Sample Ana.lysis Report 

Sample Name : AF7336 

Dala File Name : C:\PEAKNE'N>ATA\ANIONS\DX-100\Anloos..,AAH086.DXD 

Low Range DeleetOr: U120 Universal Interface Oilibralion Date : 2008/08/"20 4:33:03 PM 

Mel!lod File Name : c:lpeaknetlmethod\300anions.met · 

Schedule File. !'lame: ... \anlons0820:sch 

Date T"uoe Collected : 2008/081"21 l 2:40:59 PM 

Systeui Operator : Ll.B 

Caijbf;o~oo Type : EXTERNAL ' . 

Colllp!>nent Amourtt l.Jnits : mgiL 

Dilution Factor : 10.00 

Peak li:lfonnation : All Components 

P<tk # Compooeilt Compooenl Name 

Number 

I 2 

2 3 

4 

3 s 

10.0 

8.0 

6.0 

~ 4.0 

' 2.0 

0 

0 

Iii : PtaltNtl S.l 

Chloride 

Nitrite (as N) 

Bromide 

Nitrate (as N) 

~ I 

I 

1.0 2.0 

3 

I 

I 

3.0 

_\ l 

Component Peak Retention. Peak Area Peak H<igbt 

Aniount ~g/L)Time 

50.6025 

1.2082. 

34.1440 

AP7336 

.4.0 5.0 

1.67 

1.95 . 

3.15 

6.0 7.0 

214344325 41889741 

96o2441!. 178~163 

365291148 44876688 

8.0. 

co-Dole: 200Mle/21 

CumM Time : 12::49:09 

VES 005601 
Sample Analysis Report 

Sampt; Name : AF7337 . 

futa File NlUJie: C:\PEAKNE'N>ATA\ANIONS\DX-100\Anlons..A YSOll.DXD 

Low R•nge Detector : UI20 Universal Interface 

·Method FUe·Name: e:~ons.met 

Schedule File N.ame: ... \aoions082l.sch. · 

D~ TiJ)>C Cotlet:tcd : 2008/08121 2:52:49 PM 

SY,~tem Operat'Qr : Ll.E . 

Calibration Date: 2008108120 4:33:03 PM 

Calibration Type : EXlERNAL 

Component Amoont Units : mg/L 

Dilution Factor: 10.00 

Peak Infonnation :AU Components 

Peat # Component . .C"!"pooent Name 

Number 

Component Peak Retenli9n Peak Area Peak Helgbt 

V) 

2 

3 

4 

"-

2 

3 

s 

6 

. 10.0 

8.0 

6.0 

4.0 

2.0 

0 

0 

II : PcatNuS.2 

I 

Cblori<le 

Nitrite (as N) 

Nitrate (as N) 

Pbosphate-ortho 

2 

I 

lJ u!1 

I 

1.0 2.0 

4 

. I 

.I 

! 

3.0 

Amount (mg(L)Time · 

50.0565 

1.1944 

37.2584 

AF7337 

4,0 

Pate I orl 

5.0 

1.64 

1.94 

3.13 

6.0 7.0 

211804262 

9481706 

~4786 

8.0 

416212~ 

1656626 ' 

49735778 

CuneM D.ftc : l008J08121 

Curr<* Time : I S:QO::S2 . 

VES 005602 
Sample Analysis Report· 

Sample Name : AF7338 

Data FOe Name: C:\l'EAKNE1\DATA\ANIONS\DX·l00\AD!ons...AXW012.DXD 

lAW Range Detector: Ul20 Universal Inlelface 

Mtthod FUe Name : c:\peaknel\melbod\3008nions.met 

· Sca.idole File Name: ... laniondl821.sch 

Dere Time Collected: 2008/08/ZI 3:01:48 PM 

Sysrem Operator : U..E 

'Calibntion Dare : 2008Al8120 4:33:03 PM 

Calibral'ion Type :EXTERNAL · 

Component Amount Units : mg/L 

Dilution Factor : 10.00 

Peak Information : All Co!nponents 

Peak # Component Gomponent Name · Coniponent Peak Retention Peak Area Peak Height. 

· Number · Amount (mg/L)Time . 

: 

<I) 

2 

3 

4 

"-

2 

3 

5 

10.0 

8.0 

6.0 

4.0 

2.0 

0 

0 

II :P~et.S.l 

Chlori~ 

N'rtrire (as N). 

Nitrate (as N) 

2 

I 

l i , 1i I 

I I 

1.0 2.0 

4 

I 

I 

I 

3.0 

#.3538 

0.8511) 

29:5624 

AF7JJ8 

4.0 

Poio I of I 

5.0 

1-«>:i 

1.93 

3.12. 

6.0 7.0 

194726450 

6473045 

311781731 . 

8.0 

38027390 

1132809 • . 

386517i I 

Glnent Di.e: 2003108121 

C'tirrtllt Time : IS:09:S2 

VES 005603 
.. 

Sample Analysis Report 

Sample Name : AFT.l39 . 

Data File Name: C:IPEAKNE'N>ATA\ANIONS\D"·100\Anlons..AXU013.DXD 

Low Range Detector: UT20 Unive,ml Interface 

Method File Name : c:\pea nel~lhod\300anions.met 

Schedule File !:lame: ..• \anions082l.sch 

Date 1iq>e Collected' 2008/0SI21 a: 10:47 PM· 

System Operator: LLE. 

Calibration Date: 2008/08120 4:33:03 PM 

Calibration Type : EXTERNAL 

Component Amount Units : mg'L 

· DiiU.tion FactQr : 1.00 

Peak lnformatioo : All Components 

Peak It Component ·component Name Comp<ineot Peak Relention Peak Area Peak Height 

Number 

I I PlllQride 

3 2 Chloride 

4" 3 .ffltrite (as N) 

6 7 Sulpbate . 

. 10.0 I 

8.0 

I 

6.0 

"' "" 4 . .0 

12 3 I I 

s 

2.0 

I 

V\1 

0 

I 

0 1.0 2.0 

II : PeUNet S.2 . 

Amount (mg/L)Tiro.e 

1.9983 1.15 

3._7.394 1.45 

4:5458 . 1.94 . 

18.3169 6.35 

AF7339 ....., 

t 

3.0 4.0 5.0 6.0 

Pate I ott 

9 

A 

. ' 

127922793 31334260 

. 154405982 295.24633 

\ 1 

7.0 

44~08468 81292425 

575209348 "40199205 

8.0 

Cine. Oaae : 2008108121 

Curtett11mt: t5:t8:..S) 

VES 005604 
.,...~"':"": 

~~\: •: 

.SaQlple A~aly.sis Report 

Sample N~ : AF7339 

D.ola Flk N'IJDt: Cl\PEAICNE'N)ATA\ANIONS\DX·looiAoioos.)\Al087.DXD 

Low Range Detector: UI20 Universal lnlerface 

Metllosl File Na~: c-.lpeakliellrnelhodl3ooailions.met 

Schedule File Name: •.. laoions<f820.$ch· 

Date Time.Collceted : 2008108121-12:49:58 PM 

Sys1em OpemtO< : ll.E 

Calibration Date: 2008108120 4:33:03 PM 

Calibration Type : EXTERNAL 

Componein Amount Units: ing/L 

Dil~tion Factor : 10.()0 · 

Peak Infonnation :All C~ponents 

Peak # Cnmpooeat 

Number · Colppoa.ent Name Cnmpo~t Peak Retelllioo · Peak Area Peak Height 

·Amount. (mg!L)Time . " 

I . I Fluoride 1.9132 ·h'o 1.15 10864232 ~%,230 

3 z · Chloride 4.()_854 ~'·.' · ... 1.65 15116813 ~1947 

'4 3 Nitrile (as N) 4.5131 !:·R::: 1.94· 38809896 664S!i()l 

6 5 Nitrate (as N) 30.7477 3.14· 325480142 41294950 

7 7• phate 18.4033-. 6.42 502731~ 3$07448. 

A.F7339 

10.0 

8.0 

6.0 6 

I 

"' "- 4.0 

i 3 4 7 

2.0 1 I JJJf I I . ! ! 

0 I I i 1 1 

0 1.0 2.0 3.0 4.0 .5.<) 6.0 7.0 8.0 

II : Peal:Nct S.l 

Qwrcnt Daae : 200810812 I 

hle l of1 Qaru,I:Time: I2:SS:II 

VES 005605 
Sample ~milysis Report 

Sample Name : CC'..B 

Data File Naine : Ci\PEAKNE'N)f. TA\ANIONSIDX·lOO\Anloos_A W0016.DXD 

Low Range Detector : U12Q Universal lnterfa<:e 

Method File Niune : c:lpeaknetlmelhod\300anions.met 

Sclledul.e File Name : ... \anions082l.sch · · 

Dale Time Co~ : io0810$121-3:)7:43 PM 

Srstem Openuor : rp; 

Calibratioo Dace : 2008108120 4:33:03 PM 

cilibralion TYPe : ExTERNAL 

Component Amount Units : mgiL 

Dilution Factor : 1.00 ·• 

Peak lnfo'!JI.&tiOn : All Components 

~·:.f . • , 1 

Peak It Component 

Number 

. . Component Name Component Peak Retention 

Amonot (mg,IL)Time 

Peak Area P~k IJelgbl 

.:f: :;:' . 

10.0 

8.0 

6.0 

(I) · 

"' 4.0 

2.0 : t . I 

0 I. 

0 1.0 2.0 

II : I'WN<tS.2 

CCB 

3.0 4.0 5.0 6.0 

Paa.elot'l 

·1.0 

'· 

· .. 

8.0 

Cattm Date : 2008108121 

. CWYICOI'nrt.e: tS:,.S:48 

VES 005606 
Sample Analysis· Report ,, 

Sample Name : 'ccv. _Data File Name i C:\PEAKNE'IWATA\ANIONS\DX-100\Anions_AVWOI7.DXD 

Low Range Detector : UI20 Universal Int~rface 

Medtod Pile Name : c:\peaknet\methodl300anions.met 

Schedule File Narpe: ... \anioos0821.sch 

·Date Ti111e Colle<:ted : 2008108121 3:46:42 PM 

Systell\ Operator : I..LE · 

C:llibratioo Date: 2008/08120 4:33;03 PM 

Calibration Type : EXTERNAL 

Component Amount Units: mg/L 

Dilution Factor·: 1.00 

Peak Information·: All Components 

Peak II Component Component Name 

Nnmb~r 

2 1 Fluo!idt 

3 2 Chloride 

4 3 Nitrite (as N) 

5' 4 Bromide 

6 5 Nitrate (as N) 

7 6 Pho<phate-ortb? 

8 7' Sulphate · 

10.0 

8.0 

6.0 

II) 2 3 6 "' 4 

4.0 I I I 5 I 

I 

2.0 I ' I l \1 I /\• \ I 

0 l I 

0 Lll 2.0 3.0 

Component POak Retention . Peak Area P<;&J< H.eigbt 

. Amount (mga.)Time 

1.9583 1.14 

2.9371 1.64 

1.4795 1.92 

5.9676 2.74 

1.9774 3.08 

5.9078 4.89 

11.8635 -6.26 

CCV 

8 

7 AI I . 

/\ i 

I ! 

4.0 5.0 6.0 .... 

Pate I of I 

7.0 

12525067,6 . 23747474 

11944~51 22893094 . 

13i8i5LS8. 23081!)()9 

104713176 ' 155tn642 

202215649 ' 26383157 

221838869 18219807 

360432086 25107134 

8.0 

Cll.11'tftl o* : 200&'08121 

ciwn:.l Time : IS:S.C:49 

VES 005607 
. . Sample Analysis Report . ~· . 

Salllple Name : AF734l . . . Dala File Name : C:\PEAKNE'l\DATA\ANIONS\DX-100\Anloos....A VL018.DXD 

Lo"" Range Detector : Ul20 Uni~llnlerfacc 

·t.fethOd File Name·: c:\peaknet\J!lelhod\300•nionunet 

Schedule File Name : _,\anion5082l.sch 

Date lime Collecte<l: 2008/08121. 3:55:41 PM 

System Operat9< : u.i · 

Calibration Date: 2008108120 4:33:03 PM 

Calibrlllioo Type: EXTERNAL 

Component Amount Units : mgiL 

Dilution Factor: 5.00 

Peak 1 Component 

Number 

;2 • I 

4 2 

s 3 

6 7 

10.0 

8.0 

6.0 

4.0 

2.0 

0 

0 

Ill : rtaa.Ntc ).2 

~k Information : All Compone.ots 

Co!Dponent Name Cqmpooent Peak Retention 

Amount (mg/L)'Iime 

FlU«! de 

Ollciridi 

Nitrite (a$ N) 

· Sulphate 

4 

2 s 

l1~ ~ ll l I I I l 

L.O 3.0 

2.67~ 

20.5131 

1.6012 

89.8!'39 

ltfl73of2 

4.0 

hac I ori 

5.0 

1.14 

1.64 

1.92 . 

6:25 

1 

6.0 7.0 

• 

.. 

.;. . Peak Area Peak Heogbt .•. ,:f· .... 

• 

3262225~ 

17058,6772 

27171486 

563068787 

~ 

.,. ' ' ' ·'-' 

.. 

. · 

8.0 

4836>470 

339711023 

4902309 

39694752 

Clln'tllll OIIC : l008108/21 

Cum:11t nme : 16 03 49 

------------------·- - -------------

VES 005608 
·• 

S'!lmple AnalySis Report · 

Sample Name : AF'734Z 

Data File Name: C:\PEAKNE1\DATA\ANIONSIJlX-100\AJiions_AAI088.DXD 

Low RangeDetect9r: 0120 Univeo;al In.tcrface Calibratioo Date : 2008108120 4:3~:03 PM 

Med!od P'llc Name: c:\peaknet\melhod\300ailions.ruet Calibr!'lioo Type: EX'IllRNAL. 

Scbcdule File Name : ... \anions0820.sch Colll[lOiltnl Amount UniiS : mgll.. 

Date Time Collected : 2008/08121.12:58:5'1 PM . Dilution Factor: 10,00 

Sy&iem Operator : LLB 

Peak Ioronnatlon : AU CompooentS 

Peak • CompoDa>t Compo~>ea.t Name Comp<>Dea.t Peak Retendon 

Number AII>OW!t'(mgiL)Thne 

I I Ruoride 2.6917 I:IS 

3 2 Chloride 19.8144 1.66 

4 3 Nitrite (as N) 1.6767 1.95 

s s Niu:ate (as N) 61..7933 3.14 

fj 7 Sulphate · 87.3835 6.45 

AP'TJin 

10.0 

8.0 

6.0 

~ 4.0 3 6 

' I 

2.0 A 4 .I r: d! , j 

0 i i l 

0 1.0 2.0 0 4.0 5.0 6.0 7.0 

Peak At"d Peale Heigbl 

\ 

157~1 2396748 

78995064 JSIS36112 

13714858 2388089 

81971 1~ 90116964 

260921537- 17939862 

8.0 

Oancnc 0.1c: : lt'OMlSI'21 

Curmlt 'l'1mt-: 1);07: I I 

.. ---·---- - --

VES 005609 
-r . ... ~ . ~ ~ ;1; • • '-1-' 

. "" Sample Analysis Report 

V.: 

Sa01pl.e Name : AF7342D :~· 

Data File Name.: C:\PEAKNE'N>ATAIANIONl>'\DX-100\Anloos...-'UWOl 9.DXD 

... 

.. 

LOw Ran&e Detector : UUO .Uoiversallnlerface Calil!ratioa bare : 2008108~ 4:33:03 PM . .. l'>fllhod File Name : c:\peakilet\m¢tllod\300<utionunet Calitiratloo Type : EX'Il!RNAL ... ~t"f;' 

Scllc-.dule File Name: ... lanions0821.ocl\ Component Amount Unit$ : m8/L 

Dale Time Collec:kd: 20081081214:04:40 PM Dilqtion Fa<IX>r : 5.00 ' 

Syllem Operator : lLB . - ' ... 

. .. Peak Infarmati<in : All Components 

Peak I Component Compoaent Name 

Numba2 I Flu<Jride 

4 2 Ebl<Jride 

s 3 Nitrile (as N) 

6 Phosphate-ortho 

6 7 Sglpba1e 

10.0 

8.0 

6.0 4 

~ 4.0 

I 

2 5 

2.0 l. l .3 

i it\_ i I ~ I 

0 . II ; ' J ' . ' i 

0 1.0 2.0 3.0 

li1 : PQtNet .u 

Componmt· Peak Retentl001 P.eak Am Peak Hei&bt 

AIDOUill (~)Time . ..,, . '~"~~~ . ... f "" r: . 

3.2289. --~- us 396227~. 5413470· 

20.4754 ' .1.66 1702481 . . 35290214 

1.3345 ··:ti 1.93 ' 2l4SS , . 3954489 ·. 

' - ·t:'~·· ·'lt 

87.6657 ~. ,., 6.31 . 5483~3 i 38272963 ··:··.· ·.:. , . .. . . ;:;- . . -. .. 

.·. ,:, .. :~~. 

·. 

,•: 

·;J,.,,• 

,·. 1f. 

~·~~-· 

A.P73nD 

6 

A 

__ \I 

4.0 5.0 6.0 7.0 8.0 ·; 

h,t<lofl 

(j--:-c :J-O·lff!5'fl p!YJ 

Iii ;.aJf·~l· ).2 C.ntaOnc: 200&U/2.l 

CllrmtTiftle : 16:11:44 

·. 

VES 005610 
w· ., . 

. , 

~ .. ;. 

Sainple Analy~ Report 

Sa1bplt Name : AF7343 . 

Da1t1 Fil.e Nam~: C,\PEAKNE'N>ATA\ANIONS\DX lOOIAJJio~_AUKOZO.DXD 

Low Range Detector: Ul20 Univen;al lnletface · 

Method File Name : ~lj)ealcnet\method\300a ions.met 

Schedule File Name : ... lanionsOSZ I .sch 

Dale Time Coli~: 2008/081214:13:39 PM 

Syltem Opcrntor :.IJ£ 

calibration Date: 2008/08120 4:33:03 PM' 

Clllibtation Type : EXmRNAL 

Component Amount Units : mgll.. 

Dilution factor: 5.00 

Pea.l: Information : All Components 

Pcakf~t 

Nlllllbu · 

2 I 

4 2 

5 3 

6 

6 . 7 

10.0 

8.0 

6.0 

'a 

4.0 

2.0 

0 

0 

IIJ ·: Ptu.Hct.U 

Compooent Nllllt cOm~t Peak Reteotion Put Area Puk Height 

Ar:aocurt (mg/L)Thne . ·~ .. 

-Fluoride 

Chloride 

1-1 

Nitrite (8$ N) 

