### SUMMARY OF NON-EPA TEST METHOD REFERENCES

Submitted by Santa Barbara County APCD July 11, 2012 Item Rule No., Definition or Section Test Method Internet Website Where the Te st Method is Available Other Information

1 102, Alternative Diesel Fuel definition ASTM D 975, “Standard Specification for Diesel Fuel Oils,” ASTM International. www.astm.org/Standards/ D975.htm Listed in 40 CFR 60.17

2 102, Gasoline definition Test Method for the Determination of the R eid Vapor P ressure E quivalent U sing an A utomated Vapor P ressure Test Instrument ccr.oal.ca.gov/linkedslice/ default.asp?SP=CCR

1000&Action=Welcome This test method is found in the California Code of Regulations, Title 13, Division 3, Chapter 5, Article 4, section 2297.

3 102, MultipleChamber Incinerator definition Standard Test Method for Pyrometric Cone Equivalent (PCE) of Fireclay and High Alumina Refractory Materials , ASTM Method C-24. www.astm.org/Standards/ C24.htm

4 102, Organic Solvents definition Standard Test Method for Distillation Range of Volatile Organic Liquids, ASTM D 1078-05 www.astm.org/DATABA SE.CART/HISTORICAL/ D1078 -05.htm Listed in 49 CFR 173.121.

5 102, South Coast Air Quality Management District Method 303- 91, “Determination of Exempt Compounds,” August 1996 d efinition South Coast Air Quality Management District Method 303 -91, “Determination of Exempt Compounds, ” August 1996 www.aqmd.gov/tao/meth ods/labmethtoc.html Listed as a method technically acceptable by EPA Region IX for inclusion into the SIP in conjunction with SIP approved rules. (Reference: www.arb.ca.gov/fcaa/tv/tvi nfo/accp_mth.htm web page.) 6 102, South Coast Air Quality Management District Method 313- 91, “Determination of Volatile Organic Compounds by Gas Chromatography

Mass Spectrometry,” June 1993 definition South Coast Air Quality Management District Method 313 -91, “Determination of Volatile Organic Compounds by Gas Chromatography

- Mass Spectrometry,” June 1993 Same as item 5. Same as item 5.

7 202.I.3, 202.U.2.c, 202.U.2.d.i, 202.U.3 Same as item 6. (SC 313-91) Same as item 5. Same as item 5.

8 202, Section U.2.b Same as item 4. (ASTM D 1078) Same as item 4.

9 202, Section V.2 ASTM D-4057-06, “Standard Practice for Manual Sampling of Petroleum and Petroleum Products,” ASTM International www.astm.org/Standards/ D4057.htm ASTM D4057-95 (reapproved 2000) is listed in 40 CFR 60.17. The District plans to change the

“

- 06” reference during the next Rule 202 amendment. 10 321, Initial Boiling Point definition, and Section P.2 Same as item 4. (ASTM D 1078) Same as item 4. Same as item 4.Submitted by Santa Barbara County APCD July 11, 2012 Item Rule No., Definition or Section Test Method Internet Website Where the Te st Method is Available Other Information

11 321, Section P.3 Environmental Protection Agency method described in 40 CFR, §52.741(a)(4)(iii) www.gpo.gov/fdsys/searc h/pagedetails.action?colle ctionCode=CFR&searchP ath=Title+40%2FChapter +I%2FSubchapter+C%2F Part+52%2FSubpart+O& granuleId=&packageId=C FR -2010-title40- vol1&oldPath=Title+40% 2FChapter+I%2FSubchap ter+C%2FPart+52&from PageDetails=true&collaps e=true&ycord=1066 The reference to this test method is in t he SIPapproved Rule 321 that was adopted on September 18, 1997. The District plans to delete this reference whenlowering the solvent ROCcontent limits.

12 321, Section P.4 Environmental Protection Agency method described in 40 CFR, §52.741(a)(4)(iv)

a nd 40 CFR, §52.741(a)(4)(vi) Same as above. The reference to the test method in §52.741(a)(4)(iv) is in the SIP

- approved Rule 321 that was adopted on September 18, 1997. The District plans to delete this reference when lowering the solvent ROC

- content limits. 13 321, Section P.7 Standard Practices for General Techniques of Infrared Quantitative Analysis, ASTM E 168 -06 www.astm.org/Standards/ E168.htm Listed in 40 CFR 60.17 as “ASTM E168

- 67, 77, 92.” The District plans to update the E168 reference to reflect the EPA incorporated by reference version during the next Rule 321 amendment. 14 321, Section P.7 Standard Practices for General Techniques of Ultraviolet -Visible Quantitative Analysis, ASTM E 169 -04 www.astm.org/Standards/ E169.htm Listed in 40 CFR 60.17 as “ASTM E169

- 63, 77, 93.” The District plans to update the E169 reference to reflect the EPA incorporated by reference version during the ne xt Rule 321 amendment. 15 321, Section P.7 Standard Practice for Packed Column Gas Chromatography, ASTM E 260

- 96 (2006) www.astm.org/Standards/ E260.htm Listed in 40 CFR 60.17 as “ASTM E260 -73, 91, 9 6.” In an email dated July 6, 2011, Stanley Tong of EPA, indicated the “

- 96(2006)” designation was appropriate. 16 330.I.1, 337.I.1, 349.E.5, 353.N.2 ASTM D 4457-1991,

“ Standard Test Method for Determination of Dichloromethane and 1,1,1

- Trichloroethane in Paints and Coatings by Direct Injection into a Gas Chromatograph, ” ASTM International. www.astm.org/DATABA SE.CART/HISTORICAL/ D4457 -85R96E1.htm Listed in 40 CFR 60.17.Submitted by Santa Barbara County APCD July 11, 2012 Item Rule No., Definition or Section Test Method Internet Website Where the Te st Method is Available Other Information

17 330.I.1, 337.I.1, 349.E.5, 353.N.2 Same as item 5. (SC 303-91) Same as item 5. Same as item 5.

