4 condensate (ug): 2.26

trans,1,2-Dichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Vinyl Acetate Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1-Dichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

2-Butanone Average of 4 Trials, Run 3 (ug): 0.02+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20]

cis,1,2-Dichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Chloroform Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1,1-Trichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Carbon Tetrachloride Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,2-Dichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Benzene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; 0.01+0.01; [<0.01]+[<0.01]; 0.01+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Trichloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,2-Dichloropropane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Dibromomethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Bromodichloromethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

cis,1,3-Dichloropropene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

trans,1,3-Dichloropropene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

4-Methyl-2-Pentanone Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20]

1,1,2-Trichloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Chlorodibromomethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

2-Hexanone Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<20]

Toluene Average of 4 Trials, Run 3 (ug): 0.1+0.05; 0.23+0.18; 0.03+0.01; 0.03+0.02; plus 1/4 condensate (ug): [<0.50]

Tetrachloroethene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Ethylene Dibromide Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Chlorobenzene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1,1,2-Tetrachloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Ethylbenzene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; 0.04+0.06; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

M&P-Xylene Average of 4 Trials, Run 3 (ug): [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; [<0.03]+[<0.03]; plus 1/4 condensate (ug): [<1.0]

O-Xylene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Styrene Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

Bromoform Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,1,2,2-Tetrachloroethane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

1,2,3-Trichloropropane Average of 4 Trials, Run 3 (ug): [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; [<0.01]+[<0.01]; plus 1/4 condensate (ug): [<0.50]

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Spec Volit Org HAP Emis Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/13/2010 5/13/2010

Steam Output (1000 lb/hr) 5318 5324 5232 1000 lb/hr

Total Heat Input (MMBtu/hr) 7491 7510 7522 MMBtu/hr

Basis (Wet/Dry) Wet Wet Wet N/A

Exhaust Steam % Moisture 9.31 9.95 9.02 %

Exhaust Flow Rate (acfm or dscfm) 1,587,454 1,740,618 1,646,576 dscfm

Exhaust Temperature (deg C or deg F) 313.79 320.83 321.63 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow Measurement 

Method Other Supporting Information

No.6 Fuel Oil (residual or bunker C) 409400 410400 411000 lb/hour gas fuel meter

Compound 

(use drop down to define for as 

many rows as needed)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 1 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 1 

(μg @ 7% O2)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 2 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 2 

(μg @ 7% O2)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 3 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 3 

(μg @ 7% O2) Test Method Used Other Supporting Information

N-nitrosomethylethylamine [<7.97E-06] [<9.24] [<7.97E-06] [<9.24] [<7.97E-06] [<9.24] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<9.45]+[<9.45]+[<9.45] - Run 2 (ug): [<9.45]+[<9.45]+[<9.45] - Run 3 (ug): [<9.45]+[<9.45]+[<9.45]

Methyl methanesulfonate [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05]

N-Nitrosodiethylamine [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

Ethyl methanesulfonate [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

Aniline [<1.56E-06] [<1.81] [<1.56E-06] [<1.81] [<1.56E-06] [<1.81] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.85]+[<1.85]+[<1.85] - Run 2 (ug): [<1.85]+[<1.85]+[<1.85] - Run 3 (ug): [<1.85]+[<1.85]+[<1.85]

Phenol [<2.18E-06] [<2.53] [<1.97E-06] [<2.28] [<8.66E-06] [<10.04] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.95]+[<3.85]+[<1.95] - Run 2 (ug): [<1.95]+[<3.1]+[<1.95] - Run 3 (ug): [<1.95]+[<26.9]+[<1.95]

Pentachloroethane [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] [<2.28E-06] [<2.64] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.7]+[<2.7]+[<2.7] - Run 2 (ug): [<2.7]+[<2.7]+[<2.7] - Run 3 (ug): [<2.7]+[<2.7]+[<2.7]

Bis(2-chloroethyl)ether [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9]