Ph9spbJUe-ortho 

SUlphate 

4 

I 

s 

~~~I j 

1.0 2.0 . 

"·· 

A.P734J 

3.0 4.0 

h~ttloll 

5.0 

1.16 

1.67 

1.!)4 . 

6.31 

I 

\i 

1.0 

43751928 566!982 

284346501 . 59286~8' 

2S51p79 4520082 

734015349. 5JI60619 

8.0 

Cumet OIIC : lOQ&,'()$121 

OntntTimc : 16:21 :4S 

VES 005611 
Sample Analysis Report 

Sample Nllmt : AF7344 

Dola F.lle Name: C:\PEAKNE'N>ATA\ANlONSIDX·lOO\Anious..J<'fZOZLDXD 

Low Range Detector: UI20 Universal buerfa~ 

Melhod File Name : c:~lmethod\300anlons.niet 

Schedule File Name : ... lanions082l.sch 

Dale Time Collecled : 2008/081214:22:38 PM 

S)'llean Operator : u.B · 

Cllibnili.oo Datt: 2008108/20 4:33:03 PM 

Callbtadon Type : EXTERNAL · Compoueot Amount Units : mgiL 

Dilutioo factor: 5.00 

Puk lnronnAtioo : AU Comi>onenu 

Peak I Compooeot Compontol Name Compooent Peak Retentioo 

Amount (m&IL Tl~ . 

J'eak AI'U hal< H.t 

Number 

2 I FluQride 

4 2 Chloride 

s 3 Nitiite (.as m 

6 s Nill]lte (l$ N) 

7 7 Sulphate 

8 Iodide 

10.0 

8.0 

6.0 

"' 4 .. I 4.0 

2.0 

0 • 

0 1.0 2.0 3.0 

3.3614 1.16 

17.3340 1.66 

1.9210 . 1.94 . 

39.2511 3.04 

68.23~8 6.30 

AP7:u4 

4.0 s.o 6.0 

Pa~~Jt I of I 

7 

I 

1424~860 

41314131 

2912575? 

~ 

32840947 5696122 

999401098 9012696~ 

. 418471207 29366343 

. 

7.0 8.0 

Cum:nt O.et : 20081081Z-I 

O.rteol T~ : ! 6:30:.46 

VES 005612 
•' 

S;~mple Analysis Report 

Sa11ple Name : D·SPIKED . 

Dala File Name: C:\PEAJ<NE'N>ATA\ANIONS\DX·l00\Anloos..AUJ024.DXD 

Low Ra"'e DeiOCU>r: UT20 Uoivet>lllnterfaee 

Method File Name : c:lpeaknet\method\300oos.mel 

Schedule Pile Name : ... laoiocu0321.sch 

Datt Tune ~cted : 2008108121 4:49-.35 PM 

System Opera10< : u.e 

Calibmioo Dm: 2008108120 4:33:03 PM 

Calibiation Type: EXTERNAL 

Component Amount Units : ftli/L 

Dilution Factor : 2.00 

Peale lnfoi'IIUition : ~II Components 

Peak 'II . Component Comp<inent Name Compooe~~.t Peak Retention Peak Area Peak Height 

., 

2 

3 

4 

"' 

Number A10001nt (mg!L)~ 

I 

2 

3 

10.0 

8.0 

6.0 

4.0 

2.0 

0 

. 0 

Fluoride ' 

C!ioOOe' •. 

Nitrite (as N) 

3 

I 

4 l!2 I : -j \IA. l 

11 ; I 

1.0 2.0 

r3.0 

0.4618' 

10J)343 

1.281) 

B-SPTKBD 

4.0 s.o 

1.17 

1.66 

1.94 . 

6.0 7.0 

133SlS92 

212338011 

SS798336 

8.0 

888214 

30497368 

1.663214 

0......-: :ztlOI/Oit21 

o.we.n.:n::: ~~:42 

VES 005613 
. . 

Sample Analysis Report. 

Sample Name : II-SPIKED 

Data File Name: C:IPEAKNE1\DATAIANIONSIDX-IOOIANIONS.,AUJ02CI.DXD 

l..o1v. Ran go Detcetor : VI20 Universal lnterfll<:e Calibration Pare : 2008108120 4:33:03 PM 

Method File Name : c:~lmethod\300an s.mel C•llbration Type: ~AL 

Schcd~le File Name: ... \aD\90~2l.SCb Component Amount Units. : mgiL 

Dote Time Collected: 200Stll8/21 4:49:3S PM Dilution Factor : 2.00 

Syaein Operator : ll.E 

Peak Info~tion : All CODljlODcnts 

Peak j Compooenl Compo~! Name Componeat PUk Retention 

Number Amoont (aog/L)1ime 

2 I Fluoride 0.4618 1.11 

4 2 OtJOride 9.8S44 1:66 ' 

s 3 Nitrite (as N) I.U23. i.94 . 

.. 

B-SPIKBD 

10.0 ,..... 

8.0 

6.0 

., 4 ... I 4.0 

s 

2.0 I 2 ·t 1j1 I lli\ 1 

0 I I I I 

0 i.G z.o 3.0 4.0 s.o 6.0 7.0 

ho. l otl 

Peak Area Peak Htight 

l33S3S92 888214 

203164925 30497368 

SS798336 7663274 

8.0 

o.ntna Due : liXl8K4I2l 

CuntlliiTimt ! 11:J6:Sl 

VES 005614 
Sample ~alysis Repol"t 

Sample Name: CCB 

Dita F11eName : c :\PEAKNE'l\DATAIANIONS\DX-100\Anions_ASR025.DXD 

Low Range Detector: Ul20 Univers~llnterface Calibra#on Date·: 2008108120 4:33:03 PM . 

Mctllod File Name: G;lpeaknetlmelhod\300anions.met CalibratiQO Type : EXTERNAL 

Scbcdule File Name : ... lanions0821.sch C<lmpooeat Amoun1 Units : mgll.. 

Date Time Colleclcd : 2008108/21 :58:3~ PM 

System Operator: LL8 

Dilution Factor': 1.00 

Peale Information :AU C<lmponents 

' Ptak I Compooent ComponeDI Name Compooe~~t Peak· Retelllle>o 

Number Amount (mgiL)Time 

CCB 

10.0 

8.0 

6.0 

<g_ 

4.0 

2.0 l I 

0 I 

' 

0 1.0 2.0 3.0 4.0 5.0 6.Q 7.0 

~~ ' l'utNel S.2 ~lof'l 

Peale Area Peak ~~ 

8.0 

Cum.M o.~ : 1(108A)8121 

O.IT'tfll -nmc : 17:06:41 

VES 005615 
i 

i 

-·--·

-~. · · . ... 

Sample Analysis Report ; 

Sample Name : CCV· · 

Data File Name : C:IPEAKNE1\DATA\ANTONSIDX·l001Aniom..i\SGOZ6.DXD 

Low Ritnge Detector: !1120 Universallnter[ace 

Mc.thod File Name : c:\peaknel\method\300anions.met 

Scl)edulc File Name : ... \anioos082l.sch 

D11e Time Collected : 200&'o8/2J 5:07:33 PM 

System Operator : LLE 

Calibration Date : 2008108120 4:33:03 I'M 

Calibration Type: EXTERNAlComponent Amount Uhlts : rng/L 

Diiution FO!!IO<: 1.00 

Peak lnformalioo: Ali Components 

CompontD~ Name Component Peak Reta~tloD Peak Area Peak Jldgbt 

AllloDDt (mg(L)Thne .., 

2 I Fluoride 1.9971 I.IS (21846196 2422&5!2 

4 2 Chlolide ).jl229 !.65· 123112921 234%067 

~ 3 Nitrite (as N) 1.5201 1.93 13663643~ 23675loi 

6 4 Bromide 6.0914 2.76 107002227 16129933 

7 5 Nitrate (as N) ~87 3.10 207812239 27790214. 

8 6 Pbosphote-<>rtlto 5.9529 4.93 22~662971 ' 18539:127 

"9 7 Sulphate 12.1665 6.31 370225002 26470281 

CCV 

10.0 

8.0 

6.0 

., 7 9 "' I 4 I .0 

2.0 

0 

0 1.0 2.0 3.0 4.0 s.o· 6.0 7.0 8.0 

II : l'ea!CNtc S.l . OIRUII Oaac : 2008108121 

Pw I of I Ou'ruttTimc ; 17:1S:J7 

VES 005616 
. ;; : .. ' . 

S~mple Analysis Report 

Sanple Name : CCV 

Data File Name; C:iPEAKNE'NlA TA\ANIONS\DX·~OO\A lions.J\RYOZ7 .DXD 

Low Range Dete~: UI20 tiniverul loterf~te 

Mttbod File Name : ~:\pealcnet\methodiJOOuiionunct 

Scllcdule File Name: ... lanioos0821,sch . 

Dille Time Collected : 2008/08/22 9:55:49 AM 

System Ope.ator: lLE 

Calibration Date : 2008108/20 4:33:03 PM 

·Calibcilian Type : ~AL 

Compon<Dt Amount Unh$ : mg!L 

Dilution.Factor : 1.00 

Peak l:lfon:natiOD : AJJ Compoocu!s, 

Peak t CompoJient 

Nu.mWr 

COmpooeot Name ~ :V •Peak Reteotf.on Peale Aru Peale lleiiht -· . AIIIQIIA1 (lDg(L)Time ... - (-. . ~ 

2 J Flu<lride 1.9828 - ·. . 1.14 

3 2 f 

·' O.iorjde 2.92'34 ·~-: ....¢~"-.J.64 .· ·- ~-- . 4 3 :!'litrlt; (as N)' 1'.4710 .. " .. · 1.93 . 

s 4 Br~ 5.90'7Q ,. ·;, :in 

6 5 Nitrate (as N) 1.9618 . .3.11 

7 6 · Pbospba~nho 5.8383 . ·4.91. 

8 ·1 Sulphate 11.7449 6.30 

'. .. 

.. '" ' 

CCV 

10.0 

8.0 

6.0 

"' 2 4 6 .. 3 4.0 I I I I 

2.0 I, 

II 

0 I i 

0 1.0 2.0 3.0 4.0 5.0 6.0 

II : PutNa s.z Pqc.lo(l 

8 

I 

7.0 

126887222 23845488 

118830320 21899912 - . 

IJ202S002 22665855 

103593925 15215956 

200513338 25957905 

219034852 1(672816" 

356603117 24342024 

8.0 

~Dote 2008101112 

()wTUit1"~mc : t0:03:S3 

VES 005617 
:-

Sample Analysis Report 

Sa01ple Name : AF7340 

Data Flit Nilme: C;\PEAKNE'NlATA\ANlONS\DX·IOOIAoions..ARW028.DXD 

Lo" Range Detector: UI20 Unjvers•llnterfa<:e 

Mctl1od Fil6 Name: c:lpeakneflrilelhod\3o0anions.met 

Schedule Pili Name : .. ,\anionsOall.sch · 

Dale Time Col!ecled: 2008108122 10:04~ AM · 

·System Operator: lLB 

Calibration Date: 2008108/20 4:33:!)3 PM 

Cillibrali9o Type: EXTERNAL 

Component Amount Units : m&IL . Dilution Factor : 2.00 

Pea]< lnfonnatioo : Ajl CompooeJns 

P<alt I Compooeot 

NUIJibtt 

Cl) 

3 2 

4 3 

6 

6 7 

10.0 

8.0 

6.0 

,. 

4.0 

2.0 

0 

0 

Com~ Name 

Chloride 

Ni!rite (as N) 

Phosphate-!)rlho 

Sulphate 

4 

I 

h 3 s Jli ~ i. 

j 

! 

1.0 2.0 3.0 

.. Coml"""'it. Peak Rdeo&D 

ADIOOat (ui'gli)Time 

:· 

4- 0.81SO '€.·.:,. 1.65 

4.6UJ· 1.94 

,_ 1.2443 .,. 

. ' 6.35 

" 

A.P1340 

?_I 

I 

•1-.0· s.o 6.0 7.0 

Paatloll 

Peak A~• Peak Beigllt 

· l626S376 31401S6 

212405286 386!9129 

14246888 IOSS660 

8.0 

O.:tcnl o.tc : 2008108122 

CumDt Time: 10: 12:5) 

VES 005618 
Satllple Analysis Report 

Samplt Name : AF7340 

Data FUe 'Name: C:\P~KNE'NlATAIANIONS\DX·lOO\Anions...A WX014.DXD 

Low Range Detector: UI20'Universallntertlce 

Method File Name : o:\peaknclXmetbod\300anions.met 

Schedule File Name : .. \aqio<is08~ .sch . 

DaicTimc Collected: 2008108121 3:19:46 PM . Syttem Operator: u.E · · 

Calibration Date: 2008/08120 4:33:03 PM 

C8U!l<a~on Type : EXTERNAL 

Co!Dpooent AII\OUnt !)nits : mg/L 

Dilution Factor : 1.00 

Peak Information : AU Co)Tlponents 

Patk ' Componen! 

Number 

Compoueal Name Compooent Peale R~tmlloa Puk Arp ~k Heigbt 

Amount (mg/L)Thne 

2 I Fluoriile 14.4947 1.24 1443718228 8766235 1 

3 2 Cbloride 0.8981 1.66 34667154, 7206069 

4. 3 Nitrite (as N) 4.6iJS . 1.95 . 458664906 $47159i8 

4 Bromide 

6 1 Sulphate 1.2345 6.43 32315146 2281376 

AP7340 

10.0 r8.0 

6.0 

'a 

4.0 s 

3 I 

2.0 ~ V\ , 1 I \ 

0 I J l 

0 LO 2.0 3.0 4.0 s,o 6.0 7.0 8.0 

""""' l>ou : 200WS/ll 

hu I oil OJ(re.U Time ; I S:l7:S3 . 

VES 005619 

Sample Analysis Report 

Sample Name : AF7341 . 

Data File Name : C:\PEAKNET\DATA\ANI6NSIDX-100\Anions_A WSOIS.DXD 

Low Range Detector': Ul20 Univ.:nal lnterfaoe 

!llelbod.File Name: c:'fleal<roel\mothod\300anlons.met 

S<hedule File Name: , .. \anions()821.s<:h · · 

om' Tin;>e Collected : 2008108121 ·3:28:44 PM 

~ystem Oper.rlor : Ull 

Calibration Date : 2008108120 4:33:03 PM 

Calibration'Tyjie : EXTERNAl. 

Compoooot Amount Units: mg!L 

Pllutioh Factor ; 1.00 

Pl:ak lnfonnation : AU Components 

Peak II Conrponeat 

Nalllber 

Compoli<Dt Nanae Compo;;_..t PeU R<ttDiioo Peak Area Poak Height 

Amollll1 (mllfL)'Thne 

2 2 O>JO<ide 0.6077 ; .1.66 23036985 5502435 

3 3 Nitrite (as N) s.403? ~ 1.96 SS1963SSS 8919,0941 

' 4 Bromide ' . 

s 7 Sulphate 1.0979. 6.38 28278107 1984169 

II :PutNecU 

Oln'ent Ollc : 2008J06IZ I 

Pw I oil Cwm!t1'iow:: 1$:'36:-43 

VES 005621 
. 

Sample Analysis Repi>rt 

Sanple Name ~ CCB 

Data File Name : C:\PEAKNET\DATA\AN10NS\DX·l00\Awoo5..ARR032.DXD 

Low Range Derec10r: UI20 Unlve,.allnlerface 

Method File Name : c:\peaknetlmethod\300anion¥.met 

Scloedulo F'ilc Name: : .. lanioos0821.sch 

Date Time Collecied: 20081Q8122 10:40:44 AM 

System ?perator : ll.E 

Catibratioo Date: 2008/08120 4:33:03 PM 

. Calibration Type : EXTERNAL 

Compon011t An>ount Units.: mg!J.. 

Dilution Factor : 1.00 

Peak lofonn1tioo : All Com~nu 

Q>Dlj>OIWit Name CompoDtJ>t Peal\ Rettolloo Peak Aru Peak H~~t 

~!lW!l (m&fL)Thue 

CCB 

10.0 

8.0 

6.0 

"' .. 4.0 

2.0 

0 

0 1.0 2.0 3.0 4.0 

II : Pu.lN.ct .U Pate rot I 

' 

· . 

. , 

5.0 6.0 7.0 8.0 

~ Dltt:21X1&08fl2 

Cun tlll Time-: 10:43:47 

VES 00562.2 
. ,. .... ' :;;r.: .. . 

Sample Analysis Repo~ 

Sample Name: CCV 

Data File Name: C:\PEAKNE'I\DATA\ANIONSIDX·lOO\Anions,._AR0033DXD .. 

Low Range Deleaor : Ul20 Univeriallnterface Catibratioo Date : 200&108/20 4:33:03 PM 

Method Ale Name: c:lpeaicnetlmethodl300anions.met Calibration type: EXTER!"AL 

Schedule Hie Name: ... \anions082l.s!'h <:;omponent Amount Uohs : mg/L 

Date Time ColleOted : 2008108J22.10:49:43 AM Dilution Factor: 1.00 

System Operator : u.s .• 

- ·Peak J,nfoonation : AU Componeots .. 

Peak I Compo-' ComporteD! NatDe 

Number 

2 I Fluoride 

3 2 Chloride 

4 3 Nirlite(as N) 

. 5 4 Bromi<le 

6 s Nilll!te (as N) 

1 6 Phosphate-ortho 

8 1 Sulphnte 

10.0 

8.0 

6.0 

"' 2 3" 4 6 ... 4.0 I I I I 

2.0 

0 

0 1.0 2.0 · 3.0 

' Compooeof Peak Retention :; Peak Area Peak Heigbt 

Amount (mgll,.)'l'ime .. ' 

•·. :··,; 

' tl .... 

1.9622 1,15 . , 125508573 2352926()• 

2.9S87 1.65 <; t203mn 2238~ 

1.4908 1.93 . ;, 1338"81442 22674.812 

5.9699 2.16 ·~ . 104'756164 15395567 

i.9913 3.09 203734111 26557040 

. 5.876.1 4.9~ 22056I9ii 17810080 

11.8500 6.31 36oi8~4 25013022 

· .

. :.· 

CCV 

8 

I 

4.0· 5.0 6.0 7.0 8.0 

Pue I of I 

OlcftN Om: 2008i08IU 

Curr=cTime : 10:57:49 

VES 005623 
' 

Method 7471A -:-Mercury In Solid Or 

Semisolid Waste. 

Milxxaril Analytics Inc .. 

6140 Campobello Rd. 

Mississauga, Ontario, Canada, 

LSN2L8 

l-800-668-0639 

www.max:xamanalytics.eom 

VES 005624 
.. 

- IISoilbyCVM•Soi 

(Ufllill 

~~~ ..... -~ 

. ..;, , . 

.~· 

VES 005625 
• 

0. i 

RUSH ~ 

" 

: 

-

d 

~ 

:s 

· 6 

( 

IJ 

I 

·. I 

( 

~ 

l 

Rcpon ~-: WO<I: Sk¢. (Uquids Olld Solids) 

A.tsi--Dite: llwnday; Augwt21,2001 

Alliped 10: PUSIIPA BIIARDWAJ 

f : 15925117 

Test Cocke HO·S lt1SU'\ll'.nCnt ld: 

Tau Dcoui1•ion: TO DETERMINI! fER.CURY BY COIJ) 

VAPOURAA. 

Job S~e 'll 

N ....... l'luonl>« D San1lleiD P MoiR 

WTRX SPK U't_ ICP2 AJI66n.<)l 

REP MAT r.9'f SSIDol. .Jl:.f(, 

BLANK 

A891112 ~IR ABDJIJNEOI tJ,S 

;..ulnz AF46Z1.01R ABDJUi.Yoa /),0 

AI914&S Am16-0IR WCSS· I f) . 

AS914SS AF6677.01R 0 WCSS·2 AlP . Al9141~_ AF6<117.01R I . wcss.2 0 /JI . 

.AI914SS AF 7S.O R wc.si1 · ')(.. hl ~q 

A8914U AF6679.01R WC.SS-4 /It' 

t.m~4a AF7342-0IR CS.UZ..Rl )C 10 ,. t. ao 

'A891648 AI'734J.OI R CS.UZ.R2 ~ fb - 'J:J'}_ 

' A891648 M1Jolli-O 1 R CS.UZ.R3 x.ro ' t.t/ 

•AI929lS AG126S-OIR TANK BACKFILL ~ 

' AI9292S A032~1 R WSW .ko. 

WI 

ot Filla! 

Vol Vol 

~l ~ 

o,.p 

CUIO 

OSlO 

0..110 

o:s2o 

(1 .... ,. 

O.SIO 

. 0.520 

O:soo 

0.506 

0.510 

O.SIO 

0..110 

r~ •AI92:91S A03271-QIR FLOOR I ,M:1 o.soo . 

.. . ....... 

f--1-"' 

-- . .............. --

--

--RSlmpl ............ by: PIJSf!lA DRAitD~AI 

-pod-by. 

Cokulallooo.,.._by. 

V-by. ~ 

P1id: I of I 

, 

DF 

or . • llxJ>irl' Tosl 

AF . learu Date o..dllac C>il<ria 

·. 

· I :!00&'06/IS 200WII'.I2 I 8:00 

I 200&1nl1S 2 11:00 

>.( 200Mll/19 200110&'2lii:OO 0 

·· 2 . 200Mll/19 200Mll/22 -18•00 

... 2 200Mliil9 200Si01122 I 1:00 

I :ro08/08119 18;00 

2 zoOsrol/19 200111UI!I22.J 8:00 

2 2008/0S/18. 2008101121 17:00 

2 2008101119 200Mlll21 t7:oo 

2 200Mll/2ll 2o0Solll/21 17:00 

I 200Mll/27 17:30 

I it"lO -~ I 200SIOSIZ7 ~u..rf ___..... 

~ 

! 

~ 2 t:..o.d,u-7'!::1. 

0...: 1-r 

Dsrc 

· oaro: 

VES 005626 
.. 

/.Qll..l:ig, Ia C!l;ot N!!p! 

MA891l i:M.CRSI LaWTen .. Cemea!·Ine 

MAI9148s:Ji.M Goolvar Ontario lne 

........ 

I 1• l""n-eetation Ranmlcs 

RUSH 

1: lS92S87. 

~ 

Or. June• P. 1obswon 

Tabitha Lee 

El& . il&:miiU . (905)82Z-2A9l Plcase"'!C'l;,alyll.oiflcocahbolcl'b;. ~­

SmaJ'I..; do Dot read ~c to wcbivin&; intomt 

Moria Uy or MCR after wei&b!•C· Project~: SOUD 

SAMPLES 

. NATiONAL: St IAwrt•ce Ce111rac lAc 

(905)475-599-4 s•Tt ProjeCt#: 08-116-IO 

. NATlONAI. CROUPtOQNS£1!-CEI«V~ 

INC 

(315)437~ RUSH ICP+l!G, TOTALOILORIDBS,Im.l, 

%ASH. SUB TO PSC RI!PUBUC W ASre FEEDS 

Proj<a f : I 002.-011 

NA110NAL: INSitlNTUNA~NAL . 

(416) 391-1931 RI!O.I Sl, T ~1.83/1 OO!hlo Pr•jecU: 1'3381 

. NAnONAL: CII,U It T'rM.Ebllll< (CTl) · 

M<lhod S!ril:e 

-

VES 005627 
-~In< . 

811 

tc~• ol 1 .. 

Pnip Batch Reagent Tr.acklng Record · Worksheet#. i 'S."''l."~ g 7 

Volume lull 

Sunoliate/Splke iolulions Solllllon 10 ~ Cone. Blk:spk MS . .Sampl•• 

.. 

ICPMS 

!CAP ICI' SoH Spk. A(SPK-08-0a)&B Variable 1ml/SOn!l. 

Gf'~ ., . . 

Hg Hg Splke(Hg Spk-08·08) . 0.25ppm .'1ml. /SOn!!; 1-:l- i 

.. 

'SOlvent SuppUer Lot No. Splkod by; 

HHO, tiShet 308144 PIH 

HQ Roher 206051 "Spllclng W'rtneeaod by: 

HA .. . 

HaSO• Spike DatA! (yyyy/mm/i · . ~011.';)..(. 

Comments 

.. * •• 

VES 005628 
. . 

. I Data 1 - Metal$ and Wei Chem 

'-

I 

I limo 

I 1 nple 10 •erified • ' 10 <watertl 

' IYPO • matril< soilce aooear ' lilar. lniUal samolo as well as fin8l e>«ract 

~-.cleo<ly 

Ito 10~ •amlll .. 

I 

lr1!IO - lnd ' •lracldna rOCORI and 

I IOIOO!nll - le¥01 

'llntomol 

~ ; I , 

'entered in ~ 

I by: . 

land' land ~~-~ I 9t9iF 

lo.~e : 

'cntena 

. 

I by. -- !Dote: 

~l-J . 

. 

_....,... .... CAM~ 

P19t10ft 

. .. 

no_ "'-"· I. ,... ....... 

L 

I. 

v 

.... _j 

" 

v.• ,.., 1)/8 

" 

/ 

" / 

/ 

" / 

, 

/ 

/ 

-- I' _.,. , 

,.,. 

;' 

/ 

,.,. 

I ves no nta 

/ 

/ 

/' -

; 

VES 005629 
Pnkin-&l_mer AAwi'nLa.b: 2008.-08-2!, 01: 16:39 PM 

Saap1e f~toraation Fiie C:\AAUStn\SAMPINFQ\~-8-2lA.S~F 

Dosc;r i p,tion 

Batch ID 

Volume· Unit.s 

lleiqht · on i ts 

Analyst 

Semple Voluae 

AB Saaple lD 

Loo 

17 15922.94 :REFMAT 

18 8LANK ' 

19 MTRX SPJ( 

20 AG06513· 03: 01 

21 AG0658-03 

22 AEB352:6.3 

23 AF8 098-02 

24 AF889.9 02 

25 AFB 1oo-o2 

26 AF8101-02 

27 AG0659-03 

28 ~0660 03 29 AG0661-03 

30 REMT 

31 Al'l 193-0.4 

32 AF1194 -04 

33 AE8352-03 K 2 

3 4 AG0660-03 K 5 

3s cca 

36 cCv 

3 7 1592587:REFMAT 

, 38 BLAJII( 

39 11\'RX SPK 

40 AF6617-0l: Ol 

fl AF6617-0l 

4 2 AF1 3!2-01 • 43 AF7 343- 0i ) j(.l O 

44 AF1344-0Y 

45 AF4626- 0l 

46 AF462.7- 01 

41 AF6618- 0l i-u'iJ 

48 AF6619-0l 

4 9 AG3265• 01 

SO AG3256- 01 

51 AG3271-D1 

~2 AF6676- 01 

53 RECW.T 

54 CCB 

55 CCV 

Lily 

0.00 

s..pie s..Pi· 

'K!ivht ""it• 

0.5000 

0.5000 

0.52QO 

o·. 51oo 

0 .5100 

0 .• S100 

0.5100 

0. 5.000 

0.5200 

0 .5000 

0.5000 '0.$200 

o. 5100 

0.5009 

. 0 . 5000 

0.5.100 

o.sooo 

0.5200 

0 .5100 

o.sooo 

0.5100 

0.5200 . 

0.5200 

0.5060 

0 . 5 100 

0.5100 

0.5200 

0.5100 

0 . 5100 

0. 5200 

0.5100 

0.5100 

0,.5000, o:s1oo. 0. 5100 

user Reaark• 

Dilution 

50.0000 

50. 0000 

SO,OOOQ· 

so.oooo sO.oooo 

50 .. 0000 5o.ocioo 

50.0000 

50.0000 

50.0000 

so.oooo. 

so.oooo 

so. oooo .' 

so.oooo 

50.0000 

50.Q000 . 

100.000'0 

250.0000 

50.0000 

50.0000 

50.0000 

50.0000 

so.oooo 

so.oooo 

50.0000 

50.0000 

50. 0 000 

50 .0000 

50.0000 

so.o'ooo 

50.0000 

50.0000 

50.0000 

50.0000 

.n.,-v 

Page -16-

VES 005630 
Perlcln- Eolaer l\1\lU,nL<Ib: 2008-oS- 21 ,_ 09:22:22 11M 

Method ---------~------ HaM: HGS JOB .. ------- -----..-~-------

Method Descripti on: Soil- -Campobello Rd. (509 uL locp] 

Ele .. ent .: H9 

Dlte: 2008- 08 - 21 ·Tochni que:FI•MHS 

C•llbrotion Type: ijq , ZerO Intercept: Linear 'wavelength: 253 . 7. nm 

Sample I nfo Name: 8-2ll\. F Ro~ulto Data s et· Name : 8·8-2lo 

_____ ....,..________ -~--~ ---------

E1e~en : H9 Seq. No.: 1 

Stmple 10: Calib Blank 

Rtpl 

I 

I 

2 

Mt&n: 

StndCo.nc 

mq/t. . 

Aato·~ero perf orQed . 

AS .Loc.: 9 Date: 2008- 08• 21. 

Peak 

HeiQbt 

0.0000 

0.0000 

Time Pealt 

Stored 

09:23:16 No 

09:23:56 No 

--=- ---.----.. ~··------~---·--------== El ement : H9 Seq. No .. : .2 AS Loc.: 10 · Dat e : 2008-08- 21 Sa~p1e ID: 0 . 20 ppb 

----------------·---·------------------·-------------·------------------------------------- i\epl Sa.mpl econc StndConc Peak Tia~ . · a.k . 

I m9/L . 1119/L HeiQht St or ed 

1 o. ooi7 09:24:51 No 

2 0. 0011 o~:2S:3o No 

Htai,: 

{KQ] ·Standard nuaber l applied. (0.000201 . COr-relation Co ~.:cient: 1·. 00000 Slope: 8 . 47340 

-----= £1•ent: Hg =-=="' Seq. No.: =-----

3 ···-----=AS Loc.: 11 

·=

Dote: ---2008... - 08-~ - 21 

S&apl e ID: O.S PP.b -----------------------------------------·--------------------------------------------· R4pl 

• l 

2 

Mean: 

Sa.spleConc 

J19/L 

StildCOnc 

109/L 

Peak 

HeiQht 

0 .0042 

0.0042 

"tixle Peak 

Storf:d 

09 :26:25 110 

09:.27:03 NO 

IH9l Standard nv»ber 2 opplied. {0.00050] 

Correlation Coef ficient: 0.99989 Slope: 8.35155 

__ .,..,. ____ .,.~-·•-•- w-• --·-•• -"'-c••••·----"'•.z6le~>ont: Hg Seq. No. ; 4 

Sample ro: 1. 0 ppb 

Ropl 

•• 

l 

2 

rtean: 

SarQPl eConc 

mg/L 

StndConc 

mg/ L 

AS Loo.: 12 Date: 2008 - 08-21 

Beak 

!Ieight 

0.0084 

0.0084 

Tirn& Peale 

Storad 

09:27:58 No 09:28: 37 No 

{H9) Sto.ndsrd nual>er 3 applied. {0.001001 

correlation Coefficient: 0.99998 Slope: 8. 35920 

L!LSO=-=-••--.....:=------------.._-ma-•---·----·-•--~---~~ tlur.ent: Hq ·seq . No.: 5 1\S Loc.: 13 Date: 2008-08-21 

sample ID: 2.0 ppb . . ------ -- --------- -- -----------------~------------------- --------- ------- ------- llepl 

t 

l 

2 

SampleConc StndConc 

mq/L 019/L 

Peak 

HaiQht 

0.0169 

0.0168 

Time Peak 

Stored 

09: Jo:o8 No 

09:-30: 47 No 

~age - 1-

i. 

VES 005631 
. ·' 

Perldn-Elooor AAIIinLab: 

Ke&n: ·:· 

l!lg) Standard nwnbe[ ·C appiied. '(0.00200) 

OOrralatlon Coefficient : 0.99998 

. -:""# >:. ~V;:'· . 

2008-08- 21. 09; 30: '1$ 1\K 

~:.f.· . ~ ... ;~!!~ 

'.~Slope: 8. 41364 ·.;.~~ 

tlt10ent: H,g Seq. No . : 6 AS toe.: 14 

Sample ID:·. 5:0 ppb '~: 

·-------------------------------------------------------------------------------------- Ropl 

• 1 

2 

Sampleconc 

mrj1L 

StndConc 

11<9 / L 

Peak 

H,ight 

0 .04 27 

0 . 0426 

•rime Peak 

Stored , 

09:32:20 No · 09:32:5&' No 

Kean: 

,l!lql Standard ·,nwllber S,. appliod. (0.00500) 

COrrelation Coe fi~ient: 0.99997 · Slope: 8.51039 

U.,..,nt: ~9 ' Seq. No.: 1 ' liS Loc.: 15 ~te: 2008-08-21 . -~-· ·. Sample 10. 10.0 ppb .• .., .;?, ---· ---·---.:.- --...---~ -: .............. _ .. _______ ._ ................ _· ·:.:-.......................................................... ~-.:;;_ -----

Repl SaopleCOnc StndCOnc Peok Tiooo . ·Peak a 

f ag/L ag~ Height .st'ored '"-!t': 

2

1 " 0.0195 09i34 :Jl., No ~l;M~ 6 o. 0793 09: 35: 1o·::·No 

~;r: St4ndar-d. number · ,applied. (0.0100} ~·?;·f' ~~ Corrolo.ti on Coef.ficie'1t: 0. 99918 Slope: 8. 01758 . ·,<.:<.: 

·-~------ ------·---- ---------------------' ------------------------------~- ----;~ ------~ 

C411brati 9 n data t or. ttg •. ;, 

, Eote red ··. ;alcula.te~ ~~; 

·.Mean Siqnal Conceptrati9n Co'nce.ntrattOn Standard ·' ~· 

Standard ID l Pk Heiqht) (llq/1.) · · l,.q/Ll Deviation 'RSJ:l · 

Calib Blank · 0. 0000 ----~ "'· -,-~.· 0.20 ppb 0:0017 0.00020 : . 0.00021- 0.000063 3.7 ~· 

0.~ ppb · .• O.O.OC2 0.00050 ., . 0 . 00052 0'.000001 ---• 

1.0 ppb o.oos4 o.ootoo o.o0104 o.oooo'12 0.1 

2.0 ppb 0:0169 4.00200 0.00209 0.000033 o.z 

5.0 ppb ·• O.OU7 0.00500 0 . 00528 0.000097 0.2 

10.0 ppb 0.079C 0.01000 0 . 00983 0 . 000102 0.1 

COrrelation Coefficien<: 0.99918 Slope: 8.07758 ~---

·----------·-----------------------r•-----------.-------------------------------------

;. 

Page -2-

I 

VES 005632 
Perkin-Elaer ~WinLab: 2008-08-21, 09: 35:52 AM 

Hg 0.10 1 

1 0.~8 1 

l 

0.06 .1 

0 0.005 0.010 0.015 

Concentrat!on 

VES 005633 
Perkin- £Laor AA~inLab: 2008-08-21, 10:09:57 AM 

S~le lnfo...,tion Fil.e C: \MUSER\!WU>IN!'0\8-8-21A.SIF 

Description 

Batch ID Volu.~te Onit.s 

lfeiqht Onit• 

Analy•t Sa.wpl~ Volwae 

AS Saepl.c> ID 

Loo 

17 1592294:REFMAT 

18 8~- 19 H7RX SPK 

20 'AG06~-03: Dl 

21 AGD658-03 

22 11&8352-03 

23 1\FSO!B-02 

2 4 AF801.9-02 

25 IIFBl00-02 

'26 l\rS~01•02 

27 AG06l9-03 

20 /IG0660-0J 

29· AG066l-03 

30 RE!'MAT 

8-8-21• 1592294 

Lily 

0 .00 

S&~Qple Saaple 

Weigh.t Unit• 

0.5000 

0.5000 

0.5200 

o:5·loo 

0.5100 

0.5100 

0.5100 

0.5000 

o·.5zoo 

(). 5000 

0.5000 

0.5200 

0.5100 

0.5000 

tJaer Reaa.rk8 

DUutioh 

50.0000 

SQ. 00.00 

50.0000 

50.0000 

50.0000 .• 

50.0000· 50.0000 

50.0000 

50. 000'0 50.~.000. 