18 330.I.1, 337.I.1, 349.E.5, 353.N.1 Same as item 6. (SC 313-91) Same as item 5. Same as item 5.

19 330.I.2, 337.I.2, 349.E.4, 353.N.7 South Coast Air Quality Management District Method 25.1,

“ Determination of Total Gaseous Non

- Methane Organic Emissions as Carbon,” February 1991 www.aqmd.gov/tao/meth ods/stm/stm -025-1.pdf Listed in 40 CFR 53-59, Fi nding Aids, Material Approved for Incorporation by Reference

20 330.I.2, 337.I.2, 349.E.4, 353.N.7 South Coast Air Quality Management District Method 25.3,

“ Determination of Low Concentration Non

Methane Non

- Ethane Organic Compound Emissions from Clean Fu eled Combustion Sources,” March 2000 www.aqmd.gov/tao/meth ods/stm/stm -025-3.pdf Listed as a method technically acceptable by EPA Region IX for inclusion into the SIP in conjunction with SIP approved rules. (Reference: www.arb.ca.gov/fcaa/tv/tvi nfo/accp_mth.htm web page.)

21 330.I.2, 330.I.7, 337.I.2, 337.I.10, 349.E.4, 349.E.8, 353.N.7, 353.N.14 Air Resources Board Method 4 22, “Exempt Halogenated VOCs in Gases,” September 12, 1990 www.arb.ca.gov/testmeth/ vol3/meth422.doc Same as item 20.

22 330.I.3.b, 337.I.3.b, 349.E.3.b, 353.N.6.b South Coast Air Quality Management District

“ Protocol for Determination of Volatile Organic Compounds (VOC) Capture Efficiency,” May 1995 www.aqmd.gov/tao/meth ods/protocols/cap_eff_pro tl.pdf Same as item 20.

23 330.I.4, 337.I.4, 353.N.10 South Coast Air Quality Management District Method “ Spray Equipment Transfer Efficiency Test Procedure for Equipment User, ” May 1989 www.aqmd.gov/permit/do cspdf/Spray -Eqpt-Trfr

Efficiency.pdf Same as item 20.

24 337.I.5, 353.N.5 ASTM D 2879- 1997,“Standard Test Method for Vapor Pressure

- Temperature Relationship and Initial Decomposition Temperature of Liquids by Isoteniscope,” ASTM International www.astm.org/DATABA SE.CART/HISTORICAL/ D2879 -97.htm Listed in 40 CFR 60.17.Submitted by Santa Barbara County APCD July 11, 2012 Item Rule No., Definition or Section Test Method Internet Website Where the Te st Method is Available Other Information

25 337.I.8, 353.N.8 South Coast Air Quality Management District's, "General Test Method for Determinin g Solvent Losses from Spray Gun Cleaning Systems," dated October 3, 1989 Listed as a method technically acceptable by EPA Region IX for inclusion into the SIP in conjunction with SIP approved rules. (Reference: www.arb.ca.gov/fcaa/tv/tvi nfo/accp_mth.htm web page.) 26 337.I.9, 353.N.13 ASTM D 1084-88, “Standard Test Methods for Viscosity of Adhesives,” ASTM International www.astm.org/DATABA SE.CART/HISTORICAL/ D1084 -97R05.htm Stanley Tong of EPA, indicated in an email dated July 6, 2011, that the D 1084 -88 was one of the latest EPA

- approved ASTM methods. 27 349.E.1 ASTM D2369-95, “Standard Test Method for Volatile Content of Coatings,” ASTM International www.astm.org/DATABA SE.CART/HISTORICAL/ D2369 -98.htm Listed in 40 CFR 60.17.

28 349.E.2 Static Method for Determination of Volatile Emissions from Polyester and Vinyl Ester Resins www.sbcapcd.org/rules/dl rules.htm This test method is found in Attachment A of Rule 349. It is consistent with the ARB RACT/BARCT Guidance Document dated Janu ary 8, 1991. EPA approved the April 27, 1993 version of Rule 349 into the SIP on January 6, 1995 (60 FR 2025). 29 353.B, Flexible Vinyl definition ASTM Method E260- 96(2006), “Standard Practice for Packed Column Gas Chromatography,” ASTM International www.astm.org/Standards/ E260.htm Same as item 15.

30 353.N.3 South Coast Air Quality Management District Test Method 305

- 91, “Determination of Volatile Organic Compounds in Aerosol Applications,” June 19 93 www.aqmd.gov/tao/meth ods/lab/305 -91.pdf Listed as a method technically acceptable by EPA Region IX for inclusion into the SIP in conjunction with SIP approved rules. (Reference: www.arb.ca.gov/fcaa/tv/tvi nfo/accp_mth.htm web page.)Submitted by Santa Barbara County APCD July 11, 2012 Item Rule No., Definition or Section Test Method Internet Website Where the Te st Method is Available Other Information

31 353.N.3 Air Resources Board Method 310, “Determination of Volatile Organic Compounds in Consumer Products and Reactive Organic Compounds in Aerosol Coating Products,” June 22, 2000 www.arb.ca.gov/testmeth/ cptm/cptm.htm Same as item 30.

32 353.N.4, 353.N.9 South Coast Air Quality Management District Method 316A -92, “Determination of Vo latile Organic Compound (VOC) in Materials Used for Pipes and Fittings,” October 1996 www.aqmd.gov/tao/meth ods/lab/316A -92.pdf Same as item 30.