# AppendixE Calibration Data

# BARR Engineering Company Project Sample Lac. Date Operators United Taconite Co. 

### Line 1 Waste Gas Stack 

### 5/3/2005 T. Kuchinski Analyzer Make 

## 1 Mod. 

## 1SN API 100AH Analyzer Range (span), PPM: 

### 500 Stripchart Speed (units): 20 cmlhr


## ANALYZER CALIBRATION DATA Note: Difference must be less than +/- 2 percent of span 

### Cylinder Test Runs: Test 1 R1 Value, PPM Zero Gas 0 Mid-range 245.7 High-range: 461


## SYSTEM CALIBRATION BIAS AND DRIFT DATA: EPA METHOD 7E - Nox ANALYZER CALIBRATION

Cylinder Serial No. Zero Gas 

# - Mid-range CC12793 High-range CC40072

Analyzer Absolute Difference, Calibration Difference Percent of Response, PPM PPM Span 0.1 0.1 0.02% 243.4 2.3 0.46% 461.8 0.8 0.16%

Note: System Cal bias cannot exceed +/- 5 percent of span. Drift cannot exceed +/- 3 percent of span
Initial Values Final Values Analyzer Cal System Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response, Cal. Bias TEST RUN 1 Time (sec) PPM PPM % of Span PPM % of Span Zero Gas 0.1 0.4 0.06% 2.0 0.38% Upscale Gas 243 238.1 -1.06% 239.9 -0.70% TEST RUN 2 Zero Gas 2.0 2.0 0.00% 1.7 -0.06% Upscale Gas 243.4 239.9 -0.70% 234.2 -1.84% TEST RUN 3 Zero Gas 2 1.7 -0.06% 1.5 -0.10% Upscale Gas 243.4 234 -1.84% 233 -2.08% TEST RUN 4 Zero Gas 2 1.5 -0.10% 2.2 0.04% Upscale Gas 243.4 233 -2.08% 237 -1.28% System Calibration Bias 

# =[(System Cal. Response
- Analyzer Cal. Response) / Span] x 100 Drift 

### = [(Final System Cal. Response
- Initial System Cal Response) / Span] x 100 Cert. PPM 0 245.7 461

Drift, Percent of span 0.32% 0.36%

-0.06% -1.14%

-0.04% -0.24%

0.14% 0.80%

# BARR Engineering Company Project Sample Loc. Date Operators United Taconite Co. Line 1 Waste Gas Stack 

### 05/03/05 T. Kuchinski 

### Analyzer Make 

## I Mod. 

## I SN 100AH Analyzer Range (span), PPM:

__**1.:..0::...;0~_** 

### Stripchart Speed (units): 20 cm/hr


## ANALYZER CALIBRATION DATA Note: Difference must be less than +/- 2 percent of span 

### Cylinder Test Runs: Test 4 R1 Value, PPM Zero Gas 0 Mid-range 50.5 High-range: 93.1


## SYSTEM CALIBRATION BIAS AND DRIFT DATA: EPA METHOD 6C - 502 ANALYZER CALIBRATION

Cylinder Serial No. Zero Gas Nitrogen Mid-range CC68786 High-range CC121446

Analyzer Absolute Difference, Calibration Difference Percent of Response, PPM PPM Span 0.1 0.1 0.08% 51.5 1.0 1.00% 92.9 0.2 0.20%

Note: System Cal bias cannot exceed 

### +/- 5 percent of span. Drift cannot exceed 

### +/- 3 percent of span
Initial Values Final Values Analyzer Cal System Cal System Cal System Cal System Cal Response Response, Response, Cal. Bias Response, Cal. Bias TEST RUN 1 Time (sec) PPM PPM % of Span PPM % of Span Zero Gas


## - 0 0.9 0.82% 1.3 1.22% Upscale Gas 

# - 52 47.6 -3.90% 48.1 -3.38% TEST RUN 2 Zero Gas 

# - 0 1 1.22% 1.7 1.58% Upscale Gas 

# - 52 48.1 -3.38% 49.3 -2.20% TEST RUN 3 Zero Gas 

# - 0 1.7 1.58% -0.03 -0.11% Upscale Gas


## - 51.5 49.3 -2.20% 48 -3.20% TEST RUN 4 Zero Gas 

# - 0 -0.03 -0.11% -0.10 -0.18% Upscale Gas


## - 51.5 48.3 -3.20% 48 -3.70% System Calibration Bias 

### = [(System Cal. Response
- Analyzer Cal. Response) / Span] x 100 Drift 

# =[(Final System Cal. Response
- Initial System Cal Response) / Span] x 100 Cert. PPM 0 50.5 93.1

Drift, Percent of span 0.40% 0.52%

0.36% 1.18%

-1.69% -1.00%
-0.07% -0.50%

# BARR Engineering Company Project United Taconite Co. 

### Sample Lac. Line 1 Waste Gas Stack 

### Date 05/03/05



# ------------------- Operators T. Kuchinski**--~---------------** 

### Analyzer Make 

## I Mod. 

## I SN Vig Model 20 Analyzer Range (span), PPM: 

### 100 Stripchart Speed (units): 20 cm/hr


## Linearity Demonstration EPA METHOD 25A-THC as methane ANALYZER CALIBRATION

Cylinder Serial No. Zero Gas Zero Air Low-range SG9165492 Mid-range CC2937 High-range CC4777

Note: Response must be less than +/- 5 percent of actual calibibration gas values. Cert. PPM System Respon Percent Diff Zero Gas 0 0.4 0.4 Low-range 30.2 29.6 1.99 Mid-range 46.5 45.6 1.94 High-range 90.4 90 0.44 

### SYSTEM CALIBRATION AND DRIFT DATA: Cert. PPM 0 30.2 46.5 90.4

Note: System Calibration cannot exceed +/- 5 percent of span gas value. Drift cannot exceed +/- 3 percent of span
Initial Values Final Values

System Cal System Cal Drift, Response Response, Response, Percent of TEST RUN 1 Time (sec) PPM PPM span Zero Gas 0.4 0.8 0.40% Upscale Gas 30 31.2 1.19% TEST RUN 2 Zero Gas 0.8 0.8 0.00% Upscale Gas 31.2 30.5 -0.66% TEST RUN 3 Zero Gas 0.8 1.0 0.20% Upscale Gas 30.5 31.0 0.47% TEST RUN 4 Zero Gas 1.0 1.1 0.10% Upscale Gas 31.0 30.3 -0.70%Control Module Project: Date: Technician: Orifice Dry Gas

Diff Volume Pressure H Cubic Feet

Nominal Final 

### 0.500 291.795 Actual Initial 

### 286.745 0.50 Total 

### 5.050 Nominal Final



### 1.000 299.870 Actual Initial 

### 292.810 1.00 Total 

### 7.060 Nominal Final 

### 2.000 305.935 Actual Initial 

### 300.885 2.00 Total 

### 5.050 Nominal Final 

### 3.000 311.985 Actual Initial 

### 306.950 3.00 Total 

### 5.035 Nominal Final 

### 4.000 319.080 Actual Initial 

### 313.000 4.00 Total 

### 6.080 C-1 Routine 03/19/05 NRS WetTest Volume, Cubic Feet Final 

### 2772.00 Initial 

### 2767.00 Total 

### 5.00 Final 

### 2780.00 Initial 

### 2773.00 Total 

### 7.00 Final 

### 2786.00 Initial 

### 2781.00 Total 

### 5.00 Final 

### 2792.00 Initial 

### 2787.00 Total 

### 5.00 Final 

### 2799.00 Initial 

### 2793.00 Total 

### 6.00 Leak checks Negative
- ok Positive
-- ok Dry Gas Meter WetTest Temp, F Meter Inlet Outlet Temp, F Final Final Final 

### 69.0 68.0 67.0 Initial Initial Initial 

### 69.0 67.0 67.0 Average Average Average



### 69.0 67.5 67.0 68.3 Final Final Final 

### 71.0 68.0 67.0 Initial Initial Initial 

### 69.0 68.0 67.0 Average Average Average



### 70.0 68.0 67.0 69.0 Tm Final Final Final 

### 72.0 69.0 67.0 Initial Initial Initial 

### 71.0 68.0 67.0 Average Average Average



### 71.5 68.5 67.0 70.0 Tm Final Final Final 

### 74.0 69.0 67.0 Initial Initial Initial 

### 73.0 69.0 67.0 Average Average Average



### 73.5 69.0 67.0 71.3 Tm Final Final Final 

### 75.0 70.0 67.0 Initial Initial Initial 

### 74.0 69.0 67.0 Average Average Average



### 74.5 69.5 67.0

72.0 Tm 

# I

Control Module 1 >5W.C. > in.Hg Barometric Pressure Previous Y
--- Previous Delta H - Elapsed Meter Time of Coefficient Cal. Point Y Minutes SEC



### 12 42.14 Minutes


### 12.70 0.9912 Minutes SEC



### 12.0 47.68 Minutes



# . 12.79 0.9928 Minutes SEC 

### 6 30.45 Minutes


### 6.51 0.9907 Minutes SEC



### 5.0 20.53 Minutes


### 5.34 0.9935 Minutes 

### 5.0 35.53 Minutes


### 5.59 0.9863 Average 

# I 0.9909 29.19 0.9905 1.9111
Orifice Coefficient dH@



### 1.8451

1.9084

1.9334

1.9526

1.9792 1.9237

# BARR Routine Dr'} Gas Meter Calibration 

## \\, 

### , Control Module Number: 

## c.-1- Leak Checks Barometric Press.: 

### 2 c 

### r.(t Date: 

### 3-19 

## -oS' Positive 

### erk 5 in. W.C. Previous Y: .C{QO:> Technician: A.)f?- '; Negative 

## c\!... 15 in.Hg Previous**~H:** 

### i.**~r** l! (
Orifice Dry gas WetTest Dry Gas Meter WetTest Elapsed Meter Orifice DiffPres. Volume Volume Temp (""F) Meter Time of Coefficient

("H2O) (Fe)**(Ft~)** Inlet Outlet Temp (""F) Nominal Rnal Rnal Rnal Rnal Rnal



## ,S- Z"l**(.1'1~** 

### 2..112- 

## &4 <.of' 

### Gf Actual. Initial Initial Initial Initial 

### .)**2~c..** 

### ..1LjS- 

### 21&,'1 

# t;; Gl Average Average

(.:,""1**~IS** AverageTm Dry Gas Meter DiffPres. Volume Temp (""'F)

("H 2O)**(Ft~)** Inlet Outlet Nominal Rnal Rnal Rnal /.0 

### '1 &;8 

## G1 Initial Initial Initial**~"'i** 

### G::s' Average Average 

## ltl c."**~** Average Tm Orifice Dry gas WetTest Dry Gas Meter DiffPres. Volume Volume Temp (""F)

("H 2O) (Fe)**(Ft~)** Inlet Outlet Nominal Rnal Rnal Rnal Rnal Rnal 

### 2.0 3Q$','13S' 

### 2lXG 2.. 

## (0'1 

## Gl Actual Initial Initial Initial Initial Initial 

### LO ')OU 

### .'iSS- 

### 21**~l** 

## l?Y' 01 Average Average

( 1.S' <,,:>1).SAverageTm Orifice Dry gas WetTest Dry Gas Meter DiffPres. Volume Volume Temp (""F)

("HzO) (Fe)**(Ft~)** Inlet Outlet Nominal Rnal Rnal Rnal Rnal Final 

### ·S .0 

## l.?'1 

# Gl Actual Initial Initial Initial Initial Initial 

### 3CG. c

### l"S 

### 2(£'1 

## iii**G~** 

## Col Average Average 

### /3.:S-**G~** AverageTm Dry Gas Meter Volume Temp("'"'F)

(Ft') Inlet Outlet Nominal Rnal Rnal Rnal Rnal 

## {i .0 31'1.0g'**l~** 

### 10 

## 01 Initial Initial 

## 1.0"1 Gl Average Average 

### 0cr.S- 

# <0, Average TmControl Module Project: 

# Q Routine 05/10105 NRS Date: Technician: Orifice Dry Gas WetTest

Diff Volume Volume, Pressure H Cubic Feet Cubic Feet

Nominal Final Final 

### 0.500 102.360 3292.00 Actual Initial Initial 

### 97.345 3287.00 0.50 Total Total 

### 5.015 5.00 Nominal Final Final



### 1.000 108.395 3298.00 Actual Initial Initial 

### 103.370 3293.00 1.00 Total Total 

### 5.025 5.00 Nominal Final Final 

### 2.000 96.345 3286.00 Actual Initial Initial 

### 91.340 3281.00 2.00 Total Total 

### 5.005 5.00

l'<UIIIIIIClI Final Final

,., "')0 

### 114.450 3304.00 Actual Initial Initial 

### 109.410 3299.00 3.00 Total Total 

### 5.040 5.00 Nominal IFinal Final 

### 4.000 120.480 3310.00 Actual Initial Initial 

### 115.460 3305.00 4.00 Total I-:-otal 

### 5.020 5.00 Leak checks Negative
- ok Positive
- ok Dry Gas Meter Wet Test Temp, F Meter Inlet Outlet Temp, F Final Final Final 

### 75.0 73.0 74.0 Initial Initial Initial 

### 73.0 72.0 74.0 Average Average Average



### 74.0 72.5 74.0 73.3 Final Final Final 

### 76.0 74.0 74.0 Initial Initial Initial 

### 75.0 73.0 • 74.0 Average Average Average



### 75.5 73.5 74.0 74.5 Tm Final Final Final 

### 73.0 72.0 74.0 Initial Initial Initial 

### 72.0 72.0 74.0 Average Average Average



### 72.5 72.0 74.0 72.3 Tm Final Final Final 

### 78.0 74.0 74.0 Initial Initial Initial 

### 76.0 74.0 74.0 Average Average Average



### 77.0 74.0 74.0 75.5 Tm 

# I Final Final Final 

### 79.0 75.0 73.5 Initial Initial Initial 

### 78.0 74.0 74.0 Average Average Average



### 78.5 74.5 73.8

76.5 Tm 

# I >5W.C. > in.Hg Barometric Pressure Previous Y - Previous Delta H - Elapsed Meter Time of Coefficient Cal. Point 

### Y Minutes SEC



### 12 24.17 Minutes


### 12.40 0.9943 Minutes SEC



### 8.0 57.89 Minutes



### 8.96 0.9934 Minutes SEC 

### 6 23.6 Minutes


### 6.39 0.9907 Minutes SEC



### 5.0 15.24 Minutes


### 5.25 0.9873 Minutes SEC 

### 4.0 34.52 Minutes


### 4.58 0.9911 Average 

# I 0.9914 

# c -( K 00-\

# ~'V\. 12. 

# C q r

# ~ 

# b I CA.

# +**~** dl.--' 

# fJ<.r;Cu J 

### .-"Le.

# J**~A-** C

# ~·--r,**~** 

# .**p~~+-** 

# +-..; --J r ..... I

CC-t./ 

# J/L1. 

# c1-v C

# ~ r

# ~ b f q

# -r~**d~** .

Control Module 1 

### 29.00 0.9909 1.9237
Orifice Coefficient dH@



### 1.8009

1.8783

1.9159

1.9336 

# I

1.9514 1.8960

### Routine Dry 

### Gas' Meter 

### Calibration 

# BARR

,-' 

### Control Module Number: --'=---'"'=_ 

### Leak Checks Barometric Press.: 

### Z"i .cO Date: ::;- - 

### j

### C -0'::;; Positive u Ie 

### at 5 in.H20 Previous Y: ' 

## 7709 Technician: --=-,'-'=:.'tZ-::::..::S'--

_______ _ Negative

__ 

### C'_k...

__at 15 in.Hg Previous**~H: /.~**  

### 237
Orifice DiffPres.
Nominal**l~**

DiffPres.

("H 20) Nominal



### i.O Actual {,O

Diff Pres.

("H 2O) Nominal



### 2.C Dry gas Volume

(Ft') WetTest

Volume

(Ft') Final 

### 3**2.~G::** Dry Gas Meter WetTest Elapsed Time of Meter OrificeControl Module Project: Date: Technician:

## Onf~GaS Diff lume Presu ic Feet INomlna Inal 

### 0.500 42.565 Actual Initial 

### 37.530 0.50 Total 

### 5.035 INominal IFinal 

### 1.000 48.610 Actual Initial 

### 43.575 1.00 Total 

### 5.035 INomlnal Final 

### 2.000 54.690 IActual Initial 

### 49.625 2.00 Total 

### 5.065 

## I Nominal Final 

### 3.000 60.785 Actual Initial 

### 55.710 3.00 Total 

### 5.075 INOminal Final 

### 4.000 67.885 Actual Initial 

### 61.805 4.00 Total 

### 6.080 

## I C-2 Routine 

### 4/23/2005 NRS Wet Test Volume, Cubic Feet !Final 

### 3045.00 Initial 

### 3040.00 Total 

### 5.00 ·Final 

### 3051.00 Initial 

### 3046.00 Total 

### 5.00 IFinal 

### 3057.00 Initial 

### 3052.00 Total 

### 5.00 Final 

### 3063.00 Initial 

### 3058.00 Total 

### 5.00 IFinal 

### 3070.00 Initial 

### 3064.00 Total 

### 6.00 

## I



## I Leak checks Negative
- Positive
- Dry Gas Meter Temp, F Inlet Outlet Final Final 

### 73.0 70.0 Initial Initial 

### 71.0 69.0 Average Average



### 72.0 69.5 70.8 Final Final 

### 76.0 71.0 Initial Initial 

### 73.0 70.0 Average Average



### 74.5 70.5 72.5 Tm 

## I rlnal Final 

### 79.0 72.0 Initial Initial 

### 77.0 71.0 Average Average



### 78.0 71.5 74.8 Tm Final Final 

### 81.0 72.0 Initial Initial 

### 79.0 72.0 Average Average



### 80.0 72.0 76.0 Tm Final Final 

### 83.0 73.0 Initial Initial 

### 81.0 72.0 Average Average



### 82.0 72.5

77.3 Tm 

## I ok ok Wet Test

Meter Temp, F

Final 

### 69.0 Initial 

### 69.0 Average



### 69.0 Final 

### 69.0 Initial 

### 69.0 Average



### 69.0 Final 

### 69.0 Initial 

### 69.0 Average



### 69.0 Final 

### 69.0 Initial 

### 69.0 Average



### 69.0 Final 

### 68.5 Initial 

### 69.0 Average



### 68.8 Barometric Pressure Previous Y - >5 W.C. Previous Delta H - > in.Hg Elapsed Meter Time of Coefficient Cal. Point Y Minutes SEC



### 12 36.25 Minutes


### 12.60 0.9951 Minutes SEC



### 9.0 2.3 Minutes



### 9.04 0.9971 Minutes SEC



### 6.0 29.3 Minutes



### 6.49 0.9929 Minutes SEC



### 5.0 19.27 Minutes



### 5.32 0.9908 Minutes SEC



### 5.0 31.4 Minutes



### 5.52 0.9928 Average 

## I 0.9937 29.34 0.9909 1.8875
Orifice Coefficient dH@



### 1.8143

1.8624

1.9159

1.9311

1.9228 1.8893 

## I

# BARR
Control Module Number: 

# c..-2 Date: j-l3 

### -oS" 

### Routine Dry Gas Meter Calibration Leak Checks Positive 

## ck Technician: tJ(LS**~~==------------------** Negative 0 

# It..
Orifice DiffPres.

("H 20) Dry gas Volume

(Ft') Nominal Final



## oSc 42. 50S"

Orifice Diff Pres.

("H 20) Nominal \.0 Actual



### 1.0

Diff Pres.

("H 20) Nominal 2...6 Actual

Orifice DiffPres.

("H 20) Nominal 

### "3 0

Diff Pres.

("H 20) Nominal



### 'i.e) Dry gas Volume

(Fe) Final 

### 4 "

Initial 

### LJ3S7<;

Dry gas Volume

(Fe) Final

### ~,1ff;" Initial

Volume

(Fe) Final 

### cOT WetTest Volume

(Fe) Final 

## 3o'-i 

## SInitial jO,-{O

WetTest Volume

(Fe) Final 305"'(

Initial 

### 3Uil.o

Volume

(Ft') Final 

### 305"1

Initial 3"lS"2

WetTest Volume

(Fe) Final 

### 30<03

Initial

Volume

(Fe) Dry Gas Meter Temp ('""'F) Inlet Outlet Final Final j{3 

# 70

Initial 

## 71. Average 

### tL AverageTm Dry Gas Meter Temp ('""'F) Inlet Outlet Final 

### -11.0 Initial 

## 13 Average

### 74.SAverageTm Dry Gas Meter Temp (""F) Inlet Outlet Final Final 

### 7'1 "12.. Initial Initial 

# 71 II Average 

### is liS

AverageTm Dry Gas Meter Temp (""'F) Inlet Outlet Final Final**~,** 

### i 

## 72.. Initial 

## 1"2. Average Average 

### 80 

## 1"2... AverageTm Dry Gas Meter Temp ("""F) Inlet Outlet Final**~.** Initial 

### 8'( Average



## 1'- Final 

# i3 Initial 

### \.L
Average Tm WetTest Meter Temp ('""F) Final**~,9**

Final 

## "''1 Initial 

### (,'1

Final 

# (09 Initial 

## CCI Barometric Press.: 

### 29.3,-( at 5 in.H20 Previous Y: 

### .9"10 c( at 15 in.Hg Previous D.H: 

### t. 'i< 

### 3' 

### 1 ':l"' Elapsed Time of Calibration Point Minutes Meter Coefficient Orifice

### EPA M5 POST TEST METER CALIBRATION 

# BARR Project Name: United Taconite Module Number: C-2 

# -=--=---- Date: 7-May-05 Tech: ..;.NR.:.:..:::S=--
__

Orifice Dry Gas Wet Test Diff Volume, Volume, Cubic Feet Cubic Feet Final Final 768.400 3201.00 Initial Initial 763.330 3196.00 Total

Initial 3202.00 Total

Initial 3209.00 Total Nominal sample conditions Delta H: 1.3 W.C. Vacuum: 7 in. Hg

Dry Gas Meter Wet Test Tern, F Meter Inlet Outlet Tern , F Final Final Final 80.0 74.0 Initial Initial Initial 81.0 73.0 Average Average Average 80.5 73.5 

# . 77.0 Tm Final 75.0 Initial Initial Initial 80.0 74.0 Average Average Average 80.5 74.5 77.5 Tm Final 75.0 Initial Initial Initial 81.0 75.0 Average Average 81.0 Project No.: 23/69-948-TAK Barometric Pressure: 29.07