2-Chlorophenol [<1.56E-06] [<1.81] [<1.56E-06] [<1.81] [<1.56E-06] [<1.81] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.85]+[<1.85]+[<1.85] - Run 2 (ug): [<1.85]+[<1.85]+[<1.85] - Run 3 (ug): [<1.85]+[<1.85]+[<1.85]

1,3-Dichlorobenzene [<2.02E-06] [<2.35] [<2.02E-06] [<2.35] [<2.02E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.4]+[<2.4]+[<2.4] - Run 2 (ug): [<2.4]+[<2.4]+[<2.4] - Run 3 (ug): [<2.4]+[<2.4]+[<2.4]

1,4-Dichlorobenzene [<2.36E-06] [<2.74] [<2.36E-06] [<2.74] [<2.36E-06] [<2.74] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.8]+[<2.8]+[<2.8] - Run 2 (ug): [<2.8]+[<2.8]+[<2.8] - Run 3 (ug): [<2.8]+[<2.8]+[<2.8]

1,2-Dichlorobenzene [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05]

Benzyl alcohol [<3E-06] [<3.47] [<3E-06] [<3.47] [<3E-06] [<3.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<3.55]+[<3.55]+[<3.55] - Run 2 (ug): [<3.55]+[<3.55]+[<3.55] - Run 3 (ug): [<3.55]+[<3.55]+[<3.55]

Bis(2-chloroisopropyl)ether [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

Hexachloroethane [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

N-Nitrosodi-n-propylamine [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9]

2-Methylphenol [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

4-Methylphenol&3-Methylphenol [<4.77E-06] [<5.53] [<4.77E-06] [<5.53] [<4.77E-06] [<5.53] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5.65]+[<5.65]+[<5.65] - Run 2 (ug): [<5.65]+[<5.65]+[<5.65] - Run 3 (ug): [<5.65]+[<5.65]+[<5.65]

Acetophenone [<2.49E-06] [<2.89] [<2.5E-06] [<2.9] [<3.52E-06] [<4.08] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): [<1.8]+5.25+[<1.8] - Run 2 (ug): [<1.8]+5.3+[<1.8] - Run 3 (ug): [<1.8]+8.9+[<1.8]

N-nitrosomorpholine [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05]

o-Toluidine [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5]

N-nitrosopyrrolidine [<1.27E-06] [<1.47] [<1.27E-06] [<1.47] [<1.27E-06] [<1.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.5]+[<1.5]+[<1.5] - Run 2 (ug): [<1.5]+[<1.5]+[<1.5] - Run 3 (ug): [<1.5]+[<1.5]+[<1.5]

N-nitrosopiperidine [<7.09E-06] [<8.22] [<7.09E-06] [<8.22] [<7.09E-06] [<8.22] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<8.4]+[<8.4]+[<8.4] - Run 2 (ug): [<8.4]+[<8.4]+[<8.4] - Run 3 (ug): [<8.4]+[<8.4]+[<8.4]

Nitrobenzene [<1.65E-06] [<1.91] [<1.65E-06] [<1.91] [<1.65E-06] [<1.91] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.95]+[<1.95]+[<1.95] - Run 2 (ug): [<1.95]+[<1.95]+[<1.95] - Run 3 (ug): [<1.95]+[<1.95]+[<1.95]

Isophorone [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25]

2-Nitrophenol [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

2,4-Dimethylphenol [<2.19E-06] [<2.54] [<2.19E-06] [<2.54] [<2.19E-06] [<2.54] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.6]+[<2.6]+[<2.6] - Run 2 (ug): [<2.6]+[<2.6]+[<2.6] - Run 3 (ug): [<2.6]+[<2.6]+[<2.6]

Bis(2-chloroethoxy)methane [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

2,4-Dichlorophenol [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

1,2,4-Trichlorobenzene [<1.31E-06] [<1.52] [<1.31E-06] [<1.52] [<1.31E-06] [<1.52] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.55]+[<1.55]+[<1.55] - Run 2 (ug): [<1.55]+[<1.55]+[<1.55] - Run 3 (ug): [<1.55]+[<1.55]+[<1.55]