50.0000 

so·.oooo · · 50.0000 

50.0000 

Page -6-

.• 

. _;; ·o(-· ·~t: .f.,~ 

. '"'•:'f': . ~. 

,~·' 

~· ' :ij(.~~···' 

·~·~· m,;. 

·:N: 

VES 005634 
/ o). h 

it~7. 

(o117t 

I '-fl. 

5a"Ple 

tlemen ------------------------------~ t: 

ID: 

Kg 

CCII 

Seq. No.: 11 AS Loc.: 1 Date: 2008-08-21 ====------------~ 

---------·------------·---·-·-------- . ·---------·-·---------·----------·------------------. - llepl SupleConc StndConc Poak Time Pea~ 

• 10qfL "'9/L Height Stor ed 

1 0.00002 0.00002 0.0002 10:11:03 No 

2 0.00002 0.00002 0.0001 10: ~l: 41 No 

Mean·: 0.00002 0.00002 

QC voluo within speoifie<l limite. 

1'!-... ~-.. -~-----·-·----.--...... ____________ "' _____ .-,~---

tlementl Hq . Seq. No . : 12 AS Loc.! 2 Date1 2008-0B-21 

Suple 10: .CCV 

----------------------- ---------------------- ------------- --------------~--------- Bepl Sam.pl&Conc StndConc Peak time Peak 

I mg/L mg/L ~eight Stored 

1 0.00408 0 .• 00408 0.0330 10:12:35 No 

2 0.00410 o. 00410 0.03~1 10:13: 13 No 

Mean: 0.00409 0 . 00409 

OC value Mitb~ specified lln.lts. 

Ue .... nt: Hq Seq. No.: 13 ,Baaple 10: ICV-!.000 

AS Loc.: 3 Da~e: 2008- 08-21 

-~--- -~~--- -------- ---------~-------------------------- -- ------·------ ------------ Rep1 SupleConc StndConc Peek Time Peak 

• mq/L ·"'9/L !Ieight Stoied 

1 o:ooo3o 0.00030 0.0024 10:14:41 No 

2 0.00028 0.000~8 0.0023 10:15:19 ' No ttean : 0.00029 0 . 00029 

QC value wi t hin specified limits. 

----------· &lemont: Hg Seq. No.: 14 ···--AS ----~----- Loo.: 4 o~te: 2008-08 21 ------ -- Sa..ple ID: I CV- A 

·----- ------- ------------------------------------------- ---- ----------- --- Repl 

I 

SampleCoqc StndCOnc 

mg/L mg(L 

o.00214 o:oo214 

0.00214 0.00214 

Mean: O.OQ214 0 . 00214 

1 

2 

Peak 

Height 

0.0113 

0.0113 

OC •alua within specified 11aita . 

Time Pe-ak 

Stored 

10:16:13 No 

10:16:51 No 

&lcaent: ...w·---,------------~------~------ Hg Seq. , No.: 15 AS Loc.: ------====a~~------~~~-------------------- S Date: 2008- 08-21 

Sample ID: ICV-5 

·------·-----------------·------------------·----------------------------------------.--- ~•p1 SampleConc StndConc P•ak Tim~ P~ak 

I mg/L mg/L Height Stored 

1 0.00411 . {), 00417 0.0337 10:18: 21 No 

2 0. 00411 0 . 09417 0.0331 10:18 :59 No 

Hea'n: 0.60417 0.00417 

QC value within specified limits. 

•-••---=-===<= ---l'llW14Ula•~----~ =-••--.•Oil•--••• .. •-=. Element: Hq Seq. No.: 16 AS Loc.: 17 Date : 2008-08- 21· Sample 10: 1592294: REFMA'I'· 

·-------------------~--------- --- -- ---- -- ----------------------- ----------- lep1 Samp1eCon.c St ndConc Peak Time Peak 

• aq/L mg/L Haight Stored 

1 0.317 0.00317 0.0256 10:20:27 No 

2 o. 311 0.00311 0.0251 10:21:06 No 

Kean: o.3u 0 . 00314 

E.lec.e.nt: Hg Seq. No.; ------ 11 AS Loc.: 18 Date: 2008- 08-21 

Sample ID: . B!Jl.NK 

·--------------------------------------------------------------------------------------

Paqe -7-

VES 005635 
.. 

wr! 

lll-nt: Hq Seq. !'0·: 4l 

S&ftple ID: l592587 :R£FHAr 

AS Loc.: 37 Date : 2008- 08- 21 

--------- -~ ------- --- --------------- ---·------------------ ------------------------ Repl SaapleConc StndConc Peak Tillie Peak 

• •9/L mg/L Ho:J.ght Stored 

l 0. 308 0 . 00314 0.025 4 01:18 : 18 No 2 0. 299 OA0305 0.0246 :18 5~ No 

t-tean : 0. 304 o . 00310 

---------~- --•••--••""..,a ==-•-==-•---==---•- •- Element : ' nq . Seq. No. : 42 .M Loc . , 38 Date: 2008- 09-21 

Saople ID: BLANK 

-----------------~---------~ ~--~------- ~-------------------- ------------------- Sampl eConc >lg/L 

. 0 . 00250 

0.00065 

0 . 00157 

St ndConc 

109/L . 0. 00002 

0.00001 

0.00002 

lll .... nt: Hg Seq. No.: 43 

SUple ID; lflllX SPK 

· Peal< 

Height 

0.0002 

0.0001 

Ti me 

01:20:24 

01:21:02 

Peak 

Store<! 

No 

No 

AS Loc.: 39 Date: 2008- 08-21 

-------- -~---------- -- ------------------- ------------------ -- ------ -- ---- -- Repl 

·• 1 

2 

Neon; 

Sampl eConc 

raq/L 

0.598 0.~29 

0.613 

StndConc: 

mg/L 

0.00610 

0.006,41 

0 .00626 

Peak 

Hoi9ht 

0.0493 

0.0518 

T . .lme Peak 

Stored 

01:21:56· No 01:22: 34 No . 

._._.__.•e====~== ••--•••-••• •••••••--••uuc.==-z=- --••-------·••••••---------------

Element: ~9 Seq. No . : 44 · AS Loc . : 40 Dat e : 2008- 08- 21 

SOrnplc l D: Ar6677- 0l :Dl 

·-- ------- -- -- --------- ---------~- ---------------------·-------------------- Repl Sai.QpleConc Stnc!Cono Poak Tilll.e Peak 

• ~> /L mg/L Haight Stored 

1 0.0263 0.00027 0. 0022 01:24:02 No 

i 

2 0.0265 0.00028 0.0022 01 •2• • 4l No f:jl · ttean:. 0.0264 0. 00027 

~ 

)( ID 

£loment: Hg Seq. Ho.: 45 AS Loc.: 41 Date: 2008-08-21 

SUp1e ID: I\F6677-0l 

-----~-- ---- ------ ---- --------------------------------- ---------------- ---- --- Ropl 

t 

1 

2 

"ean: 

SaaphtConc 

roq/L 

0.0228 

0 .02 48 

0.0238 

stndConc 

NJ/L 

o:oo02f 

0 . 00026 

0 . 00025 

Peak 

lteiqllt 

0.0019 

0.0021 

t'i>le 

01:25:35 

01:26:14 

Pea l< 

Stor ed 

No 

No 

----.-·==--=-=·-----------------.. ------·-·----·-- = .. Slome nt : hq Seq. Ho .: 46 

Sample 10: AF7342-01 

liS Loc.: 42 Date:. 2009-0B- 21 

--------------------------------------------------------------------------------------- lloopl Sampl eConc St ndConc Peek Time Peak .; 

I mg /L mg/ L Height St o r ed 

1 6. 43 0 . 0651 0.5257 01:27;08 No Sbph absorbilince s 9r:-eat.er than t hat ot tho bighast s eandi:ard . 

2 6.41. 0 .0649 0 . 5241 01:27: 46 No 

S&IIPle absotbcince i .s qreater than t .hat ot the highe st s1:andard. 

Mean: 6 .42 0 . 0650 

S&J:il)le absorbance is qreater than that or the highest: s tandard. 

-== 

U.ement ' Kg Seq. No.: 47 AS ·-Loc.: 43 Date: 2008-08-21 

S&ople ID: AF'7 343-0l 

--------------------------------------------------------------------------------------- l!epl 

• Sataple.Conc mg/L 

StndConc mq/L Time Peale 

Stored 

Fage -17-

VES 005636 
.. 

~ f-/0 

·· -=·~~. ~ ~-. - Perkin-Elloer AAllinLab: 2oo:S-os~21, 01: 29: 16 Pt1 

1 6.02 0.0614 

~ple ab~orbance gre~ter 

2 6.00 0.0612 

Sa~plo absorbance is greater H<pan: 6 .01 0.0613 

Sa•ple. absorbance i.,: 9reater 

.o . 4962 

than that 

0. 494 ~ 

than that 

-~ -~ 

~ :· 

01:29: 1·6 No 

of the ~qhest standard. 

01:29:54 No 

of the hlghes~ standard. 

th-an that o! the' hi¢'e~t standard. 

w.w---..._•••••••••--~·~~·-•••--.-----•~----.-....-~~--.c==•=--••••----•••~---·-•oo-•--= 

ElerO<tnt : Hg seq. No .: 48 

Snple tO:· AF13H -01 

AS Loc.: 44 Pate : 2008-08-21 • 'I • • . . ----------~--~ ------- ------~--------------~-~--~--~- -------------------------------- llepl SOJnp1eConc StndConc Peak Time l'~ak 

• "'g/L 1119/L ueigh t Stored 

1 6.70 0.0683 0 . 5516 Ol:3l:25 !IO 

Sa.aple absorbance is greater than that of th~ hiQheSt standard, 

2 6.68 0 . 0681 0.5500 01:32:03 No' 

J;anople absorbance is greater th&n that of the~ighest standard. 

ato•n: 6.69 0.0682 .. Sa.aple ab.sorbaOoe i.s gre•tor thao that ot tbe :hlqhest standac"d: :! . .... lltment: Hg ,Seq . No.: 49 AS Loc.: tS~ Date: 2008 - 08-21 

~ "Repl ~~~~ SantpleCo ~~~ ~~~~~=~~ nc StndConc ------------------· Pe~k Time --- ~:- Peak. ~~~--~---- --------------... ,._, ~~~---------- .f, t "g/L 1\g/L fleight .1if-stored • i·"!'t' · u,. 1 0 .121 0.00126 0.0102 · 01:33:35· No 

f'I.AT> ·2 0.0895 o.ooo9~ o : oo75 01:34:11 No . · . · . . 

......... ::,...J~~ear: 0.105 0 .00109 ·,_ . . . 

.. 11' "'r --------------..----·-...;,-... --~~,.,.-""' ________________ --="""""· 

M'.KJ :::~\D gAF46i;~O o.: 50 ·. AS Loe .: 46 "i Date: 2098-08-21 . . 

--.;. __ ......... r .. - - --- --..... --- ------~-------- -:- ... - ___ .._.:.. ----- - ------... --.. --..... -: ... --·--------- ----·-

P.cpl . S&DpleConc StndCOnc ~oak Time·~· a!< 

t 109/L mg/L Height ,., Sto"ed 

1 0.0687 0.00070 0.0057 01:35: 45 No D.b1 2 0.0704 0 . 00072 0.0058 01:36:23 No 

Mean: 0.0695 0.00071 

'I Ji) 

~ 

11-ot:. Hg Seq. No.: 51 AS Loc. : 47 Date: 2008- 08- 21 

S&mple ID: AF6678-0l 

llopl Samp1eConc StndConc Peak Tiloe Peak 

t mg/L mg/L Height. stored 

1 10 .8 0 . 110 0.8911 01:37;55 No 

saupl e absorbance i s g-reater than thot of the hi 9hest standard. ~ 10.7 0 .109 0.8794 01:38:33 " No 

Sl,luple abs orbance i s greater than thot of the hi ghest standard. 

t:tean: 10.7 0.110 

sa .. ple absorbance i s greater than t hat of the highest s tl2ndard. 

_____ =---c:: ___ .;.... _______ ~--------------===-

El ement: Hg Seq·. No.: 52 

Sal!l(>lo IDi AF6'679- 01 

Repl SampleConc StndConc 

' rag/L Rq/L 

L 0.0532 0.00055 

z 0.0451 o :ooot7 

!lean: 0. 0491 0.00051 

AS Loc .: 48 Date: 2008 - 08 - 21 

Peat Ti .... Peak 

Height Stored 

0 .0045 01:40:02 No 

0.0038 01:40: n t<o 

----~==~ .£1.etHnt: Hg ===---· Seq. ==~~=-~·--------~bb~=------~----==~----- No. : 53 ·-----=~~ 

Sa.Rple ID: _AG3265- 0l 

AS Loc.: 49 Date : 2008-08 - 21 

--·-----------------------------·------------... ---·.--------------------------------------

Page - 19-

VES 005637 
lh· 

f/'1. 

fN 

c-'1 

lo~Z 

Per~i.n -&lmer AAII1nl.ab: 2008-0~ u, 01:40:43 PH 

~pl Sii.pleConc StndConc Peat Time Peale 

• tnq/L mq/L Ho1ght Stored 

l 0.00180 0.00002 0.0002 01: 41:35 No 

2 0.00169 0.00002 0.0001 01:42:13 No 

Mean: 0.00175 0.00002 

&lcllont: --===~======-----·--------= ====---------··-· -.... ·==--= Hg : Seq. No:: 54 AS Loc.: so Date: 2008-00-21 

Sample I D: AGn 66-01 

-~~--------------------------------~----------------------------·------------~--------- l!epl SampleConc Stncteono Peak rime Peak 

• mq/L 109/L Hai ght Stored 

l ,0.0335 0.00034 0.0028 01:43:07 No 

2 0.0337 0.00034 0.0028 01:43:46 No 

tban: 0.0336 0.00034 

~~ue...nt: =-----=-~----------------·=--- Hg ~q. No.: 55 1\S. Loe.: 51 ' Date: 2008- 0.8-21 · Sample ID: AG3Z71-01 

lepl SaapleCooc StndConc Peat u •• Peak 

,. ff¥J/L J09/L He1;ht ~tored 

l 0.00137 0.00001 0.0001 01:44:40 No 

2 ,0.00253 o:oooo3 0.0002 01:45:18 N!> 

!loan:: 0.00195 . 0.00002 

Element: ----------~-- Hg Seq . Mo . : 5.6 AS Loe.: --- 52 bate : 

-----·--~ 2008-08-21 ... -·---- S~~pl~ ID: AF6676-01 . 

Repl ----~----- Sa~pleConc -- -------~-----------------------------------~---------------~------ -~------- StnfJConc . 

• mq/L .. mg/L 

·l ·0.614 0. 00~81 

2 0.660 0.00673 

Moan: 0.667 0. 00680 

-

S:lement: ·Hg -·· Seq. -No.: 57 

S-le 

lepl 

• l 

2 

Heap: 

ID: R&FKI\T 

Saapleconc 

INJ/L 

0.00630 

0. 00627 

0.00629 

· StndConc 

:og/L 

0 . 00322 

0.00320 

0.00321 

Peak 

Uei9ht 

0,0555 

o.osu 

AS 

Peak 

Height 

0.0260 

0.0258 

fiae Peak 

Stored 

01:46:12 No 

01:46:50 No 

Loc.: -----~ ------- 53 

TilDe 

01:48:'18 

0 1:t8 :57 

Date: 2008-08-21 

Peak 

Stored 

No 

No 

----MH--~·----------.------~---~----------~====----~--~-------------------~ Element: Ug Seq. No.: 58 AS Loc.: 54 Date: 2008-08 -21 

Saoaple I D: CCB 

--·"---- ----------- ----------- ----- -------------- ~--~ -- -------- ------------- -- Repl 

1 • 

2 

Mean: 

Sa~pl~Onc StndConc 

11111/L "9/L 

0.00000 0.00000 

0.00000 .0.00000 

0.00000 o.ooooo 

Peak 

Height 

o.oooo 

o.oooo 

Tille P.eak , stored 

01:50:25 " No 

ot': s1, OJ No 

Cleoo.ent: HIJ Seq. No.: =-59 --------------------------------- . AS Loc.: 55 Date: 2008-08-21 

SIIIOple ID: ccy 

-----------------------·-------·---------------- ------------------------------- aepl SupleConc StndConc Peak nee Peale 

• "'9/L J09/L Ro'igbt Stored 

l 0.00429 0.00429 0.,0347 01:51:57 No 

2 0.00432 0 .00432 0.0349 01:52:35 No 

Keo.n: o·.oono 0.00430 

Page -19-

VES 005638 
().o1 

~leuent: Rg · Seq. No.: 60 

Saaple ID: AF4626- 0l 

... ..,_ .... 

~ LOC. : 45 Oat<! ... ~008•08-21 

--·------------ -..;._------------ ----- -- --------------------- --- --~---

Repl· SampleConc StndCOnC:: Peak Time Peak 

• mq/L mg/L Reight Stored 

1 O.OlSO 0 . 00078 0 . 0063 02:21:02 No 

2 .0. 0709 0:00074 0.0060. 02:21·:40 No 

Mean: 0.0729 . 0.00076 

.• 

Pago -20-

VES 005639 
• . . . • . ----------.. --==a~-=:=---·---_,.;_._...; . - ~-==-·== . --.... ---~ Elament: H~ Seq. No. : 61 

S&mple ID: AF7342-01 X 10 

AS Loc.: 56. Date; 2008· 08 · 21 i 

-... --------- -------- -----------------------------~--------.,.--- ---... --·-·------·---------- l<epl SalapleConc StndCooc Peak Time Peak 

f mg/L mg/L Hei ght St o red 

1 ,'(, l L83 0 .00793 0.0~40 Q2 :.27 ;10 No 

2 7.78 0.00787 0 . 0636 02:27:.4 9 No 

Mean: 7.80 0 . 00790 

-= ----.. ·-----... ------==-----.. --....... ·•'!11•-.!!----~--~o:===-·---·- .Element: llg Seq. No. : 62 

Sample 10: AF7343- 01 X 10 

. AS Loc.: 57 Oat : 2008-08- 2 1 .. 

---~------------- ------------ -~------ ---------------------------------~-------------- l<eP.l Sample-Cone Stn~Conc Peak Time Peok 

:t mg/L. mgfL Height stoied 

7!' 'f 

L 7.18 0.00733 0.0592 02;29: 18 llo 

2 7 . 10 0 . 00724 0 '.!)585 02:29:56 No 

M&an: 7,14 0.00728 

<---·----·----·--- ··-----.,....__-............ -~-----c:'~--~-= nernent: Kg Seq. No, . : '63 

SaoPle ID: AF7344"0l X 10 

AS Loc . : 58 Date: 2008- 08- 21 

--------·---------·- ---- -------~~---~--~~--------~------~-7------------- --~------~-~ 

1\epl S.ampleConc StndConc Peak T1'1"' Peak · · · t mg/L mg/L ~eight S.tored 

1 .. . a.n Q.Q083S o~77 02:~1:26 No 

2 a .o1 o; ooan o.o&69 02:32.; 04 llo 

~an : -a .u 0.00828 

cmaswww= •'!"•=-= -=••••-= wa••----=-=••· m~ - . U ment: Kg S~q. ·No.: 64 AS Loc. : 59 Dote: 2008-08-21 

Sa•ple I D: AF6678·01 X 50 

--------------~---- ~--~~-------------------~--~~~~---- ---~---- --------------- -- ---- P.epl . Sam.pleCOnc StndCOnc Peak · me Pea" * · mQ/L mgi~ HeiQht St ored 

1 21.0 · 0 .. 00 427 0.0345 02:~3:34 No 

2 20.9 0 : 00426 Q.0344· 02:34:12 No 

Mean: 20.9 0 . 00427 

Page -21-

VES 005640 
, 

•.' ., El-en~: Hg Seq.· llo. ; 65 

Suq>le JD; CCB ~ Loc.: 60 Date' 2008-08- 21 

---------.. ----- ---------.---,---·-------------------------·----------------- Rapl ' . ' Sample<:O(IC Sqldeonc Peak Time P~ak 

I ~/L 11.g/L Height stoie.d 

I 0. 000.00 0 . 00000 o.oooo· 02,36:00 llo 

z 0 ·.00001 0 . 00001 0.0001 02:36!38 No 

M)on: 0.00000 0.00000 

.. eo~=:=======a= -------•~•--••••••~·--------•••--== ==-••••• ---•• ••• ww ~· • 

~lement: Hg Seq . No.: 66. liS Loc. : 61 Datei 2008 ·00;21 · Smple ID: CCV 

Ropl SaJliPleConc Stp<ICo.nc Peak u ... Peak 

IO' ~ I lllg/j. ·mg/L "'ight Stored· 

I 0,00423 0.00423 0. 0341 02:37:32 No 

z 0.00422 0 .00'422 D. 0341 02:38:10 No 

l-Ie en: 0.00423 0.00423 

Page -22-

VES 005641 
.. 

htorcury in Weltef by r:;vM- WIN!t 

("''IA.) • ' 

I . ... .. - · · ....... ,.,._.., ..... -. ·- ! 

l

p _ _ ;:;:..;.:-- - - - .•• -1 ... at~:~·-·--- .-.. ··· - · · ·-· · " ' 

.... "ll' I!!Sll . . •...• ·-· ···•·• --·· ·~ ' 

~ • •• OL

1 

• j 75 

IOL' -·o: 

VES 005642 
.. 

•• RYSH 

Aar-t Dt<e: Th~Utday; AttgU$1 21,2008 

Aalaoed lb: AIIDlilt.AH J<.RUDijAlR 

Test Code: HO·L lnsh\ltnent ld: 

1·os1 Oacriplion: To'detcrmiot Hg byCVAA. Nov 16.2000 

MDL chaogcd ftom O.OOIP.Pm to 

O.OOOIJli>CL 

lob S1111>1e % 

Numh.. .. Number D ......,_m P Molll 

MTJUCS~K nc:nc Al'2.263"'8 

Sl'IKB OC2lC 

BLANK· 

AS90621 ~ SWI 

Al90621 AI'125$.08R SW2 

Al90621 Al'1257.o811 sws 

Al90621 · nzm.ccR o SW !l 

A890621 Al'2263-08R I sw 11 

AB"'""9 A"'l31·1l4R REMINO'TON 

A89106l AP~~4R 47732 

A89t411 AP61AS.08R SBWBRI7 

A891lll AF678S.01R 81656 

'AII9164R • 1'73l3.01R llBlU-UZ.RI <!>•F 

~A801648 AI'7334-0IR llBlU·II2·R2 •P' 

' AI91641 AP733S.OIR HB'fU.U2·1l3 I <r i 

'AI916tl " "'31>QIR l..lm.I·U2-RI l .... i · 

' AI91"'• A1'7337.01R umJ.U2-R2 ·-/ 

•Abl648 A1'7331-0 I R IJllU.Ul.llJ " ' AI916tl A1'733 9.() I R SP-U2·RI k. 

'AI916tl • A1'7340.0 I R Sf.U2-R2 In 

' AI9l6<1 H71AI.OIR Sf·Vl·lll .< 

•AS916U AP734S.O IR MS.Ul·RI .. 'AI91648 A1'7346-01R Ms.m.R2 ..... 6t3 AI'U47-0IR MS·Ul·RJ . ...,·, .. 

I ....- ~ 

,.., .. ~.:,:· 

lltmarloo: 

Wt 

or 

Vol 

I..,,,., 

-

-· t-r.r 

h •• 

·-' 

. -· I..,, 

L. 

h ; .. 

--~ 

ABDULI.AH ICHUDHAIJI, 

F!nol 

Voi 

1-t 

,.. 

j 

G 

.( 

' 

.I 

r 

-

s.m,t .. e>tti'I<Ud by. 

.,_,.. ........ pcd'.......t by. 

Calc:uiUiau pafvt 

Validai>Odby. 

mcd by. t(T ::~ • 

~ .. · ·~· 

llF . 

... • AP Coat 

-.. •. 

-

;~. :>! 

'IY· "~l 

;$";.., ;1 

···I 

'I 

I 

' I 

I 

I 

2 

: 2 

2 

2 

2 

2 

2 

2• 

2 

I 

I 

I 

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lhplry 

Dale 

2001101111 

200110&'21 

200&'0&111 

. 200110&'21 

20011108/ll 

20011/08121 

2008/0S/22 

2008/011125 

2008/011122 

2008/08/18 

2008/08/19 

2008101120 

2008/08/11 

2001101119 

200110f120 

20011081 II 

2001108119 

200&10&110 

2008/08118 

2008108119 

2008/081'20 

Pip): I ort 

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1'<ol 

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!OOIIOIIl2 11.110 

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!00111011.!21 i.OO 

IOOIMS/l218:00 

' '"'00 PWOO . 

200liJIIlll22 11:00 

200111011.!2 U:OO 

200111011.!2 11:00 

20Qtt.ml21 l?:oo 

200110&121 17too 

2001101121 17:00 

:100110&121 17:00 

2001101121 11;(10 

2001101/ll 11:00 

117:00 

1D08io&l21 17:00 

2008108/ll 17:00 

20011011ll 17:00 

117:00 

2008101i21 i 7:00 

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_____ ., ___ _ 

. ·. 

VES 005643 
.'• . 

~ B!R ct:ent Nanie . MA890621SCO G1eer Giolloway<lt'o•p Joe 

MA89086!CHM A.11as Co.pontion 

t,{AI914)W31\ PPO~)nc 

MA89152~AS ReslooofP~ (V59S2) . . . . ~ . 

s .. 

sano>~e Pre..,..onRemms 

Li.. . ' rn-·· 

A r.':, .: .. 

tJ..- --i~'-'' 

"'~'~ ~u 

• 

I 

RUSH 

. ., 1592563 

Dh~Buot 

kii'Oo<mao 

f!l . l!.!lmadll 

(70S) 743-9592 SAMPLES AAAJVl!D IN Bl!l>PORD AUGUST 19. 

2008. JDW. Project Ji, BUCIOIORN SPRING 

LANtil'tLL(SW) • . 

( ) .• 7C . 

PWQO ~learc mal:< 611 un~ !118iL UJ>(\"ible Ptojec 

. #' SURPACEWATERQUAU1'Y/j)7-50S~SB 

MDL) . . . 

(5 .. 9)&'37;1226 S"C/0\aelpb·WWI'P MOB C of A Project II: 

. . 2112915RAWSI!WAOB .. 

NA TIONAi.. Ctly of 'Gotlptl 

(90S) JSS-@7 22"C Pro!f« #' Peel ~ 

. NA TIQNALl We C.\N;.DA INC · 

(90S) 566-4628 l!>cecclinee IU>1ification nat~ Project'' • 81656-81667 (USll MI>LJ . • • NATIONAL:Recloo of Pul 

(31})437-0509 RUSH TCP+Ho, TPTALC!ll.OIUOBS. BW. 

%ASJ!.SUB 1:0 PSCREPUBUC WASTI!FilllJ)S. · 

Project#' 1002-022 

NATIONAL> ENSR INTIIRNATIONAL 

- · 

J I . u . . .... {/. f-:2'. 'M d--.. 1 ./.. .d 

'" . t: . ... h , I ' 

' .,. , ~ • I ... /.• ..... .,. J. ... /1. 

" , ' v . 

VES 005644 
.... . . '*' ' ~it • •'' It .. 

.. ·' .• . . !R:~ ~.: )!"' .. 

... ~ . f:} . 

Wof1.s~ 59~00lii)Sirument ~\1011Ces ~1 

·- ·(:-":·; . ~·· 

MTRXSPK 1. ·u•nmiiiUDlllm . ~ MTRXSPi< .. 

•• 

SPIKE. 2. IIWIIIIIIImiU ... , SPIKE ~· · 

3. IIIIIIII II AI ~ '~. rN• •~· 

BLAN1< BLANK 

4. IIII IIII IUIIRIIII ~I B ~· .. : 

AF2254·08 SIJ\"1 

s. iUIIIIIDi mnmiBRIB ;·. 

AF2255-08 SW2 ·.; .•. · ,.;. 

AF2257-08 ~- lllllllrniBIBIJIHUIDD SW5 

- 1. llllllmiiDRIIImllq AF2263-08 -:::' . sw 11 pg·b= 

;~ i:;~ .. · 

8. IHIIIIIIIUIII-11111 {~· ···: .. AF2263-08:01 SW 1,1 :1>1 · ... .. ~ ,. J 

9. lniiiii.IIIOIIIOIIDIIU "~ Rl;MINQT9N 

,'tNt-.. AF3~1-04 "1'··· .;; 

·· ~' ··;.. ... .1o fti ii ii iiii IIIRII II I :.f.,. .*.\1.~"'" 

AF4402-04 . 'J 47·732 · 

~ .. ~'f.Jl . 

11. OBIJIIIIIIIIBIUIWin .. AF634§-08 SEWER#7 '*./•;· -; · 

12. IOIIIIIII!IIllliftlEIIID ·.'· t:·· •. -e 

·AF6788-01 81656 } : ,_ 

AF7333-,01 13. lmi!UQIIiiiBIBIIIIRI • HBTU·U2-RI t{~ ~: ' .. • • 1 

14. lllll.llllmOIWIIIIID HBTU-U2-R2 

!' ( • 

AF1334.Q1 ' ~ 

AF7335-01 ·rt/!: 1s. UIIIIIDIIIIIIUIIIII R ·~· HBTU-U2...R3 

AF7336..()1 16. llllllllllllmlm!lllta LaTU-U2-R1 

AF7337-<i1 11. IIIIIIIIIIIIIIUIIIIID LBTU-U2·R2 '.· 

AF7333..()1 1s. lllllllllllmtiiiUWIIIIU LBTU·U2·R3 

.. 

10. lllillililllllmHiiiRD AF7339-01 SF-U2-RI 

AF7340-01 ·20. IIIIIIIIIIIIRIIIU!IIIIR SF·U2·R2 

AF7;l41..01 21. IIIIIIIIIIUIIIniUI IIU ' SF·!.J2·R3 ' ' 

AF7345..01 22. UIIIIIIIIIIIIIW.UIID MS-U2·R1 

-AF7;l46-01 23. Dlllllmiiiii. UWIIIII MS-IJ2-R2 .,._ .. > 

~F734 ;01 24. UIIIIIIIIIIUI910UIIII MS-V2·R3 .. 

. ;, . 

' ·. 

. ' 

VES 005645 
MwYrm 1.\nl lylies Iii<: 

~ FCQ.(I02A811 

•. · Page.1oH., 

Prep Batl:h Reagent Tratl<lng Record Worksheet g _ 1592 ~ Volume hill 

Surrogate/Spike solutions Solution 10 # · Cone. ·Bik·Spk MS Sampies 

la>MS 

!CAP 

GFAAS 

Hg ·20ppb o.sn.smL . . o.m.7mL 20 

' 

. . ----· -- --- ·-· 

Solvent Supplier Lot No. Spiked by: 

HNO, Fisher 307292 2008..07·29 .f-e.:.- H 

' NH2QH.HCl Asher . 72276 200.08·19 . . Splklng Witnessed by: 

NaCI Asher 67655 2Q0.07·31 • ' 

H2S04 Asher 108003 2008..05·23 Spl.ke Date (Wyylmmtdd) 

K2Slo8 F"~ther 75812 2008-08·19 2008·.0S.21 

KMN04 Asher SC6354483: 2008-08·19 . 

Comments 

.. ·-

VES 005646 
.. 

~ ,,. 

1 

~ .7 ...,_.. IUinO 

~lr<lle 10 Lab 10~•!•1'111 ipiki~~ I to t tvoe 

~ 'SjllkO 1 aample as well 

111lal I volumo. dearly I 

I anv I dKutlon 

QC aPIJ(Iod to IOl. satnl)les 

ISoil<lno 

I Sample ' land 'and~ 

II>)': f.:.. . f..( 

• and 

1 moe!! ' a!t&fla 

~-· land r ·-

<meell 

I Matert;ll 

1 alieno 

..... et. ' 

rTOblo 

t Uodated • Trend · I Notocl 

IIMeiS 

• lranQO ~-· ... tedand 

1tracklna· 

I hilt> level 

~ 

;I 

• P>eo oection labovel 

....,.IPteo r 

l'_ < 0 

lgned 

loato: ., ,.,. o ,.. , v 

. . 

. 

~ durino data uoloed 

. 

!Data: 

< .::.---<> -j vq/ <.I 

, o I l'liL C.•ff-_., .t I.~ 

I V • 

/ 

2NJ//8/:Z.( 

voa. no Ria 

v 

.L. 

VES 005647 
. . 

. . 

\ -sVoc J,.~ t ~ .; ?) .~ .. . ,..-- :, -

~; . 

. , 

' ,. 

VES 005648 
- Folde~: ll\lg_08a Page 1999 ! 

Pro t ocol : HG-.L JOB 

··•POST- RON REPORt~· · 

t.1ne COne. Units SD/RSD 1 2 3 . 4 ~ 

-------------------------------------------------------------------------------- ••• Standa.rd: 1 Rep: 1 Seq: 1025 13:27:26 21 1\ug 08 HG 

Hg .ooo pPb 1~ 

• ft<l: . Standard : 2 Rep: 1 Seq: 1026 13: 30: 05 2! llu<j 08 HG 

Hg .10,0 ppb 535 ' 

... s tandard: 3 Rep:· 1 ·Seq: 1027 13:32:53 21 Aug 08 HG 

Hg .200 ppb 1070 

••• Standard: 4 Rep: 1 Seq: 1028 13:35:35 21 /lug 08 JIG 

HIJ .5oo · ppb 2637 

••• S t aJ>da rd : 5 Rep_: 1 Seq: 1029 13:38:15 21 Aug 08 HCi 

H9 1.00 ppb 5241 

••• Standard: 6 Rep.: 1 ~e;q: 1030 13:40:56 21 Aug 08 HG 

Hg '2 .. 00 ppb. 10~79 

••• Standard: 1 Rep: I Seq: 1031 13: 43:45 2i 1\UIJ 08 HG 

.Hg 5.00 ppb, 26101 

••• Check Standard: 3 Gk3: ICV- L Seq: 1o.n 13:53:39 21 1\ug 08 HG 

Line Flag \ Rev . Found 'l'rua Units SD/RSD 

Hg 103. .~58 .250 ppb . 000 

.... Cheok Standard: 4 Ck4 : ICV- 1\ Seq: 1033 13:56: 42 21 1\uq 08 HG 

Line Flag \Rev. Found T<ue Units SO/RSD 

HIJ 99.3 . 993 1. 00 ppb .000 

••• Check s~anoard : 5 Ck5: !CV- 8 Seq: 1034 13: 59: 2 2 21 1\ug oe HG 

Line Flag \Rev. found Tr·ue Units SD/RSD 

llq 99 . 5 . 3 .'98 4.0 0 ppb :000 

•• • Cheek Standard: 2 Ck2: CCV seq: 1035 ' 14:02:04 21 Aug 08 HG 

Line Flag 'Rev. Found True Units SD/RSD 

Hg 101. 1 , 01 1.00 ppb . 000 

... Check Standard: 1· ckl: CCD S•q: 1036 14 :04:44 2.1 Aug 06 HG 

Line Flaq Found Range (+/-1 units SD/ RSO 

Hg .003 . 100 ppb .ooo 

VES 005649 
.. .. ~ .. ~ .. ~r: ~~~ -~· ~·: ... ~r~~: 

'!; ~·~:.... .. . . . .. ·:.. ~' ~~ ~~ · / ~~: f · FOl de·r:; Aug 08~ ;~..: 

·:::. $t~; ·; ·:., ·: .,;!~~~~!~tiH~~~~~ ~. Line Cone . Un!ts SD/Rsb . .l 2 . 3 . 4 5 

.......... _;._~~~- :. .: -=- -_; ...... .:.7 .... ~--- -----------:--"- ---~------ -- -- ---- ------- -.

... S~mple D:" SPIKE Seq: "1037 14:07:34 2 1 Auq 08 HG 

•• . . :~· . WSil$92373 

~q ,z~< ~pb,\' .000 . 1, 29 •. . ...... -'b 

~---== •• ==~=== ~~~==-~==-••~~- ==•========-- c==--••P•••= 

... sa.npte' '~ ro!BLI\Nt< · · ·s eq: 1038 · 14,10: i2 2 1 "1\uq c8 RG . 

Hg 

••• 

. 006 : L ppb 

.. ~' 

S"'!'Ple ·IO: LIXBL 

.coo 

.000 

.006 

• 

Seq: 1039 14:12:50 21 Auq 08 KG 

.012 -:f,. :-r~­ )l "Sf~ 

=•~== ~~~===a == ~·~--~~--=•••• 

HG 

KG 

HG· 

Hg 

Hg .106 .000 . 106 

.!;.~· . ~ . .. Q-- ~===-••• -==~aca•aca*----•=~~fte.c==?•- =--•••••••.-c•~~~-==:=•ww•• 

• •• Samp le "ro: AF3262-01 Seq: 1044 14:26: 19 21 Auq 08 HG 

.126 ppb .000 

Wgt . 50000 Vol 7 .5000 

. 126 

- •=•·••=•--=-....-••••-=·•·••••=·=-•• .. ••-••••--• == •--===•oe ••••••• ""~• 

**• SMple·.JD: AF3263-01 Seq: 1045 14:2,:0·3 21 Aug 08 HG 

llgt .. 50000 ·Vol 7. 5000 

Hg . 060 L .ppb . 000 . 060 • • ~KU·-~- --=-====•·•-=?=.S~ -----~== ====---===·--- -···5·-~·-- =g= =-----· 

••~ Sample ID: Ar3264~01 Se q: ·1046 14: 31 : H 2 1 Aug 08 HG 

w9t .sopoo vol 7.5ooo 

Hg .054 L ppb .000 .054 

' . . ~of· 

VES 005650 
Line . Cone . o·nlts 

Foldn: Aug_08a 

Protocol : HG- L J 08 

·· ·POS~·RuN REPORT··· 

SD/RSD 1 2 3 s 

-~--------------·---·---------------------~--------------------------------

... 

Hq 

Sample ID: AF326S-Ol 

.206 .ppb .000 

Seq: 104 '1 

.206 

1 4; 34:24 21 Aug 08· 

Wgt . 50000 Vol 7.5000 

HG 

•• ==============~==2••••••••••••~~--------•~••= =====a~•c••••••••••••••••••••• 

••• SMple IO: AF3526- 01 Seq: 1048 . 14: 37:03 21 Aug 08 . IIG 

02~ L ppb .000 .021 

___ , _____ .,..,.._,..,..,..,.. _______ =--=---··---=======···-------·-·- ... S&P!IPl G ID: AF4982-01 Seq: 1049 14 ; 39:41 21 Aug 08 HG 

Hg .006 L ppb .000 .006 

----·------- ~---

___ ,. ___ ... Suple I D: AF8098-0l soq: 1050 14:42:21 21 Aug 08 HG 

Hq .011 L ppb .000 .011 

• 

------- ••• sampl411 10: AF8Q99- 01 --- Seq: 1051 - ·=-===--

14 :44:59 21 -Aug OB HG 

~ 

Hg : 013 I.. ppb .OOQ . 013 

--------------========-~~----······--·· ·---------====··----------- ···------- · 

••• 5&>\JP.le I,D: AFBl00-01 Seq: 1052 IIG 

Hg . 023 L ppb .000 .023 

• •.• Sample ID: A~10l-0l Seq: 1053 14; ;o, 51. 21 Aug 08 HG 

Hg . 021 · L ppb .000 .021 

• 

••• Samp le ID; AF951 3- 04 Seq: 1054 14:53:34 21 Aug 08 HG 

Hq .oos J>~ .000 .008 

_____ ...__ _________ ~ ... ~----·-=======:c--------·-

... 

Ug 

Sample I D: AF9663- 01 

50.9 H ppb 

.,. ._. Sa"f>le 10: AG0 313- 0l 

.073 L ppb 

.000 

.ooo 

seq: 

50.9 

1055 14: 56:34 21 ~uq 08 

Wgt .50000 Vol 7. 5000 

Seq: 1056 · 14:59 :16 21 Auq 08 

. 073 

HG 

HG 

.. 

VES 005651 
~ine Cone . Units 

Folder:. Aug 08a 

Protocol: HG-L J08 ***POST-RUN REP<5RT'.t.t-. 

SD/RSD . 1 ·2 3 4 5 

~ Check Standa rd: 2 

Lin·e Flag $Rev . 

Ck2: CCV seq: 

Found 

LO~ 

True Upits 

1.00 ' > ppb 

1057 • 15 :01:55 21 Aug 08 

SD/RSD 

Hq .101. .000 

••• Check Standard: 1 · Ckl: \=Cf3 Seq: 1058 15 :·04 : 3~ 71 Aug 08 

Line · Fl ag Found 11an<;~e ( f/- >. On i ts SD/RSD 

Hg -.004 . 100 ppb .QOO . 

••• Sample ID :· Af3261-01 Seq : 1059 15:07: ~ 21 i'.uq 08 

Hq .036 L ppb .000 .036 

Page 1999 

RG 

HC 

HG -

----· ··-------------------~-----=~ ···-==~~-·--·--·· ·--~~==c===----~~-== 

••• ·s.,.p1e t o: P.F3262-0~. seq: ·1o6s> 15:10:04 21 Aug o.a HG 

Hg .031 L ppb .000 .031 .. ••• ·------- ==e••o-. ==-- •a-------=--- ==-=-••==--w•••• ••••• •••~•---••===c= 

••• Sa~ple ID: AF3263-01 15il2:43 21' Aug Q8 

. O:iQ L ppb .000 

Seq; 1061 

.030 

=~~==••••-==·--···~~-~---~-===- c===~.a=====••====-c==~••••••••••• =~ •• = 

• • • Sample ID:' AFl264-0'l Seq: 1062 15:15:23 21 Auq 08 

Hg .034 L ppb .000 

*•' Sample ID: AE3265-01 

Hg .072 L ppb .. 000 : 

••• Sample ID: AF9663- 01 

44 .3 H ppb . 000 

•• • Sainple 10: TRIP. llLK . ... 

Hq - .184 L ppb .000 

.. .... s,a.mpl e ID: blank 

Hq -.032 L ppb .. 000 

. 034 

Seq: 1063 

. 072 

Seq: 

44.3 

Seq: 

- .184 

1064 

106 5 

,Seq: 1066 

on 

HG 

• 

15 :1-8:03 21 Aug 08 HG 

15:20 : 44. 21 Aug 08 HG 

15:2'3:23 21 1\ug 08. HG 

15: 26.:40 21 Aug 08 fiG 

VES 005652 
'roldor: Auq· 08a 

r~~oqol: BG-L308 

***POST-RUN REPORT~*~ 

age 199~ 

~ine Cone. Unit~. ' SD/RSD 1 2 3. 4 . 5 

-------:--------.. ----·---- ------,-.--":"-:----.. ----.----'":'--o.-----------------------·--

••• 

8g 

Sample ID: TRI~ BLK 

- . 049 L ppb .000 

"'<fl• check Standard: . 2 Ck2 £ 

· Line Fl ag \ Rev. FOund · Hg· · 100. i.oo 

CCV 

·'f.rue 

. l. 00 

_,., ._ Check Standard:· 1 Ckl: COB 

Line Fl aq round Ranqe(+/- ) Units 

Hg . - .054 .100 pp)? 

•** Check Standara: 

Line Flag 'ReV" ,H9 103 . 

2 Ck2: 

Fo:und 

1.03 

CCV 

1'rue 

1.00 

••"' Check Standard: 1 Ckl: CCB : t.lne ·' Flag POund Ranqe J+ / - ). uflit s H9 . - . 004 ·. 100 .ppb 

*~* ·Sample 10: SPIKE 

Seq: 

Units 

ppb . 

.1067 

1068 15:31:59 2 1 Aug .08. 

. SD/RSO . . ooo 

seq: i069 

SO/ RSO 

.000 

15 :34:37 21 Aug 08 

Seq: 1070 15:58 :56 21 Aug 08 

Uni(s 

ppb 

SD/ RSD 

seq: 1071 

SD/RSD 

.000 

Seq: 107Z 

.ooo 

16:01:34 2 1 Aug 08 

16:04:21 21 Aug 08. 

W$11592563 

1.40 pp)> 

~~,~, • Sampl e tO: BLANK 

.028 L ppb 

:ooo . L.4o 

.ooo 

Seq: 1073 

. 028 

16:07 :02 21 Aug 08 

HG 

HG 

IIG 

• 

HG 

HG 

I!G 

HG 

==•• ~•== •- ~--=•-==~=-z=,. ..,•••-• •-• """'" .0.== -• 

"* Sample rD : H1'RX SPK Seq : 1074 16 0~:40. 21 Aug 0 8 HG 

l .25 ppb .000 1.25 .q~ -~ ' . • •---•----•=~••••--•--~•••--==..,•••~•·=--~·-----~·••~•~== =-•.-•---= = 

••• Sa11pl e 10: Af'22 63-08! Seq: 1015 16:12:29 2 1 Aug 08 I!G· 

f'41)>. Hg .020 L ppb . 000 .020 

••••~--.. ~•••--••••••••••••••••••-•••••••• •••c• === =:.•• •••••--•~ =-••••• 

••• Sample ID: Af'2263-08 Seq: 1076 16: 15: 09 Zl Au9 08 HG 

. . 024 L ppb .000 

·*•• Sample ID: AF2254- 08 

.040 L ppb . 000 

. 024 

Seq: . 107.7 

. 040 

16:18:02 21 Aug OS BG 

••••••-•·-·-=--••'1" •••-,.·-•-•--'"'"=n=w ===- =--• ---= •~••••....,•• --

VES 005653 
ot · . .• 

--- ~' 

~ Folder: Aug 08~ 

Protocol: HG L_JO~ 

P~qe 1999 

• • "- P0$1"- RUW REPORT• •. • Line Cone . lJnits SD/RSO 1 2 3 4 5 

----- -- -- -- ------~-------- -------~-- -- ----- ---- ---------------------

••• Sample I D: AF2255.·08 

. 032 L p pb .000 

S<>q: 

.032 

1018 16 : 21:02 21 Aug 08 HG 

••---••••••----••••••••••••••••••••~---~-------~•••••---•~=Q•Da•••m.-._•~·--•• 

"' Sa~> le I D: AF2251·08 Seq : 1079 16: 23: 40 21 Aug 08 IIG 

f\Y Hg . 070 L ppb 

••• Sample I D: AF3531- 04 

Hg . 037 L ppb 

.000 

.000 

.070 

. S<tq: 

.037 

1080 

!.J' 

~:; 

16:26:19 21 Aug 08 HG 

---~ ••• Saaple ~-------·-----~·------~--- ID: .AF4402-04 · -== ····- -----

llq .040 L ppb 

~· · Sampl e ID: Ar6345- 08 

~, Hg .OSl t. ppb 

••• Sampl e to: f6788·0~ 

Hq :272 ppb 

.000 

.000 

.000· 

Seq: 

.040 

Seq: .1082 

• 051 

S~q . 1083 

.272 

16:28':58 21 Aug 08 OG 

16 : 38:30 21 Aug 08 HG 

16 : 41:1 4 21 Auq 08 HG 

~ ~-~ -~ ---- --------------------=-·--.-G=-·-.. ··----... = ........ Sample 10 : A"f 7333 ~t Seq: ;1084· 16: 44 :04 21 Aug 08 

Wqt .50000 Vol 7.5000 

llg 45.8 . H ppb .000 

...... Sampl• ID: AF7333- 01 

Hg 18.0 

_.., •. o~g-

... SaJ11Ple IO: bl k 

- .081 L ppb .000 

... Sample ID : AF7334-0l 

Hg 2.83 ppb . 000 

45 . 8 

Seq: 

Seq: 

-.081 

seq: 

2. 83 

1085 17:12:19 21 Aug ~8 

~ .SOOOO Vol 1 .5000 

1086 17 : 15:03 21 Aug 08 

Wgt . 50000 v_ol 7. sooo 

IJG 

1087 17: 11: 41 

'-11 .. 

21 Aug 08 HG 

v..t.. ::. ~ -> 

4'2. • As- . ·~·=•••••••~==== ~=~••••--==~~••----·--~===~••••••~ --~a~·----• 

VES 005654 
Folder : Aug 08a· ~· · 

Protocol: HG- L J 08 

·~*POST-RUN REPORT*•• 

Pago 199.9 

Li·ne Cone . 1,Jnits S.D/RSD l 2 · 3 

--,..-------------------------.--------------------------·---------..---------------- ... 

Hg 

••• 

$•.mp1e I D: b1k . 

-.• 01 6 L' ppb . 000 . 

seq: 1008 · 17:20:20 21 Aug 08 RG 

01~ · . .. w 

17 : 23:04 21 Aug 08 RG 

'-'1\-" .,. ....- v•io .. ~ ·~ ~ 

" Hg 2.67· ppb .000 2.91 · · · • . 

Samp~e I D: l>.F7335- 01 Se q: · '1989 

o · v.,.~ ~· 0 s:-· . . . J)~ ,..,. 't>O uo-. 

--;,o~:: s::;~=~~;-;~-----A······ -· ~~~;~==~;7; ~~~~:; -- =-

.000 - . 013 . ·. 

·•. • wa••••••••--------~.-e--• . =----•--••••-----·-------..-•••--•-- . . a=~=o= •-=• 

~~ Sampl e ~D: AF1336-0l 

not in 

.0.00 

Seq: 1091 11 :.29:09 21 Aug 08 RG 

order with ws Wgt . SOOOO .Vo1 7,50QO 

Hg 6.84 H ppb 6.:8 4 · .. ·~ .. :;r~ · · · · .l> L ~ "" 

-"' ., • ., .. b8'" . ~ · *** Check Standard: 

Line F'lag \Rev. 

ilg 103 . 

2 Ck2,: 

r"ound 

1.0.3 

CCV 

True 

1.00 . 

... 

Line 

Hq 

Check Standard: 1 Ckl: ccs Flag Found Ran e{+/~) Units . . 004 . .100. ppb 

••• 

Sample !0: AF7338- 61 

1 .23 p pb .000 

• • • Samp le ID: ~~73~? 01 

S.e<J; 10 92 . 17:31;50 21 .1\ug 08 HG 

U~its SD/ RSD 

ppb . 000 

Soq.r 1093 

SO/ RSD 

.ooo· 

Seq: 1094 

Seq: 1095 

1. 23 

17:34:28 2 1 Aug 08 

17:38 : 00 21 Aug 08 

Wgt . 50000 Vol 7.5000 

11:40 : 55 21 Aug 08 

ilgt . 50009 Vol 7.5000 

HG 

RG 

HG 

Seq: ! 096 17:43:36 21 Aug oe HG 

Rgt • 50uoo· Vol 1·. sooo .. 

•••· Salllple !D: AF7J40· 01 Seq: 1097 , 17:46: IS 21 Aug 08 HG 

Wgt .50000 Vql 7. 5000 

Hq 6.00 H ppb . 000 6.00 .._ , . 0 0 c.. . ..... ~,. 0 ' ., .. ~- • 

----~ =-=====--- =======--==-~c:==--==~ ==== ft·--~~ ··---~==~====~..---·~==== 

i 

VES 005655 
Li ne Cope. Unit:s 

Folder : · Aug:_ OBa. 

Protocol: ·HG-L JOB 

• w*POST-RUN ~EP0 • 

SO/RSO 1 2 3 4 5 

----------:-.------------------:-.. -- --- -- -- ---.. --------------------,--------- ••• SaJIPle ID: AF73 41- 0 1 

Hg 9 . 16 H ppb 

~o· o o'\L ,ooo 9 . 16 

1098 17:48: 54 

wgt . snooo 

.f?; .: 

2 1 Aug 08 ~: HG 

Vo l 1 . 5,000 · · 

;!) \.. :: oo ~ 

'•--===== ====-===========.w&:==••• ===~===--• •••••••~• vs--~~~~••• := 

..... _. Sarf!Pl e ·IO: bl. k. Seq: 

Hg -. 044 L ppb . QOO -.044 

~~ Sample ID: AF7345- 0l s eq: 

1099 

1100 

· 1 7:51 : 3 3 .21 Aug 08 

17 ; 54 :11 2 1 Auq 08 

Wg t 1 .0000 Vol 750000 

.. H<i' 

HG 

Hg 987000H ppb . 000 987000 ;<·•·2 1:;. . 

-> ""'~,_ . ~L ~ f~ .· ~- ~----.-------•-••••••--•----•wo•••---..- •• == ====== =aa . ··•··~·• 

*** .Sampl e .ID:. blk Seq: 11Ql .' 17 : 56:52 2 1 Auq OS ; 

Hg -,007 L ppb . 000 -; .007 m'<f. . . . . ff.:;V;. . --•••••••• ··· -===n-====•~==== •----•-.----=-•=== -=-~* ••••••· 

*** Sample ! D: AF7 346-0l . Seq: 1102 17 : 59:42 2 1 Aug 08 \r,;,J:!j 

Hgt 1. 0000' Vo l 7SOOOO?l 

Hg 667000H ppb . 000 667000 . .J:> 1 · ;· 

-?-~.Je±-.:==.:. = .... --=-- ==== ... ·--=--=-----·Q ......... ~= =-;;3:_£_: • •• Sampl e r'D: bl k Seqi 1103 1S :02 : 22 21 Aug 08 ·~;,.: n~ 

·t ,;:·,.o{' 

Hg ·.< - . 004, L PPb . . 000 -. 004 

• 

;;.,., Sampl e ID: bl k Seq: 1105 18:07: 44 21 Aug 08 . RG 

Hg . 001 L ppb .000 . 00 1 .J> 

••• Sample I D: af7339· 01 .Se q : 110 6 18: 13:02 21 Aug 08 HG 

Wgt 1 .0000 Vo l 225 . 00 

Hg 141. H ppb .000 14 1. !) L. :; O O Z,.?...$"' ~ 

- "o· I &,L · . .. •••••• ~ •••---•••.-•-----••••--•••••~ •• =~ =- •••• •••••a& ==-=a--• •••-

••• Samp l e 1 0 : s p i ke 

Hg 1. 34 ppb 

L _ _ -----'-- · 

Seq: 

11511592768 

.ooo 1.34 

1107 18: 18 :43 21 llug 08 HG 

VES 005656 
. .. ' 

Line Cone. Units 

Folder: Auq_08a 

Protocol: HG-L J08 •~*POST-RUN REP0aT•~~ 

SO/RSQ 1 , 2 3 4 • 

, 

Page 199? i 

5 

~-------------------------------- --- ------------ ---~------- ~- ----------

••* Check Standard: 2 tk2: CCV 

Lin& Flaq \;ftC'( . rot,tnd. 'Erue 

Hg . 113 . 1. 13 1 . 00 . 

• .,. Check Standard : 1 Ckl: CCB 

Line Fla9 Found Ranqe(+/-} Onits 

Hg .001 . 100 ppb 

Seq: 

Uni ts 

ppb 

1108· 18:21:22 21 Aug 08 

SD/RSD 

Seq.: 1109 

SD/RSD 

.000 

.060 

18:2~:00 21 Aug 08 

BG 

HG 

VES 005657 
. . 

Method 6010 ~Test Method for Total 

) 

Metals by ICP 

Maxxam Analytics Inc. 

6740 CatnpobeUo Rd. 

Mississauga, Ontario, Canada 

L5N2L8 

1-800-668-0639 

www.maxxamana!ytics.com 

I 

VES 005658 
Unique Calibration St~nidards 1.0. table for ICP-5 (Axial) 

!(Standards prepared in 2% HN03) .. . . 

Generati.D. Unique !D. 

BLA~ /ICS/ CCB ICP-WC-0834 

STO,A ICP-WC.OS32 .. .. , STO·~ ICPcWC-0831 

CAl·16KNa· ICP·WC-0833 

HH<na ICP·W0·08$ 

ICV /CCV ICP-WQ.0854 ._.. 

ICS'AB ICP.-WQ·0841 

CRJ ICP·If/0·0852. .. UBuffer ICP·WQ.08S3 

Analvstlnilials: fa 

oa1e:· zpot,/ ~; ;Z ( ... 

M8>0<8m Analytics Inc. 

CAMFC~7911 

. Page ·.1 ol1 

VES 005659 
Auto9ampler Report Table : AUG21A 0~/.2..1/08 11:05:06 PM 

Table Name: AUG21A 

Sample Positions: 2/~92 

Ripse Stati on location.' is 

: __ Racks "--. . 

Autosampler Type: TYPE TJA. QC Positions: 13/19 · B Sets: 1 ~ack - 1, · pos · -~ : 

page 1 

Rack II TyPe \!!lag~ #¥>os Left Analyse.s/Pos ... .. -.. -- -------------------- ------------ 1 Aux.· (L) Ra.ck ·a sample 

3 sample 

4 Sample 

5 SamPle 

- -- ·Sal!'ple Sets 

·setll . ·Type 

(l 6mm) 

(l 6mml. (16mm) 

(}6llll1) 

Prepare? 

STD/QCjB~K 

Samples 

Samples 

Samples 

Samples 

Description 

--------- ............. ........ .... 

•1.3 ?0 . ·0 . 1 

0 1 

0 l 

12 l 

Method #¥>os Rackll 

-------------------- -------- 1 Normal No m?-=am .. PSC34 180 2 

--- Preparation Info -~

Set# Uptake Upt,akell2 Final t>il . Factor 

No Samples Prepar~cj. 

Rae)< Ill 

Pos Row Col Sampl e Name Set;: ·ll II Used Type .. ..: .. --- -------------------- ------------ 1 l 1 NONE -NA-' 1 Standard 

2 1 2 knahi 15 ·-NA- 1 Standard 

3 1 · 3 STD-A- -NA- 1 Standard 

4 1 4 STD-'B -NA- 1 St;:andard 

5 1 5 CAL-BLK -NA- 1 Standard 

6 1 6 HCL -NA- 1 · QC Standard ·t'T': • . 1'9 Not Used·) 

Rack 112 

Poe Row Col Sample Name Set II #Used Type 

-- -- ----~-------- ------- -~

1 l 1 ICVAX 1. . -NA- Sample 

2 1 2 ICB 1 -NA- sample 

3 1 3. CRI 1 -NA- Sample 

4 1 4 . ICSJ\BAX 1 -NA- sample. ,5 1 5 HI.KNA . 1. -NA- Sample . 6 1 6 1.591852 :AF734l :DUP 1 -NA- Sample .7 1 7 15~1 852 ;AF7341: 1000 1 -NA- sampie .8 1 8 . 1591852 :AF7339: 1000 1 -NA- . Sample 

9 1 .9 1591852:AF734!):1000 1 -NA- Sample 

10 1 10 .CCV 1 - NA- Sample 

ll 1 ll CCB 1 -NA- Sample 

12 1 12 1592280:BLANK:100 ·1 -NA- Sample 

13. :t 1 1S92280:RBFMAT:100 1 -NA- Sample 

14 2 2 1592280 :MTRX SPK :'98 l -NA- Sample 

15 2 3 . 1592280:AG2290:DUP 1 -NA- Sample 

StartPos 

--------

1 

VES 005660 

'"'-"''. 

--~

: :' 

. . . AutoSampler Report Table: AUG21A . ., '08/21/0!l 11 05:0~ PM page 3 

"· ·..-! 

Rack #3 .•. 

~.r 

.. 

~ 

Poe Rov col Sample Name ~ Set # #Used Type :~ __ ______ __ _________ , . 

.... ---------·-- 16 2 4 159105S:AD6033:600 ~ 1 -NA- Sample ... 17 2 5 CCV ·•: 1 -NA- Sami>-le 

18 2 6 CCB . " 1 -NA- Sample 

19 2 7 1589843:BLANK:SO 1 -NA- Sample 

20 2 8 1589843:RBAGBL:50 1 -NA- Sample 

21 2 9 1589843:SPIKS:DUP 1 -$- Sait!ple 

22 2 1,0 l68984-3: SPIKB: 50 W< 1 -NA- Samp.l~ 

23 2 11 ~5~9843:AB0772:50 ,, 1 m- Sampl.e a_4 2 12 1589843:AB0773:50· ::- 1 - NA- Samp_le 

-25 3 1 158984 3 :AB0774 ,·so ' 1 - NA- Satilple ,. 

26 3 2 1589843 ;Ml0775: 50. .. 1 ·NA- sample · 27 j 3 1589843 :AB0716 :'50 ;.·~. 1 - NA- Sample -: 

:28 3 4 1S89.843 :AB0717 ,·5Q t~. 1 - NA- Samp~e ' 

29 3 5 l5898~3:AB0778:50 .~· l -NA- Sampie .. , 

30 3 6 1589843:1\20779:50 ·"'· i -NA- Sampl(O 'i 

- Sample ·. 31 3 7 CCV .. l . -NA· 32 3 8 CCB :t· 

.·~ 1 -NA- Sample 

33 3 9 1589843, A.Bono :·so ;,, 1- :NA- Sample < 

34 3 10 ,1589843 :AB0.701: SO, .·{ 1 · NA- Sampte 

35 3 11 l589843':AE0782: 50 :•;.,. 1 · tiA- Sample 

36 3 12 1589843:ABo7oJ:so ·:.:- 1 -NA- Sampl~ 

37 4 1 1589.843 :ABCl1S4: s.o ·~ 1 -NA- sample 

) 8 4 2 1589813:AE0785 :50 ·:: 1 -NA- flample 

39 4 3 1589~43:AE0786:SO 1 NA~ Sample 

40 4 4 1589843:AE0787:50 .·;. 1 -NA- SaJl1Ple · 

4t 4 5 1S89843:ABQ788:50 ... 1 -NA- Sample 

42 4 6 1589843:AB0789:50 1 -NA- Sample 

43 4 7 158984):AB0790:50 1 -NA- Sample· 

44 4 8 l589843:A.E0791:50 1 -NA- Sa'!'Ple 

45 4 9 CCV 1 -NA- Sample 

46 4 10 CCB 1 -NA- Sample 

. 47 4 1l 1589557:8LANK: 100 l - NA- Sampl e •• 4•8 4 12:' ''l589SS7'!'REPMAT: 102 ... 1 . ·-NA" Sampl:e 

. Rack #4 

Pos Row Col Sample Name Set • II Used Type 

-------------------- ---- 4------- 1 1 1 l589557:MTRX SPK:96 1 -NA- sarnpie 

2 l. 2 1589557:AP1 858:DUP 1 - NA- SalliPle 

3 l. 3 1589557:AF4858:100 1 -NA- SalliPle 

4 1 4 1589557:~F4747:104 l -NA-. Sample 

5 1 5 1589557:~F4748 :96 1 -NA- Saniple . 6 1 6 1589SS1:AP4749: 102 1 -NA- San:ple 

7 l. 7 1589557: AF475 6:9~ l ·-NA- Sample 

8 1 8 l589557:AF4835:100 l -NA- SaJl1P1.e 

9 1 9 lS89557:AF4837:98 1 -NA- Sample 

10 1 10 l589557 :A.F4838:96 l -NA- Sample 

11 1 11 CCV 1 . -NA- Sample 

12 1 12 CCB 1 -NA- Sanj>le 

13 2 1 1589557:AF484l:l04 l -NA- Sample 

14 2 2 l5B9557:AF1842:96 l -NA- Sample 

15 2 3 . l589557:AF4846:96 1 -NA.- Samp,le 

VES 005662 
AutoS ampler Report Table: AUG2,1A 08/21/08 11:05:06 PM page 4 

Rack #4 

Pos Row Col Sample Name Set # lfl!a ed Type 

------- -------~- -- ----- ------------ 16 2 4 l589557:AF4847:102 1 -Nih Sample 

17 2 5 1589551:AF4848:98 l -NA- SaJ!lPle 

18 2 6 1589557:AF4853:96 1 -!<A- Sample 19 2 7 1589557:AP4855:100 1 -NA- Sample 

20 2 8 1589557:AF4860:98 1 -NA- Sample . 21 2 9 1589567:AF4863:104 1 -NA- Sample 22 ,2 10 l589557:AF4877:98 1 -NA- Sample. 23 2 11 l589557:AF4884:96 l "NA- Sample 

24 2 12 l589557:AF4885:99 1 -NA- Sample 25_ 3 1 1589557:REPMAT:102 1 -NA- Sample 2'6 3 2 CCV 1 -NA- Sample 27 3 3 ,CCB 1 NA~ SaiiJPle 

28 3 4 1590,!)92: BL/INK: 100 l -NA- SaJ!lPle 

29 3 5 1590092:REPMAT:102 l , -NA- Samp1e 30 3 6 l'590092iMT~ SPK:~B 1 ~W\ Sample 

31 3 7 15900~2:AF4769:0UP. 1 -NA- ~ample 

32 3 8 1590092:AF47G0:99 1 -NA- Sample 

33 3 9 159009;2 :AF4743': 102 . 1 -NA7 Sample 

34 3 10 1590092:AF4745:l04 1 -NA- Sample 

3:> 3 ll 1590,092 :AF4752: 9.8 1 -NA- Sample 

36 3 12 1590092 :AF4753:98 1 -NA- Sample 

3-7 '4 1 1590092:AF4754i98 1 -NA-. Sample 

39 4 2 1590092 :'AF4755: 98 l - NA- S!>RIP.le 

39 4 3 CCV ' l -NA- Sample 

40 4 4 C~ 1 -NA- Sample 41 4 5 1590092:AF4?70:98 l -NA- Sample 42 4 6 1590092:AF4771:102 l -NA- Sample 

43 4 7 1590092:AF4772:102 l · NA- Sample 44 4 8 1590092:AF4773:96 l -NA- Sample 45 4 9 1590092:AF4778:102 1 -NA- Sample 

46 4 10 1590092:AF4801:102 1 -NA-' Sample 

47 4 11 1590092:AF4805:96 l - NA- Sample 48 4 12 l590cr92:AF4819:98 l -NA- San'Iple 

Rack liS 

Pos Row Col Sample Name Set II #Used Type 

-------------------- ------------ 1 1 1 1590092:AP4821:96 1 - NA- Sample 

2 l 2 1590092:AP4826:100 l - NA- Sample 

3 1 3 l590092:AP4862:100 1 -NA- Sample 

4 1 4 l590092:RBPMAT:102 1 -NA- Sami>le 

5 l 5 CCV 1 -NA- Sample 

6 1 6 CCB l -NA- sa~le 

7 1 7 WASH1 1 -NA- Sample 8 1 8 WASH2 l -NA- Sample 

9 1 9 WJ\SH3 1 -NA- Sample 

10 1 10 1592280:REFMAT:1000 1 -NA- Sample 

ll 1 11 l592280:AE5685:980 1 -NA- sample 

12 1 12 1 592280:AE5685:9800 1 -NA- sample 

13 2 1 1592280:AP4626:980 1 -NA- Sample 

14 2 2 1592280:AP4627:960 1 -NA- Sample 

15 2 3 CCV 1 -NA- Sample 

VES 005663 
Ad coS all\' leo' ~eport 'l'able: AUG21A Q8/21/08 11:05:06 PM page 5 

Rack 115 

Pos Rov Col Sample Name Set ll #Used Type . · 

-------------------- . ----- ----·-.------- . 1 6 2 4 ccs · . l -NA- sample 

17 2 5 ( emp.ty" ) 1· -NA- · - NA18 2 6 ( empty ) l · NA- -NA19 2 7 "< empty ) 1 -NA- -NA20 2 8 ( empt y ) 1 -NA- -NA~ 

21 2 9 ( empty ) 1 -NA:- : NA22 2 10 ( empty ) 1 -NA- -NA23 2 11 ( empty ) 1 -NA- -NA- 24 2 12 ( empty ) 1 -NA- -NA- 25 ) 1 ( empty ) 1 -NA- -NA26 3 2 ( empty ~ 1 -NA- · NA- 27 3 3 ( empty ) . 1 -NA- ·NA; 

28 . 3 4 ( empty l 1 -NA- -NA~ 

29 3 5 ( empty ) 1 -NA- W>. 30 ) • q ( ~tY ) 1 NA . ·NA·- 31- 3 7 ( empty ) 1 •NA· -·NA-· 

;12 ) 8 ( empty ) 1 -NA- CNA- ~3 ) 9 ( empt y. l l -NA- -NA- . 3.4 ) 10 ~ empty ) 1 " cNA- -NA~ 

35 3 11. ( empty ). 1 -NA- -NA· 

36 3 12 ( empt y ) 1 -NA- -NA-

(37 ..• 48 . ~t Used) 

·.• 

VES 005664 
1479 

PrQfile line : As 189.~(2 

Peak Position : . . 02~993 

Peak Intensity; 1345.7. 

Peak Width, · I '} .16961 

ll Hew Spec. Shift at ;, 0 

0 

., 

.. 

~ v 

., 

c 

.. 

-31 0 

~pectnm Shifter Posit.ion I . . 

31 

VES 005665 
,. 

. AI).alysis Report QC Sta!ldard DS/21/08· 12 : 38:5j PM page 1 

·Method: PSC34 sampl~ Name : HCL Operat.or: gbu 

RUn. Time: 08/-21/08 12 :33-:32 

comment : 

M\:>de: CONC Cor.r, Factor; 1 

Elem 1\g Al · As B . Ba 'Be Bi 

units ppm PPJ!I ppm ppm ppm ppm ppnl 

Avge . 0007 .0184 . 0171 .0011 .00038 . 00038 - . 0923 

#1 . 0025 . 0374 , 0326 ,0034 . 0.0052 . 00944 . 0 120 

#2 . 0000 - . 0016 . Ol41 . 0003 .OOQ22 . .00030 -.0~00 

-#~ - .000;3 . 0 195 .0044 - . 0005 . 00039 . 00040 - . 0089 

El em .Ca Cd co Cr cu Fe K 

Uni ts ppm ppm ppm PP'!I. ppm ppm ppm 

Avge .0392 . ooooo . 0027 . 0000 .0001 • 0054 -.1077 . 

# 1 .0417 . 00011 . 0023 .001 9 . 00'13 .0063 - . 0250 

li2' .0~64 - . 000.05 . \)011 - . 00.0.8 -. oof9 .0041 - . 0963 

#3 . 0396 - . 0.0006 . . 0048 - . 0010 .0008 ,0057 - . 2017 

Elem Mg Mn · Mo Na Ni p 220J/1 

Units ppm ppm ppm ppm ppm ppm. ppin 

Avge . 0291 -. 0000.5 . . 0001 .0471 . . 0022 .0158 -.0170 

#1 -9262 . 00029 . 0015 . 0483' . 0032 .01 61 ~ ;01:57 

#2 . 0204 - ·. 00018 -.0009 . 0445 , 0031 . 0.063 -.0119 

#3 . . 0408 - .00027 - . 0005 . 0486 . 0002 .0248 - .0236 

Elem 2203/2 s Sb 1960/1 1960/2 Si Pb 

Units ppm ppm ppm ppm ppm ppm ppm 

;Avge . 0078 .0058 - . 001 4 -. 0169 . 0144 . 0489 - .0005 

# 1 .0082 .028.1 .0092 -. 0169 . 0153 .0517 . 0002 

112 .0014 - . 0137 -.0044 -. 0145 .012 1 .04 48 -.0030 

#3 .0138 .0031 - .0091 - . 0191 . 0157 . 05 01 . 0013 

Elem Se S.n Sr Ti Tl u v 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge .0040 . 0007 , 00022 . 00187 .0045 .0409 .0029 

# 1 .0046 .0037 .00020 . 00246 . 0027 .1488 .'0036 

# 2 .0033 -·. 0013 . 00017 . 00108 . 0049 -. 0 093 . . 002'7 

#3 . 0041 -. 0002 . 00028 . 00206 . 0059 -. 0 169 . 0025 

Elem '[ 213Zn Zn Zr 

Unit!' ppm .ppm ppm ppm 

}\vge 37.43 . 0.010 .0025 . 0027 

#1 . 37 . 20 .0013 .0026 .0030 

#2 37.49 . 0006 .0014 . 0019 

#3 37.58 . 0011 . 0036 . 0033 

VES 005666 
Standardization Rpt. . . -08 / 21/08 12.:.47:01 PM page 1 

Method: PSC34 Standard: CAL·BLK' / 

Run Time: OS/21/08 12:41:30 

Blem Ag Al As B Ba .Be Bi 

Avge - . 0346 1.137 ,0323 .1219. . 01566 - . 15459 :-0466 

til - •. 1369 1.108 - . 0870 . 076.0 -.00500 -.1739J. •.1169 

. 112 .0030 1.17.0 - . 0.230 ,l.449 .031 98 - .13593 - . 0470 

H3 . 0300 1.133 . 0130 . 14<19 .01999 - .15392 .0240 

Elem Ca Cd Co Cr cu Fe Fe· 

Avge .0120 ,02066 - . 0573 - .0090 . 4518 -·. 0170 . .0330 

til .0030 -. 093 9~ - .0750 -.. 0520 . .4708 -.0820 - . 0140 

tl2 . 0180 . 01199 - .0370'. .obo .4128 .0300 .0690 

tl3. • 015() .!1.4393 - .. 0600 :ouo .4718 .001 9 . OHO 

Ble111 K lolg Mg Mn Mo Na Ni 

~vge 6024 - , 0133 . 020()' .qoop . -.op:p 22 . 61 .. o·o.Jo 

Ill -·. 7096 -.0780 -. 001 0. - . 01299 - . 1;1.5 9 21 . 68 - . 0590 

112 - . 5887 .0080 .0630 . 00600 .. . 0930 23 . 19 . 0010 

113 - . 50.87 ·.0309 - . 002'0 .00900 . 0190 22· •. 95 .0670 

Eiem p 2203/.l 2203/2 s Sb 1960/1 1960/2 

Avge .2849 . 3155 -. 0630 .2'795 .. 0010. - . 0633 .0546 

Ill .2769 . 7306 -.1279 . 2539 - .1669 .0500 -. 0440 

112 .2969 - . 3578 .1079 . 3028 .0560- - . 1859 . 1469 

113 .2809 .5737 - .1689 . 2819 .1139 - .0540 . . 0610 

Elem .Si Sn Sr Ti Tl u · v 

Avge . 0856 - .0140 .05197 • . 01033 - . 0720 :o21o - .0020 

Il l -.0560 - . 0450 . 04798 - . 07296 - . 0920 - .1199 - .0450 

112 . 1859 - . 0310 .'05597 . 02099 - . 0430 . 0760 . 0360 - '·113' .1269' .·o3a o : Of?'I 9'7' • . : 0:!()99' .. -. 0'810' . :· ro~9 ·:·oo:Jo 

Bl em 213Zn zn Zr 

Avge - .0080 - . 0386 -1 . 384 

#1 -. 0180 - .0520 -1.487 

112 .0020 - .()200 - 1.296 

113 -. 0080 .- .0440 . - l. 369 

VES 005667 
• ·'r.<' 

Standafdization Rpt. 08/21/0_8 12: 5;1.: 48 PM page 1 

Method: PSC34 Standard:· STD-B . / 

Run Time: 08/21/08 12:.7:05 

Elem Ag Fe Mg Mq . p s . Sb 

Avg~ . 11.74 31.66 ~.090 18.62·. 18 . 43 8.393 4". 803 

#1 11.73 31. 70. 4.066 18.33 .18.50 8.371 4. 554 

#2 11.72 31.'53 . 3,9.95 18.6'3 18.21 . 8.363 4 : 867 

#13 11 . 77 31 . 71 4 .2lQ 18.90 18.57 8.447 4 . 989 

Elem Si sn Ti 213Zn Zr 

Avge 14.10 1 0.90 145.15 4. 922 171.5 

Ill 14.14 ~0.86 144.99 4.912 171.3 

112 13.SI8 10 , 84 144.61 4.911 170.8 

113 14.19 11. .01 145.84 4. 945 112.4 

VES 005668 
~:r· .,, :: .... 

Standardization . . Rep9rt 08/21/08 12:S1!4Q ~ page 1 

Method; PSC34 Slope • Conc (SIR)/IR 

Element Wave len High s t d Low std · Slope· , Y- inte rcept Date; Standardized ' Ag 3'28 .. 068. STO-B CAL-BLK . 042686 ·. 001479 08/21/08 12:,47:05 . Al 3·08. 215 STO-A CAL B~K . 367275 -.417750 01)/21/08 12 : 47:05 

As 18? . 042 STD- A CAL· BLK .099394 . 003212 08/21/08 12:47;05 .· .B 249 . 678 STD- A CAL·BLK. . 0'!7'[87 -. 00579,1 08/2.1/0s 12:,47 ; 05· Ba 455 . 404 STD-A CAL· BLK · . 03·3364 - . OQ0522 08/21/08 12:47;05 . se 313 . 042 STD- A CA.j:.-BLK . 0.!!7804 . 001206 08/21/08 12:47:05 

Bi 223 . 0.61· STD•A CAL·BLK .092664 '00.4322 08/21/08 12:47.:05 

Ca 317.933 STD-A CAL·BLK .786360 -.009432 08/21/08 12 :47:05 

Cd 226 . 502 STD-A CAL-BLK . 005890 - .000122 08/21/08 12;47 :05· co 228.616. STD-A CJ\.L-BLK .032474 . 001861 08/2i /08 12:47:05. .Cr 267,'116 STD-A CAL a~. .088471 oo67~6 08/21/08 12 : 47:05 ·' · Cu 324 . 753 STD-A CAL:BtJ< . 01!02E!!! - . 0],8190 '08/21/08 12:47:05 

Fe .'25.9: 940 STD~J;I CAL-BLK .063228 -. 002!185 08/21/08 1.2:i7:os· Fe :Pl.441 STD-/1. CAL-BLK 1. 24065 .021080 08/ 21/08 12;47:05 · K 766 . 491 knahi 15 CAL-BLK 1 ' 02'189 . i41451 08/2~/08 1.2:47:Q5 . t~g 2t9 . o7a STD·B- cAL BLK . 2~5704 -. 094.912 08/21/08 · 12 : 47:05 

38.3 ,,23J.. . ' Mg STD-A C~·BLK . 80.2240 . 01069.1 08/21/08 12:4'7:05 .. Mn 257.610. STD-A 'CAL-BI,l< . 048008 - .'000032 08/21{08 12 : 47 : 05 

Mo 202' .. oo.o STD-B CAL-BL,K .02685!> .000036 08/21/08 •12:47:05 ' Na SfltL 995· knahi 15 CAL-BLK .941266 -~2.15 3 08/21/0Q 12:~7:05 . Ni 231. 04 STD-lC CAL-BLK . 041558 - . 000125 . 08/h/08 12:47;05 

p 1'7•8'.287 STD-B CliL- BLK . 275610 -. 078510 08/2'1/08 12;47;05 

2203/.1 220.35i . . . 

STD· A. CAL-BLK .'02J403 ~ '00.7;384 08/21/0S 12 :~17 :05" 

22·03(2 2:io·. 35~ STD-A CA!'-BLK . 04,3703 . 002752 08/21./08 12:47 :·o5 

s i 82 . 04.o STD-B CAL-BLK .246489 - . 06890p· 08/21/08 12:4'7 :05' · sb 206 ,·838 STD-B C\L·BLK . 103216 - .000103 08/2i/08 12:47:05 

1960/1 196:'. 021 STD-A CAL·B·LJ< .OIJ9628 . 005674 08/21/08 12:47:05 

1960/2 196 . 022 STD-A CAL-BLK .088082 - . 004813 08/2i/08 12:47:05 

Si 251 . 612 STD-B CAL-BLK . 071896 -.006156 08/21/08 12:47:05 

Pb 220.353 ·NONE NONE . QOOOOO .000000 *NOT STANDARDI ZED 

Se 196.026 NONE' NON!:; · .000000 . 000000 *NOT· STANDARDIZED 

sn 189.989 STD-B CAL-BLK . 091702 . 001283 08/21/08 12:47:05 

Sr 407.7.71 STD- A CAL-BLK . 008924 -.000464 08/21/08 12 : 47:05 

Ti 33~. '941 STD"-S CAL-BLK . 0068'89 .OU0071 0'8/2170'8 12 · :-4'7': ·o 5 

Tl 190.864 STO-A CAL-BLK .203239 . 014626 98/21/08 12:47:05 

u 367 . 000 STD· A ' CAL-BLK 1. 25463 -.026334 08/21/08 12: 47:05 

v 292.402 STD-A CAL-BLK . 083312 . 000167 08/21/08 12 :47·:05 

y 371.000 NONE NONE 1. 00000 .000000 *NOT STANDARDIZED 

213Zn 21 3.856 STD·B CAL-BLK ' 101430. . 090811 0!)/2l/08 12:47:05 

Zn 206 .• 200 STD-A CAL-BLK . 020396 . 000788 08/21/08 12:47:05 

Zr 339. :!.'98 STD· B CAL-BLK . 005790 . 008015 08/21/08 12:47:05 

VES 005669 
Standardization Rpt, 

Me.thod: PSC34 Standard: STP-A 

Run :rime: 08/2 /~8 12 :S2:27 

Elem Al As B 

Avge 6.103 4 . 948 20.43 

'Ill 6.076 5 . 020 . . 20 . 48 

112 6.062 . 4·. 9.24 21) .42 

#3 6.171 4 ,900 2Q ,:p 

Elem Cd Co cr 

Avge 86.985 30.86 11 .29 

Ill 86-.801 30·. 74 11.29 

#2 86.724 30.75 11.26· 

#3 87 ; '*.29 31.10 11.32 

.Elem Ni 2203/1 - 2203/;! 

Av.ge 1:). u 43 : 7i . 22.91· 

Ill 12.12 44. 12 22.71 

112 12. 01 44 : 3i 22. 91 

#3 12.22 42 , 70 23-i!ll 

Elem u v Zn · 

Ayg_e 3 . 973 5,894 102.2 

.; 

111 4.066 5 ,sa8· 101.9 

112. 3 . 820 5 .849 101.8 

#3. .4. 033 5 . 953 1\)2. ~ 

. i~',"!,:·· 

~:~ 

· 

08./21/08 12 :57 :54 

./·. 

.f) 

. ~· .. Ba ··~· . . Be 

28 . 531 J;-63. 045 

28 . 3·86 :., 62.889 

28.679 :'{ · . . ' ;., 63. 202 

28·. 528 ; -63. 044 

2. 

~;;- · . Cu ·*: Pe· 24 . 24 ·. 8 . 039 

24.16 l!¥8. 017 

24 : 30 t:'· 981 2~ 26 ~· 8 .118 

4{--

1960/1 1960 /2 

5 . 250 334 

·5 . 233 lis.rl28 

5 : 399 ';i 5.327 

5.118· ;.s. 445 .. ~ . 

. ·. • r5 :, . 

~:-. · 

; •.. 

ZV.Lf ~3 . 

21f • zq 

0. 84'5 

PM page 1 

~i ca 

5.129 12 . 80 

5.262 12.76 

4,957 12.79 

5. 1:~ 8 12 . 8.4 

Mg Mn · 5:912 20 . 48'8 

5 . 947 20.42? 

5,1)66 2o.sp. 

5.923 2Q , S27 

Sr Tl 

53 .!;l,i ·4 .860-

53.332 4. 836 

53.7.44 4 . 825 

s_3. 466 4.921 

VES 005670 
Stapdardiz.ation Report 08/21/08 12:57:54 PM page 1 . 

Method: PSC34 Slope • Conc(SIR)/IR 

Blement Wavelen High std Low std Slope Y-in t ercept · Date Standardized 

Ag 328.068 STD- B CAL·BLK .042686 .001479 08/21/08 12:5~:27 

Al 308.215 STD- A CAL-BI.d< :394283 -. 44&470 oa/21/08 12:52:27 

As 189.042 STD-A CAL· BLK .1.00398 . 003245 08/21/08 12:52:27 ,8 249.678 STO·A CJ\1,.· BJ.d{ .0493.88 ·- . 006022 08/21/08 12:52:27 

Ba 455.404 STD-A CAL· BLK .035069 -. 000549 08/21/08 12:52:27 

Be 313.042 STD-A CAL·BLK·. .00'7913 . 001223 08/21/08 12:52:27 

Bi 223,061 STO·A CAL-BI.d< .09~655 . 004508 08/21/08 12:52:27 

Ca 317.933 STO-A CAL-Bi.K .782405 -. 009384 08/21 /08 1:!:52 : 27 

Cd 226.502 STO-A CAL·BLK . 005756 - . 000119 OB/21/08 1 2:52:27 

co 228.6i.6 S'ID-A CAL· BLK .032357 .001854 08/21/08 12:52:27 

Cr 267.716 STD·A CAL- BI.d< . 088659. . 000798 08/21/08 12: 52:27 .. 

cu 324.753 STD· A CAL-BI.d< .042221 -. 019074 08/21/08 12:52 :27'. 

Pe 259 .9(0 STD·B CAL·BI.d< . 06322.8 -. oo2o85 · 08/21/08 ~2:5:1:27 

Fe 271.441 STD-A CAL-BLK 1 . 24137 . 021093 08/21/08 12:52:27 

K 766.4 91 knahi_lS CAL·BLK l. 02189 .141451 08/21/08 12:52i27 

Mg 279.078 STD-B CAL·BLK .24$704 -. 004912 08/21/08 12:52:27 

Mg 38·3 . 231 STP-A CAL·.BLK . 84.3829 . 011245 .08/-21/08 12 :52:27 

Mn 25'7.610 STD-A CAL-BLK . 0 488·33 -. 000033 08/21/08 '12:52:27 

Mo 202 . o·oo STD·B CAL·BLK . 0268$0' . 000036 08/21/08 12:52:21 

Na sas.99S kpahi_15 . CAL·BLK .941266 - 32 . 1543 08/21/08 12:52:27 

Ni 231.60( STD· A CAL·BLK . 04120'7 - . 000124 08/21 /08 12:52:27 ·p 178 .287 STD- B CI>,Io·BLK . . 2 75610 • . OJ.8510 08/21/08 12.:s2:n 

2203/1 22Q. 351 STO-A CJ\L-BLK . 023124 -.:oon\16. 08/21/08 2: ~2!27 

22o3 /2 22'0.352 STD-A CAL-BLK .043653 . 002749 08/21/08 ),2:52:27 

s 182.040 STO- ll CAL-BLI<; . 2464.89· - .068900. 08/21/08 12: 52:27 

sb 206.838 STO·B ·0\L· BLK . 103216 - . 000103 08/.21/08 12': 52:27 

1960/1 196.021 STO-A CAL- BLK .093928 . 00.5946 08/21/08 12: 52:27 

196'0/2 196.022 STD- A CAL·BLJ<i . 094014 - . 005137 08/21/08 f:a: 52:,27 

Si 251.612 sTb-s GAL- BLK .'071896 - . 006156 08/21/08 12:52:27 

Pb 220.35l liONE NONE . 0000.0.0 . 000000 *NOT STANDARDIZED 

Se 196.026 NONE NONE . 000000 . 000000 •NOT· STANDARDIZED · Sn 189.989 STD- 8 CAL· BLK .091702 . 001283 08/21 /08 12:52:27 

Sr 407.771 STD-A CAL·BLK . oo9352 -. 000486 08/21/08 12:52:27 

Ti 334.941 STP-B CAL- BLK . 006889 . 000071 OB/21/08 12:52:27 

Tl 190.864 STO-A CAL· BLK . 2057·10 . 014804 OB/21/08 12:52:27 

u 367.000 STD·A CAL-BLK 1.27980 - .026862 09/21/08 12:52:27 

v 292.402 STO·A CAL- BLK .084696 . 0001 69 08/21/08 12:52:27 

y 371.000 NONE NONE 1 .00000 . 000000 • NOT STANDARDIZED 

213Zn 213.856 STO- B CAL- BLK .101-430. . 000811 08/21/08 12:52:27 

Zn 206.200 STO-A CAL- BLK .019575 .000757 08/21/08 12:52:27 

zr 339.198 STO-B CAL·BLK .005790 .008015 08/21/08 1 2:52:27 

VES 005671 
Staridardi zation Rpt ·. 

Method: PSC34 Standard: ·knahi_lS 

Run Time: · OB/21/0B 12 : sa: 34 

Elem X Na 

Avge 23.00 3083 . 

Ill 23.00 3084. 

112 ~3. 18 3088. 

113 22.83 3076. 

08/21/08 01:02 : 26 PM 

7 

' !' 

' . { 

page l 

VES 005672 
Standard~zation Report 0!!/21/08 01:!)2:29 PM page 1 

Metho.d: •PSC34 Slope Conc(SIR)/IR 

Bl·ement Wa.vel~n High etd Low etd Slope Y·iricercept Date Standardized 

Ag 328.Qp8 STD-B CAL-BLK .042686 .001479 08/21/08 12:58:34 

Al 308.215 STD-A CAL-llLK .394283 - .4.48470 08/2!/08 12:58:34 

1\s 189.042 sio-A CAL-BLK .100398 . 003245. 08/21/08 12:58:34 

B 249.678 STD-A CAL-BLK . 049'388 -.006022 08/21/08 12:58:34 

Ba 455.404 !;TD-A CAL-BLK .0351)69 - .OOOS49 08/21/08 12;58:34 ' 

Be 313 .. 042 STD-A CAL-BLK . 007913 .001223 08/21/0P 12:58:34 

Bi 223.061 STD-A CAL-BLK . 096'655 . 004-508 08/21/08 12:58:34 

ca ~17.933 STD-A CIIL-BLK .782405 009384 08/21/08 12:58:34 ·cd 226.502 STD-A CAL-BLK .005756 - .000119 08/21/08 12:58:34 

Co 228.616 STD-A CAL-BLK .032357 .001854 ·08/21/08 12:58:34 

Cr 267.716 STD-A CAL-BLK .088659 .001)79!! 08/21/08 12:58:34 

cu 324.753 STD-A CAL-BLK .04 ~221 - . 019074 · oa/21/08 12:58r3~ 

Fe 259.940 STD- 8 CAL•BLK. .063228 - .002085 08/21/08 12:58:34 

Fe 27~.441 S'rD-A CAL-BL~ 1 . 24137 .o:nb93 08/~i/08 12:58:)4 .. K •711_6 . 491 knahi 15 CAL-Bl.K 1.o37n ·15.0SI.99 '08/21/08 l2:58:34 'Mg ·279. 07Q STO B-

:t~ ''245,704. -. O.Q49l;! 08/21/PB 12:58 :·34 .!-lg· 383 '.23 1 St,P-A .843829 .01124$ 08/21/08 12 : 58:34· Mn 257.6,10 STO.A CAL-BLK .048833' -.000033 08/21/08 '12:.8:34 

f'lo 202.QOO STD-8 CAL-BLK ; 026850. ' .. I)'QQ036. 08/:il/08 12:S8:34 .Na 588.995 l<nahi 15 CAL-BLK . 928835 -31 . 8733 08/'J;l./08' 1'2: 58:.34 

Ni 231 .604 s~-A- CAL-BLK ' . 041207 - . 000124 '08/21/.08 12:58:34 

p 1'78. 287 STD-8 CAL-BLK .275610 • . 078510 08/21/08 12 : 58.:34 

2·203/l 220.351 STD-A CAL-i3LK .023124 - . OP7,296 08 / 21/08 12:58:34 ~203/2 220.352 S,TD-A CAL"BL!< .0~3(153 . 00274!1 riV21/0~ 12:58:34 

s 182 :04Q STD-B CAL-BLK , 246489 - . 068900 08/21/08 12:58:34 

Sb 206.838 . STO-B CAL- BLK .103216 - .000103 08/21/08 12:56:34 

1960/1 196.021 STO-ll CAL-BI,K . 0!!3928 .005.946 08/21/08 2:58:3~ 

1!160/2 196.022 STO-A CAL-BLJC . 094014 -. 00"5137 '08/21/08 12: 58"': 34 

Si 2~1.612 STO-B CAL-BLK . 071896 - . 006156 08/21/08 12: 58:l<1 

Pb 220.35~ NONE NONE .000000 .QOOOOO *NOT STANDARDIZED 

Se 196.026 NONE NONE .000000 .000000 *NOT STANDARDIZBD 

sn 189.989 STO-ll CAL-BLK .091702 .001283 08/21/08 12:58 : 31 

Sr 407.771 STO- A CAL-BLK .009352 -.000486 . 08/21/08 12: 58:34 

Ti 334.941 STO-B CAL-BLK .006889 . 000071 08/21/08 12:58:34 

Tl 190.864 STO- A CAL-BLK .205?10 .014804 08/21/08 12:58: 34 

u 367.000 STO- A CAL-BLK 1. 279'8o -.026864 08/21/08 P:58:34 

v 292 . 402 STO-A CAL-BLK .084696 . . 000169 08/21/08 12:58: H 

y · 371.000 NONE NONE 1.00000 . 000900 . *NOT STANDARDIZBD 

213Zn 213.856 STD-B CAL-BLK .101430 . 000811 08/il/08 12:58 : 34 

Zn 206.200 STD-A CAL-BLK .019575 .000757 09/21/08 12:58:34 

Zr 339.198 ST0- 8 <;AL-BLK .005790 .008015 08/21/08 12 : 58:34 

VES 005673 
linalysi.s RepoJ:.t. 0.8/21/08 O:j-:10:21 . PM page .1. 

M~tho!i: / .PSC34 Sample Name : . I~ · Qp~J:ator: gbu 

Run Time: . 08/'21/08 . . . . 

co~ri,t, 

13:04:55. 

~de: . .cooc Corr. Factor: 1 

Elem Ag Al As B sa; ·Be Bi 

Units ppm ppm ppm. ppm ppm ppm ppm 

Avge .2580 1 ·.024 .a614 . 5079. . 51322 ~5554 .2656 

#1 .2619 l. 041 .. 2~8 8 . . 5109 .Si4~S . 25537 . 2725 

#2 .2576 . 1 . 023 .2570 · . 5091 . 51294· .255;4 . 266? 

#3 . . 25ol6 1·. o·o9 2!?8~ .503.7 . 51228 .25550 · : 2577 

Elem Ca Cc;l <;o Cr Cu Fe . K 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge .s·. 1o8 . 25488 .5119 ', 5092 .5065 6.136 · 5.029 

#1 5 . q3 . 25713 .5144 . 5132 . 5066 6. 221· 5 .. 031 . 

#2 5.101 -~5396 .sus . 5079 .5052 6 . il9. 5 . 025 

113 5 .091 : ;!5354: .so9& :so65 .S078 6 . 067 5.032 

E!em Mg r~n Mo Na Ni p 2203(1 . . 1Jnits, PJ?.!ll ppm PPIII ppm ppm . PPm ppm.• 

Avge ~.111 . 51349. .2.539 2.3~2 . . 2579 2. 540 .. 52~4 

#1 3.164 . 51472 .2519 t~~~ ·. 2596 2.571 . 5175 

#2 3 . llQ . 5.P13 :2544 . 2580 2.515 .5381 

fl.3 3 . 060 . 51261 . 2552 2 .378 . 2561 · 2.!;i34 . 5325 

2203/2 1~60/l 1960/2. ) Elem s Sb Si Pb 

Units • .·PPm ppm ppm ppm ppm ppm ppm 

.Avge .5023 1 . 007 2~43 . 2796 .!!427 .4514 . 5113 

Ill .5023 1 .007 .2528 . 2?:17 . 2442 .4579 .5074 

#2 . 5008 1. 008 .2704 . 2781 . 2351 L. 4.481 . 5132 

#3 . 5038 1. 006 .2697 . 2890 .2487 L. 4482 .5134 

Blem se Sn sr Tt . Tl u v 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge .2550· . 51'46 .25661 . 50921 . 5157 2 . 648 . 2526 

Ill .2534 . 5154 . 25682 . 51061 . 5210 2 .821 . 2555 

#2 .2494 .5153 . 25670 : 50934 . 5098 2 . 643 .2520 

#3 .. 262:j. . 5133 . 25631 . 50768 .5163 2 . 480 . .2503 

Elem y al3Zn zn Zr .. :Units ppm ppm ' ppm ppm Avge. 39.;.51 1 :25·9 1.274 . 5(!47 

#1 38. 49 1.257 1.27.7 . 5080 

#2 38.51 i.258 1.273 . 5044 

#3 38.51 1 . 258 1.272 .5016 

VES 005674 
Analysi$ Rep.ort 

Method i · PSC34 

Run Ti~; OQ/21/08 

Comment: . Mode i coN· ..• , . co rr. 

El em · Unit 

Avge 

#1 

#2 

#3 

. Elem 

Units 

AVge 

. #1 

#2 

#3 

Elem 

Units 

Ayge 

#.1 

#2 

#3 

Elem 

Units 

Avge 

#1 

112 

113. 

Blem 

Units 

Avg.e 

Ill 

#2 . 

#3 

·"i 

.H. 0074 

- . 0049 

H.004'7 

Ca 

ppm 

.0050 

.0104 

.OOll 

.0035 

Mg 

ppm 

012~ 

H.0278 

-· .. 0063 

.. 0148 

2203/2 · 

ppm 

.0067 

.\)073 

.0136 

-.0007 

Se 

ppm 

.. -. 0037 

- . 0049 

- . 0011 

- . 0051 

Elem Y 

Units ppm · Avge 38 , 1·9 

Ill 38.29 

#2 ~8.00 

#3 38.27 

Samp~e Nam~ : ICB 

13:1+;37'. 

Al 

ppm. '~ .014 7 : 

.0324 

-. 0065 

.018:1: 

Cd )}.·. 

ppm ~ . 00054 

.001f6 

'* 

-,00119 

. 00154 

Mn -~ .... 

p pm ,.. 

. 000.31 

,. 000~~ 

- . 00064 

.00062 

s 

ppm 

- ' 0027 

.0043 

- . 0145 

. 0021 

Sn 

ppm 

. 0058 

H. Ol27 

- :0033 

.0062 

213zn 

ppm .• . 0011; 

.0!)20 

. 0004 

. 0008 

H.0124 

-.0092 

.0092 

co 

ppm 

. 0017 

.0041 

. Ojl16 

. 0026 

Mo 

ppm . 0025 

H. 00"6i 

-:ooo·e . 0019 I 

Sb 

ppm 

H.0179 

a.o:i63 

-.0080 

H.0255 

Sr 

ppm 

. 00010 

.00024 

-.00003 

.00007 

Zn 

ppm 

. 00:1.4 

.0029 

- .0003 

. 0015 

.. ... 

; f " . . ' 

08/21/0B. 01:17:06 PM page 1 

Operator: gbu 

B 

ppm 

.002·7. 

. . 0060 

-:oo37 

. 0057 

~··'Y":'·-" 

Ba 

: .PPm ,, ·'·;·ooo51 

~ 00106 

::09001 

.00047 

Cr · ppm· 

. 002 6 

.· .. · -cu 

\•'ppm 

"\· -.0001 ''f:, H . 0071 :: ..• 0019 

, . oo36 . A f ,9o1 1 

H . 005Q · ,·.0032 

Na 

ppm 

. 0045 

.0.103 

- .0036 

. 0066 

1960/l . 

ppm 

- .0071 

.0028 

• . 0241 

c . 00.01 

Ti · ppi!l 

. 00075 

H.00177 

- .00032 

.00081 

~r 

ppm 

: oo12 

H.0030 

-. 0008 

. 0016 

. . •.-> 

~ ., 

.. Ni 

ppm 

.0008 

:: ~~~!3 • 0021 ' 

1960/2 

.PPm 

- . 0020 

- . 0087· 

. 0104 

- . 0076 

Tl 

ppm 

.0046 

·.0148 

. . 0031 

.0022 

· Be 

ppm 

- .·00001 

.00015 

· . OQ018 . 

.00000 

Fe 

ppm 

.0040 

.0075 

.0010 

.0035 

p 

ppm 

.0084 

:Q099 

.qo5o 

.0105 

Si 

ppm 

. 0027 

H . 0102 

- .0059 

. 0039 

u 

ppm 

.1398 

.3824 

- .2597 

.2967 

Bi 

ppm 

. 0,03 6 

H . 0214 

- , o25o 

. 0143 

K 

ppm 

-. 0003 

. 0483 

.. 1012 

. 0521 

2203/1 

ppm 

-.0112 

- . Q080 

- . 0303 

. 0046 . 

PI;> 

ppm 

.0007 

.0022 

-. 001 0 

.0011 

v 

ppm 

.0036 

.0063 

.0009 

. 0036 

----------•. -:- . ------- ----- ·-· · ... 

VES 005675 
.. . . . 

Analysis Report 08/,21 /()8 01:25 : 47 PM. page .1 

Method: PSC34. Sample Name: ICVAX / Operator: .gb':J 

Run Tillie": . 08/21/08 13,20:21 

Co""""nt .: 

Mode: CON!= Co)."r. FactOr: 1 

.El.em Ag Al As B sa l!j3• Bi Un ts PPm ppm PPIJ.I PPJll ppm ppm ppm 

AVg.e . .2-524 1 . 027 . 2554 .5041. .512a9 .25564 . 24'75 

Ill : ~~~~ . 1.017 .2543 . 502l . 5125.6 . 25544 .2455 

112 1 . 048 .2621 .!?075 :.5:J.203 .2560.8 .2502· 113 .2517 1 .. 016 . 2498 . 50.27 . 51200 .25540 . 2467 

Elem · C.iil Cd Co . . Or Cu l'e . . K 

Ul)i'ts ppm ppm ppm ppm. ppm ppm ppm . · Avge 5.102 . . 25273 \5097 . 5033 .5Q59 6.130 4.922 

Ill 5 . 097 • 25l48 • 5094 .5Q08 • 51"00 6, 097 4 . 837 . 

112 5.108 . 25409 .5126· .. 5057 .5079 6.134 4.937.· 

{t3 5 . 103 . 25261 . 5072 .5034 .4_g98 . 6.158 4. 992 . 

Elem Mg Mn . Mo Na Ni p 2203/1 

·units ppm ppm ppm . ppm ppm ppm ppm 

Avge 3 , 033 .51273 .2535 2.378 . 2540 2.539 , 4991 

ltl 2 .994· ·. 51263 .2497 2. 367 .2537 2.53'1 .496Q 

112 3 . 092 . 5l323 . 2553 . 2.388 . 25"51 2,530 . 5128 · 

·#3 3 :o12 .51233 . 2556 2.37~ . 2531 2.554 .4884 

Elem 2203/2 ·s Sb 1960/-1 196.0/2 Si Pb 

Units ppm ppm ppm ppm ppm ppm ppm ." 

Avg!' .5144 1.010 .2504 .2457 .2583 .4539 .5093 

. . 111. .5131 . 9936 . 2252 .2400 . 2581 .4521 . 5074 

#2 .5!)55 1 .023 . 2758 .2566 .2546 .4546 . 5080 

#3 . 5247 1. 0i4 . 2501 .2404 .2621 .4549 . 5126 

Elem se Sn Sr Ti -Tl u v 

Units ppm ."ppm ppm ppm ppm ppm ppm 

Avge . . 2541 . 5077 •. 25569 . 50763 .5167 2.429 .2517 

#1 . 2521 . 5024 . 25645 . .5!)784 . 5185 2.256 .2516 

#2 .2553 .5132 . 25522 . 50786 . 5213 2 .643 .2518 

#3 . 2548 .5073 • 25541 ,50719 . 5104 2.389 .2517 

Elem y 21 3Zn zn Zr 

Unit's ppm ppm ppm ppm 

Avge 38 . '79 1.256 1 . 267 .5030 

#1 38.75 1 . 258 1 .265 . 5037 

#2 38.86 1 . 256 1 . 272 .5044 "113. 38.77 1. 254 1.264 .5009 

VES 005676 
Analysis. Report 

Method:. PSC3 4 

Run Time: 08/21/08 

S,ample ~me : ICB 

13:27:0.3 

Comment: 

Mode: ~c Corr. Factor: 1 

Elem 

Unit 

Avge . 

#1 

~~~ 

#3 

Elem 

··units 

'·Avge 

#1 

112 

#3 

Elem 

Units 

A.vge 

·#1 

112 

113 

Elem 

Units 

Avge 

Ill 

112 

113 

Elem 

Units· 

Avge 

#1 

ll2 

#3 

9 . 0012 . 

H. 0031 

.Ca 

ppm . . .. 003~ 

. 0045 

. 0046 

. 0014 

Hg 

ppm 

.0026 

- . 0037 

.0004 

. 0112 

'2203/2 

ppm 

.0049 

.0022 

.0112 

. 0013 

se 

ppm 

. - .0010 

- .0008 

- .0031 

.0008 

Elem Y 

Units ppm 

Avge 37.78 

·#1 3'7.76 

#2 37 .79 

~3 37 . 78 

Al 

pp.m 

.0074 

.0046 

-. 0 100 

.027S 

Cd 

. ppm 

.. 000?5 

, 09082 

:.00.027 

. 000.57 

Mn 

ppm 

.00033 

.00049 

.00.030 . 00020 

s 

ppm 

·. - , 0001 

. 0028 

-. 0014 

- . 0016 

Sn 

'Ppm 

. 0042 

.0058 

. 0021 

.0046 

213Zn 

ppm 

.0098 

. 0013 

. 0005 

.0007 

As 

. PP'!I: ·. ooss 

.00 07 

,0037 H·: 0 121' 

Co 

pp'm 

.. 0:010 

. 0009 - . 0'0 1 0 

. 0030 

Mo 

ppm 

.00 15 

. ooo.s· • 0018 

. 0021 

Sb 

ppm · 

H. Ol36 

..._.....,1 

- . 0038 

H.0236 . 

Sr 

ppm 

. 00004 

. OOQ09 

- .00004 

. 0 0007 

Zn 

ppm 

.0011 

. OOl.l 

-.0002 

.0023 

08/:21/08 . 01:32:30 . PM 

B 

ppm 

.'0022 

.0035 

.0008 

.0021 

Cr 

ppm 

, OO'l6 

.6045 

. 0010. 

.Q022 

Na 

ppm 

.0036 

. 0039 

- .0002 

.0070 

1960/l . 

ppm . .0009 

.0077 

-.0166 

.0116 

Ti 

ppm 

. 00024 

.00037 

- . 00062 

. OOO liS 

Zr 

ppm · . 000,4 

. 0004 

- : 0013 

H . 0020 

. Operator: gbu 

A9/ SL 

Ba 

ppm 

. 00029 

. 0.004'0 

.00036 

. 0.0012 

Cu 

ppm 

-.0040 

L- , 0061-· 

- . ()035 

- . 0024 

Ni 

ppm 

.00,08 

.0012 

- . 0008· . . 0.019 

1960/2. 

ppm 

-. 0020 

- . 0050 

. 0037 

-. 0047 

Tl 

ppm 

- . 0014 

.Q018 

0070 

. 0008 

Be 

ppm . · - . O.Q01 9 

- .00018 

- . QoP;J.S - . 00025 

Fe 

ppm 

. 0035 

.0050 

.0035 . 

.OQi~ 

p 

ppm 

. 0065 

.0052 

. 0036 

. 0;1.07 

Si 

ppm 

. 0017 

. 0010 

. 0 035 

. 0006 

u 

ppm 

.1228 

.'1663 

. 0499 

. 1522 

page 1 

Bi 

ppm 

.0036 

. 0102 

. 0023 

- . 0017 

K 

ppm . .0586 

.0~28•. 

.0809 

.0122 . 

2203/1 

ppm 

- .·0036 

.0061 

- . 0183 

. 0014 

Pb 

ppm 

·.092 1' 

• 0035 

.0014 

.0013 

v· 

ppm 

.0023 

. 0015 · 

. 0035 

• 0021 

VES 005677 
Standardi zation ,Rpt, 08/2'3:/.08 0 1 :35:52 PM page . 1 

M~thod : p'sC34 Standard : CAL-BLK 

Run ·Tirne: OB/21/0B 13:33:24 

El em Ag Sb ,Avge . 1049 "1952 

' Ill . 07l:O . 1209 

#2 .0710 .·1699 . 

113 . 1729 . 29<t9 

! 

:• 

•, 

VES 005678 
Standardization 

Method : ·PSC34· 

Element ·wavelen : 

J>,g 328.068 

Sb . 20~. 838. 

Report 08/21/0S·.Olt·35:57· PM . . . . . . . . . P'!-9e 1 

. 'slope s Cone (SIR) /IR 

High atd 

s:ro-s 

STD-B 

Low· atd 

CAL-i!Li<. 

CAL-BLK 

Slope 

.043198 

.107~67; 

'!-intercept -. 004534 -. 021001. 

' . 

Date Standardized 

08/21/08 01:33:24 08/2 /~8 01:33: 24 

VES 005679 
Analysis Report 

Method: PSC34 

Ruri' ·Ti me : 08/21 /08 

Cq~ent: 

Mode: CONC C~rr. 

Sarople Name : . ICVAX 

13 :37:14 

Factor: 1 I' 

:7 t,v,/J. '~''~"' vv.Y 

Elem Al As 

Units 

AVge 

J>.g 

ppm 

.2497 . . Hl.313 .· .25'77 . ppm 1 ppm 

#1 

#2 

#3 

Elem 

Units 

Ayge 

Ill 

#2 

#3 

Elem 

.units 

Avge 

#1 

#2 

#3 

Elem 

Units 

,Avge 

Ill 

112 

113 

Elem 

units 

Avge 

Ill 

112 

#3 

Elem 

Units 

· Avge 

#1 

# 2 

#3 

. 2502 ' . 24'29 

.·2559 

Ca 

ppm 

'5. 085 

5 . 07Q s,o69 

5.108 

Mg 

.. ppm 

3.052 

3 . 045 . 2 . 963 

3 . '1.48 

2203/2 . ppm 

. 5073 

. 5'077 

. 5261 

.4880 

Se 

ppm 

. 2600 

. 2619 

. 2662 

.2519 

y 

ppm 

38 . 19 

38 . 23 

38.13 

38.21 

1. 039 • 2574 

Hl'. 432~j • 243'9 

H1. 468 . 2720 

C<;l 

ppm 

.. 25276 

. 25208 

. 24.920 

• 257 0.0 

Mn 

ppm 

.51095 

.5102 2 . 50922 

.5134'1 

s 

ppm 

1.00~ 

1.008 

. 9975 

1.001 

Sn 

ppm 

.5048 

• 5014 

.4955 

• 5174 

213Zn 

ppm 

l.2SO 

1.248 

1.247 

1.255 

Co 

ppm 

,!;066 

.5049 

.5029 

.s121· 

Mo 

ppm 

.2504 

.2·456 

,2503 

. 2553 

Sb 

PPm 

.2505 

. 2291 

. ;!314 

. 2910 

Sr 

ppm 

.25583 

.25562 

.25600 

.25588 

Zn 

ppm 

1.258 

1. 255 

1. 251 

1. 2:68 

.. 08/21/08 ·01 :4.2:41 PM . 

/. Ope;rator: gbu 

B 

ppm 

·.5004 

.4987 

.4 929 

.5096 

Cr 

ppm 

.5020 

.4982 

:198? 

.5095 

Na 

ppm 

2 . 377 

2 . 37ti 

2 . 36A 

2.392 

19 .. 60./'1 

ppm 

.2.649 

.2567 

.2454 . 2927 

Ti 

ppm 

.50S69 

. 50463 

. 504 52 . 50'191 

Zr 

ppm 

.5010 

; soos 

. 4991 

. 5033 

Ba 

ppm 

. Sl OSS 

. 51116 

.' 5'i070 

. 50979 

Cu 

ppm 

.5043 

.5005 

'SP5'1, 

. SO?J. 

Ni 

ppm 

. 5~3 

.· ;!S28 

. 2512' 

.2588 

1!)60/2 

ppm 

.257 5 

.2645 

.2766 

.2315 

Tl 

ppm 

.5064 

. 5002 

.4891 .S298 

se 

ppm. . 25601 

.25544 

.25564 .2569.4 

Fe 

ppm 

6 . 097 

6 . 126 

6 . 049 

6 . 116 

p 

ppm 

2 . 514 

2 .. 511 

2 . 5p 

2 . 513 

S.i 

ppm 

.4511 

. 4509 

L.4497 

.4528 

u 

ppm 

2.467 

2 . 457 

2.204 

2 . 801 

page 1 

Bi : . 

ppm 

.2458 

.242!il 

.2269 

.2676 

K 

ppm· 4.!)78 

' 

5.008 

4 . 922 . 5.003. 

2203/1 

ppm 

. 50.6Q 

. 5003 

· 4.854 . 5324 

Pb 

ppm 

. 5069 

.5052 

.5125 

.5028 

v 

ppm 

.2512 

. . 25 02 

.2512 

.252 2 

VES 005680 
•l\\'C ·. ~~.l·' 

··r }~' ,, ' V.•l 

;or ! ·~::1~ Analysis R~port O.S/21/08 01:4'9:22 .PM :1€ page l 

'7 

Mel; hod: PSC34 ' Sample Name: ICB ·.:. Operator: gqu ;,<;;· . 

Run Time : 08/21/08 13:43 :56 i~ ·{;::· 

Comment: -~ ·~:.: 

. Mode : CONC Co=. Factor: l '·: . ~~ · r·· 

Elem ·GfuJ Al As B Ba Be Bi .U!"its · ppm PP!tl ppm ppm 1 ppm ppm ,;/·ppm 

Avge L· .00 1 .0180 - . 0016 . 0000. - . 00005 • . 009.34 " ' .0006 

#.1 L-. 0059 • 00.07 - . 0023 .. 0009 . 001)01 -.00028 ik: ll063 

#2 -.0032 . 0543. . 0021 . 0036 - .000,17. -.000:}6 i•, • QllO #3 L-.0093 - ."01)10 - . 0047 :oo~6 .00001 - .00038 ·- .0156 

Elem ca Cd Co .Cr cu F.e :-f ·, 

·J,Jnits ppm ppm ppm ppm ·:~: ppm ppm ·VJlPIII 

Avge .0003 .. 0002!i .. 0002 . 0006 - . 0002 .0018 . ;li;;., • 0 0 91 

· ~:f~$~ 

Il l . 0000 .00012 -.0010 . 0008. .0013 .0032 . 1ll94 112 . 0005 .00055 .0046 . 00,38, . -.0008 .00~6 ~'.0529 

113 . Q002 . 00006. .,6029 -.0027 . -.0009 .0008 ~~0064 

i• 1'(t'X:. ··~· •.Y , Elem Mg Mn Mo Na Ni p . '2203/l 

Units PJ?III ppm PJ?III ppm ' ppm ppm 'i ppm, 

Avge - .. 0026 . 00003 .0005 .0025 :ooo1 . 007.3 ' - . Q024 ., 

Ill ~ .. 0140 . OO,Ql2 .0026 .. 0007,. . 0000 ,0105 ··.-'.0036 . 

112 H.0267 • 00034 . - . 0014 . 0!05 . 0011. 0~68 '' :.'OlJl 

il3 L· .·0205 - .OP036 . 0003 • .OQ36 - .0007 - .0052 -·. 0166 

Elem 2203{2 s Sb ) 196~( 1 1960/'2 Si · .. Pb 

Unit s ppm , ppm PJ?III ppm ppm ppm ppm 

Avge .OQ16 · .0062 L-. 0219 .0051 - . 0034 • . 0044 -:0003 . 

¥ ~ ~ 

Ill . 0029 · .0073 x; 3 . 0052 · .0023 -.0039 . ; 0007 

112 • . 0055 • . 0048 • . 0061 . 0161 .. 0132 - .0048 .0007 

.113 .0074 · .0066 L· . 0352 · . 0059 . 0055 -.0046 - .0006 

Elem Se Sn Sr Ti Tl u v 

Units ppm ·ppm PJ?III ppm ppm ppm : ppm 

Avge - .0005 . 0013 .00003 .00006 .0021 . 005S ·.0002 

Ill .0002 .0006 . 00003 - :00052 - .0053 - .0090 - .0016 . 

H2 - .0034 .0031 . 00018 H.00183 H.Ol79 .1765 .0005 

113 . 0017 .0000 ·.00010 .. 00115 • . 0062 - .1509 .0005 

Elem 'f· 213Zn zn Zr .;}<t· 

Units ppm ppm ppm ppm < if~ Avge 37.64 . 0,007 .oooi; · .0001 ,:;;. 

Ill 37.71 . 0012' .0004 - .0008 

112 31.71 . 0005 . 0023 H. 002? 

113 37.50 .0003 -. 0008 L· . oo;n . . 

' .·~~

•

' : . 

' •'<>~~ 

....• .. 

VES 005681 
. -. ' . 

Standardization Rpt. 08/21/08 01 : 53 :18. PM . · Pag'e 1 

Method·: PSC34 . St andard: CAL-BL~ 

Run -Time : 08/21/08 11.: so: 49 

/ 

Elem· Ag . ®b "-. <J '"") 

Avge ·. 0830 . 182_2 _r c 

#1 .0.610 ; l 9 

#2 .1399 . 2869 

#3 .0480 . 0730 

VES 005682 
I 

Standardization Rpt . 08/21/0~ Ot;57:38 PM ·.page 1 

l~ethod: PSC34 . Standard: CAL- BLK 

'Run Ti me: 08/21/08 13:55:10. 

Elein 1\g . Sb 

Avge . 0640 . 0126 • ' ' . 

#1 . 0270 - ·.·0590 

#2 .O!l80 •. 1329 

113 .0670 .1439 

eve wAtflt7J · 

&" 

.::; . 

/ '-: 

VES 005683 
Standardization 

.Method : PSC34 

Element 

Ag 

Sb 

Wave len 

328 . 068 

20"6 . 838 

Report 

Slope ~ Cone (SIR) /IR -1:, 

-High std 

STD·B 

STD-B 

. . 

Low std CAL~~LK 

CAL· BLK 

< "" · sl ope : interce t 

. 043046 c. 0027S4 .104779_, ,_ . 007~10 

... 

< . 

----------- - - - ·····- -· 

page l 

Date Standardized 

08/21/08 01:55:10 . 

08/2i/.08 01:55:10 

VES 005684 
Analysis Report 

!'let hod: PSC34 

Run Tine: 08/21/08 

Sample ~ame: ICVAX 

13;58:40 

C!'rrrnent; 

Mode: CO.!o!C Corr. Factof: 1 

-

1

' \ I CAlc~<. f~ AIOIJ Blem 

Units 

Avge . 

ill 

#2 

113 

Elem 

Units 

Avge 

#1 

112 

#3 

Elem 

UnJtp 

Avge . 

Ill 

#12 

#1 3 

Elem. 

Units 

.Aovge 

Ill . #2 

#3 

!Hem 

Units 

Avge 

Ill 

112 

113 

Blem 

· Units 

Avge 

Ill 

112 

#3 

·Ag 

ppm 

.2505 

.2532 

. 2480 

:2502 

ca 

ppm 

5.140 

5.130 

5.154 

5.135 

. Mg 

ppm 

3.o5p 

3.071 

:) . 024, ).056 

·2203/2' 

ppm 

.5185 

.5084 

.5378 

.5094 

Se 

ppm 

.2562 

.2541 

.2598 

.2546 

y 

ppm 

38.64 

38 .56' 

38.75 

38.61 

A \ As 8 

{ Hi~~s9} ~rs'53 ~ro42 

~ . 2554 . 5075 

Hl . 135 : 251~ . 5035 

Hl. 602 . 2591 . 5016 

Cd 

ppm 

. 25598 

.25641 

.25769 

:25385 

Mh 

ppm . . 51589 

• 515,0.4 . 

. 5179~ 

. 514 7'0 

s · 

ppm 

l.OU 

1.029 

. 9998 

1.005 

Sn 

ppm 

.5109 

.5121 

.5082 

. 5124 

213Zn 

ppm 

1. 261 

1.260 

1.267 

1.255 

Co 

ppm 

.5142 

.5135 

• 51'74 

.5116 

Mo 

ppm 

, 2551 

.2536 

.2_564. .2554 

Sb 

ppm 

. 2575 

.2385 

.2582 

.2757 

Sr 

ppm 

. 25611 

.25545 

.25125 

.25564 

Zn 

ppm 

1. 280 

1·.281 

1.284 

1.276 

c:r 

ppm 

,5070 

.5080 

. 5059 

. 506.9 

Na 

ppm 

2.4Q3 

2.395 

2.4Qi! 

2.405· 

1~60/. l 

ppm 

.2626 

.2789 

.2500 

.2587 

Ti 

ppm 

.50957 

.50823 

.51246 

.50801 

Zr 

ppm 

.5047 

.5043 

.5070 

.5029 

-'r~~ >9Jti 

~-. 1+;} ·~< 

~' page 1 

~era tor: gb~ 

,•rcu 'l:.~l>Pm i\:::::- ~·' . . 

l2 ' --: 5062 

.-:~ i 

;,;:.ppm 

.;¢; 2575 ... 

r;~ .. .J~ . 2 5'·96 

*; : 2567 

< · : 2·s.li3 

,:~, 1·960/2 . ppm . 

.2530 

. 2418 

.2646 

. 2525 

Tl 

ppm 

. 5269· 

• . 5170 

.'5355 

.5281 

: ~-

,· . ·

Be 

ppm 

.25846 

.25833 

.25957 

.25749 

Fe 

ppm . 6.140 

6 .124 

6 .158 

6. 139 

p 

ppm 

2.55!i 

2.544 

2.576 

2. 546 

Si 

ppm 

.4555 

.4520 

. 4604 

.4541 

u 

ppm 

2.510 

2 .. 634 

2.335 

2.560 

: 

~· .... ~ 

Bi ... ppm 

.2506 

' :2556 

,24~7 

.2496 

K • 

ppm ¥ ~ . 94 1 

~} ': ·, 

:;,. ·5. 035 

-,;..-'! -800 

f. 4 .988 

-220:3/1 

ppm 

.•5180 . 

·:·5'361 

.49'15 .. 

.5204 

P.b 

ppm _ 

.5~84 

.5177 

.5244 

.5131 

v 

ppm 

.254 6 

.2533 

.2563 

.2542 

.. 

VES 005685 
Analysi s Report 

Method : .PSC3 4 

Run ·Tirne ! 08/21/08 

Sample Name.: ICB 

14 :QS:27 

Comment; 

od~: OONC Corr. Fa ctor: 1 . 

11:1~!11 

.Units 

Avge 

#1 

112 

113 

. Elem 

Units 

Avge 

E.l.em 

Units 

Avge 

Ill · H2 

113 

·Elem 

Un.its 

Avge 

# 1 

112 

#.3 

Elem 

Uni ts 

Avge 

Ill 

112 

113 

Elem 

Unit; a 

Avge 

# 1 

#2 

113 

Ag 

ppm 

·- . OQ34 

L- . . OOS!l 

- . 00?8 - . 0023 

Ca 

ppm 

· . . 0012 

. :0001 

· :oo3o 

. 0006 

Mg 

ppm 

- , 001!1 

- . OQ.95 - . 0079 . 0131 

2403/2 

ppm 

-.()015 

. 0008 

-.0010 

- . 0043 

Se 

ppm 

-.0035 

- •. 0046 -·. 0030 - . 0029 

y 

ppm 

38 .. 06 

38.05 

38. 10 

3.8 .04 

· . Al 

ppm 

.oo8o 

~ .·.0049 . .o<p'9 . 

. 0250 

Cd. 

PPI1l 

: 00024 

.-.00004 

. 00037 

. 00039 

Mn 

ppm . 000()8 . 

. 00002 . . 0001-5 

. 00()05 

,s 

ppm . OQ35 

- .. 0063 . 0151 

: 0018 

Sn 

ppm 

. 0045 

. 0029 

. 0037 

. 0068 

213Zn 

ppin 

. 0005 

• 0095 

. ·ooo6 

. 0004 

As . 

PPf!l 

.0017 

.0010 

• 0012' 

.0028 

co 

J;>pm 

.0010 ·

. 0004 

.0003 

.0023 

Mo 

ppm - ·• OQ16 

7.~1n5 

- :0013 

- .002'1. 

Sb 

ppm 

-,0026 

- . 0027· - . 0017 - .Ob34 

Sr 

. ppm 

.00005 

,00007 

.00000' 

.00007 

Zn 

ppm . . OOQ6 

.0006 

. 0003 

.0008 

08/21/..08 07:10: 54 PM 

B 

ppm 

. 000.6 

·-. 0003 . 6o-o6 

.0016· 

Cr 

ppm 

. Q009 

-,0003 

. 0020 . 

. 90:1,1' 

Na 

ppm 

, oo49 

• 0025 

.00,30 . .OQ92 

1960/.l 

ppm 

. 00'75· 

. 0111 . 0017 

.0098 

Ti 

ppm 

. 00031 

.00015 

.00007 

. 00071 

Zr 

ppm. .0003 

- . 0001 - . 0006 . 0015 

Opera~:or.: gbu 

Ba 

ppm 

- . 00001 

-. 0.0013 

' 0001'9 - . 00009 

.' cu . 

··: ppm ~·. -. 0011 

. ,: -. 0015 

'< ' -.0001 

.. . -. 0017 

Ni: 

ppm 

.. 0001 

- . oon· . . 0!)02 

. 0014 .· 

19.60/2 

ppm 

- .0090 

- .0125 

- .0053 

- . 00!13 

Tl 

ppm 

.0016 

. 0021 ' 

- . 0012 

.0041 

Be 

ppm 

- .. 00035 

- .00036 

-.0003.7 

- . 000·34 

Fe 

ppm 

:oo;i-7 

.OQ20 · .0021 

.•. 000~ 

p 

ppm 

.0051 

. ()041 

.0014 

. 0099 

S,i 

.ppm 

-·.0()19 

- . 0052 

.0019 

·:. 0026 

u 

ppm . . 0550 

- .0499 

.0882 

. 1266 

_____________________ ... -- .. - ·· 

page 1 

B1 

ppm 

. 0022 

- . 0079 

. 0.02 9 . OllG 

K 

PPll). •• OOOJ. 

-. 00 46 . 0496. 

~. 04'54 

2203/1 

ppm 

• QOlO . . 

-.0007 . - .0021 . . 0058 

Pb 

ppm 

- . 0007 

. 0003 

- . 0014 

-.. 0009 

y 

ppm 

.'0001 

- . 0009 

.0004 

. 0009 

VES 005686 
Analysis Report 08/21/08 02 :16: 24 PM . page l 

Method: PSC34 Sample Name: .CRI Op~rator: gbu 

Run Time : 08/21/08 14:10:57 

Comment: Tt'f ~"ll) Mode: CONC corr. Factor: ' 1 

Elem Ag -·;\ Al As B Ba Be Bi ··units ppm ppm ppm ppm ppm ppm PP.Ill 

Avge . 0060 ' . 1127 . 0515 .0457 . 00497 . .00467 .. 0723 

#1 L:0042 . 0995 . 0499 . 0449 . 00509 .00473 . 0648 

#2 . 0092 H.l398 . 0549 . 0.85 . 00470 .·00460 :086.7 

11 3 L: 0046 . . 0988 . 0497 . 0438 . OOS13 · :oo<t68 . . Q655 

El,em .Ca .Cd Co C+ Cu Fe K 

. Unite ,ppm ppm ppm ppm ppm ppm . ppm 

Av.ge ,152?' .01031 .01.11 . 0102 .0082 10~1! .'2190 

.. Ill .1539 . 00995 .0106 . 009.2 .OQ88 . 1052 .2221· 

112 . i505 . Oll31 ·H. 0141 . 0122 .0072. .1028 . 1982 

#3 . 1531 . 009.65 .. .ooas . 0092 .ooas .l.Ol4 . 23.6'1 

Elem Mg· Mn Mo Na Ni. p 2203/1 

Units ppm ppm ppm PPm ppm ppm pPm 

Avge . . 0805 . 00509, . 0137 ,2340 .0145· . .1556 . 0476 

Ill . 0701· .00493 ,ope . 2316 · .0133 . 1573 . 0356 

#2 H.1043 .00545 .0120 .2425 .0174 .1609 . 071~ 

#3 .0.670 . 0048'8 . 0153 .2277 . 0127 .1488 .0352 

Blem 2203/.2 s Sb 19.60/1 1960/2 Si Pb 

Units ppm ppm ppm ppm ppm ppm . ppl'n . 

Avge .0590 .1576 .Q370 :0506 . 0435 .0445 . 055 2 

#1 . 0612 .1622 L. 0200 .0471 .0597 .0461 . 0527' 

#2 .0472 . 1627 .0564 . 0651 .0233 .0403 . 0554 

#3 . 0686 .147.9 L.0347 . 0397 .0473 . 0469 . 0575 

Elem Se Sn Sr Ti Tl u v 

U!'>its. ppm. ppm ppm ppm ppm ppm ppm 

Avge . 0458 . 0504 -90507 . 0053.0 . 0'794 . 2164 .0157 

. #1 .0555 . 0500 .00501 .00481 . 0739 .1·222 . 0171 

#2 .0372 . 0534 .00522 H.00662 .0909 .3588 .0143 

#3 .0448 . 0478 .00499 .00448 . 0733 .1683 . 0157 

Elem 'i 213Zn Zn Zr .Units ppm ppm ppm ppm 

Avge 38.31 .. 0257 .0265 .0085 

Ill 38.36 . 0256 . 0258 · .0074 

#2 38. 32 . 0256 .0281 !1. 0112 .#3 38 . 25 .0259 .0256 .0068 

VES 005687 
' 

Analysis .Report Q8/2l/08 02:21:53 PM page 1 

Method: PSC34 Sample Name: IGSABAX /.• Operat<:>r: gbu ·Run Time: 08/Zl/08 14:16 : 27 

Coll1llent: 

Mode.: p:>NC Corr. Pact,or: 1 .. Elem Jig Al As B Ba 8!10 Bi 

Units ppm ppm ppm· p~ ppm ppm· ppm 

Avge . 2000 143 .2 .191!2 -. 0012 .09957 .10017. .0067· 

#1 .2005 143.5 .1981 - .0004 .10908 .1006() -.00~4 

#2 20~~ 143.4 . 2019 - .0004 .. 0997\) .190~5 .0246 

1!3 . 1 982 142.8 ;1940 - . 0026 .09893 . 0997.4 . -.0029 

Elem ca Cd C,R Cr cu Fe. K 

. Unit.s ppm .ppm ppm ppm: Pl?m ppm ppm 

J\\lge '236,0 .-19l.9Q .1007 . 1001 . 0952 . 9'6 . 79 - ,0071 

Ill 23·6 . 9 ' 19289. .099-8 . 1008 .09,52 97, 07 .0005 

#2 236 . 4 ·.19187 : roo9 . ,lOU .0943 96.95 .0387 · 

#3 234. T .;19095 .1015 . 098-l .0960 96;35 - . 0'604' 

Elem 11g Mn Mo Na Ni· P . 220.3/1 

Units ·PPM ppm ppm. .PpM . ppm ppm ppm 

Avge 246 . 0 . 10347 - . 0001 : 0047 .1921 01~9 . .2093 

Ill 246 .5 . ],03'85 . .0027 .0.032 .1941 .0149 . .198( . 

#2 246.0 .10370 -.000~ . 0051; .1922 .0105 . .2075. 

#3 245.4 . l028a -.0026 . .0054 .1900 .0077 .2218 

Ell em 2203/2 s Sb 1960/1· 196()/2 Si' Pb 

units ·ppm ppm ppm ppm ppm ppm ppm 

· Avg e . 1881 .. 0 181 . 2012 . 1861 .1959 .0031 .1952 

Ill .1918 .0239 .1869 . 177:6 .1945 .0037 .1941 

#2 . 18.99 . 0217 . 2103 .1818 . 2011 . 0077 .1957 

#3 . 1827 . 0086 .2065 .1990 . 1 920 -. 0020 . 1 958 

Elem Se sn Sr Ti Tl u v 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge· . 1926 ,0038 . 00313 -. 00419 .·0298 .2876 .0989 

IIi . 1889 .0028 . OQ3Q9 - .00455 .0350· .~44,2 .1010 

112 . 1947 . 0058 .003'14 - . 00.424 .0260 . 3549 .1011 

#3 . 1943 . 0027 . 00316 -. 00379 . 0284 .26j6 . 0945 

El em· '{ 213Zn ~n Zr 

U!lits ppm ppm ppm ppm 

AV9!!! 37.05 .1910 . 1'887 - : ooo1 

#1 36.03 .1922 .1892 - .0006 

112 37.60 .1920 . .1889 -.oooi 

1!3 37 . 50 .1889 . 1882 .0005 

VES 005688 
i 

Analysis Report 8/2~J08 02:28:34 PM page 1 

Method: PSC34 Sample Name: 

Run Ti,me: 08/21/08 14:23 :08 

HIKNA / Operator:· BGI 

Cononenc: 

Mode: ~NC Corr. Factor: 1 

Bl em Ag Al As B Ba Be Bi 

Un.it:s ppm ppm ppm ppm ppm ppm ppm Avge .0005 .0329 .0101 .0037 . 00009 -. 0004 5 ' .0184 

Ill .0018 .0527 .0089 . 0043 . 00019 - . ooo;n .0270 

112 -.0016 .0264 .0068 . 001.9 . 00001 -. 00051 .0093 

#3 .0015 .0196 .0147 .0649 .00008 -.00048 .0189 

Blem Ca Cd Co ·cr cu Fe K 

Units ppm , ppm ppm ppm ppm ppm ppm 

Avge .0628 . 00105 .·0017 .0041 . - .0018 . 022 . 100.7 

. #1 .1146 . 0014 1 .0Ql2 . .0053 -.0.032 .0448 1 00 , '9 

#2 .'0476 . 00057 · .. 0023 • 0.018 -.0007 .0172 100,3 

#3 . 02?2 . 00118 .00 15 . .0053 - .oots .·0068 100.9 

Elem Mg. Mn Mp · Na . Ni P ·· 2203/1 

Units ppm ppm ppm . ppm PPm ppm . PPm 

Avge . 0651 . 00038 . 0006 106.3 . 002 0 ,' 00 ~5 .0198 

til, . 1 096 . OOQ52.· : oo22 1 06.5 . 0031 .. 0011 .0203 

112 .0499 . OOOi:Q - . 001 4 i o5.8 .001? .0110 .0136 

113 . 0359 . 0005'3 .0008 1 06. 7 . 0010 .0044 .0255 

Elel\1 2203/2 s Sb 1960/1 1960/2 Si Pb 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge -.0091 .0042 . 0106 .0224 - . 0131 -. 0005 .0005 

ftl - . 0065 .0075 .0198 . 01:71 - .0124 . 0011 .0024 

#.2 -.0081 .0102 -. 0062 . 0141 - .oon -. 0007 -. 0009 

#3 - . 0 1 28 . . 0051 .0181 ,0359 -. 0177 -. 001 7 - .0000 

Blem Se S.n Sr Ti Tl u v 

Units ppm ppm ppm ppm ppm p pm ppm 

Avge - . 0013 .0064 .00007 .00067 .0047 .2233 -. 0014 

Ill -.0025 .0061 . OOQ06 .00053 . 0074 .2901 - .0014 

ll2 -. 0014 .0046 .00007 .00067 . 0045· .0984 -. 0018 

!13 .0001 .0087 .00009 .00082 . 0023 .2814 -. 0010 

Blem y 213Zn Zn Z%' 

Units ppm ppm ppm ppm Avge 37.85 .0002 . 0010 . 0008 

til 37.85 .0003 . 0004 .0004 

!12 37 . 70 -.0001 .0013 .0007 

#3 38.00 .0005 .0012 . 0013 

VES 005689 
'i11 ,. ,, ;:i~ ~ . ··: ~~ 

Analysi s ;" . ..;,~ ... . Report 08/?.l/.08 0~ : 36:19. PM page 1 

CRI/ 7 : .., ,. 

M.ethod: PSC34 Sa!!lPle Name: ! Operator: gbil Run .T.i~: 08/21/08 14 : 3.0: ?0 .. ~~ 9omment:: ('t'lt 

Mode: CQNC Corr. Factor: 1 ~·t 

Elem · Ag / Al .y. · l\S B . . ~ ... Ba Be · Bi 

units ppm .ppm ppm ppm· ~~ ppm ppm ppm 

Avge .0075 .125.9 .0518 .0472 ~. .00502 ; 0'0463 .0762 

#1 L. 005Z . .1193 :o497 . 0456 J;~ . 00474 , 00457 .0.683 . #2 .0076 H.1324 . 0547 ,~ .0470 'K'l!· . 00516 .00466 .0809 

113 . 00,6 , 1259 .0509 .0489 ¥ ,00516 . 00465 ,0795 

Elem · Ca Cd Co lj/ql' ' cu Fe K . cr ~ ·.units PJ;llll ppm ppm . a:{., ppm .ff;: ppm ppm ppm 

Avge . 15.21 . 01022 ' f{, 0137 .'Oll3:.t· .0082 .1030 . 1945 

Ill . 1484 . 00974 . 0127 · . 010·11 .0111 .1019 . 164 7: 

112 . 1537 .Ql.021 H:0143 • 0113 ." . 0070 19~3 .1767 

113 .~543 .01071 H. Ol42 ,o12~ : L:oo6s . 1037 . 2423 . 

Elem Mg Mn Mo Na ~~ "" Ni p 2203/1 

units ~P9' ppm ·ppm ppm 'I ppm ppm I?Pm . Av<;~e .. 0958 . 00516 : 0153 . 250.0 ·:£4 .0163 1~70 .. J)512 

#1 .6965 .OOSQ3 .Q126 .2587 !- . 0156 .1587 . 0557 

112 li. 0997 . 00502 . . 0168 . 2491 "' . 0].55 .1-:793 .0461 

#3 .0912 .. OOS4'4 .0166 . 2422 '·: . 0177 : t6J1 . 0517 

Elem 2203/2 s Sb 1960fl ;~ 1960/2 Si Pb 

uri.i.ts ppm ppm ppm ppm ppm ppm ppm 

Avg'e . 0528 . 1512 . . 0434 . 0559 ~ .0478 .0433 .0522 

Ill .0466 .1454 L.0296 

.d· . 0640 . . 0410 .0380 . 04!)6 

#2 . 0615 .1597 .0470 .0508 . 0516 .0444 .0564 

#3 .0502 .1484 .0537 .0528 .OS09 . 0474 . 0507 

Elem Se Sn Sr Ti Tl u v 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge .0505 .0530 .00516 . 00606 . 0838 . 2915 . 0154 

·Ill . Q487 . 0523 .00516 . 00599. .0854 .1836 . 0131 

112 .0513 . 0526 . 00517• .00635 .0875 . . 273 i . 0161 

113 .0516, . 0539 .0051& .00583 .0784 .4177 .0170 

Elem .Y 213Zn Zn Zr 

Units ppm ppm· ppm ppm ~ Avge 37.92 .0256 .0270 H. Ol02 <::, 

u 37 .·86 .0251 .0261 .0098 

ft2 37.94 .0251 .0276 8.0108 

ft3 37.97 . 0265 .0272 II. 01 01 .. 

. { 

" 

VES 005690 
! 

Analysis Report 0~/21/98 02:43:01 PM page 1 

Method: PSC34 Sali!Ple Name: }.591852: ~734:). :DUP-("' Operator: BG! 

RUn Time: 08/21/08 14:37:34 co~nt : 1"5-91852 

Mode: CONC Cor·r. Factor: 1 

Elem Ag Al As B Ba !le Bi 

unite ppm PP.Jil pp!!l ppm ppm PPII! P.Pm 

Ayge -. 0041 . . 0459 - .0001 . . OQlO . 00002. - . 00051 - .0018' 

Ill -. 0030 .088.0 -.0049 .0(}:).5 . 0002.9 -. 00041 • 0120 . 

11.2 ~ .0015 .0324 ·. 0073 ·:o025 -.00034 -.0006S .()002 

#3 -. 0 077 .0175 - .0028 ~.oo:i1 .00012 - . 00049 - . 0176 

. Elem Ca Cd Co Cr cu Fe K 

Units ppm ppm ppm P,Pm ppm ppm ppm 

Avge .0706 - .·00010 -.0005 ,0010 10 . 98 :0304 58.37' 

Ill . 1250 .OQ009 • 0019' :0024 . 10 . 97 ~~·~~ 58.33 

#2 . 0530 . 00053 ~:oo~3 . 0032 10.98 58.35 

113 ;0339 - . 00091 - .0020 -. 00f7 10:98 . 0152 59;42 

Ele.m Mg Mn Mo Na Ni p · 2203/1 

Units ppm ppm ppm ppm ppm ppm ppm 

AV:ge .0618 .. 0()003 ·.- . 0001' 2.163 .'0018 .OI)S5 - . 0041 

. #1· .p09 . 0.0020 .0002 2.169 . 0036 .01)(}0 -. 0111 . 

112 . 0131 .00035 - .0010 2.160 . 0031 .0102 .0285 

113 .0113 - . 000'45 .0004 2 .161. . - . .0012 .0063 -. 0296 

Elem 2203/2 s · Sb 1960/1 1960/2 Si Pb 

:units ppm ppm ppm ppm . ppm ppm ppm 

Avge . 0028 .0341 -.0018 ,0070 -.0014. .0062· . 0005 

Ill .0094 .0378 . 0043 . 0016 . 0013 . 0110 . 0025 

#2 -. 0171 . 0218 . 0053 . 0300 - . 0253 .0002 - . 0019 

113. .0163 . 0427 - .0149 -. 0105 .0199 . 0074 . 0010 

Elem Se Sn Sr Ti: Tl u v 

Units ppm ppm ppm ppm . ppm ppm ppm 

Avge . 0014· . 0832 . 00007. - .00005 -. 0014 . 0109 -. 0001' 

ft.l . 0014 .0823 .00016 . OOQ80 .oo::10 . o867 .0021 

112 - . 0069 . 087.2 .00006 -. 00043 .0062 .1227 -. 0032 

113 . 0097 .0800 .00001 - .00053 - . 0134 - .'1766 . 0007 

Elem y 213Zn Zr:t Zr 

Units pj:>m ppll) ppm ppm ·Avge · 37.66 .0007. . .0007 -,00()3 

Ill 37.64 . 0008 .0018 .0014 

#2 37 . 58 .ooo:i .0002 - . 0007 

113 37.76 .0010 .0000 - .0016 

VES 005691 
Analysis Report 0~/21/08 02:48:30 PM 

Method : PSC3~ · Sample Name: 1591852:~F7341:1000 ~Operator: BGI 

Run Time: 08/21/08 14:4 3:0~ 

Comment: 1591852 

Mode: CONC Corro Poactor: 1 

Blem 

Unite 

l\.vge 

Ill 

#2 

113 

0 l!lem 

Upi~s 

J>..vge 

ft1 

112 

1#3 

Elem 

Upit"s 

Avge · 

Ill 

·112 

113 

'Elem 

units 

Av.ge 

Ill 

112 

#3 

Elem 

Units 

Avge 

Ill 

112 

113 

Elem 

Units 

Avge 

IIi 

112 

ftJ 

Ag 

ppm 

- o0006 

o0002 

- o0032 

oOOll 

ca 

ppm 

o0073 

o0060 

o0093 

o0067 

Mg. ppm 

o0188 

o0324 

:out 

oOlOO 

2203/2 

ppm 

o0008 

-00026 

o0l11 

-.0060 

Se 

ppm 

-00018 

•o0063 

- o0009 

.0020 

y 

ppm 

37 o89 

37o79 

37o9l 

37o98 

Al 

ppm 

o0328 

o0507 

o0237 

o0238 

Cd 

ppm 

o00079 

o00081 

•o00003 

o00160 

Mil 

ppm 

o00037 

oOOO;l'\ 

o00016 

0 0006'2 

s 

ppm 

0 0397 

o0309 

o0430 

0 0454 

Sn 

ppm 

• 0167 

o0178 

o0158 

o0164 

213Zn 

ppm 

0 0008 

o0004 

o0014 

o0007 

AS 

ppm 

.0062 

o0076 

• o0010 

o012~ 

f=O 

ppm 

.0025 

o004.4 

o0021 

oOOll 

Mo 

ppm 

• o0006 

- 0 0011 

•oOOOO 

-, 0006 

Sb 

ppm 

o0026 

o0062 

- .0122 

o0137 

Sr 

ppm 

o00021 

o00030 

0 0001:6 

o00016 

Zn 

ppm 

.0024 

.0034 

.0021 

.0017 

B 

ppm 

o0021 

o0018 0002 

o0048 ° 

Cr 

ppm 

.003l 

.0037 

.ooos 

. 0 0049 

Nll. 

ppm 

20133 

2.140 

2:130 

2 o130. 

196Q/l 

ppm 

o0047 

0 0116 

- o Oll5 

0 0141 

T~ 

ppm 

0 00ll3 

o00221 

0 00077 

.00042 

Zr 

PP11l 

o0018 

0 0035 

o0010 

o0010 

Ba 

ppm 

o00016 

.. . ooop .. ~ .'OOP19o ·o00019 

,. cu 

" ppm 

"';~ 10 74 o~- ;0 7 

.>i;1.Q 0 76 ~~. 10 .. '74. )<l ... 1o'on . ~ . . ,. 

' Ni 

.· ppm . ;0035 

' 0 005.3. . 0 00,!)5 

o0046 

1960/2 

ppm . 

-. 0050 

- . 0153 

oOOH 

-0 0041 

Tl· 

~m 

o0019 . 

o0098 

.~on · 

- .0008 

Be 

ppm 

- 0 00.051 

-.00053 

- . 00047 ·- o00053 

Fe 

ppm 

. 0036 . 

o0028 

o0048. o0030 

p 

ppm 

o0092 

oOJ,24 

o0039 

.01'13 

Si 

PPm 

o0071 

.0061 

.0083 

o0070 

u 

ppm 

o1607 

.1842 

o0307 

.2673 

pase 1 

Bi 

ppm . .

0o008? 

•. 01190 

o0010 

o0132 

K 

PP!" 

56.084 

56.48 

56o99 

57 ."0.5 

2203/1 

ppm 

.0024 

o0086 .0 Ol52 

o0137 

Pb . ppm 

o00l3 

o0012 

.0023 

o0006 

v 

ppm 

o00l7 

.0010 

o0025 

.0016 

j 

VES 005692 
. ,: ..... 

i 

Analysis Report 08/21/08 02:54:35 PM page 1 

Method: PSC34 Samp~e Name: 1591852 :AF7339: ~ooo / Operator: BG:t 

Run Time' 08/2l/08 14 : 49 : 09 

coaunent: 159l852 

. Mode: .CO!lC Corr. Factor: 1 

Elem Ag Al As B Ba Be Bi. 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge -. 0018. . 0129 .001!1 . 0016 - .00008 - . 0.0057 .0083 

#1 - .0040 ·: . 0 1 51 .0010 -.0009 -.00013 - . 00064 7-00 02 

#2 . 0004 . 0350 .0003 . 00.43 - ·. 00009 •. OP5~ . : .0110 

#3 • . 0017 . oui8 .0(143 .oo·l4 - .00002 . - .00052 . .014~ 

El~m Ca C!i co Or cu Fe K 

Units ppm ppm ppm PP!D ppm PP"': pprfl. 

Avge . . 004.0 . 00039 . !)009 . 0012 5 . 608 ;0016 19.82 

111 . 0.039 . 00008 -. oo;n - .0095 5 .588 .0015 19 . 91 · #2 . 0044 ' 00.0$.1' ,0032 . 0027 5. 623 • 00.3,5 . 19.78 

#~ . 0038 .OQ.057 :o.o21 . 001S 5.6>1:5 .Q020 19 .. 78·: 

Elem Mg Mn · Mo · Na Ni p 2203/1. Units ppm ppm PP"' ppm ppm ppm . ppm Avge . 0056 .00019 -.OOH .6933 .0013 ·.0084 .0052 

Ill -. 03:85 -.00008 •. 0017 . 6855 . 0001 ,0008 .0006 

#;! . 0231 .. 00053 -.0000 . 6994 . 0027 .0058 • o·i5s 

# 3 . .0122 . 0001l - . 0023 . 695 0 . 0010 . 0185 -. 0009· 

Elem 2203/2 s Sl:> 1 960/1 ~60/2 Si Pb 

Units ppm ppm ppm ppm ppm ppm ppm 

Avge - . 0024 .0404 - . 0001 , 0116 - . 0078 .0000 .0001 

#1 .0015 .0412 ~.0054 .0083 - .0021 . 0002 .0012 

#2 -.0081 .042() . 0063 . 0162 - .0126 . 0002 -.0001 

#3 . . 0006 .0380 -.001 3 .0102 - .0088 ".0003 -. 0007 

Elem se Sn Sr Tl Tl u v 

Unit s ppm ppm ppm ppm ppm ppm ppm 

Avge .. 0014 .2288 .00007 . 0004 2 .0026 .0883 - .0004 

# 1 . 0013 .2262 -. 000!)7 - . 00.083 - . 0],62 -.0166 .0003 

112 - . 00'30 .2349 . 000.18 . 00124 .00 97 . 1 995 -.0010 

tt3 .. 0025 . 2253 . 00011 .00 086 .0144 .0819 - .0005 

Elem y 213Zn Zn Zr 

Units ppm ppm ppm ppm 

Avge 37 . 92 . 0004 . 0008 . 00'06 

#1 37 . 84 . 0004 - .0011 . . 002·0 

#2 38.06 .0007 . 00!'9 . 0021 .#3 37.86 . 0003 . 0016 . 0017 

VES 005693 
VES 005694 
Analysis ReJ>orc 08/21/08 03:07:22 .:PM page ·1 ! 

Method: PSC~4 Sample Name: Run Time: 08/21/08. 15 ,o1: ss 

CCV / 0p!"rator: BGI 

CO«Wnent : 1591852 

Mode: CONC Corr. Fact<llr: l 

Elem Ag Al A.s a Ba ae .. Bi 

Units ppm. ppm ppm ppm .ppm PPm ppm . Av:g:e . 2494 .9900 .2525 . 5053 . 50948' . 26163 . 2520 

lt1 2~83 1.004 .2482 .5044 . 50884 . 262QO . 2454 

#2 . 2475 . 9655 .2481 ,5025 .50891 . 26075 .2466 

#3 . 2524·. 1·001 . 2606 .5090 .51070 . 26215 .2640 

Elem Ca Cd Co Cr cu· Fe K 

T.lnits ppm ppm ppm ppm ppm ppm ppm 

Avge 5 . 156 .25725 .5125 .5036 .5018 6.159 ' 5 : 0'74 

#1 5 , 162 .25679' .5147 .5028 . 5074 6.185 4 . 961 

#2 !;.127 .25568 .5.0.67 • 4998 .4987 . 6.102 5 . 152 

#3 5'. 177 .25929 . 5161 . 5o8.2 .4993 6.191 5 .1iO 

El:em Mg Mn Mo Na. .Ni p · 2203/1 

Units ppm ppm ppm ppm PP1!1 ppm ppm , 

~vge . 3 ', 039 . 51824 . 25'59 . 2 -412 . 2582 2.570 . 5164 

Ill 3.021 . 51795 . 2591 2.419 . . 2587 2. ~!1 0 . 5016 '•f12 . 3.012 .51638 . 25S4 2.394 .2560 2.539 . 52'24 

#3 3 . 085 . 52041 . 2622 2 . 423 .2599 2.590 . 5252 

Elem 2203/2 s Sb 1960/1 . 1960/2 Si . PI:> 

Units ppm ·ppm ppm ppm ppm ppm ppm 

Avge . 5226 .1. 008 .2473 .2594 . 2565 . 4551 . 5205 

'#l . 530.5 1.008 .2139 . 2399 .2638 .4579 .5209 

#2 . 5227 . 9951 . 2544 .2654 .2511 L.4498 . 5226 

#3 . 5147 1.021 .2736 .2730 .2548 .4575 .5182 

Elem Se Sn Sr Ti Tl u v 

Units · Qpm ppm ppm ppm ppm ppm ppm 

Avge .2575 . 5084 . 25748 .50947 .5177 2 . 434 .2529 

#l :~m .5038 . 25732 .. 50!184 .5260 2.323 .2527 

#2 .5061· . 25694 . 50716 . .5076 2.380 .2507 

#3 . 2608 . 5154 . 25817 . 51142 .5196 2 .598 . 2552 

Elem '{ 213Zn Zn Zr. Units ppm _ppm ppm pp!ll 

1wge 38.26 1,266 1.277 .. S029 

Ill 38.34 1.266 .27~ . 5046 

#2 3Q.03 1.262 1 .268 . 4990 

#3 38.39 1.270 1. 285' . 50'49 

VES 005695 
Analysis R,epqrt 

Method: PSC34 

Run Tillie: 08/.21/08 

Comment: 159i652 

Sampl!l Name: CCB 

~5!9 : 01 

· Mode : CONC i::ox:r . . Factor:- l . 

El em ·units 

· Avge 

Ill 

11.2 . lf3. 

Elem 

Uri.its 

Avge 

Ill 

~~~ 

11,3 

Elem 

Uni t 

Avge 

lf1 

112 

113 

Elem · -Units 

Avge 

#1 

112 

. #3 

Elem 

Units 

Avge 

Ill 

112 

113 

Elem 

Units 

Avge 

#1 

#2 

113 

.A9 . 

ppm 

.0003 

.-. 0020 . 

. 00.15 . 0()15 

Ca 

ppm 

. . 0041 

Al 

ppm 

.011$9 

, 0081 

.Oi87 

.0240 

Cd 

. ppm 

. 00073 

As 

· ppm 

.0062 

- . 0,016, . P079 

H. Oi22 

co 

ppm 

. 0029 

• 00097 • 0021 . 00054 . 00.25 

.0053 

. 0'067 

.0.0.04 . .00069 . 0041 

/Jf:..{U .f.f:~, "'-.{ p,., f::( 

Mn '" ftrMovMo _,.. "'-'1 ppm ppm 

. 0),12 

8:.0173 

8.0278 

. 22.03/2 

PPm 00~3 

.0024 

.0009 

-. 0163. 

Se 

ppm 

.0008 

- . 0016 

.0044 

- '0_003 

y 

ppm 

38.07 

37.98 

38.09 

38.15 

. 00065 ·. 0023 

· .poo5, 

. O<i0.82 

'0005'3 

s 

ppm 

.()025 

.0085 

.003) 

- . 0041 

Sn 

ppm 

.0075 

, 0083 

.0077 

.0064 

213Zn 

ppm 

. 0017 

.0021 

. 0023 

. 0008 

.QQ2.9 

H.0055 

-.0016 

'l:t-.~7 

H. Ol89 

H.Ol25 

.Vf. 

Sr 

ppm 

'00020 

, 00025 

.00017 

. 00019 

Zn 

ppm 

.01)25 

• 0024. .0025 

.0026 

· .... ·.¥" ·-. ·. "i 

~ ~ .•• ::~ . 

I ~8/21/08 03:13 !28 PM : page 1 

Operator: BGI 

B 

ppm 

. 004!) 

. 00·35 

.'0.045 

. . 0.064 

Cr 

ppm 

.0035 

. 0023 

.0043 

.0039 

Na 

ppm 

. (>.10 6 

.0095 

. 0106 

.0118 

1960/1 

ppm 

.0142 

.0080 

.0041 

,0305 

Ti 

ppm 

H.00122 

H.OOll..4 

H, 09113 

H.00138 

Zr 

PP'1' 

.0020 

.0012 

. 0019 

H. 0027 

'-:· 

Ba 

ppm 

.00020 

.00()33 

. 0005() 

-. 0002~ 

Gu ,·; ppm 

' ·' . -' 001? 

. ·.· . .; . -: :·0041 :,-.~; ' ~: POl2 

·it·''· . o·oo2 

Ni 

ppm 

. 0020 

-.ooo5 

(!~20 

. 0044 

1960/2· ppm 

- . 0059 

- . 0064 . 0045 

- .0158 

Tl 

ppm 

.0097 

. 0006 

H.Ol81 

.0103 

·Be 

ppm 

- . 00054 

- . 0004-7 . - .00051 -. 00064 

Fe 

ppm 

.OOH 

. 0049 

. OO·P. 

. 0006 

p 

·ppm 

. . 0141 

.0052 

.Oi74 

.0198 

Si 

. ppm 

-. 0011 

-.0005 

.0022 

-.0050 

u 

ppm 

. 2200 

.·1 381 

.2366 

.2852 

·.:· . 

Bi 

ppm . :0118 

.0043 

.0139'. H. 0172 

K .-. 

PPI!I :· 

.0051 

0027 

~~ g~~~ ... ...... 2203/1 

ppm 

. 0069. 

.oou . . ·- .00 54 

.!\251 

PI;> 

ppm 

~ .·9006 

.0020 

.- .0012 

-. 0025 

· v 

ppm 

.0017 

. 0015 

.0037 

.0000 

VES 005696 
,Analysis Report 

Method: PSC34 Sample »a me: CCB 

15:2 :54 

Pactor: 1 

Run TiDe : 08/21/08 

Comment : 1592280 

Mode: C~ Corr. 

~i -) . Avg~ .0067 

AS 

ppm 

.0002 

#1 L-. 0056 

112 L·. 0061 

113 L· : 0055 

Blem 

Units 

Avge 

Ill 

#2 ' 

#3 

Blem 

Units 

Avge 

#.1 

#2 

#3 

Elem 

On its 

Avge 

#l 

#2 

#3 

Elem 

Units 

Avge 

Ill 

112 

113 

Elem 

Units 

Avg.e 

#1 

#2 

OJ 

Ca 

ppm 

- .0012 

-.0053 

. 0009 

·:ooo8 

Mg 

ppm 

-.0042 

- .P047 

- .. 0042 

.0038 

2203/ 2 

ppm 

.0063 

- .0025 

.0124 

.0090 

Se 

ppm 

.0005 

- .0043 

.0019 

.0041 

y 

ppm 

38 . 00 

38 . 0). 

38.07 

37.93 

.0042• 

.ono 

.ooso 

Cd 

~~6oo8o 

·.OOQ.73 - .OQ083 

-.00085 

Mn 

ppm 

- .00036 

- ·. 00031 

- .00037. 

• . 00037 

s 

PPill 

-.0005 

-. 0103 

.0050 

.0038 

Sn 

ppm 

-. 0025 

-.0024 

- .0018 

- .0033 

213Zn 

ppm 

.0004 

.0001 

.0005 

.0006 

-. 0046 

.0027 

.0()23 

Co 

ppm 

- .OOOj; 

-.0013 

-.oooo 

-.0004 

Mo 

PP'~ 

- .0001 

-. '0015 

-.0004 

. 001 5 

- -""· Sb 

ppm I 

L- .0183 I . ,./· 

- . '212 

L-. 0187 

L". 0149 

Sr 

ppm - . 00004 

-.ooop5 - .00004 - ·.00003 

Zn 

ppm 

-.0001 

-.0006 

.0002 

.0002 

08/21/08 03: 2 7:20 PM 

B 

ppm 

-.0015 

- .00~9 

- . \)004 

- . 00~1 

Cr 

PP!lt 

;. . 0014 

-. 00.2.5. 

-. 0.011 - .0004 

Na 

ppm 

. 0023 

. 0019 

.'00'28 

.0021 

1960/l 

'Ppm 

- . 0030 

. 0072 

·-·. 0089 

" .0073 

Ti 

ppm 

-.00035 

- .00035 

- . 00021 

- . 00049 

Zr 

ppm 

-.0006 

-. 0006 

-.0006 

-. 0006 

Operator: BGI 

Ba 

PP'l' 

-.00027 

• . 00065 

-. 000!)2 

-. 0\)013 

cu 

ppin 

-:.ool3 

::ggg; 

·-. o'o23 · 

.Ni 

ppm 

, .0013 

-.• 0018 

- . 00,19. 

.- .opo2 

i960/2 

ppm 

.OQ23 

-.01 01 

. 0073 

.Q098 

Tl 

ppm 

.0053 

.00 62 

-. 0029 

.0125 

Be 

ppm 

- . 00071 

- . 00085 

-.Ob060 

-. 00068 

FJ> 

ppm 

-. 0002. 

-. 0027 

:0013 

.0007 

p 

ppm 

.0062 

,0149 

-.002~ 

.0066 

si 

ppm . -.OQSS 

L-. 0118 

- .001 5 

- . 0032 

u 

~~802 

-. 1164 

-.0895 

- .0345 

page 1 

Bi 

ppm . -.0076 

.90~6 

· - .0021 

- . 0152 

K 

ppm 

-.0314 ·. 

-. 0278 . 

- .0397 

-. 0266 

2203/1 . 

ppm 

-. 0'071 

.0097 . 

7 . 0.172 

-.0155 

Pb ' 

ppm 

. 001 6 

.0016 

.0025 

.0008 

v 

ppm 

- . OOll 

-.0030 

· -.0015 

.0013 

VES 005697 
I · 

· .st.andardi zat.ion Rpt. 08/21/08· '03 : 36:16 PM ·.pag~ l 

' ' 

Method: PSCl4 .Standard: CAL-BLK 

Rlll_l Ti~ . OB/21/08 15:33: 4 8 

Elem Ag Sb. 

Avge -. 01 20 ._ 0~40 

#1 .0020 .0050 

112 - . 014'0 .oo7.o . . 113 -.0240 ~ .024.0 . 

VES 005698 
Standa:rdization 

Method: PSC34 

Blem(!nt 

1\9 . 

Sb 

Wave len 

328.068 

206.838 

Report QS/21/JJS 03:36: 20 PM page 1 

Slope • Conc(SIR)/IR 

High std 

STO,B 

STD-B 

Low std 

'CAI,.-BLK 

CAL-BLK 

Slope 

.042768 

.1,03108 

Y-intercept 

,000513 

.000~12 

Date Stand~rdized ·. 08/21/08 03:33 :48 

08/21/08 03:33:48 

VES 005699