71.0 Previous Y : -"""0-.9-93-7- Previous Delta H : 1.8893 --..:...:..:..:.-
Elapsed Time of Cal. Point SEC

Pre cal 

### + 5% Pre cal- 5% Within 5% 

### YIN Meter Coefficient 

### Y

1.0434 0.9440 

### YES Orifice

1.9838 1.7948 

### YES

## EPA lVI5 POST TEST METER CALIBRATION

-/



### , 

# ----- Project Name: 

### !.td_,J 

## 11<"",. Le_ 

### vIodule Number: 

# c..- 2- --='--"'=-------



### Orifice Diff Date: 5 - 

## 7 - 0 ') Tech: 1'0f<..S 

### Dry Gas Volume, Cubic Feet Final·



### -;"( ?'-f Initial



### PTe Template WetTest Volume, Cubic Feet Final



### &

## 32Ct Initial



## 3 

## ! G) (-;



### Initial



### '3202



## .5 2.IL{ c 

### Initial



## 3201. Nominal sample conditions DeltaH: 

## 1·3 

## W.e. Vacuum: 

### I,e in.Hg Dry Gas Meter WetTest Temp, F Meter Inlet Outlet Temp, F Final Final Final 

### : Q ·.,ii 

## g i/ jj 

### Initial Initial Initial 

## 3"'1 

## (3 II Average Average 

## 1St)**~** 

## 75.C:;- Tm Final**l~-** 

### Initial Initial Initial**~()** 

### 7'-t. ""It Average 

## gus Tm Final Final 

### 8'/ 

## le;;- If Initial Initial Initial 

## 8"( 7S- t! Average Average 

## 3"1 

# isProject No.: 

## Z

# ~/6 c 

### 1
_ 

# 9 L{

# Y Barometric Pressure: 

### 2.<1.0'1 Previous Y : 

## ,'1 

## 'i 

# .37 Previous Delta H : 

### I . 

### S' gj 

## 3

Elapsed Meter Orifice Time of Coefficient Cal. Point Y



# . Minutes SEC 

### 7 

## i.f7.71

## EPA lVI5 POST TEST METER CALIBRATION 

# 'BARR

Project Name:

## ~A**l\:k~1 1:c,-",,~**  vIodule Number: (.

- 

## L**~~=-----------** 

### Date: 

### S - 

# 7 -0 

## "5" Tech: 

## /0:2.. S
Orifice Dry Gas Wet Test Diff Volume, Volume, Presure dH Cubic Feet Cubic Feet Final Final**-~.** 

### -S**31~:L** 

### Initial



### 3\11 Total



### PTe Template Nominal sample conditions DeltaH: 

## s· 3 Vacuum: 

### q ,0 

### Dry Gas Meter Inlet Final 

# lJ Initial



### 1'f( Average**l~** 

### Temp, F Outlet Final



## '(5 Initial



### 73 Average 

## 13 Tm Final 

# 13 Initial 

### 1'2
.. 

# .

Average Average 

## l1 1 Z:S

### Initial



## 2'0 Average 

## gO.) Tm Final**(~** 

### Initial 

# 13 Average



## tJ W.e. in. Hg Wet Test Meter Temp, F Final 

### if Initial 

# 7( Project No.:

## Z~!b7 

## - '-(c.fJJ Barometric Pressure: 

## 2. C( 

### ,07 Previous Y : . 

### '1 '1 

## 37 Previous Delta H : 

## IsS' '13

Elapsed Meter Orifice Time of Coefficient Cal. Point Y Minutes SEC 

### S-

### EPA M5 POST TEST l\tIETER CALIBRATION 

# BARR Project Name: United Taconite Module Number: C-2 

## -=...:=----- Date: 27-Jan-05 Tech:**.:..N:..:.R=S~**__

Orifice Dry Gas Wet Test Diff Volume, Volume, Presure dH Cubic Feet Cubic Feet Nominal Final Final 1.57 556.820 2086.00 Actual Initial Initial 551.765 2081.00 Total

Initial 2087.00 Total 5.080 5.00 Nominal Final Final 1.57 568.990 2098.00 Initial Initial 563.920 2093.00 Total 

## IINominal sample conditions Delta H: 1.57 W.e. Vacuum: 4 in. Hg

Dry Gas Meter WetTest Tern, 

### F Meter Inlet Outlet Tern
. F Final Final Final 73.0 69.0 Initial Initial Initial' 72.0 69.0 Average Average 72.5 70.8 Tm Final 70.0 Initial Initial Initial 73.0 69.0 Average Average 74.0 71.8 Tm Final Final 77.0 71.0 Initial Initial Initial 76.0 70.0 Average Average Average 76.5 70.5 Project No.: 23/69-923-TAK Barometric Pressure:
___ 2_9_.6_3_

68.0 Previous Y:
__ 0...:..9-,-9_1_7_ Previous Delta H: _...:1..:..;.8:...;.8-,-0,-9_

Elapsed

. time of Cal. Point SEC

Pre cal 

### + 5% Pre cal- 5% Within 5% 

### YIN Meter Coefficient 

### Y

1.0413 0.9421 YES Orifice

1.9749 1.7869 YESControl Module Project: Date: Technician:

# ~s e ·c Feet omlna Ina



### 0.500 144.650 Actual Initial

### 139.640 0.50 Total 

### 5.010 INomlnal • final 

### 1.000 150.675 IActual Initial

### 145.650 1.00 Total 

### 5.025 INomlnal (-Inal 

### 2.000 156.735 Actual Initial

### 151.690 2.00 Total 

### 5.045 Nominal Final 

### 3.000 162.805 ,Actual Initial

### 157.745 3.00 Total 

### 5.060 INomlnal (-Inal 

### 4.000 168.885 IActual Initial

### 163.825 4.00 Total 

### 5.060 C-3 Routine 4/2/2005 NRS Wet Test Volume, Cubic Feet Final 

### 2933.00 Initial 

### 2928.00 Total 

### 5.00 rlnal 

### 2939.00 Initial 

### 2934.00 Total 

### 5.00 Final 

### 2945.00 Initial 

### 2940.00 Total 

### 5.00 Final 

### 2951.00 Initial 

### 2946.00 Total 

### 5.00 Final 

### 2957.00 Initial 

### 2952.00 Total 

### 5.00 Leak checks Negative
- Positive
- Dry Gas Meter Temp, F Inlet Outlet Final Final 

### 75.0 70.0 Initial Initial 

### 73.0 70.0 Average Average



### 74.0 70.0 72.0 r-Inal Final 

### 80.0 71.0 Initial Initial 

### 76.0 70.0 Average Average



### 78.0 70.5 74.3 Tm Final Final 

### 83.0 73.0 Initial Initial 

### 81.0 72.0 Average Average



### 82.0 72.5 77.3 Tm Final rlnal 

### 86.0 74.0 Initial Initial 

### 84.0 73.0 Average Average



### 85.0 73.5 79.3 Tm Final Final 

### 87.0 75.0 Initial Initial 

### 86.0 74.0 Average Average



### 86.5 74.5

80.5 Tm ok ok Wet Test

Meter Temp, F

Final 

### 69.0 Initial 

### 69.0 Average



### 69.0 Final 

### 69.0 Initial 

### 69.0 Average



### 69.0 Final 

### 68.5 Initial 

### 69.0 Average



### 68.8 Final 

### 68.5 Initial 

### 68.5 Average



### 68.5 Final 

### 68.5 Initial 

### 68.5 Average



### 68.5 >5W.C. > in.Hg Barometric Pressure Previous Y
-- Previous Delta H
--**t-I::lno:::~~** Meter Time of Coefficient Cal. Point Y Minutes SEC



### 12 24.19 Minutes


### 12.40 1.0024 Minutes SEC



### 8.0 51.93 Minutes



### 8.87 1.0024 Minutes SEC



### 6.0 23.01 Minutes



### 6.38 1.0020 Minutes SEC



### 5.0 13.9 Minutes



### 5.23 1.0007 Minutes SEC



### 4.0 32.79 Minutes



### 4.55 1.0005 Average 

### 1.0016 29.22 0.9999 1.8261
Orifice Coefficient dH@



### 1.7624

1.7992

1.8568

1.8655

1.8750 1.8318

### Routine 

### Dry Gas Meter Calibration 

# BARR
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### Control Module Number: 

# C -3 Date: 

## -:zr('i-Z**-O~**

## Techn?c;an:~~A~)Lf,L~S~____________ _ Positive 

## .,;1- Negative 

## "k.
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rH 2 O) (Fe) (Ft") Inlet Outlet Temp (-;:,F) Nominal Rnal Rnal Rnal Rnal Rnal**~C;** 

## /'/'/. loS- 

## 2'133 "1S" '10 

## 0'1 Initial Initial 

### 1"3

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## \.0 ISV.lo7$" 

## 2.13trt 

## 90 II 

# Ceq Initial Initial Initial Initial 

## 1'1 S".(.?S" 

## 293A f{P 

### 'lb Total Average

# -nAverage Tm**I~** ,25"" Orifice Dry gas WetTest Dry Gas Meter DiffPres. Volume Volume Temp (-.>F)

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### 2..0 

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## 5" 

## Jl3 

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### 2'140 'Is' 

## -12-**<O~**

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### 2crS-( 

## 8'& 

# 7'-1 Initial Initial Initial Initial 

### 2'1t.j(o C;S L.( 

## 70 Average**~S** AverageTm 

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## 4.0 I 

## Ce'&'.5?iS" 2.95"7 

## 'b7 '1SInitial Initial Initial Initial Initial 

### Z9S"2 ;?&i 

## 'I 1'o'6,SAverage

### g-It"SAverage Tm 

## g-O cSBarometric Press.: 

# 2**~** 

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## Z. 5 in. W.C. Previous Y: • '191 

### 'i 15 

### in.Hg Previous t>H: 

### IS2Gl Elapsed Meter Orifice Time of Coefficient Calibration Point Minutes



### {**.'(i"~1S'**

### EPA M5 POST TEST METER CALffiRATION 

# BARR Project Name: United Taconite Module Number: C-3 ...:;....:..---- 

### Date: 7-May-05 Tech: NRS ..;;...;;;....:...---



### Orifice Dry Gas WetTest Diff Volume, Volume, Presure dH Cubic Feet Cubic Feet Nominal Final Final 1.48 989.860 3230.00 Initial Initial 982.800 3223.00 Total

Initial 323l.00 Total

Initial 3237.00 Total Nominal sample conditions Delta H: 1.48 W.e. Vacuum: 8 in. Hg

Dry Gas Meter WetTest Tern, F Meter Inlet Outlet Tern , F Final Final Final 81.0 74.0 Initial Initial Initial
. 78.0 73.0 Average Average Average 79.5 73.5 76.5 Tm Final 75.0 Initial Initial Initial 81.0 74.0 Average

Initial Initial Initial 83.0 75.0 Average Average 83.5 Project No.: 23/69-948-TAK Barometric Pressure: 29.07 --....;...;..-'-'-



### 70.5 Previous Y : l.0016 Previous Delta H : --:-1'-'-.8";"31;;";8-

Elapsed Time of Cal. Point SEC

Pre cal 

### + 5% Pre cal- 5% Within 5% YIN Meter Coefficient Y

l.0517 0.9515 YES Orifice

1.9234 1.7402 

### YES

## EPA M5 POST TEST lVlETER CALIBRATION 

# \··BARR
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## 7g Average 

## 7'1S**~3** 

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### 70.SInitial 

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# ~l1'~:i~;i1J;!~\t~~ H2S0411(MN04

# BARR Engineering Company

Pitot Tube Number: Length: 

# 4' Function: 

### Free

1. Are face openings perpendicular to tube axis? DYES ( go to 2) 

### @ NO (go to 1a)

2. Are face openings parallel to longitudinal axis? 

## IiS1 YES ( go to 3)

3. Are legs of equal length? 

### g] YES ( go to 4) 

## _ 0 NO (go to Za)



# o NO (go to 3a)

4. Are center-lines of legs coincident? 

# o YES (got05) 

# o NO (go to 4a)

5. Does this pitot tube pass all of thepbO;e**I~ria?** 

# - j 

# ibl/ 

# t Technician Signature:

# //lL~I/Z 

# I L... 

# J S-Type Pitot Tube Geometry Check Inspection Date: 

### I Z -2.{-04 Technician: /\Jll. 

## S**----~~~---------------**

1a. If NO, is angle less than 10°? 

### gj YES ( go to 2)
IJo.; I

# --8:--~--. . 

## -

, I 

# . .

2a If NO, is angle le,ss than 50?

_ 

## D YES ( go to 3) 

## D NO (discontinue use)

# ~ .. 

### - 

### -.:... 

# : -- 

# ---: --.

- 

## - I I 

# . .

D NO (discontinue use)**----~-:J:--** 

# -1;-' ..... -. -:",-

____ .::'l_

3a. If NO, is difference less than 1/8 inch? 

## D YES (got04) 

## . D NO (discontinue use)

4a If NO, are center-lines of face openings less than 1/32 inch? 

## D YES (go to 5) 

## D NO (discontinue use)



## lRl YES DNO

# BARR Engineering Company

Pitot Tube Number: 

## )-1 Length: 

## S 1 

### --""'==::--- Function: 

# e.9 1 Free

1. Are face OPenings perpendicular to tube axis? 

## bQ. YES ( go to 2) 

## D NO (go to 1a) J**~~** 1

# '-~

# .. E=Ej-------

]**~** t**~.~--I** I**~:~** I 

# . .

2. Are face openings parallel to longitudinal axis? 

## I2Sl YES (go to 3)

3. Are legs of equal length?**~** YES (go to 4) 

## . D NO (go to Za)



## D NO (go to 3a)

### -k----~:"---*-)-----

4. Are center--fmes of legs coincident? 

## 123-.YES (go to 5)

. 

## D NO (go to 4a)

### -k----~~---_<--)-----

5. Does 

### Otis

# ~trube pass

# ~ 

# 'lY1Itteria'

Technidan Signature: V 

# V..
. 

# L
-- J S-Type Pitot Tube Geometry Check Inspection Date: 

## !-2. - 

## L \ -(:'-1 

### Technician: l\Ji'2..'::,**~--~~-----------------**

1a If NO, is angle less than-10°? DYES ( go to 2)

tJoj" I

# --~--~--. . 

# - I I 

# . .

2a. If

## NO. is angle le;;s than 50?
. 

# o YES ( go to 3)**r.$~--:::::'V**

-.o..:'.:r
_____ 

## -="**~-:::** 

# ,"""" 

# o NO (cflScontinue use)**/** 

### .. I I . I 

# -- -- 

### -- 

# -_.. 

### . .**~** 

### !



# o NO (discontinue use)**r-i'--~-V** 

### Lc**~**



## .......

3a. If NO. is difference less than 118 inch? 

## D YES (go to 4) 

# o NO (discontinue use)

4a. If NO, are center...Jines of face openings less than 1132 inch? DYES ( go to 5) 

# o NO (discontinue use)

E&YES DNO

# BARR Engineering Company

Pitot Tube Number: Length: 

## S \**r---··-:·~** 

### Function:**~** 

### I 

### Free

1. Are face openings perpendicular to tube axis? 

### @ YES ( go to 2) 

# o NO (go to 1a) I**~~** I

# '~~

# ..i .:

# * .**--~-----** 

# .

t ('-..--.. I**:-----~-!** I •
2. Are face openings parallel to longitudinal axis? 

### gJ YES ( go to 3)

3. Are legs of equal length? 

## lS1 YES ( go to 4) 

## . 0 NO (go to Za)



# o NO (go to 3a)

### -t----~'!----*-)-----

4. Are center-lines of legs coincident? 

## I2Sl YES ( go to 5) 

# o NO (go to 4a)

5. Does this pitot tube pass all ofthjaIDOVe;critena?

Technician

# Sigoaru~ 

# lidi

# L**~ ./t/~;V**  

### S-Type Pitot Tube Geometry Check Inspection Date: Technician:**~p-s, ------~~---------------** 

1a If NO, is angle less than' 10°? DYES ( go to 2) 

# o NO (discontinue use)

rJ.i I

# --~--~--. . 

# - 

# fL 

# .--11'**-~~--.** I I I 

# . 

# . .

Za. If NO, is angle**I~** than 5'? DYES ( go to 3) 

# o NO (discontinue use)**r-$~---'_-V**



# ."**~-** ,,,.A

3a. If NO, is difference less than 1/8 inch? DYES (go to 4) 

# o NO (discontinue use)

4a. If NO, are center-lines of face openings less than 1132 inch? 

# o YES (go to 5) 

# o NO (discontinue use)



## lSi YES ONO

### Engineering Company

Pitot Tube Number: 

# / -2. I,O 

### Length: i I I$; 

### Function:

# ~I Free

1. Are face openings perpendicular to tube axis? 

## '0 YES ( go to 2) 

# o NO (go to 1a)

2. Are face openings parallel to longitudinal axis? 

### BYES ( go 

### to 3)

3. Are legs of equal length? 

### gJ YES (go to 4) 

# o NO (go to 2a)



# o NO (go to 3a)

### --k----~~---=<~)-----

4. Are center-lines of legs ccincident? 

## IS!. YES ( go to 5) 

# o NO (go to 4a)

## --~----~~----<-=)-----

5. Does this pitot tube pass all of the aqt)v!'l criteria? 

### Mnlo," Signaw,e 

# i'jl/I 

# L S-Type Pitot Tube Geometry Check Inspection Date: 

# i Z - 

### 21**~O** Y Technician: 

### l,)fl-S**~--~~~---------------**

1a. If NO, is angle less than 10°? 

### DYES ( go to 

### 2) 

# o NO (discontinue use)**~** I



# f3e- . I

__ I

__ _ _ __ .


## . .**~L** 

# --t!.**-;.~--.**
, I I I I • 

# . .

2a. If NO, is angle less than 50? 

### DYES ( go to 3) 

# o NO (disccntinue use)

3a. If NO, is difference less than 1/8 inch? 

### DYES ( go to 4) 

## D NO (discontinue use) V t=.--.**---£.,..-.i~_.**

4a. If NO, are center-lines of face openings less than 1/32 inch? 

### DYES ( go to 5) 

# o NO (discontinue use)



## 8J YES ONO

# THERMOCOUPLE CALIBRATION 

# BARR

REFERENCE STANDARDS Hart Scientific 91 03-A sIn A 1B289 Hart Scientific 9140 sIn A1B086 CaJ;Date:
TRACEABILITY



### Temperature Calibraion Points 20 Reference Deg F (To) 20 Probe Temp (deg F) 20 Reference Temp (deg R) deg F + 460 480 Probe Temp (deg R), deg F 

### + 460 480 Difference (degrees) 0 % Diff Abs. T 0.0% Is difference less than 1.5% at all measured points? YES 

# THERMOCOUPLE ID**C~~** 

### 1212212004 

## Meter In CALIBRATION TECHNICIAN: NRS DATE LABORATORY 12/11/2003 12/11/2003 

## 70 150 70 150 

### 70 148 

### 530 610 530 608

0 2 0.0% 0.3%**1700~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**

### 1600~~~~==========~==========~~~~~~~~~~~~~~~ 1500**+~~~21**

### ~ 

### 1400**t'-c:~~":1** <> 

## ..,**~1300+2~~+===========================~~~~~~~~~~~~~~~~~~** ::;)**~ 1200~-~~~~~~~~~~~~~~~~~~~·~~~~~~~~~~~~~**  n:: w**~ 1100~~~~~c~~~~~~~~~~=-~~~,~~~-~~~~~~c~~~~~~~**  w**~ 10001~~~~~~~~~~~~~~~~~.~~~~~~~~~~~~~~~~·~~~~**  ..J a. 

## 5**900+-~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** o

### ~**800~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~12** n:: w**~ 700+-~~~~~~~~~~~~~~~~** **600~~~~~~~~~++~~~=-~~~ 500+-~~~~~~~~~~~~~~~~~~--=-=-~~=-=---~~--~~~** **400~--~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 1.5%? YES


### If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 

### -20 1200

# BARR Engineering Company
Thermocouple Number: 

## Te.**~ c..~** 

# -l

Media Std Used 

### D-8 Reference Deq F (To) Reference Corr Temp (deq R) deq F + 460 Probe Temp (deg F) Probe Temp (deg R). deg F + 460 Difference (degrees) % Diff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's function: 20

"20 

### '-{ go 

# 2..0 ,-{gO

0 0-0

## c:..~·hn 

# I I'v\ <:) 

## c\.,",-\ e. 

# i.**\y~** 

## fV\ I "-

If not acceptable, describe corrective procedures undertaken: 70


### -ZO S"3C 

## '10 S-::So

0 

### 0.0 

### THERMOCOUPLE CALIBRA 

### TION

150 ( S1:;, &;{O**(L/~** (008 

### -"2-**D_~** @NO) @fNO) Date: 1,--2.'-.-OL{ Technician: -.:...N-'--'-"R.:.::"'--
__ _

to

# BARR

REFERENCE STANDARDS Hart Scientific 91 03-A 

### sIn A1 B289 Hart Scientific 9140 

### sIn A1B086 

### Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F + 460 Probe Temp (deg R), deg F + 

### 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points?


### 1700**--,.--,c--:-----,-,-~~~---=-~** 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE ID 

## C-1-0 Cal;Date: 12/22/2004 

## Meter Out CALIBRATION TECHNICIAN: NRS TRACEABILITY DATE LABORATORY Report No. A1B0718 Report No. A1 B2024 12/11/2003 12/11/2003 

### Hart Scientific Hart Scientific 

## 20 20 

### 21 480 481 -1 0.2% YES 

## 70 70**~n** 0:::; 

### 530 529



### 1 0.2% 

## 150 150 610 607



### 3 0.5%

## 1600~S7~~============~======~~~~~~S7~~~~~ 1500**+---'-'~~**

### ~1400~~~ 

### "

## ~1300~~~~~====~==~~~~====~~~~~~=~~~~~~~~~~~ ::>**~ 1200~~~~~~~~~~~~~~~~~~~-~~~~~~~~~~~~~** **~** w**~ 1100~~~~~~~~~7=~~~~~~~~~'~~~~~~~~~~+~-~-~~~**  w**~ 1000~~~'~~~~·c~~~~~~~~~~~c~~:~~~~~~~~~~~~~~~~**  -' Co 

## 5**900~~~~~~~~~~~~'~~~~~~~~~~~~~~~~~~++~** u**~ 800~~~~~~~~~4~~~~~~~~~~~~~~~~~~~~~** **~** w**~ 700~++~~~~++~~~~~++++~++++~** **600~~++~~~~++++~~++~~~++~ 500~~~~~~~~~~~~~~~~~--~~--~~--~~~----~~~** **400~~~~~~~-.~~~~~~~--~~~~~~~~~~~~~~~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 1.5%? l<irapolation limit of calibration from graph: If not acceptable, describe corrective action: NO Enter Upper FAHRENHEIT Limit CALIBRATION RANGE -20 1200

# \



# BARR Engineering Company
Thermocouple Number: 

# TC**-<2-~** 

# - 

# O.

Media Std Used 

### 'D-Z Reference**De~** F (To) Reference Corr Temp**(de~** R)**de~** F + 460 Probe Temp (deg F) Probe Temp (deg R), deq F + 460 Difference (deqrees) % Diff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's function: 20 

### 2..0 4fW 

## 2..t 

## '{g (

-r- 

### I 6·2.

If not acceptable, describe corrective procedures undertaken:



# .----- 70 

# 10 530

## 6~ 

## S2.., -( O.L 

### THERMOCOUPLE CALIBRATION

150 

# [so (';'ID 

## i1-\ 

## 7 (pal 

## -"3 

# o.s- (6§) No) @JNo) Date: i2.-2..2..-Ci..1 Technician: --=-fv_'_f2--..:;.S

___ _

to

# BARR

REFERENCE STANDARDS Hart Scientific 9103-A sIn 

### A 1B289 Hart Scientific 9140 sIn 

### A1B086 

### Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F 

### + 460 Probe Temp (deg R), deg F 

### + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points? 

# THERMOCOUPLE CALIBRATION
THERMOCOUPLE 10**C~~** 

### Cal Date: 

### 4/15/2005 

# Meter In or Out CALIBRATION TECHNICIAN: JMM TRACEABILITY Report No. A1B0718 Report No. A1B2024 

## 32 212 32 212 32 210 492 672 492 670

0 2 0.0% 0.3% YES DATE LABORATORY 

### 12/11/2003 Hart Scientific 

### 12/11/2003 Hart Scientific 

## 400 650 70 400 650 70 392 

### 645 68 860 1110 530 852 1105 528

8 5 2 0.9% 0.5% 0.4%**1700~~~~~~~~~~~~~~TF~~~~73?7~~~~~~~~~~** 

### 1600 1500**--fo--'-~.,..-.j**

### ~ 1400 

# .. "C**~** 

### 1300 :::l**~** 

### 1200**--f2:C~,-,,-**

### ~ 1100

### --fo--'-~~ w 

### :;; 1000 ..J a. 

## is 900 u

### ~**800--fo--'-~** 0:: w 

### ¢: 

### 700 +-=:'-,--:--:7 

### 600**+:-:'-~~=** 

### 500**-+7"~-QI''''-+~ ~~~** **400+,~~r=~=+~~~~~~~~~~~~~~~~=T~~~~=r~=,~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 

### -20 1200

# BARR Engineering Company

Thermocouple Number: 

# --,-C_o----.:::d.'--_"".b""-_

Media Std Used Reference Deg 

### F (To) Reference Corr Temp (deg R) deg F + 460 Probe Temp (deg F) Probe Temp (deg R), deg F + 460 Difference (degrees) % Diff Abso T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's function: 32**3~** 

### 3)..

If not acceptable, describe corrective procedures undertaken: 212 

## dtd.. ;:210 THERMOCOUPLE CALIBRATION

400 

### ,{00 

# 0'Sq d..-

(Yes/No) (Yes/No) 

# I U_I·r-O('"" Date: _:2.L-

__ :::>

__ "">

__ _ Technician: 

## ,i (IA (V"- "

650 Ambient 

# 0,0 "70 CoL.( 

# 5 

# &'1**~**

to

# THERMOCOUPLE CALIBRATION 

# BARR THERMOCOUPLE 10 C-2-0 Cal Date: 

### 4/15/2005 

# Meter In or Out CALIBRATION TECHNICIAN: JMM 

## REFERENCE STANDARDS Hart Scientific 9103-A sIn 

### A18289 Hart Scientific 9140 sIn 

### A1B086 

### Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F 

### + 460 Probe Temp (deg R), deg F 

### + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured pOints? 

### TRACEABILITY 

### Report No. A180718 Report No. A1 B2024 

## 32



# . 32 

### 32 492 492



# o 0.0% YES 

## 212 212 

### 2'11 672 671



### 1 0.1% 

### DATE 

### 12/11/2003 12/11/2003 

### 400 400 

### 394 860 854



### 6 0.7% 

### LABORATORY 

### Hart Scientific Hart Scientific 

### 650 650 

### 645 1110 1105

5 0.5% 

## 70 70**~Q o~**  

### 530 529



### 1 0.2%**1700T:7~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**

### 1600~~~~~~============~==~~~~~~~~~~~~ 

### 1500 +,-:,=.,.-,-'f'-=j

### ~ 

### 1400**-f--:"-~-:-,,-:,I** <If 

## "**~1300~~~~~~~~~~~23~~~~~~** :::l**~ 1200~~~~~~~~~~~~~~~~~** 

### ~**1100~~~~~~~~~~~~~~~~~~~~~~~** w 

### ;

## 1000~~~~~~~~~~~~~~~~~~~~~~~~~~~ Co 

## 6 900**+'-'~=.,.-,-** u

### ~**800+=~~~~~~3** a:: w 

### i!: 700**~=--","","** 

### 600**500~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200\ \,



# BARR Engineering Company

Thermocouple Number: 

# C
- d.- 

# 0

Media Std Used Reference Deg F (To) Reference Corr Temp (deg R) deq F + 460 Probe Temp (deg F) Probe Temp (deq R), deq F + 460 Difference (deqrees) % Diff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's function: 32 

# 32 3:)..

If not acceptable, describe corrective procedures undertaken: 212

### ~td- 

### (;2 L

## i 

# THERMOCOUPLE CALIBRA 

# TION

400 

# 1CJO 

## "$**~7** 

# '1

(Yes! No) (Yes! No) Date: 

## y**~** 

# i 

# s-**~** 

### 0 

# STechnician: 

# J**~**

650 Ambient 

## &5- 0 

# 70 &'1.S**~1**

to

# THERMOCOUPLE CALIBRATION 

# BARR THERMOCOUPLE 10 C-3-1 Cal Date: 12/27/2004 

## Meter In or Out CALIBRATION TECHNICIAN: NRS REFERENCE STANDARDS TRACEABILITY DATE LABORATORY Hart Scientific 91 03-A 

### sIn A1 B289 Report No. A1B0718 12/11/2003 

### Hart Scientific Hart Scientific 9140 

### sIn A1B086 Report No. A1 B2024 12/11/2003 

### Hart Scientific Temperature Calibraion Points 

## 20 70 150 Reference Deg F (To) 20 70 150 Probe Temp (deg F) 21 

### 69 148 Reference Temp (deg R) deg F + 460 480 530 610 Probe Temp (deg R), deg F + 460 481 529 608 Difference (degrees) -1 1 2 % Diff Abs. T 0.2% 0.2% 0.3% Is difference less than 1.5% at all measured points? YES I 

### THERMOCOUPLE CALIBRATION**1700~~~~~--~·~~~~~--~~--~~~~--~~~~------~~~ 1600+=-3+~~~~~~~7'~~~~~~~~~~~~~~~~~~~~TS~~~** **~1500 +=-'---:'-'-~-"1** 

OJ

### ~J400 +='---:'-'--:-'-'-:''-'-1 w**~1300+L~~~========================~~~~~;~~~~~~~~~~** f-

### ~1200T0~~~~~~~~·~~~~~~~=~~~:~S~'~~~~~~~~~~~~ w**~1100+=-~~~~~~~~~~=-~~~~~~~~~~~~~~~~~~~** w**~1000+=~~~~~~~~~~J~~~~~~9~~~~~"~~~~~~~~~~~~~~** -l**~ 900+=~~~~~~~.~~~~~~~~~~~~~~~~~~~~~·~~~~~~**  

### o 

# g**800~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**

## ~ 700

## +=~~~~~~~~~~~~~~~ w

## ~ 600**500~~~~~~~~~~~~~~~~**

### __**~~~~~~**

### __**~~**

### __**--~L~ 400~-~~~~~~~~~~~~~,=~~~~~~~~~~~~~~~**  

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R 

### Enter Upper FAHRENHEIT Are extrapolated limits less than 1.5%? x:trapolation limit of calibration from graph: NO Limit CALIBRATION RANGE -20 1200 If not acceptable, describe corrective action:

# BARR Engineering Company
Thermocouple Number: 

# "'-c
- 

# c..-::; - L

Media Std Used**!)-~** Reference Deg F (To) Reference Corr Temp (deg R) deg F + 460 Probe Temp (deg F) Probe Temp (deg R). deg F + 460 Difference**(de~rees)** % Diff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's. function: 20


### 2C**4~a** '2- 

# !**~1:f(** 

### +1 O.L.

If not acceptable, describe corrective procedures undertaken: 70
1.0 

### 5""30 ( c' 

### ..Ql 

### 52"1



### -I c!:1 • "L 

# THERMOCOUPLE CALIBRATION

150 

### (SO G:> 

## I a il.\**~'** 

### Co<J'i? 

### -2. 0.3, 

### <GINo) 

# <Q;yl No) Date: if 

### -?;-1- - 

### c'-i Technician: i\;/'_) 

## ----=-----

to

# THERMOCOUPLE CALIBRATION 

# BARR THERMOCOUPLE 10 

## C-3-0 Cal Date: 

### 12/27/2004 

## Meter In or Out CALIBRATION TECHNICIAN: NRS REFERENCE STANDARDS TRACEABILITY DATE LABORATORY Hart Scientific 9103-A 

### sIn A1B289 Report No. A1B0718 

### 12/11/2003 Hart Scientific Hart Scientific 9140 

### sIn A1 B086 Report No. A1 B2024 

### 12/11/2003 Hart Scientific 

### Temperature Calibraion Points 

## 20 70 150 Reference Deg F (To) 

### 20 70 150 Probe Temp (deg F) 

### 20 6S 148 

### Reference Temp (deg R) deg F 

### + 

### 460 480 530 610 Probe Temp (deg R), deg F 

### + 

### 460 480 529 608 Difference (degrees) 

### 0 1 2 % Diff Abs. T 

### 0.0% 0.2% 0.3% Is difference less than 

### 1.5% at all measured pOints? YES THERMOCOUPLE CALIBRATION**1700~~~~~~~~---~~~~~~~~~-=~~~~:~~-=---~~~~~-~ 1600~=--+~~~~~~~~~~'~"~~~'~~~~f~2~~~~~~~~~,~~~~~-~~**  

### cr; 

### 1500**~~"'-"-i** OJ

### ~_ 

### 1400**+-:~-'-'-':-:l** w 

# 5**1300~~~~~~~~~~~~~~~==~~~~~~~~~~~~~~ffj** I-**~ 1200+-:~~~~·~~~~~~-:~~~~~~-~~~~~2~~;'~~~~·~~22~~~~**  w**~ 1100~~~~==22~~22~~~~~~~:~~~~~~~~~~~~~~**  W**~ 1000+~~~~~~~~~~~~~~~:~~~~~~~~~'~~~~~~~'~1**  ..J 

## §**900+-:~~~~~~~~~-~~~~~F~~'~~~~~22~~~~~~~22~~~~~** 

## o 

# g**800~~~~~~~~~~~~lb~~~~~~~~~~~~~~~** 

## ffi 700

## +-:~~~~-=-----,--':;;~~~~~~~~':'-'-l**~** 

### 600**~~~~~~G',-,-:--~~~~~-"--'~~-'-i 500~~~7+~~~~-=~~~~~~~~~~~~~--~~~~~:** **400~~-T~~~~'=~-T~~~~~~~~~--~~~-'~~~~~--~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 

### 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE 

### -20 1200

# BARR Engineering Company
Thermocouple Number: 

## TC Q.'-

## 3'- D

Media Std Used**b-~** Reference Deg F (To) Reference Corr Temp (deg R) deg F + 460 Probe Temp (def:j F) Probe Temp (def:j R), def:j F + 460 Difference (degrees) % Diff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of the thermocouple's. function: 20

2.0**L../~o** 

### 2..0 "fifO

0 0.0 70


### Ie S36 

### l?Cj 

## S-2'1

-{ 0· 

### 2- 

### THERMOCOUPLE CALIBRA 

### TION

150

j 

### s;-c**~IO** 

## l'i 

# ?**<Co~ -~**  

## 0_"3

## (~NO)**~NO)** Date: 11

... - <-4--<)',( 

# '. Technician:**_.L/'-.J~I2...=S,,--** __ _

to



## c:.....ttbl MoJ.,,\&. -S

## ~r?M 

# o ....

# -Hd- tL....-.-.C>c."'
....

# rk

If not acceptable, describe corrective procedures undertaken:

# THERMOCOUPLE CALIBRATION 

# BARR <\\4) L 

## r

## THERMOCOUPLE 10 

## TC4-Z { 7)7(0) { 

### Cal;Date: 12/31/2004 

## M-5 Probe CALIBRATION TECHNICIAN: NRS REFERENCE STANDARDS Hart Scientific 91 03-A 

### sIn A 1B289 Hart Scientific 9140 

### sIn A1B086 

### Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F + 460 Probe Temp (deg R), deg F 

### + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points? TRACEABILITY Report No. A1B0718 Report No. A1B2024 

## 32 212 32 212**,.,~** ")L 

### 213 

### 492 672 492 673

0 -1 0.0% 0.1% YES DATE LABORATORY 12/11/2003 

### Hart Scientific 12/11/2003 

### Hart Scientific 

### 400 650 

### Ambient 400 650 70 

### 398 651 

### 69 860 1110 530 858 1111 529

2 -1 1 0.2% 0.1% 0.2%**1700~~~~~~~~~~~~~~~~~~~~~~~~--~~~~-,**

## 1600~~~~====================~tt~~~~ttjt~~~~~~~**1500~~~**

### ~ 

### 1400**~~-?'-:i** 

## '"**~1300~~~C===~~==~~==~======~~~~~~~~~~~~~~~** :::l

### ~**1200~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** w**~ 1100~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**  w**~ 1000~~~~=~~~~~~~~~~~~~~~~~~~~==~==~~~~~i**  ..J 0.. 

## 5**900~~~~** u

### ~**800+7~~~~~~~~~~~~~~~** 0:: w 

### i!: 700**-!---'-'==~** 

### 600**500~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# 'BARR Engineering Company / 

# 1/,/07**~\V** Thermocouple Number: 

## T 

# eLl**-~** 

# { I Y\

Media Std Used 

## D-<? Reference Deq F (To) Reference Carr Temp (deg R) deg F + 460 Probe Temp (deg F) Probe Temp (deg R), deg F + 460 Difference (degrees) % DiffAbs. T (Renkin)
Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

,.,jescription of the thermocouple's function: 

### 32

'52... 

### <-{'11.. 

## 32- '1'12.

0 

### 0.0



# clef-Lei S- 

# fro,!'£- &CiX'-ccot..fk

If not acceptable, descnbe corrective procedures undertaken:

P:\OO\02\OEM\Oatasheets\calibration.xls 

### 212

L.l2... 

## l.91-z.. 2.\ 

### 3> 

## &>73

.... \ 

# 0.' THERMOCOUPLE CALIBRATION

400

-

- l..{(.J'D 

### .: 8"(gO



### 3 

## eLf gc;-g 

## -"L 0:2-

# @~o) @;/NO) Date: 

### i '- -5 \**-c~** Tec.'lnichian: r..; 

### t:..-5. 

### ---==------

650 Other**(..,~t;** 

### to LIIO 

## 5'3 0 

### (pSt 

## !'.fl7'1 ( 1(( 

### 52..'1 -t-I -I 0.( 

### 0.2

to

# THERMOCOUPLE CALIBRATION 

# BARR THERMOCOUPLE ID TC5-1 Cal;Date: 

### 12/23/2004 

## M-5 Probe CALIBRATION TECHNICIAN: NRS REFERENCE STANDARDS Hart Scientific 9103-A 

### sIn A1 B289 Hart Scientific 9140 

### sIn A1B086 Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F 

### + 460 Probe Temp (deg R), deg F 

### + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points? TRACEABILITY Report No. A1B0718 Report No. A1B2024 

## 32 212 32 212 

### 32 211 492 672 492 671

0 1 0.0% 0.1% YES DATE LABORATORY 

### 12/11/2003 Hart Scientific 12/11/2003 Hart Scientific 

### 400 650 Ambient 400 650 70 

### 3 CiQ**V~** 

### 652 hO UV 

### 860 1110 530 859 1112 529

1 -2 1 0.1% 0.2% 0.2%**1700~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**

## 1600~~~~~==================~~~~tT~~~~~~~~.~~ 1500 +-,",......,-'-......,-'-'7l

### ~1400~~~ 

## '"**~1300~~~J=======~~~~~~~==~~~~~~~~~~~~~~~~~~** ::J**~ 1200+7~~~~~~~~~~~~~~~~~~~'~~~~~~~~~~~~**  w**~ 1100~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**  w**~ 1000~~~~~~~L2~~~~~~~~~~~~~~~~~~~~~~~~~**  ...I a. 

## 5**900~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** u

### ~**800~==========~====~~~~==~======~** a:: w**~ 700~~~~~~~~~~~~====~~~** **600~====~~~~~~==~~~~==~~~ 500~~~~~~~==~~~==~~~~~~~~~~~~~~~~~~~~~** **400+,~~~~~~~~~,r~~~~~~~~~'-~~~~--~~~-T~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

# I REFERENCE TEMPERATURE, deg.R I


### Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE I


### -20 1200

# ·BARR Engineering Company

Thermocouple Number: 

# .,..c S- 

## -1-

Media Std Used 

## D-8' Reference Deq F rro) Reference CorrTemp (deq R) deq F + 460 Probe Temp (deq F) Probe Temp (deq R), deq F + 460 Difference (deqrees) % Diff Abs. T (Renkin)

Oiff. less than 1.5% at all points Graph Attached Extrapolated Range with Oiff. <= 1.5%

Description of the thermocouple's function:

If not acceptable, descnbe corrective procedures undertaken:

'.. :.:"

P:\OO\02\OEM\Datasheets\calibration.xls 

### 32 212 

### 3"2- "2..i2 

## '4'12.**~[2.** 

### 32- 2(( 

### t{CJ 2.. 

## 0t{

0 

## -I C).O 0.1 

### THERMOCOUPLE CALIBRATION

Date: 

## /7...- 23-0'1 Technichian: 

### NiLS 

### --!..:=--=-----

400 650 Other

-

- LiOO**G::~** 

## 70**::~00** 1110 

## SSo 

# 311**[~S** 

## 2.**0~ ~9"'1**  I IlL 

### 5'2.'1



### -( +L. 

### - ( 

# a.1 0.1- 6'L

to

# BARR

REFERENCE STANDARDS Hart Scientific 9103-A sIn A 1B289 Hart Scientific 9140 sIn A1B086 Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F 

### + 460 Probe Temp (deg R), deg F 

### + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points? 

# THERMOCOUPLE CALIBRATION

THERMOCOUPLE 10 TC5-2 Cal;Date: 

### 12/23/2004 

## M-5 Probe CALIBRATION TECHNICIAN: NRS TRACEABILITY Report No. A1B0718 Report No. A1B2024 

## 32 212 32 212 

### 32 210 492 672 492 670

0 2 0.0% 0.3% YES 

### DATE 

### 12/11/2003 12/11/2003 

### 400 400 

### 395 860 855

5 0.6% 

### LABORATORY Hart Scientific Hart Scientific 

### 650 Ambient 650 70

..... ,-.r'"'I 0O'"' 

### 70 1110 530 1113 530

-3 0 0.3% 0.0%**1700~~~~~~~~~~~~~7===~~~~~~~~~~~~~~~**

### 1600~~~~~~==~~==~====~~~~~~~~~~~~~~7~~ 

### 1500**~~~ ~**  

### 1400**+---~~** 

# .. ""**~1300~~~~~~~~~~~~~~~==~~~~~~~~~~~~~~** ::l**~ 1200~~~~~~~~~~==~~~~~~~==~~;~~~~~~~~~~~**  0:: w**~ 1100+-~~~~~~~~==~~~~~~~~~~~~~~~~~~~~**  w

### ~**1000+-~:~s+~==~s+~~~~~~~~~~~~~~~~~~~~~~** ...I a. 

## 5**900~~~====~~~~==~~==~~~==~~~~~==~~==~~==~** u

### ~**800tt~~~~~~f4~~~~~~~~~~~~~;r.~~~~~~~** 0:: w**~ 700~====~~==~7~~~==~~~~~** **600~~~~~~~~~~~~~~~~ 500~~~~~~~~~~~~~~~~==~~~~~~~~~~~~~**  

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 

# I REFERENCE TEMPERATURE, deg.R 

# I
Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# "BARR Engineering Company

Thermocouple Number: 

## Tc...S

- L

Media Std Used Reference Deq F (To) Reference Carr Temp (deo R) deq F + 

### 460 Probe Temp (deg F) Probe Temp (deg R). deg F + 460 Difference (degrees) % Oiff Abs. T (Renkin)

Diff. less than 1.5% at all points Graph Attached Extrapolated Range with Diff. <= 1.5%

Llescription of the thennocouple's function: 

# t1-s=

If not acceptable. descnbe corrective procedures undertaken:

P:\OO\02\OEM\Datasheets\calibration.xls 

### 32 212**D-~ ~L**  

### LiZ- 

## <-19<- (';'l2 

### -32- 

### ZIO 

# 492 4>10

<::) 

### -L 0.0 

## 0·3 THERMOCOUPLE CALIBRATION

400



## - L/oo 'i'Co6

### .3""iS1?S5 

# -s 0.10

### (~/NO) r@fNO) Date: 12...-2..3 

### -01..{ Technichian: NiLS --'.-.:::..:....::----



### 650 Other
"'I 

### G"S"O 

## 70 I [{ 0 

### S;:SO 

## <05"-3 

## 1D I 

### (1:5 

# . S30



## t-3 0 

## O·s 0.0

to

# THERMOCOUPLE CALIBRATION 

# BARR THERMOCOUPLE 10 TC 6·2 Cal;Date: 

### 12/22/2004 

### M-5 Probe CALIBRATION TECHNICIAN: JMM REFERENCE STANDARDS Hart Scientific 91 03-A sin A 1B289 Hart Scientific 9140 sin A1B086 

### Temperature Calibraion Points Reference Deg F (To) Probe Temp (deg F) Reference Temp (deg R) deg F + 460 Probe Temp (deg R), deg F + 460 Difference (degrees) % Diff Abs. T Is difference less than 1.5% at all measured points? TRACEABILITY Report No. A1B0718 Report No. A1B2024 

## 32 212 32 212 32 2'11 

### 492 672 492 671

0 1 0.0% 0.1% YES DATE LABORATORY 

### 12/11/2003 Hart Scientific 

### 12/11/2003 Hart Scientific 

### 400 650 

### Ambient 400 650 70 

### 396 649 69 860 1110 530 856 1109 529

4 1 1 0.5% 0.1% 0.2%**1700~=--~~~~~~~~~~~~~~~~~~~~~~~~~~~~**

### 1600fT~~~====================~~~~~~~~~~~~~~~ 

### 1500**+'-::::~~**

### ~1400~~~ 

## ., "0

### ~1300~~~~~====================~~~~~J~~~~~~~~~~ :::l**~ 1200~~~~~~~~~~~~~~~~~~~'~~~~~~~~~~~**  w**~ 1100~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~**  w

### ~**1000~~~~~~~~~~~~~7~'~~~~~~~~~~~~~~~~** ..J a. 

## 5**900~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~~** u

## ~**800f2~~~~~~8P28~~ff~~SFt1~~~~~~~~~~;.re~~** w**~ 700~~~~~~~~~~~~~~~~** **600~~~~~~~~~~~~~~~~~**

## 500~~~~~22~~~~~~~~==~~~~~~~~~-J.**400~--~~~~~~~~~~~~~~~~~~='~~~~-r~~~~** 

### 400 500 600 700 800 900 1000 1100 1200 1300 1400 1500 1600 1700 REFERENCE TEMPERATURE, deg.R


### Are extrapolated limits less than 1.5%? YES
If not acceptable, describe corrective action: FAHRENHEIT CALIBRATION RANGE -20 1200

# BARR Engineering Company

Thermocouple Number:

Media Std Used**D-~** Reference Deq F (To) Reference CorrTemp (deq R) deq F + 460 Probe Temp (deq F) Probe Temp (deq R), deq F + 460 Difference (deqrees) 

### % Diff Abs. T (Renkin)

Diff. less than 1.5% at all pOints Graph Attached Extrapolated Range with Diff. <= 1.5%

Description of thE; thennocouple's function: '\ • i 

### ;f r _,1'</\-( ·:fIAt: 

### t l I.,) "**-~"** h' '" 

### i 

### Y" ./ k

If not acceptable, describe corrective procedures undertaken:

P:\OO\02\OEM\Oatasheets\calibration.xls 

### 32 212**'3~ ~**  j 

### )..,C 

# f.,i 

# 7 1- 

# G7). 

## "3).. 

# J.i/ i{ tJ 

## ,f- 

# 61/ 

# 0 I -I 

### 0.0 6.\ 

### THERMOCOUPLE CALIBRATION

400

- t-f {;' 

## 6**''i;~6 '~(l**  

## C 5>.5"**~** 

## -4 O.S"
@/NO) 

### C@NO) Date: 

### _i 

# d---,-I_J.._J_I_tl_vl

__ Technichian:**_....;J~,~** 

## ___ _

650 Other
!.(.Q 

### /Y),O lllO

### ~:SO**~,<{** 

# '1 

# ret ,..-;, 7 \ \0 

# '1**<;-:.~** 

# 1 -( 

## -I 0·\ O.'L

to

# BARR ANEROID BAROMETER CALIBRATION

Barometer 1.0. Number: 

# bA**-6~­** Barometer Reference: 

# f '''< 0 

### Project Name: l/j,q..c.. 

## 1Vt'j _0::)



### Pretest Calibration:

Before Adjustment After Adjustment

Postiest Check:

Notes:

Barr Engineering Co. 4700 W. 77th St Minneapolis, MN 55437 (952) 832-2600 Reference ("Hg) 

## 2 ';1. I -; r--.

Reference ("Hg)



# 28 . 9 t.{ 

### Project Number: 

# Z ..vEer**~** 

### 9 (-('2; !,fj1( 6(. 

## <- ,

Barometer ("Hg) Date Technician 

### 29·· ZcJ S--Z-cj;- 

# 7tIf !C



# ---- - '----

Barometer ("Hg) Date Technician



# 2fJ, 

# q 0**p~lO'C,7** 

# rA/C

# Appendix F Cylinder Gas Certifications

# 51111

BARROI 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD.• RIVERSIDE, CA 92507 TELEPHONE (909) 653-6780 • FAX (909) 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: 

### June 25 2004 Barr Engineering Co 7390 OHMS Lane Edina**~rn** 

### 55439-2330

CUSTOMER ORDER NUMBER: 

### 20040420ASMF2



# ---------------------------------------------------------------- ---------------------------------------------------------------- COMPONENT CONCENTRATION(vlv) REFERENCE ANALYZER EXPIRATION REPLICATE ± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC67233 VARIAN HODEL 1860 TCD 06/25/04 Carbon Dioxide 5.01 ± 0.05% GHIS SiN NONE 06/25/07 5.01% CYLINDER #: THERHAL CONDUCTIVITY 5.01% CC4.2814 GAS CHROHATOGRAPHY 5.01% @ 8.01% LAST CAL DATE: 06/25/04 MEAN: 5.01%
VARIAN HODEL 1860 TCD 06/24/04 Oxygen 19.98 ± 0.2% GHIS SIN NONE 06/24/07 19.94% CYLINDER #: THER}rnL CONDUCTIVITY 20.05% Nitrogen Balance cA03201 GAS CHROHATOGRAPHY 19.96% CYLINDER PRESSURE: 2000 psig @24.82% LAST CAL DATE: 06/23/04 MEAN: 19.98%

ppm =**~ole/mo1e** % 

### = mo1e-% The above analyses were performed in accordance with Procedure G1 of the EPA Traceability Protocol, Report Number EPA-600/R97/121 ,d ted Se tember 1997. This cylinder

# SW{I " ot b . d if the pressure is less than 150 psig. 

# r, )
I , /l 

## L /7'"'

# II-~**~** ANALYST:**APPROVED:~~~I.~ J_,_/~J~I_~~(4-**  __________________ __ M. S • CALHOUN 

### 6:;;'1" J. T. MARRIN \..
The only liability of this company for gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# 51111

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. a 

### RIVERSIDE, CA 92507 TELEPHONE (909) 653-6780 III 

### FAX (909) 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: John Stock DATE: September 3 2003 Barr Engineering Co 7390 OHHS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: 20030707A



# ---------------------------------------------------------------- ---------------------------------------------------------------- COMPONENT CONCENTRATION(vlv) REFERENCE ANALYZER EXPIRATION REPLICATE ± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC73045 VARIAN HODEL 1860 TCD 09/03/03 Carbon Dioxide 9.05 ± 0.09% GHIS SIN NOliE 09/03/06 9.04% CYLINDER #: THERHAL CONDUCTIVITY 9.04% CC42814 GAS CHR01·I."<TOGRAPHY 9.06% @ 8.01% LAST CAL DATE: OS/29/03 MEAN: 9.05%
VARIAN HODEL 1860 TCD OS/28/03 Oxygen 8.99 ± 0.05% Gl-lIS SIN NONE 08/28/06 8.98% CYLINDER#: THERJ.!."<L CONDUCTIVITY 8.97% l'Iitrogen Balance CCS1204 GAS CHROJ.lATOGRAPHY 9.01% CYLINDER PRESSURE: 2000 psig @ 9.88% LAST CAL DATE: 08/28/03 MEAN: S.99%

ppm 

### =**~~ole/mole** % 

### = mole-% The above analyses were performed in accordance with Procedure G1 of the EPA Traceabili Protocol, Report Number EPA-600iR97/121, dated September 1997. This cylinder should used 

### if the pressure is less than 150 psig.**ANALYST:~~~~~~~------------------APPROVED:----_T~~------------------------** J.

f The only liability of this company for gas which fails to comply with this analysis shall be replacement or**rean~ysis** thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# 51111

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. til RIVERSIDE, CA 92507 TELEPHONE (909) 653-6780 \I FAX (909) 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: John Stock DATE: July 2 2003 Barr Engineering 

### Co 7390 OHMS Lane Edina 

## 1m 55439-2330

CUSTOMER ORDER NUMBER: 20030417A**~--~~~~~~~---~-~----------~~----------~---------------~--------­ -~~-~----~------~--------~~---------------------------** **----------** COMPONENT CONCENTRATION(v/v) REFERENCE ANALYZER EXPIRATION REPLICATE ± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC12793 !-IONITOR LABS HODEL 8440 06/25/03 07/02/03 Nitric Oxide 461 ± 3 ppm Gl-lIS SiN 136 07/02/05 461 ppm 460 ppm NOx 461 ppm CYLINDER #: CaNTIl-lUaUS 461 ppm 461 ppm Nitrogen,02-Free Balance CC50638**CEE~!ILUl-IINESCENCE** 461 ppm 461 ppm CYLINDER PRESSURE: 2000 psig @519 ppm LAST CAL DATE: 06/18/03 MEAN: 461 ppm 461 ppm

ppm 

### =**~ole/mole** % 

### = mole-% The above analyses were performed in accordance with Procedure G1 of the EPA Tractability Protocol, Report Number EPA-600/R97/121, dated September 1997. 1 

### 10;,

## 'YIiOde,,~~the p,."uce ;, 1m thao 150 

### p';g.

## i~**~** \'nOn ANALYST: .'

# ~ APPROVED:

__

# -!~I-l:i**i-O-i\~~!i.L:)'£:;:":X11~**___________ _ B • M .101ARRIN J . 

### T**.~IN** 

# I The only liability of this company for gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# SIIII

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD. 0 

### RIVERSIDE. CA 92507 TELEPHONE (909) 653-67800 FAX (909) 653·2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: 

### John Stock DATE: 

### October 13 2003 

### Barr Engineering Company 7390 

### OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: 200309l2A**--~~~-~--~-~--------~~------~-------------~~---------~----~~---~ ---~-~--------------------------------------------------~-------**  COMPONENT CONCENTRATION(vJv) REFERENCE ANALYZER EXPIRATION REPLICATE :!: EPA UNCERTAINTY STANDARD MAKE, MODEL, SIN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC29033 I·\ONITOR LABS HODEL 8440 10/06/03 10/13/03 Nitric Oxide 245.7 :!: 1.3 ppm 

### GIns SIN 136 10/13/05 245.5 ppm 246.1 ppm NOx 245.7 ppm CYLINDER #: CONTINUOUS 245.2 ppm 245.0 ppm Nitrogen r 02-Free Balance ccn078 CHEIoIILUIoIINESCENCE 245.4 ppm 246.5 ppm CYLINDER PRESSURE: 2000 psig @252.6 ppm LAST CAL DATE: 09/23/03 MEAN: 245.4 ppm 245.9 ppm

ppm 

### =**~ole/mole** % 

### = mole-'/; The above analyses were performed in accordance with Procedure G1 of the EPA Traceability Protocol, Report Number EPA-600jR97j121, dated September 1997. "

# :::::~c

# 'fj35J6'flh

# e p,",,"ce I, 

# 1mfuan 150::':ROVEO

# _...,y~<=-- ______________ _

# B.M.~N The only liability of this company for gas which fails to comply with this analysis shall be replacement 0 reanalysis thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# 51111

BARROl 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS BLVD .• RIVERSIDE. CA 

### 92507 TELEPHONE 

### (909) 653-6780. FAX 

### (909) 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: John Stock DATE: 

### August 27 2003 Barr Engineering Co 7390 OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: 

### 20030707A



# ----------------------------------------------------------------**-----~-~---------~---------~----------~--------~-----~------~---** COMPONENT CONCENTRA T10N(v/V} REFERENCE ANALYZER EXPIRATION REPLICATE ± EPA UNCERTAINTY STANDARD MAKE, MODEL, SiN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC68786 BOVAR HODEL 922H 08/12103 08/19/03 Sulfur Dioxide 50.5 ± 0.6 ppm**G~lIS** SIN VD92284844 08/19/05 50.4 ppm 50.5 ppm CYLINDER #: CONTINUOUS 50.5 ppm 50.5 ppm Nitrogen Balance CC12643 UV PHOTOHETRY 50.5 ppm 50.6 ppm CYLINDER PRESSURE: 2000 psig @55.8 ppm LAST CAL DATE: 08/07/03 MEAN: 50.5 ppm 50.5 ppm

ppm 

### =**~~o1e/mole** % 

### = mo1e-% The above analyses were performed in accordance with Procedure G1 of the EPA Trac ability Protocol, Report Number EPA-600/R97/121. dated September 1997. This cylinder should not be used if the pressure is less than 150 psig. ANALYST:

# n~~~ APPROVED:

__

### ~~---- ____------------------- H.J.HONSON
The only liability of this company for gas which fails to comply with this analysis shall be replacement or reanalysis thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# 51111

BARR01 

# SCOTT-MARRIN, INC. 6531 BOX SPRINGS 8LVD. Q 

### RIVERSIDE. 

### CA 92507 TELEPHONE 

### (909) 653-6780. FAX 

### (909) 653-2430 

## REPORT OF ANALYSIS EPA PROTOCOL GAS MIXTURES

TO: Sam Foss DATE: July 13 

### 2004 Barr Engineering Co 7390 OHMS Lane Edina MN 55439-2330

CUSTOMER ORDER NUMBER: Vbl/s 

### FOSS



# ---------------------------------------------------------------- ---------------------------------------------------------------- COMPONENT CONCENTRATION(v!v) REFERENCE ANALYZER EXPIRATION REPLICATE :!: EPA UNCERTAINTY STANDARD MAKE, MODEL. SIN, DETECTION DATE ANALYSIS DATA CYLINDER NO: 

### CC121446 BOVAR HODEL 92211 07/12/04 Sulfur Dioxide 93.1 :!: 0.9 ppm**G~IIS** SIN VD92284844 07112/06 93.1 ppm CYLINDER#: CONTINUOUS 93.1 ppm Nitrogen Balance CC12025 UV PHOTOl1ETRY 93.3 ppm CYLINDER PRESSURE: 1150 psig @ 111.8 ppm LAST CAL DATE: 06/14/04 MEAN: 93.2 ppm

ppm 

### =**~ole/mo1e** % 

### = mole-% The above analyses were performed in accordance with Procedure G 1 of the EPA T racea i1ity Protocol, Report Number EPA-600/R97/121, dated September 1997. This cylinder should not be used if the pressure is less than 150 psig. ANALYST:

# }~J~**APPROVED:~~~----------- ~1.**  J .1010NSON 

# I J. T .101ARRIN
The only liability of this company for gas which fails to comply with this analysis shall be rePlacement£reanalYSiS thereof by the company without extra cost. STANDARD CALIBRATION GASES IN ALUMINUM CYLINDERS

# iIIIII SCOTT-MARRIN, INC.

CHRONOLOGICAL RECORD OF CERTIFIED CONCENTRATIONS CUSTOMER: Barr Engineering CO 

### PURCHASE ORDER: Vbl/5 Foss



### CYLINDER NUMBER: CC121446 COMPONENT 502 

### DATE 07/10/02 07/17/02 07/12/04



### AVERAGE
NOTES: 93.0 

### ppm 93.0 

### ppm 93.2 

### ppm

93.1 

### ppm

St>'ITECH\CHRONO I.DOC 6/96 

### CUSTOMER CODE: BARR01 

### DATE: 07/13/04

## CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE Customer: Twin City Oxygen Reference # 88-91148 NSG PO# 4424096 Certification Date: 06/15/04 Customer PO# 43778 Expiration Date: 06/15/07 Cylinder # SG9165492BAL Pressure, psig* 2000 

### ANALYTICAL INFORMATION METHOD: This standard was analyzed according to EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards: Procedure G1 (September 1997) 

### ANALYZED CYLINDER Components Methane Balance
- Air

REFERENCE STANDARD Type/SRM Sample # GMIS ( Traceable to SRM # 2750 )

INSTRUMENTATION Instrument/Model/Serial # Rosemount 400A THC 00335 Certified Concentration 30.2 ppm

Cylinder 

### #

CC16937

Last Date Calibrated 

### 06/08/04 Analytical Accuracy** +/-1%



### Concentration 51.57 ppm CH4/AIR

Analytical Method Flame Ionization Detector

Analyst:

___________**~R.;.;..ic;.;..h;.;..a;...;rd.;.;..S~y...;.;k...;.;es~_** 

### This report states accurately the results of the investigation made upon the material submitted to the analytical laboratory. Every effort has been made to determine objectively the information requested. However, in connection with this report, National Specialty Gases shall have no liability in excess of established charge for this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772 "Do not use this standard when cylinder pressure is below 150 psig.

....Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument. NSG 020149LNATIONAL SPECIALTY GASES 630 UNITED DRIVE DURHAM, NC 27713



## CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE Customer: Twin City Oxygen Reference # 88-78516 NSG PO# 3558412 Certification Date: 08/01/02 Customer PO# 39278 Expiration Date: 08/01/05 Cylinder # CC2937 .Pressure, psig" 2000 

### ANALYTICAL INFORMATION METHOD: This standard was analyzed according to EPA Traceability Prctocol for Assay and certification of Gaseous Calibration Standards: Procedure G-1: September 1997. ANALYZED CYLINDER Components Methane Balance
- Air

REFERENCE STANDARD Type/SRM Sample # GMIS ( Traceable to SRM # 2751 )

INSTRUMENTATION Instrument/Model/Serial # Rosemount 400A THC 00335 Certified Concentration 46.5 PPM

Cylinder #

CC36118

Last Date Calibrated 07/16/02 Analytical Accuracy"" 

### +/-1%

Concentration 100.3 ppm CH4/AIR

Analytical Method Flame Ionization Detector

Analyst:

___________ ....:Am:....::..:...:Ly..=J.;..

. .:...P.:..:ro:.:.k:;:0.c:.p.::.ow:..:.i:;:c::::.--z This report states accurately the results of the investigation made upon the material submitted to the analytical laboratory. Every effort has been made to determine objectively the information requested. However, in connection with this report, National Specialty Gases shall have no liability in excess of established charge for this service. Assayed at National Specialty Gases, 630 United Drive, Durham, NC 27713 (919) 544-3772 *00 not use this standard when cylinder pressure is below 150 psig.**~**Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument. NSG 020149L

### NATIONAL SPECIALTY GASES 630 UNITED DRIVE DURHAM, NC 27713



## CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS MIXTURE Customer: Twin City Oxygen Reference 

### # 88-89053 NSG PO# 4271165 Certification Date: 

### 02119/04 CustomerPO# 42921 Expiration Date: 

### 02119/07 Cylinder#: CC47777 Pressure, psig* 2000 

### ANALYTICAL INFORMATION METHOD: This standard was analyzed according to EPA Traceability Protocol for Assay and Certification of Gaseous Calibration Standards: Procedure G1 (September 1997) 

### ANALYZED CYLINDER Components Methane

Balance
- Air

REFERENCE STANDARD Type/SRM Sample #: GMIS (Traceable to SRM # 

### 2751 )

INSTRUMENTATION InstrumentIModellSerial 

### # Rosemount 400A THC 00335 Certified Concentration 

### 90.4 ppm

Cylinder 

### #

CC361i8

Last Date Calibrated 

### 01/23/04 Analytical Accuracy** 

### +/-1%

Concentration 100.3 ppm CH4!AIR

Analytical Method Flame Ionization Detector

Analyst:

____________**J_e_re_m--"-y_K....;.e....;.nw~ort..;.;h.;.;:.y_** 

### This report states accurately the results of the investigation made upon the material submitted to the analytical laboratory. Every effort has been made to determine objectively the information requested. However, in connection with this report, National Specialty Gases shall have no liability in excess of established charge for this service. Assayed at National Specialty Gases, 630 United'Drive, Durham, NC 27713 (919) 544-3772 "Do not use this standard when cylinder pressure is below 150 pslg.**~**Analytical accuracy includes typical known error sources which, at least, include precision of the analytical instrument. 

### NSG 020149l

# Appendix G Visible Enzissions Evaluator Certification'. 

# I 

# I E I IONS

This is to certify that

met the specifications of Federal Reference Method 9 and qualified as a visible emissions evaluator. Maximum deviation on white and black smoke did not exceed 7.5% opacity and no single error exceeding 15% opacity was incurred during the certification test conducted by Eastern Technical Associates of Raleigh, North Carolina. This certificate is valid for six months from date of issue.

. .']28689 Certificate Number



### President 

## eIIknneajtoliJj eIIiinne:.wJ.Cl/ Location Date of Issue

# ~~~ W.

# ::I~/~**~U** Director of Training

# VISIBL E I SIONS T R

Th is is to certify th.at 

# O)fto

metthe specifications of Federal Reference Method 9 and qualified as a visible emissions evaluqtor. Maximum deviation on white and black smoke did not exceed 

# 7.5% opacity and no single error exceeding 15% opacity was incurred during the certification test conducted 

# by Eastern Technical Associates of Raleigh, North Carolina. This certificate is valid for six months from date of issue.

328686 eIlUnnea/wli3-j Jliinn€/J-ol'a' Certificate Number Location Date of Issue

# ~~~ to.

# f~/~
. 'ZJU Director of Training

. President

# AppendixH Process Operating Data

### OPERATING DATA SUMMARY FOR PROCESS SOURCES Test Date(s): 

### 5/2/2005 Company Name: 

### United Taconite 

### Equipment & Operating Data June-99 Process Equipment Number/ Identification: Line 1 Pellet Cooler Ex.

- SV047

I. Process Equipment Description: 

### Pellet cooling after induration- Line 1 2. Were the process and control equipment operated consistent with nonna! operating procedure? YES NO 

# I

.... y_e_s ___ -' 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months X 

# I Remains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

### ratios as appropriate)**--~--~----------------------------------------------------------------------** Process Parameter: list type and units Run I Run 2 Run 3 

### Greenballs out of drums, LTPH 

### 294 285 264 Greenball Feed Rate to the grate, L TPH 

### 265 264 239 Fired Pellet production Rate, L TPH 

### 231 230 208

Fuel Input (list units) Natural Gas MCF 

### 146 144 105 Heat Input (106 British thennal units/hour) 

### 146 144 105
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type ofscrubber): ,iP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: ,iP (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OF;nlet ,OFoutleJ and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoperating temperature) APC equipment and parameter monitored Run I Run 2 Run 3

NONE

List pollutant & averaging basis-should reflect permit Continuous Opacity Monitor (list hourly average) 

## NA

Abbreviations: Monitor (list averaging basis): Monitor (list averaging basis):
APC-air pollution control lbs.-pounds 

## NONE

Run I

gpm.-gallons per minute psig-pressure per square inch gauge 

## NONE NONE

Run 2 Run 3

in. w.c.-inches ofwater column ,iP- pressure drop NOTE: This forlll provides ollly a summary of the operatillg cOllditiolls durillg theperformallce test. Additional alld more detailed records are required to meet the requiremellts of Millll. R. 7017.2035. Tlzisform is to be submitted aspart of theperformallce test report to: North, Metro, or SOl/th District, Performallce Test Coordillator, MN Pol/I/tioll COlltrolAgellcy, 520 Lafayette Rd., St. Pal/I, MN 55155-4194.

### OPERATING DATA SUMMARY FOR PROCESS SOURCES Test Date(s): 

### 5/2/2005 Company Name: United Taconite Equipment 

### & Operating Data June-99 Process Equipment Number/ Identification: 

### Line 1 

### Waste Gas
- SV046



### 1. Process Equipment Description: Line 1 Kiln Gas Exhaust

- Wet Scrubber Control Device 2. Were the process and control equipment operated consistent with nonnal operating procedure? YES NO L-IY;...e;...s=--
__ -I 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months x IRemains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and ratios as appropriate)**--~--~----------------------------------------------------------------------** Process Parameter: list type and units Run 1 Run 2 Run 3 Greenballs out of drums, L TPH 

### 294 285 264 Greenball Feed Rate to the grate, L TPH 

### 265 264 239 Fired Pellet production Rate, L TPH 

### 231 230 208

Fuel Input (list units) Natural Gas MCF 

### 146 144 105 Heat Input (106 British thennal unitslhour) 

### 146 144 105
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type of scrubber):**~P** (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone:**~P** (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OFinlcl ,oFoUlle0 and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (0FoperJ.ting temperature) APC equipment and parameter monitored Run 1 Run 2 Run 3 Scrubber Pressure Drop, In.W.C. 

### 20.5 21 19.9 Scrubber Water Pressure, PSI 

### 72 

# - - Note: NaOH added to scrubber water during test on on on

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 Continuous Opacity Monitor (list hourly average) Monitor (list averaging basis): Monitor (list averaging basis):
Abbreviations: APC-air pollution control lbs.-pounds gpm.-gallons per minute psig-pressure per square inch gauge in. w.c.-inches ofwater column**~P-** pressure drop NOTE: This form provides ollly a summary of the operatillg cOllditiollS durillg theperformallce test. Additiollal alld more detailed records are required to meet the requiremellts of Mill II. R. 7017.2035. This form is to be submitted aspart of theperformance test report to: North, Metro, or Sout/z District, Performallce Test Coordillator, ]}fN Pollutioll COlltrolAgellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194.'<Oe{, , 5.0.'0 

### 0:> c,,G

### 0.~C:J\ f\ 

### 0"

# ~~ ,0"

# I>~**~** 1\.0

### ~ 

### '!:-.e{, :-- e'O f0'OC:J1 S0.{,

## ~**\.O~ ~**  \!}{,e S

### '?~**O~ ~**  " " . " \j;' 0.'0'0 

### t>c"**t>c~** C:Jc,{, 

### t>c"':-'"'\ / ';)'"59\/

## ~~0:> 0«0

## ~0« ,1

# ~**.~~ ~'O''"~.,.** **~~** r.f'<1



## . "" '"

# ~'O?**~~"'-** ,1'()'

# ~001> 0"''0

# ~o,~\1:' ,.

# O~'" )". /

# o,"~':: 0,7'

# .~,::**o,,"~O' ,;.,0.J>~\&** **~",~",0 ~"'-** **~'O<e'** "S'",

# 'V<y,~**o.~'"** ,-,,)'

# 'VO~'" / 

### N )"

# 0<~\e**~0'\0\' .,~,"?**  y,'i;J-" Lone 1 Wasle 

### '011' 

### <\\.."'- / "'- 

# ,,0'" #"'" 1><,,01> o,"?\/

# ~o,'~' 0"'\«-./ s"'\(;../ 

### 00'? 0 

### 0\0. eY 

### 0 «0. e \**'?~ ~~** **~'O\e; ~'O\e** **~'O\e;** 

### '?'?" / '?'?" / 0V.c,0 0V.c,0 0V.c,0 

### 5/2/2005

# 13'0~as PM lesl and Pell I 

### <'\.. /

# 0<e0~'O**,o"'~\· rrt<;'~v** **~** .,.'i;\'V/ 5/2/200513:15 292 71 e Cooler PM 5/2/05

# 'V~**~~,)!, ~"**  / 5/2/200513:30 291 71 43 264

# ~~ / 

### 229 229 229 230 -7.3 2260 2223 2274 2328 1833 1827 1819 1820 -27.6 -20.3 13562 13338 13646 13966 136 133 136 140 5/2/200513:45

# ~93 74 43 263 

### 91 69 43 264 Run 1 1400-1507



### 5/2/2005 14:00 295 5/2/2005 14:15 294 5/2/2005 14:30 292 5/2/2005 14:45 293 5/2/2005 15:00 297 5/2/200515:15 292 Averages 294 Run 2 1555-1704



### 5/2/2005 15:45 290 5/2/2005 16:00 297 5/2/200516:15 295 5/2/2005 16:30 278 5/2/2005 16:45 279 5/2/200517:00 274 Averages 285 Run 3 1750-1859



### 5/2/200518:00 261 5/2/200518:15 265 5/2/2005 18:30 263 5/2/2005 18:45 265 5/2/2005 19:00 263 Averages 264 

### 70 70 69 77 

### 69 76 72


### 70 67 70 39 68 65 63
67 68 69 70 71 69 42 42 41 47 41 47 44
43 40 42 42 43 40 42
43 43 44 45 45 44 267 266 263 263 269 264 265


### 263 270 267 281 254 248 264


### 237 241 238 240 238 239 

### 232 231 229 229 234 229 231


### 229 235 232 245 221 216 230


### 207 209 207 209 207 208 

### -7.3 -7.3 -7.2
-7.2 -7.1 -7.1 -7.1 -7.1 -6.9 -7.1
-7.0 -7.2 -7.1 -6.9 -6.8 -6.8 -7.0
-6.8 -6.9 -6.8 -6.9 -6.8 -6.8 2396 2469 2480 2448 2430 2394 2436
2431 2431 2431 2426 2360 2328 2401
1608 1691 1773 

### 1821 1841 1747 1814 1815 1835 1834 1836 1837 1828
1825 1836 1826 1836 1842 1838 1834
1807 1815 1814 1823 1822 1816 -27.6 -27.6 -27.6
-27.6 -27.6 -27.6 -27.6 -27.6 -27.6 -27.6
-27.6 -27.6 -27.6 -27.6 -27.6 -27.6

-28
-26.6 -26.7 -26.7 -26.7 -26.7 -26.7 -20.3 -20.3 -20.4
-20.4 -20.5 -20.5 -20.5 -20.5 -20.6 -20.5
-20.6 -20.4 -20.5 -20.7 -20.8 -20.8

-21
-19.9 -19.9 -19.9 -19.9 -19.9 -19.9 14374 14814 14879 14688 14578 14361 14616
14589 14589 14589 14557 14160 13968 14409
9646 10144 10641 10927 11048 10481 144 148 149 147 146 144 146
146 146 146 146 142 140 144
96 101 106 109 110 105".'

.. :' ...

" .. :.'.' 

# Gc-. s .. 

# s 10,-**~**

# /( l04Iey"'"

# ~r-ess u

# ~**f~~** 

# f- "

# §~**I£M:~** '"' f«-rf,**-v~** 

# Af- 

# J.. 100/,1>\

(3 or- 

# 3.5 hr fc.s+ )



# - ;)./00**J.~/.5 .~·30**  

# -**'~'I5** 

# --

'..

# 7~pSi**7~fJS** 

# (**)~51**

\. 

# \

,

### OPERATING DATA SUMMARY FOR PROCESS SOURCES Test Date(s): 5/3/2005 Company Name: 

### United Taconite 

### Equipment & Operating Data Process Equipment Number! Identification: Line 1 Pellet Cooler SV047 

### PM Test No.2

1. Process Equipment Description: 

### Pellet cooling after induration- Line 1 June-99

2. Were the process and control equipment operated consistent with normal operating procedure? YES NO 

# I

.... Y_e_s

___ ......I 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months X 

# I Remains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

### ratios as appropriate)**-~--~----------------------------------------------------------------------** Process Parameter: list type and units Run 1 Run 2 Run 3 

### Greenballs out of drums, L TPH 278 280 283 

### Greenball Feed Rate to the grate, LTPH 251 252 255 

### Fired Pellet production Rate, LTPH 219 219 222
Fuel Input (list units) Natural Gas MCF 124 131 123 Heat Input (106 British thermal units/hour) 124 131 123
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type ofscrubber):**~P** (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone:**~P** (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OFinlel ,oFoUIle0 and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoper.lting temperature) APC equipment and parameter monitored Run I Run 2 Run 3

NONE

List pollutant & averaging basis-should reflect permit Continuous Opacity Monitor (list hourly average) NA

Abbreviations: Monitor (list averaging basis): Monitor (list averaging basis):
APC-air pollution control lbs.-pounds NONE

Run 1

gpm.-gallons per minute psig-pressure per square inch gauge NONE NONE

Run 2 Run 3

in. w.c.-inches ofwater column**~P-** pressure drop NOTE: Thisform provides only a summary of the operating conditiol/s during theperformance test. Additional alld more detailed records are required to meet the requirements of MillII. R. 7017.2035. Thisform is to be submitted aspart of theperformallce test report to: North, Metro, or South District, Performance Test Coordinator, MNPollutiol/ COl/trolAgel/cy, 520 Lafayette Rd., St. Paul, MN 55155-4194.**~r:,\ o.~,.y.**  

# ,0' 0

### 0 ':\ 

# ,,'0°<1

# ~ \.0" 0'0:1'
...0:1> 

# ,,'00" 

# ,,0'" <t"

# _,~ 1 

## J3' .I> 

## &' -" "G 

# .,1- ?'_

# "'~ 0 ' °

# ~0 0,0'

# (,~"" ';'0'



## .

# ,,~\')> \

# ,~",o'l>.**,~",oO?~O"\~'O ~"'(O~O** **."'~** '"'" S >lS'0\ 

### 0"-

# ~~,,' e""",e 0

# ,~''2'. _,-.\ '}>

# ~,;:V / ,.,,\/ 

# .,0 G 

# \\e'" ,O",?·

## >J.'iy

# ~"'~**~** -<" W, ?O

# CP~ ",-4/ 

### N

# ~.. G'· 0?0 \ • 

# ,,'0· ," ?'- ,

# O~'" dl'\-\-/

# ~ (,0

# (,O~ /

# ~\~,0 0

# «,,0

# ~**~,;?** /

# .~\(,;? .-0:' \ b.'l-"\). v<..0\}:P' 

### Lin v

# ~\" / ,:. /

# 0~'O**\~,0** ",'i-"c"/.'. .,. e;? / 

# ,,0 5 

# Ru: ;

# ~:!~_~;~~'er PM 

# Test 2 513105

# ~, G,0

# (,~\O" ??'

# ;l' ??' 

# f""'/

# ,3<!-"'~<!-/**"'rs~'i-J·** ,eO?'? 0' 

# 0 ,,,e"

# (,~'"**,,~ >J.(,~**  51312005 8:30 

### ?? ??'/

# ,~o ,,\0,0 

# ,eO

# ~ 513120058:45 (,0 (,,,,0

# cP~O 276 280 

### 277 278 281 278 70 65 70 

### 71 70 69 42 40 42 44 43 42 249 254 249 251 254 216 221 -9.9 -10.0 2055 2070 2105 2070 1831 1818 1828 1842 -23.4 -23.4 -13.5 -13.4 12333 12418 12633 12418 12326 12426 123 124 126 124 123 124 5/3/20059:00 5/3/20059:15 5/3/2005 9:30

Averages Run 21018-1128



### 5/3/2005 

### 10:15 282 5/3/2005 

### 10:30 279 5/3/2005 

### 10:45 278 5/3/2005 

### 11 :00 281 5/3/2005 

### 11: 15 283 5/3/2005 

### 11 :30 282

Averages 280 Run 3 1225-1331



### 5/3/2005 

### 12:30 282 

### 5/3/2005 

### 12:45 282 

### 5/3/2005 

### 13:00 283 

### 5/3/200513:15 281 

### 5/3/2005 

### 13:30 287

Averages 283 

### 72 

### 71 65 69 74 67 69
68 68 68 67 70 68 45 44 38 41 43 38 41
41 40 40 39 41 40 251


### 255 252 251 254 251 253 252


### 255 254 255 253 257 255 

### 217 219 221 219


### 222 219 218 221 218 221 219
222 221 222 220 

### 224 222 

### -10.0 -9.9 -9.9 -9.9
-8.3 -7.5 -7.4 -7.3 -7.3 -7.3 -7.3
-7.0 

### -7.2 -7.1 -7.0 -7.2 

### -7.1 2054 2071
2054 2031 1905 2010 2358 2603 2181
2242 2138 1998 1939 1939 2051 1824 1829
1831 1843 1854 1782 1761 

### 1777 1803
1879 1855 1856 1835 1833 1852 -23.4 -23.4 -23.3 -23.4
-27.1 -28.1 -28.1 -28.1 -27.7 -27.6 -27.9
-27.6 -27.6 -27.6 -27.6 -27.6 -27.6 -13.5 -13.4 -13.4 -13.4
-18.8 -20.6 -20.8 -20.8 -20.5 -20.3 -20.6
-20.6 -20.4 -20.5 -20.6 -20.4 -20.5 12323 12185 11427 12058 14151 15618 13088
13449 12826 11990 11632 11632 12306 123 122 114 121 142 156 

### 131
134 128 120 116 116 123

### OPERATING DATA SUMMARY FOR PROCESS SOURCES
Test Date(s): 

### 5/3-4/2005**~~~~~~---------­** Company Name: 

### United Taconite 

### Equipment & 

### Operating Data Process Equipment Number/ Identification: Line 1 Pellet Cooler SV047 PM10 Test June-99



### 1. 

### Process Equipment Description: Pellet cooling after induration- Line 1 

### 2. Were the process and control equipment operated consistent with normal operating procedure? YES NO lL..y;..;e;:..:s::..-

__ -l 

### 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months X 

# I Remains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and ratios as appropriate)**--~--~----------------------------------------------------------------------** Process Parameter: list type and units 

### Run 1 Run 2 Run 3 Greenballs out of drums, LTPH 

### 279 274 282 Greenball Feed Rate to the grate, L TPH 

### 256 246 252 Fired Pellet production Rate, L TPH 

### 223 214 219
Fuel Input (list units) Natural Gas MCF 

### 116 166 156 Heat Input (106 

### British thermal unitslhour) 

### 116 166 156
6. Summmize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type of scrubber):**~P** (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone:**~P** (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OFinlel ,oFoUlleJ and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoperating temperature) APC equipment and parameter monitored 

### Run 1 Run 2 Run 3

NONE NONE NONE NONE

List pollutant & averaging basis-should reflect permit 

### Run 1 Run 2 Run 3 Continuous Opacity Monitor (list hourly average) Monitor (list averaging basis): Monitor (list averaging basis):
Abbreviations: APC-air pollution control lbs.-pounds gpm.-gallons per minute psig-pressure per square inch gauge in. w.c.-inches ofwater column**~P-** pressure drop NOTE: Tlzisform provides ollly a summary of the operatillg cOllditiollS durillg theperformallce test. Additiollal alld more detailed records are required to meet the requiremellts of Millll. R. 7017.2035. Thisform is to be submitted aspart of theperformallce test report to: North, Metro, or South District, Performallce Test Coordillator, MN Pollutioll COlltrolAgellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194.

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### 68 70 69 69 71 42 43 262 259 263 228 225 -7.1 -6.9 1993 1993 1993 2040 2011 1824 1830 1828 1824 -27.6 -27.6 -20.5 -20.7 11959 11959 11959 12240 12065 11420 11041 120 120 120 122 121 114 110 105 116 5/3/2005 

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### 17:45 275 5/3/2005 

### 18:00 272

. 274 Averages 279 PM10 Run 2 (1150.1310) 5/4/2005 

### 11 :45 276 5/4/2005 

### 12:00 269 5/4/2005 

### 12:15 276 5/4/2005 

### 12:30 266 5/4/2005 

### 12:45 268 5/4/2005 

### 13:00 279 5/4/200513:15 282 274 PM10 Run 3 (1350·1553) 5/4/2005 

### 13:45 282 5/4/2005 

### 14:00 284 5/4/200514:15 282 5/4/2005 

### 14:30 284 5/4/2005 

### 14:45 278 5/4/2005 

### 15:00 277 5/4/200515:15 282 5/4/200515:30 281 5/4/2005 

### 15:45 280 5/4/2005 

### 16:00 285 282 

### 72 71 45 67

71 71 72 74 72 73 75 73

75 76 75 74 73 71 73 70 68 69 72 

### 42 43 45 45 44 45 44

44 44 45 45 43 44 44 44

45 45 44 44 44 42 42 41 41 41 43 249 246 248 246 273 256



### 250 242 249 237 239 250 251 246



### 252 253 251 254 249 249 252 253 253 257 252 

### 229 216 214 216 214 238 223



### 217 211 217 206 208 218 219 214



### 219 220 219 221 217 216 220 220 220 223 219 

### -6.9 -6.9 -7.0 -7.1 -7.0 -6.9 -7.0

-7.2 -7.1 -7.1 -7.2 

### -7.6 -7.7 

### -7.6 -7.4

-7.4 -7.5 

### -7.5 -7.4 -7.3 -7.4 -7.6 -7.6 -7.5 -7.3 -7.4 1903 1840 1747 1940

2802 2802 2802 2802 2753 2686 2694 2763

2812 2891 2964 3059 2621 2552 2242 2250 2276 2276 2594 1847 1851 1845 1847 1837

1821 1829 1834 1829 1847 1843 1821 1832

1813 1811 1816 1805 1823 1835 1830 1817 1824 1828 1820 -27.6 -27.6 -27.6 -27.6 -27.6 -27.6 -28

-27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -28

-27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -28 -20.7 -20.7 -20.6 -20.5 -20.6 -20.7 -21

92.3 92.3 92.3 92.3 92.3 92.3 92.3 92

92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3 92 10484 11641

16812 16812 16812 16812 16515 16117 16165 16578

16871 17348 17783 18356 15727 15314 13455 13498 13654 13654 15566 168 168 168 168 165 161 162 166

169 173 178 184 157 153 135 135 137 137 156

### OPERATING DATA SUMMARY FOR PROCESS SOURCES
Test Date(s): 

### 5/3/2005 Company Name: 

### United Taconite 

### Equipment 

### & Operating Data June-99 Process Equipment Number! Identification: 

### Line 1 Waste Gas
- SV046 Fluorides and Gases



### 1. Process Equipment Description: Line 

### 1 Kiln Gas Exhaust
- Wet Scrubber Control Device 

### 2. Were the process and control equipment operated consistent with normal operating procedure? YES NO L-IY_e_s

___ -, 

### 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) ofJast maintenance/cleaning within 6 months x 

# I Remains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (Jist fuel type(s) and ratios as appropriate)**~~~-------------------------------------------------------------** Process Parameter: list type and units 

### Run 2 Run 3 Run 4 Greenballs out of drums, LTPH 

### 284 287 274 Greenball Feed Rate to the grate, L TPH 

### 254 261 259 Fired Pellet production Rate, L TPH 

### 221 227 226
Fuel Input (list units) Natural Gas MCF 117 120 108 Heat Input (106 

### British thermal unitslhour) 117 120 108
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type of scrubber): tlP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: tlP (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OFinlet ,oFoutleU and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoperating temperature) APC equipment and parameter monitored 

### Run 2 Run 3 Run 4 Scrubber Pressure Drop, In.W.C. 

### 20.4 20.5 20.6 Scrubber Water Pressure, PSI not collected not collected not collected 

### Note: NaOH added to scrubber water during test on on on

List pollutant & averaging basis-should reflect permit 

### Run 1 Run 2 Run 3 Continuous Opacity Monitor (Jist hourly average) Monitor (Jist averaging basis): Monitor (Jist averaging basis):
Abbreviations: APC-air pollution control lbs.-pounds gpm.-gallons per minute psig-pressure per square inch gauge in. w.c.-inches ofwater column tlP- pressure drop NOTE: This form provides ollly a summary of the operatillg cOllditiolls durillg theperformallce test. Additiollal alld more detailed records are required to meet the requirements of MimI. R. 7017.2035. This forl1l is to be submitted aspart of theperformallce test report to: North, Metro, 01' SOl/th District, Performallce Test Coordillator, MN Pol/utioll COlltrolAgellcy, 520 Lafayette Rd., St. Pal/I, ilfN 55155-4194.

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5/3/2005 12:00 281 G' 74 67 64 66 67 68 68 43 38 251 253 254 255 218 221 221 222 -7.3 2358 2603 2804 2898 2533 2242 2573 1761 1777 1789 1831 1922 1879 1826 -27.7 -20.5 14151 15618 16827 17386 15196 13449 15438 142 156 168 174 152 134 154 . 283 5/3/2005 12:15 5/3/2005 12:30 Averages Run 2 1345-1449 282 282 282
5/3/2005 13:45 284 5/3/2005 14:00 286 5/3/200514:15 283 5/3/200514:30 284 5/3/200514:45 285 Averages 284 Run 3 1545-1650

5/3/2005 15:45 286 5/3/2005 16:00 285 5/3/200516:15 289 5/3/2005 16:30 285 5/3/2005 16:45 290 Averages 287 Run 41730-1837

5/3/2005 17:30 275 5/3/200517:45 272 5/3/200518:00 274 5/3/2005 18: 15 273 5/3/2005 18:30 270 5/3/2005 18:45 278 Averages 274 71 71 72 72 73 72
66 66 68 70 69 68
72 71 45 29 67 69 59 37 38 39 41 39
41 41 41 42 42 41
41 42 42 43 42 42
45 44 45 44 44 45 44 254 255 254
253 255 253 254 254 254
261 260 262 259 263 261
248 246 273 288 247 254 259 221 222 221
220 222 220 221 221 221
227 226 228 225 229 227
216 214 238 251 215 221 226 -7.3 -7.2 -7.3 -7.1 -7.0 -7.2
-7.1 -7.2 -7.2 -7.3 -7.2 -7.2
-7.3 -7.1 -7.1 -6.9 -6.9 -7.1
-7.1 -7.0 -6.9 -6.9 -6.9 -7.0 -7.0 1906 1907 1953 1992 1992 1950
1993 1993 1993 1993 1993 1993
1903 1840 1747 1734 1767 1779 1795 1835 1823 1822 1830 1827 1827
1829 1827 1824 1830 1828 1828
1851 1845 1847 1828 1821 1837 1838 -27.6 -27.6 -27.6 -27.6 -27.6 -27.6
-27.6 -27.6 -27.6 -27.6 -27.6 -27.6
-27.6 -27.6 -27.6 -27.6 -27.6 -27.6
-27.6 -27.6 -27.6 -27.6 -27.6 -27.6 -27.6 -20.3 -20.4 -20.3 -20.5 -20.6 -20.4
-20.5 -20.4 -20.4 -20.3 -20.4 -20.4
-20.3 -20.5 -20.5 -20.7 -20.7 -20.5
-20.5 -20.6 -20.7 -20.7 -20.7 -20.6 -20.6 11436 11441 11716 11950 11950 11698
11959 11959 11959 11959 11959 11959
11420 11041 10484 10404 10602 10674 10771 114 114 117 119 119 117
120 120 120 120 120 120
114 110 105 104 106 107 108

### OPERATING DATA SUMMARY FOR PROCESS SOURCES Test Date(s): 5/4/2005 Company Name: 

### United Taconite Equipment 

### & Operating Data June-99 Process Equipment Number/ Identification: 

### Line 1 

### Waste Gas· SV046 Ontario Hydro Test

I. Process Equipment Description: 

### Line 1 

### Kiln Gas Exhaust
- Wet Scrubber Control Device 2. Were the process and control equipment operated consistent with normal operating procedure? YES NO 

### I'-y_e_s

___ -' 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months x 

# I Remains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and 

### ratios as appropriate)**--~--~----------------------------------------------------------------------** Process Parameter: list type and units Run I Run 2 Run 3 

### Greenballs out of drums, L TPH 276 266 274 

### Greenball Feed Rate to the grate, L TPH 247 238 241 

### Fired Pellet production Rate, LTPH 215 207 210
Fuel Input (list units) Natural Gas MCF 166 148 133 Heat Input (10 6 British thermal unitslhour) 166 148 133
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generalIy monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type ofscrubber): LlP (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: LlP (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OFinlet ,oFoUlleJ and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoperJling temperature) APC equipment and parameter monitored Run 1 Run 2 Run 3 

### Scrubber Pressure Drop, In.W.C. 20.4 20 21 Scrubber Water Pressure, PSI 

### 72 72 72 Note: NaOH added to scrubber water during test 

### on on on

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 Continuous Opacity Monitor (list hourly average) Monitor (list averaging basis): Monitor (list averaging basis):
Abbreviations: APC-air pollution control lbs.-pounds gpm.-gallons per minute psig-pressure per square inch gauge in. w.c.-inches ofwater column LlP- pressure drop NOTE: This form provides ollly a summary of the operatillg cOllditiolls during theperformance test. Additional alld more detailed records are reqllired to meet the requiremellts of MbllI. R. 7017.2035. Thisform is to be submitted aspart of thepeljormance test report to: North, Metro, or South District, Performallce Test Coordinator, MNPol/utioll COlltrolAgellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194.A'\'i>'1**o.~V"·** 

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Test 3 Run 11130-1341 5/4/2005 11 :30 276 5/4/2005 11 :45 276 5/4/2005 12:00 269 5/4/200512:15 276 5/4/2005 12:30 266 5/4/2005 12:45 268 5/4/2005 13:00 279 5/4/200513:15 282 5/4/2005 13:30 282 5/4/2005 13:45 282 Averages 276
5/4/2005 14:00 284 Test 3 Run 2 1410-1618

5/4/200514:15 282 5/4/2005 14:30 284 5/4/200514:45 278 5/4/2005 15:00 277 5/4/200515:15 282 5/4/200515:30 281 5/4/2005 15:45 280 5/4/2005 16:00 285 5/4/200516:15 147 Averages 266
5/4/200516:30 112 5/4/200516:45 209 5/4/200517:00 235 68 71 71 72 74 72 73 75 73 75 72
76
75 74 73 71 73 70 68 69 64 71
62 73 75 42 44 44 45 45 43 44 44 44 45 44
45
44 44 44 42 42 41 41 41 41 42
43 46 46 254 252
250 250 242 249 237 239 250 251 252 252 247
253
251 254 249 249 252 253 253 257 125 238
93 181 206 221 219
218 217 211 217 206 208 218 219 220 219 215
220
219 221 217 216 220 220 220 223 109 207
81 158 180 -7.8 -7.6
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2753 2802 2802 2802 2802 2753 2686 2694 2750 2812 2766
2891
2964 3059 2621 2552 2242 2250 2276 2276 1938 2464
1709 1902 1534 1816 1823
1825 1821 1829 1834 1829 1847 1843 1821 1819 1813 1828
1811
1816 1805 1823 1835 1830 1817 1824 1828 1843 1825
1898 1889 1833 -27.8 -27.6
-27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8
-27.8
-27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -27.8 -22.9 -27
-23.5 -26.0 -26.2 -20.0 -20.0
-20.4 -20.6 -20.7 -20.7 -20.7 -20.2 -20.1 -20.2 -20.3 -20.4 -20.4
-20.4
-20.4 -20.4 -20.5 -20.4 -20.2 -20.2 -20.3 -20.5 -17.8 -20
-18.3 -18.7 -19.4 92.3 92.3
92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3 92.3
92.3**~~ ~~** **~~ ~~** **~~ ~~** **~~ ~.3** **~B** 90
74.1 83.2 83.6 16226 16495
16516 16812 16812 16812 16812 16515 16117 16165 16503 16871 16594
17348
17783 18356 15727 15314 13455 13498 13654 13654 11627 14785
10255 11411 9202 162 165
165 168 168 168 168 165 161 162 165 169 166
173
178 184 157 153 135 135 137 137 116 148
103 114 92

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Test 3 Run 3 1805-2035 5/4/200518:00 274 5/4/200518:15 276 5/4/200518:30 273 5/4/200518:45 273 5/4/200519:00 274 5/4/200519:15 274 5/4/2005 19:30 273 5/4/2005 19:45 273 5/4/2005 20:00 272 5/4/200520:15 275 5/4/2005 20:30 280 Averages 274
5/4/2005 20:45 283 5/4/200521 :00 289 5/4/200521:15 287 5/4/2005 21 :30 288 5/4/2005 21 :45 284 5/4/2005 22:00 289 5/3/2005 19:45 285 5/3/2005 20:00 276 5/3/200520:15 266 5/3/2005 20:30 277 5/3/2005 20:45 287 5/3/200521:00 287 5/3/200521:15 286 5/3/2005 21 :30 286 5/3/2005 21 :45 285 5/3/2005 22:00 287 76 77 80 79 77 82 77 77 77 76 77 78
77 77 77 78 79 79 74 76 74 75 76 72 73 74 75 78 43
44 44 47 46 45 47 44 45 45 44 44 45
42 42 41 43 43 43 47 48 47 47 47 45 45 47 47 49 231 241 240
242 242 240 240 242 240 241 241 240 242 246 241
248 254 252 252 249 253 258 248 239 249 258 259 258 258 257 258 201 210 209
210 211 209 209 211 209 210 209 208 211 214 210
216 221 219 219 217 220 224 216 208 217 224 226 224 225 224 225 -7.4 -7.0 -7.1
-7.2 -7.2 -7.3 -7.4 -7.3 -7.3 -7.2 -7.4 -7.5 -7.6 -7.6 -7

-7.7 -7.6 -7.6 -7.6 -7.5 -7.4 -6.9 -6.9 -6.9 -6.9 -6.9 -6.9 -7.0 -7.0 -7.0 -7.0 1717 1957 2309
2307 2317 2383 2375 2327 2282 2229 2145 2088 1994 1948 2218
1948 1948 2006 2105 2152 2158 2342 2339 2225 2091 2010 1966 1998 2067 2093 2136 1833 1819 1826
1834 1818 1819 1838 1840 1842 1843 1846 1843 1849 1839 1837
1826 1825 1818 1806 1823 1827 1821 1839 1858 1855 1846 1835 1817 1817 1823 1822 -27.6 -27.7 -27.7
-27.9 -27.9 -27.9 -27.9 -27.9 -27.9 -27.9 -27.9 -27.9 -27.9 -27.9 -28**~~ ~~** **~.9 ~~** **~~ ~~** **~~ ~~** **~~ ~~** **~~ ~~** **~~ ~~** **~~ ~~**  -20.2 -20.7 -20.6
-20.7 -20.7 -20.6 -20.5 -20.6 -20.6 -20.7 -20.5 -20.4 -20.3 -20.3 -21
-20.2 -20.3 -20.3 -20.3 -20.4 -20.5 -20.7 -20.7 -20.7 -20.7 -20.7 -20.7 -20.6 -20.5 -20.6 -20.6 90.4 91.8 91.8
91.8 91.8 91.8 91.8 91.8 91.8 91.8 91.8 91.8 91.8 91.8 92
91.8 91.8 91.8 91.8 91.8 91.8 92.1 92.1 92.1 92.1 92.1 92.1 92.1 92.1 92.1 92.1 10300 11744 13857
13840 13901 14295 14248 13963 13693 13375 12873 12528 11964 11688 13306
11688 11688 12039 12633 12915 12950 14051 14033 13352 12548 12058 11798 11991 12399 12557 12816 103 117 139
138 139 143 142 140 137 134 129 125 120 117 133
117 117 120 126 129 129 141 140 134 125 121 118 120 124 126 128

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### 7,J7./- 2;;<- 7';1-. 7;;;- 7;;;l. 7::;L "7-;?- 

### 7;;;-- 

### 7,..?- 7.,;1 7::z.. 1:>- 

### 77- 

### ??- 7'?-- 

### 7:r 

## Contractor Checklist**.;~~~::'** ,. 

### MSHA Site Specific 

### -NAME.- , 

### Vehicle pass 

## # Certificate? Hazard Training?



# .

### OPERATING DATA SUMMARY FOR PROCESS SOURCES Test Date(s): 

### 5/5/2005 Company Name: United Taconite Equipment 

### & Operating Data June-99 Process Equipment Number! Identification: Dump Zone Scrubber- SV116

1. Process Equipment Description: Scrubber serving the Line 1 Pellet Cooler Discharge Zone- Line 1 2. Were the process and control equipment operated consistent with normal operating procedure? YES NO IL.Y;..-e:..;s:.-

__ ..J 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months x 

# I Remains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting (list fuel type(s) and ratios as appropriate)**~~~-------------------------------------------------------------** Process Parameter: list type and units Run I Run 2 Run 3 Greenballs out of drums, LTPH 

### 282 285 286 Greenball Feed Rate to the grate, LTPH 

### 256 258 254 Fired Pellet production Rate, LTPH 

### 223 224 221

Fuel Input (list units) 

## NA NA NA Heat Input (106 British thermal units/hour) 

## NA NA NA
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter) Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test plan approval letter. 

## • Scrubber (list type of scrubber): 6P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: 6P (in. w.c.) (gpm and psig) 

## • Catalytic Incinerator:(OFinlel ,OFoUlleU and Thermal • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoperJting temperature) APC equipment and parameter monitored Run 1 Run 2 Run 3 Scrubber water flow rate, GPM 

### 94.3 93.7 93.6 Scrubber pressure drop, in.We 

### 3.9 4.0 4.0

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 Continuous Opacity Monitor (list hourly average) Monitor (list averaging basis): Monitor (list averaging basis):
Abbreviations: APC-air pollution control lbs.-pounds gpm.-gaIIons per minute psig-pressure per square inch gauge in. w.c.-inches ofwater column 6P- pressure drop NOTE: This form provides ollly a slimmary of the operatillg cOllditiolls dllrillg tlteperformallce test. Additiollal alld more detailed records are required to meet the requiremellts of Millll. R. 7017.2035. This form is to be submitted aspart oftlteperformallce test rep011 to: North, Metro, or South District, Performallce Test Coordillator, MNPol/lltioll COlltrolAgellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194.

### SV116 Time dP GPM 1144 3.94 95.0 1203 3.91 94.0 1218 3.95 94.5 1234 3.96 93.5 1246 4.00 94.6 1300 3.91 94.0 Average R1 3.95 94.27
1431 3.99 93.4 1446 3.92 93.7 1500 3.97 94.6 1516 4.08 93.5 1531 3.95 93.3 Average R2 4.0 93.7
1616 3.98 92.8 1631 3.9 93 1646 4 94.7 1649 3.95 95.5 1716 3.98 91.7 1727 3.94 93.7 Average R3 4.0 93.6 1745 3.89 94.1 Readings Taken to coincide with SV045 Run 4 1800 3.92 92.1 Readings Taken to coincide with SV045 Run 4 1816 4.02 91.9 Readings Taken to coincide with SV045 Run 4 1830 3.96 91.2 Readings Taken to coincide with SV045 Run 4 1845 3.99 93.7 Readings Taken to coincide with SV045 Run 4 1900 3.94 93 Readings Taken to coincide with SV045 Run 4 Average R4 4.0 92.7

### ~~~\ ruO\

### ru~1**~ O~**  ru'O''V 0'"

### x~\**~'I.**0 1'(l'**~ee ~** G**~**

# ,0**~ ~**  0.... z,.c,e**~~e** 1

### "}~**«~ «~ ~z,.'l.e** **~~t(\ ~I'-S** 

### ~ ...,bo
.... • ,\,:,7-'0<0. 

### .......,7-0'0·**C;~c,~ ~\e'l.~** **~** ....

### '0~

### ...,'!j~ ..

### ~~\..**o;~\..** c:p'l.e

. eO

### ~e . \G.3 •

### G~0**~G<; ~).** **~-.l..** N ..., N ..., '1. 0

### ~\t**bo"~ \~e\** **<;~e\ «6\(\'1.~**  cP

### GO~"**GO~" ~z,.\\~** **~z,.'l.eo ~\.~..**  'l-.1>\e o 'l-.1>\e

## o \)1>\1> <ol'-\'\''' <;\\.'\.. <;\\.'\

..

### 6tee~ c,z,.\c,v 

# ««""**G~c,-S** G1>\c,-S Line 1 Cooler Discharge SV045 and SV116 Run 1 (1155-1259 SV116) (1155-1259,1329-1340 SV045) 5/5/2005 12:00 281 78 46 248 5/5/200512:15 279 78 46 248 5/5/2005 12:30 284 79 46 252 5/5/200512:45 285 76 45 253 5/5/2005 13:00 283 46 43 280 SV116 282 256 5/5/2005 13:30 284 23 42 303 5/5/200513:45 281 62 45 264 SV045 282 63 45 264

Run 2 1430-1545 5/5/200514:30 282 69 46 258 5/5/2005 14:45 285 72 46 259 5/5/2005 15:00 285 73 46 257 5/5/2005 15: 15 292 75 45 263 5/5/2005 15:30 283 74 46 256 5/5/2005 15:45 284 78 48 254 SV045 and SV116 285 73 46 258
Run 3 1610-1725 5/5/200516:15 286 81 51 257 5/5/2005 16:30 287 81 51 257 5/5/200516:45 286 83 52 255 5/5/200517:00 287 89 56 254 5/5/200517:15 285 95 59 249 SV116 286 86 54 254 5/5/200517:30 287 102 64 249 SV045 286 89 55 253 Run 4 SV045 only 5/5/2005 17:45 288 111 69 247 5/5/2005 18:00 283 116 71 237 5/5/2005 18: 15 289 120.6 71 240 5/5/2005 18:30 273 111.7 67 228 5/5/2005 18:45 245 107.8 69 206 5/5/2005 19:00 250 107.5 66 209 Average 271 112 69 228 216 215 219 220 244 223 264 230 230

225 225 224 229 223 221 224

223 223 222 221 217 221 216 220
215 206 209 198 179 182 198 2134 2074 2090 2090 2098 2097 2140 2140 2110

2140 2163 2190 2152 2213 2236 2182

2163 2137 2110 2087 2121 2124 2087 2118
2106 2138 2113.8 2143.6 2158.1 1933.5 2099 12805 12446 12541 12541 12586 12584 12841 12841 12657

12841 12976 13142 12911 13280 13414 13094

12976 12824 12659 12523 12724 12741 12524 12705
12635 12826 12683 12861 12948 11601 12593 128 124 125 125 126 126 128 128 127

128 130 131 129 133 134 131

130 128 127 125 127 127 125 127
126 128 127 129 129 116 126

### OPERATING DATA SUMMARY FOR PROCESS SOURCES June-99**-:-:--:-:----:-=-.;:,.5/;..;5:.;./~2.;:,.0.;:,.0.;:,.5----ss** Equipment Number/ Identification:

____ S=..V..:....::O;..;4.,::5
________ _ Company Name: United Taconite Test Date(s):


### Equipment & 

### Operating Data

1. Process Equipment Description: Scrubber serving Line 1 Vibrating feeder 2. Were the process and control equipment operated consistent with normal operating procedure? IYes 3. Include copy ofproduction records or instruments which indicates rate ofproduction or operation ofthe equipment, i.e. units per hour, pounds per hour, pressure, air flow, etc. 4. Date(s) and procedure(s) oflast maintenance/cleaning within 6 months I X IRemains unchanged from Test Plan

5. Process rate (amount ofraw material or finished product per hour, wet or dry basis) while combusting ratios as appropriate)**-~--~----------------------------------------------------------------** Process Parameter: list type and units Run 1 Run 2 Run 3 Greenballs out of drums, 

### L TPH 282 285 286 Greenball Feed Rate to the grate, 

### L TPH 264 258 253 Fired Pellet production Rate, 

### L TPH 230 224 220
Fuel Input (list units) 

## NA NA NA Heat Input (106 British thermal unitslhour) 

## NA NA NA
6. Summarize control equipment operating data documented during testing. Values reported should reflect maximum, minimum, averages, or as approved in the test plan. (See test plan and approval letter)
Examples ofAPC equipment and parameters generally monitored. Monitor as specified in the test 

## • Scrubber (list type ofscrubber): L'.P (in. w.c.) and feed rate • Baghouse, Cyclone, and Multi-clone: L'.P (in. w.c.) (gpm and psig) Run 4 271 228 198 

## NA NA



## • Catalytic Incinerator:(OFinlct ,oF**outle~** and Them1al • Number and identity ofoperating electrostatic precipitator field(s) Incinerator: (OFoperating temperature) APC equipment and parameter monitored Run 1 Run 2 Run 3 Run 4 Scrubber Pressure Drop, in 

## we 0.81 7.5 7.5 7.6 Scrubber Water Flow Rate, GPM 6.60 49.6 49.9 49.9

List pollutant & averaging basis-should reflect permit Run 1 Run 2 Run 3 Run 3 Continuous Opacity Monitor (list hourly average) 

## NA Monitor (list averaging basis): Monitor (list averaging basis):
Abbreviations: APC-air pollution control Ibs.-pounds gpm.-gallons per minute psig-pressure per square inch gauge in. w.c.-inches ofwater column L'.P- pressure drop NOTE: Thisform provides ollly a summary of the operatillg conditiolls durillg theperformalice test. Additiollal alld more detailed records are required to meet the requiremellts of Millll. R. 7017.2035. Thisform is to be submitted as part of theperformallce test report to: North, Metro, or Soutlt District, Performallce Test Coordinator, MNPollutioll COlltrol Agellcy, 520 Lafayette Rd., St. Paul, MN 55155-4194.

### SV045 Time dP GPM 

### 1143 0.80 6.6 1202 0.80 6.6 1217 0.8 6.6 1233 0.82 6.6 1245 0.81 6.6 1301 0.82 6.6 Average R1 0.81 6.60


### 1432 7.6 50 1445 7.5 49.5 1501 7.5 49 1515 7.5 49.5 1532 7.5 50 Average R2 7.5 49.6 

### 1615 7.5 50 1631 7.5 50 1646 7.6 49.5 1649 7.5 50 1716 7.5 50 1727 7.5 50 Average R3 7.5 49.9


### 1745 7.6 50 1800 7.6 50 1816 7.5 50 1830 7.6 50 1845 7.5 50 1900 7.6 49.5 Average R4 7.6 49.9

# :ts-;6~ 

# _-- .

} I 

# . , 

# #20 ?/aW if

# 5 

# v**~/**

# 4:. 5 Y 

## II**~** 

## ;1i

## ~51'"'

__ .6.. 

# e fliT**~~,** 

## (/ J,91**:;?~/<..<!** 

## I j/: 

## 7"S- {;l,CJ'If'1 /;(,o' 

## Ie, 

# I 3.94> r,,2 

## ',J.s /rJ! 

## ti7 .3,9/ 

## p,'S'tJ j,c}1 ,.;2; 

## 30 

## I J.1':2**;2:~7** 

## 3.1,7 

## o<.:S'7 3:/7 

### 3:.30 

## 3,98 f'/7 .- 

### :S,90

## 'f.~9 

# Ii? '/;y.> SO/ Sf(t/ 

## 93.1 

## CJId. I qt. ;;L



### I 

# rezPf- 

# V-<:'h-l.t) 

# 17

# 0~**~ .~**  

# s-/s-fos;;,. .

·f;. 

# :, UNITED.TACONITE·

.... FAIRLANE PELLET PLANT' 

## ;,KILN OPERATORS. 

## SHIFT REPORT



# r _r(;;{_ () rSHIFT:' ·ct..2. '3

()PERATOR'
.

CONCENTRATE'
.
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE'
GRATE FACTOR FIRED PELLET TONS" TONS TO PAN CONVEYOR GRATE OPERATING HOURS NU:'vlBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL:

#22X CONVEYOR PELLET BI:-.1 MEASUREMENT

PELLET TRAINS

INSPECT AREA FOR:

___ a) Spills and leaks 

### .L1NEL .'

# ·/~·l~~·.
#5-#4
RECLAIl'.IED
LIMESTONE

17),

__**2={J.!...>9:;;~** 20B)v"Ji

### b H 200) 

## 30CZ TOT)
____ _ (17

- TOT)

### ~7 

## //;)$'

GAS) 

### 900 

### 1'-:0=- OIL)
___ _ COAL)
___ _ HEATING GAS

2

REGULAR #5 SCALE (,

.



# .. {MCF} {GAL} {TON}

3 3

I have examined 

## my arell. #4 SCALE
STOCKPILED

BINDER

17A)

### /.f~3 (+)**~/q3** 18A) TOT) 

## L-/o5& (-) 

## 30'1 20D) 

### 37Lf7 (TOT

- 20D) 

# -;7 f' 3;;;60

GAS) OIL)
____ _ COAL)
__ 

### 4-,-0::......_

TIME TIME TIME) 

### c.;!.)

HOPPERS

__ --:-b) Cleor uccess to electrical disconnects

___ c) EmergenC)' I.i¥hting

__ -,-d) Guards on**conveyo~** Date--,-
__**~**__ Shift

______ -'-
__

___ e) Trip cables Name
_______ ----------- Cleur walbl,:;j)'s
.

__ --"g) Floor gr;jding, ha.nd rails.**~nd** toe bOJrds

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT REPORT
" SHIFT: 

# 2 ( 3)

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL:

#22X CONVEYOR PELLET BIN MEASUREtvlENT

PELLET TRAINS

INSPECT AREA FOR:

___ a) Spills and leaks 

### LINE 1 ;4, 

## J--

# 5 - #4 '\ (C", RECLAIMED
LIMESTONE

20B)

__ '_-'--

___ H L ! .,_/ 20D)

__ --'

__ _ TOT)
___ -'--_
(17" TOT)



# 87

, 

### ;)



### Cl '" , GAS) (1 

## y-! OIL)
____ _ COALl

___ _ HEATING GAS

2 2 B/L)
____ _
REGULAR #5 SCALE

{MCF! {GAL! (TON!

3 3 ENG)
____ _
HI SIDES

___ ,b) Cleur access to electric.1I disconnects

___ c) Emergency lighting I have examined my area. 

# '--' LINE 2 

## 1M -!.-'

#4 SCALE
STOCKPILED

BINDER

17A) (+) [8A)

__ ' _C'

__ "'_,'_ TOT)
____ _ H -, ) 20D)

__ 

### 1_,
__ _ (TOT" 20D)

/

GAS) 

### J

### i~' 

### '/ OILl

_____ _

TI!-.IE TIME TIME)
_____ _ HOPPERS

___ d) Guurds on conveyor Date'
________ Shift

__________ _

_____ e) Trip canies Name'
___________________________ ___

_____ 0 Clear wnlk\,,,'uys

___ -l!'!) Floor grading, iwnd rails, and to.! boards;:."

.
:."

,; ....

.... ;.,' .:"

....**~.** "..

:.**.~** 

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT REPORT DATE,
____

# ~C)~I~J~~/.)------------

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NU"lBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL:

#22X CONVEYOR PELLET BIN jv!EASUREMENT

PELLET TRAINS

INSPECT AREA FOR:

___ 01 Spills and leaks # 5 - #4
RECLAIMED
LIMESTONE 

# 'd**~)(/** 20B)

## ~S 

# '1**~6D)**

# __ '.=.3_(-.L(_(1-( _.-J,- 17)

### TOT)--,-/_C:-,--r~')_ 

# -) o((i r; " (17

- TOT)

.-., 

# -'**~/** GAS)-'-;'o--')!..,i!..../**_\L-'~f::A** OIL)
_____ _ COAL)
___ _ HEATING GAS
2 2 B/L) 

### ! ( / 

### Ii C
REGULAR SHIFT:

#5 SCALE

(MCFI (GALl (TONI

3 3

HI SIDES

___ b) Clear**ilcces~** to electrkal disconnects

___ c) Emergency lighting I have examined my area. 3

#4 SCALE
STOCKPILED

## '7/~**:"/0~**

BINDER

17A) 

# ? ;:;- 0 '::> (+) 18A) ;;;. 

## 7 7 (/ TOT) H 20D) 

# 3 C( " ( cj 

# 7'3 c.) (TOT

- 20D)


### / / :-::J :x" (/'**~-;/** "'7'\.. ,-'**(~)**

GAS) 

## A) '-ill' OIL) COAL) 

# 5-2-

TIME TIME TIME)
____**\-=~_',**1_'---_::'_-
HOPPERS

___ ,d) Guards on conveyor Date
_________ Shift

___________ _

___ ,e) Trip cables

____ 'f) Clear \\,.alkwilYs Name
_____________________________ _

___ ..og) Floor grading. hand rails. and toe boardsDATE

OPERATOR 

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT REPORT \,),'7,

### /'.LL,' (;/ ", /1,

### (~) /-"" 

### ! _ l-C

## U J UJ SHIFT: 

### (",1----) 

### LINE 1

I / ;;::j

### I/~::-j 2

FILTER CAKE PRODUCTION # 5· #4 

# j? SCALE , 

# 6( il 

### I 

## 1/1, U CONCENTRATE RECLAIMED FILTER ADDITIVES W.IESTONE BENTONITE GREEN BALL SCALES -"") "..., 17)_-=..£-'0'-:'" -::.:',,-,,':>'--...



# -. --; 20B) _---.c'l-'-',"-\,'-'-{

_ (-) 20D)

__ ",--,c.:/''-- ROLL FEEDER REJECT TOT)
____ _ GREEN BALLS TO GRATE ! 

### i/ (; (17
- TOT) GRATE FACTOR FIRED PELLET TONS
r Lr' !/[ij TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL: GAS) :/G :2 t-\(**1~** {MCF} OIL) {GAL} COAL) {TON} #22X CONVEYOR HEATING GAS PELLET BIN**~!EASUREtv!ENT**

### !~~; 

# .. J fe; :J r:,--**~**

### • ..:J 2 3 2 3**LlNE~** ).! 1_

.. 1 j/{,L.,i

STOCKPILED**'-i~','** 

### :'; ,':;'

BINDER

17A) _...:::::...:::...c,--_:..'l-_ (+) 18A)
__ "----'-"'-- TOT) (-) 20D) _---"""-.2..-'.:..._ (TOT· 20D)

GAS) !, ( I OIL)
____ _ COAL) _'::;.,'**,_::_~-_**

TIME PELLET TRAINS B/L) )(; 

# /s9 3 ENG) 

## L/I**(~)** 

## / :::..:J 1 I 0;**~~** 

### 1\, TIME)
____ I ,

INSPECT AREA FOR:

___a) Spills and leaks

___ b) Clear access to electricli disconnects

___ c) Emergency lighting

___ d) Guards on conveyor

___ e) Trip cables

____ 0 Cle:'Jr \valbvuys

___ -"g) Floor gmding, hund rails, and toe bourds ,: .•.. REGULAR HI SIDES HOPPERS

I have examined my area. Date'
______ Shift

_______ _ Name
______________ ___ I' ! i':.... ::.: .\.

.:' ; 

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT REPORT DATE 

## <;-- 

# 7 - {; (" SHIFf: 2

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUi\-lBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL:

#l1X CONVEYOR j'< <7' )

PELLET BIN MEASUREMENT

PELLET TRAINS

INSPECT AREA FOR:

___ -0) Spills and leaks 

### LINE 1 

# lk-::::;t<-.-

# 5**~** #4

LIMESTONE

20B) ---"'--'---'-
__ (-) 20D)**~-'-~**__**~-'j** / TOT)_-,-",--,,-,-'_ ([7

- TOT)



# 77

GAS) OIL) COAL) ./ 

### ,-I


## / (, ! 

# 7

HEATING GAS 

# )? 7 

### /0

l 2 B/L)
____ _
REGULAR ---7 I ! ' 

### ////

(MCFI (GALl (TONI



# - ( L

3 

## -, 'J .-:.-\.- 3 ENG)
HI SIDES

____ b,) Clear uccess to electrical disconnects

___ 'c) Emergency lighting I have examined my area, 3 

### LINE 2 

### --(

/. I,

......_-
'--;' #4 SCALE
STOCKPILED

BINDER

I 7A) -'-'---'--'--=-_ (+) lSA) _=----'-'-_ TOT)**-"'--~_-'--_**

## ~dD)**---,-=--L_/",~_--'_** ! ,**l~-** .' (TOT -10D) 

## iP7

GAS) i f 

## l 

## t:. 1// Co<- 0 OIL) COAL) ,) i(:**c.~**

-->

TIME 

### c-I, 

## Gr)

TIME TIME)
HOPPERS

___ d) Guards on conveyor Dnte
______ Shift

________ _

___ e) Trip cables

____ 0 Clear walkways Name
_______________ _

___ ..gg) Floor grading. hand mils. and toe boards**.:~** 

# .

.J;.

"." 

# UNITED TACONITE FAIRLANE PELLET PLANT KILN OPERATORS SHIFT REPORT

.z:;-I

### L{ DATE
___**~v~/~-------**

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS: 

## (>

PROCESS FUEL: # 5**~** #4
RECLAIMED 

### /-' -) <_) -;**c~** '-' -:\ / I LIMESTONE

17) ) <.. 

## JC) 0 / / 20B) _-,--,,:,(-'.-'
__ H "< 

## 1/' '? 20D)
__ ./---,--"...-"::-"_ TOT)

## ---'1----'"1'-.J'-~'_'

_ 

# f }_ (17

- TOT)



# 87 

# +r /0 

# 37

GAS) 

### I), 2.. (. OIL) COAL) SHIFT:

#5 SCALE



# c

{MCF} {GAL} {TON} #22X CONVEYOR HEATING GAS PELLET BIN MEASUREi\IENT

PELLET TRAINS 

# Cf) BIL) j /;

## /5:..q

REGULAR INSPECT AREA FOR:

____ a) Spills and leaks 2 

### Il 3 2 3 ENG) 

## 1./13 

# /39 HI SIDES f rlll

# Cv

___b) Clear access to electrical disconnects

____ c) Emergency lighting I have examined my area. 3 

### LINE 2 

### /j-- /lli/ilL..--' 

# ) 

# ; #4 SCALE
STOCKPILED

BINDER

17A) 

## )--6/0 (+) -J \

.. 

# 7**~** 18A) / f '-,I TOT) 

### 5'-(. 

## P 

## '7**~6D)** '7 

### it' 

# s

Lj 

## 7 '-Ie..

(TOT-20D) 

## t37

GAS) OIL) COAL) 

### j- 

# et

TIME 

### I 

### '-i ,) C! TIME; tJ 

### 3 

## STIt-.-lE) I I f..j 

## 5'

HOPPERS

___ d) GUilrds on conveyor Date'
______ Shift

_______ _

___ e) Trip cables Name
_______________ ___

____0 Clear walkwuys

___ -£!!) Floor grading, hand rails, and roe boards;.-' 

# UNITED TACONITE FAIRLANE PELLET PLANT KILN OPERATORS SHIFT REPORT

# D~E___ (;
__

# ~~~-~-_~~~~__ SHIFT:

OPERATOR ,.. ; FILTER CAKE PRODUCTION # 5**~** #.+ ( CONCENTRATE i RECLAINIED FILTER ADDITIVES LIMESTONE BENTONITE GREEN BALL SCALES 17),

_____ _ 20B)

____ _ H 20D)

____ _ ROLL FEEDER REJECT TOT)_...:.I-,C_,_)
__ GREEN BALLS TO GRATE (17
- TOT) GRATE FACTOR 

### )
FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTIKGS REPLACED DELAYS:

PROCESS FUEL: ). GASJ_-'-
__ _ {MCF} OIL)
____ _ {GAL} COAL)
___ _ {TON} #22X CONVEYOR HEATING GAS PELLET BIN MEASUREivlENT 2 3 2 3 PELLET TRAINS B/L) -,-/
__ 

## '_\_7 ENG) 

### 'i'
. ./ ; 

### . REGULAR HI SIDES INSPECT AREA FOR:

___ oj Spills "nd leoks 2

___ b) CIeJr access to electricul disconnects

____ 'c) Emergency lighling I have examined my area. 3

#.+ SCALE
STOCKPILED

BINDER
,--", 17A)

__ /:.......

__ _ (+) 18A)

___ ...:-_ TOT) ---''--_-'--_ (-) 20D)

__ ---'

__ (TOT- 200) -1 

## / (

GAS)
____ _ OILl

____ _ COAL)
___ _

TIME TIME TINIE) ....:..:..-'--
__ HOPPERS

___ d) Glmrds on conveyor Date
______ Shift

________ _

___ c) Trip cables Name
_______________ _

____ 0 Clear \vnlkv
..'nys

___ -Ecl Floor grueling, hand r.lils, and IOc boards ,.....

## --..... ,:!. :.,';

.. 

# UNITED TACONITE FAIRLANE PELLET PLANT KILN OPERATORS SHIFT REPORT



# 1 - DATE,

____**J_~~~**__________ __

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NU:VIBER OF CASTINGS REPLACED DELAYS: l..':

PROCESS FUEL: # 5 - #4
RECLAIMED
LI?-.IESTONE
17) ') i _0 20B)

________ __ H 20D) / TOT) )
(17

- TOT) 

## 7

GAS) :**~-** 

# -, I OIL1
___ _ COAL)
___ _ SHIFT:

#5 SCALE

!lvlCF) {GAL) {TON) #22X CONVEYOR HEATING GAS PELLET BIN MEASUREMENT

PELLET TRAINS

INSPECT AREA FOR:

___ a) Spills and leuks

______b) Clear access to electrical disconnects

___ c) Emergency lighting ) 

# --**-~ ~** 

B/L) / /. / 

## t),:::,

REGULAR 2 2 3 ENG) 

## loS .fLl{) HI SIDES

I have examined my area. 3


### ) ! #4 SCALE
STOCKPILED _l BINDER

17A) --'-'

__ --'-_ (+) [8A)

__ -"-

__ _ 

### C-i ---, TOT)
_____ _ (-) 20D)

____ ---'

__ _ 

### '-I /-/ (TOT- 20D)**-+~~** --'-----'---

GAS)
_____ _ OIL)
___ _ COAL) _---"'''----_

TIt-.lE C' )'."> 

### 1 TIME) t; 

### '-I**:~** 

### 'SHOPPERS

___ d) Guurds on conveyor Date
_______ Shift

__________ _

___ e) Trip cables

_____0 Clear \l,.'Jlbvays Name
_______________________ _

___ g) Floor grading, hand ruils, and toe boardsOPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS 

# UNITED TACONITE FAIRLANE PELLET PLANT KILN OPERATORS SHIFT REPORT

# 5
w #4
RECLAIMED 

### ( i..../// LIMESTONE

20B) _-=-';;;"'::"--_ (-) 200)**_~-'-'-L.-_** TOT)_--=2:..:/_C_'

_ ,?( :;,l/ (17
- TO'h SHIFT:

--/ I / I 

## (j)

#5 SCALE (

NU"IBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL: {MCFI OIL)
___ _ (GALl COAL)
___ _ {TON} #22X CONVEYOR HEATING GAS PELLET BIN MEASUREMENT 3 2 3 2

PELLET TRAINS B/L)
____ _ ENG)
____ _
REGULAR HI SIDES INSPECT AREA FOR:

___ ,oj Spills ond leaks

___ ,b) Clear access to electrical disconnects I haye examined my area. 3

STOCKPILED i:l7L /,) BINDER

I7A) (+) 18A)

__ -,--'--'./_ TOT) _--,-,,-"--"--_ (-) 200)**_~'--'-''-'-_**

GAS)_---"·,-'-, 

## _'-Lf_ OIL)
____ _ COAL)**~"1**

TIME TIME TIME)
____ _
HOPPERS

___ 'c) Emergency lighting

__ ----'d) Guards on conveyor

___ 0) Trip cables

____ 0 Cle>.lf walbvaY5 Date
______ Shift

_______ _ Name
______________ ___

____ g) Floor £nlding. hand mils. und tOl! bourds:-:.' 

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT**RE~ORT**

### DATE_~S-_-_·_)_- __ C

__

### .~ ____ __

OPERATOR FILTER CAKE PRODUCTION # 5 #4
,-)**J'~** 

### 15-'17 CONCENTRATE**RECLAI~IED** FILTER ADDITIVES 

# t7f-J)'9 LIMESTONE BENTONITE GREEN BALL SCALES (7)**~):})7** 20B) H 

### :2,[ i

# l. 20D) _/ -r ROLL FEEDER REJECT TOT)

### ~ol GREEN BALLS TO GRATE (17

- TOT) GRATE FACTOR 

# 1'7
FIRED PELLET TONS 

# r27/ TONS TO PAN CONVEYOR 

# o GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL: GAS) / (') 

### 0 

# 7 OIL)
____ _ COAL)
___ _ #22X CONVEYOR HEATING GAS PELLET BIN MEASUREMENT 2 2 PELLET TRAINS B/L) -'--':z.--'-
__ REGULAR INSPECT AREA FOR:

_____'n) Spills nnd lenks SHIFT:

#5 SCALE 

# to

(MCF} (GAL} (TON}

3 3 ENG)---'.<-!_!_(
__ -1 (.;, HI SIDES

____ b,) Clear access to electrical disconnects

_____ 'c) Emergency lighting I haye examined my area. #4 SCALE 

## ! STOCKPILED

BINDER



# ') u t

# ·/7 I7A) C' i ' (+)
. -,--;J 

# -70 I8A) 

### .:I
__

'_}

____ _ TOT) 

# 4- S )7 H2LJ)**20D)·f(~.,** (TOT· 20D)



# \--' '7

o
(' 

### 6

GAS) I**'~7** ()tl' OIL)**(.-~:** / COAL) ../ t:?

TIl<.IE



# --- C)L i. / Tli\-IE)

__ -L.

__ HOPPERS

____ d) Guards on conveyor Date
______ Shift

________ _

___ e) Trip cables Name
_______________ _

____ 0 Clear wulkways

___ ..gc) Floor grading, hand rails, und toe hoards.".,
. ·ii
. . ' ::'
.

.**;~-;:**: 

# :

.



### '


## ..... . OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS :.:; 

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT REPORT

LINE 1 

# 1/1---' [.' '
# 5**~** #4
RECLAIMED 

### 71)/).. LIMESTONE 

## /)/7 17),
____ _ 20B) _'--"

__ _ H 20D) --"'---'--'-

__ TOT)
__ J_,_'-,-'l

__
(17, TOT)

,**~i** SHIFT:

#5 SCALE

NUMBER OF CASTINGS REPLACED DELAYS: 

### D

PROCESS FUEL:

li22X CONVEYOR PELLET BIN MEASUREMENT

PELLET TRAINS

INSPECT AREA FOR:

____ 'il) Spills und leuks GAS) / 

### c '-i" 

# , ) OIL)
____ _ COAL)
___ _ HEATING GAS
2 2 B/L) 

# /b(0-(

REGULAR D

(MCF) (GAL) (TON)

3 3 ENG) 

# if()/

HI SIDES :2

___ b) Cle.lr access to electrical disconnects

___ 'c) Emergency lighting I have examined my area. 3

t..,; '\.; c.., ..-L #4 SCALE
STOCKPILED

BINDER

17A) -,-_'--,)--=."_ (+) 18A)**"'-::'~'-:""-L-_** TOT) ----'--'--
__ _ 

### H :20D) _'--'-'-
__ (TOT, lOD)

## ~7 ',1. 

### 1I_"'---'_--L_

GAS)_--,-I
__ _ OILl

____ _



## - --} COAL) I**TI~IE** TIME TIME)%;2 j'- 

## ':-';:3 \.-,.

HOPPERS .I

____ d) Guards on conveyor Date,
______ Shift

_______ _

___ e) Trip cubles

____ f) Cle:lr walkwuys Name
_______________ _

___**~!!)** Floor gntding, hund ruBs. ;lIld to\! board::;

### ,;, ,"'" DATE

OPERATOR 

# ;.'

UNITED TACONITE FAIRLANE PELLET PLANT KILN OPERATORS SHIFT REPORT 

# ) /) '\ ('5 /J



### /

!1d..L+ c;1 I 

## 'Q SHIFT: 

### U...? 2 

### U /

FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS: 

## ()

PROCESS FUEL:

#22X CONVEYOR PELLET BIN MEASUREtvlENT

PELLET TRAINS

INSPECT AREA FOR:

___ ,al Spills and leaks # 5 - #4
RECLAIMED**(~)<"1n** 

### 'i LHvlESTONE

17) 

## d / C( 

# ? 20B)

__**<;_-~,,-,)---,q_** 

## H 

## 3037 20D)

____ _ TOT)_LI_'e.- 

## f

_ C _)
_ (l7

- TOT)

I 

# (2 ")


# o

GAS) 

### 2 D (C,/ OIL) COAL) HEATING GAS



## --- 2
::: B/L)
REGULAR #5 SCALE



### ()

(MCF) (GAL) (TON) 

# r-. 3 3 ENG)
HI SIDES

___ ,b} Cleur access to electrical disconnects

___ ,e) Emergency lighting I have examined my area. 3 

### LINE 2 

# lift "))-' \ 7 #4 SCALE
STOCKPILED 

### c(!'? -) BINDER

17A) 

# J (( C L (+)**'~.** -5> 6 U 18A)

____ _ TOT) 

## '-I70L (-) -'2." 20D) --'--' 

### ij 

## :/,C-, :':, (TOT

- lOD) 

# ,,27 377<,- 

## I/O

GAS) !{t) 

## ? OIL)
____ _ COAL) ') C. 

### (0:,) () TIME TIME TIME)
___ _
HOPPERS

___ d) Guards on conveyor Date
______ Shift

_______ _

___ e) Trip cubles

____i) Clear walkv,:uys Name
________________ ___

___**~g)** Floor gmding, hand fnils, and toe boards..

. '.

..

..... .'**~** ' ..
; .. ,:.'

..


### ..

..

..
.. : 

# UNITED TACONITE FAIRLANE PELLET PLANT 

### KILN OPERATORS SHIFT REPORT**DATE.~(~~·_-~/~-** __ 

### C_··_)
____ _ SHIFT:

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS**NU~!BER** OF CASTINGS REPLACED DELAYS: 

# ..

PROCESS FUEL:

#22X CONVEYOR PELLET BIN MEASUREMENT

PELLET TRAINS

INSPECT AREA FOR:

___ in) Spills and leaks 

### LINE 1 

# ;) ,- !.\..

# 5**~** #4
RECLAIMED
LIMESTONE

20B)

### _-",Se:...-::::.:'_:'-.c..tf~

## ~6D)**~~,,-.~_,** U_/-'>s.:....-'_·
_

### TOT)---,-,;;2~O..::::{;_:_ (17

- TOT)

GAS) 

### /05(.., OIL)
____ _ COAL)
___ _**#~;SCALE** 

### .b

{t-.ICFI {GALl (TONI HEATING GAS
2 3 2 3 B/L) / ( 

## ! 

# 5" 3 ENG) 

## ell ( / '/"C) REGULAR HI SIDES

# 2~_'

v LINE 2 

# I-ID i' 

# ,1---
I #4 SCALE

STOCKPILED

BINDER
--) -) ',\\.;. 17A)**,.~** ::..' /)/> 

# iiA)**J-~:3t(O** TOT) H --:.'£...**J(~'** 20D)
___ ''_f_(5_,_
(TOT-20D)



## ,". -7 .:> /

GAS)_-,-i'_-'-..)_<_)

__ OIL)
__

### (~_A) __ COAL)



## oj; I

# r;

TIME TIME 

### C i/) TIME)? ) 0
HOPPERS

____ I b) Clear access to electrical disconnects I have examined my area. ..I**-'\~.** 

### ()f...(;-

___ 'c) Emergency lighting

____ d) GU<1rds on conveyor

___ 0) Trip cables

____ 0 Clear walbvuys Date
______ Shift

_______ _ Name.
________________________ _

___ -&!!) Floor grading. hand rails, and toe boards':r;,.. 

# UNITED TACONITE FAIRLANE PELLET PLANT 

## KILN OPERATORS SHIFT REPORT (. j 

### /1 r·- DATE,
____ -'_'

### -L!.!-+!....:..:./;_'_.
__ SHIFT:

OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TOi\S TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL:

#22X CONVEYOR PELLET BIN MEASUREMENT L-·

# 5**~** #4 RECLAII\IED
LIMESTONE
17) 20B) (-) 200) TOT) ..

(17
- TOT)I ! 

### / r- (

GAS),--,!_'-'----...:..-.-,')_ OIL)
____ _ COALl

___ _ HEATING GAS

2 2 

### ; I #5 SCALE

{MCF) {GAL) {TON)

3 3 2

PELLET TRAINS BfL)

____ _ ENG)
____ _
REGULAR HI SIDES INSPECT AREA FOR:

___ uJ Spills und leuks I ha\'e examined my area, 3

STOCKPILED
BINDER

L_ I7A)
____ _ (+) 18A)

___ ---'-_ TOT) _-'---_-----"_ 

### H**~,_** 20D)
__**~**__ (TOTc 200)

GAS)
____ _ OIL)
____ _ COAL) ---'-
__ _

TIME TIME TIME)
____ _
HOPPERS

___ b) Clear acceSs to electrical disconnects

___ c) Emergency lighting

___ d) GUHrds on conveyor Date
______ Shift

________ _

____ 'e) Trip cubles Name
_____________________ _

____ 0 Clear \I,!ulkv.ays

___ -"!!) Floor gwding. hand )"uils, and t('le boards

## UNITED TACONITE FAIRLANE PELLET PLANT KILN OPERATORS SHIFT REPORT DATE 

# oltur! J '

# 0-.5 SHIFT: 

# 0 2 3 

## U**~**
OPERATOR FILTER CAKE PRODUCTION
CONCENTRATE
FILTER ADDITIVES
BENTONITE GREEN BALL SCALES

ROLL FEEDER REJECT GREEN BALLS TO GRATE
GRATE FACTOR FIRED PELLET TONS TONS TO PAN CONVEYOR GRATE OPERATING HOURS NUMBER OF CASTINGS REPLACED DELAYS:

PROCESS FUEL:

#22X CONVEYOR PELLET BIN MEASUREMENT

PELLET TRAINS

## t!lJ~j-~j- fj; 

## )

INSPECT AREA FOR:

___ 0) Spills and leaks .I -::::;.) 

## IA/..-/

# 5**~** #4
RECLAIMED " 1 or> I LIMESTONE

17) 20B) (-) "d 200) _",,::,:,,_'_0:.. 11

_ TOT) (17

- TOT) 

# cCC!

()

GAS) OIL)
____ _ COAL)
___ _ HEATING GAS 

### AI-f 2 2 BIL) 

# Ifo**10~** REGULAR #5 SCALE

{MCF} {GAL} {TON}

3 3 ENG)_L-LI.:-! L-L/

__
HI SIDES #4 SCALE
STOCKPILED

17A) 

### 2 e;-L( 

### r:;!

## i~~-\) 9 

# 3 I V-> TOT) 

### H 200) 

## Lf15 

# C:' ( (**~'S-~** 

## L/ 

## s-"c C,," (TOT

- 200)

GAS)_---->'6"-..:

## -,-'~_\_7:..... OIL)
____ _

TIME**~::Je-** ,-,. TIME) 

### "J/q;;.**--{~-** 

### )'::-

HOPPERS

___ b) Clear uccess to electrical disconnects I have examined my area.

___ 'c) Emergency lighting

___ d) Guards on conveyor

___ eJ Trip cubles

____f) Clear \valbvays

___ -l'e:) Floor grilding. hand rails. nnd toe bourds Dat",
______ Shift

_______ _ Name:
__________**~**____ ---

# Appendix I Stack Test Plan

## Tom Kuchinski From: Sent: 

### Anderson, Bradley E. [BEAnderson@cci-united.com] Wednesday, June 22,200510:49 AM To: 

### 'Olson, Beckie' Cc: 

### Place, Andrew; Paul Taylor Subject: 

### RE: Stack test results
- delayed report to the MPCA Attachments: 

### aq-f2-chOO-050622.pdf; aq-f2-ch01-050622.pdf

aq-f2-chOO-050622 aq-f2-chOl-050622 .pdf (37 KS) .pdf (35 KS) 

### Beckie, Here are forms CH-OO and CH-01, which you requested. Brad. -----Original Message----- From: Olson, Beckie [mailto:Beckie.Olson@state.mn.us] Sent: Wednesday, June 22, 2005 6:48 AM To: Anderson, Bradley E. Cc: Place, Andrew Subject: RE: Stack test results

- delayed report to the MPCA
Thanks! you will also need to include the CH-OO and the CH-Ol Beckie Olson 651/297-8305 -----Original Message----- From: Anderson, Bradley E. [mailto:BEAnderson@cci-united.com] Sent: Tuesday, June 21, 2005 1:40 PM To: Olson, Beckie Cc: Beresford, Robert; Paul Taylor Ph. D. (E-mail); Pruchnofski George (E-mail); Roth, Todd D.; Mlinar, Michael P.; Tom Kuchinski (E-mail); 'place, Andrew' Subject: RE: Stack test results

- delayed report to the MPCA Beckie, As I disucssed over the telephone and in the preceding emails with Andy Place attached are five PDF files that should suffice as the administrative amendment needed to address the delay in reoprting our latest stack tests. I will also send this with an original signature via US mail. Thanks for your help. Sincerely, Bradley E. Anderson Section Manager

- Environmental -----Original Message----- From: Place, Andrew [mailto:Andrew.Place@state.mn.us] Sent: Tuesday, June 21, 2005 8:52 AM To: Anderson, Bradley E. Cc: Beresford, Robert Subject: RE: Stack test results

- delayed report to the MPCA Brad, I appreciate the heads-up on the situation. Since no discussion took place prior to now about extending the test report deadline, your permit requires you complete an administrative amendment to propose an extension request. In the future, if we discussed this matter during the pretest meeting or at least prior to the completion of testing, we could probably address 1

### the issue at that time. If you have any additional questions or concerns, please let me know. Thanks. Andy Place Performance Test Coordinator Minnesota Pollution Control Agency 520 Lafayette Road St. Paul, MN 55155-4194 (651) 296-7169 -----Original Message----- From: Anderson, Bradley E. [mailto:BEAnderson@cci-united.com] Sent: Monday, June 20, 2005 2:55 PM To: Place, Andrew Cc: Tom Kuchinski (E-mail) i 

### Beresford, Robert Subject: Stack test results

- delayed report to the MPCA Andy, The report for the latest stack testing conducted at United Taconite is due to the MPCA 45 days after the last test of the plan, which is June 20, 2005. Among the tests are metals analyses, which generally take extra time due to laboratory turn around. We neglected to take the extra lab time into account in the test plan, therefore we will not be able to submit the test report within 45 days of the last test. Additionally, preliminary results of the tests indicate that all of the stack tests were in compliance for emissions limits. We propose that we submit the test results by July 15, 2005. Thank you for your consideration. Sincerely, Bradley E. Anderson Section Manager

- Environmental
######################################################################## ####### This electronic message and any attachments included with this message are for the exclusive use of the individual or entity to which it is intended to be addressed. This message may contain information that is privileged or confidential and thereby exempt and protected from unauthorized disclosure under applicable law. If the reader of this message is not the intended recipient, or an employee or agent responsible for delivering the message to the intended recipient, be aware that any disclosure, dissemination, distribution or copying of this communication, or the use of its contents, is not authorized and is strictly prohibited. If you have received this communication and are not the intended recipient, please notify the sender immediately and permanently delete the original message from your e-mail system. ######################################################################## #######
############################################################################### This electronic message and any attachments included with this message are for the exclusive use of the individual or entity to which it is intended to be addressed. This message may contain information that is privileged or confidential and thereby exempt and protected from unauthorized disclosure under applicable law. If the reader of this message is not the intended recipient, or an employee or agent responsible for delivering the message to the intended recipient, be aware that any disclosure, dissemination, distribution or copying of this communication, or the use of its contents, is not authorized and is strictly prohibited. If you have received this communication and are not the intended recipient, please notify the sender immediately and permanently delete the original message from your e-mail 2

## Message



## Tom Kuchinski From: Sent: To: 

### Place, Andrew [Andrew.Place@state.mn.us] Friday, April 22, 200510:27 AM Anderson, Bradley E. Cc: 

### Beresford, Robert; Tom Kuchinski Subject: 

### Test Plan Approval 

## Page 1 of 1

Attachments: 

### MICROFICHE CD SUBMITTALS.doc; OPERATING DATA SUMMARY FOR COMBUSTION SOURCES.doc; OPERATING DATA SUMMARY FOR PROCESS SOURCES.doc; United Tac Approval, 5-05.doc; CERTIFICATION PAGE.doc
Brad The test plan approval forms associated with the upcoming performance test on SV046, SV047, SV045, and SV116 are attached to this message. They include the Test Plan Approval, Process Source Operating Data Summary, Combustion Source Operating Data Summary, Certification, and Microfiche/CD Submittal. Please use the forms attached as they have recently been updated. Also, please print a copy of this email message and include it in the report with the 

### approval letter. The email provides authentication for the test plan approval. If you have problems with any of the attachments feel free to contact me. Additional forms are provided at www.pca.state.mn.us/air/performancetest.html Sincerely, Andy Place 

### Performance Test Coordinator Minnesota Pollution Control Agency 520 Lafayette Road St. Paul, MN 55155-4194 (651) 296-7169



### 6/3012005

# ~ Minnesota Pollution Control Agency 

# Performance 

# Test Plan Approval
Minnesota Pollution Control Agency 520 Lafayette Rd. N. Saint Paul, MN 55155-4194(651) 296-6300 www.pca.state.mn.us


### Facility Name: United Taconite LLC Fairlane Plant Facility Contact: Brad Anderson, Environmental Section Manager Address: 8470 Townline Road (Hwy 16) Forbes, MN 55734 Fax: (218) 774-7647 Emission Unites): SV046, SV047, SVl16, and SV045 Scheduled For: May 2,2005, at your Facility located in Forbes, Minnesota. AQ#869A

Your test plan submitted on 

### April 13, 2005, and discussed on April 22, 2005, has been approved by the Minnesota Pollution Control Agency (MPCA) as follows: 

# D Shortened test notification approved 

### [g] Test plan approved without modification 

# D Test plan approved with the following provisions: SV045 and SVl16 emissions combine to serve EU039. SV045 serves the new portion of equipment for EU039. SV045 is subject to NSPS and will be tested according to 40 CFR § 60 subp. LL, while SVl16, along with SV046 and SV047, will be tested according to Minn. Rule. ASTM Method Ontario-Hydro will be used for Mercury, Antimony, Arsenic, Barium, Beryllium, Cadmium, Chromium, Cobalt, Copper, Lead, Maganese, Nickel, Phosphorus, Selenium, Silver, Thallium, and Zinc emissions. Equipment should be operated at maximum capacity during testing. Include process equipment and control equipment operating rates on the Operating Data Summary forms. Include in the final test report(s) the full reference method data record (strip chart and/or datalogger output) used to calculate emissions. The data record should include calibration values for any instrumental analyzers used for emissions compliance testing.

Attached Forms:



### [g] Operating Data Summary- Combustion Sources 

### [g] Operating Data Summary- Process Sources 

### [g] Certifications Form 

# D Operating Data Summary- Waste Combustors 

# D Operating Data Summary- Asphalt Plants 

### [g] Microfiche/CD-ROM Submittal Form Note: Forms are also available at: www.pca.state.mn.us/air/performancetest.html 

### Approved by: Date: 

### April 22, 2005

### Andrew Place Performance Test Coordinator Compliance and Enforcement Section Industrial Division Please contact me at (651) 296-7169 if

### you have any questions regarding this approval. Please be aware that enforcement action will be takenforpelformance test failures indicating emissions above applicable limits (excess actual emissions to the environment). Failures commonly result in assessment of a monetalYpenalty. Upon the first test failure, the Company should take immediate measures to minimize emissions. The measures taken should be documented, as they will becomepart of the record of corrective actions. Hard Copy Pelformance Test Reports and Microfiche or CD Copy submittals will be addressed to: Compliance Tracking Coordinator, Compliance alld Enforcement Unit, Industrial Division, Minnesota Pollution Control Agency, 520 Lafayette Road North, St. Paul, Minnesota 55155-4194
cc: 

### Bob Beresford, MPCA, Duluth Tom Kuchinski, Barr Engineering Co., Edina

### TEST PLAN FOR A TACONITE PROCESSING FACILITY

UNITED TACONITE LLC EVELETH, MINNESOTA
Date test plan created/revised: April 11, 2005 Scheduled test date(s): May 2-10,2005


### PART I. 

### GENERAL INFORl"VIATION

Name and address ofemission facility:

Facility contact person and telephone number:

MPCA AQD File Number: MPCA AQD Air Emission ID Number:

Reason the Emission Units are to be Tested: United Taconite LLC Fairlane Plant 8470 Townline Road (Hwy 16) Forbes, Minnesota
Brad Anderson (218) 744-7849 (218) 744-7647 (fax) email: beanderson@cci-united.com
101EV 13700113-004

Emissions testing will be performed at the Fairlane processing facility on the Line 1 pellet process as part ofthe post modification testing following the Emissions and Energy Reduction Project (EERP). This portion ofthe project will include testing the waste gas stack serving the Line 1 Pellet Induration (SV046) for criteria pollutants to quantify expected emission reductions from the EERP. Determinations will be made for particulate matter, NO x, 

### SOl, CO, VOC, fluorides, mercury and metals 1. 

### This stack must be in compliance with the Standards of Performance for Fossil-Fuel-Buming Direct Heating Equipment, Minn. R. 7011.0610 for particulate matter and sulfur dioxide. The Line 1 Pellet Cooler Exhaust (SV047) will be tested for particulate matter for demonstration ofcompliance with the industrial process equipment rule, Minn. R. 7011.0715, subpart 1(A) 

### and PM lO 

### for use in emissions inventory and permitting. In December of2004 a new vibrating feeder was installed on

Metals list includes: Antimony, Arsenic, Barium. Beryllium, Cadmium, Chromium, Cobalt, Copper, Lead, Manganese, Nickel, Phosphorus, Selenium, Silver, Thallium and Zinc. Metals will be determined by analysis of front halfcatch (dry) and reagent from irnpingers 1-3 from the mercury sample train. 

### 1

### Line 1 pellet discharge, this change requires the source to be tested under NSPS rules v.rithin 180 days of completion. Particulate emissions ofthe vibrating feeder, emissions unit 039, are controlled by 

### CE055/SV045. Particulate emissions from the dump zone, also emissions unit 039, are controlled with 

### CE065/SV116 (new scrubber). Emission of SV045 and SV116 will be combined to demonstrate compliance with the industrial process equipment rule, Minn. R. 7011.0710, subpart 1 (A) ofEU039. Opacity determined by EPA Method 9 will be performed once for each ofthe aforementioned sources during emissions testing. Diagrams ofeach sampling location giving all relevant dimensions are attached. Testing Company and Contact: Barr Engineering Company Tom Kuchinski (952) 832-2727 (952) 832-2996 (fax) email: tkuchinski@barr.com



## 2

### PART II. TESTING REQUIREMENTS
The table below gives a summary ofthe pollutants to be tested and test methods.

StackIVent #: Limitation Basis Pollutant Tested and Specific Source Description ofPollutant Applicable Emission Limit MethodslProcedures Tested Required Citation SV046 Minn. R Criteria Pollutants: 40 CFR Part 60, 7011.0710, subp. PM, NO x, 

### S02, CO, Appendix A Line 1 Pellet 1(A) Induration-Waste VOC, F, Metals (EPA EPA Methods 1-5, 6C, 7E, Gas Exhaust Stack S02- Minn. R. Method-29 list) & 

### Hg 9, 10, 13B,25A, 202 7011.0610, subp. 2(B) PM Limit

- 42.6 Ih/hr ASTM Method D6784-02 (Ontario-Hydro) with PM emissions shall comply reagent solution from impingers 1-3 analyzed for with the less stringent limit EPA Method 29 metals ofMinn. R. 7011.0730 or 7011.0735, and regardless

ofthe limit allowed by 7011.0730, PM emissions shall not exceed 0.3 grains/dry standard cubic foot (gr/dscf). Opacity not to exceed 20 percent except

for one six-minute period per hour ofnot more than 60 percent as specified in

Minn. R. 7011.0710, subpart l(B).



## 3

### Stack/Vent #: Limitation Basis Pollutant Tested and Specific Source Description ofPollutant Applicable Emission Limit MethodslProcedures Tested Required Citation SV047 Minn. R 

### PM andPM JO 

### 40 CFR Part 60, 7011.0710, subp. Appendix A Line 1 Pellet Cooler 1CA) PM emissions shall comply with the less stringent limit EPA Methods 1-5,202 Minn. R. 

### ofMinn. R. 

### 7011.0730 or EPA Method 20lA, 202 7011.0710 subp. 7011.0735, and regardless EPA Method 9 l(B) ofthe limit allowed by 7011.0730, PM emissions shall not exceed 0.3 Minn. R. 

### grains/dry standard cubic 7017.2020, subp. foot (gr/dscf). Opacity not 1 to exceed 20 percent except for one six-minute period per hour ofnot more than 60 percent as specified in

Minn. R. 7011.0710, subpart I(B). 

### PM limit 

## = -41Ib/hr PM SV116 Minn. R PM emissions shall comply 40 CFR Part 60, 7011.0715, subp. with the less stringent limit Appendix A Line 1 Kiln Cooler 1(A) ofMinn. R. 7011.0730 or Discharge Scrubber 7011.0735, and regardless EPA Methods 1-5,202 ofthe limit allowed by (New) 7011.0730, PM emissions EPA Method 9 shall not exceed 0.3 grains/dry standard cubic foot (gr/dscf). Opacity not to exceed 20

percent as specified in Minn. R. 7011.0715, subpart 1(B)
Vendor Guarantee is 0.008 gr/dscf 

### PM Limit 

## = -41Ib/hr combined with SV045



## 4

### StackIVent 

### #: Limitation Basis Pollutant Tested and Specific Source Description ofPollutant Applicable Emission Limit MethodslProcedures Tested Required Citation SV045 Minn. R PM 

### 40 CFR Part 60, 7011.0715, subp. PM emissions shall comply Appendix A Line 1 Kiln cooler l(A) with the less stringent limit Discharge Scrubber ofMinn. R. 7011.0730 or EPA Methods 1-5,202 (Existing) 7011.0735, and PM EPA Method 9 emissions shall not exceed 0.022 grains/dry standard (3 I-hour runs) cubic foot (gr/dscf) per 40 CFR Part 60, Subpart LL 

### for NSPS. Opacity not to exceed 20 percent except for one sixminute period per hour of not more than 60 percent as specified in Minn. R. 7011.0710, subpart l(B)

Similar to the pre-EERP testing, the Pellet Cooler exhaust stack (SV047) will be tested while the Cooler Discharge dump zone emissions are being controlled with CE065

- SVl16 only. Pending successful testing on SV047, CE055

- SV045 will be permanently disconnected from the Cooler Dump zone (part ofEU039). Since CE065 and CE055 serve the same emission unit (EU039), the emissions measured at SV045 and SV116 will be added together to demonstrate compliance with the Industrial Process Equipment Rule. In addition, the emissions from CE055

- SV045 must comply with 40 CFR Part 60, Subpart LL 

### NSPS as it applies to the new source.
PART III. OPERATING CONDITIONS


### The table below includes a summary ofthe industrial processes and related control equipment.

Process Equipment Description for Units to be tested:
SV046 EU040 Line 1 Pellet Induration SV047 EU04l Line 1 Pellet Cooler Exhaust: pellet cooling after induration SV1l6 EU039 Line 1 Kiln Cooler Discharge Dump Zone (new scrubber) SV045 EU039 Line 1 Kiln Cooler discharge Vibrating Feeders (existing scrubber) SV045 EUI13 Line 1 Pellet Conveyor Transfer SV045 EU1l4 Line 1 Pellet Conveyor Transfer



## 5

### Process Operating Parameter Monitoring During Performance Test: SV046, SV047, SV116, SV045

- Line 1 operations will be monitored by: Greenball feedrate (produced), Normal Range 250 LTPH Fired Pellet Production, Normal Range 204 LTPH Fuel Consumption

- Line 1 will be flring on natural gas only A sulfur mass balance will be performed by collecting process samples ofgreenball feed and flred pellet and analyzing for sulfur content. The data will be used with the measured stack emissions to determine a sulfur removal efficiency ofthe scrubber.
Control Equipment Description: SV046

- CE056 Ducon Wet Scrubber type VV-O, Size 222 SV047

- No control device serves the pellet cooler exhaust SV116

- CE065 Ducon Wet dynamic Scrubber UW-4 Model IV Size 120 SV045

- CE055 Ducon Wet Scrubber Control Equipment Operating Parameter During Test: SV046

- CE056 Gas stream pressure drop across scrubber and water pressure rates at 15 minute intervals SV047

- None SV116

- CE065 Gas stream pressure drop across scrubber and water flow rates at 15 minute intervals SV045

- CE055 Gas stream pressure drop across scrubber and water flow rates at 15 minute intervals

PART IV. TEST METHODS
1. The following is a description ofthe test methods, number oftest runs, length oftest runs, and sampling rate for each pollutant A. EPA Method 1 for the location of sampling ports and points. One determination per test location. A determination ofcyclonic flow 

### will be made at each source and results included in the test report.
B. EPA Method 2 for stack gas velocity and volumetric flow rate. One determination per EPA Method 5 test run.
C. 

### EPA Method 3 or 3A to determine stack gas molecular weight at the waste gas stack. Ambient concentrations ofoxygen and carbon dioxide are expected for the non-combustion sources and will be assumed for the calculation of stack gas molecular weight. SV046 is only source expected to have subambient levels ofoxygen.


## 6 ,

### D. EPA Method 4 for determination ofmoisture content in stack gas. One determination per EPA Method 5 test run.
E. EPA Method 5 for the determination ofparticulate emissions from stationary sources. Three 6O-minute test runs. A minimum of 32 dry standard cubic feet will be obtained for each sample with the exception of SV045 which requires a minimum sample volume of 60 dry standard cubic feet per NSPS regulations.

F. EPA Method 202 for the determination ofcondensible particulate. Performed in conjunction with EPA Method 5.
G. EPA method 201A for determination ofparticulate matter < 10 microns to be performed at the pellet cooler exhaust. 

### It is expected that isokinetic sampling (80 percent<I<120 percent) as required by the method may not be achievable due to the conditions ofthe stack (hot gases with low velocity). During previous tests on Line 2 Pellet Cooler for PM 10 

### the tester was able to maintain the cut point between the required 9.0 to 11.0 microns.

H. EPA Method 6C for the detemrination of sulfur dioxide emissions. Three 60 minute runs in conjunction with EPA Method 5.
I. 

### EPA Method 7E for the determination of oxides ofnitrogen emissions. Three 60 minute runs in conjunction with EPA Method 5.



### J. EPA Method 9 will be used to determine the visible emissions. A single one-hour test will be made on all
sources except SV045 will be tested for 3 one-hour periods as required by NSPS.

K. EPA Method 10 for the determination ofcarbon monoxide emissions. Three 60 minute runs in conjunction with EPA Method 5

L. EPA Method 25A for the determination ofVOC emissions. Instrument will be calibrated using either propane or methane calibration standards in air, the results will be reported as propane. Three 60 minute
runs in conjunction with EPA Method 5.

M. EPA Method l3B for the determination offluoride emissions. Three 60 minute test runs
N. ASTM Method Ontario-Hydro for the determination ofmercury emissions and analysis ofreagent solution from irnpingers one through three for the determination ofAntimony, Arsenic, Barium, Beryllium,


## 7

### Cadmium, Chromium, Cobalt, Copper, Lead, Manganese, Nickel, Phosphorus, Selenium, Silver, Thallium and Zinc. Three 120 minute test runs.


### PARTV.CEMS
There are no CEMS located at the emission points to be tested.



### PART VI. OTHER
The particulate, mercury and metal emission measurements will be reported in units oflblhr, and lbllong ton process feed (i.e. greenball, fired pellet production or ore feed rates). Particulate emission measurements will also be reported in units ofgr/dscf. EPA Method 51202 

### results will be reported as fllterable, fllterable plus organic condensibles, and total including filterable, organic condensibles and aqueous phase condensibles. Filterable plus organic condensibles emission rates and concentrations are used to compare to MN. Rules. The total particulate number representing filterable, organic condensibles and aqueous condensibles is used to represent PM lO 

### emissions at the waste gas scrubber stack and kiln cooler discharge stack(s) since Method 201A typically cannot be performed
on sources with wet scrubbing devices which create a moisture saturated gas stream. Composite greenballs, fired pellets will be analyzed for sulfur content to be used in the mass balance study. 

### Testing Schedule: WeekI

Sunday Monday Tuesday Wednesday Thursday Friday Saturday 5/1/05 5/2/05 5/3/05 5/4/05 5/5/05 5/6/05 5/7/05
Setup Test Test both Line I Test Line I Pellet Test Line I Waste Setup Test Equipment Pellet Cooler Cooler Stack Gas Stack Equipment (II00-1800) (SV047) (SV047) (SV 046) Line I Cooler and PM IO Mercury and Discharge Scrubber Waste Gas Stack (0800-1500) Metals Stacks (SV046) (0800-1600) (SV045 and PM and Opacity Test Line I Waste SV116)

(0800-1500) Gas Stack (SV 046) Fluorides, NOx, SOl, CO and VOC (0800-1500) 

### 8

### Testing Schedule Continued: Week 2

Sunday Monday Tuesday Wednesday Thursday Friday Saturday 5/8/05 5/9/05 511 0/05 511 1105 5/12105 5113/05 5114/05

Test Test Line 1 Cooler Discharge Line 1 Cooler Discharge Scrubber Stack Scrubber Stack (SV045) (SVI16) PM and Opacity PM and Opacity

(0800-1500) (0800-1500)
Relocate Test Equipment Demobilize Test Equipment (1500-1700) (1500-1700)



### Last Maintenance Performed. Line 1 was restarted November 29,2004 after being shut down since June of 1999. The line was in operation until February 2005 when it was shut down for modifications related to the Emissions and Energy Reduction Project. Line 1 was restarted April 3, 2005. The vibrating feeder replacement on Line 1 pellet discharge was completed in December of2004. A list ofrepairs or maintenance activity, for the sources listed, performed 30 days prior to the testing will be provided in the stack test report.


### Test Report: One complete test report (one hard copy) will be post marked on or before 45 days from the last performance test date. A CD-ROM copy ofthe report in PDF format will be submitted within 105 days ofthe test last performance date.
Submittal Address: Andy Place Performance Test Coordinator Minnesota Pollution Control Agency 520 Lafayette Road St. Paul, Minnesota 55155-4194


## 9

### Phone: (651) 296-7169 Email: andrew.place@pca.state.mn.us



### 10

# AppendixJ Project Participants

### Minnesota Pollution Control Agency Andy Place- Performance Test Coordinator Robert Beresford

- MPCA Duluth Area Office
United Taconite Company Brad Anderson

- Section Manager, Environmental

Barr Engineering Company Tim Russell- Vice President / Chemical Engineer George Pruchnofski

- Vice President R. 

### Paul Taylor

- Ph.D. Tom Kuchinski

- Project Manager Dan Koschak

- Team Leader Bill Scott

- Stack Test Technician Jason McCann

- Stack Test Technician 

# Project Participants