Naphthalene [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9]

4-Chloroaniline [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5]

2-Chloronaphthalene [<2.24E-06] [<2.59] [<2.24E-06] [<2.59] [<2.24E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.65]+[<2.65]+[<2.65] - Run 2 (ug): [<2.65]+[<2.65]+[<2.65] - Run 3 (ug): [<2.65]+[<2.65]+[<2.65]

2,6-Dichlorophenol [<2.24E-06] [<2.59] [<2.24E-06] [<2.59] [<2.24E-06] [<2.59] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.65]+[<2.65]+[<2.65] - Run 2 (ug): [<2.65]+[<2.65]+[<2.65] - Run 3 (ug): [<2.65]+[<2.65]+[<2.65]

Hexachloropropene [<1.35E-06] [<1.56] [<1.35E-06] [<1.56] [<1.35E-06] [<1.56] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.6]+[<1.6]+[<1.6] - Run 2 (ug): [<1.6]+[<1.6]+[<1.6] - Run 3 (ug): [<1.6]+[<1.6]+[<1.6]

Hexachlorobutadiene [<1.43E-06] [<1.66] [<1.43E-06] [<1.66] [<1.43E-06] [<1.66] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.7]+[<1.7]+[<1.7] - Run 2 (ug): [<1.7]+[<1.7]+[<1.7] - Run 3 (ug): [<1.7]+[<1.7]+[<1.7]

N-Nitrosodi-n-butylamine [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

4-Chloro-3-methylphenol [<2.45E-06] [<2.84] [<2.45E-06] [<2.84] [<2.45E-06] [<2.84] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.9]+[<2.9]+[<2.9] - Run 2 (ug): [<2.9]+[<2.9]+[<2.9] - Run 3 (ug): [<2.9]+[<2.9]+[<2.9]

2-Methylnaphthalene [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

Isosafrole [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

Hexachlorocyclopentadiene [<2.11E-05] [<24.45] [<2.11E-05] [<24.45] [<2.11E-05] [<24.45] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<25]+[<25]+[<25] - Run 2 (ug): [<25]+[<25]+[<25] - Run 3 (ug): [<25]+[<25]+[<25]

1,2,4,5-Tetrachlorobenzene [<1.81E-06] [<2.1] [<1.81E-06] [<2.1] [<1.81E-06] [<2.1] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.15]+[<2.15]+[<2.15] - Run 2 (ug): [<2.15]+[<2.15]+[<2.15] - Run 3 (ug): [<2.15]+[<2.15]+[<2.15]

2,4,6-Trichlorophenol [<1.98E-06] [<2.3] [<1.98E-06] [<2.3] [<1.98E-06] [<2.3] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.35]+[<2.35]+[<2.35] - Run 2 (ug): [<2.35]+[<2.35]+[<2.35] - Run 3 (ug): [<2.35]+[<2.35]+[<2.35]

2,4,5-Trichlorophenol [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25]

2-Nitroaniline [<1.98E-06] [<2.3] [<1.98E-06] [<2.3] [<1.98E-06] [<2.3] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.35]+[<2.35]+[<2.35] - Run 2 (ug): [<2.35]+[<2.35]+[<2.35] - Run 3 (ug): [<2.35]+[<2.35]+[<2.35]

Safrole [<1.1E-06] [<1.27] [<1.1E-06] [<1.27] [<1.1E-06] [<1.27] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.3]+[<1.3]+[<1.3] - Run 2 (ug): [<1.3]+[<1.3]+[<1.3] - Run 3 (ug): [<1.3]+[<1.3]+[<1.3]

Dimethyl phthalate [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

Acenaphthylene [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

2,6-Dinitrotoluene [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

m-dinitrobenzene [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3]

3-Nitroaniline [<2.91E-06] [<3.37] [<2.91E-06] [<3.37] [<2.91E-06] [<3.37] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<3.45]+[<3.45]+[<3.45] - Run 2 (ug): [<3.45]+[<3.45]+[<3.45] - Run 3 (ug): [<3.45]+[<3.45]+[<3.45]

2,4-Dinitrotoluene [<1.81E-06] [<2.1] [<1.81E-06] [<2.1] [<1.81E-06] [<2.1] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.15]+[<2.15]+[<2.15] - Run 2 (ug): [<2.15]+[<2.15]+[<2.15] - Run 3 (ug): [<2.15]+[<2.15]+[<2.15]

4-Nitrophenol [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9]

2,4-Dinitrophenol [<2.11E-05] [<24.45] [<2.11E-05] [<24.45] [<2.11E-05] [<24.45] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<25]+[<25]+[<25] - Run 2 (ug): [<25]+[<25]+[<25] - Run 3 (ug): [<25]+[<25]+[<25]

Acenaphthene [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3]

Dibenzofuran [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3]

Pentachlorobenzene [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

2-Naphthylamine [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5]

1-Naphthylamine [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] [<4.22E-06] [<4.89] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<5]+[<5]+[<5] - Run 2 (ug): [<5]+[<5]+[<5] - Run 3 (ug): [<5]+[<5]+[<5]

2,3,4,6-Tetrachlorophenol [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25]

Fluorene [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

Diethyl phthalate [<4.29E-06] [<4.97] [<1.19E-05] [<13.74] [<2.04E-05] [<23.69] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): 6.35+7.05+[<1.85] - Run 2 (ug): 28.8+11.5+[<1.85] - Run 3 (ug): 39.3+31.5+[<1.85]

4-Chlorophenyl phenyl ether [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+[<2.25]+[<2.25]

4-Nitroaniline [<1.27E-06] [<1.47] [<1.27E-06] [<1.47] [<1.27E-06] [<1.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.5]+[<1.5]+[<1.5] - Run 2 (ug): [<1.5]+[<1.5]+[<1.5] - Run 3 (ug): [<1.5]+[<1.5]+[<1.5]

Azobenzene [<1.43E-06] [<1.66] [<1.43E-06] [<1.66] [<1.43E-06] [<1.66] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.7]+[<1.7]+[<1.7] - Run 2 (ug): [<1.7]+[<1.7]+[<1.7] - Run 3 (ug): [<1.7]+[<1.7]+[<1.7]

2-Methyl-4,6-dinitrophenol [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

Diphenylamine [<2.4E-06] [<2.79] [<2.4E-06] [<2.79] [<2.4E-06] [<2.79] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.85]+[<2.85]+[<2.85] - Run 2 (ug): [<2.85]+[<2.85]+[<2.85] - Run 3 (ug): [<2.85]+[<2.85]+[<2.85]

4-Bromophenyl phenyl ether [<1.81E-06] [<2.1] [<1.81E-06] [<2.1] [<1.81E-06] [<2.1] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.15]+[<2.15]+[<2.15] - Run 2 (ug): [<2.15]+[<2.15]+[<2.15] - Run 3 (ug): [<2.15]+[<2.15]+[<2.15]

Phenacetin [<3.08E-06] [<3.57] [<3.08E-06] [<3.57] [<3.08E-06] [<3.57] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<3.65]+[<3.65]+[<3.65] - Run 2 (ug): [<3.65]+[<3.65]+[<3.65] - Run 3 (ug): [<3.65]+[<3.65]+[<3.65]

Hexachlorobenzene [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] [<1.86E-06] [<2.15] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.2]+[<2.2]+[<2.2] - Run 2 (ug): [<2.2]+[<2.2]+[<2.2] - Run 3 (ug): [<2.2]+[<2.2]+[<2.2]

1,3,5-Trinitrobenzene [<1.31E-06] [<1.52] [<1.31E-06] [<1.52] [<1.31E-06] [<1.52] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.55]+[<1.55]+[<1.55] - Run 2 (ug): [<1.55]+[<1.55]+[<1.55] - Run 3 (ug): [<1.55]+[<1.55]+[<1.55]

4-Aminobiphenyl [<1.69E-05] [<19.56] [<1.69E-05] [<19.56] [<1.69E-05] [<19.56] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<20]+[<20]+[<20] - Run 2 (ug): [<20]+[<20]+[<20] - Run 3 (ug): [<20]+[<20]+[<20]

Pentachlorophenol [<4.18E-06] [<4.84] [<4.18E-06] [<4.84] [<4.18E-06] [<4.84] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<4.95]+[<4.95]+[<4.95] - Run 2 (ug): [<4.95]+[<4.95]+[<4.95] - Run 3 (ug): [<4.95]+[<4.95]+[<4.95]

Phenanthrene [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

Pentachloronitrobenzene [<1.65E-06] [<1.91] [<1.65E-06] [<1.91] [<1.65E-06] [<1.91] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.95]+[<1.95]+[<1.95] - Run 2 (ug): [<1.95]+[<1.95]+[<1.95] - Run 3 (ug): [<1.95]+[<1.95]+[<1.95]

Anthracene [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.8]+[<1.8]+[<1.8] - Run 2 (ug): [<1.8]+[<1.8]+[<1.8] - Run 3 (ug): [<1.8]+[<1.8]+[<1.8]

Dinoseb [<1.43E-06] [<1.66] [<1.43E-06] [<1.66] [<1.43E-06] [<1.66] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.7]+[<1.7]+[<1.7] - Run 2 (ug): [<1.7]+[<1.7]+[<1.7] - Run 3 (ug): [<1.7]+[<1.7]+[<1.7]

Di-n-butyl phthalate [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] [<1.52E-06] [<1.76] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.8]+[<1.8]+[<1.8] - Run 2 (ug): [<1.8]+[<1.8]+[<1.8] - Run 3 (ug): [<1.8]+[<1.8]+[<1.8]

Fluoranthene [<1.35E-06] [<1.56] [<1.35E-06] [<1.56] [<1.35E-06] [<1.56] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.6]+[<1.6]+[<1.6] - Run 2 (ug): [<1.6]+[<1.6]+[<1.6] - Run 3 (ug): [<1.6]+[<1.6]+[<1.6]

Pyrene [<1.48E-06] [<1.71] [<1.48E-06] [<1.71] [<1.48E-06] [<1.71] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.75]+[<1.75]+[<1.75] - Run 2 (ug): [<1.75]+[<1.75]+[<1.75] - Run 3 (ug): [<1.75]+[<1.75]+[<1.75]

p-(dimethylamino)azobenzene [<8.44E-07] [<0.98] [<8.44E-07] [<0.98] [<8.44E-07] [<0.98] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1]+[<1]+[<1] - Run 2 (ug): [<1]+[<1]+[<1] - Run 3 (ug): [<1]+[<1]+[<1]

Speciated Semi Volatile Organic HAP Emission Data

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Spec SemiVol Org HAP Emis Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/13/2010 5/13/2010

Steam Output (1000 lb/hr) 5318 5324 5232 1000 lb/hr

Total Heat Input (MMBtu/hr) 7491 7510 7522 MMBtu/hr

Basis (Wet/Dry) Wet Wet Wet N/A

Exhaust Steam % Moisture 9.31 9.95 9.02 %

Exhaust Flow Rate (acfm or dscfm) 1,587,454 1,740,618 1,646,576 dscfm

Exhaust Temperature (deg C or deg F) 313.79 320.83 321.63 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow Measurement 

Method Other Supporting Information

No.6 Fuel Oil (residual or bunker C) 409400 410400 411000 lb/hour gas fuel meter

Compound 

(use drop down to define for as 

many rows as needed)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 1 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 1 

(μg @ 7% O2)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 2 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 2 

(μg @ 7% O2)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 3 

(lb/MMBtu)

Semi-Volatile Organic HAP 

Emission Rate 

Sample 3 

(μg @ 7% O2) Test Method Used Other Supporting Information

Speciated Semi Volatile Organic HAP Emission Data

Benz(a)anthracene [<1.22E-06] [<1.42] [<1.22E-06] [<1.42] [<1.22E-06] [<1.42] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.45]+[<1.45]+[<1.45] - Run 2 (ug): [<1.45]+[<1.45]+[<1.45] - Run 3 (ug): [<1.45]+[<1.45]+[<1.45]

Butyl benzyl phthalate [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

2-Acetylaminofluorene [<2.02E-06] [<2.35] [<2.02E-06] [<2.35] [<2.02E-06] [<2.35] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.4]+[<2.4]+[<2.4] - Run 2 (ug): [<2.4]+[<2.4]+[<2.4] - Run 3 (ug): [<2.4]+[<2.4]+[<2.4]

Chrysene [<1.27E-06] [<1.47] [<1.27E-06] [<1.47] [<1.27E-06] [<1.47] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.5]+[<1.5]+[<1.5] - Run 2 (ug): [<1.5]+[<1.5]+[<1.5] - Run 3 (ug): [<1.5]+[<1.5]+[<1.5]

Bis(2-ethylhexyl)phthalate [<1.9E-06] [<2.2] [<1.9E-06] [<2.2] [<1.3E-05] [<15.03] U.S. EPA Method 0010 with SW-846 Method 8270D DLL: Run 1 (ug): [<2.25]+[<2.25]+[<2.25] - Run 2 (ug): [<2.25]+[<2.25]+[<2.25] - Run 3 (ug): [<2.25]+41.6+[<2.25]

Di-n-octyl phthalate [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] [<1.94E-06] [<2.25] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.3]+[<2.3]+[<2.3] - Run 2 (ug): [<2.3]+[<2.3]+[<2.3] - Run 3 (ug): [<2.3]+[<2.3]+[<2.3]

7,12-Dimethylbenz(a)anthracene [<1.39E-06] [<1.61] [<1.39E-06] [<1.61] [<1.39E-06] [<1.61] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.65]+[<1.65]+[<1.65] - Run 2 (ug): [<1.65]+[<1.65]+[<1.65] - Run 3 (ug): [<1.65]+[<1.65]+[<1.65]

3-Methylcholanthrene [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05]

Benzo(b)fluoranthene [<1.48E-06] [<1.71] [<1.48E-06] [<1.71] [<1.48E-06] [<1.71] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.75]+[<1.75]+[<1.75] - Run 2 (ug): [<1.75]+[<1.75]+[<1.75] - Run 3 (ug): [<1.75]+[<1.75]+[<1.75]

Benzo(k)fluoranthene [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] [<1.73E-06] [<2.01] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.05]+[<2.05]+[<2.05] - Run 2 (ug): [<2.05]+[<2.05]+[<2.05] - Run 3 (ug): [<2.05]+[<2.05]+[<2.05]

Benzo(a)pyrene [<1.14E-06] [<1.32] [<1.14E-06] [<1.32] [<1.14E-06] [<1.32] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.35]+[<1.35]+[<1.35] - Run 2 (ug): [<1.35]+[<1.35]+[<1.35] - Run 3 (ug): [<1.35]+[<1.35]+[<1.35]

Indeno(1,2,3-cd)pyrene [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] [<1.6E-06] [<1.86] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<1.9]+[<1.9]+[<1.9] - Run 2 (ug): [<1.9]+[<1.9]+[<1.9] - Run 3 (ug): [<1.9]+[<1.9]+[<1.9]

Dibenz(a,h)anthracene [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] [<1.77E-06] [<2.05] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2.1]+[<2.1]+[<2.1] - Run 2 (ug): [<2.1]+[<2.1]+[<2.1] - Run 3 (ug): [<2.1]+[<2.1]+[<2.1]

Benzo(g,h,i)perylene [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] [<1.69E-06] [<1.96] U.S. EPA Method 0010 with SW-846 Method 8270D BDL: Run 1 (ug): [<2]+[<2]+[<2] - Run 2 (ug): [<2]+[<2]+[<2] - Run 3 (ug): [<2]+[<2]+[<2]

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls Spec SemiVol Org HAP Emis Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/11/2010 5/11/2010

Steam Output (1000 lb/hr) 5327 5325 5329 1000 lb/hr

Total Heat Input (MMBtu/hr) 7506 7508 7514 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 9.216040761 9.216040761 9.216040761 %

Exhaust Flow Rate (acfm or dscfm) 1469055.512 1474423.975 1481305.477 dscfm

Exhaust Temperature (deg C or deg F) 320 320 320 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method Other Supporting Information

No.6 Fuel Oil (residual or bunker C) 1,001 1,001 1,002 gallon/minute gas fuel meter

Emission Test Results

Hydrogen Cyanide 

Emission Rate 

Sample 1

 (lb/MMBtu)

Hydrogen Cyanide 

Emission Rate 

Sample 2 

(lb/MMBtu)

Hydrogen Cyanide 

Emission Rate 

Sample 3 

(lb/MMBtu)

Test Method Used

(ex. U.S. EPA Conditional Test Method 033)

Other Supporting 

Information

0.00072721 0.000691752 0.00070177 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls HCN Emission Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/11/2010 5/11/2010

Steam Output (1000 lb/hr) 5327 5325 5329 1000 lb/hr

Total Heat Input (MMBtu/hr) 7506 7508 7514 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 9.216040761 9.216040761 9.216040761 %

Exhaust Flow Rate (acfm or dscfm) 1469055.512 1474423.975 1481305.477 dscfm

Exhaust Temperature (deg C or deg F) 320 320 320 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow

Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 1,001 1,001 1,002 gallon/minute gas fuel meter

Emission Test Results

HCl Emission Rate 

Sample 1 (lb/MMBtu)

HCl Emission Rate 

Sample 1 

(ppmvd @ 7% O2)

HCl Emission Rate 

Sample 2 (lb/MMBtu)

HCl Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

HCl Emission Rate 

Sample 3 (lb/MMBtu)

HCl Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA

Method 320)

Other Supporting 

Information

0.000948084 0.72 0.000454868 0.35 0.000313145 0.24 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls HCl Emission Data
EIA Facility Code Facility Name Boiler ID

6042 Manatee PMT2

Parameter Sample 1 Sample 2 Sample 3 Unit of Measure

Other Supporting 

Information

Date of Testing 5/11/2010 5/11/2010 5/11/2010

Steam Output (1000 lb/hr) 5327 5325 5329 1000 lb/hr

Total Heat Input (MMBtu/hr) 7506 7508 7514 MMBtu/hr

Basis (Wet/Dry) Dry Dry Dry N/A

Exhaust Steam % Moisture 9.216040761 9.216040761 9.216040761 %

Exhaust Flow Rate (acfm or dscfm) 1469055.512 1474423.975 1481305.477 dscfm

Exhaust Temperature (deg C or deg F) 320 320 320 deg F

Fuel Type Selection

Fuel Input Rate

Sample 1

Fuel Input Rate 

Sample 2

Fuel Input Rate 

Sample 3 Unit of Measure

Fuel Flow Measurement 

Method

Other Supporting 

Information

No.6 Fuel Oil (residual or bunker C) 1,001 1,001 1,002 gallon/minute gas fuel meter

Emission Test Results

HF Emission Rate Sample 

1

 (lb/MMBtu)

HF Emission Rate Sample 

1

(ppmvd @ 7% O2)

HF Emission Rate 

Sample 2 

(lb/MMBtu)

HF Emission Rate 

Sample 2 

(ppmvd @ 7% O2)

HF Emission Rate 

Sample 3 

(lb/MMBtu)

HF Emission Rate 

Sample 3 

(ppmvd @ 7% O2)

Test Method Used

(ex. U.S. EPA

Method 18)

Other Supporting 

Information

0.000449851 0.63 0.000329767 0.46 0.000271498 0.38 U.S. EPA Method 320 #VALUE!

EPA-HQ-OAR-2009-0234-DRAFT-1850.xls HF Emission Data