## Sa m p l e A n a . l ys is R e p or t Sample Na me : AF7336 Da la Fi l e N a me : C:\PE A KNE'N> A TA\AN IO NS\DX - 1 00\Anloos..,AAH 0 86. D XD 

### Low Range DeleetOr: U120 Universal Interface 

### Oilibralion Date : 2008/08/"20 4:33 : 03 

### PM 

### Mel!lod File Name : c:lpeaknetlmet h

od\300anions . met · Schedu l e File . !'lame: .. . \anlons0820 : sch 

### D ate T"uoe Collected : 2008/081"21 l 2:40:59 

### PM Systeui Operator : Ll.B**Caijbf;o~oo** 

### T ype : EXTERNAL ' . Colllp!>nent Amou rtt l.Jnits : mgiL Di l ution Factor : 10.00 

### P

eak li:lfonnation : All Components P <t k # Co mpo oe il t Co mpo oenl 

### Nam e Numb e r I 2 

### 2 3 4 

### 3 

# s

10.0 8.0 6.0

### ~ 4.0 

### ' 2.0 0 0 

# Iii : PtaltNtl S.l Chl oride Nitrit e (as N ) Bromide Nitra te (as N )

# ~ I 

# I 1.0 2.0 3 

### I 

# I 3.0 

## _ \ l Co mponen t P ea k Retenti o n . P ea k Area P ea k H <igbt 

### Ani oun t**~g/L) Tim** **e** 50 . 6025 1.2082 . 34 . 1440

AP 7336

. 4. 0 5.0 

### 1. 67 1.95 . 3.15



### 6 . 0 7 . 0 21 4 344325 

### 4 18 8 9741 96o2441! .**178~163** 365291148 

### 44876688

8 . 0.



### co- Dole: 200Mle/21

CumM Time : 12::49:09



### V E S 0 056 0 1

### Sam ple A nal ysis Report Samp t ; 

# Name : AF7337 . futa 

### Fil e 

### NlUJie: C :\PEAKNE'N>ATA\ANIONS\DX- 100\Anlons..A 

### YSOll.DXD Low 

### R•nge Detector : UI20 Universal Interface



### · Method FUe · Name:**e:~ons.met** Schedule File N . ame: .. . \aoions082l.sch . ·**D~** TiJ)>C Cotl et:tcd : 2008/0812 1 2:52:49 PM**SY,~tem** Operat'Qr : 

## Ll.E . Calibration Date: 2008108120 4: 33:03 PM Calibration Type : 

### EXlERNAL Component Am oont Units : mg/L Di lution Factor: 10.00 Peak Infonnatio n :AU 

### Components Peat # 

### Component . . C"!" pooent Name Number 

### Co mponent P ea k Retenli9n Peak Area Peak Helgb t

V) 2

3 4

"- 2 3 

# s 6

. 10 . 0

8 . 0 6.0 4.0 2.0



### 0 0 

# II : PcatNu S.2 

# I Cblori<le Nitrite (as N) Nitrate (as N) Pbosph ate -ortho

2 I 

# l J 

# u! 1 I 1. 0 2.0 4



### . I



# . I 

# ! 3.0 Amount (mg(L ) Time · 50.0565 

## 1.1944 37.2584

AF7337

4,0

Pate I o rl 

### 5.0 1.64 1.94 3.13

6 . 0 7.0 211804262 9481706**~4786**

8.0**416212~** 1 656626 ' 49735778

CuneM D .f tc : l008J08121 Curr<* Time : I S:QO::S2 .


### VES 005602

### Sampl e Analy sis R e p o r t · Samp l e Name : AF7 338 D ata FOe N am e: C:\l' E AKNE1\DA T A \ANIO NS\DX·l 00 \AD!ons...A XW012.DXD 

### lAW Range Detector: 

### Ul20 Universal Inlelface Mt t h od FUe Name : c:\peaknel\melbod\3008nions.met · Sca.idol e 

### File N a me: ... laniondl821.sch 

### Dere Time Collected: 2008/08/ZI 3:01:48 P M Sysrem Operator : U..E ' Calibntion 

### Dare : 2008Al8120 4:33:03 

### PM Calibral'ion Type :EXTERNAL · 

### Component Amount Units : mg/L Dilution Factor : 10.00 

### Pea k Information : All Co!nponents P

eak # 

### C omp o n e n t Gompo n en t Name · C oniponent P ea k R e ten tion P eak A rea P eak Hei ght . · N u mbe r · Am ount (m g/L)Time .



### :

<I) 

### 2 3 4

"- 

### 2 

### 3 5

10.0 8.0 6.0 4.0 2 . 0

0 0 

# II**:P~et.S.l Chlori~**  

### N'rtrire (as N) . 

### Nitrate (as N)

2 I 

# l i , 1 i I 

# I I 1.0 2 . 0 4 

### I 

# I 

# I 3.0 #.3538 

### 0 .8511) 29:5624

AF7JJ8

4.0



### Poio I of I 5.0 

### 1-«>:i 1.93 

### 3.12.

6.0 7 .0 194726450 6473045 

### 311781731 .

8.0 

### 38027390 1132809 • . 386517 i I

Glnent Di.e: 2003108121

C'tirrtllt Time : I S:09:S2



### VES 

### 005603

# . . Sample Analys is Report Sample Name : AFT.l39 . 

### Data Fil e Name: C:IPEAKNE'N>ATA\ANIONS\D"·100\Anlons..AXU0 1 3.DXD Low Range Detec t or : UT20 Unive,ml Interface Method File Name :**c:\pea nel~lhod\300anions.met**  

### Schedule File !:lame: .. • \anions082l.sch Date 1iq>e 

### Collected ' 2008/0SI21 

## a: 10:47 PM · 

### System Operator: 

### LLE . Calibration Date: 2008/08120 4:33:03 PM Calibration 

### Type : 

### EXTERNAL Component Amount Units : mg'L 

### · DiiU.tion FactQr : 1.00 

### Peak ln formatioo : All Components Pea k It 

### Component · component Name Comp<ineot Peak Relention Peak 

### Area Peak 

### Height 

### Number I I PlllQride 

### 3 2 Chloride 4" 3 

### . ffltrite (as 

### N) 6 

### 7 Sulpbate .

. 10.0 

### I

8.0 I 6.0 

# "' 

# "" 4 . 

### .0 12 3 

### I 

### I 

# s 2 . 0 

### I 

# V\1 0 I



### 0 1.0 

### 2.0 

# II : PeUNet S . 2 . 

### Amount ( mg/L)Tiro.e 1.9983 1.15 

### 3._7.394 1 .45 4:5458 . 1.94 . 18.3169 

### 6.35

AF7339 

### .....,



## t 3.0 4.0 5.0 6.0

Pate I ott 

### 9 

# A . ' 

### 127922793 31334260

. 154405982 295.24633



# \ 1 7.0**44~08468** 

### 8 1 292425 575209348 "40199205

8.0

Cine. Oaae : 2008108121

Curtet t 11mt : t5 : t8:..S)



### VES 005604**.,...~"':"": ~~** **\: •:** 



### . Sa Qlpl e**A~aly .sis**  

## Re port Sam p le**N~ :**  AF7339 

### D

. ola Flk N'IJDt: Cl\PEAICNE'N)A T A\ANIO N S\DX·looiAo i oos.)\A l 087. D X D Low Range Detector: UI20 Un iversal l nlerface 

### Metllosl File**Na~:** c-.lpeakliellrnelhodl3ooailions.met Schedu le 

### File Name: •.. laoions<f820 .$ ch · Date Time . Collceted : 2008108121-12:49 : 58 PM Sys1em OpemtO< : ll.E Calibration Date: 2008108120 4:33:03 PM Calibration Type : EXTERNAL Componein Amount Units: ing/L**Dil~tion** F ac t or : 10.()0 · Peak Infonnation :All**C~ponents** P ea k # Cnm po oeat 

### Number · Colppoa.ent Name**Cnm po~** **t** P eak Re tellli o o · P eak A r ea Peak H ei ght

· Am ount . (mg!L )Time 

# . " I . I Fluoride 1.9132 

## · h'o 1.15 10864232**~%,230** 3 

# z · Chloride 4 . ()_854

### ~'·.'**·** ... 1.65 15116813**~1947** ' 4 3 Nitrile (as N) 4 .5 131 

## !: · R: : : 1.94· 38809896 

### 664S!i()l 6 5 Nitrate (as N) 30 . 7477 3.14· 325 480142 41294950 7 7 •**phate** 18 .40 33 -. 6.42

### 502731~ 3$07448 .

A.F7339 1 0.0 8.0 6 . 0 

### 6 I 

# "' "- 4.0 

# i 3 4 7 2 . 0

# 1 I 

# J JJ f I I . ! 

# ! 0 

# I I i 1 1

0 1.0 2.0 

### 3.0 4 . 0 

### . 5.<) 6 . 0 7 . 0 8 .0 

# II : Peal:Nct S.l Qwrcnt Daae : 200810812 I hle l of1 Qaru,I:T ime: I2 : S S : II



### VES 005605

## Samp l e**~milysis** 

## Report Sample Name : CC'..B Da ta File N aine : Ci\P EA KNE'N)f. T A \ANI O N SIDX ·l OO\Anloos_A W0016.DXD Low 

### Range Detector : U12Q Universal lnterfa<:e Method Fil e N iune : c:lpeaknetlmelhod\300anions.met Sclledul.e File Name : . . . \anions082l.sch · · 

### Dale Time**Co~** 

### : io0810$121-3:)7:43 PM 

### Srstem 

### Openuo r : 

## rp; Calibratioo Dace : 2008108120 4 :33:03 PM 

## cilibralion 

## TYPe : ExTERNAL Com pon ent Am ount 

### Units : mgiL 

### Dilution F actor : 1 .00 ·• Peak 

### lnfo'!JI.&tiOn : All Components**~· :.f**  

### . • , 1



### Peak It 

### Componen t 

### N

umber . 

## . Com pone n t Name 

### Component Peak Re tention Amonot 

### ( mg,IL ) Tim e Peak Area**P~k** 

### IJ e l g bl 

# .:f: :;:' .

10.0 8.0 6 .0 (I) · 

# "' 4 . 0 2.0 

## : t

. I 0 

### I.

0 1.0 2.0 

# II : I'WN<tS .2 

### CCB

3 . 0 4 .0 5.0 6 . 0

Paa.elot'l 

### · 1.0 

### '·

· 

# . .

8.0

Cattm Date : 2008108121

. CWYICOI'nrt.e: tS:,.S:48



### V E S 005606

## Samp l e Ana l ysis · Report 

## ,, Sam ple Name : 

## ' ccv.



# _ Data File Name 

# i C:\PEAKNE'IWATA\ANIONS\DX-100\Anions_AVWOI7.DXD Low 

### R ange Detector : UI20 Universa l**Int~rface** 

### Medtod Pile 

### Name : 

### c:\peaknet\methodl300anions . met Schedule File Narpe: ... \anioos0821.sch



### · Date Ti111e Colle<:ted : 2008108121 3 : 4 6 :42 PM Systell\ 

### Operator : I..LE · 

### C:llibratioo Date: 2008/08120 4 :33;03 PM 

### Calibration Type : EXTERNAL Component Amount Units: mg/L 

### Dilution Factor · : 1.00 Peak Information · : All Components Peak II 

### Component Component Name**Nnm b~r** 



### 2 1 

### Fluo!idt 3 2 Chloride 

### 4 3 Nitrite (as N) 5 ' 4 Bromide 

### 6 5 Nitrat e (as N) 

### 7 6 Pho<pha te -ortb? 

### 8 7' Sulphate ·



### 10.0 8.0 6 . 0 II) 

### 2 

### 3 6 

# "' 4 

### 4.0 I I I 

### 5 I I 

### 2 . 0 I ' 

# l I 

# /\ • \ I I 

### \1 0 

# l 

# I

0 

### Lll 2 . 0 3. 0 

### Component POak Retention . Peak Area 

### P<;&J< H.eigbt



### . Amount (mga. )Time

1.9583 1.14 

## 2.9371 1.64 

### 1.4795 1.92 5.9676 2 . 74 1.9774 3.08 5 . 9078 4.89 11.8635 -6.26



### CCV

8 

### 7 

# A I I . 

# /\ i I ! 4 .0 

### 5 .0 6.0


# .. ..

Pa te I of I 

### 7 . 0 12525067 , 6 . 23747474**11944~51** 

### 22893094 . 1 3i8i5LS8 . 23081!)()9 1 04713176 ' 155tn642 202215649 ' 26383157 221838869 18219807 360432086 25107134

8.0

Cll.11'tftl o* : 200&'08121

ciwn:. l Time : IS: S.C : 49



### VES 005607

# . 

# . Samp l e A n alysis R e po rt 

## .**~·** 

## . Sa

lllple Name : AF734l . 

# . 

# . Dala File Name : C :\PE A

KNE'l\DATA\ANIONS\DX -100\Anloos ....A VL018.DXD Lo"" Range Detector : Ul20**Uni~llnlerfacc** · t.fethOd File Name · : c : \peaknet\J!lelhod\300•nion unet 

### Sched ule File 

### Na m e :

_ ,\anion5082l .sc h Date lime Collecte<l: 2008/08121 . 3:55:41 PM System Operat9< : 

# u.i · Calibration Date: 2008108120 4 :33:03 PM Ca l ibrlllioo Type: 

## EXTERNAL Co mponent Amount Units : mgiL Dilution Factor: 5 . 00
Peak 

### 1 Component Number ;2 • I 

### 4 2 

# s 3 

### 6 7

10.0 8 . 0 6.0 

### 4 .0 

### 2.0

0 0 

# Ill : rtaa.Ntc ).2**~k** Information : All Compone.ots Co!Dponent Name Cqm pooent Peak Retention Amount (mg/L) 'Iime 

### FlU«! de 

### Ollciridi Nitrite (a$ N) · Sulphate

4 2 

# s

# l1~**~ ll** **l** I I I l L.O 

### 3.0**2.67~** 20.5131 1.6012 89.8!'39

ltfl7 3of2



### 4 .0

hac I ori 5.0 1.14 

### 1.64 1.92 . 6:25



# 1 6 .0 

### 7.0 

### • 

# . . .;. 

### . Peak Area Peak H eogbt 

# . •

. , :f ·



# .... •**3262225~** 17058 , 6772 27171486 

### 563068787**~** 

### ' 

## .,. ' ' ·'-'



## ..



# .**·**

8.0 4836>470 339711023

4902309 

### 39694752

Clln'tllll OIIC : l008108/21

Cum:11t 

### nme :**16 03** **49**



# ------------------ · - - --- -- -- ---- -- VE S 005608· • 

## S'!lm p le 

## AnalySis Rep ort · Sample Name : AF'734Z 

### Data File Name: C:\PEAKNE1\DATA\ANIONSIJlX-100\AJiions_AAI088.DXD 

### Low RangeDetect9r: 

### 0120 Univeo;al In . tcrface Calibra tioo Date : 2008108120**4:3~:03** 

### PM M

ed!od P'llc Name: c:\peaknet\melhod\300ailions.ruet 

### Calibr!'lioo Type: EX'IllRNAL. Scbcd ule File 

### Name : ... \anions0820 .sc h Colll[lOilt nl Am ount UniiS : mgll.. Date Time C ollected : 2008/08121.12 : 58:5'1 PM . Dilution Factor : 

### 10,00 

### Sy&iem Operator : 

### LLB 

### Peak Io ronn a tlon : AU 

### CompooentS Peak • CompoDa>t**Compo~>ea.t** Name Comp<>Dea.t Peak Retendon Number AII>OW!t ' (mgiL)Thne 

### I I Ruoride 

### 2.6917 I:IS 3 2 Chloride 

### 19 . 8144 

### 1.66 4 3 Nitrite (as N ) 

### 1.67 6 7 1.95 

# s s N i u

:a

te (as N) 

### 61..7933 3.14 fj 7 

### Sulph ate · 8 7.3 835 6 . 45

AP'TJin 1 0.0 8 . 0 6.0

### ~ 4 .0 3 

### 6 

### ' I 2.0

# A 4 

# .I j 

# r: d! , 0 

### i 

# i 

# l

0 1.0 2.0**0** 

### 4 . 0 5.0 

### 6.0 7 .0 Peak At"d Peale Heigbl \**157~1** 

### 2396748 

### 78995064 JSIS36112 13714858 

### 2388089**81971 1~**  

### 90116964 26092 1 537- 

### 17939862

8 .

0

Oan cnc 0.1c: : lt'OMlSI'21

Curmlt 'l'1mt- : 1);07: I I



## . . 

## --- 

# ·--- - - -- VES 005609**-r** 

### . 

# ...**~** .**~ ~**  

### ;1; • • '-1-'



### . 

# "" Sample Analysis 

## Report V.: Sa01p l . e Name : AF7342D

### :~· D ata File 

### Name . : C : \PEAKNE'N>ATAIANIO Nl>'\D X-100\Anloos...-'UWO l 9. D XD 

# ...

. . LO w Ran&e Detector : UUO . Uoiversallnlerface 

### Calil!ratioa bare :**2008108~** 

### 4:33 : 03 PM . 

## . . l'>fllhod File Name : c:\peakile t \m¢tllod\300<utionunet 

### Calitiratloo Type : 

### EX'Il!RNAL 

## .. .**~t"f;'** 

### Scllc-.dule File Name: . . . lanions0821.ocl\ Component Amount 

### Unit$ : 

## m8/L Dale Time 

### Collec:kd: 20081081214 :04:40 PM Dilqtion Fa<IX>r : 

### 5.00 

### ' Syllem 

### Operator : lLB 

# - . ' 

## ...


## . 

# .. Peak Infarmati<in : All Components 

### P eak I Component 

### Compoaent N ameNumba2 I Flu<Jride 

### 4 2 Ebl<Jride 

# s 3 

### Nitrile ( as N) 

### 6 Phosph ate-ortho 

### 6 7 Sglpba1e



### 10

. 0 8.0 6.0 4**~** 

### 4.0 

### I 2 

### 5 2 . 0 l. l .3

## ~ 

# I i 

### i

t\_ 

## i I 0 

# . I I ; 

## ' J ' 

## . ' 

# i 0 

### 1 . 0 2.0 

### 3 . 0 

# li1 : PQtNet 

### . u Componmt · Peak Retentl001 P.eak Am Peak Hei&bt AIDOUill**(~)Time** 

## .

# '~"**~~ ~**  . . 

# ..,,

. .. f 

# "" r: . 

### 3.2289 .**--~-** 

## us**396227~ .**  

### 5413470 · 20.475 4**'** 

### . 1.66 1702481 . . 35290214 1.3345 

# ·· :ti 1.93 ' 2l4SS , . 3954489 · . 

## ' 

# -**·t:' ~··**  

## ·'lt

# 5483~3 

# i 38272963 

### 87 .66 57**~.** 

### 6.31 . ,. , 

### · ·: ·· . · 

### ·.:. , 

### . 

# .. . . ;:;- 

## . . 

# - . 

# .. . ·. ,:, 

### . .**:~~.**

·. ,•

: ·;J,.,,• ,· . 1f .**~·~ ~-** **·** A. P73nD

6 

# A



# __

\I

4 . 0 5.0 6.0 7 .0 8 . 0 ·;

h,t<lofl 

# (j--:- c 

# :J-O ·lf f!5'fl 

# p!YJ Iii**;.aJf·~l·** ).2 C.ntaOnc: 200&U/2.l CllrmtTiftle : 16 : 11:44 

# ·.

VES 0 05 6 10

# w · ., . 

## . ,**~** 

## .. ;. Sainp l e

## Analy**~** R epo r t S a1bplt Name : AF7343 . Da1t 1 Fi l . e**Nam~: C,\PEAKNE'N>ATA\ANIONS\DX** **lOOIAJJio~_AUKOZO.DXD** 

### Low Range Detector: 

### Ul20 Univen;al lnletface · Method 

### Fi l e Name :**~lj)ealcnet\method\300a ions.met**  

### Schedule File Nam e : ... lanionsOSZ I . sch 

### Dale Time**Coli~:** 

### 2008/081214:13:39 PM 

### Syltem Opcrntor :.IJ£ 

### calibration Date: 

### 2008/08120 4 :33:03 PM' Clllibtation Type : 

### EXmRNAL Comp onent Amount Units : mgll.. Dilution factor : 

### 5.00 Pea.l: Information : All 

### Components**Pcakf~t** 

### Nlllllbu · 2 I 

### 4 2 

### 5 3 

### 6 

## 6 . 7

10 . 0 8 . 0 6 . 0 

## 'a 4.0 

### 2.0



### 0 0 

# IIJ · : Ptu.Hct.U Compooent 

### Nllllt

### cOm~t Peak Reteotion Put Area Puk 

### Height Ar:aocurt (mg/L)Thne



### .**·~** 

## ..

- Fluoride Chloride



## 1 - 1

Nitrite (8$ N) 

### Ph9spbJUe-ortho SUlphate

4 I



## s

# ~~~I

j 1 . 0 2.0 . 

## "··

A.P734J



### 3 .

0 4 . 0**h~ttloll** 

### 5.0 1.16 

### 1.67 1.!)4 . 

### 6.31



# I 

# \i 1 . 0 

### 43751928 566!982 284346501 .**59286~8'**



### 2S51p79 4520082 734015349 . 5JI60619

8.0

Cumet OIIC : lOQ&,'()$121

OntntTimc : 1 6:21 : 4S


### VES 0056 11

### Sample Analysis Report Sam ple Nllmt : AF7344 Dola F.lle Name: C:\PEAKNE'N>ATA\ANlONSIDX·lOO\Anious..J<'fZOZLDXD Low Range Detector: UI20 

### Universal**buerfa~** 

### Melhod File Name :**c:~lmethod\300anlons.niet** Schedule File Name : ... 

### lanions082l.s ch 

### Dale Time Collecl ed : 2008/081214:22:38 PM 

### S)'llean Operator : 

### u.B · Cllibnili.oo 

### Datt: 2008108/20 4: 33:03 PM 

### Callbt adon Type : 

### EXTERNAL · Compoueo t Amount 

### Units : mgiL 

### Dilutioo 

### factor: 5. 00 Puk 

### lnronnAt i oo : AU 

## Comi>onenu Peak 

### I Compooeot Compontol Name 

### Peak R etentioo Compooent Amount**(m&IL Tl~**  . 

### J'eak AI'U 

### hal< H .t Number 2 I FluQride 4 

### 2 Chloride 

# s 3 Nitiite (.as 

# m 6 

# s Nill]lte (l$ N) 

### 7 7 Sul phate 

### 8 Iodide

10

. 0 8 . 0 6 .0 

# "' 4 

# .. I 

### 4 .0 2.0

0 •

0 1.0 2.0 3 .0 3.3614 1.16 17.3340 1 . 66 1.9210 . 1.94 . 

### 39.2511 3 . 04**68.23~ 8**  

### 6.30

AP7:u4



### 4 . 0 

## s.o 6.0**Pa~~Jt** I of I 7 

### I 4 13 141 31**~ 1424~860**  

### 2912575? 32840947 5696122 999401098**9012696~**



### . 418471207 29366343



### .

7.0 8 . 0

Cum:nt O.et : 20081081Z-I

O. rteol**T~** : ! 6:30:.46


### VES 0056 1 2• '**S;~mpl e**  

### Analysis Report Sa11ple Nam e : D ·SP I KED . Dala 

### File Name: C:\PEAJ<NE'N>ATA \ANIO NS\DX·l00\Anloos..AUJ024 .DXD Low Ra"'e 

### DeiOCU>r: 

### UT20 Uoivet>lllnterfaee Method File Name : c:lpeaknet\method\300oos.mel 

### Schedule Pile Name : ... laoiocu0321.sch 

### Datt Tune**~cted** : 

### 2008108121 4:49-.35 PM System 

### Opera10< : 

## u.e Calibmioo Dm: 2008108120 4 :3 3:03 PM 

### Calibiation Type: EXTERNAL Component Amount Units : 

### ftli/L Dilution Factor : 2.00 Peale lnfoi'IIUi t io n :**~II** 

### Components P eak ' II . 

### Component Com p<inen t Name**Co mpooe~~.** **t** 

### Peak 

### R e tention Peak Area Peak 

### H eig ht



# ., 2

3 4



# "' Number A10001nt**(mg!L) ~**  I 2 3



### 10 . 0 8.0 6.0 4.0 

### 2.0



### 0

. 0 Fluoride ' 

### C!ioOOe ' •. Nitrite 

# (as N)

3 

### I 4 

# l! 2 I : - 

## j 

# \IA. l 11 ; 

# I 1.0 2.0 r

### 3 .0 0.4618 ' 10J)343 1.281)



### B-SPTKBD

4 .0 

## s.o 1.17 1.66 1.94 .



### 6 . 0 7 . 0 133SlS92 212338011

SS798336

8.0 888214 30497368



### 1 . 663214

0......- : :ztlOI/Oit21



### o.we.n.:n:: :**~~:42** 

### VES 005613

# . . Sample A nalysis Re port . Sam pl e Name : II- SPIKED 

### Data File Name: C : IP EAKNE 1\D ATAIANIONSIDX-IOOIANIONS.,A U J0 2CI. DXD l..o1 v . Ra n 

### go Detcetor : VI20 U ni v ersa l lnterfll<:e Calibration P a re : 2008108120 4:3 3: 03 PM Method File N am e :**c:~lmethod\300an s.mel**  

### C•llbrat ion Type:**~AL Schcd~le**  File N ame: ...**\aD\90~2l.SC b**  

### Component Amount U ni t s. : mgiL Dote Time Collected: 200Stll8/2 1 4 : 49:3S PM Dilution Factor : 2.00 Syaein Operator : 

### ll.E Peak**Info~tion** : All CODljlODcnts

Peak j 

### Compooenl**Compo~!** 

### Name Componeat PUk R etention N u mber Amo o nt (aog/L) 1im e 2 I Fluoride 0.461 8 1.11 4 

### 2 OtJOride 9 . 8S44 1:66 ' 

# s 3 N i trite (as N) 

### I.U23 . 

### i.94 .



## ..

B-SPIKBD 1 0.0 

# ,..... 8.0 6 . 0 

# ., 4 

# ... I 4.0 

# s 2.0 I 2 

# · t 1 j1 I 

## lli\ 1 0 

# I I I I

0 i.G 

## z.o 3.0 4.0 

# s . o 6.0 7.0

ho. l o tl Pea k Area Peak Htigh t l33S3S92 888214 203164925 30497368

SS798336 7663274



### 8 .

0

o.ntna Due : liXl8K4I2l

Cunt lliiTimt ! 11:J6:Sl


### VES 0 0 56 14

## Samp l e**~aly sis**  

## Repol"t S ample Name: CCB 

## Dita F11eName : 

### c : \PEAKNE'l\D A T

AIANIONS\DX-100\Anions_ASR025.DXD Lo w Range Detec tor : Ul20**Univers~llnterface** 

### Calibra#on Date · : 2008108120 4:33 : 03 

### PM . M

c tllod File Name: G;l peaknetlmelhod\300 anions.me t 

### CalibratiQO Type : 

### EXTERNA L Sc bcdule 

### Fi le Name : ... lanions0821.sch 

### C<lmpooea t Amoun1 

### Uni ts : mgll.. Date Time Coll eclcd : 2008108/21**:58:3~** 

### PM System Operator: 

### LL8 

### Dilution Facto r': 

### 1.00 Peale 

### Information :AU 

### C<lmponents ' 

### Ptak I 

### Compooent ComponeDI Name**Compooe~~ t**  

### Peak · R e telllle>o Number Amount ( mgiL)Time



### CC B 10.0 8.0 6.0 <g_ 4 .0 

### 2.0 

# l I

0 I 

## ' 0 

### 1.0 2.0 

### 3.0 4.0 

### 5.0 6 . Q 7.0

# ~~ ' l'utNel S . 2**~lof'l** 

### Peale Area Peak**~~**



### 8 .0

Cum.M**o.~ :**  1(108A)8121

O. IT'tfll 

### -nmc : 1 7:06:4 1


### VES 005615

## i i 

# - · -- · ·**-~.** 

### · .



# ... Sample Analysis Report ; Sample Name : CCV · · 

### D ata File 

### Name : C:IPEAKNE1\DATA\ANTONSIDX·l001Aniom..i\SGOZ6.DXD Low 

### Ritnge Detector: !1120 Universallnter[ace Mc.thod 

### File Name : 

### c:\peaknel\method\300anions.met Scl)ed ulc File Name : .. . 

### \anioos082l.sch 

### D11e Time Collected : 

### 200&'o8/2J 5 :07:33 PM 

### System Operator : 

### LLE Calibration Date : 2008108120 4 : 33:03 

### I'M Calibration 

### Type: EXTERNAlCompon ent Amount Uhlts : rng/L 

### Diiution FO!!IO<: 

## 1.00 Peak 

### lnformalioo: 

### Ali Components**CompontD~** 

### Name Component Peak**Reta~tloD** Peak 

### Area Peak 

### Jldgbt AllloDDt ( mg(L)Thne 

# .., 2 I Fluoride 

### 1.9971 

### I.IS (21846196 2422&5!2 4 

### 2 Chlolide ).jl229 

## !.65 · 1 2311292 1 234%067**~** 

### 3 Nitrite (as N) 

### 1 .520 1 1.93**13663643~** 

### 23675loi 

### 6 4 Bromide 

### 6 . 0914 2.76 107002227 16129933 

### 7 5 Nitrate (as N)**~87** 

### 3 . 10 207812239 27790214 . 8 

### 6 Pbosphote-<>rtlto 

### 5.9529 

### 4.93**22~662971** 

### ' 18539:127 " 9 

### 7 Sulphate 

### 12.1665 6.31 370225002 26470281



### CCV 10 .0 8 . 0 6.0 

# ., 7 9 

# "' I 

### I 4 .0 2.0

0 0 1. 0 2.0 3.0 4 .0 

# s . o

· 6.0 7.0 8.0 

# II : l 'ea!CNtc S . l . OI RUII Oaac : 200810812 1 Pw I of I Ou'ruttTimc ; 17:1S:J7


### VES 005616

### . ;; : 

### . . ' 

### .

### S~mple 

## Ana l ysis Report Sa npl e Name : CCV Data Fi l e Name; C:iPEAKNE'NlA**TA\ANIO NS\DX·** **~OO\A lions.J\RYOZ7**  

### .D XD 

### Lo w Range**Dete~:** 

### UI20 tiniverul**loterf~te** 

### Mttbod Fi l e Name :**~:\pealcnet\methodiJOOuiionunct** Scllcdule File Name: .. . la nioos08 2 1, sch . Dille Time Collect ed : 2008/08/22 9:55:49 AM 

### System Ope.ator: 

### lLE Calibration Date : 2008108/20 4:33:03 PM

· Cal i bcilian 

## Type :**~AL** Com pon<Dt Amoun t Unh$ : mg!L Dilution . Factor : 1.00 Peak l:lfon:natiOD : AJJ Compoocu!s , 

### Peak t 

### CompoJient Nu . mWr 

### COmpooeot Name**~** 

## :V • Peak 

### Reteotf.on Peale Aru 

### Peale 

## lleiiht

- · . AIIIQIIA1 (lDg(L)Time


### ... - 

### (- . 

## .**~** 2 J Flu<lride 1.9828 - · .**.** 1.14 3 2 f

· ' O.iorjde 2.92'34**·~-: ....¢~** **"-. J.64**  

### . · · -**~--** 

### . 4 3 

## : !'litrlt; (as N )' 1 '.4710 .. " .. · 1.93 . 

# s 4**Br~** 5.90'7Q , . · ;, 

## : in 6 5 Nitrate (as N) 1.9618 . .3.11 

### 7 6 ·**Pbospba~nho** 5.8383 . · 4.9 1. 

### 8 · 1 Sulphate 11. 7449 6.30



# ' . 

# .. .. ' " 

### ' CC V 1 0 .0 8.0 6.0 

# "' 2 4 

### 6 

# .. 3 4.0 

### I I I 

### I 2 . 0 I, 

### II 0 

# I i

0 1.0 2.0 3 . 0 4 . 0 

### 5 . 0 6.0 

# II : Pu t Na s.z Pqc.lo(l 

### 8 I

7 . 0 126887 222 23845488 11 8 8 3 0320 21899912 - . 

### IJ202S002 22665855 103593925 15215956 20051 3 338 25957905 219034852 1(672816 " 356603 117 24342024

8 . 0**~Dote 2008101112** **()wTUit1" ~mc** **:** t0:03:S3


### VE S 00 5 6 1 7

### :- 

### Sample Analysis Report Sa01ple Name : AF7340 Data Flit Nilme: 

### C;\PEAKNE'NlATA\ANlONS\DX·IOOIAoions..ARW028.DXD 

### Lo" Range Detector: 

### UI20 U njvers•llnterf a<:e 

### M ctl1od Fil6 Name: c:lpeakneflrilelhod\3o0anions.met Schedule 

## Pili Name : .. ,\anio nsOall. sch · Dale 

### Time Col!ecled:**2008108122 10:04~**  AM ·

· System 

### Operator: lLB Cali bration Date: 2008108/20 4 : 33 : !)3 PM 

### Cillibrali9o Type: EXTERNAL 

### Componen t Amount Units : 

## m&IL . Dilution 

### Factor : 

### 2 . 00 Pea]< lnfonnatioo : Ajl 

### CompooeJns P

<alt I Compooeot 

### NUIJibtt

Cl) 

### 3 2

4 3 6 

### 6 7

10

. 0 8 . 0 6 . 0 

# ,. 4.0 2 . 0

0 0**Com~** 

### Name Chloride Ni!rite (as N) 

### Phosphate-!)rlh o Sulphate

4 I 

# h 3 

# s 

# Jli**~** i. j ! 

### 1.0 2.0 

### 3 . 0 

# .. Coml"""'it . Peak Rdeo&D ADIOOa t (ui'gli)Time 

## :· 

## 4- 0.81SO '€ .·.:,. 

### 1.65 4.6UJ · 1.94 

# ,_ 1.2443 .,. 

### . ' 6 . 35



# "

A.P1340 

# ?_I I •1-.0 · 

# s.o 6.0 7 . 0

Paatloll 

### Peak**A~•** 

### Peak Beigllt

· l626S376 31401S6 2 1 2405286 386!9129

14246888 IOSS660



### 8 .0

O.:tcnl o.tc : 2008108122

C

umDt Time: 10: 12:5)


### VES 005618

### Satllp l e A n a l ysis Repo rt Samplt Name : AF7340 D ata FUe 'Name:**C:\P~KNE'NlATAIANIONS\DX·lOO\Anions...A** WX014.DXD 

### Low Range Detector: UI20 ' Universallntertlce 

### Method File Name : o:\peaknclXmetbod\300anions . met Schedule File Name : ..**\aqio<is08~ .sch**  . DaicT imc Collected: 2008108121 3:19:46 PM



## . Syttem Operator: 

### u.E · · Calibration Date: 2008/08120 4:33:03 PM**C8U!l<a~on** Type : EXTERNAL Co!Dpooent AII\OUnt !) nits : mg/L Dilution Factor : 1.00 Peak Informati on : AU Co)Tlponents 

### Patk ' Componen! 

### Number Compoueal Name Compooent Peale**R~tmlloa** 

### Puk Arp**~k** 

### Heigbt Amount ( mg/L)Thne 2 I Flu oriile 14.4947 1.24 144 37 18228 8766 235 1 3 2 Cbloride 0.8981 1.66 34667154 , 7206069 

## 4 . 3 Nitrite 

### (as N) 

### 4.6iJS 

### . 1.95 . 458664906 $47159i8 4 

### Bromide 

### 6 1 Sulphate 

### 1.2345 6.43 323 1 5146 2281376

AP734 0 10 . 0 r8.0 6.0 

## 'a 4 . 0 

# s 3 I 2.0

# ~ 

# V\ , 

# 1 I \ 0 

# I J 

# l

0 LO 

### 2 . 0 3.0 4.0 

# s , o 6.0 7.0 8.0

""""' l>ou : 200WS/ll hu I oil OJ(re.U Time ; I S:l7:S3 . 

### VES 005619

### Sa mp le Ana l ysis 

## R e p o rt Sa

m p l e Name : AF734 1 . Da ta F il e Name : C: \PEAKNET\D A T A\ANI6NSID X- 100\Anions_A WSO I S .DXD Low 

### Range Detector ' : Ul20 Univ.:nal lnterfaoe !llelbod.File Name: c: 'fleal<r oel\mo t hod\300anlons.met 

### S<hedu l e File Name: , .. \anions()821.s<:h · · 

### om ' T in;>e Collected : 2008108121 · 3:28:44 PM**~ystem** Oper.rlor : Ull 

### Cali b ration Date : 2008108120 4:33:03 PM 

### Calibration'Tyjie : EXTERNA l . Compoooot A m o u nt Units: mg!L Pl l u

ti oh Factor ; 1.00 Pl:ak 

### lnfonnation : AU 

### Components 

### Peak II Conrponeat N a lllber Compoli<Dt Nanae Compo;;_..t 

### PeU R <ttDiioo Peak A rea Poak Heigh t 

### Amollll1 (mllfL)'Thne 2 2 

### O>JO<ide 0.6077 ; .1.66 23036985 5502435 3 3 Nitrite (as N)

## s.403?**~** 1.96 

### SS1963SSS 8919,0941 ' 4 Bromide 

## '**.** 

# s 7 Sulphate 

### 1.0979 . 6.38 28278107 1 984169



# II : PutNecU Oln'ent Ollc : 2008J06IZ I Pw I oil Cwm!t1'iow:: 1$:'36:-43


### VES 005621

# . Sam p l e Ana lysis Repi>rt Sanple**Name ~**  

### CCB Data File Na me : C:\PEAKNET\DA T A\AN10NS\DX·l00\Awoo5..A RR 032.DXD 

### Low Range Derec10r : UI20 Unlve,.allnlerface Method File N ame : c:\peaknetlmethod\300anion¥ . met Scloedulo F'ilc Name: : .. lanioos0821 .sc h 

### Date T i me Collecied: 20081Q8122 10:40:44 

## AM System ?perator : ll.E 

### Catibratioo Date: 2008/08120 4: 33:03 PM

. Calibration Type : 

### EXTERNAL Compon011 t An>o un t U ni ts . : mg!J.. Dilution 

### Factor : 1.00 Peak lofonn1tioo : All**Com~nu** 

### Q>Dlj>OIWit Name CompoDtJ> t Peal\ Rettolloo Peak Aru Peak**H~~t ~!lW!l**  ( m&fL)Thue



### CCB 10.0 8 .0 6.0 

# "' 

# .. 4 .0 2.0

0 0 1.0 

### 2.0 3 .0 4 .0 

# II : Pu.lN.ct . U Pate rot I 

## '

· 

## .

. 

# ,

5.0 

### 6.0 7.0 8 . 0**~** Dltt :2 1X1&08fl2 Cu n tlll Time- : 10:4 3: 47


### VES 

### 00562 . 2. ,. . .. . ' :;;r.: ..**.** 

## Sa m p l e Analy sis**Repo~** 

### Sam p le Name: CCV 

### Data File Name: 

### C:\PEAKNE'I\D AT A\ANIONSIDX·lOO\Anions,._AR 0033DXD



## . . Low 

### Range Deleaor : 

### Ul20 Univeriallnterface Ca ti bratioo Date : 200&108/20 

### 4:33:03 PM 

### Method Ale Name: c : lpeaicnetlmethodl300anions.met Calibration 

### type: 

## EXTER!"AL Sc h edule Hie Name: . . . \anions082l . s!'h <:;omponent Amount 

### Uohs : mg/L 

### Date 

### Time ColleOted : 2008108J22.10:49:43 

### AM Di lution Factor: 1.00 

### System Operator : 

## u.s . •



### -

· Peak 

### J,nfoonation : AU 

### Compo n eots 

# . . Peak I 

### Compo-' ComporteD ! NatDe 

### Number 2 

### I Fluoride 3 2 Chloride 4 3 Nirlite(as N)



### . 5 4 

## Bromi<le

6 

## s Nilll!te (as N) 

### 1 6 Phosphate-ortho 8 

### 1 S ulphnte

10.0 8 . 0 6.0 

# "' 2 3 " 4 

### 6 

# ... 4 . 0 

### I I I I 

### 2.0

0 

### 0 1.0 2 . 0 · 3 . 0 

## ' Compooeof Peak Re t e n tio n : ; Peak Area Peak 

### Heigb t A

mount ( mgll,.)'l'ime 

### .. ' 

### •·. :· · , ; 

## ' t l . ... 1.9622 

### 1 , 15 . , 125508573 2352926() • 2.9S87 1.65 

## <; 

# t 203mn**2238~** 

### 1.4908 1.93 . ;, 1338"8 1 442 22674.812 5.9699 

### 2 . 16**·~ .**  

### 104'756164 153 95567 i.9913 

## 3.09 203734111 26557040

. 5 . 876.1**4.9~** 

### 22056I9ii 1 78 1 0080

11.8500 6.31**36oi8~4** 

### 25013022 

# · .

. 

### : .· CCV

8 I

4 . 0 · 

### 5 . 0 6.0 7 . 0 8.0

Pue I of I OlcftN Om : 2008i08IU Curr= c Time : 1 0:57 : 49


### VE S 

## 00 5 62 3' 

# Method 7471A -:-Mer c ury In Solid Or Semisolid Wa s te .

Milxxaril Analytics Inc . .



## 6140 Campobello Rd. Mississauga, Ontario, Canada , LSN2L8 l-800-668-0639 

## www.max:xamanalytics.eom

VES 005624

# . .

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Test Cocke HO ·S lt1SU'\ll'.nCnt ld: Tau Dcoui1•ion : TO DETERMINI!**fER.CURY** BY COIJ) VAPOURAA . Job**S~e** 'll N ....... l'luonl>« D San1lleiD P Mo iR WTRX SPK 

### U't_ ICP2 AJI66n.<)l REP MAT 

## r.9'f SSIDol. 

### .Jl:. f(, BLANK A891112**~IR** ABDJIJNEOI 

### tJ,S 

## ;..ulnz AF46Z1.01R ABDJUi.Yoa /),0 A I914&S Am16-0 IR WCSS · I f) . AS914SS AF6677.0 1R 0 WCSS·2 

## AlP .**Al914 1~** **_** AF6<117.0 1R I 

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### wc.si1 · ')(. . 

### hl**~q** A8914U AF6679.01R WC.SS-4 

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# ,. t. ao 'A 891648 AI'734J.OI R CS.UZ.R2**~** fb 

### - 'J:J'}_
' A891648 M1Jolli-O 1 R CS.UZ.R3 

## x.ro ' t .t / •A I929lS AG126S-OIR TANK BACKFILL**~** ' AI9292S**A032~1 R**  WSW 

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### · .

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I 200&1nl1S 2 11:00 > . ( 200Mll/ 19 200110&'2lii:OO 0
·· 2 . 200Mll/19 200Mll/22 -18•00

... 2 200Mliil9 200Si01122 I 1:00

I :ro08/08119 18 ; 00 2 zoOsrol/19 200111UI!I22 . J 8 : 00 2 2008/0S/ 1 8 . 200810112 1 17:00 2 2008101119 200Mlll2 1 

## t 7: oo 2 200Mll/2ll 2o0Solll/21 17:00 I 200Mll/27 17:30 I it"lO

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### VES 005626

# ..
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MAI9148s:Ji.M Goolvar Ontario lne



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. NATiONAL: St IAwrt• ce Ce111rac lA c (905)475 - 599-4 s•T t ProjeCt#: 08 -1 16 -I O

.**NATlONAI. CROUPtOQNS£1!-CEI«V~**  INC**(315)437~** RUSH ICP+l!G, TOTALOILORIDBS,Im.l, %ASH. SUB TO PSC RI!PUBUC W ASre FEEDS Proj<a f : I 002.-011 NA110NAL:**INSitlNTUNA~NAL** . ( 41 6) 391 - 1 931 RI!O . I Sl, T**~1.83/1** OO!h lo Pr•jecU: 1'33 81

. NAnONAL: CII,U It T'rM . Ebllll< (CTl) · M<lhod S!ril:e



### -

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### Batch Reagent Tr.acklng Record · W orksheet# . 

# i**'S. "'** **'l."~** 

## g 

# 7 Volume lull Sunoliate/Spl k e io lu lions Solllllon

### 10**~** Cone. B lk :sp k MS . 

### . Samp l ••



## . . ICPMS !CAP 

### ICI' SoH Spk. A(SPK-08-0a)&B Variable 

### 1m l/

SOn!l .**Gf'~** 

## . ,

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### Hg Hg 

### Splke(Hg Spk-08·08) . 0.25ppm .' 1ml. /SOn!! ; 

# 1-:l- i



## ..

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### Supp U er Lot 

### No. Splkod by; 

### HHO, tiShet 

### 30 8144 

## PIH HQ 

### Roher 

### 206051 " Spllclng W'rtneeaod by : 

## HA 

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## (yyyy/mm/i

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### V E S 00 5628

# . 

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### and Wei Chem 

## '- I I 

## limo I 1 np le 10 •erified • ' 10 <watertl ' IYPO • matril< soilce aooear ' lilar. lni Ua l samolo as well as fin8l e>«ract**~-.cle o<ly**  Ito**10~** •amlll .. I

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### VES 005629Pnkin-&l_mer AAw i'nLa . b: 2008 . -08-2!, 01 : 16 :39 PM Saap1e**f~toraation** Fiie**C:\AAUStn\SAMPINFQ\~-8-2lA.S~F** Dosc; r i p , tion Batch ID Volume · Unit . s ll eiqht · o n i ts Analyst Semple Voluae AB Saaple lD Loo

17 15922.94 :REFMAT 1 8 8LA NK ' 19 MTRX SPJ( 20 A G

06513 · 03: 01 21 AG0658-03 22 AEB352:6.3 23 AF8 098-02 2 4**AF889.9 02**  25 AFB 1 o o- o2 26 AF81 01 -02 27 AG0659-03 28**~0660 03**  29 AG0661-03 30 

### REMT 31 Al'l 193 - 0 . 4 32 AF119 4 -04 33 AE8352-03 K 2 3 4 AG0660-03 K 5 

### 3 s cca 3 6 cCv 3 7 1 592587 :RE FMAT , 38 BLAJII(

39 11\'RX SPK 4 0 AF6617-0l : Ol fl AF6617-0l 4 2 AF1 3 !2-01 • 43 AF7 343 - 0i ) j(.l O 44 AF 1 3 44-0Y 45 AF4626 - 0l 4 6 AF46 2.7 - 01 41 AF6618 - 0l 

## i-u'iJ 48 AF66 1 9-0l 4 9 AG3265 • 01 SO AG32 5 6 - 01 51 AG32 71-D 1**~2** AF66 7 6 - 01 53 RE CW. T 5 4 CCB 55 CCV 

### Lily 0.00 s..pie 

## s..Pi· 'K!ivht ""it• 0.50 00 0.5 000 0.52QO 

## o

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### o. 5100 0.5009

. 0 . 5000

0.5 . 100 

## o.sooo 0.520 0 0 .510 0 

## o . sooo 0.5100 0.5 200 . 0.5200 0.5060 0 . 5 100 0.5 100 0.52 00 0.5100 0 . 5 1 00 0. 5200 0.510 0 0.5100 0 , .5000 , 

## o:s 1oo . 0. 51 00 

### user Reaark• Dilution

50.0000 50 . 0000 SO,OOOQ · 

## so.oooo sO.oooo 5 0 .. 0000 

## 5o.ocioo 50.0000 50.0000 50.0000 

## so.oooo. so.ooo o so. oooo .' s o.oooo 50.0000 50.Q000 . 1 00.000'0 250.0000

50.0000 50.0000 50.0000 50 .0000 

## so.oo oo so . oooo 50.0000 50.0000 5 0. 0 000 50 .00 00 50.0 000 

## so.o' ooo 50.0000 50.0000 50.0000 50.0000 

# .n.,-v

Page -16 - 

### VES 005630Perlcln - Eolaer l\1\lU,nL<Ib: 2008-oS - 2 1 , _ 09:22:22 11M

### ---------~------ 

# . .**------- -----** **..-~---- ---**  Method HaM: HG S JOB Method Descript i on: Soil - -Campobello Rd. (509 uL loc p ] Ele .. ent . : H9 Dlte: 2008 - 08 - 2 1

· Toc hn i que:FI• MH S C•llbrotio n T ype: 

### ijq , Ze r O Int er ce pt: Li nea r ' w

a v elen g th: 2 53 . 7 . n m Sa

mp le I nfo N a me:**8-2ll\. F** **Ro~ ul** **to** Dat a s et · Nam e : 8·8-2lo 

# _____ 

# ....,.. _ _______**-~--~ ---------** **E1e~en :**  

### H9 Seq. N o.: 

### 1 Stmple 10: Calib B la n k Rtpl

I I 2 Mt&n: S tndCo.nc mq/t. .**Aato·~ero** per f orQ e d . AS . Loc.: 9 Date: 2 0 0 8 - 0 8 • 21 . Peak HeiQbt 0.0000 0.0000 Time Pea lt Sto r ed 09:23:1 6 No 09:23:56 No



## --=- ---.---- ..**~··------~---· ---** **---- -==**  E l ement : H9 Seq. No . . : . 2 AS Loc.: 10 · Da t e : 2008-08 - 21**Sa~p1e** ID: 0 . 20 p pb



# -------- - - - - --- - · - -- · - -- - - -------------·-- ------- -- - - · -- --- - - - --- -- - - -- - --- ---- - - - --------- i\epl Sa.mp l e co n c Stn dC onc Peak**Tia~ .**  ·**a.k** . I m 9/L . 1119/L HeiQht S t o r e d 1 o. o oi 7 0 9:2 4 :51 No 2 0. 001 1**o~:2S:3o** No Htai,: {KQ ] · Standard nuaber l applied. (0.000201 . COr-relation**Co ~.:cient:**  1·. 00000 Slope : 8 . 473 4 0 

# -----= =-=="' =----- · ··-----= ·= --- ...**-~** £1•ent: Hg Seq. No.: 3 AS Loc.: 11 Dote: 2008 - 08 - 21 S&ap l e ID: O.S 

### PP.b



# - --- -- - -- ------- ----- ------- - - -----------·- ----------- ----------------------- -- ----- --· R4pl



# • l 2 Mean: Sa.spleConc J19/L StildCOnc 109/L Peak HeiQht 0 .0 042 0.0042 "tixle Pea k Storf:d 09 : 26:25 110 09: . 27:03 NO IH9l Standard nv»ber 2 opplied. {0 .000 5 0 ] Correlation Coe f ficient: 0.99989 Sl ope: 8.35 1 55



### __ .,..,. ____**.,.~ -·•-•-** **w-• --** **·-•• -"'-c••••·----"'•.z** **6le~>ont:** Hg 

### Seq . N o. ; 4 Sam p le ro: 1. 0 ppb Ropl 

## • • l 2 rtean: S arQP l eC o nc 

### mg/ L St n dConc mg / L AS Loo.: 12 Date: 2 008 - 08-21 Bea k !I eig h t 0.0084 0.0084 Tirn& Pea le Sto rad 09:27:58 N o 09:28 : 37 N o { H9) Sto.ndsrd nual> e r 3 applied. {0 .0 010 01 correlation Coefficient: 0.99998 Slope: 8. 35920**L!LSO=-=-• •--.....:=------** **------.._-ma-•---·----·-•--~-- -~~**  tlur.ent: Hq · se q . No.: 5 1\S Loc.: 13 Date: 2008-08-21 sample ID: 2.0 ppb 

# . .**------ --** **---- -----** **-- -----------** **------~- -----------** **------- ----** **-- ---** **----- --** **-- -----**  llepl



### t l 2 SampleConc StndCon c mq/L 019/L Peak HaiQht 0.0169 0.0168 Time Peak Stored 09: Jo:o8 No 09:-30: 47 No**~age** - 1 - 

### i.

VES 005631

### . ·' Perldn-Elooor AAIIinLab: Ke&n: ·:· l!lg) Standard n wnbe[ · C appiied. ' (0.00200) 

### OOrralatlon Coe ffi cient : 0.99998 . -:"" # >:.**~V;:'·** . 2008-08 - 21. 09; 30: '1$ 1\K**~:.f.·** 

### .**~** 

# ...**;~!!~ '.~** **Slope:** 8. 41364**·.;.~~** tlt10ent: H , g Seq. No . : 6 

### A S toe.: 14 Sample ID:· . 5: 0 ppb**'~:** 

# ·---- ---- - -------------- --- - -- - ------ ----- ---------- - -- --- - - - -- - ------------- -- ----- --- Ropl



# • 1 

### 2 Sampleconc 

### mrj1 L StndCon c 11< 9 / L Peak H,ight 0 .04 27 0 . 0426 •r ime Peak Stored , 09:32:2 0 No · 09:32:5&' N o Kean: , l !lql Standard · ,nwllber S ,. appliod. (0.00500) COrrelatio n**Coe fi~ient:**  0.99997 · Slope : 8.51039 U.,..,nt:

### ~9 ' Seq. No.: 

### 1 ' liS Loc.: 15

### ~te:**2008-08-21 .** **-~-·** ·. Sample 10. 10.0 pp b .• .., 

## .;?,**-- -·** **--- ·-** **--.:.- --...-** **--~ -:**  

## ........ ...... 

# _ .. 

# ____ __ _ . _

...... .......... 

# _ · · :.:- 

## .. ......... . ..... .............. .......... .. . ........... . ..**~-.:;;_ ---** **--** Repl SaopleCOnc StndCOnc Peok Tiooo . · Pea k 

# a

f ag /L**ag ~**  Height 

### . st ' ored 

## '"-!t': 2 1 " 0.0195 09i34 :Jl ., No

### ~l;M**~** 6 

## o. 0793 09: 35: 1o ·::· No

# ~;r: St4ndar-d.

# number**·** ,applied. (0.0 100}

# ~·?;·f'**~~** Corrolo.t i o n Coef.f ic ie'1t: 0. 99918 Slope : 8. 01758 . 

### ·,<.:<.:**·-~------ --** **----·---- -------------------** **-- -----** **------ -----** **------ ---** **-----~- --** **-- ------** **~** '**;~** C411brat i 9 n da ta 

### t or . tt g • . ;, , Eot e red ··.**;alcula .te~** **~~;** · . M

ean Siqnal Conceptrati9 n Co ' nce.ntra ttOn Standard ·'**~·** Standard ID l P k Heiqht) ( llq/ 1.) · · l,. q /Ll Deviation 'RSJ:l · 

### Calib Blank · 0. 000 0**----~** "'·**-,- ~.·**  0.20 ppb 0:0017 0.00020 : . 0.00021- 0.000063**3.7 ~·** **0.~** ppb · .• O.O . OC2 0.00050 ., . 0 . 000 52 0'.000001 --- • 1.0 ppb o.oos4 o.ootoo o.o0104 o.oooo ' 12 0.1 2.0 ppb 0:0169 4.00200 0.00209 0.000033 o.z 5.0 ppb · • O.OU7 0.00500 0 . 00528 0.000097 0.2 10.0 ppb 0.079C 0.01000 0 . 00983 0 . 000102 0.1 

### COrrelation Coefficien<: 0.99918 Slope: 8.07758**~---** 

# ·---- --- - --·----- -- --- ---- - --------r•----------- . --- ------- ------ ------------ ----- --- -

;.

Page -2 - 

# I

VES 0 056 32

### Per ki n - Elaer**~WinLab:** 

### 2008-08-21, 09 : 35 :52 AM Hg 

# 0.10 1 1**0.~8 1**  

# l 0. 06 

# . 1

0 0 . 005 0.010 0.015 Concentrat!on



### VES 

### 005633Perkin - £Laor**AA~inLab:** 2008-08-21, 10:09:57 AM**S~le** lnfo..., tion Fil.e C: \MUSER\!WU>IN!'0\8-8-21A.SIF Description 

### Batch ID**Volu.~te** Onit.s lf

eiqht Onit• An aly•t**Sa. wp** **l~** V ol wae AS Saepl.c> ID 

### Loo

17 159229 4:REFMAT 18**8~-** 19 H7RX SPK 20**'AG06~-03:** Dl 21 AGD658-03 22 11&8352-03 23 1\FSO!B-02 2 4 AF801 . 9-02 25 IIFBl00-02 

### '26**l\rS~01•02** 27 AG06l9-03 20 /IG0660-0J 29 · AG066l-03 30 RE!'MAT 8-8-21 • 1 59 2294 

### L ily

0 .00**S&~Qple** Saaple Weigh.t Unit• 0.5000 0.5000 0.5200 

## o:5 · loo 0.5100 0.5100 0.5100 0.5000 

## o

· .5zoo (). 5000 0.5000 0.5200 0.5 100 0.5000 tJaer Reaa.rk 8 DUutioh

50.0000 SQ. 00.00 50.0000 50.0000 50.0000 .• 50.0000 · 50.0000 50.0000 50. 000'0**50.~.000 .**  50 .0 000 

### so · . oooo · · 50.0000 50. 0000



### Page -6 - 

# . •

. _;; 

### ·o(-·**·~t: .f.,~**  

## . '"'• :'f': .**~.**

### ,~·'**~·** '**:ij(.~~···'**

### ·~·~·



# m,;. ·:N :

VES 005634

### / o). 

# h**it~7.**

(o117t
I 

# '-fl.**------------------------------~ ====** **------------ ~**  tlemen t: 

### Kg Seq. No.: 11 

### 5a"Ple ID: CCII AS Loc.: 1 Date: 2008-08-21



# - - - ---- -- · --- -- --- ---- · --- · -·-------- · --- ------ · - ·

- -------- · ---------- · ------- -- --------- - . . llepl SupleConc StndConc Poak Time**Pea~**



# • 10qfL "'9/L Height Sto r ed 1 0.00002 0.00002 0.0002 10:11:03 No 2 0.00002 0.00002 0.0001 10:**~l:** 41 No Mean · : 0.00002 0.00002 QC 

### voluo within speoifie<l limi te. 1'!- ...**~-** ..**-~-----·-·----.--** ...... ____________ "'

_____**.-,~ ---**  tlementl Hq . Seq. N o . : 1 2 AS Loc.! 2 Da te 1 2008-0B-21 Suple 10: . CCV**-------- ------------** **--- -------** **--------- ------** **----- ---** **----- ----** **----------~ ------** **---** Bepl Sam.pl&Conc S tndConc Peak time Pea k

I mg/L mg/L**~eight** 

### Stored 1 0.00408 0 . • 00408 0.0330 10:12:35 No 2 0.00410 

### o. 00410**0.03~1** 1 0:13 : 13 No Mean: 0.00409 0 . 00409 OC value**Mitb~** speci fied lln.lts. Ue .... nt: Hq 

### Seq . No.: 13 , Baap le 10: ICV-!.000 AS Loc.: 3**Da~e:** 2008 - 08-21**-~--- -~~** **--- --------** **--- ------~----------------** **-- ---** **----- --** **------ ·------** **---------- --**  Rep1 

### SupleConc StndConc Peek Time Pea k



# • mq/L · "'9/L !Ieight Stoi e d 1 o:ooo3o 0.00030 0.0024 10:14:41 No 2 0.00028**0.000~8** 0.0023 10:15:19 ' N o 

### ttea n : 0.00029 0 . 00029 QC value w i t h in sp ec if ied limits.

## ----------·**···-- ----~-----** **-- ----** **--** &lemont: Hg Seq . No.: 14 AS Loo.: 4**o~t e:** **2008 -08** **21** Sa..ple ID : I CV - A**·- ----** **--- ----** **-- ------** **------------------------ --** **--- --** **---- ----** **----------- ---**  Repl

I SampleCoqc StndCOnc mg/L mg(L

o.00214 o:oo214 0.0021 4 0.00214 Mean: O.OQ214 0 . 00214

1 2 Peak Height 0.0113 0.0113 

### OC •alua within specified 11aita . 

### Time Pe-ak Stored 10:16:13 No 10:16:51 No

### ...w·---,------------~------~------**------====a~~------~~~--------------------** &lcaent: Hg Seq. , No.: 15 AS Loc.: S 

### Date: 2008 - 08-21 Sample 

### ID: ICV-5 

# ·---- - -

· -- -- - -

-------- --- · ------------------ · ---------------------------------------- . ---**~•p 1**  

### SampleConc StndConc P•ak**Tim~ P~** **ak** I mg/L mg/ L H eight Stor ed 1 0.00411 . {), 00417 0.0337 10:18: 21 

### No 2 0. 00411 0 . 09417 0.0331 10:18 :59 

### No H ea ' n: 0.6 041 7 0.00417 QC value w ithin spe cified li m its.**•-•• ---=-** **===<= ---l'l** **lW1 4Ula•~----~** **=-••--.•Oil•--•••** 

### .. •-= . Element: Hq Seq. No.: 16 AS Loc.: 17 D at e : 2008 -0 8 - 21 · Sample 10: 1592294: REFMA'I' ·**·-- ----------** **-- -----~-** **------ --** **--- --** **---- --** **-- -------** **---- ----------** **----- --** **----** lep1 Samp1eCon.c S t ndConc Peak Time Peak



# • aq/L mg/L Haight Stored 1 0.317 0.00317 0.0256 10:20:27 No 2 o. 311 0.00311 0.0251 10:21:06 No Kean: o.3u 0 . 00314



# ----- - E.lec.e.nt: Hg Seq . No.; 11 AS Loc.: 18 Date: 2008 - 08-21 Sample ID: . B!Jl.NK


# ·------ -- - - - --- - -- -- -- - ----- ------------ --- -- ------- - -- ------ -- ------------ -- ------- - - - Paqe -7 - 

### VES 005635

# .. 

# wr! lll -nt: Hq Seq. 

### !'0·: 4l S&ftple ID: l592587 : R£FHAr AS Loc.: 37 Dat e : 2008 - 08 - 21**--------- -~** **------- ---** **------- --------** **-- -·** **----- ------** **------- --** **------------- --** **---- ---**  

### Repl Saapl e Con c St nd Co n c 

### Pea k Tillie Peak



# • •9/L mg /L Ho:J.ght Sto red l 0 . 3 08 0 . 00 3 14 0.025 4 01:18 : 18 N o 2 0. 299 O A0305 0.02 4 6**:18 5~**  No t- te a n : 0. 30 4 o . 0 0 3 1 0**---------~- --•••--••** **""..,a ==-•-=** **=-•---==-- -•-** **•-** Elemen t : ' nq . S eq . N o. : 42 . M Loc . , 3 8 Da te: 2008 - 0 9-2 1 S aople I D: B LANK

### -----------------~--**----- --~** **~--~----- --** **~- ---------** **---------- -------------** **---- --**  S amp l eCon c >lg/L

. 0 . 002 5 0

0.000 6 5 0 . 00 1 57 S t n dCon c 109/L . 0. 00002 0.00001 0. 00 002 lll .... nt : Hg S eq. N o.: 43 SUple ID; lflllX SPK · Peal< H

ei g ht 0.0002 0.0001 T i me 01:20:2 4 01:2 1 :02 Peak S to re<!

N

o N

o AS Loc.: 39 Date : 2008 - 08-21**---- ----** **-~---- ----** **-- --** **-------- -----------** **------------- ---** **-- --** **------ --** **---- --**  Repl 

# · • 1 2 Ne on; Samp l e Co nc raq/ L 0. 59 8**0.~29** 0.613 St nd Conc: mg/L 0.0 0 610 0. 006 , 41 0 .00626 Pea k H

oi9ht 0.0493 0.0518 T . .lme P e ak S tored 01:21:56 · N o 01:22: 34 N o .**._._.__.• e=** **=== ~==** **••--•••- •••** **••••• ••--••** **uuc.= =-z=-** **--••-------·••••••---------------** El e m e nt:**~9** Seq . No . : 44 · A S Loc . : 4 0 Da t e : 2008 - 08- 2 1 SO rnp lc l D: Ar 66 7 7 - 0 l :D l**·-- -------** **-- --** **-- -------** **---------~- ----------** **-----------·---------- ---** **----- --**  Re p l Sa i.Q pl eCon c Stnc!Con o 

### Poa k Tilll.e P eak 

# •**~> /L**  mg/L Haig h t Sto red 1 0.0 263 0.000 27 0. 0 022 01:2 4:0 2 No 

## i

2 0.0 2 65 0.0 0028 0.0022 0 1 • 2 • • 4l No 

## f:jl · ttean: . 0.026 4 0. 00027

# ~ )( I D £l oment: Hg S eq. Ho.: 45 AS Loc.: 41 Date: 2008-08-21 SUp1e ID: I\F6677-0l**----- ~--** **---- ------** **---- ----------------------------** **----- --** **--- ---** **-------- ----** **---** Ropl

t 1 2 " ean: SaaphtConc roq/L 0.0228 0 . 02 48 0.0238 stndConc NJ/L o:oo02f 0 . 00026 0 . 0 0 0 25 Pea k lteiqllt 0.0019 0.0021 t'i>le 01:25:35 01:26 :14 Pea l< Sto r e d

No No



# ---- . -· = =-- =-= ·- - ---- -- ------ -- - ..**--- ---·-·----·** **-- =**  

# .. Slo m e n t : h q S eq . Ho .: 4 6 S a m

pl e 10: AF 7 3 42- 0 1 li S Loc.: 42 D ate: . 2 0 0 9-0B- 2 1



# --- --- - -- - - ---- -- ----- - - ----- - - - ---------- -- -- - - --- ---- - - - - -- - - --- - -------- --- --- ----- - lloo p l Sa mp l eC o n c S t nd Conc 

### Pee k Ti m e 

### P e a k .; I m g /L m g / L H eig h t S t o r ed 1 6 . 4 3 0 . 0 6 5 1 0.5257 01 :2 7 ;0 8 N o Sbph a bs o r b ili n ce**s** 9r:-eat.er than t h at 

### ot tho bi gh as t s e a n d i:ar d .

2 6.41 . 0 .0649 0 . 5241 01:27: 4 6 No S&IIPle absotbcinc e i . s q reater than t . hat 

### ot the hi g h e st s 1: a ndard. Mean: 6 .4 2 0 . 0650 S&J:il)le absorba n c e is qreater than that 

## or the hig hes t: s tandard. 

### -== 

# ·- U.ement**'** Kg Seq . N o.: 47 AS Loc.: 43 Dat e: 2008 - 08-21 S&ople ID : AF'7 343 -0l



# --- ---- -- - --- - --- - -- ---- --------------- - - - - - - -- ------ -------- --- ---------- - --- ------- -- l!epl 

# • Satap le. C onc mg/L St ndConc m

q /L T ime Pe ale Stor ed Fa g e -17- 

### VES 005636

# ..

# ~ f-/0**·· -=** **·~~. ~** **~-.** 

### - Per k in-Elloer AAllinLab:**2oo:S-os~21,** 01: 29: 16 Pt1 1 6.02 0.0614**~ple ab~orbance** **gre~ter** 

### 2 6.00 0.0612**Sa~plo** absorbance is greate r H<pan: 6 .01 0.0613 Sa•ple. absorbance i.,: 9reater . o . 4962 than that

0.**494 ~**  than that**-~ -~** **~** 

## :· 01:29: 1 · 6 No 

### of the**~qhest** standard. 01:29:54 No 

### of the**hlghes~** standard . th-an that o! the '**hi ¢'e~t**  standa rd.**w.w---..._•••••••••--~·~~ ·-•••--.-----•~----.-....-** **~~--.c==•=--•• ••--** **--• ••~-** **-- ·-** **•oo-• --=**  Ele r O<tn t : Hg seq . N o .: 48 Snple tO : · A F 13H -0 1 AS Loc.: 44 

### Pate : 2008- 08-21 • 'I

• • 

## . 

# .**----------~ --~** **--- ----** **-- ----** **~- -----------** **--~-~- -~--~-** **-- -----** **-- --** **---- -------** **------- ---**  llepl SOJnp1eCo nc Stn dConc 

### Peak Time**l'~ak**



# • "'g/L 1119/L u eig h t Stored 1 6.70 0.0683 0 . 5516 Ol:3l:25 

### !IO Sa.aple absorbance is greater than that of**th~** hiQheSt standard,

2 6.68 0 . 0681 0.5500 01:32:03 No ' J;anople absorbanc e is greater th&n that of**the~ ighest** **standa rd.**  ato•n: 6.69 0.0682 

# .. Sa.aple ab.sorbaOoe i.s gre•tor thao tha t 

### ot tbe 

### :hlqhes t standac"d : 

### :! . 

# .... lltment: Hg ,Seq . No.: 49 

### AS Loc.:**tS ~**  

### Date: 2008 - 08-21

# ~**~~~~ ~~~** **~~~~~=~~ --** **------- ---------·** **--- ~~~** **-- ~----** **-------------- ~~~** **----- -----**  " Repl SantpleCo nc StndConc**Pe~k Time** **~:-** Peak. ... ,._, .f, t "g/L 1\ g/ L fleight .1if - stored • 

## i·"!'t' · u,. 1 0 .12 1 0.00126 0.0102 · 01:33:35 · No f'I.AT> · 2 0.0895**o.oo o9** **~** o : oo75 01:34:11 No . · . · . . 

# .........**::,...J~~ ea** **r:** 0.105 0 .00109 ·, _ . . . 

# .. 11' 

# "'r --------------..----·-...;,- ...**--~~,.,.- ""'**  

# ____ ___ __ __ __ ___ --="""""· 

# M'.KJ**:::~\D gAF** 

# 46**i; ~O** **o.:** 50 ·. AS Loe .: 46 "i 

# Date: 20 98 -08- 21 . .

-- .;. __ ......... r .. - - -- - -- ..... ---**-- --** **-- ~-** **-- --**  -- - -: - ... - ___ .._ .:.. -- - - - - ------ ... -- .. -- ..... -: ... -- ·-------- - --- - · - P.cp l . S&DpleConc StndCOnc**~oa k** **Time ·~·** **a!<**



### t 109/L mg/L Height ,., Sto"ed 1 0.0687 0.00070 0.0057 01:35: 45 No 

## D.b1 2 0.070 4 0 . 00072 0.0058 01:36:23 No 

### Mean: 0.0695 0.00071



# 'I Ji)

# ~ 11-ot: . Hg Seq. No.: 51 

### AS Loc. : 4 7 

### Date: 2008 - 08 - 21 S&mple ID: AF66 7 8-0l llopl Samp1eConc StndConc 

### Peak Tiloe Peak

t mg/L mg/L Height. stored 1 10 . 8 0 . 110 0.8911 01:37;55 No saup l e absorbance i s g-reater 

### than thot o f the h i 9hest standard .**~** 10.7 0 .10 9 0.8794 01:38:33 " No Sl,luple ab s orba nc e i s greater 

### than thot of the h i ghest standard. 

### t:tean : 10.7 0.110 

## sa .. ple absorba nce i s greater than t h at 

### of the highest s tl2 nd ard.

_____ =---c:: ___ .;.... _______**~- -------------===-**  

### E

l e m ent: Hg Seq · . No.: 52 Sal!l(>lo IDi AF6 ' 679 - 01 Repl SampleConc StndConc



# ' rag/L Rq/L L 0.0532 0.00055 

# z 0.0 4 51 o :ooo t7 !lean: 0. 0491 0.00051 AS Loc .: 4 8 

### Date: 2008 - 08 - 21 Peat 

### Ti .... Peak Height Stored 0 .0 045 01:40:0 2 No 0.0038 01:40: 

### n t<o**----~==~ ==** **=---· ==** **~~=-~·--------~bb~=------~----==~----- ·--** **---= ~~**  .£1.etHnt: Hg Seq. No. : 53 Sa.Rple ID:

_ AG3265 - 0l 

### AS Loc.: 49 

### Date : 2008-08 - 21



# --·--- - ------------ - ---- ---- -- --· --- - --- ----- ... 

# ---· . - - -- - -- ---- ---- -- --- ----- - -- ---- -- --- - Page - 19 - 

### VES 005637

# lh · f/'1. 

# fN



# c

- '1**lo~Z Per~i.n** **-&lm er**  AAII1nl.ab:**2008-0~ u,**  01:40:43 PH**~pl** Sii.pleConc StndConc Peat Time Peale 

# • tnq/L mq/L Ho1ght Stored l 0.00180 0.00002 0.0002 01: 41:35 No 2 0.00169 0.00002 0.0001 01:42:13 No Mean: 0.00175 0.00002

## --===~**===== =-----** **·--------=** 

# ==== --------- · · -· - .... ·==--= &lcllont: Hg : Seq. No:: 54 AS Loc.: 

## so Date: 2008-00-21 Sa

mp le I D: AG n 66-01

### -~~-----**-- ----** **-------------- -------~----------------** **-------- ----·------------~-** **--------** l!epl SampleConc Stncteono Peak rime Peak 

# • mq/L 109/L Ha i ght Stor ed l , 0.0335 0.00034 0.0028 01:43:07 No 2 0.0337 0.00034 0.0028 01:43:46 No tban: 0.0336 0.00 03 4

### ~~**=-----=-~----------------·=---** ue...nt: Hg**~q.** No.: 55 1\S. Loe.: 51 ' Date: 2008 - 0.8 -2 1 · Sample ID: AG3Z71-01 lepl SaapleCooc StndConc Peat 

### u •• Peak



# , . ff¥J/L J09/L He1;ht**~tored** l 0.00137 0.00001 0.0001 01:44:40 No 2 , 0.00253 o:oooo3 0.0002 01:45:18 N!> !loan:: 0.00195 . 0.00002**----------~--** 

# ---**-----·--~** 

## ... 

# -·---- Element: Hg Seq . Mo . : 5.6 AS Loe.: 52 bate : 2008-08-21**S~~pl~** 

### ID: AF6676-01 .

### ----~-----**-- -------~------** **----- ---------** **-- ----** **------- --~----** **-------- ---~------** **-~- ------**  Repl**Sa~pleConc** StnfJConc . 

# • mq/L .. mg/L

· l · 0.614 0.**00~ 81**  2 0.660 0.00673 

### Moan: 0.667 0. 00680 

# - · - ·· 

# - S:lement: Hg Seq. No.: 57 S-le lepl



# • l 2 Heap: ID: R&FKI\T Saapleconc INJ/L

0.00630 0. 0062 7 0.00629 · StndConc :og/L 0 . 00322 0.00320 0.00321 Peak Uei9ht 0,0555 

## o.osu AS Peak Height 0.0260 0.0258 fiae Peak Stored 01:46:12 No 01:46:50 No**----- ~**  

# --- --- - Loc.: 53 TilDe 01:48:'18 0 1:t8 :57 Date: 2008-08-21 Peak Stored

No No

### ----MH--~·-------**---.------~---~----------~ ====** **----~--~-------------------~** Element: Ug Seq. No.: 58 AS Loc.: 54 Date: 2008-08 -2 1 S aoaple I D: CCB**-- ·"----** **----------- -----** **-- ----** **----- --------------** **~--~ --** **---- ----** **---------- ---** **--** Repl



# • 1 2 Mean:**Sa~ pl~Onc**  StndC o nc 11111/ L "9/L

0.00000 0.00000 0.00000 . 0.00000 0.00000 

## o.ooooo Peak Height 

## o.oooo o.oooo Tille P.eak , stored 01:50:25 " N o 

### ot': s1, OJ No 

# =- -- ------------------------------- Cleoo.ent : HIJ Seq. No.: 59 . AS 

### Loc.: 55 

### Date: 2008-08 -21 SIIIOple ID: ccy



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### VES 005638

# ().o1**~leuent:** Rg · Seq. No.: 60 

### Saaple ID: AF4626 - 0l 

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### Peak Time Peak



# • mq/ L mg/L 

### Reight Stored 1 

### O.OlSO 0 . 000 78 0 . 0063 02:21:02 No 2 .0 . 0709 0:00074 0.0060 . 02:21 · :40 No Mean: 0.0729 . 0.000 76

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### VES 005639

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### -- ....**--- ~**  Elament:**H~** Seq. No. : 61 

### S&mple ID : AF7342 -01 

### X 10 

### AS Loc.: 56. 

### Date; 2008 · 08 · 21 

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## 10 AS Loc . : 58 

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# ... Hq Sample ID: AF326S -Ol .206 .ppb .000 Se q: 1 04 '1 .206 1 4; 34:2 4 2 1 Aug 08 · Wgt . 50000 Vol 7.5000 H G**•• ===** **=== ===** **=====~== 2•** **•••••• ••••** **•~~--------•~• •=** **==== =a~•c•** **••••••••• ••••** **•••••••** ••• SMp le IO: A F3526 - 01 Se q: 10 48 . 14: 3 7:03 21 Aug 08 . IIG**02~** L ppb .000 .021 

# ___ , _____ . ,..,.. _,..,..,..,.. __ _ _ _ __ =--=---··---= ====== ··· - ------ · -·- 

# ... S&P!IP l G ID: AF4982-0 1 S eq: 1049 14 ; 39:41 21 Aug 08 HG Hg .0 0 6 L ppb .000 .006 

# ----·-------**~---** 

# __ _ ,. 

# ___ ... Suple I D: AF8098-0l soq: 1 05 0 14:42:21 21 Aug 08 HG Hq .0 11 L ppb .000 .011 

### • 

# ------- --- - ·=-===-- -**~** 

## ••• sampl411 1 0: AF8Q99 - 0 1 Seq: 1 051 1 4 :44:59 21 Au g OB HG Hg : 0 13 I.. ppb .OOQ . 013**------------- -======** **==-~ ~----···** **···--·· ·-** **-------- ====·** **·----------- ···-------** **·** 

## ••• 5&>\JP. le I,D: AFBl00-01 Seq: 10 52 II G Hg . 023 L p pb .000 .023 • • . • Sample ID:**A~10l-0l** Seq : 1053 1 4 ; ;o, 5 1 . 2 1 Aug 08 HG Hg . 021 · L ppb .000 .021 

### • •• • Sam p l e ID; AF951 3 - 04 Seq: 1054 14 :53:3 4 21 Aug 08 HG Hq .oos**J>~** .000 .008



### _____ ...__ _____ ___ _**~** 

### ...**~----· -=======:c** **--------·-** 

# ... Ug Samp le I D: AF9663 - 01 50.9 H ppb

.,. ._. Sa"f>le 10: A G

0 3 1 3 - 0l .073 L ppb .000

.ooo s eq: 50.9 1 0 55 14: 56:3 4 21**~uq** 08 Wgt .5 0000 V ol 7. 50 0 0 S e q: 1056 · 1 4:59 :1 6 21 Auq 08

. 073 HG H

G



# ..

VES 00565 1**~ine** 

### Cone . Units Fol der: . Aug 08a Protocol: 

### HG - L J08 * **POST -R UN REP<5RT ' .t.t-. SD/RSD . 1 ·2 3 4 5**~** Check St anda rd: 2 Li n · e F lag $Rev . Ck2: CCV 

### s eq: F ound**LO~** True Upits 1. 00 ' > ppb 10 5 7 • 15 : 01:55 21 Aug 08 SD/RSD Hq . 1 01. .000 

## • • • Check Standard: 1 · Ckl: \= C f3 Seq : 1058 15 : · 04 :**3~** 7 1 Aug 08 

### Line · F l ag Found**11an<;~e** ( f/- >. On i ts SD/RSD 

### Hg -.00 4 . 10 0 ppb .QOO . 

## ••• Sample I D :· Af326 1-01 Seq : 1059**15:0 7:** **~** 21 i'.uq 08 Hq .036 L ppb .000 .036 Page 1 999

RG HC



# - HG**--- -·** **··------- ------------~-----** **=~ ···** **-==~~ -·--·--··** **·-- ~~** **== c==** **=----~ ~-==**  

### ••• · s.,.p1 e t o:**P.F3262-0 ~.**  seq: 

### · 1o6s> 1 5: 10:04 2 1 Aug 

### o.a HG Hg .031 L ppb . 000 .03 1 

# ..**••• ·-------** **== e•** **•o -.** **== --** **•a ----** **--- =---** **==- =-** **•• ==** **--w•••• •••••** **•• •~** **•---• •===** **c=** 15il2:43 2 1 ' Aug Q8 

## • ••**Sa~ple** ID : AF3263-01

. O:iQ L ppb .000 Seq; 1061 .030**=~ ~==** **•••• -==** **·-- ···** **~~-~ ---~** **-== =-** **c=== ~.a** **== ===** **•• ====-** **c== ~•** **•• ••••••••** **=~ ••** **=** • • • Sample ID : ' AFl264-0'l S eq : 1 062 1 5:15: 23 2 1 Auq 08 Hg .03 4 L ppb .0 00 

### *•' Sampl e ID : AE3265-0 1 Hg .072 L ppb .. 000 : 

## ••• Sample ID : AF9663 - 01 44 .3 H ppb . 000 •• • Sainple 10: T RIP . llLK . .. . Hq - .184 L ppb .000

. . .... s , a.mp l e ID: blank Hq -. 032 L ppb .. 000 . 034 Seq: 1 063

. 072 Se q: 44.3 Seq:

- .184 1 064 1 06 5 ,Seq: 1 066**on** HG 

## • 15 :1-8:03 2 1 Au g 08 HG 15:20 : 44 . 21 

### Aug 08 HG 1 5:2'3:23 21 1\ug 08 . HG 15 : 26 . :40 2 1 Aug 0 8 fiG



### VES 005652'ro l dor: Auq· 08a**r~~oqol:** BG-L30 8 ***POST-R UN**RE PO** **RT~*~****age 199~** **~ine** Cone.**Un it~** **.** ' SD/RSD 1 2 3 . 4 . 5


## --- ----:---- -- -- .. -- --·--- - - - - --- , - .

--":"-: - -- - .. ----. -- - -'":'- - o. ----- - --------- -- - ---- -·- - ••• 8 g Sampl e ID :**TRI~** BLK

- . 049 L ppb .000 

### "'<fl • check S tandard : . 2 Ck2 £
· Li ne F l ag \ Re v . FO und · Hg · · 100. 

## i.oo CCV ·'f.rue

. l. 00

_,., ._ Ch ec k Standard:· 1 Ck l: CO B Line F l aq ro u nd Ranqe(+/ - ) Un its H

g . - .054 .100 pp)? 

## •** Chec k St andara: Line Fla g 'ReV " , H9 103 . 2 Ck2: Fo

:und 1.03 

### CCV 1'rue 1. 00 ••"' Ch eck Standard: 1 Ck l: CCB : t. lne ·' F lag POund Ranqe J+ / - ). ufli t s

H9 . - . 004 · . 100 .pp b***~*** · S ample 10 : SPIKE Seq: Units

ppb . . 106 7 10 68 1 5:31:59 2 1 Aug . 08 .

. SD/ RS O



### . . ooo seq : i069 SO / RSO

.000 15 :34:3 7 21 Au g 08 Seq: 1 0 70 15 :5 8 :56 2 1 Aug 08 Uni( s

pp b SD / RSD seq: 1071 S D/RSD

.000 Seq: 107Z 

## . ooo 1 6:0 1 :34 2 1 Aug 08 16:0 4:21 21 Aug 0 8 . W$11592563 1.40 pp)>**~~,~,** • Samp l e tO: BLAN K .028 L ppb 

## :ooo . L . 4o



## . ooo Seq : 10 73

. 028 16:07 :02 21 Aug 08 HG HG IIG 

### • HG HG I!G HG**== ••** **~• ==** **•- ~--=•-=** **=~=-z=,. ..,** **•••-• •-•** **"""'" .0.** **== -•**  

### "* Sample rD : H1'RX S P K Se q : 10 74**16 0~:40** **.** 21 Au g 0 8 HG l .2 5 ppb .0 00 1.2 5**.q~ -~**  ' 

### . 

### •**•---•----• =~••** **••--•-- ~•** **••--= =..,** **•••~•·=--~·-----~·••~•~== =-** **•.-•---= =**  ••• Sa 11 p l e 10: A f'22 63-08! Seq: 1 015 1 6:12:29 2 1 A ug 08 I!G· 

### f'41)>. H g .020 L ppb . 000 .020**••••~--** ..**~•••-- ••** **•• ••** **••••••••••••-•••••••• •••** **c• ===** **=:. ••** **•••••--•~ =-•••••**  ••• Sample ID : Af'22 6 3-08 Seq: 1076 16: 1 5: 09 Z l Au9 08 HG

. . 024 L ppb . 000



## · * •• Samp le ID: AF2254 - 08 .040 L ppb . 00 0 . 024 Seq: . 10 7 .7

. 0 4 0 16:1 8: 0 2 21 Au g 

### OS BG**••••••-•·-·-=--•• '1"** **•••- ,.·-•-•--** **'"'"=n=w ===-** **=--• ---=** **•~••••....,•• --** 



### VES 005653**ot ·**  . . •**--- ~'** **~** Folder: Aug**08~** Protocol:**HG L_JO~** **P~qe** 1999 • • "- P0$1" - RUW REPORT • • . • 

### Line Cone . lJnits 

### SD/RSO 1 2 3 4 5**--- --** **-- --** **-- ------~----** **---- -------~--** **-- --** **--- ----** **------ -------** **--------** 

### • •• Sample I D : AF2255 . ·08

. 032 L p p b .000 S<>q: .032 101 8 16 : 21:02 21 Aug 08 HG**••---••••••----•••••••••••••••• ••** **••~--- ~------** **-~ •••••---•~=Q•Da** **•••m.-._•~·-- ••**  "'**Sa~> le**  I D : A F 2251·0 8 Se q : 1 0 7 9 16 : 2 3: 40 21 A ug 08 I I G 

# f\Y Hg . 070 L ppb


## • • • Sample I D : AF 353 1 - 04 Hg 

### . 037 L ppb .000
.000 .070

. S<tq: .037 1080 !.J'**~:;** 16:26:19 21 Aug 08 HG**---~ ~-------·-----~·------~---** **· -==** **··· ·-** **-- ---**  

## •• • Saaple ID: . AF4402 -0 4 llq .040 L ppb**~· ·**  Samp l e ID : Ar6345 - 08**~,** Hg 

### . OSl t. ppb


## • • • Samp l e to :**f6 78** **8·0~** Hq :2 72 p p b .000 .000 .000 · Seq: .0 40 Seq: . 1082 • 051**S~q .**  1 083 .272 16:28 ' :58 21 Aug 08 

### OG
1 6 : 38:30 21 Aug 08 HG 1 6 : 41:1 4 21 A uq 08 

### HG

# ~**~-~ -~**  

# -- - - - ---- --- -------- - -

-- =-·--.-G=-·- .. ··---- ... =

........ Sample 1 0 : A"f 733 3**~t** Seq: ; 1084 · 16 : 4 4 :0 4 21 Aug 08 

## Wqt .50000 Vol 7.5000 llg 45.8 . H ppb .000



# .... . . Samp l• ID: AF733 3 - 01 Hg 18.0 

## _.., •.**o~ g-**  

# . .. SaJ11Ple IO: bl k

- .081 L ppb .000


# . .. Sam pl e ID : A F733 4 -0l Hg 2.83 ppb . 000 45 . 8 Seq: Seq:

-. 081 

### seq: 2 . 83 1085 17:12:1 9 21 Aug**~8 ~**  .SO OOO Vol 1 .50 00 1086 17 : 15:03 21 Au g 08 Wgt . 50000 v

_ ol 7. 

### sooo IJG

1 087 1 7: 11: 41 

### '-1 1 .. 2 1 

### Aug 08 HG 

### v

..t.. ::.**~** 

# -> 4'2. • 

## A s- .**·~·=•••••••~ ====** **~=~••••--= =~~••----·--~** **===~••••• •~** **--~a~· ----•** 



### VES 005654Folde r : Aug 08a ·**~· ·**  Protoc ol: HG - L J 08**·~*****POST-RUN** 

### REPORT*•• Pago 199 . 9 Li · ne 

### Cone . 1,J nit s S.D/RSD l 2 · 3 

# --,..-- -------- - --- ----- - ----- . --- -- - --- -- -- - --- --- -- ---- · -- - ---- --..- -- - -- --- --- -- - - 

# . .. Hg 

## •• • $• . mp1e I D: b1 k .

- . • 0 1 6 L ' p p b . 00 0 . s e q : 1008 · 17:20:20 21 Aug 08 RG**01~** · . .. w 17 : 23:04 21 A ug 0 8 RG 

### '-'1\- " .,. ....- 

## v• io ..**~ ·~** **~** " Hg 2.67· ppb .000 2.91 · · · • .**Samp~e** I D : l>.F 7335 - 01 S e q: · ' 19 8 9 

# o ·**v.,.~ ~·**  0 

# s:- · . . .**J)~** ,. ., . 't>O 

## uo- .**--;, o~** **:: s::;~=~~;-;~-** **---- A·** **····· -·** **~~~;~ ==~;** **7; ~~~~:;** **-- =-**  .0 00 - . 013 

### . 

## · . · • . 

### •**wa••••••••--------~.-e--• =--** **--•--••••-----·-------..-•••--•-- a=~=o=** **•-= •**  

### . 

## . .**~~** S amp l e**~D:** AF 1336-0l not in .0

. 00 Seq: 1091 11 : .2 9:0 9 2 1 Aug 08 R G order w ith ws Wgt . SOOOO . Vo1 7,50QO 6. :

8 4 · . .

### ·~ ..

### :;r~ 

# · · · · .l> L

### ~ "" H

g 6.84 H ppb 

### -"' ., • ., .. b8'" .**~** 

### · * ** Check Standard : Line F'lag \Rev. ilg 10 3 . 2 Ck2,: r"ound

1.0 . 3 CCV Tru e 1.00 . 

# . .. Line Hq Check Standa r d: 1 C kl: ccs Flag F ou n d**Ran e{+/~)**  Units

. . 004 . .10 0 . pp b 

## ••• Sample !0 : A F 7 338 - 61 1 .23 p p b .000

• • • S am p le ID :**~~73~? 01**  S.e<J; 1 0 9 2 . 17: 31 ;50 2 1 . 1\ug 08 HG**U~its** SD / RSD ppb . 0 00 Soq . r 10 9 3 SO / RS D



## .oo o · Seq : 1094 Seq: 1 095 1. 23 17:34:28 2 1 A ug 08 1 7:38 : 00 21 Aug 08 W

gt . 50000 Vol 7.5000

11:40 : 55 2 1 A ug 08 il gt . 5 0009 Vo l 7.5000 HG RG
HG Seq: ! 096 17:43:36 21 Aug 

## oe HG Rgt • 50uo o · Vo l 1 · . 

## s o oo ..

••• · Salllple !D: AF7J40 · 01 Seq : 10 97 , 17:46: IS 2 1 Aug 08 H G Wgt .50000 Vql 7 . 5000 Hq 6.0 0 H pp b . 0 0 0 6 .0 0 .._ ,

. 0 0 

# c.. . .....**~,.** 0 ' ., ..**~-** •

## ----~**=- =====---** **=== ===** **=--== -~** **c:==--==~ ====** **ft ·--** **~~ ··---~** **== ~=** **=== ~..---·~** **====** 

# i

V ES 005655L i n e Cop e. Unit:s Fold e r : · Aug :_ O B a . P ro toco l: · H G -L JOB • w

* PO S T-RUN**~E P0** **•** SO/RSO 1 2 3 4 5



# --- - ----- -: - . - -- - -- - - ------- - - - :- ..**-- ---** **-- --** **---** 

# .. ----- -- - -- - - --- - --- - , -- - -- ---- • • • S a JIPle ID: AF7 3 4 1 - 0 1 Hg 9 . 1 6 H ppb**~o·** 

## o o'\L 

## , oo o 9 . 1 6 10 98 17: 4 8: 5 4 w

gt . 

## sn oo o . f ?; . : 2 1 Au g 0 8**~: HG**  V

o l 1 . 5,000 · · ;!) \.. ::

### oo**~ '•--** **===== ====-======** **== ===** **.w &:** **== •••** **=== ~===** **--• ••** **••••• ~•** **vs --~** **~~ ~•••** **:=**

..... _. S arf!P l e · I O: bl. k . S eq: H g -. 0 4 4 

## L ppb . QO O -. 044**~~** S ampl e ID : AF 73 4 5 - 0 l s eq : 10 99
11 00 · 1 7:5 1 : 3 3 .21 A u g 08
1 7 ; 5 4 :11 2 1 A uq 0 8 W

g t 1 .0000 Vol 7500 0 0 

## .. H<i '
H

G Hg 987 000 H ppb . 0 00 98 7000 ;< · • · 2 1:; . .

## ->**""'~,_** 

# .**~L ~** **f~** 

# . ·**~- ~----.-------•-••••••--•** **----•wo• ••---..-** **•• ==** **====== =aa**  .**·· •·** **·~·•** * ** . S amp l e . ID : . blk S eq: 1 1 Q l .' 17 : 5 6:52 2 1 A uq

### OS**;** Hg -,00 7 L ppb . 000 -; .007 

# m'<f.

. . . .**ff.:;V;.** 

## .**--••• ••** **••• ···** **-== =n-====** **•~ ====** **•---- •-.--** **--=-• ===** **-=- ~** ***••••••·** 

### ** * S ample ! D: A F7 3 46- 0 l . Se q: 1102 17 : 59 :42 2 1 A u g 08 

## \r,;, J:! j H

gt 1. 00 00' V o l 7 SOOO O?l Hg 66 7 00 0 H ppb . 0 00 6670 00 . 

### .J:> 1**·** ; ·

# -?-~.Je±-.:**==.:. =**  

# ....**--=-- ====**  ... 

# · --=--= -----·Q .........**~= =-** **;;3:_ £_:**  • •• Samp l e r' D: b l k S eqi 11 03 1 S :02 : 22 21 A u g 08**·~ ;,.:** **n~** 

### · t ,; :·, .o { '

· . < Hg
- . 0 0 4 , 

### L P P

b . . 0 0 0 -. 0 0 4 

### •

;;.,., S amp l e I D: b l k Seq: 11 0 5 18:07: 44 21 Aug 08 . RG 

### H

g . 001 L p pb .000 . 0 0 1


### . J> 

## •• • S am pl e I D: af7339 · 01 .S e q : 11 0 6 H G 1 8: 13: 0 2 21 Au g 08 Wg t 1 .0 0 00 Vo l 22 5 . 0 0 Hg 1 4 1. H p p b . 000 1 4 1. 

### !) L. :; O O Z, .?...$"'

### ~



## - "o· I & ,L ·

. .. •••• ••**~ ••** **•---•••.-•-----•••• --••** **•••~ ••** **=~ =-** **•• ••** **••••• a&** **==-=a --•** **•••-** 

## ••• Sam p l e 1 0 : s p i k e Hg 1. 34 ppb



# L

_ _ --- --'- - · Se q: 115 11 5 9 276 8



## . o

o

o 1.3 4 11 07 1 8: 18 :4 3 2 1 ll u g 08 H G



### VES 005656

# . .. ' Line Cone. Units Folder: Auq

_ 0 8a Protocol: HG-L J08**•~*****POST-RUN REP0aT•~~**  SO/RSQ 1 , 2 3 4 • 

# , Page 199? 

# i 5**~-------------------------------- ---** **------ ----** **-- --** **-~-- -----** **~- ---** **----- --**  

## ••* Check Standard: 2 tk2 : CCV Li n& Flaq \;ftC'( . ro t,tnd. 'Erue Hg . 113 . 1. 13 1 . 00 . • .,. Check Standard : 1 Ckl: CCB Line Fla9 Found Ranqe(+/ - } Onits Hg .001 . 100 ppb Seq: Un i ts

ppb 11 08· 1 8:21:22 21 Aug 08 SD/RSD Seq . : 11 0 9 S D/RSD

.00 0 .060**18:2~:00** 21 Aug 08 BG HG



### VES 005657

### . 

## . 

# Method 6010**~Test** 

# Method for Total

) 

# Metals by 

# ICP

Maxxam Analytics Inc. 6740 CatnpobeUo R d . Mississauga, Ontario, Canada 

### L 5N2L8 

## 1-800-668-0639 

## www.maxxamana!ytics . com I

VES 00 5 658

## Unique Calibration

## St~nidards 1.0. table 

## for ICP-5 (Axial) ! (Standards p r epared 

## in 2% HN03)



## .. . . Generati . D . Unique !D.**BLA~** /ICS/ CCB ICP-WC-0834 STO,A ICP-WC.OS32



### .. 

## . . ,**STO·~** ICP c WC-0831 CAl·16KNa· ICP · WC-0833 

### HH< n

a ICP·W0 · 08$ ICV /CCV I CP - WQ.0854

. _. . ICS'AB ICP. - WQ · 0841 CRJ ICP·If/0 ·08 52 . 

## .. UBuffer ICP · WQ.08S3

Analvstln i lials : 

# fa oa1e : ·**zpot,/ ~;**  ;Z

( 

# . .. M8>0<8m Analytics Inc.**CAMFC~7911**



### . Page · . 1 

### ol1



### VE S 0 0 5659

### Auto9ampler Report Table : AUG21A**0~/.2..1/08** 

### 11:05:06 PM Table 

## Name: AUG21A Sample**Positions: 2/~92**  

### Ripse Stat i on location.' is : __ Racks "-- . . Autosampler Type: 

### TYPE TJA . 

## QC Positions: 13/19 · 

## B Sets : 1**~ack** - 1 , ·**pos ·** **-~ :**  

### page 1

Rack II 

### TyPe**\!!lag~** 

### #¥>os Left Analyse . s/Pos



# ... .. 

# - .. 

# -- ------ ---------- -- - - 

# ------------ 1 Aux. · (L) 

### Ra . ck



## · a sample 3 sample 4 

### Sample 5 SamPle

- -- · Sal!'ple Sets

· setll . · Type ( l 6mm) ( l 6mml . (16mm) (}6llll1) Prepare?**STD/QCjB~K** 

### Samples Samples Samples Samples Description 

# ----- -- - - ............. ........ .... • 1 .3 

### ?0 .

· 0 . 1 0 

### 1 0 l 12 l Method #¥>os Rackll



# ------ - ------------- --- - ---- 1 

### Normal No m?-=a m 

## . . PSC34 180 2

--- Preparation I nfo**-~** 

### Set# Up take Upt , akell2 Final t>il . Factor No Samples**Prepar~cj.** 

### Rae)< Ill Pos Row Col Samp l e Name Set;: · ll II Used Type

.. ..: 

## .. 

# - - - - - -- - -- - - ----- ------ 

# --- - -- - ----- 1 

### l 1 NONE 

### - NA- ' 1 Standard 2 1 

### 2 knahi 15 · -NA- 1 Standard 3 1 

### · 3 STD - A- 

### -NA- 1 

### Standard 4 1 4 

### STD-'B -NA - 1 St;:andard 5 1 

### 5 CAL - BLK - NA - 1 Standard 6 1 6 

### HCL -NA- 

### 1 · QC Standard

· t'T' : • . 1'9 

### Not Us ed · ) Rack 112 Poe 

### Row Col S ample Name Set II 

### #Used Type**-- --** **----~-------- -------** **-~** 

### 1 l 1 ICVAX 1 . . -NA- 

### Sample 2 1 2 ICB 

### 1 -NA- sample 3 1 

### 3 . CRI 1 

### -NA- Sample 4 1 4 . ICSJ\BAX 1 -NA - sample . , 5 1 5 HI . KNA . 1. 

### - NA- Sample

. 6 

### 1 6 1 . 591852 :AF734l :DUP 1 -NA- Sample

. 7 1 7**15~1 852**  

### ;AF73 4 1: 1000 1 - NA- sampie

. 8 1 

### 8 . 1591852 : AF7339: 1000 1 -NA- . Sample 9 1 . 9 1591852:AF734!): 1000 1 - NA - Sample 10 1 10 . CCV 1 - NA - Sample ll 

### 1 ll 

### CCB 1 

### - NA- Sample 12 1 1 2 1592280:BLANK:100 · 1 - NA- Sample 13. 

# :t 1 1S92280:RBFMAT:100 1 

### -NA - Sample 14 2 2 15 92280 :MTRX SPK :'98 l 

### - NA - Sample 15 2 3 . 1 592280:AG2290:D U P 1 -NA - 

### Sample StartPos



# -- ------ 1



### VES 005660'"'- "''.

## --~ : :'



# . . 

# .
. 

# ' AutoSampler Report Table: AUG21A 

## ., 08/21/0!l**11 05:0~**  

### PM 

### page 3 "· · ..-! 

### Rack #3 . • .**~.r** 

# ..**~** 

### Poe Rov col Sample Name**~** 

### Set # 

### # U sed Type**:~** 

## __ _ _

____ __ _________ , .



# -- -- -----·-- .... Sample 16 2 

### 4 159105S:AD6033:600

# ~ 1 

### - NA - 

# ... 17 2 5 

### CCV 

## ·•: 1 -NA - Sami>-le 18 2 

### 6 CCB 

# . 

# " 1 -NA- Sample 19 2 

### 7 1589843:BLANK:SO 1 - NA - Sample 20 2 

### 8 1589843:RBAGBL:50 1 -NA- 

### Sample 21 2 9 

### 1 589843:SPIKS:DUP 1 -$ - 

### Sait!ple 22 2 1,0 

### l68984-3: SPIKB: 50 W< 

### 1 

### - NA -**Samp.l~** 

### 23 2 11**~5~9843:AB0772:50** 

## , , 1**m-** 

### Sampl.e a_4 2 

### 12 15 89843:AB0773:50 · 

## : :- 1 

### - NA - Samp

_ le

- 25 3 

### 1 15898 4 3 :AB0774 

# , · so 

# ' 1 - NA- Satilple ,. 26 3 2 

### 1589843 ;Ml0775: 50 . 

# .. 1 

### ·NA- sample · 27 j 3 

### 1589843 :AB0716 : ' 50**;.·~.** 1 

### - NA - Sample -: 

### :28 3 4 

### 1S89.843 :AB0717 , · 5Q**t~.** 

### 1 

### - NA-**Samp~ e**  

## ' 29 3 

### 5**l5898~3:AB0778:50 .~** **·** 

### l


### - NA- Samp ie 

## .. 

# , 30 3 6 

### 1 5898 43:1\2 07 79:50 

# ·"'· i 

### - NA - Sampl(O 'i 

# - S ample 

# ·. 31 3 7 

### CCV 

# . . l . -NA · 32 3 8 

### CCB :t· 

### 1 

### - NA- Samp le**.·~** 

### 33 3 9 

### 15898 43, A. Bono : · so ;, , 

### 1- 

### : NA- Sample < 

### 34 3 

### 10 , 1589843 :AB0 . 70 1: SO , 

# . · { 1 · NA- Sampte 35 3 11 

### l589843 ' :AE0782: 50 :•;. , . 

### 1 · tiA- Sample 36 3 

### 12 1589843:ABo7oJ:so ·:. :- 

### 1 

### - NA-**Sampl~** 

### 37 4 

### 1 1 589 . 843 :AB C l1S4: s . o**·~** 

### 1 

### - NA- sample ) 8 4 2 

### 1589813: AE 0785 :50 ·: : 

### 1 -NA - flample 39 4 3**1589~43:AE0786:SO** 

### 1**NA ~**  

### Samp le 40 4 4 

### 1589843:AE0787:50 .· ;. 

### 1 

### -NA- SaJl1Ple · 4t 4 

### 5 1 S 89843:ABQ788:50 ... 

### 1 - NA- Sample 42 4 

### 6 1589843:AB0789:50 1 

### - NA- Sampl e 43 4 

### 7 158984):AB0790:50 1 

### - NA - Sample · 44 4 

### 8 l5898 43:A.E0791:50 1 

### -NA- Sa'!'Ple 45 4 

### 9 

### CCV 1 

### - NA- Sample 46 4 

### 10 CCB 1 

### -NA - Sample

. 47 4 1l 

### 1589557:8LANK: 1 00 l 

### - NA - Samp l e •• 4

• 8 4 

### 12 :' '' l589SS7 '!' REPMAT: 102 .. . 1 . · -NA" Samp l:e

. Rack #4

Pos Row Col Sample Name Set 

# • II Us e d Type



# ---------- ------- -- - ---- 4------ - 1 

### 1 1 

### l589557:MTRX SPK:96 1 

### -NA - sarnpie 2 l. 

### 2 1589557:AP 1 858:DUP 1 

### - NA - SalliPle 3 l. 

### 3 1589557:AF 4 858:100 1 

### - NA- SalliP le 4 

### 1 4**1589557:~F4747:104** l 

### -NA - . Sample 5 1 

### 5**1589557:~ F4748** **:96** 

### 1 

### - NA- Saniple . 6 1 6 1589SS1: AP4749: 102 1 

### -NA- San:ple 7 l. 

### 7**1589557: AF475** **6:9~** 

### l 

### · - NA - Sample 8 

### 1 

### 8 l589557:AF4835:100 l 

### -NA - SaJl1P1.e 9 

### 1 9 lS89557:AF4837:98 1 

### - NA - Sample 10 1 

### 10 l589557 :A.F4838:96 l 

### -NA - Sample 11 

### 1 11 CCV 1 

### . -NA- Sample 12 1 

### 12 CCB 1 

### -NA- Sanj>le 1 3 2 

### 1 1589557:AF484l:l04 l 

### -NA- Sample 14 2 

### 2 l5B9557: AF1 8 42:96 l 

### -NA- Sample 15 2 

### 3 . l589557:AF 4 846:96 1 - N A. - Samp,le



### VES 005662

### AutoS ampler Report Table: AUG2 , 1A 08/21/08 11:05:06 PM page 4 Rack #4 Pos 

### Row Col Sample Name Set 

### # lfl! a ed Type**------- -------~-** **--** 

## ----- 

# ----------- -

16 2 4 

### l589557:AF4847:102 1 -Nih 

### Sample 17 2 

### 5 1589551:AF4848:98 l 

### -NA- SaJ!lPle 18 2 

### 6 1589557:AF4853:96 1 

### -!<A - Sample 19 2 

### 7 1589557:AP4855:100 1 

### -NA- Sample 20 2 

### 8 1589557:AF4860:98 1 -NA- 

### Sample

. 21 2 9 

### 1589567:AF4863:104 1 

### - NA- Sample

22 , 2 

### 10 l589557:AF4877:98 1 -NA - 

### Sample . 23 2 11 

### l589557:AF4884:96 l "NA - 

### Sample 24 2 

### 12 l589557:AF4885:99 1 

### -NA- Sample 25 _ 3 

### 1 1589557:REPMAT:102 1 -NA- 

### Sample 2 ' 6 3 

### 2 CCV 1 -NA - 

### Sample 27 3 

### 3 

### , CCB 1**NA ~**  

### SaiiJPle 28 3 4 

### 1590,!)92: BL/INK: 100 l -NA- 

### SaJ!lPle 29 3 

### 5 1590092:REPMAT:102 l 

### , -NA - Samp1e 30 3 

### 6**l'590092iMT~ SPK:~B**  

### 1**~W\** 

### Sample 31 3 

### 7**15900~2:AF4769:0UP.** 1 

### - NA-**~ample** 

### 32 3 

### 8 1590092:AF 4 7G0:99 1 

### - NA- Sample 33 3 

### 9 159009;2 :AF4743': 102 . 1 - NA7 Sample 34 3 

### 10 1590092:AF4745:l04 1 

## -NA - Sample 

### 3:> 3 ll 

### 1590 , 092 :AF4752: 9 . 8 1 

### -NA - Sample 

### 36 3 

### 12 1 590092 :AF4753:98 1 -NA- Sample 3 -

7 ' 4 

### 1 1590092:AF4754i98 1 

### -NA- . Sample 39 4 

### 2 1590092 :'AF4755: 98 l - N A - S!>RIP.le 39 4 

### 3 CCV ' l - NA- Sample 40 4 4**C~** 

### 1 -N A - Sample 41 4 

### 5 1590092:AF4?70:98 l 

### -NA - Sample 42 4 

### 6 1590092:AF4771:102 l -NA - 

### Sample 43 4 

### 7 1590092:AF4772:102 l · N A - Sample 44 4 8 

### 1590092:A F477 3:96 l -NA- Sample 

### 45 4 

### 9 1590092:AF4778:102 1 -NA - Sample 46 4 

### 10 1590092:AF4801:102 1 -NA-' Sample 47 4 11 

### 1590092:AF4805:96 l - NA- Sample 48 4 

### 12 l590cr92:AF48 19 :98 l - NA- San'Iple Rack liS 

### Pos Row 

### Col Sample Name Set II #Used Type



# ----- - ----- --- -- -- -- - - - - -- -- --- - 1 1 1 1590092:AP 4 821:96 1 - NA - Sample 2 l 

### 2 1590092:AP4826:100 l - NA- 

### Sample 3 1 

### 3 

### l590092:AP4862:100 1 - NA- 

### Sample 4 

### 1 4 l590092:RBPMAT:102 1 -NA- 

### Sami>le 5 l 

### 5 CCV 

### 1 

### -NA - Sample 6 1 6 

### CCB l -NA -**sa~le** 

### 7 1 7 WASH1 1 -NA- 

### Sample 8 1 8 WASH2 l -NA- Sample 9 1 9 WJ\SH3 1 -NA- 

### Sample 10 1 

### 10 1592280:REFMAT:1000 1 

### -NA - Sample ll 1 11 

### l592280:AE5685:980 1 

### - NA- sample 12 1 12 1 5922 80:AE5685:9800 1 -NA - 

### sample 13 2 1 

### 1592280:AP4626:980 1 -NA - Sample 14 2 2 

### 1592280:AP4627:960 1 -NA- 

### Sample 15 2 3 

### CCV 1 

### -NA - Sample



### VES 0 0 5 6 6 3

### Ad coS 

# all\' leo'**~eport** 

### 'l'able: AUG21A Q8/21/08 11:05:06 

### PM page 5 

### Rack 115 Pos Rov 

### Col 

### S a mp le Nam e Set ll 

### #Used Type . ·



# --- - - -- - - ---- --- - -- - . 

# - - -- - ---- · - . - --- - --

. 1 6 2 4 

## ccs · . l -NA- 

### sample 17 2 

### 5 ( 

### emp.ty" ) 

### 1 · -NA - · - NA

### 18 2 6 ( 

### empty ) 

### l · NA- -NA 

### 19 

## 2 7 

### " < 

### empty ) 

### 1 

### -NA - -NA20 2 8 ( 

### emp t y ) 

### 1 -NA -**-NA~** 

### 21 2 

### 9 ( 

### empty ) 

### 1 

### -NA:- : NA

### 22 

### 2 10 ( 

### empty ) 

### 1 -NA- -NA

### 23 2 11 ( 

### empty ) 1 

### -NA- -NA - 24 2 

### 1 2 ( 

### empty ) 1 

### - N A- 

### -NA - 25 ) 1 ( 

### empty ) 

### 1 

### -NA - 

# - NA26 3 

### 2 ( 

### empty**~** 1 

### -NA - · N A- 

## 27 3 

### 3 ( 

### e mpty ) 

### . 1 

### -NA- ·NA ; 28 . 3 4 ( 

### empty l 1 -NA-**-NA~** 

### 29 3 

### 5 ( 

### e mpty ) 

### 1 

### -NA -**W>.** 

### 30 ) • 

### q (**~tY** ) 1**NA .**  

### ·NA · - 31- 3 7 ( 

### empty ) 1 

### • NA· - · NA- · ;12 ) 

### 8 ( 

### empty ) 

### 1 

### -NA - CNA-**~3** ) 9 ( 

### emp t y . 

## l l 

### -NA - -NA-

. 3 . 4 ) 

### 10**~** 

### empty ) 

### 1 " 

### cNA -**-NA~**



### 35 3 11 . ( 

### empty ) . 1 -NA- 

### -NA· 36 3 

### 12 ( 

### emp t y ) 

### 1 

### -NA - - NA- (37 ..• 48 .**~t** 

### Used)

· . •

VES 005664

### 1479 PrQfile line : 

# As**189.~(2** 

### Peak Position : . .**02~993** 

### P

eak Intensity; 13 45.7 . Peak Width , · I '} .16961 ll Hew Spec. Shift at ; , 0

0 

# ., 

# ..**~** v 

# ., c 

# ..

-31 0**~pectnm** 

### Shifter Posit . ion I . . 

### 31

VES 005665

## , .

. AI).alysis Report QC Sta!ldard DS/21/08 · 12 : 38:5j PM page 1

· Method: PSC34**sampl ~**  Name : 

### HCL Operat . or: 

### gbu RUn . Time: 08/-21/08 12 :33-:32 commen t : M\:>de: CONC Cor.r, Factor; 1

Elem 

### 1\g A l · 

### As B . Ba ' Be Bi units p pm 

### PPJ!I ppm ppm ppm ppm ppnl Avge . 0007 .0184 . 0171 .0011 .0 0038 . 00038
- . 0923 #1 . 0025 . 0374 , 0326 ,0034 . 0 . 0052 . 00944 . 0 1 20 #2 . 0000
- . 0016 . Ol4 1 . 0003 .OOQ22 . .00030**-.0~0 0** **-#~** - .000;3 . 0 195 .0044 - . 0005 . 00039 . 00040 - . 0089 E l em . Ca 

### Cd co Cr 

### cu Fe 

### K Un i ts ppm ppm ppm 

### PP'!I . ppm pp m ppm Avge .0392 . ooooo . 0027 . 0000 .0001 • 0054 -.1077 . # 1 .0417 . 00011 . 0023 .00 1 9 . 00'13 .0063 - . 0250 li2 '**.0~64** - . 000 . 05 . \)011 - . 00 . 0 . 8 -. oof9 .0041 - . 0963 #3 . 0396 - . 0 . 0006 . . 0048 - . 0010 .0008 ,0057 - . 2017 Elem Mg Mn · Mo 

### Na Ni p 220J/1 Un it s ppm ppm ppm ppm ppm ppm . ppin Avg e . 02 9 1 -. 0000 . 5 . . 0001 .0471 . . 0022 .0158 -.0170 #1 -9262 . 00029 . 0015 . 0483' . 0032 .0 1 61**~** ;01 : 57 

## #2 . 0204
- · . 00018 -.0009 . 0445 , 003 1 . 0 . 063 -.0119 #3 . . 0408 - .00027 - . 0005 . 0486 . 0002 .0248 - .0236 Elem 2203/2 

## s Sb 1960/1 19 6 0/2 Si 

### Pb Units ppm ppm ppm ppm p pm ppm ppm ; Avg e . 00 7 8 .00 58 - . 00 1 4 -. 0169 . 014 4 . 0489 - .0005 # 1 .0082 .028 . 1 .0 092 -. 0169 . 0153 .05 17 . 0002 112 .00 14 - . 0137 -.0044 -. 014 5 .012 1 .0 4 4 8 -.0030 #3 .0138 .0031 - .0091 - . 0191 . 0157 . 0 5 01 . 0013 Ele m 

### Se 

### S.n Sr Ti Tl 

## u v Units ppm pp m ppm ppm ppm ppm ppm Avge .0040 . 0007 , 00022 . 00187 .0045 .0409 .0029 # 1 .0046 .003 7 .00020 . 00246 . 0027 .1488 .' 0036 # 2 .0033 - · . 0013 . 00017 . 00108 . 0049 -. 0 093 . . 002 ' 7 #3 . 0041 -. 0002 . 00028 . 00206 . 0059 -. 0 169 . 0025 Elem '[ 213Zn Zn Zr Unit!' pp m . ppm ppm ppm }\vge 37.43 . 0 . 010 .0025 . 0027 #1 . 3 7 . 20 .0013 .0026 .003 0 #2 37.49 . 0006 .0014 . 0019 #3 37.58 . 0011 . 0036 . 0033



### VE S 005666

### Standardization R pt . 

### . 

# . - 08 / 21/08 12 . : .

47:01 PM page 1 Method: PSC34 Standard: CAL·BLK' / Run T ime: OS/21/08 12:41:30

Ble m Ag Al As 

### B 

### B a . Be B i Avge - . 0346 1.137**,0323** 

### .1219 . . 01566 - . 15459 :-0466 til - • . 1369 1.108 - . 0870 . 076 . 0 -.00500 -.1739J. •.1169

. 112 .0030 1.17 . 0 - . 0.230 , l. 449 .03 1 98 - .13593 - . 0470 H3 

### . 0300 1.133 . 0130 . 14<19 .01999 - .15392 .0240 Elem Ca Cd Co 

### Cr 

### cu Fe Fe · Avge .0120 ,02066 - . 0573 - . 0090 . 4518 - · . 0170 . .0330 til .0030 -.**093 9~**  

### - .0750 - . . 0520 . .4708 -.0820 - . 0140 tl2 . 0180 . 01199 - .0370 '. .obo .4128 .0300 .0690 tl3 . • 015() . !1.4393 - . . 0600 

## :ouo .4718 .00 1 9 . OHO Ble111 K lolg 

### M g Mn 

### Mo Na N i**~vge 6024**  

### - , 0133 . 020()' 

## . qoop . 

## -.op:p 22 . 61 

## . . o

· o

. Jo Il l - · . 7096 -.0780 -. 00 1 0 . - . 01299 - . 1;1. 5 9 21 . 68 - . 0590 11 2 - . 5887 .0080 .0630 . 00600 . . . 0930 23 . 1 9 . 0010 113 - . 50 . 87 · .0309 - . 002 ' 0 .00900 . 0190 22 · •. 95 .0670 Eiem p 

### 2203/.l 2203/2 

# s Sb 1960/1 1960/2 Avge .28 4 9 . 3155 -. 0630 .2'795 .. 0010 . - . 0633 .05 4 6 Ill .2769 . 7306 -.1279 . 2539 - .1669 .05 0 0 -. 0440 112 .2969 - . 3578 .1079 . 3028 .0560 - - . 1 859 . 1469 113 .2809 . 5737
- .1689 . 2819 .113 9 - .0540 . . 0610 Elem . Si Sn Sr Ti Tl 

## u · v Avge . 0856
- .0140 .05197 • . 01033 - . 0720 

### :o21o
- .0020 Il l -.0560
- . 04 5 0 . 04798
- . 07296 - . 0920 - .1199 - .0450 112 . 1859
- . 0310 .' 05597 . 02099 - . 0430 . 0760 . 0360


# - ' · 113 ' .1269 ' . · o3 a o 

### : Of? ' I 9'7 ' • . : 0:!()99 ' 

### .. -. 0'810 ' .**:· ro** **~9** 

## · :· oo:Jo B l em 213Zn 

## zn Zr Avge - .0080 - . 0386 -1 . 384 #1 -. 0180 - .0520 -1.487 112 .0020
- .()200 - 1.296 113 -. 0080 .- .0440 . - l. 

### 369



### V E S 005667• · 'r.<' Standafdization Rpt. 08/21/0

_ 8 12: 5;1.: 48 

### PM page 1 Method: PSC34 Standard: · STD-B . 

### / Run Time: 08/21/08 12:.7:05

Elem Ag Fe Mg 

### Mq . p 

## s . Sb**Avg~ .**  11.74 31.66**~.090** 18.62 ·. 18 . 43 8.393 4 ". 803 #1 11.73 31. 70 . 4.066 18.33 .1 8.50 8.371 4. 554 

### #2 11.72 31. ' 53 . 3,9 . 95 18.6 ' 3 18 .2 1 . 8.363 4 : 867 

### #13 11 . 77 31 . 71 4 .2lQ 18.90 18.5 7 8.447 4 . 989 Elem Si 

# sn Ti 213Zn 

### Zr Avge 14.10 1 0.90 145.15 4. 922 171.5 

### Ill 14.14**~0.86** 144.99 4.912 171.3 

### 112 13.SI8 10 , 84 144.61 4.911 170.8 

### 113 14.19 11. .01 145.84 4. 945 112.4



### VES 005668**~:r ·**  

# . , , :: .. . . Standardization

. 

# . Rep9rt 08/21/08 12:S1!4Q**~** 

### page 1 Method; PSC34 Slope • Conc ( SIR)/IR Element W ave len High s t d Lo w std · Slope · , Y - int e rcept Date ; Standardized ' Ag 3'28 .. 068. STO - B CAL-BLK . 042686 · . 001479 08/21/08 12:,47:05 . A

l 3 · 08. 215 STO - A**CAL B~K**  

### . 367275 -.417750 01)/21/08 12 : 47:05 As 

### 18? . 042 STD - A CAL · BLK . 099394 . 003212 08/21/08 12:47;05 .·

. B 249 . 678 S T D - A CAL·BLK . . 0'!7'[87 -. 00579 , 1 08/2 . 1 /0s 12: , 47 ; 05 · Ba 455 . 404 S TD - A CAL · BLK · . 03 · 3364
- . OQ0522 08/21/08 12:47;05



# . s e 313 . 042 STD - A CA.j:.-BLK . 0 . !!7804 . 001206 08/21/08 12:47:05 Bi 223 . 0 . 61 · STD•A CAL·BLK .092664 '00 . 4322 08/21/08 12:47 . :05 Ca 317.933 STD-A CAL·BLK .786360 -.009432 08/21/08 1 2 :47:05 Cd 226 . 502 STD-A CAL - BLK . 005890 - .000122 08/21/08 12;4 7 :05 · co 228.6 1 6. STD-A CJ\. L -BLK .032474 . 00186 1 08/2 i /08 12:47:05.

. Cr 267,'116 STD - A**CAL a~** **.** 

### .088471**oo67~6** 

### 08/21/08 12 : 47:05 ·' · Cu 324 . 753 STD-A CAL:BtJ< . 01!02E!!! - . 0],8190 '08/21/08 12:47:05 Fe .' 25.9: 940**STD~J;I** 

### CAL - BLK .063228 -. 002!185 08/2 1/ 08 1.2:i7:os · Fe :Pl.441 STD - /1. CAL - BLK 1. 

### 2 4 065 .021080 08 / 21/08 12;47:05

· K 

### 766 . 491 knahi 15 CAL- B LK 1 ' 0 2 ' 189 . i41 4 51**08/2~/08** 

### 1 . 2:47:Q5 .**t~g** 

### 2t9 . o 7 a STD·B-**cAL BLK**  

### .**2~5704** 

### -. 094.912 08/21/08 · 12 : 47:05 38 . 3 , , 23J.. . '

### C~·BLK 08/2 1 /08 12:4'7:05 .. Mg STD-A . 80.2240 . 0 1 069 . 1 Mn 2 5 7.610 . STD - A ' CAL-B I, l< . 048008
- .'000032 08/21{08 12 : 47 : 05 Mo 202 ' .. oo . o S T D-B CAL-BL,K .02685!> .000036 08/21/08 • 12:47:05 ' Na 

## SfltL 995 · kna hi 15 CAL- B LK .941266**-~2.15 3**  

### 08/21/0Q**12:~7:05 .**  

### Ni 231.**04** 

### STD - lC CAL-BLK . 041558 - . 000125 . 08/h/08 12:47;05 p 

### 1'7 • 8 ' .287 STD - B CliL - BLK . 275610 -. 078510 08/2 ' 1/08 12;47;05 2203/. 1 220.35i . . . 

### .' 02J403**~** 

### '00 . 7;384 08/21/0S 12**:~17** 

### :0 5" STD · A . CAL - BLK 22 · 03(2 2:io · .**35~** 

### S T D - A CA!'-BLK . 04,3703 . 002752 08/21./08 12:47 : · o5 

## s i 82 . 04 . o S T D-B CAL-BLK . 246489 - . 06890p · 08/21/08 12:4 '7 :05' · sb 206 , · 838 STD-B C\L·BLK . 1032 1 6 - .000103 08/2i/08 12:47:05

1960/ 1 196 :'. 021 STD-A CAL·B · LJ< .OIJ96 2 8 . 005674 08/21/08 12:47:05 1960/2 1 96 . 022 STD-A CAL - BLK .088082 - . 004813 08/2i/08 12:47:05 S i 251 . 612 S T D-B CAL-BLK . 071896 -.006156 08/21/08 12:47:05 P b 220.353 ·NONE NONE . QOOOOO .000000 *NOT STANDARD I ZED Se 196.026 NONE ' NON!:; · .000000 . 000000 * NOT· STANDARDIZED sn 189.989 S T D - B CAL - BLK . 0 917 0 2 . 00 1 283 08/21/08 12:47:05 Sr 4 07.7 . 71 S T D - A CAL-BLK . 008924 -.000464 08/21/08 1 2 : 47:05 Ti**33~.** 

### ' 9 41 STD " -S CAL-BLK . 0068'89 .OU0071 0'8/2170'8 1 2 · : - 4'7': · o 5 Tl 190.864 S TO-A CAL-B LK .203239 . 014626 98/21/08 1 2:47:05 

## u 367 . 000 STD · A ' CAL-BLK 1. 

### 25463 -.026334 08/21/08 12: 4 7:05 

### v 292.402 STD - A CAL-BLK . 0833 1 2 . 0 00167 08/21/08 12 :47 · :05 y 

### 371.000 NONE NONE 1. 

### 00000 .0 00000 *NOT STANDARDIZED 213Zn 2 1 3.856 STD·B CAL - BLK ' 101430 . . 0 90811 

### 0 !)/2l/08 1 2:47:05 Zn 206 . • 200 STD - A CAL-B L K . 020396 . 000788 08/21/08 12:47:05 Zr 33 9 . :!.'98 STD · B CAL-BLK . 005790 . 0080 1 5 08/21/08 12:47:0 5



### VES 0 0 5669

### Standardization Rpt, 

### Me . thod: PSC34 

### Standard: S TP -A 

### Run :rime:**08/2 /~8**  

### 12 : S2:27



### Elem Al As B 

### Avge 6.103 4 . 948 20.43
' Ill 

### 6.076 5 . 020 . . 20 . 48 112 6.062 . 4 · . 9 . 24 21) .42 #3 6.171 4 ,900 2Q ,:p 

### Elem Cd Co cr Avge 86.985 30.86 11 .29 Ill 

### 86 - .801 30 · . 7 4 11.29 #2 86.724 30.75 11.26· #3 87 ; '*.29 31.10 11.3 2



### . Ele m Ni 2203/ 1 - 2203/;! 

### Av . ge 1 :). u 43 : 7 i . 22.91· Ill 

### 12. 12 44. 1 2 22.71 112 12. 01 44 : 3 i 22. 9 1 #3 12.22 42 , 70 23-i!ll 

### Elem 

### u 

## v Zn · 

### Ayg

_ e 3 . 973 5,894 102.2 .; 

### 111 4.066 5 , sa8 · 101.9 112

. 3 . 820 5 .84 9 101.8 #3 . .4. 033 5 . 953 1\)2.**~**

# i~ . ', "! ,:

··**~: ~** **·** 

### 08./21/08 1 2 :57 :54 ./

· . . f)



## .**~·**



# . . Ba**··~ ·**  . . Be 

### 28 . 531 J;- 63. 045 28 . 3 · 86 :., 62.889 28.679 : '{ · 

### . . ' 

### ;. , 63. 202 28 · . 528 ; - 63. 044 2.**~;;- ·**  

### . 

### Cu ·*: Pe · 

### 24 . 24 · . 8 . 039 24.16 l!¥ 8. 017 24 : 30 

# t: '· 981**2~ 26** **~· 8**  

### .118 4{ -- 

### 1960/1**1960 /2**  

### 5 . 250**334**



### · 5 . 2 33 li s. rl28 5 : 399 ';i 5.327 5.118· 

# ; . s . 445



### . .**~** 

### . 

# . · . • r 5 :

, .**~:-. ·** 

; 

### • .. 

## ZV . Lf**~3 .**  

# 21f • 

# zq 0. 84'5 PM page 

### 1**~i** 

## ca 5.129 12 . 80 5.262 12.76 4,957 12.79 5.**1:~ 8**  

### 12 . 8.4 

### M

g Mn · 5:912 20 . 48 ' 8 5 . 947 20.42? 5,1)66 2o.sp . 5.923 2Q , S27 

### Sr T l 

### 53 . !;l,i · 4 .860 - 53.332 4. 836 53.7.4 4 4 . 825 s_3. 46 6 4.921



### VES 005670Stapdardiz . ation Report 08/21/08 12:57:54 PM page 1 . Method: PSC34 Slope • Conc(SIR)/IR Blement W avelen High std Low 

### std Slope Y-i n t erce pt · Date Standardized Ag 328.068 STD - B CAL·BLK .042686 .001479 08/21/08**12:5~:27** 

### Al 308.215 STD - A CAL-BI.d< :394 283 -. 44 &470 oa/21/08 12:52:27 As 189.042 STD-A CAL · BLK .1.00398 . 003245 08/21/08 12:52:27 , 8 249.678 STO·A 

### CJ\1,.· BJ.d{ .0493 . 88 · - . 006022 08/21/08 12:52:27 Ba 4 55.404 

### STD-A CAL · BLK .035069 -. 000549 08/21/08 12:52:27 Be 313.042 STD-A CAL·BLK ·. .00'7913 . 001223 08/21/08 12:52:27 Bi 223,061 STO·A CAL -B I.d<**.09~655** . 004508 08/21/08 12:52:27 Ca 317.933 STO-A CAL -Bi.K .782405 -. 009384 08/2 1 /08 1:!:52 : 27 Cd 226.502 STO-A CAL·BLK . 005756 - . 000119 OB/21/08 1 2:52:27 

## co 228.6i.6 S'ID-A CAL · BLK .0323 57 .001854 08/21/08 12:52:27 Cr 267.716 STD·A CAL - BI.d< . 088659 . . 000798 08/2 1/08 12: 52:27 .. 

### cu 324.753 STD · A CAL-BI.d< .042 221 -. 019074 08/21/08 12:52 :27 '. 

### Pe 259 .9(0 STD·B CAL·BI.d< . 06322 .8 -. oo2o85 · 08/21/08**~2:5:1:27** 

### Fe 271.441 STD- A CAL-BLK 1 . 24137 . 02 1093 08/21/08 12:52:27 K 766.4 91 

### knahi_lS CAL·BLK l. 02 1 89 .141 451 08/21/08 12:52i27 Mg 279.078 STD-B CAL·BLK .24 $70 4 -. 004912 08/21 /08 12: 52:27 Mg 38 · 3 . 231 STP- A CAL· . BLK . 84 . 3829 . 0112 4 5 . 08/-21/08 12 :5 2:27 Mn 25'7.610 STD-A CAL-BLK . 0 4 88 · 33 -. 000033 08 /21/08 '12:52:27 

### Mo 202 . o · oo STD·B CAL·BLK . 0268$0' . 000036 08 /2 1/08 12:52:21 Na sas.99S k pahi_15 . CAL·BLK .941266 - 32 . 15 43 08 /2 1/08 12:52:27 

### N

i 231.60( STD · A CA L·BL K . 0 4120 '7 - . 000 124 08 /2 1 /08 12: 52:2 7

· p 178 .287 STD - B CI>,Io·BLK . . 2 75 610 • . OJ . 8510 08 /21/ 08 12 . :s2:n 2203/ 1 22Q . 351 STO-A CJ\L-BLK . 023124 

## -.: o on \16 . 08/21/08**2: ~2!27**  22 o3 /2 22'0.352 STD-A CAL-BLK .0 43653 . 00 2749 08/21/08 ),2:52:27 

## s 182.040 STO - ll C AL-B LI<; . 246 4 . 89 · - .06890 0 . 08/21/08 12: 52:27 sb 206.838 STO·B · 0\L · BLK . 10321 6 - . 000103 08/ . 21/08 12 ' : 52:27 1960/1 196.021 STO-A CAL - BLK .093928 . 00 . 5946 08/21/08 12: 52:27 196 ' 0/2 196.022 STD - A CAL ·BLJ<i . 0940 14 - . 005137 08/21/08 

### f:a: 52: , 27 Si 251.612 

### sTb - s GAL - BLK .'0 7 1896
- . 006156 08/21/08 12:52:27 Pb 220.35l 

### liO NE NONE . 0000 . 0 . 0 . 00 000 0 *NOT STANDARDIZED 

### Se 196.026 

### NONE NONE . 000000 . 0000 00 

# • NOT · STANDARDIZED

· Sn 189.989 STD - 8 CAL · BLK .09 1702 . 001283 08/2 1 /08 12:52:27

Sr 407.771 STD - A CAL·BLK . oo9352 -. 000486 08/21/08 12:52:27 

### Ti 334.941 STP-B CAL - BLK . 006889 . 000071 OB/21/08 12:52:27 Tl 190.864 STO-A CAL · BLK . 2057 · 10 . 014804 OB/21/08 12:52:27 

## u 367.000 STD·A CAL-BLK 1.27980 - .026862 09/21/08 12:52:27 

## v 292.402 STO·A CAL - BL K .084696 . 000 1 69 08/21/08 12:52:27 y 371.000 

### N ONE NONE 1 .00000 . 000000 • NOT STANDARDIZED 213Zn 213.856 STO - B CAL - BLK .101-430. . 000811 08/21/08 12:52:27 Zn 206.200 STO-A CAL - BLK .019575 .000757 08/21/08 12:52:27 

# zr 339.198 STO-B CAL·BLK .005790 .0080 15 08/21/08 1 2:52:27



### VES 00 5671

### Staridardi zation Rpt · . Meth od: PSC34 Standard: · knahi_lS Run 

## Time: · OB/21/0B 12 : 

## sa: 34



### Elem X 

### N a 

### Avge 23.00 3083 . 

### Ill 23.00 3084. 

### 112**~3. 18**  

### 30 88. 113 22.83 3076. 08/21/08 01:02 : 26 

### PM

7 

# ' !'



## ' 

# . { 

### page l



### VES 005672**Standard~zation** 

### Report 0!!/21/08 01:!)2:29 

### PM page 1 Metho . d: •PSC34 Slope Conc(SIR)/IR Bl · ement**Wa.vel~n** 

### High etd Low 

### etd Slo pe Y·iricercept Date S tandard ized Ag 

### 328.Qp8 STD-B CAL-BLK .042686 .001479 08/21/08 12:58:34 Al 

### 308.215 STD-A CAL-llLK .394283 - .4 . 48470 08/2!/08 12:58:34 1\s 

### 189.042 sio - A CAL-BLK .100398 . 003245 . 08/21/08 12:58:34 B 249.678 STD-A CAL -BLK . 049'388 -.006022 08/21/08 12:58:34 Ba 

### 455.404 !; T D-A CAL - BLK .0351)69 - .OOOS49 08/21/08 12;58:34 ' Be 313 . . 042 STD-A CAL-BLK . 007913 .001223 08/21/0P 12:58:34 Bi 223.061 STD-A CAL-BLK . 096 ' 655 . 004-508 08/ 21/08 12:58:34 

### ca**~17.933** 

### STD-A CIIL-BLK .782405**009384** 

### 08/21/08 12:58:34


### · cd 226.502 STD-A CAL - BLK .005756 - .000119 08/21/08 12:58:34 Co 228.616 STD-A CAL - BLK .032357 .001854 · 08/21/08 12:58:34 Cr 

### 267.716 STD-A CAL-BLK .088659 .001)79!! 08/21/08 12:58:34 

## cu 324.753 

### STD-A CAL-BLK**.04 ~221**  

### - . 019074 · oa/21/08**12:58r3 ~**  

### Fe 259.940 STD - 8 CAL • BLK . .063228 - .002085 08/21/08 12:58:34 

### Fe**27~.441** 

### S'rD - A**CAL-BL~** 

### 1 . 24137 .o:nb93**08/~i/08** 

### 12:58:)4 .. K • 7 11_6 . 491 knahi 15 CAL-Bl.K 

### 1.o37n ·15 . 0SI . 99 '08/21/08 l2:58:34 ' Mg 

### · 279. 07Q**STO B-** 

# :t~ ''245,704. -. O . Q49l;! 08/21/PB 12:58 : · 34

. !-lg · 

### 383 ' .23 1 St,P-A .843829 .01124$ 08/21/08 12 : 58:34 · 

## Mn 257.6 , 10 STO.A CAL - BLK .048 833' -.0 00033 08/21/08 ' 12:.8:34 

### f'lo 202.QOO STD-8 CAL-BLK ; 026850. ' . . I)'QQ036 . 08/:il/08 12:S8:34

. Na 588.995 l<nahi 15 CAL-BLK . 928835 -31 . 8733 08/'J;l./08 ' 1'2: 58: . 34 Ni 23 1 .6 04**s~-A-** 

### CAL - BLK ' . 041207 - . 000124 ' 08/21/.08 12:58:34 p 

### 1'78. 287 STD-8 CAL-BLK .275610 • . 078510 08/21/08 12 : 58 . :34 2 · 203/ l 220.351 STD - A CAL-i3LK .023124 - . OP 7 , 296 08 / 21/08 12:58:34**~203/2** 

### 220.352 S , TD-A CAL"BL!<**.0~3(153** 

### . 00274!1**riV21/0~** 

### 12:58:34 

## s 182 :0 4 Q STD-B CAL-BLK , 246489 - . 068900 08 /21/08 12:58:34 Sb 206.838 . STO - B CAL - BL K .103216 - .000103 08/21/08 12:56:34 1960/1 196.021 STO - ll CAL-BI,K . 0!!3928 .005 . 946 08/21/08**2:58:3~** 

### 1!160/2 196.022 STO - A CAL-BLJC . 094014 -. 00 " 5137 ' 08/21/08 12: 58"': 3 4 Si**2~1.612** 

### STO - B CAL-BLK . 071896 - . 006156 08/21/08 12: 58:l<1 Pb**220.35~** 

### NONE NONE .000000 .QOOOOO * NOT STANDARDIZED Se 196.026 NONE NONE .000000 .000000 *NOT STANDARDIZBD sn 189.989 STO - ll CAL - BLK .091702 .001283 08/21/08 12:58 : 31 Sr 407.771 STO - A CAL - BLK .009352 -.000486 . 08/21/08 12: 5 8:34 Ti 334.941 STO - B CAL - BLK .006889 . 000071 08/21/08 12:58:34 Tl 190.864 STO - A CAL-BLK .205?10 .014804 08/21/08 12:58: 3 4 

## u 367.000 STO - A CAL - BLK 1. 

### 279'8o -.026864 08/21/08 P:58:34 

## v 292 . 402 STO-A CAL - BLK .084696 . . 000169 08/21/08 12:58: H y · 

### 371.000 NONE NONE 

### 1.00000 . 000900 . 

### *N OT STANDARDIZBD 213Zn 213.856 STD-B CAL - BLK .101430 . 000811 08/il/08 12:58 : 34 Zn 206.200 STD - A CAL - BLK .019575 .000757 09/2 1 /08 12:58:34 Zr 339.198 ST0 - 8 <; AL - BLK .005790 .008015 08/21/08 12 : 58:34



### V E S 0 05 6 7 3

### linalysi.s RepoJ:.t . 0 . 8/21/08 O:j-:10:21 . PM page 

### .1.**M~tho!i:** / 

### ·**Qp~ J:ator:**  

### gbu .PSC34 Sample Name : .**I~** 

### Ru n T ime: . 08/'21/08 . . . .**co~ri,t,** 

### 13:04:55.**~de:** 

## . .cooc Corr. Factor: 1 Elem Ag Al As 

### B 

## sa; ·Be 

### Bi Units ppm ppm ppm. ppm ppm ppm ppm Avge .2580 1 · .024 .a61 4 . 5079 . . 51322**~555 4**  

### .2656 #1 .2619 l. 

### 041 ..**2~8 8**  

### . . 5109**.Si4~S** 

### . 25537 . 2725 #2 .2576 . 1 . 023 .2570 · . 5091 . 51294· .255;4 . 266? #3 . . 25ol6 1 · . o·o9**2!?8~** 

### . 503 . 7 . 51228 .25550 · : 2577 Elem Ca Cc;l <;o Cr Cu Fe . K 

### Units ppm ppm ppm ppm ppm ppm ppm Avge .s ·. 1o8 . 25488 .5119 ' , 5092 .5065 6.136 · 5.029 #1 5 . q3 . 25713 .5144 . 5132 . 5066 6. 221 · 5 .. 03 1 . #2 5.101**-~5396** 

## .sus . 5079 .5052 6 . il9 . 5 . 025 113 5 .0 91 : ;!5354 : . so9& :so65 .S 078 6 . 067 5.032 E!e m Mg**r~ n**  

### Mo 

### Na Ni p 

### 2203(1

. . 1J nits, PJ?.!ll ppm PPIII ppm ppm . PPm ppm .•

Avge**~.111** 

### . 51349 . .2 . 539**2.3~2** 

### . . 2579 2. 540 . .**52~4** 

### #1 

### 3.164 . 51472 .2519

# t~~~ · . 2596 2.571 . 5175 #2 3 . llQ . 5 . P13 :2544 . 2580 2.515 .5381 fl.3 3 . 060 . 51261 . 25 52 2 . 378 . 2561 · 2.!;i34 . 5325 2203/2**1~60/l** 

### 1 960/2 . ) 

### Pb Elem 

# s Sb Si 

# • Units .· PPm ppm ppm ppm ppm ppm ppm .Avge .5023 1 . 007**2~43** 

### . 2796 . !!427 . 4514 . 5113

Ill 

### .5023 1 .007 .2528 . 2?:17 . 2442 .4579 .5074 # 2 . 5008 1. 008 . 2704 . 2781 . 2351 L. 4 . 481 . 5132 #3 . 5038 1. 006 .2697 . 2890 .248 7 L . 4482 .5134 Blem se Sn sr 

### T t . 

### Tl 

## u 

## v Units pp m ppm ppm ppm ppm ppm ppm Avge .2550 · . 51'46 .25661 . 50 921 . 5157 2 . 648 . 2526 Ill 

### .2534 . 5154 . 25682 . 51061 . 5210 2 .82 1 . 2555 #2 .2494 .5153 . 25670 : 50934 . 5098 2 . 643 .2520 #3 

### .. 262:j. . 5133 . 25631 . 50768 .5163 2 . 480 . . 2503 Elem y 

### al3Zn zn 

### Zr

.. :Units ppm ppm ' ppm ppm

Avge . 39 . ; . 51 1 :25 · 9 1.274 . 5 (!47 #1 

### 38. 4 9 1.257 1.27 . 7 . 5 080 #2 38.51 i.258 1.273 . 5044 #3 38.51 1 . 258 1.272 .5016



### VES 005674

### Analysi$ Rep . ort Method 

### i · PSC34 

### Run**Ti~;** OQ/21/08 

### Comment: . Mode i 

### coN · . . • , . 

### c o rr . E l em



### · Unit



### Avge #1 

### #2 #3

. Elem 

### Units 

### AVge

. #1



### #2 #3 Elem 

### U

nits 

### Ayge #.1 #2 #3 Ele m 

### Units 

### Avge #1 

### 112 113 . 

### Blem 

### Units 

### Avg . e Ill # 2 . #3 · "i

. H . 0074

- . 0049 H.004'7



### Ca 

### ppm .0050 .0104 

### .OOll .0035 Mg 

### ppm**012~** H.0278

- · . . 0063

. .

0148 2203/2 · 

### ppm .0067 .\)073 .0136 -.0007 

### Se ppm

.. -. 0037

- . 0049

- . 0011

- . 0051 

### Elem Y 

### Units ppm 

### · Avge 38 , 1 · 9

Ill 38.2 9 #2**~8.00** 

### #3 38.27**Samp~e Nam~** **:** 

### ICB 13:1+;37 ' . 

### Al ppm .**'~** .01 4 7 : .0324 -. 0065 .018:1: Cd )}. · .

### ppm**~**

. 00054 

# ' * .001f6 -,00119

. 00154

### -~ Mn .. .. 

### p p m ,. .

. 000 . 31



### , .**000~~**

- . 00064 .00062 

## s ppm

- ' 0027 .0043

- . 0145

. 0021 

### Sn 

### ppm

. 0058 

### H . Ol27

- :0033 .0062 213zn 

### ppm . •

. 0011 ; .0!)20

. 0004

. 0008 H.0124 -.0092 .0092 

### co ppm

. 0017 .0041**.** Ojl16

. 0026 

### Mo 

### pp m

. 0025 H. 00 " 6i



# - :ooo · e

. 0019 I 

### Sb 

### ppm H.0179 

## a.o:i63

-.008 0 H.0255



### Sr 

### ppm

. 00010 .00024 -.00003 .00007 

### Zn ppm

. 00:1.4 .0029

- .0003

. 0015 .. . . . 

### " 

## ' ; f . . 08/21/0B . 01:17:06 PM 

### page 1 

### Operator: 

### gbu
B 

### ppm .002 · 7.

. . 0060

-:oo37

. 0057**~··'Y":' ·-"**  Ba 

### : . PPm , , ·

' · ;·ooo51**~** 00106 : :09001 .00047 Cr · 

### ppm·

. 00 2 6 

## . · ..**· -cu**  

### \ • ' ppm "\ · -.0001 

# ''f :, H . 0071 :: . . • 0019 , . oo36 . A f , 9o 1 1 H . 005Q · , ·.0032



### Na ppm

. 0045 .0

. 103

- .0036

. 0066 1960/l . 

### ppm

- .0071 .0028 • . 0241 

### c . 00 . 01 

### Ti · ppi!l

. 00075 H.00177

- .00032 .0008 1**~r** 

### ppm : oo12 H.0030

-. 0008

. 0016 . . •. ->**~** .,


### .. Ni 

### ppm .0008

# ::**~~~!3** • 0021 ' 1960/2

. PPm

- . 0020

- . 0087 ·

. 0104

- . 0076 

### T

l ppm .0046

· .0148

. . 0031 .0022 

### · Be 

### ppm

- . · 00001 .00015

· . OQ018 . .00000 

### Fe 

### ppm .0040 .0075 .0010 .0035 p 

### ppm .008 4 :Q099 .qo5o .0105 

### Si 

### ppm

. 0027 H . 0 10 2

- .0059

. 0039 

## u ppm .1398 .3824

- .2597 .2967 

### Bi ppm

. 0,03 6 H . 0214

- , o25o

. 0143 K 

### ppm -. 0003

. 0483

.. 1012

. 0521 2203/1 

### ppm -.0112

- . Q080

- . 0303

. 0046 . 

### PI;> 

### ppm .0007 .0022 -. 00 1 0 .0 011 

## v ppm .0036 .0063 .0009

. 0036



# --------- - •. -:-

.**----- --** **----- ·-·** **·** 

### . . . 

### VES 005675

## . .

. 

# . . Analysis Report 08/,2 1 /()8 01:25 : 47 PM . page . 1 Method: PSC34 . Sample Name: ICVAX 

## / Operator: .gb':J 

### Run 

### Tillie": . 08/21/08 13 ,20:21 Co""""nt . : Mod e: 

## CON!= Co)."r. FactOr: 1



### . El.em Ag Al 

### As 

### B 

## sa l!j3 • 

### Bi**Un ts**  

### PPm 

### ppm PPIJ.I PPJll 

### ppm ppm ppm AVg . e . .2 - 524 1 . 027 . 2554 .5041. .512a9 . 25564 . 24'75 Ill 

# :**~~~ ~**  . 

### 1.017 .2543 . 502l . 5125 . 6 . 25544 .2455 112 1 . 048 .2621 . !?075 : . 5:J.203 .2560 . 8 .250 2 · 113 .2517 1 . . 016 . 2498 . 50.27 . 51200 .2 5540 . 2467 Elem · C . iil Cd Co . . Or 

## Cu l'e . . K 

### Ul)i'ts ppm ppm ppm ppm . p pm 

### ppm ppm

. · Avge 5.102 . . 25273 \5097 . 5033 .5Q59 6.130 4.922



### Ill 5 . 097 • 25l48 • 5094 .5Q08 • 51"00 6 , 097 4 . 837 . 

### 112 5.108 . 25409 .5126 · . . 5057 .5079 6.134 4.937. · {t3 5 . 103 . 25261 . 5072 .5034 .4_g98 . 6.158 4. 992 . Elem Mg Mn . Mo 

### Na 

### Ni p 

### 2203/1 ·units ppm ppm ppm . ppm ppm ppm ppm Avge 3 , 033 .51273 .2 535 2.378 . 2540 2.539 , 4991 

### ltl 2 .994 · · . 51263 .2497 2 . 367 .25 37 2.53'1 .496Q 112 3 . 092 . 5l323 . 2553 . 2.388 . 25" 5 1 2,530 . 5128 ·

· #3 3 :o12 .51 233 . 2556**2.37~** 

### . 2531 2.554 . 4884 Elem 2203/2 

### · s Sb 1960/-1 196.0/2 Si 

### Pb Units ppm p pm ppm ppm 

### ppm ppm ppm ." Avg!' .5144 1.010 .2504 .2457 .2583 .4539 .5093



## . . 111. 

### .5131 . 9936 . 2252 .2400 . 2581 .4521 . 5074 #2 .5!)55 1 .0 23 . 2758 . 2566 .2546 .4546 . 5080 #3 . 5247 1. 0i4 . 250 1 . 2404 . 2621 . 4549 . 5126 Elem 

### s e Sn Sr T i - Tl 

## u v Units 

### ppm ." ppm ppm ppm ppm ppm ppm Avg e . . 2541 . 5 0 77 • . 25569 . 50763 .5167 2.429 .2517 #1 . 2521 . 502 4 . 25645 . .5!) 78 4 . 5185 2.256 .2516 #2 .2 553 .5132 . 25522 . 50786 . 5213 2 .6 43 .2 518 #3 . 2548 .5073 • 25541 ,50719 . 5104 2.389 .2517 Elem y 

### 2 1 3Zn z n Zr Unit ' s ppm ppm ppm ppm Avge 38 . '79 1.256 1 . 267 .5030 #1 38.75 1 . 258 1 .26 5 . 5 037 #2 38.86 1 . 256 1 . 272 . 50 44 " 113 . 38.77 1. 254 

### 1.264 .5009



### VES 005 67 6

### Analysis. 

### Report Method: . PSC3 4 

### Run Time: 08/21/08 

### S , ample**~me :**  

### ICB 13:27:0 . 3 

### Com m e nt: 

### Mode:**~c** 

### Corr . Fac tor: 1

Ele m Unit Avge . 

### #1**~~~** 

### #3 

### Elem

· · units '· Avge



### #1 

### 112 #3 

### Elem Units A.vge



### · #1 

### 112 11 3 

### Elem Units Avge 

### Ill 

### 112 113 

### Elem Uni ts· Avge 

### # 1 ll2 

### #3 9

. 0012 . H. 0031

. Ca 

## ppm . .

. .**003~**

. 0045

. 0046

. 0014 Hg 

### ppm .0026

- . 0037 .0004

. 0112

' 2203/2 

### ppm .0049 .0022 .0112

. 0013 

## se ppm

. - .001 0

- .0 008

- .0031 .0 008 

### Elem Y Units ppm Avge 37.78



### · #1 3'7.76 

### #2 37 .79**~3** 37 . 7 8 

### Al pp.m .0074 .00 46 -. 0 100 .02 7S 

### Cd

. ppm

..

000?5

, 09082 : . 00.027

. 000 . 57 

### Mn 

### ppm .00033 .00 049 .00 . 030

. 00020 

## s ppm ·. - , 0001

. 0028 -. 0014

- . 0016 

### Sn 'Ppm

. 0042 .0058

. 0021 .0046 213Zn 

### ppm .0098

. 0013

. 0005 .0007 As

. PP'!I :



## · . ooss .0 0 0 7 ,003 7 

## H

·: 0 121 ' 

### Co 

### pp'm

.. 0:010

. 0 009

- . 0 ' 0 1 0

. 0030 

### Mo p pm .0 0 15



## . ooo.s · • 0018

. 0021 

### Sb p pm · H . Ol36 

## ..._.....,1

- . 0038 H.0236 .



### Sr p p m

. 00004

. OOQ09

- .0 0004

. 0 0 007 

## Zn ppm .00 11

. OO l.l -.0 00 2 .0 0 23 08/:21/08 . 01:32:30 . PM



### B ppm .' 0 022 .0035 .0008 .0021 

### Cr ppm , OO 'l6 .6045

. 0010 . .Q022 

### Na ppm .0036

. 0 03 9

- .0 002 .0 070 1960/l . ppm . .0009 .0077 -.0166 .0 116 

### T

i ppm

. 00024 .00037

- . 00062

. OOO li S 

### Zr ppm ·

. 000,4

. 000 4

- : 0013 H . 00 20 

### . Operator: gbu 

# A 9 / 

# SL Ba ppm

. 00029

. 0 .

004 ' 0 .00036

. 0 . 0012 

### Cu 

### ppm -.0040 L- , 006 1- ·

- . ()035

- . 00 24 

### Ni 

### ppm .00 ,08 .0012

- . 0008 · .

. 0 . 019 1960/2 . 

### ppm -. 0020

- . 00 5 0

. 0037 -. 0047 

### Tl 

### ppm

- . 0014 .Q0 18**0070**

. 0008 

### B e 

### ppm .

· - . O . Q01 9

- .00018



### - . QoP;J.S

- . 00025 

### F

e ppm

. 0035 .0050 .0035 .**.OQ i~**  p 

### ppm

. 0065 .0052

. 0036

. 0;1.07 

### Si ppm

. 0017

. 0010

. 0 035

. 0006 

## u ppm .1228 .'1663

. 0499

. 152 2 page 1



### B i ppm .0036

. 0102

. 0023

- . 0017 K 

### ppm . .0586**.0 ~28** **•.** .0809 .012 2 . 2 203 /1 

### ppm

- . · 0036 .0061

- . 0183

. 0014 

### P

b ppm

· .092 1 ' • 0035 .0014 .0 01 3 

### v · ppm .0023

. 0015 ·

. 0035 • 0021



### VES 005677

### Standard i zation , Rpt, 08/2' 3: /.08 0 1 :35:52 P M page . 1**M~thod :**  p ' sC34 

### Standard : CAL-BLK Run · Tirne: OB/21/0B 13:33:24 E l em 

### Ag Sb , Avge 

### . 1049 "1952 

### ' Ill . 07l:O . 1 209

#2 .0710 

### . · 1699 . 113 . 1729 . 29<t9 ! : •

•,



### VES 005678

### Standardization Method : · PSC34 · 

### Element · wavelen : J>,g 328.068 

### Sb .**20~.** 838 . 

### Report 08/21/0S · . Olt · 35:57 · PM . 

# . . . . . 

### . . 

## . P'!-9e 1



### . ' slope s 

### Cone (SIR) /IR High 

### atd 

### s :ro - s STD-B Low · atd CA L - i!Li<. CAL - BLK 

### Slope .043198**.107~67 ;**  

### '!-inte r cept -. 004534 

### -. 02 1 001 .



# '
. 

### Date Standardized 08/21/08 

### 01:33: 24**08/2 /~8**  

### 01:33: 24



### VES 005679

### Analysis Report Method: PSC34 

### Ruri ' · T i me : 08/2 1 /08**Cq~ent:** 

### Mode: CONC**C~rr.** 

### Sarople Name : . 

### ICVAX 13 :37:14 

### Factor: 1 I' 

### :7 

# t,v,/J.**'~''~"'** 

### vv.Y Al As Ele m 

### Units AVge J>.g 

### ppm .2497 . . Hl.313 . · .25'77 . 

### ppm 

# 1 ppm #1 #2 #3 Elem 

### Units Ayge Ill #2 #3 Elem 

### .units Avge #1 #2 #3 Elem 

### Units ,Avge Il l 

### 112 113 Elem 

### units Avge Ill 

### 112 #3 Elem 

### Units · Avge

# 1 # 2 #3 

### . 2502 '

. 24 ' 29



### . · 2559 

### Ca ppm '5. 085 

### 5 . 07Q 

## s,o69 5.108 Mg



### . .

pp m 3.052 3 . 045

. 2 . 963

3 . '1.48 

### 2203/2 . 

# ppm

. 5073

. 5 ' 077



### . 5261

. 4880 

### Se 

### ppm

. 2600

. 2619



### . 2662 .2519 y 

### ppm 38 . 19 

### 38 . 23 38.13 38.21 1. 

### 039 • 2574 Hl'.**432~j** 

### • 243 ' 9 H1. 468 . 2720



### C<;l 

### ppm

.. 25276

. 25208

. 24.920 • 25 7 0 . 0 

### Mn pp m .5 1 095 .510 2 2

. 50922 .5134'1 

# s ppm**1.00~** 

### 1.008

. 9975 

### 1.001 Sn 

### ppm .5048 • 5014 

### .4955 • 5 1 74 213Zn 

### ppm l.2 S O 1.2 48 

### 1.247 1.255 

### Co ppm ,!;066 .5049 .5029 

### .s121 · 

### Mo ppm .2504 .2

· 456 

### ,2503

. 2553 

### Sb 

### PPm .2505

. 2291

. ;!314

. 2910 Sr 

### ppm .25583 .25562 .25600 .25588 Zn 

### ppm 1.258 1. 255 1. 

### 251 1. 2:68 

# . . 08/21/08 

### · 01 :4 . 2:41 PM . 

### /. Ope;rator: gbu

B 

### ppm

· .5004 .4987 .4 929 .5096 

### Cr ppm .5020 .4982 

## : 198? .5095 Na 

### ppm 2 . 377 2 . 37ti 2 . 36A 2.392 

### 19

. . 60./'1 

### ppm .2 . 649 .2567 .245 4

. 2927 Ti 

### ppm .50S69

. 50463

. 504 52

. 50'19 1 

### Zr ppm .5010 

## ; soos

. 4991



### . 5033 

### Ba ppm

. S l OSS

. 51116 .' 5'i070

. 50979 Cu 

### ppm .5043 .5005 'SP5'1,



### . SO?J. 

### Ni ppm

.**5~3**



### . · ;!S28

. 2512 ' .2588 1!)60/2 

### ppm .25 7 5

. 2645 .2766

. 2315 Tl 

### ppm .5064



### . 5002

. 489 1

. S298 

# se ppm .

. 25601

. 25544

. 2556 4

. 2569 . 4 

### Fe ppm 6 . 097 6 . 126 6 . 049 6 . 116 p 

### ppm 2 . 514 2 .. 511 2 . 5p 2 . 513 

### S.i 

### ppm

. 4511

. 4509 L.4497

.4528 

## u ppm 2.467 2 . 457 2.204 2 . 801 

### page 1

Bi : . 

### ppm .2458 .242!il .2269 .2676 K 

### ppm · 4.!)78 

## ' 5.008 4 . 922 . 5.003 . 2203/ 1 

### ppm

. 50 . 6Q

. 5003



### · 4.85 4

. 5324 

### Pb 

### ppm

. 5069 .5052 .5125 .5028 

## v ppm .2512

. . 2 5 02



### .2512 .25 2 2



### VES 005680• l\\'C**·. ~~** **.l· '**  

# ·· r**}~ '** 



## , , ' V.•l 

## !**;or**

## ·~::1~ Analysis**R~port** 

### O.S/21/08 01:4 ' 9:22 . PM 

# :1€ page l 

# '7 Mel; hod : PSC34 ' Sample Name: ICB ·.:. 

### Operator: gqu ;,<;; · . 

### Run 

### Time : 08/21/08 13:43 :56**i~** 

## · {;: :· Comment:**-~ ·~** **:. :**  

### . Mode : CONC Co=. Factor: l '·: .

## ~~**·** 

# r ·· Elem 

# · GfuJ Al As 

### B Ba Be Bi



### . U!"its · ppm PP!tl 

### ppm ppm 1 

### ppm ppm ,;/· ppm Avg e L · .00 1 .0180
- . 0016 . 0000. - . 00005 • . 009 . 34 " ' . 0006 #.1 L-. 0059 • 00 . 07 - . 0023 .. 0009 . 001)01 -.00028 ik : ll063 #2 -.0032 . 0543. . 0021 . 0036 - .000,17. -.0 00:}6 i• , • 

### QllO #3 L-.0093
- ." 01)10 - . 0047**:oo~6** 

### .00001 - .00038 · - .0156 Elem 

## ca Cd Co 

### . Cr 

## cu F . e**:-f ·,**  

### · J,Jnits ppm ppm ppm**ppm ·:~:**  

### ppm ppm 

### ·V JlPIII 

### Avge .0003 . . 0002!i . . 0002 . 0006 - . 0002 .0018 

# . ;li; ;., • 0 0 91**· ~:f** **~$ ~**  

### Il l . 0000 .00012 -.0010 . 0008 . .0013 .0032 .

### 1ll94 112 . 0005 .00055 . 00 4 6 . 00 , 38 , . -.0008**.00~6**

### ~'**.0529** 

### 113 . Q002 . 00006 . .,6029 -.0027 . -.0009 .0008

### ~~**0064** i• 1' (t' X : .**··~·** •. Y , 

### Elem Mg 

### Mn Mo 

### Na Ni p 

### . ' 2203/l Units PJ?III 

### ppm PJ?III 

### ppm ' ppm ppm 

### 'i ppm, Avge - . . 0026 . 00003 .0005 .0025 :ooo1 . 007 . 3 ' 

### - . Q024
., 

### Ill**~** 

### .. 0140 . OO,Ql2 .0026 . . 0007,. . 0000 ,0105 ·· .- ' .0036 . 112 H.0267 • 00034 . - . 00 1 4 . 0!05 . 0011.**0~68** 

### '' : . ' OlJl 

## il3 L · . · 0205 - .O P036 . 0003 • .OQ36 - .0007 - . 0052
- ·. 0166 Ele m 2203{2 

## s Sb 

# )**196~( 1**  

### 1960/'2 Si · .. Pb 

### Uni t s ppm , ppm PJ?III 

### pp m ppm pp m ppm Avge .OQ16 · .00 62 L -. 0219 .0051 - . 0034 • . 0044 -: 0003 .
¥**~ ~**  

### Ill 

### . 0029 · .007 3 x; 

### 3 . 0052 · .0023 -.00 39 . ; 0007 112 • . 0055 • . 0048 • . 0 061 . 0161 .. 0132 - .0048 .0007

. 113 .0074 · .0066 L· . 0352 · . 0059 . 0055 -.0046 - .0006 Elem Se Sn Sr 

### Ti T l 

## u v Units ppm ·ppm PJ?III 

### ppm ppm ppm : ppm Avge - . 0005 . 0013 .00003 .00006 .0021 . 005S ·.0002 Ill .0002 .0006 . 00003
- :00052 - .0053 - .0090 - .0016 . H2 - .0034 .0031 . 00018 H.00183 H.Ol79 .1765 .0005 113 . 0017 .0000 ·.00010 .. 00115 • . 0062 - .1509 .0005 Ele m 'f · 

### 213Zn zn Zr .; }<t

· 

### Units ppm ppm ppm ppm <

## if~ Avge 37.64 . 0 , 007 

## .oooi; · .0001 ,:;;. 

### Ill 

### 37.71 . 0012' .0004
- .0008 112 

### 31.71 . 0005 . 0023 H. 002? 113 37.50 .0003 -. 0008 L· . 

## oo;n

. . '**.· ~~**  

## ' • : . '**•'<> ~~** 



# • . ... .. 

### VES 005681

# . -. ' . 

### Standardization Rpt. 08/21/08 

### 01 : 53 : 18 . PM . 

### · Pag'e 1 Method · : PSC34 . S t andard:**CAL-BL~** 

### Run - Time : 08/21/08 1 1.: 

### so: 49 

### / Elem · Ag . ®b "- . 

## < J '"" ) Avge · . 0830 . 182

_ 2 _r 

### c #1 

### .0.610 ; l 9 #2 .1399 . 2869 

### #3 .0480 

### . 0730



### VES 005682

# I Standardization Rpt .**08/21/0~** Ot;57:38 PM 

### · . page 1**l~ethod:** 

### PSC34 . Standard: CAL - BLK 

### ' Run T i me: 08/21/08 13:55:10 .



### Elein 1\g . 

### Sb Avge . 0640 . 0126 • ' ' 

# . #1 . 0270 - · . · 0590 #2 .O!l80 • . 1329 

### 113 .0670 .1439 

# eve wAtflt7J · 

# &"

.::; 

### .

/ ' - :



### VES 005683

### Standardization

. Method : PSC34 Elemen t Ag 

### Sb 

### Wave len 328 . 068 20 " 6 . 838 

### Report Slope**~** 

### Cone (SIR) /IR 

### -1: ,

- High std 

### STD · B STD-B 

## . . 

# Low std**CAL~~LK** 

### CAL · BLK < 

## " " · s l ope :**interce t** 



### . 0430 4 6 c. 0027S4**.104779 _,** **,_ .** **007~10**



## . . .

< .



# ------ ---- - - - - ·· · · · - - · page l Date Standardized 08/21/08 01:55:10 . 08/2i/. 0 8 01:55:10



### VES 005684

### Analysis Report !'let hod: 

### PSC3 4 

### Run Tine: 08/21/08 

### Sample**~ame:** 

### ICVAX 

### 13;58:40 C!'rrrnent; Mode: 

### CO.!o!C Corr. Factof: 1



### - 1 ' \ I

### CAlc~<.**f~** AIOIJ 

### Blem Units 

### Avge . 

## ill #2 113 

### Elem Units 

### Avge #1 

### 112 #3 

### Elem UnJtp 

### Avge . Ill 

### #12 #1 3 

### Elem. Units 

### .Aovge Ill . 

### #2 #3 

### !Hem Units 

### Avge Ill 

### 112 113 

### Blem

· Units



### Avge Ill 

### 112 #3 · Ag 

### ppm .2505 .2532



### . 2480 :2502 

## ca ppm 5.140 5.130 5.154 5.135

. M g ppm 

### 3.o5p 

### 3.071 :) . 02 4 , ).056



### · 2203/2' 

### ppm .5185 .5084 

### .5378 .5094 Se ppm 

### .2562 .2541 .2598 

### .2546 y ppm 

### 38.6 4 

### 38 .56 ' 38.75 

### 38.61 A \ As 8 

### {

# Hi~~**s9} ~rs'53** **~ro42**

# ~ . 2554 . 5075



### Hl . 1 35 :**251~** 

### . 5035 

### Hl. 602 . 2591 . 5016



### Cd 

### ppm

. 25598 .256 41 

### .25769 

### :25385 

### Mh pp m .

. 51589 • 515 , 0 .

4 .

.**5179~**


### . 514 7'0 

# s · pp m l.OU 1.029

. 9998 1.005 

### Sn 

### ppm .5109 .5121 

### .5082

. 5124 

### 213Zn 

### ppm 1. 261 

### 1.260 1.267 1.255 

### Co 

### ppm .5142 .5135 • 51'74 .5116 

### M

o ppm , 25 51 .2536 

## .2

_ 564 . .2554 

### Sb ppm

. 25 75 .2385 .2582 .2757 

### Sr ppm



### . 25611 .25 545 .25125 .25564 

### Zn ppm 1. 280 1 · .281 

### 1.28 4 1.276 

## c:r ppm ,5070 .5080

. 5059

. 506.9 

### Na 

### ppm 2.4Q3 

### 2.395 2.4Qi! 

### 2. 405 ·**1~60/. l**  

### ppm .2626 .2789 .2500 .2587 

### Ti ppm .50957 

### .50823 .51246 .50801 

### Zr ppm .5047 .5043 .5070 

### .5 029**-'r~~** >9Jti**~-.** 1+;}**·~< ~'** **page** 

### 1**~era** 

### tor:**gb~**



# ,•r cu**'l:.~ l>Pm**  

# i\: :::: -**~· l2**  '

. 

### . ' - - : 5062

# .-:~**i** ;,;:. ppm .;¢; 2575 

## . ..**r;~** 

# ..**.J~ .**  2 5' · 9 6***; :**  

## 2567 

# <

· : 2 · s .

li3**,:~,** 

### 1 · 960/2



### . ppm . .2 530

. 24 18 

### .2646

. 2525 

### T l 

### ppm

. 5269 · • . 5170

.' 5 355 

### .5281

:**~-**

,· 

### . · Be 

### ppm .25846 

### .25 833 .25957 .25749 

### Fe 

### ppm . 6.140 

### 6 .124 

### 6 .1 58 

### 6. 1 39 p 

### pp m 2.5 5!i 

### 2.544 2.5 76 2. 54 6 

### Si p pm .45 55 

### .4520

. 46 04 

### .4541 

## u ppm 2.51 0 2 .. 

### 634 2.335 

### 2.560 

### :**~·** 

# ....**~** 

### Bi



### ... ppm .2506 ' :2556**,24~7** 

### .2496 K • ppm 

### ¥**~** 

### . 94 1**~}** ': 

## ·, :;,. · 5. 035 -,;..- '! -800 

## f. 4 .9 88



### - 220:3/1 

### pp m

. • 51 80 . ·: · 5 ' 361 .49 '15 .. 

### .5204 P.b 

### ppm _**.5~84** 

### .5177 .5244 .5131 

### v ppm .25 4 6 

### .2533 

### .2563 .25 42



# ..

VES 005685

### Analys i s Report M

ethod : . PSC3 4 

### Run · Tirne ! 

### 08/2 1 /08 

### Sample Name . : ICB 14 :QS:27 Comment;**od~:** OONC Cor r. F a ctor: 1 .**11:1~!11** 

### . Units A

vge #1 

## 112 113

. Elem



### Units Avge

E . l.em 

### Units Avge Ill · 

### H2 113

· Elem 

### Un . its Avge # 1 

### 112 #

. 3 

### E lem 

### Un i ts Avg e Il l 

### 112 113 

### Elem 

### Unit; a Avge # 1 

### #2 113 

# Ag ppm

·- . OQ34 L - . . OOS!l



### - . 00?8

- . 0 023 

### Ca 

### ppm · . . 0012

. :000 1 

## · :oo3o

. 0006 Mg 

### ppm

- , 001!1

- . OQ.95

- . 0079

. 0131 2403/2 

### pp m -.()015

. 0008 -.0010

- . 0043 

### Se 

### ppm -.0035

- •

. 0046

- · . 0030

- . 0029 y 

### ppm 38 . . 06 38.05 38. 1 0 3 . 8 . 04 · . A l 

### ppm



## . oo8o**~** 

### . ·

.0049



### . .o<p ' 9 .

. 0250 Cd . PPI1l 

### : 00024 .-.00004

. 00037

. 00039 Mn 

### p p m

. 000()8 .

. 0000 2 .

. 0001-5

. 00()05 

## ,s pp m

. OQ35



### - . . 0063

. 0151 : 0018 

### Sn 

### ppm

. 0045

. 0029

. 0037



### . 0068 213Zn 

### ppin

. 0005 • 0095



## . ·

ooo6

. 0004 

### As . PPf!l 

### .0017 .0010 • 0012 ' .0028 

# co J;>pm .00 · 10

. 0004 .0003 .0023 Mo 

### pp m

- · • OQ16**7.~1n5**



### - :0013

- .002 '1. 

### Sb 

### ppm -,0026

- . 0027 ·

- . 0017



## - . Ob34 Sr



### . ppm

.00005 ,00007 .0 0 000' .0 0 007 Zn 

### ppm .

. OOQ6 

### .0006

. 0 003 .0008 08/21/..08 07:10: 54 PM

B 

### ppm

. 000 . 6

· -. 0003



## . 6o-o6

. 0016 · Cr 

### ppm

. Q009 -,0003

. 0020 .

. 90:1, 1' 

### N

a ppm , oo49 • 002 5 .00 , 30 . .OQ92 

### 1960/.l 

### ppm

. 00'75 ·

. 01 11

. 00 1 7 .0098 Ti 

### ppm

. 00031 .00015 .00007

. 00071 

### Zr ppm . .0003

- . 000 1

- . 0006

. 00 1 5**Opera~:or.:** 

### gbu 

### Ba p pm

- . 0000 1

-. 0 . 0013 ' 0001 ' 9

- . 00009 

### .' cu .
· · : ppm**~·.** 

### -. 0011

. , : -. 0015 '< ' 

### -.0001

. -. 0017 

# . . Ni:

ppm

. . 0001



## - . oon · .

. 0!)02

. 0014 . · 1 9.60/2 

### ppm

- .0090

- .0125

- .0053

- . 00!13 

### Tl ppm .0016

. 0021 '

- . 0012 .0041 

### Be ppm

- .. 00035

- .00036 -.0003.7

- . 000 · 34 

### Fe 

### ppm 

### :oo;i-7 .OQ20 · .0021

. • .**000~** p 

### ppm .0051

. ()041

. 00 1 4

. 0099 

### S,i

. ppm

- · .0()19

- . 0052 .0019

· :. 0026 

### u ppm .

. 0550

- .0499 .0882

. 1266



# _____ __ ___ ___________ ... 

# - - .. - · · 

### page 1

B1 

## ppm

. 0022

- . 0079

. 0

. 0 2 9

. OllG K PPll) . •• OOOJ.



### -. 0 0 4 6

. 0496.**~.** 

### 0 4 ' 54 2203/1 

### ppm • QOlO . . 

### -.0007 .

- .0021 .

. 0058 

## Pb ppm

- . 0007

. 0003

- . 001 4

- .. 0009 

### y 

### ppm .'0001

- . 0009 .0004

. 0 009



### VES 005686

### Analysis Report 08/21/08 02 : 16: 24 PM . page l 

### Method: PSC 34 Sampl e Name: . CR I**Op~rator:** 

### gbu Run Time : 08/21/08 14:10:57

# ~"ll) Co mment: 

## Tt'f Mode: CONC corr. Factor: ' 1



# -

· ;\ Elem Ag A l As B Ba B e Bi

· · units ppm pp m ppm ppm pp m pp m PP.Ill



### Avge . 0 0 60 ' . 1127 . 0515 .04 5 7 . 00 4 97 . .00467 . . 0723 #1 L :0 042 . 0995 . 0499 . 0449 . 0050 9 .00 4 73 . 0648 #2 . 00 92 H .l 398 . 0549 . 0.85 . 00 4 70 . · 00460 :0 86 . 7 11 3 L : 0046 . . 0988 . 0497 . 0 438 . OOS13 · 

## : oo<t68 . . Q655 El,em . Ca . Cd Co 

## C+ Cu 

### Fe K



### . Unite , ppm pp m ppm ppm ppm ppm . ppm



### Av.ge ,15 2 ?' .01031 .01 . 11 . 0 102 .0082**10~1!** 

### .' 2190



# . . Ill 

### .1539 . 00995 .01 06 . 009 . 2 .OQ88 . 1052 .2 221 · 

### 112 . i505 . O ll31 · H. 0141 . 0 1 22 .0072 . .1028 . 1982 

### #3 . 1 53 1 . 009 . 65 

# . . .oo as . 0 0 92 

## .ooas .l. Ol4 . 23.6'1 Elem Mg · Mn Mo N a Ni . p 

### 2203/1 Units ppm pp m ppm PPm ppm 

### ppm pPm 

### A

vge . . 0805 . 00509 , . 0137 ,23 40 .0 145 · . .1556 . 0 4 76 

### Ill . 0701· .00493 

## , ope . 2316 · .0133 . 1573 . 0356 #2 H.10 4 3 .00545 .0120 .2425 .0 1 74 .160 9 .**071 ~**  

### #3 .0 . 670 . 0048'8 . 0153 .2277 . 0127 .1 488 .0 352 Blem 2203/.2 

## s Sb 1 9 . 60/1 1960/2 Si 

### Pb Units ppm ppm ppm ppm ppm ppm . ppl'n . Av g e .0590 .1 5 7 6 .Q 370 :0506 . 0435 .0 44 5 . 05 5 2 #1 . 0612 .1622 L. 0200 .0471 .0597 .0 4 61 . 0527' #2 .0472 . 1627 .0564 . 06 51 .0233 .0403 . 0554 #3 . 0686 .1 47.9 L.0347 . 0397 .04 7 3 . 0 4 69 . 0575 Elem Se Sn Sr 

### Ti Tl 

## u v U!'>its . ppm. ppm ppm 

### ppm ppm ppm ppm Avge . 0458 . 0504 -90507 . 0053.0 . 0 ' 794 . 2 164 .0 157

. #1 .0555 . 0 50 0 .0 0501 .0048 1 . 0 7 39 .1 · 222 . 0171 #2 .0 372 . 0534 .00522 H.00662 .0909 .3588 .014 3 #3 .04 48 . 0478 .004 99 .00448 . 0733 .1 683 . 0157 El em 'i 

### 213Zn Zn Z r

. Units ppm ppm ppm ppm Avge 38.31 . . 025 7 .0265 .0085 

### Il l 38.36 . 02 56 . 0258 · .0074 #2 38. 3 2 . 0256 .0281 !1 . 0 11 2



### . #3 38 . 25 .0259 .0256 .0068



### VES 005687' Analysis . Report Q8/2l/08 02:21:53 PM page 

### 1 Method: P SC34 Sample Name: 

### IGSABAX /. • Operat<:>r : gbu

· Run Time: 08/Zl/08 14:16 : 27 Coll1llent: Mode . : p:>NC Corr. Pact,or: 1 

# . . Elem Jig Al As B Ba 8!10 Bi Units ppm ppm ppm ·**p~** ppm 

## ppm · ppm Avge . 2000 143 .2 .191!2 -. 0012 .09957 .1001 7 . .0067· #1 .200 5 143.5 .1981 - .0 004 .10908 .1006()**-.00~4** #2**20~ ~**  143.4 . 2019 - .000 4 . . 0997\)**.190~5** .0246 1!3 . 1 982 142.8 ;19 40 - . 0026 .0989 3 . 0997 . 4 . -.0029 Elem ca Cd C,R Cr cu Fe . K

. Unit . s ppm . ppm ppm ppm : Pl?m ppm ppm J\\lge ' 236,0 .- 19l.9Q .1007 . 1001 . 0952 . 9 ' 6 . 79 - ,0071 

### Ill 23 · 6 . 9 ' 19289 . .099-8 . 1008 .0 9,52 97 , 07 .0005 #2 236 . 4 · .1 9187 : roo9 . ,lOU .0943 96.95 .0387 · #3 234. T .;19095 .1015 . 098-l .0960 96;35 - . 0 ' 604' Elem 11g 

### Mn M o Na Ni · P . 220 . 3/1 Units ·PPM ppm ppm. 

### .PpM . ppm ppm ppm Avge 246 . 0 . 10347 - . 0001 : 0047 .1921**01 ~9**  . .2093 Ill 246 .5 . ],03 ' 85 . .0027 .0 . 032 .1941 .0149 . .198( . #2 246.0 .10370**-.000~** . 0051; .1922 .0105 . .20 75. #3 245.4 . l028a -.0026 . .0054 .1 900 .0077 .2218 Ell em 2203/2 

## s Sb 1960/1· 196()/2 Si ' Pb units · ppm ppm ppm ppm ppm ppm ppm · Av g e . 1881 . . 0 1 81 . 2012 . 1 861 .1959 .003 1 .195 2



### Il l .1918 .0239 .1869 . 177: 6 .1 945 .0037 .1941 #2 . 18 . 99 . 0217 . 2103 .1818 . 2011 . 0077 .1 957 #3 . 1827 . 0086 .2065 .1 990 . 1 920 -. 0020 . 1 958 Elem Se sn Sr Ti T l 

### u v Uni ts ppm ppm ppm ppm ppm ppm ppm Avge · . 1926 ,0 038 . 00313 -. 00419 . · 0298 .2876 .0989 

## II i . 1 889 .0028 . OQ3Q9 - .00455 .03 50 ·**.~44,2** .1 010 112 . 1947 . 0058 .003'14 - . 00.424 .0260 . 3549 .10 11 #3 . 1943 . 0027 . 00316 -. 00379 . 0284 .26j6 . 0945 E l em · '{ 213Zn**~n** Zr U!lits ppm ppm ppm ppm AV9!!! 37.05 .191 0 . 1'887
- : ooo1 #1 36.03 .1922 .18 9 2 - .00 06 112 37.60 .1920 . .1889 -.oooi 1!3 37 . 50 .1889 . 1882 .0005



### VES 005 688

# i Analysis Report**8/2~J08** 02:28:34 

### PM page 1 Me thod: PSC34 Sample Name: Run Ti,me: 08/21/08 14:23 :08 

### HIKNA 

## / Oper ator: · BGI Cononenc: 

### Mode:**~NC** Corr. Factor: 1

B l em Ag Al As 

### B Ba Be 

### Bi Un . it:s 

### ppm ppm ppm ppm ppm 

### ppm ppm Avge .0005 .0329 .0101 .0037 . 00009 -. 000 4 5 ' .018 4 

### Ill .0018 .0527 .0089 . 00 4 3 . 00019 

## - . ooo ; n .0270 112 -.0016 .026 4 .0068 . 001.9 . 00001 -. 00051 .0093 #3 .0015 .0196 .0147 .0649 .00 008 -.00048 .0189 

### Blem Ca Cd 

### Co · cr 

### cu F e 

### K Units ppm , ppm ppm 

### ppm ppm p pm ppm Avg e .0628 . 00105 . · 0017 .004 1 . - .00 18 .**022 .**  100.7



### . #1 .1146 . 001 4 1 .0Ql 2 . .0053 -.0 . 032 .0448 1 00 , ' 9 #2 .'0476 . 00057 · .. 0023 • 0 . 018 -.0007 .0172 100,3 #3 . 02 ?2 . 00118 .0 0 15 . .0053 

## - .oots .·0068 100.9 Elem Mg . 

### Mn M p · Na . Ni 

### P ·· 2203/1 Units ppm ppm ppm . ppm 

# PPm ppm . PPm Avge . 06 51 . 00038 . 0006 106.3 . 00 2 0**,' 00** **~5** .0198 

### til, . 1 09 6 . OOQ52 .· : oo22 1 06.5 . 0031 

### . . 00 11 .0203 112 .0499 . OOOi:Q
- . 00 1 4 i o5.8 .001? .0110 .0136 113 . 0359 . 0005 ' 3 .0008 1 06. 7 . 0010 .0044 .0255 Elel\1 2203/2 

## s Sb 1960/1 1960/2 

### Si Pb Units ppm ppm ppm ppm ppm 

## ppm ppm Av ge -.0091 .0042 . 0106 .0224 - . 0131 -. 0 00 5 .0005 

### ftl

- . 0065 .0075 .0198 . 01:71 - .0124 . 0011 .0024 #.2 -.0081 .0102 -. 0062 . 014 1 

## - . oon -. 0007 -. 0009 #3 - . 0 1 28 . . 0051 .0 181 ,0359 -. 01 77 -. 00 1 7 - .0000 Blem Se S . n Sr T i 

### Tl 

## u v Units ppm ppm ppm 

### ppm ppm p pm ppm Avge - . 0013 .006 4 .00007 .00067 .004 7 .22 33 -. 0014 

### Ill -.0025 .0061 . OOQ06 .00053 . 007 4 .2901 - .00 14 ll2 -. 0014 .0046 .00007 .00067 . 0045 · .0984 -. 0018 !13 .0001 .0087 .00009 .00082 . 0023 .28 14 -. 0010 Blem 

### y 213Zn Zn Z%' Units ppm 

### ppm ppm ppm 

### Avge 37.85 .000 2 . 0010 . 0008 

### til 37.85 .0003 . 0004 .00 0 4 !12 37 . 70 -.0001 .0013 .000 7 #3 38.00 .0005 .0012 . 0013



### VES 005689

# ' i11 ,. , ,**;:i ~** **~** 

## . ·· :**~~** 

# ;" Analys i s .**..;, ~**  

## ... . Report 08/?.l/.08**0~ :**  

### 36:19 . PM page 1 

# CRI/ 7 : .., , . 

### M

. ethod : PSC34 Sa!!lPle Name: 

# ! Operator : gbil**Run .T.i~:**  

### 08/21/08 14 : 3.0: 

### ?0

..**~~** 

### 9omment:: ( 't'lt 

### Mode: CQNC Corr. Factor: 

### 1**~· t** 



### Elem · Ag 

### / Al 

# .y. · Bi l\S 

### B . .**~** 

## .. . Ba 

### Be · units pp m . ppm ppm ppm ·**~~** 

### ppm ppm ppm Avge .0075 .125 . 9 .051 8**.04 72** **~.** 

### .00502 ; 0'0463 .0762 #1 L. 005Z . .1 193 :o497 . 0456

### J;~ . 00474 , 00457 .0 . 683 . #2 .0076 H.1324 . 0547**,~** 

### . 00516 .00466 .0809 .0470 'K'l!· 

### 113 . 00,6 , 1259 .0509 .0489 

# ¥ ,00516 . 00465 ,0795 Elem · Ca Cd Co lj/ql'

### ' 

### cu Fe K . 

# cr**~** · . units PJ;llll 

### ppm pp m . 

# a : {., ppm 

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### 0137 

### .' Oll3 : .t· .0082 .1030 . 1945 

### Ill 

### . 1484 . 00 974 . 0127 · . 010 · 1 1 .0111 .1019 . 164 7: 112 . 1 537 .Q l.02 1 H:0143 • 0113 . " . 0070**19~3** 

### .1767 113**.~543** 

### .01071 H . Ol42

### ,o12~**:** L:oo6s . 1037 . 2423 . Elem 

## "" Ni 2203/1 Mg Mn Mo Na**~~** p 

### units**~P9'** 

### ppm ·ppm ppm 

# 'I ppm ppm 

### I?Pm .**Av<;~e** 

### .. 0958 . 005 16 : 0153 . 250 . 0 

## · : £4 .0 1 63**1~70** 

### .. J)512 #1 .6965 .OOSQ3 .Q126 .258 7 

# !-

. 0156 .1587 . 0557 112 li. 

### 0997 . 00502 . . 0168
. 2491 "' . 0].55 .1- :793 .0 461 #3 

### .0912 .. OOS4 ' 4 .0166 . 2422 '· : . 0177 : t6J1 . 0517 Elem 2203/2 

## s Sb

## 1960fl**;~** 1960/2 Si Pb uri.i . ts ppm ppm ppm ppm ppm ppm ppm Avg'e . 0528 . 1512 . . 0434 . 0559**~** 

### .0478 .0433 .0522 

### Ill .0466 .1454 L.0296 

### .d·

. 0640 . . 0410 .0380 . 04!)6 #2 . 0615 .1597 .0470 .0508 . 0516 .0444 .0564 #3 .0502 .1484 .0 53 7 .0528 .O S 09 . 0474 . 0507 Elem Se Sn Sr T i 

### Tl u 

### v Units ppm ppm ppm ppm ppm ppm ppm A

vge .0505 .0 530 .00516 . 00606 . 0838 . 2915 . 0154

· Ill 

### . Q487 . 0523 .00516 . 00599. .0854 .1836 . 0131

112 .0513 . 0526 . 00517 • .00635 .0875 . . 273 i . 0161 113 .05 1 6 , . 0 5 39 .005 1 & .00583 .0784 . 4177 .0170 E lem .Y 

### 213Zn Zn Zr

# ~ U

nits ppm ppm · ppm ppm Avge 37.92 .0256 .0270 H . Ol02 < ::, 

## u 37 . · 86 .0251 .0261 .0098 ft2 37.94 .0251 .0276 8.0108 ft3 37.97 . 0265 .0272 II. 0 1 01 

# ..

. 

## {

"



### VES 005 6 90

## ! Ana ly sis Report**0~/21/98** 

### 02:43:01 

### PM page 1 Method : PSC34 Sali!Ple Name: }.591852:

# ~734:). :DUP-("' Operator : 

## BG! RUn 

### Time: 08/21/08 14:37:34**co~nt :**  

### 1"5-91852 Mod e: CO NC Cor · r. 

### F actor: 1 

### Elem Ag Al As B 

### Ba !le 

### Bi unite ppm PP.Jil 

### pp!!l ppm ppm PPII! 

### P.Pm Ayge -. 0041 . . 0459
- . 0001 . . OQlO . 00002 . - . 00051 - .0018 ' Ill -. 0030 .088 . 0 -.0049 .0(}:).5 . 0002.9 -. 00041 • 0120 . 11.2**~** 

### .0015 .0324 · . 0073 · :o025 -.00034 -.0 006S .()002 #3 -. 0 077 .0175
- . 0028**~.oo:i1** 

### .00012 - . 00049 - . 0176

. Elem Ca Cd 

### Co Cr 

## cu Fe K 

### Units ppm ppm ppm P,Pm ppm ppm ppm Avge .0706
- . · 00010 -.0 005 ,0010 10 . 98 :0304 58.37 ' Ill . 1250 .OQ009 • 0019 ' :0024 . 10 . 97

# ~~·~~ 58.33 #2 . 0530 . 00053**~:oo~3** 

### . 0032 10.98 58.35 113 ;0339
- . 00091 - .0 020 -. 00f7 10: 98 . 0152 59;42 Ele.m Mg 

### Mn Mo 

### Na Ni p · 

### 22 03/1 Units ppm ppm ppm ppm ppm ppm 

## ppm AV:ge . 0618 .. 0()003 · . - . 0001 ' 2.163 .'0018 .OI)S5 - . 0041

. #1 · .p09 . 0 . 0020 .0002 2.169 . 0036 .01)(}0 -. 0 111 . 112 . 0131 .00035
- .0010 2.160 . 0031 .0 102 .0285 113 

### .0113 - . 000'45 .000 4 2 .161. . - . .0012 .0063 -. 0296 Elem 2203/2 

### s · Sb 

### 1960/1 1960/2 Si Pb : units ppm p p m p p m ppm . ppm ppm ppm Avge . 0028 .0341 -.0018 ,0070 -.0014. .0062· . 0005 Ill 

### .0094 .03 78 . 0043 . 0016 . 0013 . 0110 . 00 25 #2 -. 0 171 . 0218 . 0053 . 0300 - . 0253 .0002 - . 0019 113 . .0163 . 0427
- .0149 -. 0105 .019 9 . 0074 . 0010 Elem Se Sn Sr Ti: Tl 

### u v Units ppm ppm ppm ppm . p p m ppm ppm Avg e . 0014 · . 0832 . 00007.
- . 00005 -. 0014 . 0109 -. 0001 ' 

### ft.l . 0014 .0823 .000 16 . OOQ80 

## .oo::10 . o867 .0021 112 - . 0069 . 087. 2 .000 06 -. 00043 .0062 .1227 -. 003 2 113 . 0097 .080 0 .00001 - .00053 - . 0134 - .'1 766 . 0007 Elem y 

### 213Zn Zr:t Zr Units pj:>m ppll) p p m ppm

· Avge · 37.66 .0007 . . . 0007 -,00()3 Ill 

### 37.64 . 0008 .0018 .0014 #2 37 . 58 

## . ooo:i .0002 - . 0007 113 37.76 .0010 .0000 - .0016



### V E S 0 05 6 9 1

### Analysis Report**0~/21/08** 

### 02:48:30 PM 

### Method :

### PSC3~ 

### · Sample Name:

### 1591852:~F7341:1000**~Operator:** 

### BGI Run Time: 08/21/08**14:4 3:0~**  

### Comment: 

### 1591852 Mode: CONC Corro P o actor: 1 

### Blem Unite 

### l\.vge 

### Ill #2 113

0 

### l!lem**Upi~s**



### J>..vge ft1 112 

## 1#3 Elem Upit"s A vge · 

### Ill



### · 112 113 

### ' Elem un its Av.ge 

### Il l 

### 112 #3 

### Elem Units Avge 

### Ill 112 113 

### Elem Units Avge 

### IIi 112 

### ftJ 

### Ag ppm

- o0 006 o0002

- o0032 oOOll 

## ca ppm o0073 o0060 o0093 o0067 Mg . p pm 

### o0188 o0324 

## :out oOlOO 2203/2 

### ppm o

0008 -00026 o0l11 -.0060 

### Se ppm -00018 •o0063

- o0009 .0020 y 

### ppm 37 o89 37o79 37o9l 37o98 

### Al ppm o0328 o0507 o0237 o0238 

### Cd ppm 

### o00079 o00081 •o00003 o00160 Mil 

### ppm 

### o00037 oOOO;l'\ o00016 0 0006'2 

## s ppm 

### 0 0397 o0309 o0430 0 0454 

### Sn 

### ppm • 0167 o0178 o0158 o0164 213Zn 

### ppm 0 0008 o0004 o001 4 o0007 AS 

### ppm 

### .0062 o0076 • o0010**o012~** 

### f=O ppm 

### .0025 o004 . 4 o0021 oOOll 

### Mo ppm • o 0006

- 0 

### 0011 •oOOOO -, 0006 

### Sb pp m o0026 o0062

- .0122 o0137 

### Sr ppm 

### o00021 o00030 0

0001:6 o00016 

### Zn ppm .0024 .0034 .0021 .0017 B 

## ppm o0021 o0018**0002** 

### o0048 ° Cr 

### ppm .003l .0037 

# .ooos

. 0 0049 Nll. 

### ppm 

### 20133 2.140 2:130 2 

### o130 . 1 96Q/l 

### pp m o

0047

0 

### 0116 - o Oll5

0 

### 0141**T~** 

### ppm 0 00 ll3 o00221 0

00077 .00042 

### Zr PP11l 

### o0 0 18 0

0035 o0 010 o0010 

### Ba ppm o00016



## .. . ooop ..**~** 

### .'OOP 19 o

· o00019


### ,. cu " ppm**"';~ 10** **74 o~-**  ;0 7 .>i; 1.Q 0 

### 76**~~. 10**  

### .. '74 . )<l ... 

## 1o ' o

n .**~** 

### . . 

# ,. ' Ni



### . · p pm

. ;0035

' 0 

### 0 05.3 . . 0 0 0 , !)5 o

0046 1960/2 

### ppm . -. 0050

- . 0153 oOOH -0 

### 0041 Tl ·**~m** 

### o0019 . o0098**.~on ·** 



### - .0008 Be 

### ppm

- 0 00 . 051 -.00053

- . 00047

· - o00053 

### Fe ppm

. 0036 . o

0028 o

0048 . o

0030 p 

### ppm o

0092 oOJ,24 o0039 .01'13 

### Si PPm 

### o0071 .0061 .0083 o0070 

### u ppm o1607 .1842 o0307 .26 73 

### pase 1

Bi ppm .

. 0 o008?
• . 0119 0 o0010 o0132 K 

### PP!" 

### 56. 0 84 56.48 56o99 57 

### ."0 . 5 2203/1 ppm 

### .002 4 o0086 

# .0 Ol52 o0137 Pb . 

### ppm o00l3 o0012 .0023 o0006 

### v ppm o00l7 .0010 o0025 .0016 

# j

VES 005692

### . ,: 

### ..... 

## i Analysis Report 08/21/08 02:54:35 

### PM page 1 Method: PSC34**Samp~e** Name: 1591852 :AF7339:

### ~o**oo** / Operator: BG:t Run Time' 08/2 l/ 08 14 : 49 : 09 coaunent: 159l852

. Mode: . CO!lC Corr. Factor : 1 Elem Ag Al As B Ba Be Bi . Units pp m ppm ppm ppm ppm ppm ppm Avg e -. 0018 . . 0129 .001!1 . 0016 - .000 0 8 - . 0 . 0057 .0083 #1 - .0040 · : . 0 1 5 1 .0010 -.0009 -.00013 - . 00064 7-0 0 02 #2 . 0004 . 0350 .0003 . 00 . 43

- · . 00009 •.**OP5~** . : .0110 #3 • . 0017 . oui8 .0(143 

## .oo · l4

- .00002 . - .00052 .**.014~ El~m**  

### Ca 

## C!i co Or 

### cu Fe K Units ppm ppm ppm 

### PP!D ppm 

### PP"': pprfl. Avge . . 004.0 . 00039 . !)009 . 0012 5 . 608 ;0016 19.82 111 . 0 . 039 . 00008 -. oo;n - .0095 5 . 588 .0015 19 . 91 · #2 . 0044 ' 00 . 0$.1 ' ,0032 . 0027 5. 623 • 00 . 3,5 . 19.78**#~** . 0038 .OQ . 057 

## :o . o21
. 001S 5.6>1:5 .Q020 19 .. 78 · : Elem Mg Mn · Mo · N a 

## Ni p 2203/1 . Units ppm p pm 

### PP"' ppm ppm ppm . pp m Avge . 0056 .00019 -.OOH .6933 .0013 · .008 4 .0052 

### Ill -. 03:85 -.00008 •. 0017 . 6855 . 0001 ,0008 .0006 #;! . 0231 . . 00053 -.0000 . 699 4 . 0027 . 0058 • o · i5s # 3 . .0122 . 0001 l
- . 0023 . 69 5 0 . 0010 . 0185 -. 0009 · Elem 2203/2 

## s Sl:> 1 960/1**~60/2** Si 

### Pb Units ppm ppm ppm ppm ppm ppm pp m Avge - . 0024 .0404
- . 0001 , 0116
- . 0078 .0000 .0001 #1 .00 15 .0412**~.0054** .0083 - .0021 . 0002 .0012 #2 -.008 1 .042() . 0063 . 0162 - .0126 . 0002 -.0001 #3 . . 0006 .0380 -.00 1 3 .0102 - .0088 ".0003 -. 0 007 Elem se Sn Sr Tl Tl 

## u v Uni t s ppm ppm ppm ppm ppm ppm ppm Avge .. 0014 .2288 .00007 . 000 4 2 .0026 .0883 - .0004 # 1 . 0013 .2262 -. 000!)7 - . 00 . 083 - . 0],62 -.0166 .0003 112 - . 00 ' 30 .2349 . 000. 1 8 . 00124 .00 97 . 1 995 -.0010 tt3 .. 0025 . 2253 . 00011 .0 0 086 .0144 .0819 - .0005 

### Elem y 213Zn Zn 

### Zr Units ppm ppm ppm ppm Avge 37 . 92 . 0004 . 0008 . 00 ' 06 #1 37 . 84 . 0004
- .0011 . . 002 · 0 #2 38.06 .000 7 . 00!'9 . 002 1

. #3 37.86 . 0003 . 0016 . 0017



### V E S 00569 3

### VES 005694

### Analysis ReJ>orc 08/21/08 03:07:22 .: PM page ·1 

# ! Method:**PSC~ 4**  

### Sample Name: 

# Run Time: 08/21/08 . 15 ,o1: 

## ss CCV 

## / 0p!"rator: BGI CO«Wnent : 159185 2 Mode: CONC Corr . Fact<llr: l



### Elem Ag Al A.s 

## a Ba ae .. Bi Units ppm . ppm ppm ppm . ppm 

# PPm ppm

. Av:g:e . 2494 .9 900 . 2525 . 5053 . 50948 ' . 26163 . 2520

lt1**2~83** 

### 1.0 04 .2482 .5044 . 50884 . 262QO . 2454 #2 . 2475 . 9655 .2481 ,5025 .50891 . 26075 .2466 #3 . 2524· . 1·001 . 2606 .5090 .51070 . 26215 .26 40 Elem Ca Cd Co Cr 

### cu· Fe K 

### T.lnits ppm ppm ppm ppm ppm ppm ppm Avge 5 . 156 .25725 .5125 .5036 .5018 6.159 ' 5 : 0'74 #1 5 , 162 .25679' .5147 .5028 . 5074 6.185 4 . 961 #2 !;.127 .255 68 .5.0.67 • 4998 .4987 . 6.102 5 . 152 #3 

### 5 '. 177 .25929 . 5161 . 5o8 . 2 . 4 993 6.191 5 . 1iO El:em Mg Mn Mo 

### Na . .Ni p 

### · 2203/1 Un its ppm ppm ppm ppm PP1!1 

### ppm ppm ,**~vge .**  

### 3 ' , 039 . 518 24 . 25 ' 59 . 2 - 412 . 2582 2.570 . 5164 Ill 

### 3.021 . 51795 . 2591 2.419 . . 2587 2.**~!1 0**  

### . 5016 ' •f12 . 3.0 12 .51638 . 25S4 2.394 . 2560 2.539 . 5 2 ' 24

#3 3 . 085 . 52041 . 2622 2 . 423 .2599 2.590 . 5252 Elem 2203/2 

## s Sb 1960/1 . 1960/2 Si 

### . PI:> Units pp m · ppm ppm ppm ppm ppm ppm Avge . 5226 . 1. 008 . 2473 .259 4 . 2565 . 455 1 . 5205
' #l . 530.5 1.008 .2 139 . 2399 .2638 . 4579 .5209 #2 . 5227 . 995 1 . 2544 .265 4 . 2511 L.4498 . 5226 #3 . 5147 1.02 1 .2736 .2730 .2548 .4575 .5182 Elem Se Sn Sr Ti Tl 

## u 

## v Un its · Qpm ppm ppm ppm ppm ppm ppm Avge .2575 . 5084 . 2574 8 .50947 .5177 2 . 43 4 .2529 

### # l

# :~m .5038 . 25732 . . 50!184 .5260 2.323 .2527 #2 .5061 · . 25694 . 50716 . .5076 2.380 .2507 #3 . 2608 . 5154 . 25817 . 51142 .5196 2 .598 . 2552 Elem '{ 

### 213Zn Zn Zr . Units ppm

_ ppm ppm pp!ll 1wge 

### 38.26 1,266 1.277 .. S029 Ill 38.34 1.266**.27~** 

### . 5046 #2 3Q.03 1.262 1 .268 . 4990 #3 38.39 1.270 1. 

### 285 ' . 50 ' 49



### VES 005695

### Analysis R,epqrt Method: PSC34 Run Tillie : 

### 08/.21/08 

### Comment: 159i652 Sampl!l Name: CCB**~5!9 :**  

### 01 

### · Mode : CONC 

### i::ox:r . . Factor: - l . 

### E

l em

· units 

### · Avge

Ill 

### 11 .

2

. lf3 .



### Elem Uri.its 

### Avge Ill**~~~** 

### 11 ,

3 

### Elem Un i t Avge 

### lf1 

### 112 113 

### Elem ·

- Units 

### Avge #1 

### 112

. #3



### Elem Units 

### Avge Ill 

### 112 113 Elem Units 

### Avge # 1 

### #2 113 . A9 . 

## ppm .0003

. -. 0020 .

. 00 . 15

. 0()15 

### