AppendixE 

Calibration Data 
BARR 

Engineering Company 

Project 

Sample Lac. 

Date 

Operators 

United Taconite Co. 

Line 1 Waste Gas Stack 

5/3/2005 

T. Kuchinski 

Analyzer Make 1 Mod. 1 SN API 100AH 

Analyzer Range (span), PPM: 500 

Stripchart Speed (units): 20 cmlhr 

ANALYZER CALIBRATION DATA 

Note: Difference must be less than +/- 2 percent of span 

Cylinder 

Test Runs: Test 1 R1 Value, 

PPM 

Zero Gas 0 

Mid-range 245.7 

High-range: 461 

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

EPA METHOD 7E - Nox 

ANALYZER CALIBRATION 

Cylinder 

Serial No. 

Zero Gas - Mid-range CC12793 

High-range CC40072 

Analyzer Absolute Difference, 

Calibration Difference Percent of 

Response, PPM PPM Span 

0.1 0.1 0.02% 

243.4 2.3 0.46% 

461.8 0.8 0.16% 

Note: System Cal bias cannot exceed +/- 5 percent of span. Drift cannot exceed +/- 3 percent of span 

Initial Values Final Values 

Analyzer Cal System Cal System Cal System Cal System Cal 

Response Response, Response, Cal. Bias Response, Cal. Bias 

TEST RUN 1 Time (sec) PPM PPM % of Span PPM % of Span 

Zero Gas 0.1 0.4 0.06% 2.0 0.38% 

Upscale Gas 243 238.1 -1.06% 239.9 -0.70% 

TEST RUN 2 

Zero Gas 2.0 2.0 0.00% 1.7 -0.06% 

Upscale Gas 243.4 239.9 -0.70% 234.2 -1.84% 

TEST RUN 3 

Zero Gas 2 1.7 -0.06% 1.5 -0.10% 

Upscale Gas 243.4 234 -1.84% 233 -2.08% 

TEST RUN 4 

Zero Gas 2 1.5 -0.10% 2.2 0.04% 

Upscale Gas 243.4 233 -2.08% 237 -1.28% 

System Calibration Bias = [(System Cal. Response - Analyzer Cal. Response) / Span] x 100 

Drift = [(Final System Cal. Response - Initial System Cal Response) / Span] x 100 

Cert. PPM 

0 

245.7 

461 

Drift, 

Percent of 

span 

0.32% 

0.36% 

-0.06% 

-1.14% 

-0.04% 

-0.24% 

0.14% 

0.80% 
BARR 

Engineering Company 

Project 

Sample Loc. 

Date 

Operators 

United Taconite Co. 

Line 1 Waste Gas Stack 

05/03/05 

T. Kuchinski 

Analyzer Make I Mod. I SN 100AH 

Analyzer Range (span), PPM: __ 1.:..0::...;0~_ 

Stripchart Speed (units): 20 cm/hr 

ANALYZER CALIBRATION DATA 

Note: Difference must be less than +/- 2 percent of span 

Cylinder 

Test Runs: Test 4 R1 Value, 

PPM 

Zero Gas 0 

Mid-range 50.5 

High-range: 93.1 

SYSTEM CALIBRATION BIAS AND DRIFT DATA: 

EPA METHOD 6C - 502 

ANALYZER CALIBRATION 

Cylinder 

Serial No. 

Zero Gas Nitrogen 

Mid-range CC68786 

High-range CC121446 

Analyzer Absolute Difference, 

Calibration Difference Percent of 

Response, PPM PPM Span 

0.1 0.1 0.08% 

51.5 1.0 1.00% 

92.9 0.2 0.20% 

Note: System Cal bias cannot exceed +/- 5 percent of span. Drift cannot exceed +/- 3 percent of span 

Initial Values Final Values 

Analyzer Cal System Cal System Cal System Cal System Cal 

Response Response, Response, Cal. Bias Response, Cal. Bias 

TEST RUN 1 Time (sec) PPM PPM % of Span PPM % of Span 

Zero Gas - 0 0.9 0.82% 1.3 1.22% 

Upscale Gas - 52 47.6 -3.90% 48.1 -3.38% 

TEST RUN 2 

Zero Gas - 0 1 1.22% 1.7 1.58% 

Upscale Gas - 52 48.1 -3.38% 49.3 -2.20% 

TEST RUN 3 

Zero Gas - 0 1.7 1.58% -0.03 -0.11% 

Upscale Gas - 51.5 49.3 -2.20% 48 -3.20% 

TEST RUN 4 

Zero Gas - 0 -0.03 -0.11% -0.10 -0.18% 

Upscale Gas - 51.5 48.3 -3.20% 48 -3.70% 

System Calibration Bias = [(System Cal. Response - Analyzer Cal. Response) / Span] x 100 

Drift = [(Final System Cal. Response - Initial System Cal Response) / Span] x 100 

Cert. PPM 

0 

50.5 

93.1 

Drift, 

Percent of 

span 

0.40% 

0.52% 

0.36% 

1.18% 

-1.69% 

-1.00% 

-0.07% 

-0.50% 
BARR 

Engineering Company 

Project United Taconite Co. 

Sample Lac. Line 1 Waste Gas Stack 

Date 05/03/05 ------------------- Operators T. Kuchinski --~---------------

Analyzer Make I Mod. I SN Vig Model 20 

Analyzer Range (span), PPM: 100 

Stripchart Speed (units): 20 cm/hr 

Linearity Demonstration 

EPA METHOD 25A-THC as methane 

ANALYZER CALIBRATION 

Cylinder 

Serial No. 

Zero Gas Zero Air 

Low-range SG9165492 

Mid-range CC2937 

High-range CC4777 

Note: Response must be less than +/- 5 percent of actual calibibration gas values. 

Cert. PPM System Respon Percent Diff 

Zero Gas 0 0.4 0.4 

Low-range 30.2 29.6 1.99 

Mid-range 46.5 45.6 1.94 

High-range 90.4 90 0.44 

SYSTEM CALIBRATION AND DRIFT DATA: 

Cert. PPM 

0 

30.2 

46.5 

90.4 

Note: System Calibration cannot exceed +/- 5 percent of span gas value. Drift cannot exceed +/- 3 percent of span 

Initial Values Final Values 

System Cal System Cal Drift, 

Response Response, Response, Percent of 

TEST RUN 1 Time (sec) PPM PPM span 

Zero Gas 0.4 0.8 0.40% 

Upscale Gas 30 31.2 1.19% 

TEST RUN 2 

Zero Gas 0.8 0.8 0.00% 

Upscale Gas 31.2 30.5 -0.66% 

TEST RUN 3 

Zero Gas 0.8 1.0 0.20% 

Upscale Gas 30.5 31.0 0.47% 

TEST RUN 4 

Zero Gas 1.0 1.1 0.10% 

Upscale Gas 31.0 30.3 -0.70% 
Control Module 

Project: 

Date: 

Technician: 

Orifice Dry Gas 

Diff Volume 

Pressure H Cubic Feet 

Nominal Final 

0.500 291.795 

Actual Initial 

286.745 

0.50 Total 

5.050 

Nominal Final 

1.000 299.870 

Actual Initial 

292.810 

1.00 Total 

7.060 

Nominal Final 

2.000 305.935 

Actual Initial 

300.885 

2.00 Total 

5.050 

Nominal Final 

3.000 311.985 

Actual Initial 

306.950 

3.00 Total 

5.035 

Nominal Final 

4.000 319.080 

Actual Initial 

313.000 

4.00 Total 

6.080 

C-1 

Routine 

03/19/05 

NRS 

WetTest 

Volume, 

Cubic Feet 

Final 

2772.00 

Initial 

2767.00 

Total 

5.00 

Final 

2780.00 

Initial 

2773.00 

Total 

7.00 

Final 

2786.00 

Initial 

2781.00 

Total 

5.00 

Final 

2792.00 

Initial 

2787.00 

Total 

5.00 

Final 

2799.00 

Initial 

2793.00 

Total 

6.00 

Leak checks 

Negative - ok 

Positive -- ok 

Dry Gas Meter WetTest 

Temp, F Meter 

Inlet Outlet Temp, F 

Final Final Final 

69.0 68.0 67.0 

Initial Initial Initial 

69.0 67.0 67.0 

Average Average Average 

69.0 67.5 67.0 

68.3 

Final Final Final 

71.0 68.0 67.0 

Initial Initial Initial 

69.0 68.0 67.0 

Average Average Average 

70.0 68.0 67.0 

69.0 Tm 

Final Final Final 

72.0 69.0 67.0 

Initial Initial Initial 

71.0 68.0 67.0 

Average Average Average 

71.5 68.5 67.0 

70.0 Tm 

Final Final Final 

74.0 69.0 67.0 

Initial Initial Initial 

73.0 69.0 67.0 

Average Average Average 

73.5 69.0 67.0 

71.3 Tm 

Final Final Final 

75.0 70.0 67.0 

Initial Initial Initial 

74.0 69.0 67.0 

Average Average Average 

74.5 69.5 67.0 

72.0 Tm I 

Control Module 1 

>5W.C. 

> in.Hg 

Barometric Pressure 

Previous Y ---

Previous Delta H -

Elapsed Meter 

Time of Coefficient 

Cal. Point Y 

Minutes SEC 

12 42.14 

Minutes 

12.70 0.9912 

Minutes SEC 

12.0 47.68 

Minutes 

. 

12.79 0.9928 

Minutes SEC 

6 30.45 

Minutes 

6.51 0.9907 

Minutes SEC 

5.0 20.53 

Minutes 

5.34 0.9935 

Minutes 

5.0 35.53 

Minutes 

5.59 0.9863 

Average I 0.9909 

29.19 

0.9905 

1.9111 

Orifice 

Coefficient 

dH@ 

1.8451 

1.9084 

1.9334 

1.9526 

1.9792 

1.9237 
BARR Routine 

Dr'} Gas Meter Calibration 

\\ 

, 

, Control Module Number: c.-1- Leak Checks Barometric Press.: 2c

r.(t 

Date: 3-19 -oS' Positive erk 5 in. W.C. Previous Y: .C{QO:> 

Technician: A.)f?-'; Negative c\!... 15 in.Hg Previous ~H: i. ~r l! ( 

Orifice Dry gas WetTest Dry Gas Meter WetTest Elapsed Meter Orifice 

DiffPres. Volume Volume Temp (""F) Meter Time of Coefficient 

("H2O) (Fe) (Ft~) Inlet Outlet Temp (""F) 

Nominal Rnal Rnal Rnal Rnal Rnal 

,S- Z"l (.1'1~ 2..112- &4 <.of' Gf 

Actual. Initial Initial Initial Initial 

.) 2~c.. .. 1LjS- 21&,'1 t;; Gl 

Average Average 

(.:,""1 ~IS 

AverageTm 

Dry Gas Meter 

DiffPres. Volume Temp (""'F) 

("H2O) (Ft~) Inlet Outlet 

Nominal Rnal Rnal Rnal 

/.0 '1 &;8 G1 

Initial Initial Initial 

~"'i G::s' 

Average Average 

ltl c." ~ Average Tm 

Orifice Dry gas WetTest Dry Gas Meter 

DiffPres. Volume Volume Temp (""F) 

("H2O) (Fe) (Ft~) Inlet Outlet 

Nominal Rnal Rnal Rnal Rnal Rnal 

2.0 3Q$','13S' 2lXG 2.. (0'1 Gl 

Actual Initial Initial Initial Initial Initial 

LO ')OU .'iSS- 21 ~l l?Y' 01 

Average Average 

( 1.S' <,,:>1).SAverageTm 

Orifice Dry gas WetTest Dry Gas Meter 

DiffPres. Volume Volume Temp (""F) 

("HzO) (Fe) (Ft~) Inlet Outlet 

Nominal Rnal Rnal Rnal Rnal Final 

·S .0 l.?'1 Gl 

Actual Initial Initial Initial Initial Initial 

3CG. cl"S 2(£'1 iii G~ Col 

Average Average 

/3.:S- G~ 

AverageTm 

Dry Gas Meter 

Volume Temp("'"'F) 

(Ft') Inlet Outlet 

Nominal Rnal Rnal Rnal Rnal 

{i .0 31'1.0g' l~ 10 01 

Initial Initial 

1.0"1 Gl 

Average Average 

0cr.S- <0, 

Average Tm 
Control Module 

Project: 

Q 

Routine 

05/10105 

NRS 

Date: 

Technician: 

Orifice Dry Gas WetTest 

Diff Volume Volume, 

Pressure H Cubic Feet Cubic Feet 

Nominal Final Final 

0.500 102.360 3292.00 

Actual Initial Initial 

97.345 3287.00 

0.50 Total Total 

5.015 5.00 

Nominal Final Final 

1.000 108.395 3298.00 

Actual Initial Initial 

103.370 3293.00 

1.00 Total Total 

5.025 5.00 

Nominal Final Final 

2.000 96.345 3286.00 

Actual Initial Initial 

91.340 3281.00 

2.00 Total Total 

5.005 5.00 

l'<UIIIIIIClI Final Final ,., "')0 114.450 3304.00 

Actual Initial Initial 

109.410 3299.00 

3.00 Total Total 

5.040 5.00 

Nominal IFinal Final 

4.000 120.480 3310.00 

Actual Initial Initial 

115.460 3305.00 

4.00 Total I-:-otal 

5.020 5.00 

Leak checks 

Negative - ok 

Positive - ok 

Dry Gas Meter Wet Test 

Temp, F Meter 

Inlet Outlet Temp, F 

Final Final Final 

75.0 73.0 74.0 

Initial Initial Initial 

73.0 72.0 74.0 

Average Average Average 

74.0 72.5 74.0 

73.3 

Final Final Final 

76.0 74.0 74.0 

Initial Initial Initial 

75.0 73.0 • 74.0 

Average Average Average 

75.5 73.5 74.0 

74.5 Tm 

Final Final Final 

73.0 72.0 74.0 

Initial Initial Initial 

72.0 72.0 74.0 

Average Average Average 

72.5 72.0 74.0 

72.3 Tm 

Final Final Final 

78.0 74.0 74.0 

Initial Initial Initial 

76.0 74.0 74.0 

Average Average Average 

77.0 74.0 74.0 

75.5 Tm I 

Final Final Final 

79.0 75.0 73.5 

Initial Initial Initial 

78.0 74.0 74.0 

Average Average Average 

78.5 74.5 73.8 

76.5 Tm I 

>5W.C. 

> in.Hg 

Barometric Pressure 

Previous Y -

Previous Delta H -

Elapsed Meter 

Time of Coefficient 

Cal. Point Y 

Minutes SEC 

12 24.17 

Minutes 

12.40 0.9943 

Minutes SEC 

8.0 57.89 

Minutes 

8.96 0.9934 

Minutes SEC 

6 23.6 

Minutes 

6.39 0.9907 

Minutes SEC 

5.0 15.24 

Minutes 

5.25 0.9873 

Minutes SEC 

4.0 34.52 

Minutes 

4.58 0.9911 

Average I 0.9914 

c -( K 00-\ ~'V\. 12. C q r ~ b I CA. + ~ dl.--' fJ<.r;Cu J .-"Le. J 

~A- C ~·--r, ~ . p~~+- +-..; --J r ..... I 

CC-t./ 

J/L1. c1-v C ~ r ~ b f q -r~ d~ . 

Control Module 1 

29.00 

0.9909 

1.9237 

Orifice 

Coefficient 

dH@ 

1.8009 

1.8783 

1.9159 

1.9336 

I 

1.9514 

1.8960 
Routine BARR Dry Gas' Meter Calibration 

,-' 

Control Module Number: --'=---'"'=_ Leak Checks Barometric Press.: Z"i .cO 

Date: ::;-- j C -0'::;; Positive u Ie at 5 in.H20 Previous Y: ' 7709 

Technician: --=-,'-'=:.'tZ-::::..::S'--_______ _ Negative __ C'_k... __ at 15 in.Hg Previous ~H: /.~ 237 

Orifice 

DiffPres. 

Nominal 

l~ 

DiffPres. 

("H20) 

Nominal 

i.O 

Actual 

{,O 

Diff Pres. 

("H2O) 

Nominal 

2. C 

Dry gas 

Volume 

(Ft') 

WetTest 

Volume 

(Ft') 

Final 

3 2.~G:: 

Dry Gas Meter WetTest Elapsed 

Time of 

Meter Orifice 
Control Module 

Project: 

Date: 

Technician: 

Onf~GaS Diff lume 

Presu ic Feet 

INomlna Inal 

0.500 42.565 

Actual Initial 

37.530 

0.50 Total 

5.035 

INominal IFinal 

1.000 48.610 

Actual Initial 

43.575 

1.00 Total 

5.035 

INomlnal Final 

2.000 54.690 

IActual Initial 

49.625 

2.00 Total 

5.065 

I 

Nominal Final 

3.000 60.785 

Actual Initial 

55.710 

3.00 Total 

5.075 

INOminal Final 

4.000 67.885 

Actual Initial 

61.805 

4.00 Total 

6.080 

I 

C-2 

Routine 

4/23/2005 

NRS 

Wet Test 

Volume, 

Cubic Feet 

!Final 

3045.00 

Initial 

3040.00 

Total 

5.00 

·Final 

3051.00 

Initial 

3046.00 

Total 

5.00 

IFinal 

3057.00 

Initial 

3052.00 

Total 

5.00 

Final 

3063.00 

Initial 

3058.00 

Total 

5.00 

IFinal 

3070.00 

Initial 

3064.00 

Total 

6.00 

I 

I 

Leak checks 

Negative -

Positive -

Dry Gas Meter 

Temp, F 

Inlet Outlet 

Final Final 

73.0 70.0 

Initial Initial 

71.0 69.0 

Average Average 

72.0 69.5 

70.8 

Final Final 

76.0 71.0 

Initial Initial 

73.0 70.0 

Average Average 

74.5 70.5 

72.5 Tm I 

rlnal Final 

79.0 72.0 

Initial Initial 

77.0 71.0 

Average Average 

78.0 71.5 

74.8 Tm 

Final Final 

81.0 72.0 

Initial Initial 

79.0 72.0 

Average Average 

80.0 72.0 

76.0 Tm 

Final Final 

83.0 73.0 

Initial Initial 

81.0 72.0 

Average Average 

82.0 72.5 

77.3 Tm I 

ok 

ok 

Wet Test 

Meter 

Temp, F 

Final 

69.0 

Initial 

69.0 

Average 

69.0 

Final 

69.0 

Initial 

69.0 

Average 

69.0 

Final 

69.0 

Initial 

69.0 

Average 

69.0 

Final 

69.0 

Initial 

69.0 

Average 

69.0 

Final 

68.5 

Initial 

69.0 

Average 

68.8 

Barometric Pressure 

Previous Y -

>5 W.C. Previous Delta H -

> in.Hg 

Elapsed Meter 

Time of Coefficient 

Cal. Point Y 

Minutes SEC 

12 36.25 

Minutes 

12.60 0.9951 

Minutes SEC 

9.0 2.3 

Minutes 

9.04 0.9971 

Minutes SEC 

6.0 29.3 

Minutes 

6.49 0.9929 

Minutes SEC 

5.0 19.27 

Minutes 

5.32 0.9908 

Minutes SEC 

5.0 31.4 

Minutes 

5.52 0.9928 

Average I 0.9937 

29.34 

0.9909 

1.8875 

Orifice 

Coefficient 

dH@ 

1.8143 

1.8624 

1.9159 

1.9311 

1.9228 

1.8893 

I 
BARR 

Control Module Number: c.. -2 

Date: j-l3 -oS" 

Routine 

Dry Gas Meter Calibration 

Leak Checks 

Positive ck 

Technician: tJ(LS ~~==------------------ Negative 0 It.. 

Orifice 

DiffPres. 

("H20) 

Dry gas 

Volume 

(Ft') 

Nominal Final 

oSc 42. 50S" 

Orifice 

Diff Pres. 

("H20) 

Nominal 

\.0 

Actual 

1.0 

Diff Pres. 

("H20) 

Nominal 

2...6 

Actual 

Orifice 

DiffPres. 

("H20) 

Nominal 

"3 0 

Diff Pres. 

("H20) 

Nominal 

'i.e) 

Dry gas 

Volume 

(Fe) 

Final 

4 " 

Initial 

LJ3S7<; 

Dry gas 

Volume 

(Fe) 

Final 

~,1ff;" 

Initial 

Volume 

(Fe) 

Final 

cOT 

WetTest 

Volume 

(Fe) 

Final 

3o'-i SInitial 

jO,-{O 

WetTest 

Volume 

(Fe) 

Final 

305"'( 

Initial 

3Uil.o 

Volume 

(Ft') 

Final 

305"1 

Initial 

3"lS"2 

WetTest 

Volume 

(Fe) 

Final 

30<03 

Initial 

Volume 

(Fe) 

Dry Gas Meter 

Temp ('""'F) 

Inlet Outlet 

Final Final 

j{3 70 

Initial 

71. 

Average 

tL 

AverageTm 

Dry Gas Meter 

Temp ('""'F) 

Inlet Outlet 

Final 

-11.0 

Initial 

13 

Average 

74.SAverageTm 

Dry Gas Meter 

Temp (""F) 

Inlet Outlet 

Final Final 

7'1 "12.. 

Initial Initial 

71 II 

Average 

is liS 

AverageTm 

Dry Gas Meter 

Temp (""'F) 

Inlet Outlet 

Final Final 

~, i 72.. 

Initial 

1"2. 

Average Average 

80 1"2... 

AverageTm 

Dry Gas Meter 

Temp ("""F) 

Inlet Outlet 

Final 

~. 

Initial 

8'( 

Average 

1'-

Final 

i3 

Initial 

\.L 

Average Tm 

WetTest 

Meter 

Temp ('""F) 

Final 

~,9 

Final 

"''1 

Initial 

(,'1 

Final 

(09 

Initial 

CCI 

Barometric Press.: 29.3,-( 

at 5 in.H20 Previous Y: .9"10 c( 

at 15 in.Hg Previous D.H: t. 'i< 3' 1 ':l"' 

Elapsed 

Time of 

Calibration Point 

Minutes 

Meter 

Coefficient 

Orifice 
EPA M5 POST TEST METER CALIBRATION 

BARR 

Project Name: United Taconite 

Module Number: C-2 -=--=---- Date: 7-May-05 

Tech: ..;.NR.:.:..:::S=--__ 

Orifice Dry Gas Wet Test 

Diff Volume, Volume, 

Cubic Feet Cubic Feet 

Final Final 

768.400 3201.00 

Initial Initial 

763.330 3196.00 

Total 

Initial 

3202.00 

Total 

Initial 

3209.00 

Total 

Nominal sample conditions 

Delta H: 1.3 W.C. 

Vacuum: 7 in. Hg 

Dry Gas Meter Wet Test 

Tern, F Meter 

Inlet Outlet Tern , F 

Final Final Final 

80.0 74.0 

Initial Initial Initial 

81.0 73.0 

Average Average Average 

80.5 73.5 . 77.0 Tm 

Final 

75.0 

Initial Initial Initial 

80.0 74.0 

Average Average Average 

80.5 74.5 

77.5 Tm 

Final 

75.0 

Initial Initial Initial 

81.0 75.0 

Average Average 

81.0 

Project No.: 23/69-948-TAK 

Barometric Pressure: 29.07 

71.0 

Previous Y : -"""0-.9-93-7-

Previous Delta H : 1.8893 --..:...:..:..:.-

Elapsed 

Time of 

Cal. Point 

SEC 

Pre cal + 5% 

Pre cal- 5% 

Within 5% YIN 

Meter 

Coefficient 

Y 

1.0434 

0.9440 

YES 

Orifice 

1.9838 

1.7948 

YES 
EPA lVI5 POST TEST METER CALIBRATION 

-/ 

, ----- Project Name: !.td_,J 11<"",. Le_ 

vIodule Number: c.. -2- --='--"'=-------

Orifice 

Diff 

Date: 5 - 7 - 0 ') 

Tech: 1'0f<..S 

Dry Gas 

Volume, 

Cubic Feet 

Final· 

-;"( ?'-f 

Initial 

PTe Template 

WetTest 

Volume, 

Cubic Feet 

Final 

& 32Ct 

Initial 

3 ! G) (-; 

Initial 

'3202 

.5 2.IL{ c 

Initial 

3201. 

Nominal sample conditions 

DeltaH: 1·3 W.e. 

Vacuum: I,e in.Hg 

Dry Gas Meter WetTest 

Temp, F Meter 

Inlet Outlet Temp, F 

Final Final Final 

: Q ·.,ii 

jj g i/ 

Initial Initial Initial 

3"'1 (3 II 

Average Average 

1St) ~ 75.C:;-

Tm 

Final 

l~-

Initial Initial Initial 

~() 7'-t. ""It 

Average 

gus 

Tm 

Final Final 

8'/ le;;- If 

Initial Initial Initial 

8"( 7S- t! 

Average Average 

3"1 isProject No.: Z ~/6 c1_ 9 L{ Y 

Barometric Pressure: 2.<1.0'1 

Previous Y : ,'1 'i .37 

Previous Delta H : I . S' gj 3 

Elapsed Meter Orifice 

Time of Coefficient 

Cal. Point Y 

. Minutes SEC 

7 i.f7.71 
EP A lVI5 POST TEST METER CALIBRATION 

'BARR 

Project Name: ~A l\:k~1 1:c,-",,~ 

vIodule Number: (. - L ~~=-----------

Date: S - 7 -0 "5" 

Tech: /0:2.. S 

Orifice Dry Gas Wet Test 

Diff Volume, Volume, 

Presure dH Cubic Feet Cubic Feet 

Final Final 

-~. -S 31~:L 

Initial 

3\11 

Total 

PTe Template 

Nominal sample conditions 

DeltaH: s· 3 

Vacuum: q ,0 

Dry Gas Meter 

Inlet 

Final 

lJ 

Initial 

1'f( 

Average 

l~ 

Temp, F 

Outlet 

Final 

'(5 

Initial 

73 

Average 

13 

Tm 

Final 

13 

Initial 

1'2 .. 

. 

Average Average 

l1 1 Z:SInitial 

2'0 

Average 

gO.) 

Tm 

Final 

(~ 

Initial 

13 

Average 

tJ 

W.e. 

in. Hg 

Wet Test 

Meter 

Temp, F 

Final 

if 

Initial 

7( 

Project No.: Z~!b7 - '-(c.fJJ 

Barometric Pressure: 2. C( ,07 

Previous Y : . '1 '1 37 

Previous Delta H : IsS' '13 

Elapsed Meter Orifice 

Time of Coefficient 

Cal. Point Y 

Minutes SEC 

S-
EPA M5 POST TEST l\tIETER CALIBRATION 

BARR 

Project Name: United Taconite 

Module Number: C-2 -=...:=-----

Date: 27-Jan-05 

Tech: .:..N:..:.R=S~ __ 

Orifice Dry Gas Wet Test 

Diff Volume, Volume, 

Presure dH Cubic Feet Cubic Feet 

Nominal Final Final 

1.57 556.820 2086.00 

Actual Initial Initial 

551.765 2081.00 

Total 

Initial 

2087.00 

Total 

5.080 5.00 

Nominal Final Final 

1.57 568.990 2098.00 

Initial Initial 

563.920 2093.00 

Total 

II 

Nominal sample conditions 

Delta H: 1.57 W.e. 

Vacuum: 4 in. Hg 

Dry Gas Meter WetTest 

Tern, F Meter 

Inlet Outlet Tern . F 

Final Final Final 

73.0 69.0 

Initial Initial Initial' 

72.0 69.0 

Average Average 

72.5 

70.8 Tm 

Final 

70.0 

Initial Initial Initial 

73.0 69.0 

Average Average 

74.0 

71.8 Tm 

Final Final 

77.0 71.0 

Initial Initial Initial 

76.0 70.0 

Average Average Average 

76.5 70.5 

Project No.: 23/69-923-TAK 

Barometric Pressure: ___ 2_9_.6_3_ 

68.0 

Previous Y: __ 0...:..9-,-9_1_7_ 

Previous Delta H: _...:1..:..;.8:...;.8-,-0,-9_ 

Elapsed 

. time of 

Cal. Point 

SEC 

Pre cal + 5% 

Pre cal- 5% 

Within 5% YIN 

Meter 

Coefficient 

Y 

1.0413 

0.9421 

YES 

Orifice 

1.9749 

1.7869 

YES 
Control Module 

Project: 

Date: 

Technician: 

~s e 

·c Feet 

omlna Ina 

0.500 144.650 

Actual Initial 

139.640 

0.50 Total 

5.010 

INomlnal • final 

1.000 150.675 

IActual Initial 

145.650 

1.00 Total 

5.025 

INomlnal (-Inal 

2.000 156.735 

Actual Initial 

151.690 

2.00 Total 

5.045 

Nominal Final 

3.000 162.805 

,Actual Initial 

157.745 

3.00 Total 

5.060 

INomlnal (-Inal 

4.000 168.885 

IActual Initial 

163.825 

4.00 Total 

5.060 

C-3 

Routine 

4/2/2005 

NRS 

Wet Test 

Volume, 

Cubic Feet 

Final 

2933.00 

Initial 

2928.00 

Total 

5.00 

rlnal 

2939.00 

Initial 

2934.00 

Total 

5.00 

Final 

2945.00 

Initial 

2940.00 

Total 

5.00 

Final 

2951.00 

Initial 

2946.00 

Total 

5.00 

Final 

2957.00 

Initial 

2952.00 

Total 

5.00 

Leak checks 

Negative -

Positive -

Dry Gas Meter 

Temp, F 

Inlet Outlet 

Final Final 

75.0 70.0 

Initial Initial 

73.0 70.0 

Average Average 

74.0 70.0 

72.0 

r-Inal Final 

80.0 71.0 

Initial Initial 

76.0 70.0 

Average Average 

78.0 70.5 

74.3 Tm 

Final Final 

83.0 73.0 

Initial Initial 

81.0 72.0 

Average Average 

82.0 72.5 

77.3 Tm 

Final rlnal 

86.0 74.0 

Initial Initial 

84.0 73.0 

Average Average 

85.0 73.5 

79.3 Tm 

Final Final 

87.0 75.0 

Initial Initial 

86.0 74.0 

Average Average 

86.5 74.5 

80.5 Tm 

ok 

ok 

Wet Test 

Meter 

Temp, F 

Final 

69.0 

Initial 

69.0 

Average 

69.0 

Final 

69.0 

Initial 

69.0 

Average 

69.0 

Final 

68.5 

Initial 

69.0 

Average 

68.8 

Final 

68.5 

Initial 

68.5 

Average 

68.5 

Final 

68.5 

Initial 

68.5 

Average 

68.5 

>5W.C. 

> in.Hg 

Barometric Pressure 

Previous Y --

Previous Delta H --

t-I::lno:::~~ Meter 

Time of Coefficient 

Cal. Point Y 

Minutes SEC 

12 24.19 

Minutes 

12.40 1.0024 

Minutes SEC 

8.0 51.93 

Minutes 

8.87 1.0024 

Minutes SEC 

6.0 23.01 

Minutes 

6.38 1.0020 

Minutes SEC 

5.0 13.9 

Minutes 

5.23 1.0007 

Minutes SEC 

4.0 32.79 

Minutes 

4.55 1.0005 

Average 1.0016 

29.22 

0.9999 

1.8261 

Orifice 

Coefficient 

dH@ 

1.7624 

1.7992 

1.8568 

1.8655 

1.8750 

1.8318 
Routine BARR Dry Gas Meter Calibration M 

Control Module Number: C -3 Leak Checks 

Date: -:zr('i-Z -O~ 

Techn?c;an:~~A~)Lf,L~S~ ____________ _ 

Positive .,;1-

Negative "k. 

Orifice Dry gas WetTest Dry Gas Meter WetTest 

DiffPres. Volume Volume Temp (""'F) Meter 

rH2O) (Fe) (Ft") Inlet Outlet Temp (-;:,F) 

Nominal Rnal Rnal Rnal Rnal Rnal 

~C; /'/'/. loS- 2'133 "1S" '10 0'1 

Initial Initial 

1"3 

AverageTm 

'j 2-

Orifice Dry gas WetTest Dry Gas Meter 

DiffPres. Volume Volume Temp(-.>F) 

rHzO) (Fe) (Ft") Inlet Outlet 

Nominal Rnal Rnal Rnal Rnal Rnal 

\.0 ISV.lo7$" 2.13trt 90 II Ceq 

Initial Initial Initial Initial 

1'1 S".(.?S" 293A f{P 'lb 

Total Average 

-nAverage Tm 

I~ ,25"" 

Orifice Dry gas WetTest Dry Gas Meter 

DiffPres. Volume Volume Temp (-.>F) 

rHzO) (Fe) (Ft1 Inlet Outlet 

Nominal Rnal Rnal Rnal Rnal 

2..0 ISe:,.r3S :2.'1' 5" Jl3 7iActual Initial Initial Initial Initial Initial 

2'140 'Is' -12- <O~ 

Volume 

(Ft1 Inlet Outlet 

Nominal Rnal Rnal Rnal 

~,O 2crS-( 8'& 7'-1 

Initial Initial Initial Initial 

2'1t.j(o C;S L.( 70 

Average 

~SAverageTm 

11.2S 

Dry Gas Meter 

DiffPres. Volume Volume Temp (""'F) 

rHzO) (Ftj (Ft') Inlet Outlet 

Nominal Rnal Rnal Final Rnal 

4.0 ICe'&'.5?iS" 2.95"7 'b7 '1SInitial Initial Initial Initial Initial 

Z9S"2 ;?&i 'I 1'o'6,SAverage 

g-It"SAverage Tm 

g-O cSBarometric Press.: 2 ~ . 2 Z. 

5 in. W.C. Previous Y: • '191 'i 

15 in.Hg Previous t>H: IS2Gl 

Elapsed Meter Orifice 

Time of Coefficient 

Calibration Point 

Minutes 

{ .'(i"~1S' 
EPA M5 POST TEST METER CALffiRATION 

BARR 

Project Name: United Taconite 

Module Number: C-3 

...:;....:..----

Date: 7-May-05 

Tech: NRS 

..;;...;;;....:...---

Orifice Dry Gas WetTest 

Diff Volume, Volume, 

Presure dH Cubic Feet Cubic Feet 

Nominal Final Final 

1.48 989.860 3230.00 

Initial Initial 

982.800 3223.00 

Total 

Initial 

323l.00 

Total 

Initial 

3237.00 

Total 

Nominal sample conditions 

Delta H: 1.48 W.e. 

Vacuum: 8 in. Hg 

Dry Gas Meter WetTest 

Tern, F Meter 

Inlet Outlet Tern , F 

Final Final Final 

81.0 74.0 

Initial Initial Initial . 

78.0 73.0 

Average Average Average 

79.5 73.5 

76.5 Tm 

Final 

75.0 

Initial Initial Initial 

81.0 74.0 

Average 

Initial Initial Initial 

83.0 75.0 

Average Average 

83.5 

Project No.: 23/69-948-TAK 

Barometric Pressure: 29.07 --....;...;..-'-'-

70.5 

Previous Y : l.0016 

Previous Delta H : --:-1'-'-.8";"31;;";8-

Elapsed 

Time of 

Cal. Point 

SEC 

Pre cal + 5% 

Pre cal- 5% 

Within 5% YIN 

Meter 

Coefficient 

Y 

l.0517 

0.9515 

YES 

Orifice 

1.9234 

1.7402 

YES 
EPA M5 POST TEST lVlETER CALIBRATION 

\··BARR 

:/ 

viodule Number: _~t",--_3==--___ _ 

Date: S--l-CC) 

Tech: N{z...~ 

Dry Gas WetTest 

Volume, Volume, 

Cubic Feet Cubic Feet 

• Final Final 

\,'W '1?1 Si() 5230 

Initial Initial 

'1~z.'g ~2.23 

~"2..~( 

Initial Initial 

c l'-'! G ,crt.! ?, 23 " 

Total Total 

<::),C(..<;; 

PTe Template 

Nominal sample conditions 

DeltaH: 

Vacuum: 

1 ,Lj ~ W.e. 

6 .. H _-,,,,-__ In. g 

Dry Gas Meter WetTest 

Inlet 

Final 

'51 

Initial 

7g 

Average 

7'1S 

~3 

Initial 

&! 

Average 

~2... 

Initial 

'53 

Average 

S'3.. S" 

Temp, F 

Outlet 

FInal 

1<-( 

Initial 

73 

Average 

l3,STm 

Final 

lS"" 

Initial 

i<1 

Final 

[0 

Initial 

is-. 

Meter 

Temp, F 

Final' 

70.SInitial 

(0.<;" 

Initial 

'70,SProject No.: 23/0'7-'11:l.8 

Barometric Pressure: '7 '-I ,0", 

Previous Y: I. CO I Ie 

Previous Delta H : I . n \ X 

Elapsed Meter Orifice 

Time of Coefficient 

Cal. Point Y 

Minutes SEC 

iO 
p::::mmmUk : lcJ -Jlt c a" " J-r SmplLoc~1 ()L ~(.l.>·c"'~('C/ 

Date .; / C; I t:>"~ 

Operator')'~k 1.51 k 

Runs 1 - 2 

Pitot No. y_ / .m 

SM z... 

Test No. 1 -'---

CM J 

TEST RUN 1 

Metery &. '11 }'7 

lIH@ /.00<1., CP~ 

P .?.... 

EPA METHOD 5 

FIELD DATA SHEET 

l o ·""0 Bar. Pres u, '7' In Hg 

Stat. Pres '1e:::;J D In H20 

Probe Lngth "/ It 

Liner Type: J'l'Glass OS.S. OOther 

Sample Train Leak Rate (efm) 

Run 1 Run 2 

pretestf) 0 at 151n Hg Pretest ;."\. "'':. at 151nHg 

.' PosUest", ".:.> at q. <> In Hg PosUestC)..::> at ?J In Hg 

Pitot (3 In.) Pos.[=!- Neg.Q.--- . Pitot (3In.) Pos.lid"Neg.OJ ..... 

TEST RUN 2 

Sample Sample Meier Velocity Orifice Train Slack Sam Ie Train Tern ,'F Meter Meier Meier Veloclly Train Stack Meier Meier 

Point Time Volume liP, L1H, Vacuum Temp. Impngr Inlet Outlet Volume LIP, In lei Oullel 

':<I'P'" 

\t'6 tY 

~yVJ, 

LIT Vm, It" In H20 In H20 In. Hg Ts, 'F Probe Filter Outlet Vm, It" In H,o Temp, 'F I Temp, 'F 

; L'U &1 8-7. I <f"Y 

nj[L{i;V'l) I o,'}~-I.2II,.;--lgyT-7'b I

m

7'(X: r·.z;r()T~t,.I-k ~ jU-YO II ffn(..'>tlo.L() 'I'l~ ~\ W ,;) I,!)-t-- I (, "V" ,.$"/1 '/l.../ I 9 '2. ~e, 

/5 lll{':IJ\>'l rtJ;W-IJ,:Jfl-s-;·;-T?~1 'C'""lI1-.fv 1 f.?Y? 1,1LI,f"')JI~71)+l19.4' 1~''iS''1I-~!f~ I '~1... I ~~Io 1 "5';-~I'-4-L.1 ~~ I n 

2/..{'/ 

t-t..(!l 

2--'-( / 

'2,1 II iJ("JfiTI/J:'-l-~T 7/ycJ-1.'r) 17g 1'0L-t''tz-1 'l\rLI Ii::> '3 ,-·4ljI0 I T-=1 Ih~L\I\ 1 0. 'id .7-Y-llq(p~·/1 0.'7'1-1 ti.oj 1 ~'.>I 't)Z& 17",~ I o·)\I~-\.I-'bi~I't1-II.5«(J'051D.y~ 

Y5 'II ~ll.\P 1 {If S'lt2J ),0"1]'6.0 .1 ... 7"1 .. L?i~[;L~5=[J~[]1'LL5,·'{_lIsq6:z.,fM2.L>-D 

~I t.1-x.IJ I (j'(I7~ I 'iLL\) I 1ij<[7~L1..~~~-T:~-\TL?3 Jq~J(0"t~Lsrg,i5Jc)·_,tq 

l11r;,ntl~iI./).~;;;1 \C! '0 I "1,'; I '7 I c'/ll h;(o I b£ 1 9lLZ31JI~}.c.. Jb~;~~ 

'1 <. II i.-t~/, 1) !c)_"9l I ~;~ "J I '1 J 7"7 I? It L\ lid (L'\' "1& 1 L 'ri.~L2,~~_II~?'7LI61 \"-L.1 

(1)" Ilqyr'Tb~ 't 12 (/1 I.-"l I D 1]7 L2in~ I. ~,~L{p '3 1~-.2Lqj '1I.ss;~LQ.6{) 

({:r-lltt,~c,s,lSll? c.,(h I Ol·<t>YI (~.{) I 7 ~ 17t(rI2TTI--Z;-~ L.yLL~J[21O(() JtJ.$"? 

Run 1 

Run 2 

MOISTURE RECOVERY: 

Imolnaer 

Final wt .. q 

Inltlalwt .. q 

Difference 

!rf 5f';';~l fIiJ'L'u 

DJ'{ \ -;t,) 

Inillalization Values Test Run Times 

RUN 1 

1 2 3 4 Desiccant 

C{ 112 I I fl.) fD (p \/ f6/L.-

Iv) {;t5 ( b) " tft>jV 

7 .. ;alv~'C:\ 

(2v l '1, / 

- S-L~4:s 

-).,$7 &;7.. 

2.."~ (;,.. ) 

ORSA T System 

cclmln' I 02 

8ag No. I 8ag Vol I at 151n Hg 

Tolal 

Ih'~I~:'~.,~;;;;):): 

Sample Train Components 

. N'02'LLE 

~ A L IP>R N\\O N 

t 

Air Flows Nozzle Calibration 

Tech. TI) it Date .. ::;1::/1\ S0.·<!y~ 

2 0,. L,:?;!· 

3 G>. <-;7'/ 

Avg.ln. I c:> r '2. ,0/3> 

./ 
EPA METHOD 201A 

FIELD DATA SHEET 

Project \5lc,--,c (,u? CM ~ SM....1-. P, 5' Pitot No. p11{ DlI.-' Cp 6, ~ sf Sample Train Leak Rate (cfm) 

Sample Location G! \.-'lk.- <i>lfo'-(R'~/I- Metery D·C(L(b Bar. Press. 1-g.CeD In Hg Pretest ~ at 151n Hg 

Date S" /?/Y) Test~ Run _1__ ,-Orlff. t'lH@ • ~el'~ Stat. Press. to. <:>CJ Postlest ~ at >" in Hg 

OperatorSlt)lCI :) f\ Y- Eff. Probe Length _50_ ft Liner Type:O Glass ~-S.S. 0 Other ____ _ 

PMlO Pre-Run Data 

t'lP Min (:).0 I 

t'lP Max b.I:L 

t'lH@Avg. Ts Q7'l 

t'lH@ + 50 Ts 0, (o:i} 

t'lH@-50Ts O. C6lSample Dwell Sample Meter Velocity Orifice Point Ideal Sample Stack Sample Train Temperatures. of Oxygen 

Point Time Time Volume t'lP. t'lH. Volul11e Meter Vacuul11. Temp. Probe Filter Il11plnger Meter Meter Content. 

iii Vm. tt" in H2O In H2O iiVI11. tt" Volume In Hg Is. -t- Outlet Inlet Outlet % 

I ::';~:.<.,:.;~'::' ··";:;~U.(;:i·;;;:l':: (/1.p I 'b (101.'to 1~1~¥~if;ll':.:':'V';!:i ;~';'{"<il'i7,i':): i\~:ih:l;j!t.[!I.·,:;. I';:·,))!::; i.i :''.i:',,::,~,:: I,' if".,';)]':; 1:':':";,:':l:\H':l"~,; ·;··:'!::';':;'·:.·;:X;~:;;'i r, .. ;;:M:;'.:.;·"::· .;·.i(:~:'S.i}i~i(b 2Ii,I;;,l,Li;'(i.: .S',k,;:"',.:· 

()7 ~/) c, .. , 5b t.( PI> D·D> o.9Y ""- - ? ~ 51S z-; .... '2 'i r 6 , 7'3 73 ? "'. '1 

1- It>') I Z •. \.. }"'~. "-I O,D> <D.~ L ~ .. C·,:; 't81 ?'"Yo" ~~ 51 7~ IL 

\ (;", L 17. -v 3/°."[", 0.0'2. h~1....- -- '2,,,;,, '-!cu_ 2 \.(') 7 YD ,n. 7~ 7 -:5-

('} y.-/, ?-::>,4 ;,/ '-I. q+ L9,c>~ 0.1'-1 -. 2·~ 51'2. Z'1 ( '2 'i C. /41 -IS' +? 

L 7.'7 OZ;" L "J,(1,. If ~ (),c'1 1J.~11f - - '7..<'> .5("c. ?y r?J;;i :;I. b'tv 7(p ,.> , 

1 5, .1.. ~1. '7 Il(. (u h 0"2 O'_~.t... - - <t-", 4"Sb 25( II C?( ~p\ 78 7':::> 

I) , <?J-. I L/~.";j I yz.'S. I I C> ()y- O,"W,N ...... - "Z .... s- t" .... .5 l.. vi-=!- - bt> 7~ 7-> 

I. ~ .Cj sr-'i ~1.qHr- D,~L:. 6,~;"':; 2,0 S·~( '2.. 'I~ z.e-1. (,.,Cl J..~ 7:1 

I )..1 (,7..,1 3'.s3Yt () ,D Y D._'jy -' .... '2..6> )- 't'i. 2.'1'.!> z \,,,\;y S'1 .,.. :+1 

f'r') Cj ,f..p 12. '3 11">~p" ().D~ o ."I-..'L t..-> 'f9.Y '--YL vI (" I .. r -=tV 

1. {1).Of V1 l. y.l1.J''!! Cdi' D.'h __ .~~ -- L.b (,,"2.. 1~vr 1.. r "L (,.,0 1-<1 :rtf 

I ....... - - -, 'Z5'" t.. I '7'1 7'c( 

. KlDLl- L E. 

C. A L ,l?:>R /V\\O N A l/ .(,f'f) 

\:"::;';');'1':1:,:' /!:::: \ ji;t'. 1:;;:,iiiri.'1g'/:; ;";:;;·,:1,1':,',1;;;;:'. ',{;;;J"):;, TI11=' Ij:(:·\;·J:;\\'.'I(i~\ 1 In 

... • .... '1 ......... \\..1 

Nozzle Calibration 

Tech. Date 

Nozzle No. 

1 b ")I'\l> 

2 (0'1'10 

3 l:> • .~" 1) 

Avg.ln. l:> ,''\ Lj () 

.5:5~-) 

(cf!>'i6 

s-:n~ 

') 
BARR 

em • 

Project ",,,,:\...1 1"q"..,:1 .... 8mpl Loc Gill ... f C u.s 

Date 5' -1. ~c. '\ 

Op.;rator D'S' I, 

Test No. 

IL 

Runs A. ---- Pilot No. S ~ 1 ' 

CM C-L SM L 

Meter y .913 1-

t.H @ I. Vtf,9"') 

Cp (). "'Y 

Pr:. 

EPA METHOD 5 

FIELD DATA SHEET 

Bar. Pres l~. fu In I-Ig 

Stat. Pres I.e. .11 in H20 

Probe Lngtil s: II 

Liner Type: OGlass ~ OOlhar 

Saml)le Train Leak Rate (elm) 

Run 1 

Pretest b,c. 

Postlest 

Pilot (3 in.) Pas. 

r.= TEST RUN 1 II TEST RUN 2 

Sump Ie Sumple Motor Velocity Orifice Train Stacl. Sam Ie Train Temp, 'F Metor Meter Meter Velocity Orifice Train 

Poinl Time Volume liP, Lil-l, Vacuum Temp. hnpngr Inlet Outiet Volume liP, LiH, Vacuum 

/IT Vm, It' In 1-1,0 in 1-1,0 In. Hg Ts, 'F Probe Filter Outiet Vol, II' In H20 In 11,0 In. I-Ig 

, ""i 'r', ,,' ,.' "cg:z"" ' .. ':;. ","',,' ,,'," ' ,,' "" ".', ','" "', ,,' ,"," c',.', 

Stad: 

Temp. 

Ts, "F 

swnre Train Tern~1 Meter Meier 

hnpngr Inlel Oullet 

Probe -:::-1 Ollilet Temp, 'F Temp, "I' ;',1, 

A-lto 1, .~C.OC\ \.("t. ~.) co/r ZYf S'~ rio S-y 1()~:\-qIL,).IJ I~'l..- yo. ~{f ,'If.:. S"'t ~~Q 

5' ~ 11.~1 () ()i- I._"c::.:i.c 5'''1 ( 2f'::' Y1-5""iS Sr J1Cl.I...~ I~.",'t 1.tIi '-'/,o fo1o '-Y"f sS'" -"3 ~,~ 

I.( '2('" ~).II o.(q. 1.'2' ':\.~ (....,'- 1..'1'-1 'iCe, lou s+ lI'li~Z. t.~~ (.'i( 'Z.~ l.."-'l '2.)0 Sc.... ~~ 

j .nu'_.'+'1.tLD.e:.\ 1.'1v J .. ~ Cl~ 'Z Y'i v,'" (..{ sr )13,~"Z..1(J.1)6 1./0 ~.D 61/ 1YL flo .l.L 

-z. 'l.' _,10.0 " DP'1 D.1-1.. ~.' ~c.<" ~ Vi 'A ,,"'- S<' /lOY 0.010 1.10 1'1." bY\ ' 111 r1- ("t;. IG;~ r 1),,0. 3.t.~'b ~b.~lp ~ . .,:) S'81 2Vv. '1'6 Co1- )"l.. II{.,Sc.. 0.0'/ 11'\.':11 'L.S- b2.c;, 2 Y9 '\~ :C-.7- c.:. r~'*~ 11.)-T ~g.·O c,oTlrI, lr"" }'!:.u ("''1/ "2f1 SD b'1. 51- 11I1.~)D.DI.o l.cy 2.\ G~'1 7.tter ~~ loCo r. :--S. __ 10.u_.~o.c~ ,.51.( "l.~ Cn'l.~ '2\{'i St -l;v S-:r IIfQ:l<6hCotol.Cl'3 "2''- - .- I -~ 

--.!:L 1.1,(" .'6l.,,\ 1- to. b ~ I, ') 1. .3. '\ '1- Ilo J ,y C; ~ c.. ~ r oS r 'to'~i!t) l\ 'l. /.::''1- 'J ~ t)''> ~).\·_~.'o'i j.S'i- :1.r- l,Co~ '2<)~.>3. t..Co S"'7- 121.u G.o'-f 0.101 ~ 

l 1~j{ 1<i').1 4- 6.0) l.z1 :J.t::> Col7 2 'Ii ~ 1 b 1- S'l 11'>.2.(,., o.~ O.lo'+ ~ --1.. ,,~p ')ff:..CoI ~.().,. bjJ..G> 2.\ Co<OL 1.. fl f 2.. c.+- r)( l.'1:zy o~ O.~t.. .. 

,

I.("' .. c. :1,'2.( 0!,b 6·1.>1 /./1 3.0 }t:>o 2~"'" s'7(P(,. S4 Ill'~\ c>oq ".V~ 1 

C )CC. '('1H'Z o.o\( '.'P...iJ 3."" 7-c~ z '\" ,t"'> tpfo 5~ 1"21.~~ O.~ 1.1-, lJ I If 31.f\ ,\c .~L t>. b 1- J.e:. \ .l.u +~, Z 9Y ~'r 1e.l \1 12'l.VQ b.U- 1... u " .. 

\ 1£1.;:,.'-'> ~ f:}.t:.r l.'2..r 3.U ("LftI 2.'1'1 s!> Col( (.,.U 1~l.n O~u I.'\~ j 

.1. lfl.( I_q'l·~\ O.c'r" D.~q ~.\ Cny~ 1..'i<{' s3 (,1- ~I.'l (31.1~ p.C.C; '.4(" -:1 , 'f5·'> ~r.t:>3 D.t:."1 b.~q 2,0 c,"f2- tvg '\'2- (,,':\- l..l:) (>'(.l«, b,t:.-) O,'6~ 2 

_~yt,( 11(,.. .... ' D.c"\' 1.':>1-1 ).~ '<jr;'-( 2'(u 5C> ~ t;..b 1116./'- D.n 17.17 '1. 

. N'02'LLE 

C. A L iPJR 1\"\\0 N , St.,C> I'IB.II o.elo l.f<... 1.0 ~o 1... L)\ r I ,,1- ~~ Inlf,."'''' D.ot t.)'i '; 

l( kl.\' Cf~.'fL b.b ') o.'K\... 'l..{" Ja$..~ 'Z.{\ >'L ~ (aU /)9.1.\ G~" 1.~1.-:) J 55' . .:> /t:>:>.i'j o.oL ).:.D :3.'" 1~1< 1 fu )1 t...-=t- Cub. ,'/I.t., c.c)~ 1.,,\ J 

1. $'1,'; IC2.Zt Oll:>.~ C.ct<\ >.~ 3}'6 '2.'("'> r> ~l- C 1:1 1/'{2.'~1:I O.()1- /.1'\ '1 

, ~ :b.D 1~I:i~i~c?~:PJ .\~: ri)" '1.< T::(:t~1( '2 '{~ C> :J':~f Tmt.~l ~:~\1; ir~;;\~I~i\1.' .?}~IA "2 

1 

Initialization Vailies Tesl Run Times ORHAT System Sample Train Components Air Flows Nozzle Calibration 

Meter Oxygen Moislure cc/min' 02 1'1-1.- O.LIlI1 

Temp Conlenl Content Slart Time End Time Box No, Bag No. ilag Vol at 151n J-ig Reaciing Filler No. Nozzle No, Nozzle On ACFM DSCFM 

RIIII\8& \ --.tl.- ~c>.~ (I.--\- ,t[()b Ho\" ~~ ~ C.S'CU j~ltrt.~~ FlIjfl~~"l,. _vQt .. ,C\__ ~_·_L __ J)_'i'L Jl\)~ ________ '/btO'I" 1"'1-1- 0.'11 .. ,\ IbUt) Yf. fq~ 

Tech. e'tK._ Dale ~ ~ l·';" 

Nozzle No, • ... 1'(*1.. 

1 An;.<t.h () ~~ 

2 ~;:'(JHt" 

MOISTunE nEGOVEfW RUNtZ 

hnpill~ 2 3 Desiccant TOlal 

Filial wi, IJ j.G=1..q~ 11I'l.. UJ~ lO\(, ",.! >'" 

\';:/',;r, :,,\;,' .I,! ':.' 

Initial wI., L- 1\)0 N' 11>0 ca/Pi ItC<\ ,.'!,;:,." .,! 

;', ','" '. 

DilterencE: ... <l "l.. -[ 'it \ 

'~. 2 --"--I

RUN 

'I ~ 

q~ I~-+~~f~~-~~ 

~) -1.~~ ..1 

Avg, 

3 

In. ~OJ ~~~ 6.11 -
:,' 

BARR 

p;o]ect (Ah;-\' ...... .L 14~ .. ~h SlTIpl Lac C..,... 1 Col) S 2. \ I."'"L Test No, Runs 

Date S' • .:1 -t>o (" 

Operator Q j"JLUM 

PltotNo.~ 

CM C ~L SM ITEST RUN 1 

Meter y D.q (\"3 1-

£'ll-! @ r.~jJ 

Cp C. '3.,. 

P r 

EPA METHOD 5 

FIELD (J!ArA SHEET 

Bm. Pres 2CZ.f.,D In Hg 

St3!. Pres _<>.c:f\ In H2O 

Probe Lngth ~ It 

Liller Type: oGlass '!i(IS.S. oOther 

SmTlple Sample Meter Velocily Orifice Train Slacl< Sam Ie Train Temp, 'F Meter Meter Meier Veloclly Orifice Train 

PollIl Time Volume LIP, lIH, Vacuum Temp. Impngr Inlet Outiet Volume LIP, £'ll-l, Vacuum 

LIT Vrn, II' In 1-1,0 In 11,0 In.l1g Ts, 'F Probe Filler Oullet Temp, 'I' Temp, 'F VillI fI' InH,O In 11,0 In. H9 

, ',;',:,' : :::;' ":,:' IW:>·~ '" ,.,", ' "",.",,' ',' ",:,<." ",",::'1',"'"" /( /::/! ,t';""!', :':.,:,;1 \:\'<':I".:~; .:,(~ I,!,"',',)" lI5.1¥ i,;, "::':',"!" 'r\:'~' "':.t.;" ";', 

,q .. ~ Z.<' I HW:n. O,D -z.... o:~ 1 2.) !.f/L 1.'IY '1 Yif S'~ "s- )"r 2.11.$1. O.i::>y 1.(:;,6 '3.0 , $' $,0 '/r&> .t.~ 10.1:>1.. 6.<6'> 'l.' "lev, 2.y~ UL ~ SL sr 2l"l.(tl 6. Q .1 (.'Z. Y :a." 

'-I )-, .;- 19,~.1o 'l. b.b'l I.t{ 1b 'I.Q '( l.Y'1 Z't"J '-I~ S1- fy ,'lcS1' Doe3 1,1 0 ).4) 

l /tllb i/f&.?.o 0.03 /.1.'1 ~.D :l9f' 1.'1<' t\"o 'iCc. rCJ ~ Ul.1.Z b,DY I. S! 1- -:>., 

1.. )l,,<" 1~lNf 0.0'l.. 0."61- 1.. 'S' 1ft 1- 2Y'1 tS'" 'I~ S''l SS" ~2t.t.1- £).1::.,) I.'rl- 'i.;:. 

f ,$/1> 116'6.\01\ (:).c Z. e>. ,,)' "2.) :39 t 2V~ l,(q !fl.,. ~ _ys l1(·'1'5 D.I'::l2... ().<:t.b 1.) 

()rG It,(' 1'J()·1~ f) .c3 I. t<& l.b 38,6 Z YL "'l. r. VI.::. Sf( -- 'Sf 21':\.Tl.. o.o~ 1,91 L/.a 

S ~ .. ,<> /ql. i \ 0.(:')') 1.1..b I:\.D ~/«! 1..'/2- z. V'l 'IY ~ r-~ 1.1't.5 I c.o Cb '3.1 I .5 

'1. l1.,\ IliJ·l.1 D.c~ (). <f..u 2.\ '1'f-.J L<{~ "lfl. Yv (,.}:J ,5(" 23Z,~(Q b.elf .1. S'~ (.. 

J zO) I~ft .11. ~.i> Y ,:S '6 3,~ 'i')Y '2.. Yl t... Y<t YV '( rt.. ! z.),-I.o<c. D,t:>.,.- 1.. "'.:. V 

~ l'}i\" IQC,.1o c.c,,! t. 5~ ~.) 'trY 'Z. Y"f Z $'1 'f'{ lot. n .. Z3101S- 0,06 t.'!:.9 5 

t t o.1> (q,& .u'6 e>,D'1 /.6'{ 3. L> t.f'1 0(" 1. 'f~ '1 ye, 'If.( I C:, 'Z- ~ 1.}t.l"- 0.<>3 1.'2.) J 

c.. wfa JI.f:- 4 Cf"1:W ".~ I.Co'3 J,b vi«r t.1fl( lYe. 'Is G:>( SL t3Cf.j'Q b.O't 1·14 3 

;[ .15.0 Zcl.tct t> .0> 1.2,"Z. >.t>o ft(fl ~1(1 l t;r.:> 'ICs:, (,,1... 5tc. '2'11. '-01 b.a s- '2.Q'--/ If, 

"I ~1.\ 1 lD) ,!) \ o .t>'1 I. '5 I .3.) S~o '2Vr 'ZSb 'it,., (.,3 SI,.. 1,{J.lDo O.b)' I. «, '-I. 

l 1,/0 ,v loO'i.{ct. () .t.J I.I~ J. t:> \/~ 1 'lyj z. ~.., Y1 (p3 S'-" 'l'l~ .'t, ~.t.. '1 I.("b '1 

z. "11.,\ 1010,10 b.D) (.rr j.~ If':}ol 1.. I{ If z ~.:. '-/7- (.,y '$'1-- 'l...vl.b l.. 6.(:)3 ,.ti- ll. 

( t./ fit> ~b;:U b.b t. l):" Y t.' VII tyt.-( 1. Ylf. ~1 (py 5'1- 21(~.3 s 0.0'2... b. -=1 cr ,; 

o~C::. l{'J, \ {e.l.fI,~ b.o 3 (.1"'- :!:-.o 3<6.) 2Y'l '2 Y'1 q1- 1..3 SI6 2'11. ~ D.{:)~ 1.( ( :!.,~ 

$- )0,0 t{t>.\t.i t>.c1... b.'\,1. It.~ .Yt~ ~YJ, l)~ L(j (..( 5"'" ,<;1, "II) ~,i) Y I.~~ (! f~ 

'i '5:1,\ 11\1.'i1 b.,tH. I). i> '2. "Z..{ Yl~ ~'I..':f.. ~ yt{ '/q leo I".. r( lz~}.'1<:. oJ> r IS'\ 3.' 

-~ S r It) l\t."\t. 'O.t:> ~ t.1.S .l.b '(ly l.n z.,i> t{q (..1- S"f\ t~'(.~7... /:j.~y ,. L" >.\ 

L ~ ..:tl( 21f(,1..~ 1>.<:.1.- i) .1S" 1..( Yi.<t 1.~l.. t<:c. r v ~ loU L,!c.·1'> OP"L.. o.(p(p 1. 

" f.:,i),U Z\C;.I:)~ IO,b?.. (), 'f>~ 1..$ 3'1.1 '2- v ~ "t ~'i' su 1.0'1 Col:::. ZC;1.t/{ ().()'L o.te'\. b 

I':';;' ".' ef= vmJ<:;.\l ;":",.,, . 

,,1-1= I" \ Ts='f31. f -- -------

,'c!!'·i"i!!(i'?'.( TITI=)/'f,& vrn=I.{I.\d 1\'l~:~:Jlm',\;. lIH=I.~l 

- Initialization Values Tesl Run Times ORHAT System Sample Train Componenls 

Meier Oxygen Moislure Gc/min ~ 02 

Temp Content Conlenl Start Time End Time Box No, Bag No. ilag Vol al151n I-Ig Reading Filler No. Nozzle No, Nozzle On 

RlJn~ • Sl\ <,0,,,,- ()·S O~J.<'> 09 '3(" !lolPI.{~ Jf.t,- -z.. u. ';\)0 

Run 1> t .(o.~. 10."\ j).7 Jl>J'b /11.. q, 'ID1.0~1- I b-'1.- O.~I» - MOISTunE nEGOVERY. RUN3 RUN 4 

Irnplnner 1 2 3 4 Deslccanl Total 

Filial WI, 9 qa. IO~ I~\) 1t:.{P\Q 

Initial WI, 9 lui> I\)"" ( ,,,) .AI f\-. i:i'~:,;:);\il~t! Dillerence -~ '3 ---~--- '~_:_l _1L 

Sample Train Leak Rate (dill) ---- Run 1 Run 2 

Prelest O.D. al 15 in 1-19 Pretest O.D at 151n 1-19 

Pastiest 0..0 at 9 In HU Posltest6·o at (t'\ In Hn 

Pltot (3 in.) Pas. ®Fleg. !Sir Pitot (3 in.) Pas, I1tNe,,\E-" 

TEST RUN 2 

SlacK Sam Ie Train Temp, 'F Meter Meier 

Temp. Impngr Inlet Oullel 

1'5, 'F Probe Filler Oullel Temp, 'I' Temp, 'I' 

' I,~ '''', ,'.:. ': .' ' .... t,'";,, ' "·r, "':,' , YSb "2. "Ie.... "l 'I~ )S- 7" -ce- I.f'l~ '2.-n 1 '(u J'$' ~ -~ \j~n .. t. !1~ l j'"...> 5r f.1..( ~ y~~ 1. Y£:,. 2 fb. ~1 --lL ~ V9"L 2 Y'I l/.::. S~ _lL.. 1-Q 

"It(' ?.'i~ trio:> 5"1- ~I 1z. 

rt; 1('" "2-YL z. I!.'t( is" ~b .iL 

. N'D2'-z.. L E 

C. A L If?R N\\O N 

1 

Air Flows Nozzle Calibration 

ACFM DSCFM 

Tech tl3t..- Date~' )..j)) 

Nozzle No. I b'" 1'... --

2],$i 3Zl H$: 

':).') t>11o 11- II'" 

1 ~J 2 -D:~O 

3 Q.bD~ 

Avg. in. o <5!W 
Project 

Smpl Loc 

Date 

Operator 

. \\... , ~ ., . I \ -'" I . I '- ." "\1:'> \ 01.(.- '" \ "...... . 

(v.""k (..i"P\$ t, (!>~. fL) Test No. ~ Runs.-L.:...l 

s- Z - ".)" Pltot No. 1../- I 

-~\bl< / O;i;.·t?"S: /"1. "" CM -") :" SM ~ ~ 

TEST RUN 1 

Meteryi' ,,:.,:.; I., 

t.H@ ,. <2)1 ~ 

Cp~ 

P :.....2: 

EPA METHOD 5 

FIELD DATA SHEET 

Bar. Pres Z S. :;v In Hg 

Stat. Pres . ':: •. t~~'j In H20 

Probe Lngth i It 

Liner Type: GJGlass OS.S. OOther 

A W .' IU 

Sample Sample Meter Velocity Orlnce Train Stack Sam Ie Train Temp, 'F Meter Meter Meter Velocity Orlnce Train 

Point Time Volume AP, AH, Vacuum Temp . Impngr Inlet Outlet Voluma AP, AH, Vacuum . AT Vm, W In H20 In H20 In, Hg Ta, 'F Probe Filter Outlet Temp, 'F Temp, 'F Vm, W In H20 InHaO In. Hg 

,;;.ii';ltl;~jn'l.W. l'i:::;'{\ii\:i:iKI'\:'W '-fl..l, G ~Ii,%)l\i\\\"ti!.l?; ·!~~~)!;i.'N:!I:I",'J 1.lfiMlitl:m::{,ii:: g·r~;l'\V:i\hA'l.'AI )!.ii\)j'!~'!,li':I::Y; 11:)(~I;(;j:S::\!.%: I ~,%'i!i!;.;'r,I,; Ilii(Ci7i,JI;;:y ~{(; I. '"i li'!·:':!)I",:"I·; \"!':Hi\:1 f';"!.il:",'.,I,\,V '!.ll;,'·,'I'·\I';, 

f) ~I ';' t(15:<'c ,il /<:' j ,~{, - .J /.';;; /1./0- 2>"'- .? I J Yt' s;J· Y""/ Ivr;,v'.J;b 1,7u /.2.7 J> 

! ( .) t.{zCj·n ;> ,.,)-0 I, <;: ic. 9::>- J ~~l {.t., \.(j' 2./1 ~"0 ,'(v '-11 r{~«C.l! I. 'I~ I' <11 '~y 

I I,)' t.j !;(. t:.i\ II "/ ::. j, liz. ~. > /3"7 .2 </2., <'loS (II ..sf .~-() y~, GIL i,';- I, ( > ;J., CJ 

r ~ 2'" ·(J,~.I /, it.:, /, "')'1 .. ';'1'>"·' /].) 7 .. (v 7.J (:, .. /1./ sy .;s'. i qNJ( '7, (.:.. /'/!' "" 'i. • \j i 

L ., - •. <,) 11./3 q.J:J I· ';) ,.:, /.1/,.( .,), .:>' i4/(j i l{l.( Z..->J i-{t;- ..sZ\ ~:.;-I l(lw. (U -,; ... { I~J '-/. )' 

L >~ V/I.fl,).!:>, I 111 i,i':r .::LS" I~I/ 2--1) '1.2'-/ (/7 ..5'0 _'\'- (. 1'70(,' "Z, (j" /; (,'.~ y;.~ 

l) ') '.p,:) Lft{S Yj 'J. '!Iv i,/)) "I .J'~ ./99 7"/7.. 23} LI1- S'll .$ z., 1 '-(q:181. Id9.:.J I,)C, 'I· ! 

c.. l( .- 1..1'{9 .. N. I .. ,,) IIi :\ ') 

.. F"/~ Ji./d ~L~7G Vi- ..s ''\'.' ~. f 

...;, .... '1fJCI./ (,; /.1::; cj i'YY '7 

I Yl '(>/.15" i·{r. ,J:. '~.;. .J. .: I :r> Z v' L 7 J. f!J 3!v ..sIT ..r' ? -M. ') I. t/ u /,.:,<::.. oJ 

I) "7. 51) 'tY{(.«3 II"} d I. ( 't> >. c.. iJ.:r 7_ tj 'J l,Vb ;Jt:'1 ),V S~ 1./tJ Y, 'N /..sIJ /'J I,. .<7 

t .)S· q:" ,«'.> .. / 9.:- /' Vi.. Y,0 )t{O ?v'1 ?yG 's~O \./'4 3-;::: '1{1J.l7- t. (.:. D cl J ''7 

J '(.) ~ 'A;,III I t{.}G i·2-J 1,~) /Y't 2 '/...> ? :§-7 'It) (;,,, .!~ .. ) Wf·l,;;' /, 'I.J b. '3-; (, 

, 

J'v I"n,j't. -- ;i~1:1:'MI'i;:;)i;1: d=lo 0 Vm'~-u' 1·.·;il/t'\',\1J11,:;~,\\ AH= ,'.) I Ts= tn' ;> !.:rii\l~ll:\,I):\i( Tm= V~';>'\);? I ::'if;"kifi)?i AH=/,)/ 

(I) ~ I r: "" I 't . ( 'oj. C I e, I 10'. "" I ~. 0. Ll1: I It I \,.. • .. - . '" I / Initialization' Values Test Run Times ORSA T System Sample Train Components 

Meter Oxygen Moisture cclmln' 02 

~" - Temp Content Content Start Time End Time Box No. Bag No. Bag Vol at151nHg Reading Filter No. Nozzle No. Nozzle On 

-5,~ Run :t i"u t" ..: /e .... N\)·) . .9> " .-' I .~ ,) -) /<,r. ) o.((;2*'J7 Z ~(;; .. °-i71 

Run,#-' ''i h I lJ. \' /l,'j. 'tJ1 ' .. ;; [.> 1(,,,,-1 ~ L .. 3" () •• f rL4.. ~/(j t 'A. /' (i, C') f 7<; 

I 

RUN4 

.IL:) 1:;-, 

./'.1'; I Z I...::. 

. , 1'/ '), "V\ c ._. J. '/ .. 

Sample Train Leak Rate (o(m) 

Run 1 Run 2 

Pretes~~ . t:'. at 151n Hg Pretest (, . .:; at 151n I-Ig 

Posttestc~ D at ~,II In Hg Posttest (/." at (j In Hg 

Pltot (3 In.) Pos.G:3···Neg.I!l"· Pltot (3 In.) Pos.G'Neg.~-" 

TEST RUN 2 

Stack Sam Ie Treln Temp, 'F Meter Meter 

Temp. Impngr Inlet Outlet 

Ta, 'F Probe Filter Outlet Temp, 'F Templ'F 

·~:;:,ii\)ili'\:Y'.':i:i ·w: \,'11 Uir,til·'tl"·'; 1;'):ll

iiit!WIi:::',1 

/((~ z ijS 12 .>,~ 9'(,/ _L.r ..),- ..J 

/L/;~ ~ (I'll ?::!..( V .. J . ..[5 ;; ' .. t' I~I v 2"71 2 ],t 'I" ,'- ,'/ S'y' 

/3) J ,']':<.1 ~>.J\.. ·V.T ..j' q .. ,!j. ~/ 

/yG zV) 2..3.(, ~6 ,S'''7 sY 

! /../1) Z..JJ ,?]. l. L/7. @)cJ E 

) l',3 ") ?7 Z'S,) z/ .... ... ·-c ..'<;.'\./ 

. KlD2'2.LE 

~AL'P>RN\\ON 

t " ~ . . ~. t: 

Air Flows Nozzle Calibration 

Tech. Date 

ACFM OSCFM Nozzle No. 

g,,;~;;, t$ It(~ 1'1 l 1 .:'1 },]. -::' 

'}i'(,5/,;';' )8·0;}(I(. 2 (" ( 7 "'I 

'1 ......,) v 
BARR 

ONTARIO HYRDO D-6784-02 MERCURY TESTING 

FIELD DATA SHEET 

Project Vt\'\-\e~ \UL -"": tt CM ~ SM _4_ P ~ Pitot No. §"'. Cp 0, -r)'1 

Sample Location l/ W<:' s-'iru.(<. 51f C\.{\,. Metery I,::>:;>/G Bar. Press. 2f£.1p~ in Hg 

Date' .l{-~ Test ~ Run , ..... Oriff. &H @ 1,c"1IW~ Stat. Press. - 0 '-IS 0 

Operators '\ A- ttl::> M Ii"'\, Eff. Probe Length _>_ ft Liner Type\lL Glass D Qrtz.D Other ____ _ 

Sample Train Leak Rate (cfm) 

Pretest tJ .0.:> at 15 in Hg 

Postlest O.{)O at '1 in Hg 

Pitot (3 in.) Pos. ~Neg. >i3 

Sample Sample Meter Velocity Orifice Point Ideal Sample Stack Sample Train Temperatures, of Oxygen 

Point Time 

1'.1 

!,,:.·,{.~\;>i;.i~i: 113b 

3 5 

3 10 

2 15 

2 20 

1 25 

1 30 

3 35 

3 40 

2 45 

2 50 

1 55 . ~~ 

Filter No. ~Q OIM' 

Nozzle Dia. 0 • \0\ ').. 

NozzleNO.~ 

Volume L'lP. L'lH, Volume 

Vill, tr in H2O In H2O I'. Vill, It" 

CA"J. '\ ~ 1;····~·,·:::i(;:;i':::~.\(J. I:~,\;;i;.~i .. ;,' .:LJ;'! i',!!;;j{.!Sii:, 

fbI.) 1- I,~ 1:lJg 3.(0(.; 

lo!{.'ti., I.~) I. to ';} :Uoq 

f(>'&.1Y 1.'5~ I. CO 1... '1.~lo 

~ /7..£.0 S 1·<6S /. ~,. J. "\.1 

1Ib./~ /.t{~ I. '-11 ).'7r 

~Iq. ft{ ,.Sf> t.J't. 'S.< ~ 

tn.~b 2.(0 "Z..IY C(,(9 

i'l';j·'t>9 'l. ./ i) 'z..n. Vt"i 

+'}t'ly ~,t(o l.'-/f Cf. "1'1 

11fo,tp1 'L1'5 t.'!.'\. '1. Cfty 

'tlfD .1010 /.90 1,9 '( ')."l.l\. : 

':lUll ..... ..., , I"'J '" I t":f tJ II _ ........ 

.LE 

1\-",\0 N 

t ~ ()...1J.i17 flo-\ t:N0f \1... 

IDlfference I 

NJl\J~ C\.O\.. '\;. rv ~ ~ O· fJ\.., rv.· '\.. . ..,.\.. ,UV,o...., . '-' \2:)';'/ 0 . \, 

I 

Meter 

Volullle 

i.;,;:;li;'i;ji 

1ol.~~ 

:to.)~. t Y ~O~,IC 

'7130\ 

-;;I(o.'t'q 

121).b'L 

t~Y·'7.. ( it~.4u 

1-)~. <61. 7-31\)~ 

.,.'f1.1 't.. 

-:i\tJr .... ., 

I 

Vacuum, Temp. Probe Filter 

In Hg 1 s, -I-

\~';;;);;:;~;),~; ;i(':\.;i~d\;:~:;; :;::,.:,,'::;,.'Jm;, <i!I",',.;:.i,'}::'; 

If.S' /Clu '2.~ '2."lCf 

5'.1::> 139 <..S"r ooz:llt. 

S.<=> 139 'Z.Y"1 '2. V:3 

rs JltD 'l.'{!, '2. VV 

S.D IJer ..... ¥-z.... "L1Q 

)".0 139 -z. Y</' 'l.¥D 

&.0 I,\Cf 1.'11- 2lfc 

<0.0 I'll,) 'Z-'f( lJ"I 

fe..) 1>1 ?. Y'-( '2.. '-{Cl 

fc,.~ 1'10 'lY,( ZCf"L 

(P.~ I e(O ·l..Y~ 1..19 ,- .-:> /'!:>9 -z... Y i l.YL 

13.'1 '~y) 7....Yt 

( "1:> 7 ~l 1.. Y ~ 

I { <-'If 7.- y'''l 1.. t \ 

I 'iii> 7..- '1'-/ l~~ 

IlfO 'Ly'} 't-Y 'L 

/ '" i) l..VL 1.. yO 

1'10 'l..YC& 'LVI 

I ltD '-til.- ·?.->I 

It(D 'l.\(L '1. \.(0 

1"11> "\..'(1-- '\. l('\:.. 

I 'Ii) '1..'fb "l Y) 

(3."\ 1..,,)<.( "l.-I{v 

Ts= !,!'(',:;iJ.:\i!,·}:)':,!:i,: :i :,:'.,,;,:I'\!':~::ljj'::: 

and illlpinger content information' 

3 4 5 " 

100 100 100 

I 1 NI<CI HN03/H202 

Implnger Meter Meter Content, 

Oullet Inlet Outlet % 

:i.'ii~;"3,f\{\., li(!:!;;;li~."i;:~(2';\ I;ii.i,l·l',·;';';,,'rl':,,:#'l i;i::;:';~~:,'~,h':':. 

Co~ (0 Cf.. C!:J"6 1Cf:,.C:> 

~q '1.( b~ I 'B~c:::. 

S~ '}t. Co, I ~.<:::. 

G:,b '1« <04" I "/,vt) 

(n '3 1Y &:'9 t <'6.re1> 

(PS' 1S" 10:::. (~.'" 

&''1- 7r.r t'" I 'B,~ 

Cbl 1'+- 1-1 /Y,.ol 

tt,o 1-'1- 1- ( I ~,.;:) 

[of r'.j- 3-~ I~,( 

(d 11- '1( I'H ~) 1~ f'l- / V. .-0 

to"> f-'\- 1-t. IY,J 

(0"2 "1' 1L ('7J. ( 

lnY r9 "::}-"L ( ~-;::. 

it") t,., 71 i1 1<6..i) 

0S '19 +) ( '6.( 

Co) 11 j-1 • (<:(,./ 

~~ '71- i-3 I ~.() 

rta .~<l ,..1 I ~.o 

)~ '60 ty { ~.£J 

If;O <(,v )Y I <£J .. 

O 

tP{ «,1 1-V ( %.) 

~1.- ~v tV 

I;!::/',';:'\';:"" ::,.\'\\;(l~;:i Till = Ij",:·.:,~'!\i:il:::;~;:: 

6 7 Desiccant Total 

100 100 ~l1'~:i~;i1J;!~\t~~ 

H2S0411(MN04 
BARR 

Engineering Company 

Pitot Tube Number: 

Length: 4' 

Function: Free 

1. Are face openings perpendicular to tube axis? 

DYES ( go to 2) @ NO (go to 1a) 

2. Are face openings parallel to longitudinal axis? 

IiS1 YES ( go to 3) 

3. Are legs of equal length? 

g] YES ( go to 4) 

_ 0 NO (go to Za) 

o NO (go to 3a) 

4. Are center-lines of legs coincident? 

o YES (got05) o NO (go to 4a) 

5. Does this pitot tube pass all of the pbO;e I~ria? 

- j ibl/ t 

Technician Signature: //lL~I/Z I L... 

J 

S-Type Pitot Tube 

Geometry Check 

Inspection Date: I Z -2.{-04 

Technician: /\Jll. S ----~~~---------------

1a. If NO, is angle less than 10°? 

gj YES ( go to 2) 

IJo.; I 

--8:--~--. . - , I . . 

2a If NO, is angle le,ss than 50? _ 

D YES ( go to 3) 

D NO (discontinue use) 

~ 

.. -

-.:... : -- ---: --. - - I I . . 

D NO (discontinue use) 

----~-:J:-- -1;-' ..... -. -:",- ____ .::'l_ 

3a. If NO, is difference less than 1/8 inch? 

D YES (got04) . D NO (discontinue use) 

4a If NO, are center-lines of face openings less than 1/32 inch? 

D YES (go to 5) D NO (discontinue use) 

lRl YES DNO 
BARR 

Engineering Company 

Pitot Tube Number: )-1 

Length: S 1 --""'==::---

Function: e. 9 1 Free 

1. Are face OPenings perpendicular to tube axis? 

bQ. YES ( go to 2) D NO (go to 1a) 

J ~~ 1 

'-~ .. E=Ej-------

] ~ t 

. I 

~.~--I ~:~ I 

. 

2. Are face openings parallel to longitudinal axis? 

I2Sl YES (go to 3) 

3. Are legs of equal length? 

~ YES (go to 4) 

. D NO (go to Za) 

D NO (go to 3a) 

-k----~:"---*-)-----

4. Are center--fmes of legs coincident? 

123-. YES (go to 5) . D NO (go to 4a) 

-k----~~---_<--)-----

5. Does Otis ~trube pass ~ 'lY1Itteria' 

Technidan Signature: V V.. . L -- J 

S-Type Pitot Tube 

Geometry Check 

Inspection Date: ! -2. - L \ -(:'-1 

Technician: l\Ji'2..'::, ~--~~-----------------

1a If NO, is angle less than-10°? 

DYES ( go to 2) 

tJoj" I 

--~--~--. . - I I . . 

2a. If NO. is angle le;;s than 50? . 

o YES ( go to 3) 

r.$~--:::::'V 

-.o..:'.:r _____ -=" 

~-::: ,"""" 

o NO (cflScontinue use) 

I / .. I . I 

-- --. . -- -_ .. 

~ ! 

o NO (discontinue use) 

r-i'--~-V 

Lc ~ 

....... 

3a. If NO. is difference less than 118 inch? 

D YES (go to 4) o NO (discontinue use) 

4a. If NO, are center...Jines of face openings less than 1132 inch? 

DYES ( go to 5) o NO (discontinue use) 

E&YES DNO 
BARR 

Engineering Company 

Pitot Tube Number: 

Length: S \ r---··-:·~ 

Function: ~ I Free 

1. Are face openings perpendicular to tube axis? 

@ YES ( go to 2) o NO (go to 1a) 

I ~~ I 

'~~ .. i .: * . --~----- . t ('-..--.. I 

:-----~-! I • 

2. Are face openings parallel to longitudinal axis? 

gJ YES ( go to 3) 

3. Are legs of equal length? 

lS1 YES ( go to 4) 

. 0 NO (go to Za) 

o NO (go to 3a) 

-t----~'!----*-)-----

4. Are center-lines of legs coincident? 

I2Sl YES ( go to 5) o NO (go to 4a) 

5. Does this pitot tube pass all of thjaIDOVe;critena? 

Technician Sigoaru~ ~ ./t/~;V 

lid i L 

S-Type Pitot Tube 

Geometry Check 

Inspection Date: 

Technician: ~p-s, 

------~~---------------

1a If NO, is angle less than' 10°? 

DYES ( go to 2) o NO (discontinue use) 

rJ.i I 

--~--~--. . - fL .--11' -~~--. I I I . . . 

Za. If NO, is angle I~ than 5'? 

DYES ( go to 3) o NO (discontinue use) 

r-$~---'_-V ." ~-,,,.A 

3a. If NO, is difference less than 1/8 inch? 

DYES (go to 4) o NO (discontinue use) 

4a. If NO, are center-lines of face openings less than 1132 inch? 

o YES (go to 5) o NO (discontinue use) 

lSi YES ONO 
Engineering Company 

Pitot Tube Number: / -2. I,O 

Length: i I 

I$; 

Function: ~I Free 

1. Are face openings perpendicular to tube axis? 

'0 YES ( go to 2) o NO (go to 1a) 

2. Are face openings parallel to longitudinal axis? 

BYES ( go to 3) 

3. Are legs of equal length? 

gJ YES (go to 4) 

o NO (go to 2a) 

o NO (go to 3a) 

--k----~~---=<~)-----

4. Are center-lines of legs ccincident? 

IS!. YES ( go to 5) o NO (go to 4a) 

--~----~~----<-=)-----

5. Does this pitot tube pass all of the aqt)v!'l criteria? 

Mnlo," Signaw,e i'jl/I L 

S-Type Pitot Tube 

Geometry Check 

Inspection Date: i Z -21 ~O Y 

Technician: l,)fl-S ~--~~~---------------

1a. If NO, is angle less than 10°? 

DYES ( go to 2) o NO (discontinue use) 

~ I 

f3e- . I 

__ I __ _ _ __ . 

. . ~L --t!. -;.~--. , I I I I • . . 

2a. If NO, is angle less than 50? 

DYES ( go to 3) o NO (disccntinue use) 

3a. If NO, is difference less than 1/8 inch? 

DYES ( go to 4) D NO (discontinue use) 

V 

t=.--. ---£.,..-.i~_. 

4a. If NO, are center-lines of face openings less than 1/32 inch? 

DYES ( go to 5) o NO (discontinue use) 

8J YES ONO 
THERMOCOUPLE CALIBRATION 

BARR 

REFERENCE STANDARDS 

Hart Scientific 91 03-A sIn A 1 B289 

Hart Scientific 9140 sIn A1B086 

CaJ;Date: 

TRACEABILITY 

Temperature Calibraion Points 20 

Reference Deg F (To) 20 

Probe Temp (deg F) 20 

Reference Temp (deg R) deg F + 460 480 

Probe Temp (deg R), deg F + 460 480 

Difference (degrees) 0 

% Diff Abs. T 0.0% 

Is difference less than 1.5% at all 

measured points? YES 

THERMOCOUPLE ID C~~ 

1212212004 Meter In 

CALIBRATION TECHNICIAN: NRS 

DATE LABORATORY 

12/11/2003 

12/11/2003 

70 150 

70 150 

70 148 

530 610 

530 608 

0 2 

0.0% 0.3% 

1700~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

1600~~~~==========~==========~~~~~~~~~~~~~~~ 

1500 +~~~21 

~ 1400 t'-c:~~":1 <> .., 

~1300+2~~+===========================~~~~~~~~~~~~~~~~~~ 

::;) 

~ 1200~-~~~~~~~~~~~~~~~~~~~·~~~~~~~~~~~~~ n:: 

w 

~ 1100~~~~~c~~~~~~~~~~=-~~~,~~~-~~~~~~c~~~~~~~ 

w 

~ 10001~~~~~~~~~~~~~~~~~.~~~~~~~~~~~~~~~~·~~~~ ..J 

a. 5 900+-~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

o 

n:: 

~ 800~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~12 w 

~ 700+-~~~~~~~~~~~~~~~~ 

600~~~~~~~~~++~~~=-~~~ 

500+-~~~~~~~~~~~~~~~~~~--=-=-~~=-=---~~--~~~ 

400~--~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1 .5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: Te. ~ c..~ -l 

Media 

Std Used D-8 

Reference Deq F (To) 

Reference Corr Temp (deq R) deq F + 460 

Probe Temp (deg F) 

Probe Temp (deg R). deg F + 460 

Difference (degrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's function: 

20 

"20 

'-{ go 

2..0 

,-{gO 

0 

0-0 

c:..~·hn I I'v\ <:) c\.,",- \ e. i. \y~ fV\ I "-

If not acceptable, describe corrective procedures undertaken: 

70 

-ZO 

S"3C 

'10 

S-::So 

0 

0.0 

THERMOCOUPLE 

CALI BRA TION 

150 

( S1:;, 

&;{O 

(L/~ 

(008 

-"2-

D_~ 

@NO) 

@fNO) 

Date: 1,--2.'-.-OL{ 

Technician: -.:...N-'--'-"R.:.::"'--__ _ 

to 
BARR 

REFERENCE STANDARDS 

Hart Scientific 91 03-A sIn A1 B289 

Hart Scientific 9140 sIn A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

1700 --,.--,c--:-----,-,-~~~---=-~ 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE ID C-1-0 

Cal;Date: 12/22/2004 Meter Out 

CALIBRATION TECHNICIAN: NRS 

TRACEABILITY DATE LABORATORY 

Report No. A1B0718 

Report No. A1 B2024 

12/11/2003 

12/11/2003 

Hart Scientific 

Hart Scientific 

20 

20 

21 

480 

481 

-1 

0.2% 

YES 

70 

70 

~n 0:::; 

530 

529 

1 

0.2% 

150 

150 

610 

607 

3 

0.5% 

1600~S7~~============~======~~~~~~S7~~~~~ 

1500 +---'-'~~ 

~1400~~~ 

" 

~1300~~~~~====~==~~~~====~~~~~~=~~~~~~~~~~~ 

::> 

~ 1200~~~~~~~~~~~~~~~~~~~-~~~~~~~~~~~~~ 

~ 

w 

~ 1100~~~~~~~~~7=~~~~~~~~~'~~~~~~~~~~+~-~-~~~ 

w 

~ 1000~~~'~~~~·c~~~~~~~~~~~c~~:~~~~~~~~~~~~~~~~ -' Co 5 900~~~~~~~~~~~~'~~~~~~~~~~~~~~~~~~++~ 

u 

~ 800~~~~~~~~~4~~~~~~~~~~~~~~~~~~~~~ ~ 

w 

~ 700~++~~~~++~~~~~++++~++++~ 

600~~++~~~~++++~~++~~~++~ 

500~~~~~~~~~~~~~~~~~--~~--~~--~~~----~~~ 

400~~~~~~~-.~~~~~~~--~~~~~~~~~~~~~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? 

l<irapolation limit of calibration from graph: 

If not acceptable, describe corrective action: 

NO 

Enter Upper FAHRENHEIT 

Limit CALIBRATION RANGE 

-20 1200 
\ 

BARR 

Engineering Company 

Thermocouple Number: TC -<2-~ - O. 

Media 

Std Used 'D-Z 

Reference De~ F (To) 

Reference Corr Temp (de~ R) de~ F + 460 

Probe Temp (deg F) 

Probe Temp (deg R), deq F + 460 

Difference (deqrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's function: 

20 

2..0 

4fW 

2..t 

'{g ( 

-r- I 

6·2. 

If not acceptable, describe corrective procedures undertaken: 

.-----

70 

10 

530 

6~ 

S2.., 

-( 

O.L 

THERMOCOUPLE 

CALIBRA TION 

150 

[so 

(';'ID 

i 1-\ 7 

(pal 

-"3 

o.s-

(6§) No) 

@JNo) 

Date: i2.-2..2..-Ci..1 

Technician: --=-fv_'_f2--..:;.S ___ _ 

to 
BARR 

REFERENCE STANDARDS 

Hart Scientific 9103-A sIn A 1 B289 

Hart Scientific 9140 sIn A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE 10 C~~ 

Cal Date: 4/15/2005 Meter In or Out 

CALIBRATION TECHNICIAN: JMM 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 

32 210 

492 672 

492 670 

0 2 

0.0% 0.3% 

YES 

DATE LABORATORY 

12/11/2003 Hart Scientific 

12/11/2003 Hart Scientific 

400 650 70 

400 650 70 

392 645 68 

860 1110 530 

852 1105 528 

8 5 2 

0.9% 0.5% 0.4% 

1700~~~~~~~~~~~~~~TF~~~~73?7~~~~~~~~~~ 

1600 

1500 --fo--'-~.,..-.j 

~ 1400 .. 

"C 

~ 1300 :::l 

~ 1200 --f2:C~,-,,-

~ 1100 --fo--'-~~ w 

:;; 1000 ..J 

a. is 900 u 

~ 800--fo--'-~ 0:: 

w 

¢: 700 +-=:'-,--:--:7 

600 +:-:'-~~= 

500 -+7"~-QI''''-+~ ~~~ 

400+,~~r=~=+~~~~~~~~~~~~~~~~=T~~~~=r~=,~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: --,-C_o ----.:::d.'--_"".b""-_ 

Media 

Std Used 

Reference Deg F (To) 

Reference Corr Temp (deg R) deg F + 460 

Probe Temp (deg F) 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abso T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's function: 

32 

3~ 

3).. 

If not acceptable, describe corrective procedures undertaken: 

212 

dtd.. 

;:210 

THERMOCOUPLE 

CALIBRATION 

400 

,{00 

0'Sq d..-

(Yes/No) 

(Yes/No) 

I 

U_I·r-O('"" Date: _:2.L-__ :::>__ ""> __ _ 

Technician: ,i (IA (V"- " 

650 Ambient 

0,0 "70 

CoL.( 5 &'1 ~ 

to 
THERMOCOUPLE CALIBRATION 

BARR 

THERMOCOUPLE 10 C-2-0 

Cal Date: 4/15/2005 Meter In or Out 

CALIBRATION TECHNICIAN: JMM 

REFERENCE STANDARDS 

Hart Scientific 9103-A sIn A 18289 

Hart Scientific 9140 sIn A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured pOints? 

TRACEABILITY 

Report No. A180718 

Report No. A1 B2024 

32 

. 

32 

32 

492 

492 

o 

0.0% 

YES 

212 

212 

2'11 

672 

671 

1 

0.1% 

DATE 

12/11/2003 

12/11/2003 

400 

400 

394 

860 

854 

6 

0.7% 

LABORATORY 

Hart Scientific 

Hart Scientific 

650 

650 

645 

1110 

1105 

5 

0.5% 

70 

70 

~Q 

o~ 

530 

529 

1 

0.2% 

1700T:7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

1600~~~~~~============~==~~~~~~~~~~~~ 

1500 +,-:,=.,.-,-'f'-=j 

~ 1400 -f--:"-~-:-,,-:,I <If 

" 

~1300~~~~~~~~~~~23~~~~~~ :::l 

~ 1200~~~~~~~~~~~~~~~~~ 

~ 1100~~~~~~~~~~~~~~~~~~~~~~~ w 

; 1000~~~~~~~~~~~~~~~~~~~~~~~~~~~ Co 6 900 +'-'~=.,.-,- u 

a:: 

~ 800+=~~~~~~3 w i!: 700 ~=--",""," 

600 

500~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
\ 

\, 

BARR 

Engineering Company 

Thermocouple Number: C - d.- 0 

Media 

Std Used 

Reference Deg F (To) 

Reference Corr Temp (deg R) deq F + 460 

Probe Temp (deg F) 

Probe Temp (deq R), deq F + 460 

Difference (deqrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's function: 

32 

32 

3:).. 

If not acceptable, describe corrective procedures undertaken: 

212 

~td-

(;2 L i 

THERMOCOUPLE 

CALI BRA TION 

400 

1CJO 

"$ ~7 '1 

(Yes! No) 

(Yes! No) 

Date: y ~ i s- ~ 0 STechnician: J ~ 

650 Ambient 

&5-0 70 

&'1.S ~1 

to 
THERMOCOUPLE CALIBRATION 

BARR 

THERMOCOUPLE 10 C-3-1 

Cal Date: 12/27/2004 Meter In or Out 

CALIBRATION TECHNICIAN: NRS 

REFERENCE STANDARDS TRACEABILITY DATE LABORATORY 

Hart Scientific 91 03-A sIn A1 B289 Report No. A1B0718 12/11/2003 Hart Scientific 

Hart Scientific 9140 sIn A1B086 Report No. A1 B2024 12/11/2003 Hart Scientific 

Temperature Calibraion Points 20 70 150 

Reference Deg F (To) 20 70 150 

Probe Temp (deg F) 21 69 148 

Reference Temp (deg R) deg F + 460 480 530 610 

Probe Temp (deg R), deg F + 460 481 529 608 

Difference (degrees) -1 1 2 

% Diff Abs. T 0.2% 0.2% 0.3% 

Is difference less than 1.5% at all 

measured points? YES 

I 

THERMOCOUPLE CALIBRATION 1700~~~~~--~·~~~~~--~~--~~~~--~~~~------~~~ 

1600+=-3+~~~~~~~7'~~~~~~~~~~~~~~~~~~~~TS~~~ 

~1500 +=-'---:'-'-~-"1 OJ 

~J400 +='---:'-'--:-'-'-:''-'-1 w 

~1300+L~~~========================~~~~~;~~~~~~~~~~ 

f-

~1200T0~~~~~~~~·~~~~~~~=~~~:~S~'~~~~~~~~~~~~ w 

~1100+=-~~~~~~~~~~=-~~~~~~~~~~~~~~~~~~~ 

w 

~1000+=~~~~~~~~~~J~~~~~~9~~~~~"~~~~~~~~~~~~~~ 

-l 

~ 900+=~~~~~~~.~~~~~~~~~~~~~~~~~~~~~·~~~~~~ 

o g 800~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

w 

~ 700 +=~~~~~~~~~~~~~~~ 

~ 600 

500~~~~~~~~~~~~~~~~ __ ~~~~~~ __ ~~ __ --~L~ 

400~-~~~~~~~~~~~~~,=~~~~~~~~~~~~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Enter Upper FAHRENHEIT 

Are extrapolated limits less than 1.5%? 

x:trapolation limit of calibration from graph: 

NO Limit CALIBRATION RANGE 

-20 1200 

If not acceptable, describe corrective action: 
BARR 

Engineering Company 

Thermocouple Number: "'-c - c.. -::; - L 

Media 

Std Used !)-~ 

Reference Deg F (To) 

Reference Corr Temp (deg R) deg F + 460 

Probe Temp (deg F) 

Probe Temp (deg R). deg F + 460 

Difference (de~rees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's. function: 

20 

2C 

4~a 

'2- ! ~1:f( 

+1 

O.L. 

If not acceptable, describe corrective procedures undertaken: 

70 

1.0 

5""30 

( c' ..Ql 

52"1 

-I 

c!:1 • "L 

THERMOCOUPLE 

CALIBRATION 

150 

(SO 

G:> I a 

il.\ ~' 

Co<J'i? 

-2. 

0.3, 

<GINo) 

<Q;yl No) 

Date: if -?;-1- - c'-i 

Technician: i\;/'_) ----=-----

to 
THERMOCOUPLE CALIBRATION 

BARR 

THERMOCOUPLE 10 C-3-0 

Cal Date: 12/27/2004 Meter In or Out 

CALIBRATION TECHNICIAN: NRS 

REFERENCE STANDARDS TRACEABILITY DATE LABORATORY 

Hart Scientific 9103-A sIn A1B289 Report No. A1B0718 12/11/2003 Hart Scientific 

Hart Scientific 9140 sIn A1 B086 Report No. A1 B2024 12/11/2003 Hart Scientific 

Temperature Calibraion Points 20 70 150 

Reference Deg F (To) 20 70 150 

Probe Temp (deg F) 20 6S 148 

Reference Temp (deg R) deg F + 460 480 530 610 

Probe Temp (deg R), deg F + 460 480 529 608 

Difference (degrees) 0 1 2 

% Diff Abs. T 0.0% 0.2% 0.3% 

Is difference less than 1.5% at all 

measured pOints? YES 

THERMOCOUPLE CALIBRATION 1700~~~~~~~~---~~~~~~~~~-=~~~~:~~-=---~~~~~-~ 

1600~=--+~~~~~~~~~~'~"~~~'~~~~f~2~~~~~~~~~,~~~~~-~~ 

cr; 1500 ~~"'-"-i OJ 

~_ 1400 +-:~-'-'-':-:l w 5 1300~~~~~~~~~~~~~~~==~~~~~~~~~~~~~~ffj I-

~ 1200+-:~~~~·~~~~~~-:~~~~~~-~~~~~2~~;'~~~~·~~22~~~~ w 

~ 1100~~~~==22~~22~~~~~~~:~~~~~~~~~~~~~~ 

W 

~ 1000+~~~~~~~~~~~~~~~:~~~~~~~~~'~~~~~~~'~1 ..J 

§ 900+-:~~~~~~~~~-~~~~~F~~'~~~~~22~~~~~~~22~~~~~ 

o 

g 800~~~~~~~~~~~~lb~~~~~~~~~~~~~~~ 

ffi 700 +-:~~~~-=-----,--':;;~~~~~~~~':'-'-l 

~ 600 ~~~~~~G',-,-:--~~~~~-"--'~~-'-i 

500~~~7+~~~~-=~~~~~~~~~~~~~--~~~~~: 

400~~-T~~~~'=~-T~~~~~~~~~--~~~-'~~~~~--~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: TC Q. '-3'-D 

Media 

Std Used b-~ 

Reference Deg F (To) 

Reference Corr Temp (deg R) deg F + 460 

Probe Temp (def:j F) 

Probe Temp (def:j R), def:j F + 460 

Difference (degrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of the thermocouple's. function: 

20 

2.0 

L../~o 

2..0 

"fifO 

0 

0.0 

70 

Ie 

S36 

l?Cj 

S-2'1 

-{ 

0· 2-

THERMOCOUPLE 

CALI BRA TION 

150 

j s;-c 

~IO 

l'i ? 

<Co~ 

-~ 

0_"3 

(~NO) 

~NO) 

Date: 11 ... - <-4--<)',( '. 

Technician: _.L/'-.J~I2...=S,,--__ _ 

to 

c:.....ttbl MoJ.,,\&. -S ~r?M o .... -Hd- tL....-.-.C>c."' .... rk 

If not acceptable, describe corrective procedures undertaken: 
THERMOCOUPLE CALIBRATION 

BARR <\\4) L rTHERMOCOUPLE 10 TC4-Z { 7)7(0) { 

Cal;Date: 12/31/2004 M-5 Probe 

CALIBRATION TECHNICIAN: NRS 

REFERENCE STANDARDS 

Hart Scientific 91 03-A sIn A 1 B289 

Hart Scientific 9140 sIn A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 ,.,~ 

")L 213 

492 672 

492 673 

0 -1 

0.0% 0.1% 

YES 

DATE LABORATORY 

12/11/2003 Hart Scientific 

12/11/2003 Hart Scientific 

400 650 Ambient 

400 650 70 

398 651 69 

860 1110 530 

858 1111 529 

2 -1 1 

0.2% 0.1% 0.2% 

1700~~~~~~~~~~~~~~~~~~~~~~~~--~~~~-, 

1600~~~~====================~tt~~~~ttjt~~~~~~~ 

1500~~~ 

~ 1400 ~~-?'-:i 

'" 

~1300~~~C===~~==~~==~======~~~~~~~~~~~~~~~ 

:::l 

~ 1200~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ w 

~ 1100~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

w 

~ 1000~~~~=~~~~~~~~~~~~~~~~~~~~==~==~~~~~i ..J 

0.. 5 900~~~~ u 

~ 0:: 800+7~~~~~~~~~~~~~~~ w 

i!: 700 -!---'-'==~ 

600 

500~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
'BARR 

Engineering Company / 

1/,/07 

~\V Thermocouple Number: T eLl -~ { I Y\ 

Media 

Std Used D-<? 

Reference Deq F (To) 

Reference Carr Temp (deg R) deg F + 460 

Probe Temp (deg F) 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

,.,jescription of the thermocouple's function: 

32 

'52... 

<-{'11.. 

32-

'1'12. 

0 

0.0 

clef-Lei S- fro,!'£- &CiX'-ccot..fk 

If not acceptable, descnbe corrective procedures undertaken: 

P:\OO\02\OEM\Oatasheets\calibration.xls 

212 

L.l2... 

l.91-z.. 

2.\ 3> 

&>73 

.... \ 

0.' 

THERMOCOUPLE 

CALIBRATION 

400 

-

-

l..{(.J'D 

.: 8"(gO 

3 eLf 

gc;-g 

-"L 

0:2-

@~o) 

@;/NO) 

Date: i '--5 \ -c~ 

T ec.'lnichian: r..; t:..-5. ---==------

650 Other 

(..,~t; to 

LIIO 5'3 0 

(pSt !'.fl7'1 

( 1(( 52..'1 

-t-I -I 

0.( 0.2 

to 
THERMOCOUPLE CALIBRATION 

BARR 

THERMOCOUPLE ID TC5-1 

Cal;Date: 12/23/2004 M-5 Probe 

CALIBRATION TECHNICIAN: NRS 

REFERENCE STANDARDS 

Hart Scientific 9103-A sIn A1 B289 

Hart Scientific 9140 sIn A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 

32 211 

492 672 

492 671 

0 1 

0.0% 0.1% 

YES 

DATE LABORATORY 

12/11/2003 Hart Scientific 

12/11/2003 Hart Scientific 

400 650 Ambient 

400 650 70 

3CiQ V~ 652 hO UV 

860 1110 530 

859 1112 529 

1 -2 1 

0.1% 0.2% 0.2% 

1700~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

1600~~~~~==================~~~~tT~~~~~~~~.~~ 

1500 +-,",......,-'-......,-'-'7l 

~1400~~~ 

'" 

~1300~~~J=======~~~~~~~==~~~~~~~~~~~~~~~~~~ 

::J 

~ 1200+7~~~~~~~~~~~~~~~~~~~'~~~~~~~~~~~~ 

w 

~ 1100~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

w 

...I 

~ 1000~~~~~~~L2~~~~~~~~~~~~~~~~~~~~~~~~~ 

a. 5 900~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ u 

a:: 

~ 800~==========~====~~~~==~======~ w 

~ 700~~~~~~~~~~~~====~~~ 

600~====~~~~~~==~~~~==~~~ 

500~~~~~~~==~~~==~~~~~~~~~~~~~~~~~~~~~ 

400+,~~~~~~~~~,r~~~~~~~~~'-~~~~--~~~-T~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 I 

REFERENCE TEMPERATURE, deg.R I 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

I 

-20 1200 
·BARR 

Engineering Company 

Thermocouple Number: .,..c S- -1-

Media 

Std Used D-8' 

Reference Deq F rro) 

Reference CorrTemp (deq R) deq F + 460 

Probe Temp (deq F) 

Probe Temp (deq R), deq F + 460 

Difference (deqrees) 

% Diff Abs. T (Renkin) 

Oiff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Oiff. <= 1.5% 

Description of the thermocouple's function: 

If not acceptable, descnbe corrective procedures undertaken: 

' .. :.:" 

P:\OO\02\OEM\Datasheets\calibration.xls 

32 212 

3"2- "2..i2 

'4'12. ~[2. 

32- 2(( 

t{CJ 2.. 0t{ 

0 -I 

C).O 0.1 

THERMOCOUPLE 

CALIBRATION 

Date: /7...- 23-0'1 

Technichian: NiLS --!..:=--=-----

400 650 Other 

-

-

LiOO G::~ 70 

::~00 1110 SSo 

311 [~S 2. 0~ 

~9"'1 I IlL 5'2.'1 

-( +L. - ( 

a.1 0.1- 6'L 

to 
BARR 

REFERENCE STANDARDS 

Hart Scientific 9103-A sIn A 1 B289 

Hart Scientific 9140 sIn A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

THERMOCOUPLE CALIBRATION 

THERMOCOUPLE 10 TC5-2 

Cal;Date: 12/23/2004 M-5 Probe 

CALIBRATION TECHNICIAN: NRS 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 

32 210 

492 672 

492 670 

0 2 

0.0% 0.3% 

YES 

DATE 

12/11/2003 

12/11/2003 

400 

400 

395 

860 

855 

5 

0.6% 

LABORATORY 

Hart Scientific 

Hart Scientific 

650 Ambient 

650 70 ..... ,-.r'"'I 

0O'"' 70 

1110 530 

1113 530 

-3 0 

0.3% 0.0% 

1700~~~~~~~~~~~~~7===~~~~~~~~~~~~~~~ 

1600~~~~~~==~~==~====~~~~~~~~~~~~~~7~~ 

1500 ~~~ 

~ 1400 +---~~ .. 

"" 

~1300~~~~~~~~~~~~~~~==~~~~~~~~~~~~~~ 

::l 

~ 1200~~~~~~~~~~==~~~~~~~==~~;~~~~~~~~~~~ 

0:: 

w 

~ 1100+-~~~~~~~~==~~~~~~~~~~~~~~~~~~~~ 

w 

~ ...I 1000+-~:~s+~==~s+~~~~~~~~~~~~~~~~~~~~~~ 

a. 5 900~~~====~~~~==~~==~~~==~~~~~==~~==~~==~ u 

0:: 

~ 800tt~~~~~~f4~~~~~~~~~~~~~;r.~~~~~~~ w 

~ 700~====~~==~7~~~==~~~~~ 

600~~~~~~~~~~~~~~~~ 

500~~~~~~~~~~~~~~~~==~~~~~~~~~~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 I 

REFERENCE TEMPERATURE, deg.R I 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
"BARR 

Engineering Company 

Thermocouple Number: Tc...S - L 

Media 

Std Used 

Reference Deq F (To) 

Reference Carr Temp (deo R) deq F + 460 

Probe Temp (deg F) 

Probe Temp (deg R). deg F + 460 

Difference (degrees) 

% Oiff Abs. T (Renkin) 

Diff. less than 1.5% at all points 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Llescription of the thennocouple's function: 

t1-s= 

If not acceptable. descnbe corrective procedures undertaken: 

P:\OO\02\OEM\Datasheets\calibration.xls 

32 212 

D-~ 

~L LiZ-

<-19<- (';'l2 

-32- ZIO 

492 4>10 

<::) -L 

0.0 0·3 

THERMOCOUPLE 

CALIBRATION 

400 

-

L/oo 

'i'Co6 

.3""iS1?S5 

-s 

0.10 

(~/NO) 

r@fNO) 

Date: 12...-2..3 -01..{ 

Technichian: NiLS --'.-.:::..:....::----

650 Other 

"'I 

G"S"O 70 

I [{ 0 S;:SO 

<05"-3 1D 

I (1:5 . S30 

t-3 0 

O·s 0.0 

to 
THERMOCOUPLE CALIBRATION 

BARR 

THERMOCOUPLE 10 TC 6·2 

Cal;Date: 12/22/2004 M-5 Probe 

CALIBRATION TECHNICIAN: JMM 

REFERENCE STANDARDS 

Hart Scientific 91 03-A sin A 1 B289 

Hart Scientific 9140 sin A1B086 

Temperature Calibraion Points 

Reference Deg F (To) 

Probe Temp (deg F) 

Reference Temp (deg R) deg F + 460 

Probe Temp (deg R), deg F + 460 

Difference (degrees) 

% Diff Abs. T 

Is difference less than 1.5% at all 

measured points? 

TRACEABILITY 

Report No. A1B0718 

Report No. A1B2024 

32 212 

32 212 

32 2'11 

492 672 

492 671 

0 1 

0.0% 0.1% 

YES 

DATE LABORATORY 

12/11/2003 Hart Scientific 

12/11/2003 Hart Scientific 

400 650 Ambient 

400 650 70 

396 649 69 

860 1110 530 

856 1109 529 

4 1 1 

0.5% 0.1% 0.2% 

1700~=--~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

1600fT~~~====================~~~~~~~~~~~~~~~ 

1500 +'-::::~~ 

~1400~~~ ., 

"0 

~1300~~~~~====================~~~~~J~~~~~~~~~~ 

:::l 

~ 1200~~~~~~~~~~~~~~~~~~~'~~~~~~~~~~~ 

w 

~ 1100~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ 

w 

..J 

~ 1000~~~~~~~~~~~~~7~'~~~~~~~~~~~~~~~~ 

a. 5 900~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~ u 

~ 800f2~~~~~~8P28~~ff~~SFt1~~~~~~~~~~;.re~~ w 

~ 700~~~~~~~~~~~~~~~~ 

600~~~~~~~~~~~~~~~~~ 

500~~~~~22~~~~~~~~==~~~~~~~~~-J. 

400~--~~~~~~~~~~~~~~~~~~='~~~~-r~~~~ 

400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

REFERENCE TEMPERATURE, deg.R 

Are extrapolated limits less than 1.5%? YES 

If not acceptable, describe corrective action: 

FAHRENHEIT 

CALIBRATION RANGE 

-20 1200 
BARR 

Engineering Company 

Thermocouple Number: 

Media 

Std Used D-~ 

Reference Deq F (To) 

Reference CorrTemp (deq R) deq F + 460 

Probe Temp (deq F) 

Probe Temp (deq R), deq F + 460 

Difference (deqrees) 

% Diff Abs. T (Renkin) 

Diff. less than 1.5% at all pOints 

Graph Attached 

Extrapolated Range with Diff. <= 1.5% 

Description of thE; thennocouple's function: 

'\ • i ;f r 

_,1'</\-( ·:fIAt: tl I.,) " -~" h' '" i Y" ./ k 

If not acceptable, describe corrective procedures undertaken: 

P:\OO\02\OEM\Oatasheets\calibration.xls 

32 212 

'3~ ~ j )..,C 

f.,i 7 1- G 7). 

"3).. J.i/ 

i{ tJ ,f- 61/ 

0 I -I 

0.0 6.\ 

THERMOCOUPLE 

CALIBRA TION 

400 

-

t-f {;' 6 

''i;~6 

'~(l C 

5>.5" ~ 

-4 

O.S" 

@/NO) 

C@NO) 

Date: _i d---,-I_J.._J_I_tl_vl __ 

Technichian: _....;J~,~ ___ _ 

650 Other 

!.(.Q /Y),O 

lllO ~:SO 

~,<{ '1 ret ,..-;, 7 

\ \0 '1 <;-:.~ 1 

-( -I 

0·\ O.'L 

to 
BARR 

ANEROID BAROMETER 

CALIBRATION 

Barometer 1.0. Number: bA -6~­

Barometer Reference: f '''< 0 

Project Name: l/j,q..c.. 1Vt'j _0::) 

Pretest Calibration: 

Before Adjustment 

After Adjustment 

Postiest Check: 

Notes: 

Barr Engineering Co. 

4700 W. 77th St 

Minneapolis, MN 55437 

(952) 832-2600 

Reference ("Hg) 

2 ';1. I -; 

r--. 

Reference ("Hg) 

28 . 9 t.{ 

Project Number: Z ..vEer ~ 9 (-('2; !,fj1( 6(. <- , 

Barometer ("Hg) Date Technician 

29·· ZcJ S--Z-cj;- 7tIf !C 

---- - '----

Barometer ("Hg) Date Technician 

2fJ, q 0 p~lO'C,7 rA/C 
Appendix F 

Cylinder Gas Certifications 
51111 

BARROI 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD .• RIVERSIDE, CA 92507 

TELEPHONE (909) 653-6780 • FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: Sam Foss DATE: June 25 2004 

Barr Engineering Co 

7390 OHMS Lane 

Edina ~rn 55439-2330 

CUSTOMER ORDER NUMBER: 20040420ASMF2 

---------------------------------------------------------------- ---------------------------------------------------------------- COMPONENT CONCENTRATION(vlv) REFERENCE ANALYZER EXPIRATION REPLICATE 

± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC67233 

VARIAN HODEL 1860 TCD 06/25/04 

Carbon Dioxide 5.01 ± 0.05% GHIS SiN NONE 06/25/07 5.01% 

CYLINDER #: THERHAL CONDUCTIVITY 5.01% 

CC4.2814 GAS CHROHATOGRAPHY 5.01% 

@ 8.01% LAST CAL DATE: 06/25/04 MEAN: 5.01% 

VARIAN HODEL 1860 TCD 06/24/04 

Oxygen 19.98 ± 0.2% GHIS SIN NONE 06/24/07 19.94% 

CYLINDER #: THER}rnL CONDUCTIVITY 20.05% 

Nitrogen Balance cA03201 GAS CHROHATOGRAPHY 19.96% 

CYLINDER PRESSURE: 2000 psig @24.82% LAST CAL DATE: 06/23/04 MEAN: 19.98% 

ppm = ~ole/mo1e % = mo1e-% 

The above analyses were performed in accordance with Procedure G1 of the EPA Traceability Protocol, Report Number 

EPA-600/R97/121 ,d ted Se tember 1997. 

This cylinder SW{I " ot b . d if the pressure is less than 150 psig. r, ) 

I , /lL 

ANALYST: APPROVED:~~~I.~ J_,_/~J~I_~~(4- /7'"' II-~ ~ __________________ __ 

M. S • CALHOUN 6:;;'1" J. T. MARRIN \.. 

The only liability of this company for gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
51111 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. a RIVERSIDE, CA 92507 

TELEPHONE (909) 653-6780 III FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: John Stock DATE: September 3 2003 

Barr Engineering Co 

7390 OHHS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: 20030707A 

---------------------------------------------------------------- ---------------------------------------------------------------- COMPONENT CONCENTRATION(vlv) REFERENCE ANALYZER EXPIRATION REPLICATE 

± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC73045 

VARIAN HODEL 1860 TCD 09/03/03 

Carbon Dioxide 9.05 ± 0.09% GHIS SIN NOliE 09/03/06 9.04% 

CYLINDER #: THERHAL CONDUCTIVITY 9.04% 

CC42814 GAS CHR01·I."<TOGRAPHY 9.06% 

@ 8.01% LAST CAL DATE: OS/29/03 MEAN: 9.05% 

VARIAN HODEL 1860 TCD OS/28/03 

Oxygen 8.99 ± 0.05% Gl-lIS SIN NONE 08/28/06 8.98% 

CYLINDER#: THERJ.!."<L CONDUCTIVITY 8.97% 

l'Iitrogen Balance CCS1204 GAS CHROJ.lATOGRAPHY 9.01% 

CYLINDER PRESSURE: 2000 psig @ 9.88% LAST CAL DATE: 08/28/03 MEAN: S.99% 

ppm = ~~ole/mole % = mole-% 

The above analyses were performed in accordance with Procedure G1 of the EPA Traceabili Protocol, Report Number 

EPA-600iR97 /121, dated September 1997. 

This cylinder should used if the pressure is less than 150 psig. 

ANALYST:~~~~~~~------------------APPROVED:----_T~~------------------------

J. 

f 

The only liability of this company for gas which fails to comply with this analysis shall be replacement or rean~ysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
51111 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. til RIVERSIDE, CA 92507 

TELEPHONE (909) 653-6780 \I FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: John Stock DATE: July 2 2003 

Barr Engineering Co 

7390 OHMS Lane 

Edina 1m 55439-2330 

CUSTOMER ORDER NUMBER: 20030417A 

~--~~~~~~~---~-~----------~~----------~---------------~--------­ -~~-~----~------~--------~~--------------------------- ----------

COMPONENT CONCENTRATION(v/v) REFERENCE ANALYZER EXPIRATION REPLICATE 

± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC12793 

!-IONITOR LABS HODEL 8440 06/25/03 07/02/03 

Nitric Oxide 461 ± 3 ppm Gl-lIS SiN 136 07/02/05 461 ppm 460 ppm 

NOx 461 ppm CYLINDER #: CaNTIl-lUaUS 461 ppm 461 ppm 

Nitrogen,02-Free Balance CC50638 CEE~!ILUl-IINESCENCE 461 ppm 461 ppm 

CYLINDER PRESSURE: 2000 psig @519 ppm LAST CAL DATE: 06/18/03 MEAN: 461 ppm 461 ppm 

ppm = ~ole/mole % = mole-% 

The above analyses were performed in accordance with Procedure G1 of the EPA Tractability Protocol, Report Number 

EPA-600/R97/121, dated September 1997. 1 

10;, 'YIiOde,,~~ the p,."uce ;, 1m thao 150 p';g. i~ ~ \'nOn 

ANALYST: .' ~ APPROVED: __ -!~I-l:i i-O-i\~~!i.L:)'£:;:":X11~ ___________ _ 

B • M .101ARRIN J . T .~IN 

I 

The only liability of this company for gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
SIIII 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD. 0 RIVERSIDE. CA 92507 

TELEPHONE (909) 653-67800 FAX (909) 653·2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: John Stock DATE: October 13 2003 

Barr Engineering Company 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: 200309l2A 

--~~~-~--~-~--------~~------~-------------~~---------~----~~---~ ---~-~--------------------------------------------------~-------

COMPONENT CONCENTRATION(vJv) REFERENCE ANALYZER EXPIRATION REPLICATE 

:!: EPA UNCERTAINTY STANDARD MAKE, MODEL, SIN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC29033 

I·\ONITOR LABS HODEL 8440 10/06/03 10/13/03 

Nitric Oxide 245.7 :!: 1.3 ppm GIns SIN 136 10/13/05 245.5 ppm 246.1 ppm 

NOx 245.7 ppm CYLINDER #: CONTINUOUS 245.2 ppm 245.0 ppm 

Nitrogen r 02-Free Balance ccn078 CHEIoIILUIoIINESCENCE 245.4 ppm 246.5 ppm 

CYLINDER PRESSURE: 2000 psig @252.6 ppm LAST CAL DATE: 09/23/03 MEAN: 245.4 ppm 245.9 ppm 

ppm = ~ole/mole % = mole-'/; 

The above analyses were performed in accordance with Procedure G1 of the EPA Traceability Protocol, Report Number 

EPA-600jR97j121, dated September 1997. " 

:::::~c 'fj35J6'flhe p,",,"ce I, 1m fuan 150 ::':ROVEO _...,y~<=--______________ _ 

B.M.~N 

The only liability of this company for gas which fails to comply with this analysis shall be replacement 0 reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
51111 

BARROl 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS BLVD .• RIVERSIDE. CA 92507 

TELEPHONE (909) 653-6780. FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: John Stock DATE: August 27 2003 

Barr Engineering Co 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: 20030707A 

----------------------------------------------------------------

-----~-~---------~---------~----------~--------~-----~------~---

COMPONENT CONCENTRA T10N(v/V} REFERENCE ANALYZER EXPIRATION REPLICATE 

± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC68786 

BOVAR HODEL 922H 08/12103 08/19/03 

Sulfur Dioxide 50.5 ± 0.6 ppm G~lIS SIN VD92284844 08/19/05 50.4 ppm 50.5 ppm 

CYLINDER #: CONTINUOUS 50.5 ppm 50.5 ppm 

Nitrogen Balance CC12643 UV PHOTOHETRY 50.5 ppm 50.6 ppm 

CYLINDER PRESSURE: 2000 psig @55.8 ppm LAST CAL DATE: 08/07/03 MEAN: 50.5 ppm 50.5 ppm 

ppm = ~~o1e/mole % = mo1e-% 

The above analyses were performed in accordance with Procedure G1 of the EPA Trac ability Protocol, Report Number 

EPA-600/R97/121. dated September 1997. 

This cylinder should not be used if the pressure is less than 150 psig. 

ANALYST: n~~~ APPROVED: __ ~~----____ -------------------

H.J.HONSON 

The only liability of this company for gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
51111 

BARR01 

SCOTT-MARRIN, INC. 

6531 BOX SPRINGS 8L VD. Q RIVERSIDE. CA 92507 

TELEPHONE (909) 653-6780. FAX (909) 653-2430 

REPORT OF ANALYSIS 

EPA PROTOCOL GAS MIXTURES 

TO: Sam Foss DATE: July 13 2004 

Barr Engineering Co 

7390 OHMS Lane 

Edina MN 55439-2330 

CUSTOMER ORDER NUMBER: Vbl/s FOSS 

---------------------------------------------------------------- ---------------------------------------------------------------- COMPONENT CONCENTRATION(v!v) REFERENCE ANALYZER EXPIRATION REPLICATE 

:!: EPA UNCERTAINTY STANDARD MAKE, MODEL. SIN, DETECTION DATE ANALYSIS DATA 

CYLINDER NO: CC121446 

BOVAR HODEL 92211 07/12/04 

Sulfur Dioxide 93.1 :!: 0.9 ppm G~IIS SIN VD92284844 07112/06 93.1 ppm 

CYLINDER#: CONTINUOUS 93.1 ppm 

Nitrogen Balance CC12025 UV PHOTOl1ETRY 93.3 ppm 

CYLINDER PRESSURE: 1150 psig @ 111.8 ppm LAST CAL DATE: 06/14/04 MEAN: 93.2 ppm 

ppm = ~ole/mo1e % = mole-% 

The above analyses were performed in accordance with Procedure G 1 of the EPA T race a i1ity Protocol, Report Number 

EPA-600/R97/121, dated September 1997. 

This cylinder should not be used if the pressure is less than 150 psig. 

ANALYST: }~J~ APPROVED:~~~----------- ~1. J .1010NSON I J. T .101ARRIN 

The only liability of this company for gas which fails to comply with this analysis shall be rePlacement£reanalYSiS thereof by the company without extra cost. 

STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS 
iI III I SCOTT-MARRIN, INC. 

CHRONOLOGICAL RECORD OF CERTIFIED CONCENTRATIONS 

CUSTOMER: Barr Engineering CO 

PURCHASE ORDER: Vbl/5 Foss 

CYLINDER NUMBER: CC121446 

COMPONENT 502 

DATE 

07/10/02 

07/17/02 

07/12/04 

AVERAGE 

NOTES: 

93.0 ppm 

93.0 ppm 

93.2 ppm 

93.1 ppm 

St>'ITECH\CHRONO I.DOC 6/96 

CUSTOMER CODE: BARR01 

DATE: 07/13/04 
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer: Twin City Oxygen Reference # 88-91148 

NSG PO# 4424096 Certification Date: 06/15/04 

Customer PO# 43778 Expiration Date: 06/15/07 

Cylinder # SG9165492BAL Pressure, psig* 2000 

ANALYTICAL INFORMATION 

METHOD: This standard was analyzed according to EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards: 

Procedure G1 (September 1997) 

ANALYZED CYLINDER 

Components 

Methane 

Balance - Air 

REFERENCE STANDARD 

Type/SRM Sample # 

GMIS ( Traceable to SRM # 2750 ) 

INSTRUMENTATION 

Instrument/Model/Serial # 

Rosemount 400A THC 00335 

Certified Concentration 

30.2 ppm 

Cylinder # 

CC16937 

Last Date Calibrated 

06/08/04 

Analytical Accuracy** 

+/-1% 

Concentration 

51.57 ppm CH4/AIR 

Analytical Method 

Flame Ionization Detector 

Analyst: ___________ ~R.;.;..ic;.;..h;.;..a;...;rd.;.;..S~y...;.;k...;.;es~_ 

This report states accurately the results of the investigation made upon the material submitted to the analytical 

laboratory. Every effort has been made to determine objectively the information requested. However, in 

connection with this report, National Specialty Gases shall have no liability in excess of established charge for 

this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772 

"Do not use this standard when cylinder pressure is below 150 psig. 

.... Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument. NSG 020149L 
NATIONAL SPECIALTY GASES 

630 UNITED DRIVE 

DURHAM, NC 27713 

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer: Twin City Oxygen Reference # 88-78516 

NSG PO# 3558412 Certification Date: 08/01/02 

Customer PO# 39278 Expiration Date: 08/01/05 

Cylinder # CC2937 .Pressure, psig" 2000 

ANALYTICAL INFORMATION 

METHOD: This standard was analyzed according to EPA Traceability Prctocol for Assay and certification of Gaseous Calibration 

Standards: Procedure G-1: September 1997. 

ANALYZED CYLINDER 

Components 

Methane 

Balance - Air 

REFERENCE STANDARD 

Type/SRM Sample # 

GMIS ( Traceable to SRM # 2751 ) 

INSTRUMENTATION 

Instrument/Model/Serial # 

Rosemount 400A THC 00335 

Certified Concentration 

46.5 PPM 

Cylinder # 

CC36118 

Last Date Calibrated 

07/16/02 

Analytical Accuracy"" 

+/-1% 

Concentration 

100.3 ppm CH4/AIR 

Analytical Method 

Flame Ionization Detector 

Analyst: ___________ ....:Am:....::..:...:Ly..=J.;.. . .:...P.:..:ro:.:.k:;:0.c:.p.::.ow:..:.i:;:c::::.--z 

This report states accurately the results of the investigation made upon the material submitted to the analytical 

laboratory. Every effort has been made to determine objectively the information requested. However, in 

connection with this report, National Specialty Gases shall have no liability in excess of established charge for 

this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772 

*00 not use this standard when cylinder pressure is below 150 psig. 

~ Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument. NSG 020149L 
NATIONAL SPECIALTY GASES 

630 UNITED DRIVE 

DURHAM, NC 27713 

CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE 

Customer: Twin City Oxygen Reference # 88-89053 

NSG PO# 4271165 Certification Date: 02119/04 

CustomerPO# 42921 Expiration Date: 02119/07 

Cylinder#: CC47777 Pressure, psig* 2000 

ANALYTICAL INFORMATION 

METHOD: This standard was analyzed according to EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards: 

Procedure G1 (September 1997) 

ANALYZED CYLINDER 

Components 

Methane 

Balance - Air 

REFERENCE STANDARD 

Type/SRM Sample #: 

GMIS (Traceable to SRM # 2751 ) 

INSTRUMENTATION 

InstrumentIModellSerial # 

Rosemount 400A THC 00335 

Certified Concentration 

90.4 ppm 

Cylinder # 

CC361i8 

Last Date Calibrated 

01/23/04 

Analytical Accuracy** 

+/-1% 

Concentration 

100.3 ppm CH4!AIR 

Analytical Method 

Flame Ionization Detector 

Analyst: ____________ J_e_re_m--"-y_K....;.e....;.nw~ort..;.;h.;.;:.y_ 

This report states accurately the results of the investigation made upon the material submitted to the analytical 

laboratory. Every effort has been made to determine objectively the information requested. However, in 

connection with this report, National Specialty Gases shall have no liability in excess of established charge for 

this service. Assayed at National Specialty Gases, 630 United'Drive, Durham, NC 27713 (919) 544-3772 

"Do not use this standard when cylinder pressure is below 150 pslg. 

~ Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument. NSG 020149l 
Appendix G 

Visible Enzissions Evaluator Certification 
'. 

I I E I IONS 

This is to certify that 

met the specifications of Federal Reference Method 9 

and qualified as a visible emissions evaluator. 

Maximum deviation on white and black smoke did not 

exceed 7.5% opacity and no single error exceeding 

15% opacity was incurred during the certification test 

conducted by Eastern Technical Associates of Raleigh, 

North Carolina. This certificate is valid for six months 

from date of issue. 

. .']28689 

Certificate Number 

President 

eIIknneajtoliJj eIIiinne:.wJ.Cl/ 

Location Date of Issue 

~~~ W. ::I~/~ Director of Training ~U 
VISIBL E I SIONS 

T R 

Th is is to certify th.at 

O)fto 

met the specifications of Federal Reference Method 9 

and qualified as a visible emissions evaluqtor. 

Maximum deviation on white and black smoke did not 

exceed 7.5% opacity and no single error exceeding 

15% opacity was incurred during the certification test 

conducted by Eastern Technical Associates of Raleigh, 

North Carolina. This certificate is valid for six months 

from date of issue. 

328686 eIlUnnea/wli3-j Jliinn€/J-ol'a' 

Certificate Number Location Date of Issue 

~~~ . to. 'ZJU f~/~ Director of Training . President 
AppendixH 

Process Operating Data 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/2/2005 

Company Name: United Taconite 

Equipment & Operating Data 

June-99 

Process Equipment Number/ Identification: Line 1 Pellet Cooler Ex. - SV047 

I. Process Equipment Description: Pellet cooling after induration- Line 1 

2. Were the process and control equipment operated consistent with nonna! operating procedure? YES NO I .... y_e_s ___ -' 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months X I Remains unchanged from Test Plan 

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

ratios as appropriate) --~--~----------------------------------------------------------------------

Process Parameter: list type and units Run I Run 2 Run 3 

Greenballs out of drums, L TPH 294 285 264 

Greenball Feed Rate to the grate, L TPH 265 264 239 

Fired Pellet production Rate, L TPH 231 230 208 

Fuel Input (list units) Natural Gas MCF 146 144 105 

Heat Input (106 British thennal units/hour) 146 144 105 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): ,iP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: ,iP (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OF;nlet ,OFoutleJ and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF operating temperature) 

APC equipment and parameter monitored Run I Run 2 Run 3 

NONE 

List pollutant & averaging basis-should reflect permit 

Continuous Opacity Monitor (list hourly average) 

NA 

Abbreviations: 

Monitor (list averaging basis): 

Monitor (list averaging basis): 

APC-air pollution control 

lbs.-pounds 

NONE 

Run I 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

NONE NONE 

Run 2 Run 3 

in. w.c.-inches of water column 

,iP- pressure drop 

NOTE: This forlll provides ollly a summary of the operatillg cOllditiolls durillg the performallce test. Additional alld more detailed records are 

required to meet the requiremellts of Millll. R. 7017.2035. Tlzisform is to be submitted as part of the perform all ce test report to: North, Metro, 

or SOl/th District, Performallce Test Coordillator, MN Pol/I/tioll COlltrol Agellcy, 520 Lafayette Rd., St. Pal/I, MN 55155-4194. 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/2/2005 

Company Name: United Taconite 

Equipment & Operating Data 

June-99 

Process Equipment Number/ Identification: Line 1 Waste Gas - SV046 

1. Process Equipment Description: Line 1 Kiln Gas Exhaust - Wet Scrubber Control Device 

2. Were the process and control equipment operated consistent with nonnal operating procedure? YES NO L-IY;...e;...s=--__ -I 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months x IRemains unchanged from Test Plan 

5. Process rate (amount of raw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

ratios as appropriate) --~--~----------------------------------------------------------------------

Process Parameter: list type and units Run 1 Run 2 Run 3 

Greenballs out of drums, L TPH 294 285 264 

Greenball Feed Rate to the grate, L TPH 265 264 239 

Fired Pellet production Rate, L TPH 231 230 208 

Fuel Input (list units) Natural Gas MCF 146 144 105 

Heat Input (106 British thennal unitslhour) 146 144 105 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): ~P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: ~P (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OFinlcl ,oF oUlle0 and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (0 F operJ.ting temperature) 

APC equipment and parameter monitored Run 1 Run 2 Run 3 

Scrubber Pressure Drop, In.W.C. 20.5 21 19.9 

Scrubber Water Pressure, PSI 72 - -

Note: NaOH added to scrubber water during test on on on 

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 

Continuous Opacity Monitor (list hourly average) 

Monitor (list averaging basis): 

Monitor (list averaging basis): 

Abbreviations: APC-air pollution control 

lbs.-pounds 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

~P- pressure drop 

NOTE: This form provides ollly a summary of the operatillg cOllditiollS durillg the perform all ce test. Additiollal alld more detailed records are 

required to meet the requiremellts of Mill II. R. 7017.2035. This form is to be submitted as part of the performance test report to: North, Metro, 

or Sout/z District, Performallce Test Coordillator, ]}fN Pollutioll COlltrol Agellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194. 
'<Oe{, , 

5.0.'0 0:> c,,G 

0.~C:J\ 

~~ f\ 0" ,0" 1\.0 I>~ ~ ~ '!:-.e{, :-- e'O 

f0'OC:J1 S0.{, 

~ \.O~ ~ \!}{,e

S 

'?~ O~ ~ " " . " \j;' 0.'0'0 t>c" t>c~ C:Jc,{, 

t>c"':-'"'\ / ';)'"59\/ ~~0:> 0«0 ~0« 

,1 ~ .~~ ~'O''"~.,. ~~ r.f'<1 

. "" '" ~'O? ~~"'- ,1'()' ~001> 0"''0 

~o,~\1:' ,. O~'" )". / o,"~':: 0,7' .~,:: o,,"~O' ,;.,0.J>~\& ~",~",0 ~"'- ~'O<e' "S'", 'V<y,~ o.~'" ,-,,)' 'VO~'" / N )" 0<~\e ~0'\0\' .,~,"? y,'i;J-" 

Lone 1 Wasle '011' <\\.."'- / "'- ,,0'" #" '" 1><,,01> o,"?\/ ~o,'~' 0"'\«-./ s"'\(;../ 00'? 0 0 \0.eY 0 «0.e

\ 

'?~ ~~ ~'O\e; ~'O\e ~'O\e; 

'?'?" / '?'?" / 0V.c,0 0V.c,0 0V.c,0 5/2/2005 13'0~as PM lesl and Pell I <'\.. / 0<e0~'O ,o"'~\· rrt<;'~v ~ .,.'i;\'V/ 

5/2/200513:15 292 71 e Cooler PM 5/2/05 'V~ ~~,)!, ~" / 

5/2/200513:30 291 71 43 264 ~~ / 

229 

229 

229 

230 

-7.3 2260 

2223 

2274 

2328 

1833 

1827 

1819 

1820 

-27.6 -20.3 13562 

13338 

13646 

13966 

136 

133 

136 

140 5/2/200513:45 ~93 91 74 69 43 263 

43 264 

Run 1 1400-1507 

5/2/2005 14:00 295 

5/2/2005 14:15 294 

5/2/2005 14:30 292 

5/2/2005 14:45 293 

5/2/2005 15:00 297 

5/2/200515:15 292 

Averages 294 

Run 2 1555-1704 

5/2/2005 15:45 290 

5/2/2005 16:00 297 

5/2/200516:15 295 

5/2/2005 16:30 278 

5/2/2005 16:45 279 

5/2/200517:00 274 

Averages 285 

Run 3 1750-1859 

5/2/200518:00 261 

5/2/200518:15 265 

5/2/2005 18:30 263 

5/2/2005 18:45 265 

5/2/2005 19:00 263 

Averages 264 

70 

70 

69 

77 

69 

76 

72 

70 

67 

70 

39 

68 

65 

63 

67 

68 

69 

70 

71 

69 

42 

42 

41 

47 

41 

47 

44 

43 

40 

42 

42 

43 

40 

42 

43 

43 

44 

45 

45 

44 

267 

266 

263 

263 

269 

264 

265 

263 

270 

267 

281 

254 

248 

264 

237 

241 

238 

240 

238 

239 

232 

231 

229 

229 

234 

229 

231 

229 

235 

232 

245 

221 

216 

230 

207 

209 

207 

209 

207 

208 

-7.3 

-7.3 

-7.2 

-7.2 

-7.1 

-7.1 

-7.1 

-7.1 

-6.9 

-7.1 

-7.0 

-7.2 

-7.1 

-6.9 

-6.8 

-6.8 

-7.0 

-6.8 

-6.9 

-6.8 

-6.9 

-6.8 

-6.8 

2396 

2469 

2480 

2448 

2430 

2394 

2436 

2431 

2431 

2431 

2426 

2360 

2328 

2401 

1608 

1691 

1773 

1821 

1841 

1747 

1814 

1815 

1835 

1834 

1836 

1837 

1828 

1825 

1836 

1826 

1836 

1842 

1838 

1834 

1807 

1815 

1814 

1823 

1822 

1816 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-28 

-26.6 

-26.7 

-26.7 

-26.7 

-26.7 

-26.7 

-20.3 

-20.3 

-20.4 

-20.4 

-20.5 

-20.5 

-20.5 

-20.5 

-20.6 

-20.5 

-20.6 

-20.4 

-20.5 

-20.7 

-20.8 

-20.8 

-21 

-19.9 

-19.9 

-19.9 

-19.9 

-19.9 

-19.9 

14374 

14814 

14879 

14688 

14578 

14361 

14616 

14589 

14589 

14589 

14557 

14160 

13968 

14409 

9646 

10144 

10641 

10927 

11048 

10481 

144 

148 

149 

147 

146 

144 

146 

146 

146 

146 

146 

142 

140 

144 

96 

101 

106 

109 

110 

105 
".' 

.. :' ... 

" .. :.'.' 

Gc-. s .. s 10,- ~ /( l04Iey"'" 

~r-ess u ~ f~~ f-

" 

§~ I£M:~ '"' f«-rf, -v~ A f- J.. 100/,1>\ 

(3 or- 3.5 hr fc.s+ ) 

;)./00 - J.~/.5 

.~·30 -

'~'I5 --

'.. 

7~pSi 

7~fJS ( 

)~51 

\. 

\ , 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/3/2005 

Company Name: United Taconite 

Equipment & Operating Data 

Process Equipment Number! Identification: Line 1 Pellet Cooler SV047 

PM Test No.2 

1. Process Equipment Description: Pellet cooling after induration- Line 1 

June-99 

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO I .... Y_e_s ___ ......I 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months X I Remains unchanged from Test Plan 

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

ratios as appropriate) -~--~----------------------------------------------------------------------

Process Parameter: list type and units Run 1 Run 2 Run 3 

Greenballs out of drums, L TPH 278 280 283 

Greenball Feed Rate to the grate, L TPH 251 252 255 

Fired Pellet production Rate, L TPH 219 219 222 

Fuel Input (list units) Natural Gas MCF 124 131 123 

Heat Input (106 British thermal units/hour) 124 131 123 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): ~P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: ~P (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OFinlel ,oF oUIle0 and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF oper.lting temperature) 

APC equipment and parameter monitored Run I Run 2 Run 3 

NONE 

List pollutant & averaging basis-should reflect permit 

Continuous Opacity Monitor (list hourly average) 

NA 

Abbreviations: 

Monitor (list averaging basis): 

Monitor (list averaging basis): 

APC-air pollution control 

lbs.-pounds 

NONE 

Run 1 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

NONE NONE 

Run 2 Run 3 

in. w.c.-inches of water column 

~P- pressure drop 

NOTE: This form provides only a summary of the operating conditiol/s during the performance test. Additional alld more detailed records are 

required to meet the requirements of MillII. R. 7017.2035. Thisform is to be submitted as part of the performallce test report to: North, Metro, 

or South District, Performance Test Coordinator, MN Pollutiol/ COl/trol Agel/cy, 520 Lafayette Rd., St. Paul, MN 55155-4194. 
~r:,\ o.~,.y. 

,0' 00':\ ,,'0°<1 ~ \.0" 0'0:1' ... 0:1> ,,'00" ,,0'" 

<t" _,~ 1 J3' .I> &' -" "G .,1- ?'_ "'~ 0 '° ~0 0,0 ' (,~"" ';'0' 

. ,,~\')> \ ,~",o'l>. ,~",oO?~O"\~'O ~"'(O~O ."'~ '"'" S >lS'0\ 0"-~~,,' e""",e 

0 

,~''2'. _,-.\ '}> ~,;:V / ,.,,\/ .,0 G \\e'" ,O",?· >J.'iy ~"'~ ~ -<" W, 

O~'" ?O CP~ ",-4/ N ~.. G'· 0?0 \ • ,,'0· ," ?'- , dl'\-\-/ ~ (,0 (,O~ / ~\~ ,0 0 «,,0 ~ ~,;? / .~\(,;? .-0:' \ b.'l-"\). v<..0\}:P' 

Lin v ~\" / ,:. / 0~'O \~,0 ",'i-"c"/.'. .,. e;? / ,,0

5 

Ru: ; ~:!~_~;~~'er PM Test 2 513105 ~, G,0 (,~\O" ??' ;l' ??' f""'/ ,3<!-"'~<!-/ "'rs~'i-J· ,eO?'? 0' 0 ,,,e" (,~'" ,,~ >J.(,~ 51312005 8:30 ?? ??' / ,~o ,,\0,0 ,eO ~ 513120058:45 

276 

(,0 (,,,,0 cP~O 280 

277 

278 

281 

278 

70 

65 

70 

71 

70 

69 

42 

40 

42 

44 

43 

42 

249 

254 

249 

251 

254 

216 

221 

-9.9 

-10.0 

2055 

2070 

2105 

2070 

1831 

1818 

1828 

1842 

-23.4 

-23.4 

-13.5 

-13.4 

12333 

12418 

12633 

12418 

12326 

12426 

123 

124 

126 

124 

123 

124 

5/3/20059:00 

5/3/20059:15 

5/3/2005 9:30 

Averages 

Run 21018-1128 

5/3/2005 10:15 282 

5/3/2005 10:30 279 

5/3/2005 10:45 278 

5/3/2005 11 :00 281 

5/3/2005 11: 15 283 

5/3/2005 11 :30 282 

Averages 280 

Run 3 1225-1331 

5/3/2005 12:30 282 

5/3/2005 12:45 282 

5/3/2005 13:00 283 

5/3/200513:15 281 

5/3/2005 13:30 287 

Averages 283 

72 

71 

65 

69 

74 

67 

69 

68 

68 

68 

67 

70 

68 

45 

44 

38 

41 

43 

38 

41 

41 

40 

40 

39 

41 

40 

251 

255 

252 

251 

254 

251 

253 

252 

255 

254 

255 

253 

257 

255 

217 

219 

221 

219 

222 

219 

218 

221 

218 

221 

219 

222 

221 

222 

220 

224 

222 

-10.0 

-9.9 

-9.9 

-9.9 

-8.3 

-7.5 

-7.4 

-7.3 

-7.3 

-7.3 

-7.3 

-7.0 

-7.2 

-7.1 

-7.0 

-7.2 

-7.1 

2054 

2071 

2054 

2031 

1905 

2010 

2358 

2603 

2181 

2242 

2138 

1998 

1939 

1939 

2051 

1824 

1829 

1831 

1843 

1854 

1782 

1761 

1777 

1803 

1879 

1855 

1856 

1835 

1833 

1852 

-23.4 

-23.4 

-23.3 

-23.4 

-27.1 

-28.1 

-28.1 

-28.1 

-27.7 

-27.6 

-27.9 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-13.5 

-13.4 

-13.4 

-13.4 

-18.8 

-20.6 

-20.8 

-20.8 

-20.5 

-20.3 

-20.6 

-20.6 

-20.4 

-20.5 

-20.6 

-20.4 

-20.5 

12323 

12185 

11427 

12058 

14151 

15618 

13088 

13449 

12826 

11990 

11632 

11632 

12306 

123 

122 

114 

121 

142 

156 

131 

134 

128 

120 

116 

116 

123 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/3-4/2005 

~~~~~~---------­ Company Name: United Taconite 

Equipment & Operating Data 

Process Equipment Number/ Identification: Line 1 Pellet Cooler SV047 

PM10 Test 

June-99 

1. Process Equipment Description: Pellet cooling after induration- Line 1 

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO lL..y;..;e;:..:s::..-__ -l 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months X I Remains unchanged from Test Plan 

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

ratios as appropriate) --~--~----------------------------------------------------------------------

Process Parameter: list type and units Run 1 Run 2 Run 3 

Greenballs out of drums, L TPH 279 274 282 

Greenball Feed Rate to the grate, L TPH 256 246 252 

Fired Pellet production Rate, L TPH 223 214 219 

Fuel Input (list units) Natural Gas MCF 116 166 156 

Heat Input (106 British thermal unitslhour) 116 166 156 

6. Summmize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): ~P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: ~P (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OFinlel ,oF oUlleJ and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF operating temperature) 

APC equipment and parameter monitored Run 1 Run 2 Run 3 

NONE NONE NONE NONE 

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 

Continuous Opacity Monitor (list hourly average) 

Monitor (list averaging basis): 

Monitor (list averaging basis): 

Abbreviations: APC-air pollution control 

lbs.-pounds 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

~P- pressure drop 

NOTE: Tlzis form provides ollly a summary of the operatillg cOllditiollS durillg the perform all ce test. Additiollal alld more detailed records are 

required to meet the requiremellts of Millll. R. 7017.2035. Thisform is to be submitted as part of the perform all ce test report to: North, Metro, 

or South District, Performallce Test Coordillator, MN Pollutioll COlltrol Agellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194. 
v~'i:>' 11. o.~ ,,1 ~ ~. ~\.o ~'I-' < 1 SJ-.... ~ • ~ .-~ ~~e<) ~~e" ,)_ ,,~J' ~'!-."'_ .{) ~'I- »,<p' c' ~,. ,e ,c<' ~"') ",,,, ,c<" 

~6<.'~ 0'1-" J ~",!,'< "" ,~'" (,0">' ~,,<$'e .<'. ",e'o ~"" G 0') ... " 

Q?>\.?> ~~\.w ' G 0"'''' < _,,p;_ < d'" "." ,,!-~'- .• <~S < 'o~ ~ ,,,<' G "'~< OV •• ' ,'u • ,,(V '1-" ,e' 

Pellet Cool v ~ .. ' < , (,0 ~", ~\<. ,,~'< ,,~, - "S '1-' ," 

PM 

51312005 

1 0 Run 

16-15 

;', ~~~',ust _ 753) • SV04' PM10 t 

est 

~,\. < "" ... " 

C,e 

,c~·'·· ~~' )" ~,/-~'i-'/-J , -0" '1-' 

< 

,_~,ru ,/-'0,'/-< ,\ -<.' :-

<'i-~,,-~, < 

,,!-,, ~ ,->Ie, , c<,,~~e< '0 

51312005 16:30 289 ~~ < ~~' J ->l

P 

51312005 16:45 285 ~~' < 

< • 

,c~·,e .~ 0 '0'&'" .V c,~ • ~-:fo' ",c,~ 5131200517:00 290 C,e GO'c" ,c~o,e 51312005 ,,: 15 275 C,O 

68 

70 

69 

69 

71 

42 

43 

262 

259 

263 

228 

225 

-7.1 

-6.9 

1993 

1993 

1993 

2040 

2011 

1824 

1830 

1828 

1824 

-27.6 

-27.6 

-20.5 

-20.7 

11959 

11959 

11959 

12240 

12065 

11420 

11041 

120 

120 

120 

122 

121 

114 

110 

105 

116 

5/3/2005 17:30 272 

5/3/2005 17:45 275 

5/3/2005 18:00 272 . 274 

Averages 279 

PM10 Run 2 (1150.1310) 

5/4/2005 11 :45 276 

5/4/2005 12:00 269 

5/4/2005 12:15 276 

5/4/2005 12:30 266 

5/4/2005 12:45 268 

5/4/2005 13:00 279 

5/4/200513:15 282 

274 

PM10 Run 3 (1350·1553) 

5/4/2005 13:45 282 

5/4/2005 14:00 284 

5/4/200514:15 282 

5/4/2005 14:30 284 

5/4/2005 14:45 278 

5/4/2005 15:00 277 

5/4/200515:15 282 

5/4/200515:30 281 

5/4/2005 15:45 280 

5/4/2005 16:00 285 

282 

72 

71 

45 

67 

71 

71 

72 

74 

72 

73 

75 

73 

75 

76 

75 

74 

73 

71 

73 

70 

68 

69 

72 

42 

43 

45 

45 

44 

45 

44 

44 

44 

45 

45 

43 

44 

44 

44 

45 

45 

44 

44 

44 

42 

42 

41 

41 

41 

43 

249 

246 

248 

246 

273 

256 

250 

242 

249 

237 

239 

250 

251 

246 

252 

253 

251 

254 

249 

249 

252 

253 

253 

257 

252 

229 

216 

214 

216 

214 

238 

223 

217 

211 

217 

206 

208 

218 

219 

214 

219 

220 

219 

221 

217 

216 

220 

220 

220 

223 

219 

-6.9 

-6.9 

-7.0 

-7.1 

-7.0 

-6.9 

-7.0 

-7.2 

-7.1 

-7.1 

-7.2 

-7.6 

-7.7 

-7.6 

-7.4 

-7.4 

-7.5 

-7.5 

-7.4 

-7.3 

-7.4 

-7.6 

-7.6 

-7.5 

-7.3 

-7.4 

1903 

1840 

1747 

1940 

2802 

2802 

2802 

2802 

2753 

2686 

2694 

2763 

2812 

2891 

2964 

3059 

2621 

2552 

2242 

2250 

2276 

2276 

2594 

1847 

1851 

1845 

1847 

1837 

1821 

1829 

1834 

1829 

1847 

1843 

1821 

1832 

1813 

1811 

1816 

1805 

1823 

1835 

1830 

1817 

1824 

1828 

1820 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-28 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-28 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-28 

-20.7 

-20.7 

-20.6 

-20.5 

-20.6 

-20.7 

-21 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92 

10484 

11641 

16812 

16812 

16812 

16812 

16515 

16117 

16165 

16578 

16871 

17348 

17783 

18356 

15727 

15314 

13455 

13498 

13654 

13654 

15566 

168 

168 

168 

168 

165 

161 

162 

166 

169 

173 

178 

184 

157 

153 

135 

135 

137 

137 

156 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/3/2005 

Company Name: United Taconite 

Equipment & Operating Data 

June-99 

Process Equipment Number! Identification: Line 1 Waste Gas - SV046 

Fluorides and Gases 

1. Process Equipment Description: Line 1 Kiln Gas Exhaust - Wet Scrubber Control Device 

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO L-IY_e_s ___ -, 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) ofJast maintenance/cleaning within 6 months x I Remains unchanged from Test Plan 

5. Process rate (amount of raw material or finished product per hour, wet or dry basis) while combusting (Jist fuel type(s) and 

ratios as appropriate) ~~~-------------------------------------------------------------

Process Parameter: list type and units Run 2 Run 3 Run 4 

Greenballs out of drums, L TPH 284 287 274 

Greenball Feed Rate to the grate, L TPH 254 261 259 

Fired Pellet production Rate, L TPH 221 227 226 

Fuel Input (list units) Natural Gas MCF 117 120 108 

Heat Input (106 British thermal unitslhour) 117 120 108 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): tlP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: tlP (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OFinlet ,oFoutleU and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF operating temperature) 

APC equipment and parameter monitored Run 2 Run 3 Run 4 

Scrubber Pressure Drop, In.W.C. 20.4 20.5 20.6 

Scrubber Water Pressure, PSI not collected not collected not collected 

Note: NaOH added to scrubber water during test on on on 

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 

Continuous Opacity Monitor (Jist hourly average) 

Monitor (Jist averaging basis): 

Monitor (Jist averaging basis): 

Abbreviations: APC-air pollution control 

lbs.-pounds 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

tlP- pressure drop 

NOTE: This form provides ollly a summary of the operatillg cOllditiolls durillg the perform all ce test. Additiollal alld more detailed records are 

required to meet the requirements of MimI. R. 7017.2035. This forl1l is to be submitted as part of the performallce test report to: North, Metro, 

01' SOl/th District, Performallce Test Coordillator, MN Pol/utioll COlltrol Agellcy, 520 Lafayette Rd., St. Pal/I, ilfN 55155-4194. 
~~ o.~v.". "''''' ~ .i5 ,0 ~ ~O"'~" ~ O~1 ~~_,' ",~~0<\ ".,1. 0'0

9

'" .",1 0 ,1-~ ~ • .t> .0<" -" _,G '" 

o\.'~" . ~ ..,t" ,,~" 0'" ,.,. 0· ,<1- d~' -,'-

<"\,<>''<> '? ~ cP :p' O~) ,-,>1'/ N ".. 

"'\) ,'l' 

G'-"'. 

C~& ..,,-'" ~,,<,,' .,O~· .",1 ",-

0 ",,,-~ S ~,,_\ "",11P 

" 0'" 

< ",,0<fo 

",e .~ v ,.\.V/ 1 G 0'" / ,0 . .t> .• \/ S,,", ", ."" 

Line 1 Wa,le '0 ~\\. / \\.15' .o~\· ,.0 ~" '1-),. .~\C / .-<' .':' .~, o

· ,p~" Run 1 1120- Ga, Fluo"de, and An ~ G'.. ~o,,\· ,,'1-''0 ,,-"'.':" '1-.':" ,,9\/ ",G "" 51312005 51312005 11',';6 11:30 (up,el 283 run) alyz., Te,l, G •• ' / •• ' f' •• , / .'1-"" •• ' / ",,.s1"-/ ,0'$>.\.0 O· 0' ,~_o '" .V C~'i- 0 ~,,_\ "'c~ 51312005 11'45 282 C· d

P

' "»,,," 

5/3/2005 12:00 281 G' 

74 

67 

64 

66 

67 

68 

68 

43 

38 

251 

253 

254 

255 

218 

221 

221 

222 

-7.3 2358 

2603 

2804 

2898 

2533 

2242 

2573 

1761 

1777 

1789 

1831 

1922 

1879 

1826 

-27.7 -20.5 14151 

15618 

16827 

17386 

15196 

13449 

15438 

142 

156 

168 

174 

152 

134 

154 

. 283 

5/3/2005 12:15 

5/3/2005 12:30 

Averages 

Run 2 1345-1449 

282 

282 

282 

5/3/2005 13:45 284 

5/3/2005 14:00 286 

5/3/200514:15 283 

5/3/200514:30 284 

5/3/200514:45 285 

Averages 284 

Run 3 1545-1650 

5/3/2005 15:45 286 

5/3/2005 16:00 285 

5/3/200516:15 289 

5/3/2005 16:30 285 

5/3/2005 16:45 290 

Averages 287 

Run 41730-1837 

5/3/2005 17:30 275 

5/3/200517:45 272 

5/3/200518:00 274 

5/3/2005 18: 15 273 

5/3/2005 18:30 270 

5/3/2005 18:45 278 

Averages 274 

71 

71 

72 

72 

73 

72 

66 

66 

68 

70 

69 

68 

72 

71 

45 

29 

67 

69 

59 

37 

38 

39 

41 

39 

41 

41 

41 

42 

42 

41 

41 

42 

42 

43 

42 

42 

45 

44 

45 

44 

44 

45 

44 

254 

255 

254 

253 

255 

253 

254 

254 

254 

261 

260 

262 

259 

263 

261 

248 

246 

273 

288 

247 

254 

259 

221 

222 

221 

220 

222 

220 

221 

221 

221 

227 

226 

228 

225 

229 

227 

216 

214 

238 

251 

215 

221 

226 

-7.3 

-7.2 

-7.3 

-7.1 

-7.0 

-7.2 

-7.1 

-7.2 

-7.2 

-7.3 

-7.2 

-7.2 

-7.3 

-7.1 

-7.1 

-6.9 

-6.9 

-7.1 

-7.1 

-7.0 

-6.9 

-6.9 

-6.9 

-7.0 

-7.0 

1906 

1907 

1953 

1992 

1992 

1950 

1993 

1993 

1993 

1993 

1993 

1993 

1903 

1840 

1747 

1734 

1767 

1779 

1795 

1835 

1823 

1822 

1830 

1827 

1827 

1829 

1827 

1824 

1830 

1828 

1828 

1851 

1845 

1847 

1828 

1821 

1837 

1838 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-27.6 

-20.3 

-20.4 

-20.3 

-20.5 

-20.6 

-20.4 

-20.5 

-20.4 

-20.4 

-20.3 

-20.4 

-20.4 

-20.3 

-20.5 

-20.5 

-20.7 

-20.7 

-20.5 

-20.5 

-20.6 

-20.7 

-20.7 

-20.7 

-20.6 

-20.6 

11436 

11441 

11716 

11950 

11950 

11698 

11959 

11959 

11959 

11959 

11959 

11959 

11420 

11041 

10484 

10404 

10602 

10674 

10771 

114 

114 

117 

119 

119 

117 

120 

120 

120 

120 

120 

120 

114 

110 

105 

104 

106 

107 

108 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/4/2005 

Company Name: United Taconite 

Equipment & Operating Data 

June-99 

Process Equipment Number/ Identification: Line 1 Waste Gas· SV046 

Ontario Hydro Test 

I. Process Equipment Description: Line 1 Kiln Gas Exhaust - Wet Scrubber Control Device 

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO I'-y_e_s ___ -' 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months x I Remains unchanged from Test Plan 

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

ratios as appropriate) --~--~----------------------------------------------------------------------

Process Parameter: list type and units Run I Run 2 Run 3 

Greenballs out of drums, L TPH 276 266 274 

Greenball Feed Rate to the grate, L TPH 247 238 241 

Fired Pellet production Rate, L TPH 215 207 210 

Fuel Input (list units) Natural Gas MCF 166 148 133 

Heat Input (106 British thermal unitslhour) 166 148 133 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generalIy monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): LlP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: LlP (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OFinlet ,oF oUlleJ and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF operJling temperature) 

APC equipment and parameter monitored Run 1 Run 2 Run 3 

Scrubber Pressure Drop, In.W.C. 20.4 20 21 

Scrubber Water Pressure, PSI 72 72 72 

Note: NaOH added to scrubber water during test on on on 

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 

Continuous Opacity Monitor (list hourly average) 

Monitor (list averaging basis): 

Monitor (list averaging basis): 

Abbreviations: APC-air pollution control 

lbs.-pounds 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

LlP- pressure drop 

NOTE: This form provides ollly a summary of the operatillg cOllditiolls during the performance test. Additional alld more detailed records are 

reqllired to meet the requiremellts of MbllI. R. 7017.2035. This form is to be submitted as part of the peljormance test report to: North, Metro, 

or South District, Performallce Test Coordinator, MN Pol/utioll COlltrol Agellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194. 
A'\'i>'1 

o.~V"· , 0' •• , :1 '<f>" 

< ,0" .~" •• ~ """" ,c"~ .,1 y" .",1 "," • ,1 AI' ,,,,. ,e 9>" ,,,,, e' ~o . ,pi>"] \ ,,~<f" ,,~<:p. ,c",~e ,,,,,,,,,e ",1 ",,'0 S ,,# G ,; .", "",e ,. 

.6'"""" O"'~ , N ),:<, ' ,.:<'" o<>,e G' •• "e" • ,.~. ,.",,,~ , .",1 ,0 < ,",e' 0'" ,v-5' 1 GO" GO",N , ,'" ,0 • ,,,e· ".' , ,GO" " ", . ,~, •• '" "~",,, , • .;f. 

Onla,'o H d, '" '" ' ,,,1 , ","~ ~"e -<" .. , "~x ".' §" ~o .' ,'f' . 5/4120OS ~ 1 '~OT ost;;, Uoo 1 W .. te G .. Stack 0' G'" •• S".' :1',,,,, ... .;f. .. , ~~s1") ••• 0' ,,:,'1-

1

, .. dO 

5/4120OS 11015 280 72 72 44 43 • •• " •• " G' ,c""'· •• " ~~S1 G"O>" ",.'''~ .,s.?>'\.eO 

G~G 

Test 3 Run 11130-1341 

5/4/2005 11 :30 276 

5/4/2005 11 :45 276 

5/4/2005 12:00 269 

5/4/200512:15 276 

5/4/2005 12:30 266 

5/4/2005 12:45 268 

5/4/2005 13:00 279 

5/4/200513:15 282 

5/4/2005 13:30 282 

5/4/2005 13:45 282 

Averages 276 

5/4/2005 14:00 284 

Test 3 Run 2 1410-1618 

5/4/200514:15 282 

5/4/2005 14:30 284 

5/4/200514:45 278 

5/4/2005 15:00 277 

5/4/200515:15 282 

5/4/200515:30 281 

5/4/2005 15:45 280 

5/4/2005 16:00 285 

5/4/200516:15 147 

Averages 266 

5/4/200516:30 112 

5/4/200516:45 209 

5/4/200517:00 235 

68 

71 

71 

72 

74 

72 

73 

75 

73 

75 

72 

76 

75 

74 

73 

71 

73 

70 

68 

69 

64 

71 

62 

73 

75 

42 

44 

44 

45 

45 

43 

44 

44 

44 

45 

44 

45 

44 

44 

44 

42 

42 

41 

41 

41 

41 

42 

43 

46 

46 

254 

252 

250 

250 

242 

249 

237 

239 

250 

251 

252 

252 

247 

253 

251 

254 

249 

249 

252 

253 

253 

257 

125 

238 

93 

181 

206 

221 

219 

218 

217 

211 

217 

206 

208 

218 

219 

220 

219 

215 

220 

219 

221 

217 

216 

220 

220 

220 

223 

109 

207 

81 

158 

180 

-7.8 

-7.6 

-7.4 

-7.2 

-7.1 

-7.1 

-7.2 

-7.6 

-7.7 

-7.6 

-7.5 

-7.4 

-7.4 

-7.5 

~5 

~.4 

~~ 

~.4 

~~ 

~~ 

~B 

~.3 

~~ 

-7 

-5.1 

-7.4 

-6.8 

2704 

2749 

2753 

2802 

2802 

2802 

2802 

2753 

2686 

2694 

2750 

2812 

2766 

2891 

2964 

3059 

2621 

2552 

2242 

2250 

2276 

2276 

1938 

2464 

1709 

1902 

1534 

1816 

1823 

1825 

1821 

1829 

1834 

1829 

1847 

1843 

1821 

1819 

1813 

1828 

1811 

1816 

1805 

1823 

1835 

1830 

1817 

1824 

1828 

1843 

1825 

1898 

1889 

1833 

-27.8 

-27.6 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-27.8 

-22.9 

-27 

-23.5 

-26.0 

-26.2 

-20.0 

-20.0 

-20.4 

-20.6 

-20.7 

-20.7 

-20.7 

-20.2 

-20.1 

-20.2 

-20.3 

-20.4 

-20.4 

-20.4 

-20.4 

-20.4 

-20.5 

-20.4 

-20.2 

-20.2 

-20.3 

-20.5 

-17.8 

-20 

-18.3 

-18.7 

-19.4 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

92.3 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~.3 

~B 

90 

74.1 

83.2 

83.6 

16226 

16495 

16516 

16812 

16812 

16812 

16812 

16515 

16117 

16165 

16503 

16871 

16594 

17348 

17783 

18356 

15727 

15314 

13455 

13498 

13654 

13654 

11627 

14785 

10255 

11411 

9202 

162 

165 

165 

168 

168 

168 

168 

165 

161 

162 

165 

169 

166 

173 

178 

184 

157 

153 

135 

135 

137 

137 

116 

148 

103 

114 

92 

~G« «ve\ 
A\.'iJ"I 

o.~Q'" < , 0' 0>' , ,p" ," o~., ~ o· ,y1'" .,.,,,~ ",<, ",<,' < "JJ' ,."" .,.,,, ." <,0 

.' . R>' .'" • .' ,0'· (".' .. ' 

, """J' , ,,~o ,.",0, \0""'. ,,,, •• < ",' ~ S~' ".'S' S",·· ."."S" O,<,~J" NJ'''j'' ?!""v <,'.cP ,.".'S .,O~. \0>J.0' ,."" ,0 < ,,,e

s 

0'''' ~",,5', (,0" (,0'" ' .,\S ,0 <; .,,,.1> .g;." ,,(, i' -0 ", ' .~'O.'" <",;J" , .-<!-

00''''0 H .. 0" """, •• ~ \.'. ,,,,,,, ", ,,', , ,." <,0"' .", , 

51412005 ;;:~ 5

T 

"';: L,o, , W",. Gos S',ck ",<' (,.«" •• ' S'''' .' f""" ."'-c''''' <,p''') , 0 o. 0' ":'~' , >< (,'-C 

5141200517,30 27: 78 44 • <f?" •• " \0" .. .., <,p' ".,,,. 

5/4/200517:45 2 n 76 M 44 (,' •• " \0';' cP 

0\7>'l.eO 

G~G 

Test 3 Run 3 1805-2035 

5/4/200518:00 274 

5/4/200518:15 276 

5/4/200518:30 273 

5/4/200518:45 273 

5/4/200519:00 274 

5/4/200519:15 274 

5/4/2005 19:30 273 

5/4/2005 19:45 273 

5/4/2005 20:00 272 

5/4/200520:15 275 

5/4/2005 20:30 280 

Averages 274 

5/4/2005 20:45 283 

5/4/200521 :00 289 

5/4/200521:15 287 

5/4/2005 21 :30 288 

5/4/2005 21 :45 284 

5/4/2005 22:00 289 

5/3/2005 19:45 285 

5/3/2005 20:00 276 

5/3/200520:15 266 

5/3/2005 20:30 277 

5/3/2005 20:45 287 

5/3/200521:00 287 

5/3/200521:15 286 

5/3/2005 21 :30 286 

5/3/2005 21 :45 285 

5/3/2005 22:00 287 

76 

77 

80 

79 

77 

82 

77 

77 

77 

76 

77 

78 

77 

77 

77 

78 

79 

79 

74 

76 

74 

75 

76 

72 

73 

74 

75 

78 

43 

44 

44 

47 

46 

45 

47 

44 

45 

45 

44 

44 

45 

42 

42 

41 

43 

43 

43 

47 

48 

47 

47 

47 

45 

45 

47 

47 

49 

231 

241 

240 

242 

242 

240 

240 

242 

240 

241 

241 

240 

242 

246 

241 

248 

254 

252 

252 

249 

253 

258 

248 

239 

249 

258 

259 

258 

258 

257 

258 

201 

210 

209 

210 

211 

209 

209 

211 

209 

210 

209 

208 

211 

214 

210 

216 

221 

219 

219 

217 

220 

224 

216 

208 

217 

224 

226 

224 

225 

224 

225 

-7.4 

-7.0 

-7.1 

-7.2 

-7.2 

-7.3 

-7.4 

-7.3 

-7.3 

-7.2 

-7.4 

-7.5 

-7.6 

-7.6 

-7 

-7.7 

-7.6 

-7.6 

-7.6 

-7.5 

-7.4 

-6.9 

-6.9 

-6.9 

-6.9 

-6.9 

-6.9 

-7.0 

-7.0 

-7.0 

-7.0 

1717 

1957 

2309 

2307 

2317 

2383 

2375 

2327 

2282 

2229 

2145 

2088 

1994 

1948 

2218 

1948 

1948 

2006 

2105 

2152 

2158 

2342 

2339 

2225 

2091 

2010 

1966 

1998 

2067 

2093 

2136 

1833 

1819 

1826 

1834 

1818 

1819 

1838 

1840 

1842 

1843 

1846 

1843 

1849 

1839 

1837 

1826 

1825 

1818 

1806 

1823 

1827 

1821 

1839 

1858 

1855 

1846 

1835 

1817 

1817 

1823 

1822 

-27.6 

-27.7 

-27.7 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-27.9 

-28 

~~ 

~~ 

~.9 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

~~ 

-20.2 

-20.7 

-20.6 

-20.7 

-20.7 

-20.6 

-20.5 

-20.6 

-20.6 

-20.7 

-20.5 

-20.4 

-20.3 

-20.3 

-21 

-20.2 

-20.3 

-20.3 

-20.3 

-20.4 

-20.5 

-20.7 

-20.7 

-20.7 

-20.7 

-20.7 

-20.7 

-20.6 

-20.5 

-20.6 

-20.6 

90.4 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

92 

91.8 

91.8 

91.8 

91.8 

91.8 

91.8 

92.1 

92.1 

92.1 

92.1 

92.1 

92.1 

92.1 

92.1 

92.1 

92.1 

10300 

11744 

13857 

13840 

13901 

14295 

14248 

13963 

13693 

13375 

12873 

12528 

11964 

11688 

13306 

11688 

11688 

12039 

12633 

12915 

12950 

14051 

14033 

13352 

12548 

12058 

11798 

11991 

12399 

12557 

12816 

103 

117 

139 

138 

139 

143 

142 

140 

137 

134 

129 

125 

120 

117 

133 

117 

117 

120 

126 

129 

129 

141 

140 

134 

125 

121 

118 

120 

124 

126 

128 

~G(,; (,;Qe\ 
S-/#/J5 

Date 

II; v!? ~ 

1/; /s 

1/: 3& 

11.' if.> 

/);170 

" 15" 

.. :1(;> 

" rl{ 

I ,(Jrl 1M 

:1'; 

.3'" 

1'5" 

;1;00 

. (s~ 

. J~ 

: if" 

'? ' d'cJ 

:IS 

J~ 

'Is 

J/'/,?P 

;Ie; 

:117 

:<-15' 

"..., iJO 

; Ie;-

Jv 

'15' 

;.,. od' 

; Itt' 

:30 

''it;' 

;; QiJ 

7: 6" 

. : )() 

'/5-

Ii' .' r? ,) 

L-,'v" ~ J 

I! 0 .,a('R.5.J 

/} W?5'f~ &.?,f 

7?-

~..J7.7-

77_ 

7"2-

7.:?-

7;:2. 

7~, 

7';).. 

7;? 

7;;2 

7;;L 

7:;>.· 

7;;J. 

2:1-

7;2 

7;J. 

7.J,.. 

7;;L 

7;;4. 

7,J7./-

2;;<-

7';1-. 

7;;;-

7;;;l. 

7::;L 

"7-;?-

7;;;--

7,..?-

7.,;1 

7::z.. 

1:>-

77-

??-

7'?--

7:r 

Contractor Checklist .;~~~::' ,. 

MSHA Site Specific 

-NAME.- , Vehicle pass # Certificate? Hazard Training? 

. 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

Test Date(s): 5/5/2005 

Company Name: United Taconite 

Equipment & Operating Data 

June-99 

Process Equipment Number! Identification: Dump Zone Scrubber- SV116 

1. Process Equipment Description: Scrubber serving the Line 1 Pellet Cooler Discharge Zone- Line 1 

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO IL.Y;..-e:..;s:.-__ ..J 

3. Include copy of production records or instruments which indicates rate of production or operation of the equipment, i.e. units per 

hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months x I Remains unchanged from Test Plan 

5. Process rate (amount of raw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

ratios as appropriate) ~~~-------------------------------------------------------------

Process Parameter: list type and units Run I Run 2 Run 3 

Greenballs out of drums, L TPH 282 285 286 

Greenball Feed Rate to the grate, L TPH 256 258 254 

Fired Pellet production Rate, L TPH 223 224 221 

Fuel Input (list units) NA NA NA 

Heat Input (106 British thermal units/hour) NA NA NA 

6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, 

averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

• Scrubber (list type of scrubber): 6P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: 6P (in. w.c.) 

(gpm and psig) 

• Catalytic Incinerator:(OFinlel ,OF oUlleU and Thermal • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF operJting temperature) 

APC equipment and parameter monitored Run 1 Run 2 Run 3 

Scrubber water flow rate, GPM 94.3 93.7 93.6 

Scrubber pressure drop, in.We 3.9 4.0 4.0 

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 

Continuous Opacity Monitor (list hourly average) 

Monitor (list averaging basis): 

Monitor (list averaging basis): 

Abbreviations: APC-air pollution control 

lbs.-pounds 

gpm.-gaIIons per minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

6P- pressure drop 

NOTE: This form provides ollly a slim mary of the operatillg cOllditiolls dllrillg tlte perform all ce test. Additiollal alld more detailed records are 

required to meet the requiremellts of Millll. R. 7017.2035. This form is to be submitted as part oftlte performallce test rep011 to: North, Metro, 

or South District, Performallce Test Coordillator, MN Pol/lltioll COlltrol Agellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194. 
SV116 Time dP GPM 

1144 3.94 95.0 

1203 3.91 94.0 

1218 3.95 94.5 

1234 3.96 93.5 

1246 4.00 94.6 

1300 3.91 94.0 

Average R1 3.95 94.27 

1431 3.99 93.4 

1446 3.92 93.7 

1500 3.97 94.6 

1516 4.08 93.5 

1531 3.95 93.3 

Average R2 4.0 93.7 

1616 3.98 92.8 

1631 3.9 93 

1646 4 94.7 

1649 3.95 95.5 

1716 3.98 91.7 

1727 3.94 93.7 

Average R3 4.0 93.6 

1745 3.89 94.1 Readings Taken to coincide with SV045 Run 4 

1800 3.92 92.1 Readings Taken to coincide with SV045 Run 4 

1816 4.02 91.9 Readings Taken to coincide with SV045 Run 4 

1830 3.96 91.2 Readings Taken to coincide with SV045 Run 4 

1845 3.99 93.7 Readings Taken to coincide with SV045 Run 4 

1900 3.94 93 Readings Taken to coincide with SV045 Run 4 

Average R4 4.0 92.7 
~~~\ ruO\ ru~1 ~ O~ ru'O''V 0'" x~\ ~'I. 0 1'(l' ~ee ~ G ~ ,0 ~ ~ 0.... z,.c,e ~~e 1 "}~ «~ «~ ~z,.'l.e ~~t(\ ~I'-S ~ ...,bo .... • ,\,:,7-'0<0. .......,7-0'0· C;~c,~ ~\e'l.~ ~ .... '0~ 

...,'!j~ .. ~~\.. o;~\.. c:p'l.e . eO ~e . \G.3 • G~0 ~G<; ~). ~-.l.. N ..., N ..., '1.0 ~\t bo"~ \~e\ <;~e\ «6\(\'1.~ cP GO~" GO~" ~z,.\\~ ~z,.'l.eo ~\.~.. 'l-.1>\eo 'l-.1>\eo 

\)1>\1> <ol'-\'\''' <;\\.'\.. <;\\.'\ .. 6tee~ c,z,.\c,v ««"" G~c,-S G1>\c,-S 

Line 1 Cooler Discharge SV045 and SV116 

Run 1 (1155-1259 SV116) (1155-1259,1329-1340 SV045) 

5/5/2005 12:00 281 78 46 248 

5/5/200512:15 279 78 46 248 

5/5/2005 12:30 284 79 46 252 

5/5/200512:45 285 76 45 253 

5/5/2005 13:00 283 46 43 280 

SV116 282 256 

5/5/2005 13:30 284 23 42 303 

5/5/200513:45 281 62 45 264 

SV045 282 63 45 264 

Run 2 1430-1545 

5/5/200514:30 282 69 46 258 

5/5/2005 14:45 285 72 46 259 

5/5/2005 15:00 285 73 46 257 

5/5/2005 15: 15 292 75 45 263 

5/5/2005 15:30 283 74 46 256 

5/5/2005 15:45 284 78 48 254 

SV045 and SV116 285 73 46 258 

Run 3 1610-1725 

5/5/200516:15 286 81 51 257 

5/5/2005 16:30 287 81 51 257 

5/5/200516:45 286 83 52 255 

5/5/200517:00 287 89 56 254 

5/5/200517:15 285 95 59 249 

SV116 286 86 54 254 

5/5/200517:30 287 102 64 249 

SV045 286 89 55 253 

Run 4 SV045 only 

5/5/2005 17:45 288 111 69 247 

5/5/2005 18:00 283 116 71 237 

5/5/2005 18: 15 289 120.6 71 240 

5/5/2005 18:30 273 111.7 67 228 

5/5/2005 18:45 245 107.8 69 206 

5/5/2005 19:00 250 107.5 66 209 

Average 271 112 69 228 

216 

215 

219 

220 

244 

223 

264 

230 

230 

225 

225 

224 

229 

223 

221 

224 

223 

223 

222 

221 

217 

221 

216 

220 

215 

206 

209 

198 

179 

182 

198 

2134 

2074 

2090 

2090 

2098 

2097 

2140 

2140 

2110 

2140 

2163 

2190 

2152 

2213 

2236 

2182 

2163 

2137 

2110 

2087 

2121 

2124 

2087 

2118 

2106 

2138 

2113.8 

2143.6 

2158.1 

1933.5 

2099 

12805 

12446 

12541 

12541 

12586 

12584 

12841 

12841 

12657 

12841 

12976 

13142 

12911 

13280 

13414 

13094 

12976 

12824 

12659 

12523 

12724 

12741 

12524 

12705 

12635 

12826 

12683 

12861 

12948 

11601 

12593 

128 

124 

125 

125 

126 

126 

128 

128 

127 

128 

130 

131 

129 

133 

134 

131 

130 

128 

127 

125 

127 

127 

125 

127 

126 

128 

127 

129 

129 

116 

126 
OPERATING DATA SUMMARY FOR PROCESS SOURCES 

June-99 

-:-:--:-:----:-=-.;:,.5/;..;5:.;./~2.;:,.0.;:,.0.;:,.5----ss Equipment Number/ Identification: ____ S=..V..:....::O;..;4.,::5 ________ _ 

Company Name: United Taconite 

Test Date(s): 

Equipment & Operating Data 

1. Process Equipment Description: Scrubber serving Line 1 Vibrating feeder 

2. Were the process and control equipment operated consistent with normal operating procedure? IYes 

3. Include copy of production records or instruments which indicates rate of production or operation of the 

equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 

4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months I X IRemains unchanged from Test Plan 

5. Process rate (amount of raw material or finished product per hour, wet or dry basis) while combusting 

ratios as appropriate) -~--~----------------------------------------------------------------

Process Parameter: list type and units Run 1 Run 2 Run 3 

Greenballs out of drums, L TPH 282 285 286 

Greenball Feed Rate to the grate, L TPH 264 258 253 

Fired Pellet production Rate, L TPH 230 224 220 

Fuel Input (list units) NA NA NA 

Heat Input (106 British thermal unitslhour) NA NA NA 

6. Summarize control equipment operating data documented during testing. Values reported should reflect 

maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) 

Examples of APC equipment and parameters generally monitored. Monitor as specified in the test 

• Scrubber (list type of scrubber): L'.P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: L'.P (in. w.c.) 

(gpm and psig) 

Run 4 

271 

228 

198 

NA 

NA 

• Catalytic Incinerator:(OFinlct ,oF outle~ and Them1al • Number and identity of operating electrostatic precipitator field(s) 

Incinerator: (OF operating temperature) 

APC equipment and parameter monitored Run 1 Run 2 Run 3 Run 4 

Scrubber Pressure Drop, in we 0.81 7.5 7.5 7.6 

Scrubber Water Flow Rate, GPM 6.60 49.6 49.9 49.9 

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 Run 3 

Continuous Opacity Monitor (list hourly average) 

NA Monitor (list averaging basis): 

Monitor (list averaging basis): 

Abbreviations: APC-air pollution control 

Ibs.-pounds 

gpm.-gallons per minute 

psig-pressure per square inch gauge 

in. w.c.-inches of water column 

L'.P- pressure drop 

NOTE: This form provides ollly a summary of the operatillg conditiolls durillg the perform alice test. Additiollal alld 

more detailed records are required to meet the requiremellts of Millll. R. 7017.2035. This form is to be submitted as 

part of the performallce test report to: North, Metro, or Soutlt District, Performallce Test Coordinator, MN Pollutioll 

COlltrol Agellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194. 
SV045 Time dP GPM 

1143 0.80 6.6 

1202 0.80 6.6 

1217 0.8 6.6 

1233 0.82 6.6 

1245 0.81 6.6 

1301 0.82 6.6 

Average R1 0.81 6.60 

1432 7.6 50 

1445 7.5 49.5 

1501 7.5 49 

1515 7.5 49.5 

1532 7.5 50 

Average R2 7.5 49.6 

1615 7.5 50 

1631 7.5 50 

1646 7.6 49.5 

1649 7.5 50 

1716 7.5 50 

1727 7.5 50 

Average R3 7.5 49.9 

1745 7.6 50 

1800 7.6 50 

1816 7.5 50 

1830 7.6 50 

1845 7.5 50 

1900 7.6 49.5 

Average R4 7.6 49.9 
:ts-;6~ _-- . 

} I 

. , 

#20 ?/aW if5 v ~/ 4:. 5 Y II ~ 

;1i ~ 51'"' __ .6.. e fliT 

~~, (/ J,91 

:;?~/<..<! 

I j/: 7"S-

{;l,CJ'If'1 

/;(,o' Ie, 

I 3.94> r,,2 ',J.s 

/rJ! ti7 

.3,9/ p,'S'tJ 

j,c}1 ,.;2; 30 

I J.1':2 ;2:~7 

3.1,7 o<.:S'7 

3:/7 

3:.30 

3,98 f'/7 .-

:S,90 'f.~9 

Ii? '/;y.> 

SO/ 

Sf(t/ 

93.1 

CJId. I 

qt. ;;L 

I 

rezPf- V-<:'h-l.t) 17 0~ ~ .~ s-/s-fos 
;;,. . 

·f;. 

:, UNITED.TACONITE· .... FAIRLANE PELLET PLANT' 

;,KILN OPERATORS. SHIFT REPORT 

r _r(;;{_ () rSHIFT:' ·ct..2. '3 

()PERATOR' . 

CONCENTRATE' . 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE' 

GRATE FACTOR 

FIRED PELLET TONS" 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NU:'vlBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BI:-.1 MEASUREMENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ a) Spills and leaks 

.L1NEL .' 

·/~·l~~·. 

#5-#4 

RECLAIl'.IED 

LIMESTONE 

17), __ 2={J.!...>9:;;~ 

20B)v"Ji b 

H 

200) 30CZ 

TOT) ____ _ 

(17 - TOT) 

~7 

//;)$' 

GAS) 900 1'-:0=-

OIL) ___ _ 

COAL) ___ _ 

HEATING GAS 

2 

REGULAR 

#5 SCALE (, . 

.. 

{MCF} 

{GAL} 

{TON} 

3 

3 

I have examined my arell. 

#4 SCALE 

STOCKPILED 

BINDER 

17A) /.f~3 (+) 

18A) ~/q3 

TOT) L-/o5& 

(-) 

20D) 30'1 

37Lf7 

(TOT - 20D) -;7 f' 

3;;;60 

GAS) 

OIL) ____ _ 

COAL) __ 4-,-0::......_ 

TIME 

TIME 

TIME) c.;!.) 

HOPPERS 

__ --:-b) Cleor uccess to electrical disconnects 

___ c) EmergenC)' I.i¥hting 

__ -,-d) Guards on conveyo~ 

Date--,-__ ~ __ Shift ______ -'-__ 

___ e) Trip cables Name _______ -----------

Cleur walbl,:;j)'s . 

__ --"g) Floor gr;jding, ha.nd rails. ~nd toe bOJrds 
UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT " 

SHIFT: 2 ( 3) 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BIN MEASUREtvlENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ a) Spills and leaks 

LINE 1 

;4, J--

# 5 - #4 

'\ (C", 

RECLAIMED 

LIMESTONE 

20B) __ '_-'--___ 

H L ! .,_/ 20D) __ --' __ _ 

TOT) ___ -'--_ 

(17" TOT) 

87 

, ;) 

Cl '" , GAS) (1 y-! 

OIL) ____ _ 

COALl ___ _ 

HEATING GAS 

2 

2 

B/L) ____ _ 

REGULAR 

#5 SCALE 

{MCF! 

{GAL! 

(TON! 

3 

3 

ENG) ____ _ 

HI SIDES 

___ ,b) Cleur access to electric.1I disconnects 

___ c) Emergency lighting 

I have examined my area. 

'--' 

LINE 2 

1M -!.-' 

#4 SCALE 

STOCKPILED 

BINDER 

17A) 

(+) 

[8A) __ ' _C' __ "'_,'_ 

TOT) ____ _ 

H -, ) 20D) __ 1_, __ _ 

(TOT" 20D) 

/ 

GAS) J i~' '/ 

OILl _____ _ 

TI!-.IE 

TIME 

TIME) _____ _ 

HOPPERS 

___ d) Guurds on conveyor 

Date' ________ Shift __________ _ 

_____ e) Trip canies Name' ___________________________ ___ 

_____ 0 Clear wnlk\,,,'uys 

___ -l!'!) Floor grading, iwnd rails, and to.! boards 
;:." . 

:." 

,; .... 

.... ;.,' .:" 

.... ~. " .. 

:. .~ 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

DATE, ____ ~C)~I~J~~/.)------------

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NU"lBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BIN jv!EASUREMENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ 01 Spills and leaks 

# 5 - #4 

RECLAIMED 

LIMESTONE 

'd ~)(/ 

20B) ~S '1 

~6D) __ '.=.3_(-.L(_(1-( 

_.-J,-

17) 

TOT)--,-/_C:-,--r~')_ 

-) o((i r; " 

(17 - TOT) 

.-., -' ~/ GAS)-'-;'o--')!..,i!..../ _\L-'~f::A 

OIL) _____ _ 

COAL) ___ _ 

HEATING GAS 

2 

2 

B/L) ! ( / Ii C 

REGULAR 

SHIFT: 

#5 SCALE 

(MCFI 

(GALl 

(TONI 

3 

3 

HI SIDES 

___ b) Clear ilcces~ to electrkal disconnects 

___ c) Emergency lighting 

I have examined my area. 

3 

#4 SCALE 

STOCKPILED 

'7/~ :"/0~ BINDER 

17A) ? ;:;- 0 '::> 

(+) 

18A) ;;;. 7 7 (/ 

TOT) 

H 

20D) 3 C( " ( 

cj 7'3 c.) 

(TOT - 20D) 

/ / :-::J :x" (/' ~-;/ "'7'\.. ,-' 

(~) 

GAS) A) '-ill' 

OIL) 

COAL) 5-2-

TIME 

TIME 

TIME) ____ \-=~_', 1_'---_::'_-

HOPPERS 

___ ,d) Guards on conveyor Date _________ Shift ___________ _ 

___ ,e) Trip cables 

____ 'f) Clear \\,.alkwilYs 

Name _____________________________ _ 

___ ..og) Floor grading. hand rails. and toe boards 
DATE 

OPERATOR 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

\,), '7, /'.LL,' (;/ ", /1, (~) /-"" ! _ l-C U J UJ SHIFT: (",1----) 

LINE 1 

I / ;;::j I/~::-j 

2 

FILTER CAKE PRODUCTION 

# 5· #4 j? SCALE , 

6( il I 1/1, U 

CONCENTRATE 

RECLAIMED 

FILTER ADDITIVES 

W.IESTONE 

BENTONITE 

GREEN BALL SCALES -"") "..., 17)_-=..£-'0'-:'" -::.:' ,,-,,':>'--... 

-. --; 20B) _---.c'l-'-',"-\,'-'-{ _ 

(-) 

20D) __ ",--,c.:/''--

ROLL FEEDER REJECT TOT) ____ _ 

GREEN BALLS TO GRATE ! i/ (; 

(17 - TOT) 

GRATE FACTOR 

FIRED PELLET TONS 

r Lr' !/[ij TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

GAS) :/G :2 t-\( 1~ {MCF} 

OIL) {GAL} 

COAL) {TON} 

#22X CONVEYOR HEATING GAS 

PELLET BIN ~!EASUREtv!ENT !~~; .. J fe; :J r:,-- ~ •.. :J 

2 3 

2 

3 

LlNE~ 

).! 1_ .. 1 

j/{,L.,i 

STOCKPILED 

'-i~',' :'; ,':;' 

BINDER 

17A) _...:::::...:::...c,--_:..'l-_ 

(+) 

18A) __ "----'-"'--

TOT) 

(-) 

20D) _---"""-.2..-'.:..._ 

(TOT· 20D) 

GAS) !, ( I 

OIL) ____ _ 

COAL) _'::;.,' ,_::_~-_ 

TIME 

PELLET TRAINS B/L) )(; /s9 

3 

ENG) L/I (~) 

/ :::..:J 

1 I 0; ~~ 1\, TIME) ____ I , 

INSPECT AREA FOR: 

___ a) Spills and leaks 

___ b) Clear access to electricli disconnects 

___ c) Emergency lighting 

___ d) Guards on conveyor 

___ e) Trip cables 

____ 0 Cle:'Jr \valbvuys 

___ -"g) Floor gmding, hund rails, and toe bourds 

,: .•.. 

REGULAR HI SIDES HOPPERS 

I have examined my area. 

Date' ______ Shift _______ _ 

Name ______________ ___ 

I' ! i' 
: .... 

::.: .\. 

.:' ; 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

DATE <;-- 7 -{; (" SHIFf: 2 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUi\-lBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

#l1X CONVEYOR 

j'< 

<7' ) 

PELLET BIN MEASUREMENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ -0) Spills and leaks 

LINE 1 lk-::::;t<-.-

# 5 ~ #4 

LIMESTONE 

20B) ---"'--'---'-__ 

(-) 

20D) ~-'-~ __ 

~-'j 

/ TOT)_-,-",--,,-,-'_ 

([7 - TOT) 

77 

GAS) 

OIL) 

COAL) 

./ ,-I 

/ (, ! 7 

HEATING GAS 

)? 

7 

/0 l 

2 

B/L) ____ _ 

REGULAR 

---7 I ! ' 

//// 

(MCFI 

(GALl 

(TONI 

( -L 

3 

-, 'J .-:.-\.-

3 

ENG) 

HI SIDES 

____ b,) Clear uccess to electrical disconnects 

___ 'c) Emergency lighting 

I have examined my area, 

3 

LINE 2 --( 

/. I, ...... _-

'--;' 

#4 SCALE 

STOCKPILED 

BINDER 

I 7 A) -'-'---'--'--=-_ 

(+) 

lSA) _=----'-'-_ 

TOT) -"'--~_-'--_ 

~dD) ---,-=--L_/",~_--'_ 

! , 

l~- .' 

(TOT -10D) 

iP7 

GAS) i f l t:. 1// Co<- 0 

OIL) 

COAL) 

,) 

i(: c.~ 

--> 

TIME c-I, Gr) 

TIME 

TIME) 

HOPPERS 

___ d) Guards on conveyor Dnte ______ Shift ________ _ 

___ e) Trip cables 

____ 0 Clear walkways 

Name _______________ _ 

___ ..gg) Floor grading. hand mils. and toe boards 
.:~ . 

.J;. 

"." 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

.z:;-I L{ DATE ___ ~v~/~-------

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: (> 

PROCESS FUEL: 

# 5 ~ #4 

RECLAIMED 

/-' -) <_) -; c~ 

'-' -:\ / I 

LIMESTONE 

17) ) <.. JC) 0 

/ / 

20B) _-,--,,:,(-'.-' __ 

H "< 1/' '? 20D) __ ./---,--"...-"::-"_ 

TOT) ---'1----'"1'-.J'-~ '_' _ 

f }_ 

(17 - TOT) 

87 

+r /0 37 

GAS) I), 2.. (. 

OIL) 

COAL) 

SHIFT: 

#5 SCALE 

c 

{MCF} 

{GAL} 

{TON} 

#22X CONVEYOR HEATING GAS 

PELLET BIN MEASUREi\IENT 

PELLET TRAINS Cf) BIL) j /; /5:..q 

REGULAR 

INSPECT AREA FOR: 

____ a) Spills and leaks 

2 

Il 

3 

2 3 

ENG) 1./13 

/39 

HI SIDES 

f rlll 

Cv 

___ b) Clear access to electrical disconnects 

____ c) Emergency lighting 

I have examined my area. 

3 

LINE 2 /j--

/lli/ilL..--' 

) ; 

#4 SCALE 

STOCKPILED 

BINDER 

17A) )--6/0 

(+) -J \ .. 7 ~ 18A) / f '-,I 

TOT) 5'-(. P '7 

~6D) '7 it' s 

Lj 7 '-Ie.. 

(TOT-20D) 

t37 

GAS) 

OIL) 

COAL) j- et 

TIME 

I '-i ,) C! 

TIME; tJ 3 STIt-.-lE) I I f..j 5' 

HOPPERS 

___ d) GUilrds on conveyor Date' ______ Shift _______ _ 

___ e) Trip cables Name _______________ ___ 

____ 0 Clear walkwuys 

___ -£!!) Floor grading, hand rails, and roe boards 
;.-' UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

D~E ___ (; __ ~~~-~-_~~~~ __ SHIFT: 

OPERATOR , .. ;

FILTER CAKE PRODUCTION 

# 5 ~ #.+ 

( 

CONCENTRATE i 

RECLAINIED 

FILTER ADDITIVES 

LIMESTONE 

BENTONITE 

GREEN BALL SCALES 17), _____ _ 

20B) ____ _ 

H 

20D) ____ _ 

ROLL FEEDER REJECT TOT)_...:.I-,C_, _) __ 

GREEN BALLS TO GRATE 

(17 - TOT) 

GRATE FACTOR ) 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTIKGS REPLACED 

DELAYS: 

PROCESS FUEL: ). GASJ_-'-__ _ {MCF} 

OIL) ____ _ {GAL} 

COAL) ___ _ {TON} 

#22X CONVEYOR HEATING GAS 

PELLET BIN MEASUREivlENT 

2 3 

2 3 

PELLET TRAINS B/L) -,-/ __ '_\_7 ENG) 'i' ../ 

; . 

REGULAR HI SIDES 

INSPECT AREA FOR: 

___ oj Spills "nd leoks 

2 

___ b) CIeJr access to electricul disconnects 

____ 'c) Emergency lighling 

I have examined my area. 

3 

#.+ SCALE 

STOCKPILED 

BINDER 

,--", 

17A) __ /:....... __ _ 

(+) 

18A) ___ ...:-_ 

TOT) ---''--_-'--_ 

(-) 

20D) __ ---' __ 

(TOT- 200) 

-1 

/ 

( 

GAS) ____ _ 

OILl ____ _ 

COAL) ___ _ 

TIME 

TIME 

TINIE) ....:..:..-'--__ 

HOPPERS 

___ d) Glmrds on conveyor Date ______ Shift ________ _ 

___ c) Trip cables Name _______________ _ 

____ 0 Clear \vnlkv .. 'nys 

___ -Ecl Floor grueling, hand r.lils, and IOc boards 

, ..... --
..... ,:!. 

:.,'; .. 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

1- DATE, ____ J_~~~ __________ __ 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NU:VIBER OF CASTINGS REPLACED 

DELAYS: l..': 

PROCESS FUEL: 

# 5 - #4 

RECLAIMED 

LI?-.IESTONE 

17) ') i _0 

20B) ________ __ 

H 

20D) / 

TOT) ) 

(17 - TOT) 

7 

GAS) : ~-

-, 

I 

OIL1 ___ _ 

COAL) ___ _ 

SHIFT: 

#5 SCALE 

!lvlCF) 

{GAL) 

{TON) 

#22X CONVEYOR HEATING GAS 

PELLET BIN MEASUREMENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ a) Spills and leuks 

______ b) Clear access to electrical disconnects 

___ c) Emergency lighting 

) -~ -- ~ 

B/L) / /. / t),:::, 

REGULAR 

2 

2 3 

ENG) loS 

.fLl{) 

HI SIDES 

I have examined my area. 

3 

) ! 

#4 SCALE 

STOCKPILED 

_l 

BINDER 

17 A) --'-' __ --'-_ 

(+) 

[8A) __ -"-__ _ 

C-i ---, TOT) _____ _ 

(-) 

20D) ____ ---' __ _ 

'-I /-/ 

(TOT- 20D) 

-+~~ --'-----'---

GAS) _____ _ 

OIL) ___ _ 

COA L) _---"'''----_ 

TIt-.lE C' )'."> 1 

TIME) t; '-I :~ 'SHOPPERS 

___ d) Guurds on conveyor Date _______ Shift __________ _ 

___ e) Trip cables 

_____ 0 Clear \l,.'Jlbvays 

Name _______________________ _ 

___ g) Floor grading, hand ruils, and toe boards 
OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

# 5 w #4 

RECLAIMED 

( i....// / 

LIMESTONE 

20B) _-=-';;;"'::"--_ 

(-) 

200) _~-'-'-L.-_ 

TOT)_--=2:..:/_C_' _ 

,?( :;,l/ 

(17 - TO'h 

SHIFT: 

--/ I / I 

(j) 

#5 SCALE 

( 

NU"IBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

{MCFI 

OIL) ___ _ (GALl 

COAL) ___ _ {TON} 

#22X CONVEYOR HEATING GAS 

PELLET BIN MEASUREMENT 

3 

2 3 

2 

PELLET TRAINS B/L) ____ _ ENG) ____ _ 

REGULAR HI SIDES 

INSPECT AREA FOR: 

___ ,oj Spills ond leaks 

___ ,b) Clear access to electrical disconnects I haye examined my area. 

3 

STOCKPILED 

i:l7L /,) 

BINDER 

I7A) 

(+) 

18A) __ -,--'--'./_ 

TOT) _--,-,,-"--"--_ 

(-) 

200) _~'--'-''-'-_ 

GAS)_---"·,-'-, _'-Lf_ 

OIL) ____ _ 

COAL) ~"1 

TIME 

TIME 

TIME) ____ _ 

HOPPERS 

___ 'c) Emergency lighting 

__ ----'d) Guards on conveyor 

___ 0) Trip cables 

____ 0 Cle>.lf walbvaY5 

Date ______ Shift _______ _ 

Name ______________ ___ 

____ g) Floor £nlding. hand mils. und tOl! bourds 
:-:.' 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT RE~ORT 

DATE_~S-_-_·_)_-__ C__ .~ ____ __ 

OPERATOR 

FILTER CAKE PRODUCTION 

# 5 #4 

,-) J'~ 

CONCENTRATE 15-'17 RECLAI~IED 

FILTER ADDITIVES t7f-J)'9 

LIMESTONE 

BENTONITE 

GREEN BALL SCALES (7) ~):})7 

20B) 

H :2,[ i l. 

20D) _/ -r 

ROLL FEEDER REJECT TOT) ~ol 

GREEN BALLS TO GRATE 

(17 - TOT) 

GRATE FACTOR 1'7 

FIRED PELLET TONS r27/ 

TONS TO PAN CONVEYOR o 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

GAS) / (') 0 7 

OIL) ____ _ 

COAL) ___ _ 

#22X CONVEYOR HEATING GAS 

PELLET BIN MEASUREMENT 

2 

2 

PELLET TRAINS B/L) -'--':z.--'-__ 

REGULAR 

INSPECT AREA FOR: 

_____ 'n) Spills nnd lenks 

SHIFT: 

#5 SCALE 

to 

(MCF} 

(GAL} 

(TON} 

3 

3 

ENG)---'.<-!_!_( __ 

-1 (.;, 

HI SIDES 

____ b,) Clear access to electrical disconnects 

_____ 'c) Emergency lighting 

I haye examined my area. 

#4 SCALE 

! 

STOCKPILED 

BINDER 

') u t·/7 I7A) C' i ' 

(+) . -,--;J -70 

I8A) .:I __ '_} ____ _ 

TOT) 4- S )7 

H2LJ) 

20D)·f(~., 

(TOT· 20D) 

\--' '7 

o 

(' 

6 

GAS) I '~7 ()tl' 

OIL) 

(.-~: / 

COAL) ../ t:? 

TIl<.IE 

C)L i. 

---/ Tli\-IE) __ -L. __ 

HOPPERS 

____ d) Guards on conveyor Date ______ Shift ________ _ 

___ e) Trip cables Name _______________ _ 

____ 0 Clear wulkways 

___ ..gc) Floor grading, hand rails, und toe hoards 
."., . 

·ii . . ' ::' . 

. ;~-;: : : . 

' ..... . 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

:.:; 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

LINE 1 

1/1---' 

[.' ' 

# 5 ~ #4 

RECLAIMED 

71)/).. 

LIMESTONE 

17), ____ /)/7 _ 

20B) _'--" __ _ 

H 

20D) --"'---'--'-__ 

TOT) __ J_,_' -,-'l __ 

(17, TOT) 

, ~i 

SHIFT: 

#5 SCALE 

NUMBER OF CASTINGS REPLACED 

DELAYS: D 

PROCESS FUEL: 

li22X CONVEYOR 

PELLET BIN MEASUREMENT 

PELLET TRAINS 

INSPECT AREA FOR: 

____ 'il) Spills und leuks 

GAS) / c '-i" , ) 

OIL) ____ _ 

COAL) ___ _ 

HEATING GAS 

2 

2 

B/L) /b(0-( 

REGULAR 

D 

(MCF) 

(GAL) 

(TON) 

3 

3 

ENG) if ()/ 

HI SIDES 

:2 

___ b) Cle.lr access to electrical disconnects 

___ 'c) Emergency lighting 

I have examined my area. 

3 

t..,; '\.; c .. , ..-L 

#4 SCALE 

STOCKPILED 

BINDER 

17 A) -,-_'--,)--=."_ 

(+) 

18A) "'-::'~'-:""-L-_ 

TOT) ----'--'--__ _ 

H 

:20D) _'--'-'-__ 

(TOT, lOD) 

~7 

',1. 1I_"'---'_--L_ 

GAS)_--,-I __ _ 

OILl ____ _ 

- --} 

COAL) I 

TI~IE 

TIME 

TIME)%;2 j'- ':-';:3 \ .-,. 

HOPPERS 

.I 

____ d) Guards on conveyor Date, ______ Shift _______ _ 

___ e) Trip cubles 

____ f) Cle:lr walkwuys 

Name _______________ _ 

___ ~!!) Floor gntding, hund ruBs. ;lIld to\! board::; 
,;, ,"'" 

DATE 

OPERATOR 

;.' UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

) /) '\ ('5 /J / !1d..L+ c;1 I 'Q SHIFT: U...? 2 

U / 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: () 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BIN MEASUREtvlENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ ,al Spills and leaks 

# 5 - #4 

RECLAIMED 

(~)<"1n 'i 

LHvlESTONE 

17) d / C( ? 

20B) __ <;_-~,,-,)---,q_ 

H 3037 20D) ____ _ 

TOT)_LI_'e.-f_

C_) _ 

(l7 - TOT) 

I (2 ") 

o 

GAS) 2 D (C,/ 

OIL) 

COAL) 

HEATING GAS 

--- 2 

::: 

B/L) 

REGULAR 

#5 SCALE 

() 

(MCF) 

(GAL) 

(TON) 

r-. 

3 

3 

ENG) 

HI SIDES 

___ ,b} Cleur access to electrical disconnects 

___ ,e) Emergency lighting 

I have examined my area. 

3 

LINE 2 

lift 

"))-' \ 7 

#4 SCALE 

STOCKPILED 

c(!'? -) 

BINDER 

17A) J (( C L 

(+) '~. -5> 6 U 

18A) ____ _ 

TOT) '-I70L 

(-) -'2." 

20D) --'--' 

ij :/,C-, :':, 

(TOT - lOD) 

,,27 

377<,-

I/O 

GAS) !{t) ? 

OIL) ____ _ 

COAL) ') C. 

(0:,) () 

TIME 

TIME 

TIME) ___ _ 

HOPPERS 

___ d) Guards on conveyor Date ______ Shift _______ _ 

___ e) Trip cubles 

____ i) Clear walkv,:uys 

Name ________________ ___ 

___ ~g) Floor gmding, hand fnils, and toe boards 
.. 

. '. 

.. ..... 

.' ~ ' .. 

; .. ,:.' 

.. .. .. 

.. .. 

: 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

DATE.~(~~·_-~/~-__ C_··_) ____ _ SHIFT: 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NU~!BER OF CASTINGS REPLACED 

DELAYS: .. 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BIN MEASUREMENT 

PELLET TRAINS 

INSPECT AREA FOR: 

___ in) Spills and leaks 

LINE 1 

;) ,- !.\.. 

# 5 ~ #4 

RECLAIMED 

LIMESTONE 

20B) _-",Se:...-::::.:'_:'-.c..tf~ 

~6D) ~~,,-.~_, U_/-'>s.:....-'_· _ 

TOT)---,-,;;2~O..::::{;_: _ 

(17 - TOT) 

GAS) /05(.., 

OIL) ____ _ 

COAL) ___ _ 

#~;SCALE 

.b 

{t-.ICFI 

{GALl 

(TONI 

HEATING GAS 

2 3 

2 3 

B/L) / ( ! 5" 3 ENG) ell ( 

/ '/"C) 

REGULAR HI SIDES 

2~_' 

v 

LINE 2 

I-ID i' ,1--- I 

#4 SCALE 

STOCKPILED 

BINDER 

--) -) ',\ \.;. 

17A) ,.~ ::..' /)/> 

iiA) J-~:3t(O 

TOT) 

H --:.'£... J(~' 

20D) ___ ''_f_(5_,_ 

(TOT-20D) 

,". -7 

.:> / 

GAS)_-,-i'_-'-..)_<_) __ 

OIL) __ (~_A) __ 

COAL) 

oj; I r; 

TIME 

TIME C i/) 

TIME)? ) 0 

HOPPERS 

____ I b) Clear access to electrical disconnects I have examined my area. 

..I -'\~. 

()f...(;-

___ 'c) Emergency lighting 

____ d) GU<1rds on conveyor 

___ 0) Trip cables 

____ 0 Clear walbvuys 

Date ______ Shift _______ _ 

Name. ________________________ _ 

___ -&!!) Floor grading. hand rails, and toe boards 
':r;,.. 

UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

(. j /1 r·- DATE, ____ -'_' -L! .!-+!....:..:./;_'_. __ SHIFT: 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TOi\S TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BIN MEASUREMENT 

L-· 

# 5 ~ #4 

RECLAII\IED 

LIMESTONE 

17) 

20B) 

(-) 

200) 

TOT) 

.. 

(17 - TOT) 

I 

! 

/ r- ( 

GAS),--,!_' -'----...:..-. -,')_ 

OIL) ____ _ 

COALl ___ _ 

HEATING GAS 

2 

2 

; I 

#5 SCALE 

{MCF) 

{GAL) 

{TON) 

3 

3 

2 

PELLET TRAINS BfL) ____ _ ENG) ____ _ 

REGULAR HI SIDES 

INSPECT AREA FOR: 

___ uJ Spills und leuks 

I ha\'e examined my area, 

3 

STOCKPILED 

BINDER 

L_ I7A) ____ _ 

(+) 

18A) ___ ---'-_ 

TOT) _-'---_-----"_ 

H ~,_ 20D) __ ~ __ 

(TOTc 200) 

GAS) ____ _ 

OIL) ____ _ 

COAL) ---'-__ _ 

TIME 

TIME 

TIME) ____ _ 

HOPPERS 

___ b) Clear acceSs to electrical disconnects 

___ c) Emergency lighting 

___ d) GUHrds on conveyor 

Date ______ Shift ________ _ 

____ 'e) Trip cubles Name _____________________ _ 

____ 0 Clear \I,!ulkv.ays 

___ -"!!) Floor gwding. hand )"uils, and t('le boards 
UNITED TACONITE 

FAIRLANE PELLET PLANT 

KILN OPERATORS SHIFT REPORT 

DATE oltur! J ' 0-.5 SHIFT: 0 2 3 U ~ 

OPERATOR 

FILTER CAKE PRODUCTION 

CONCENTRATE 

FILTER ADDITIVES 

BENTONITE 

GREEN BALL SCALES 

ROLL FEEDER REJECT 

GREEN BALLS TO GRATE 

GRATE FACTOR 

FIRED PELLET TONS 

TONS TO PAN CONVEYOR 

GRATE OPERATING HOURS 

NUMBER OF CASTINGS REPLACED 

DELAYS: 

PROCESS FUEL: 

#22X CONVEYOR 

PELLET BIN MEASUREMENT 

PELLET TRAINS t!lJ~j-~j-fj; 

) 

INSPECT AREA FOR: 

___ 0) Spills and leaks 

.I -::::;.) IA/..-/ 

# 5 ~ #4 

RECLAIMED 

" 1 or> I 

LIMESTONE 

17) 

20B) 

(-) "d 

200) _",,::,:,,_'_0:.. 11 _ 

TOT) 

(17 - TOT) 

cCC! 

() 

GAS) 

OIL) ____ _ 

COAL) ___ _ 

HEATING GAS 

AI-f 

2 

2 

BIL) Ifo 10~ 

REGULAR 

#5 SCALE 

{MCF} 

{GAL} 

{TON} 

3 

3 

ENG)_L-LI.:-! L-L/ __ 

HI SIDES 

#4 SCALE 

STOCKPILED 

17A) 2 e;-L( r:;! 

i~~-\) 9 3 I V-> 

TOT) 

H 

200) 

Lf15 C:' ( ( 

~'S-~ 

L/ s-"c C,," 

(TOT - 200) 

GAS)_---->'6"-..: -,-'~_\ _7:..... 

OIL) ____ _ 

TIME 

~::Je- ,-,. TIME) "J/q;;. --{~- )'::-

HOPPERS 

___ b) Clear uccess to electrical disconnects I have examined my area. 

___ 'c) Emergency lighting 

___ d) Guards on conveyor 

___ eJ Trip cubles 

____ f) Clear \valbvays 

___ -l'e:) Floor grilding. hand rails. nnd toe bourds 

Dat", ______ Shift _______ _ 

Name: __________ ~ ____ ---
Appendix I 

Stack Test Plan 
Tom Kuchinski 

From: 

Sent: 

Anderson, Bradley E. [BEAnderson@cci-united.com] 

Wednesday, June 22,200510:49 AM 

To: 'Olson, Beckie' 

Cc: Place, Andrew; Paul Taylor 

Subject: RE: Stack test results - delayed report to the MPCA 

Attachments: aq-f2-chOO-050622.pdf; aq-f2-ch01-050622.pdf 

aq-f2-chOO-050622 aq-f2-chOl-050622 

.pdf (37 KS) .pdf (35 KS) 

Beckie, 

Here are forms CH-OO and CH-01, which you requested. 

Brad. 

-----Original Message-----

From: Olson, Beckie [mailto:Beckie.Olson@state.mn.us] 

Sent: Wednesday, June 22, 2005 6:48 AM 

To: Anderson, Bradley E. 

Cc: Place, Andrew 

Subject: RE: Stack test results - delayed report to the MPCA 

Thanks! you will also need to include the CH-OO and the CH-Ol Beckie Olson 

651/297-8305 

-----Original Message-----

From: Anderson, Bradley E. [mailto:BEAnderson@cci-united.com] 

Sent: Tuesday, June 21, 2005 1:40 PM 

To: Olson, Beckie 

Cc: Beresford, Robert; Paul Taylor Ph. D. (E-mail); Pruchnofski George (E-mail); Roth, 

Todd D.; Mlinar, Michael P.; Tom Kuchinski (E-mail); 'place, Andrew' 

Subject: RE: Stack test results - delayed report to the MPCA 

Beckie, 

As I disucssed over the telephone and in the preceding emails with Andy 

Place attached are five PDF files that should suffice as the 

administrative amendment needed to address the delay in reoprting our 

latest stack tests. I will also send this with an original signature via 

US mail. Thanks for your help. Sincerely, Bradley E. Anderson Section 

Manager - Environmental 

-----Original Message-----

From: Place, Andrew [mailto:Andrew.Place@state.mn.us] 

Sent: Tuesday, June 21, 2005 8:52 AM 

To: Anderson, Bradley E. 

Cc: Beresford, Robert 

Subject: RE: Stack test results - delayed report to the MPCA 

Brad, 

I appreciate the heads-up on the situation. Since no discussion took 

place prior to now about extending the test report deadline, your permit 

requires you complete an administrative amendment to propose an 

extension request. 

In the future, if we discussed this matter during the pretest meeting or 

at least prior to the completion of testing, we could probably address 

1 
the issue at that time. 

If you have any additional questions or concerns, please let me know. 

Thanks. 

Andy Place 

Performance Test Coordinator 

Minnesota Pollution Control Agency 

520 Lafayette Road 

St. Paul, MN 55155-4194 

(651) 296-7169 

-----Original Message-----

From: Anderson, Bradley E. [mailto:BEAnderson@cci-united.com] 

Sent: Monday, June 20, 2005 2:55 PM 

To: Place, Andrew 

Cc: Tom Kuchinski (E-mail) i Beresford, Robert 

Subject: Stack test results - delayed report to the MPCA 

Andy, 

The report for the latest stack testing conducted at United Taconite is 

due to the MPCA 45 days after the last test of the plan, which is June 

20, 2005. Among the tests are metals analyses, which generally take 

extra time due to laboratory turn around. We neglected to take the 

extra lab time into account in the test plan, therefore we will not be 

able to submit the test report within 45 days of the last test. 

Additionally, preliminary results of the tests indicate that all of the 

stack tests were in compliance for emissions limits. We propose that we 

submit the test results by July 15, 2005. 

Thank you for your consideration. 

Sincerely, 

Bradley E. Anderson 

Section Manager - Environmental 

######################################################################## 

####### 

This electronic message and any attachments included with this message 

are for the exclusive use of the individual or entity to which it is 

intended to be addressed. This message may contain information that is 

privileged or confidential and thereby exempt and protected from 

unauthorized disclosure under applicable law. If the reader of this 

message is not the intended recipient, or an employee or agent 

responsible for delivering the message to the intended recipient, be 

aware that any disclosure, dissemination, distribution or copying of 

this communication, or the use of its contents, is not authorized and is 

strictly prohibited. If you have received this communication and are not 

the intended recipient, please notify the sender immediately and 

permanently delete the original message from your e-mail system. 

######################################################################## 

####### 

############################################################################### 

This electronic message and any attachments included with this message are 

for the exclusive use of the individual or entity to which it is intended 

to be addressed. This message may contain information that is privileged or 

confidential and thereby exempt and protected from unauthorized disclosure 

under applicable law. If the reader of this message is not the intended 

recipient, or an employee or agent responsible for delivering the message to 

the intended recipient, be aware that any disclosure, dissemination, 

distribution or copying of this communication, or the use of its contents, 

is not authorized and is strictly prohibited. If you have received this 

communication and are not the intended recipient, please notify the sender 

immediately and permanently delete the original message from your e-mail 

2 
Message 

Tom Kuchinski 

From: 

Sent: 

To: 

Place, Andrew [Andrew.Place@state.mn.us] 

Friday, April 22, 200510:27 AM 

Anderson, Bradley E. 

Cc: Beresford, Robert; Tom Kuchinski 

Subject: Test Plan Approval 

Page 1 of 1 

Attachments: MICROFICHE CD SUBMITTALS.doc; OPERATING DATA SUMMARY FOR COMBUSTION 

SOURCES.doc; OPERATING DATA SUMMARY FOR PROCESS SOURCES.doc; United Tac 

Approval, 5-05.doc; CERTIFICATION PAGE.doc 

Brad 

The test plan approval forms associated with the upcoming performance test on SV046, SV047, SV045, and 

SV116 are attached to this message. They include the Test Plan Approval, Process Source Operating Data 

Summary, Combustion Source Operating Data Summary, Certification, and Microfiche/CD Submittal. Please use 

the forms attached as they have recently been updated. Also, please print a copy of this email message and 

include it in the report with the approval letter. The email provides authentication for the test plan approval. 

If you have problems with any of the attachments feel free to contact me. Additional forms are provided at 

www.pca.state.mn.us/air/performancetest.html 

Sincerely, 

Andy Place 

Performance Test Coordinator 

Minnesota Pollution Control Agency 

520 Lafayette Road 

St. Paul, MN 55155-4194 

(651) 296-7169 

6/3012005 
Minnesota 

~ Pollution 

Control 

Agency 

Performance Test Plan Approval 

Minnesota Pollution Control Agency 

520 Lafayette Rd. N. Saint Paul, MN 55155-4194(651) 296-6300 

www.pca.state.mn.us 

Facility Name: United Taconite LLC 

Fairlane Plant 

Facility Contact: Brad Anderson, Environmental Section Manager 

Address: 8470 Townline Road (Hwy 16) 

Forbes, MN 55734 

Fax: (218) 774-7647 

Emission Unites): SV046, SV047, SVl16, and SV045 

Scheduled For: May 2,2005, at your Facility located in Forbes, Minnesota. 

AQ#869A 

Your test plan submitted on April 13, 2005, and discussed on April 22, 2005, has been approved 

by the Minnesota Pollution Control Agency (MPCA) as follows: 

D Shortened test notification approved 

[g] Test plan approved without modification 

D Test plan approved with the following provisions: 

SV045 and SVl16 emissions combine to serve EU039. SV045 serves the new portion of 

equipment for EU039. SV045 is subject to NSPS and will be tested according to 40 CFR § 

60 subp. LL, while SVl16, along with SV046 and SV047, will be tested according to Minn. 

Rule. 

ASTM Method Ontario-Hydro will be used for Mercury, Antimony, Arsenic, Barium, 

Beryllium, Cadmium, Chromium, Cobalt, Copper, Lead, Maganese, Nickel, Phosphorus, 

Selenium, Silver, Thallium, and Zinc emissions. 

Equipment should be operated at maximum capacity during testing. Include process 

equipment and control equipment operating rates on the Operating Data Summary forms. 

Include in the final test report(s) the full reference method data record (strip chart and/or 

datalogger output) used to calculate emissions. The data record should include calibration 

values for any instrumental analyzers used for emissions compliance testing. 

Attached Forms: 

[g] Operating Data Summary- Combustion 

Sources 

[g] Operating Data Summary- Process Sources 

[g] Certifications Form 

D Operating Data Summary- Waste 

Combustors 

D Operating Data Summary- Asphalt Plants 

[g] Microfiche/CD-ROM Submittal Form 

Note: Forms are also available at: www.pca.state.mn.us/air/performancetest.html 

Approved by: Date: April 22, 2005 
Andrew Place 

Performance Test Coordinator 

Compliance and Enforcement Section 

Industrial Division 

Please contact me at (651) 296-7169 if you have any questions regarding this approval. 

Please be aware that enforcement action will be taken for pelformance test failures indicating emissions above applicable limits 

(excess actual emissions to the environment). Failures commonly result in assessment of a monetalY penalty. Upon the first test 

failure, the Company should take immediate measures to minimize emissions. The measures taken should be documented, as 

they will become part of the record of corrective actions. 

Hard Copy Pelformance Test Reports and Microfiche or CD Copy submittals will be addressed to: Compliance Tracking 

Coordinator, Compliance alld Enforcement Unit, Industrial Division, Minnesota Pollution Control Agency, 520 Lafayette Road 

North, St. Paul, Minnesota 55155-4194 

cc: Bob Beresford, MPCA, Duluth 

Tom Kuchinski, Barr Engineering Co., Edina 
TEST PLAN FOR A TACONITE PROCESSING FACILITY 

UNITED TACONITE LLC 

EVELETH, MINNESOTA 

Date test plan created/revised: April 11, 2005 

Scheduled test date(s): May 2-10,2005 

P ART I. GENERAL INFORl"VIATION 

Name and address of emission facility: 

Facility contact person and telephone number: 

MPCA AQD File Number: 

MPCA AQD Air Emission ID Number: 

Reason the Emission Units are to be Tested: 

United Taconite LLC 

Fairlane Plant 

8470 Townline Road (Hwy 16) 

Forbes, Minnesota 

Brad Anderson 

(218) 744-7849 

(218) 744-7647 (fax) 

email: beanderson@cci-united.com 

101EV 

13700113-004 

Emissions testing will be performed at the Fairlane processing facility on the Line 1 pellet process as part of the 

post modification testing following the Emissions and Energy Reduction Project (EERP). This portion of the 

project will include testing the waste gas stack serving the Line 1 Pellet Induration (SV046) for criteria pollutants 

to quantify expected emission reductions from the EERP. Determinations will be made for particulate matter, 

NOx, SOl, CO, VOC, fluorides, mercury and metals 1. This stack must be in compliance with the Standards 

of Performance for Fossil-Fuel-Buming Direct Heating Equipment, Minn. R. 7011.0610 for particulate 

matter and sulfur dioxide. The Line 1 Pellet Cooler Exhaust (SV047) will be tested for particulate matter for 

demonstration of compliance with the industrial process equipment rule, Minn. R. 7011.0715, subpart 1 (A) and 

PMlO for use in emissions inventory and permitting. In December of2004 a new vibrating feeder was installed on 

Metals list includes: Antimony, Arsenic, Barium. Beryllium, Cadmium, Chromium, Cobalt, Copper, Lead, 

Manganese, Nickel, Phosphorus, Selenium, Silver, Thallium and Zinc. Metals will be determined by analysis of 

front half catch (dry) and reagent from irnpingers 1-3 from the mercury sample train. 

1 
Line 1 pellet discharge, this change requires the source to be tested under NSPS rules v.rithin 180 days of 

completion. Particulate emissions of the vibrating feeder, emissions unit 039, are controlled by CE055/SV045. 

Particulate emissions from the dump zone, also emissions unit 039, are controlled with CE065/SV116 (new 

scrubber). Emission of SV045 and SV116 will be combined to demonstrate compliance with the industrial 

process equipment rule, Minn. R. 7011.0710, subpart 1 (A) of EU039. Opacity determined by EPA Method 9 

will be performed once for each of the aforementioned sources during emissions testing. 

Diagrams of each sampling location giving all relevant dimensions are attached. 

Testing Company and Contact: Barr Engineering Company 

Tom Kuchinski 

(952) 832-2727 

(952) 832-2996 (fax) 

email: tkuchinski@barr.com 

2 
PART II. TESTING REQUIREMENTS 

The table below gives a summary of the pollutants to be tested and test methods. 

StackIV ent #: Limitation Basis Pollutant Tested and Specific 

Source Description of Pollutant Applicable Emission Limit MethodslProcedures 

Tested Required Citation 

SV046 Minn. R Criteria Pollutants: 40 CFR Part 60, 

7011.0710, subp. PM, NOx, S02, CO, Appendix A 

Line 1 Pellet 1 (A) 

Induration-Waste VOC, F, Metals (EPA EPA Methods 1-5, 6C, 7E, 

Gas Exhaust Stack S02- Minn. R. Method-29 list) & Hg 9, 10, 13B,25A, 202 

7011.0610, subp. 

2(B) PM Limit - 42.6 Ih/hr ASTM Method D6784-02 

(Ontario-Hydro) with 

PM emissions shall comply reagent solution from 

impingers 1-3 analyzed for 

with the less stringent limit EPA Method 29 metals 

of Minn. R. 7011.0730 or 

7011.0735, and regardless 

of the limit allowed by 

7011.0730, PM emissions 

shall not exceed 0.3 

grains/dry standard cubic 

foot (gr/dscf). Opacity not 

to exceed 20 percent except 

for one six-minute period 

per hour of not more than 

60 percent as specified in 

Minn. R. 7011.0710, 

subpart l(B). 

3 
Stack/V ent #: Limitation Basis Pollutant Tested and Specific 

Source Description of Pollutant Applicable Emission Limit MethodslProcedures 

Tested Required Citation 

SV047 Minn. R PM andPMJO 40 CFR Part 60, 

7011.0710, subp. Appendix A 

Line 1 Pellet Cooler 1CA) PM emissions shall comply 

with the less stringent limit EPA Methods 1-5,202 

Minn. R. of Minn. R. 7011.0730 or EPA Method 20 lA, 202 

7011.0710 subp. 7011.0735, and regardless EPA Method 9 

l(B) of the limit allowed by 

7011.0730, PM emissions 

shall not exceed 0.3 

Minn. R. grains/dry standard cubic 

7017.2020, subp. foot (gr/dscf). Opacity not 

1 to exceed 20 percent except 

for one six-minute period 

per hour of not more than 

60 percent as specified in 

Minn. R. 7011.0710, 

subpart I(B). 

PM limit = -41Ib/hr 

PM 

SV116 Minn. R PM emissions shall comply 40 CFR Part 60, 

7011.0715, subp. with the less stringent limit Appendix A 

Line 1 Kiln Cooler 1 (A) of Minn. R. 7011.0730 or 

Discharge Scrubber 7011.0735, and regardless EPA Methods 1-5,202 

of the limit allowed by 

(New) 7011.0730, PM emissions EPA Method 9 

shall not exceed 0.3 

grains/dry standard cubic 

foot (gr/dscf). 

Opacity not to exceed 20 

percent as specified in 

Minn. R. 7011.0715, 

subpart 1 (B) 

Vendor Guarantee is 0.008 

gr/dscf 

PM Limit = -41Ib/hr 

combined with SV045 

4 
StackIV ent #: Limitation Basis Pollutant Tested and Specific 

Source Description of Pollutant Applicable Emission Limit MethodslProcedures 

Tested Required Citation 

SV045 Minn. R PM 40 CFR Part 60, 

7011.0715, subp. PM emissions shall comply Appendix A 

Line 1 Kiln cooler l(A) with the less stringent limit 

Discharge Scrubber of Minn. R. 7011.0730 or 

EPA Methods 1-5,202 

(Existing) 7011.0735, and PM EPA Method 9 emissions shall not exceed 

0.022 grains/dry standard (3 I-hour runs) 

cubic foot (gr/dscf) per 40 

CFR Part 60, Subpart LL 

for NSPS. 

Opacity not to exceed 20 

percent except for one sixminute period per hour of 

not more than 60 percent as 

specified in Minn. R. 

7011.0710, subpart l(B) 

Similar to the pre-EERP testing, the Pellet Cooler exhaust stack (SV047) will be tested while the Cooler Discharge 

dump zone emissions are being controlled with CE065 - SVl16 only. Pending successful testing on SV047, CE055 

- SV045 will be permanently disconnected from the Cooler Dump zone (part ofEU039). Since CE065 and CE055 

serve the same emission unit (EU039), the emissions measured at SV045 and SV116 will be added together to 

demonstrate compliance with the Industrial Process Equipment Rule. In addition, the emissions from CE055 -

SV045 must comply with 40 CFR Part 60, Subpart LL NSPS as it applies to the new source. 

P ART III. OPERATING CONDITIONS 

The table below includes a summary of the industrial processes and related control equipment. 

Process Equipment Description for Units to be tested: 

SV046 EU040 Line 1 Pellet Induration 

SV047 EU04l Line 1 Pellet Cooler Exhaust: pellet cooling after induration 

SV1l6 EU039 Line 1 Kiln Cooler Discharge Dump Zone (new scrubber) 

SV045 EU039 Line 1 Kiln Cooler discharge Vibrating Feeders (existing scrubber) 

SV045 EUI13 Line 1 Pellet Conveyor Transfer 

SV045 EU1l4 Line 1 Pellet Conveyor Transfer 

5 
Process Operating Parameter Monitoring During Performance Test: 

SV046, SV047, SV116, SV045 - Line 1 operations will be monitored by: 

Greenball feedrate (produced), Normal Range 250 LTPH 

Fired Pellet Production, Normal Range 204 LTPH 

Fuel Consumption - Line 1 will be flring on natural gas only 

A sulfur mass balance will be performed by collecting process samples of greenball feed and flred pellet and 

analyzing for sulfur content. The data will be used with the measured stack emissions to determine a sulfur 

removal efficiency of the scrubber. 

Control Equipment Description: 

SV046 - CE056 Ducon Wet Scrubber type VV-O, Size 222 

SV047 - No control device serves the pellet cooler exhaust 

SV116 - CE065 Ducon Wet dynamic Scrubber UW -4 Model IV Size 120 

SV045 - CE055 Ducon Wet Scrubber 

Control Equipment Operating Parameter During Test: 

SV046 - CE056 Gas stream pressure drop across scrubber and water pressure rates at 15 minute intervals 

SV047 - None 

SV116 - CE065 Gas stream pressure drop across scrubber and water flow rates at 15 minute intervals 

SV045 - CE055 Gas stream pressure drop across scrubber and water flow rates at 15 minute intervals 

PART IV. TEST METHODS 

1. The following is a description of the test methods, number of test runs, length of test runs, and sampling rate for 

each pollutant 

A. EPA Method 1 for the location of sampling ports and points. One determination per test location. A 

determination of cyclonic flow will be made at each source and results included in the test report. 

B. EPA Method 2 for stack gas velocity and volumetric flow rate. One determination per EPA Method 5 test 

run. 

C. EPA Method 3 or 3A to determine stack gas molecular weight at the waste gas stack. Ambient 

concentrations of oxygen and carbon dioxide are expected for the non-combustion sources and will be 

assumed for the calculation of stack gas molecular weight. SV046 is only source expected to have subambient levels of oxygen. 

6 

, 
D. EPA Method 4 for determination of moisture content in stack gas. One determination per EPA Method 5 

test run. 

E. EPA Method 5 for the determination of particulate emissions from stationary sources. Three 6O-minute test 

runs. A minimum of 32 dry standard cubic feet will be obtained for each sample with the exception of 

SV045 which requires a minimum sample volume of 60 dry standard cubic feet per NSPS regulations. 

F. EPA Method 202 for the determination of condensible particulate. Performed in conjunction with EPA 

Method 5. 

G. EPA method 201A for determination of particulate matter < 10 microns to be performed at the pellet cooler 

exhaust. It is expected that isokinetic sampling (80 percent<I<120 percent) as required by the method may 

not be achievable due to the conditions of the stack (hot gases with low velocity). During previous tests on 

Line 2 Pellet Cooler for PM 10 the tester was able to maintain the cut point between the required 9.0 to 11.0 

microns. 

H. EPA Method 6C for the detemrination of sulfur dioxide emissions. Three 60 minute runs in conjunction 

with EPA Method 5. 

I. EPA Method 7E for the determination of oxides of nitrogen emissions. Three 60 minute runs in 

conjunction with EPA Method 5. 

J. EPA Method 9 will be used to determine the visible emissions. A single one-hour test will be made on all 

sources except SV045 will be tested for 3 one-hour periods as required by NSPS. 

K. EPA Method 10 for the determination of carbon monoxide emissions. Three 60 minute runs in conjunction 

with EPA Method 5 

L. EPA Method 25A for the determination ofVOC emissions. Instrument will be calibrated using either 

propane or methane calibration standards in air, the results will be reported as propane. Three 60 minute 

runs in conjunction with EPA Method 5. 

M. EPA Method l3B for the determination of fluoride emissions. Three 60 minute test runs 

N. ASTM Method Ontario-Hydro for the determination of mercury emissions and analysis of reagent solution 

from irnpingers one through three for the determination of Antimony, Arsenic, Barium, Beryllium, 

7 
Cadmium, Chromium, Cobalt, Copper, Lead, Manganese, Nickel, Phosphorus, Selenium, Silver, Thallium 

and Zinc. Three 120 minute test runs. 

PARTV.CEMS 

There are no CEMS located at the emission points to be tested. 

P ART VI. OTHER 

The particulate, mercury and metal emission measurements will be reported in units of lblhr, and lbllong ton process 

feed (i.e. greenball, fired pellet production or ore feed rates). Particulate emission measurements will also be 

reported in units of gr/dscf. EPA Method 51202 results will be reported as fllterable, fllterable plus organic 

condensibles, and total including filterable, organic condensibles and aqueous phase condensibles. Filterable plus 

organic condensibles emission rates and concentrations are used to compare to MN. Rules. The total particulate 

number representing filterable, organic condensibles and aqueous condensibles is used to represent PMlO emissions 

at the waste gas scrubber stack and kiln cooler discharge stack(s) since Method 201A typically cannot be performed 

on sources with wet scrubbing devices which create a moisture saturated gas stream. 

Composite greenballs, fired pellets will be analyzed for sulfur content to be used in the mass balance study. 

Testing Schedule: 

WeekI 

Sunday Monday Tuesday Wednesday Thursday Friday Saturday 

5/1/05 5/2/05 5/3/05 5/4/05 5/5/05 5/6/05 5/7/05 

Setup Test Test both Line I Test Line I Pellet Test Line I Waste Setup Test 

Equipment Pellet Cooler Cooler Stack Gas Stack Equipment 

(II 00-1800) (SV047) (SV047) (SV 046) Line I Cooler 

and PMIO Mercury and Discharge Scrubber 

Waste Gas Stack (0800-1500) Metals Stacks 

(SV046) (0800-1600) (SV045 and 

PM and Opacity Test Line I Waste SV116) 

(0800-1500) Gas Stack 

(SV 046) 

Fluorides, NOx, 

SOl, CO and VOC 

(0800-1500) 

8 
Testing Schedule Continued: 

Week 2 

Sunday Monday Tuesday Wednesday Thursday Friday Saturday 

5/8/05 5/9/05 511 0/05 511 1105 5/12105 5113/05 5114/05 

Test Test 

Line 1 Cooler Discharge Line 1 Cooler Discharge 

Scrubber Stack Scrubber Stack 

(SV045) (SVI16) 

PM and Opacity PM and Opacity 

(0800-1500) (0800-1500) 

Relocate Test Equipment Demobilize Test Equipment 

(1500-1700) (1500-1700) 

Last Maintenance Performed. 

Line 1 was restarted November 29,2004 after being shut down since June of 1999. The line was in operation until 

February 2005 when it was shut down for modifications related to the Emissions and Energy Reduction Project. 

Line 1 was restarted April 3, 2005. The vibrating feeder replacement on Line 1 pellet discharge was completed in 

December of 2004. A list of repairs or maintenance activity, for the sources listed, performed 30 days prior to the 

testing will be provided in the stack test report. 

Test Report: 

One complete test report (one hard copy) will be post marked on or before 45 days from the last performance test 

date. A CD-ROM copy of the report in PDF format will be submitted within 105 days of the test last performance 

date. 

Submittal Address: Andy Place 

Performance Test Coordinator 

Minnesota Pollution Control Agency 

520 Lafayette Road 

St. Paul, Minnesota 55155-4194 

9 
Phone: (651) 296-7169 

Email: andrew.place@pca.state.mn.us 

10 
AppendixJ 

Project Participants 
Minnesota Pollution Control Agency 

Andy Place- Performance Test Coordinator 

Robert Beresford - MPCA Duluth Area Office 

United Taconite Company 

Brad Anderson - Section Manager, Environmental 

Barr Engineering Company 

Tim Russell- Vice President / Chemical Engineer 

George Pruchnofski - Vice President 

R. Paul Taylor - Ph.D. 

Tom Kuchinski - Project Manager 

Dan Koschak - Team Leader 

Bill Scott - Stack Test Technician 

Jason McCann - Stack Test Technician 

Project Participants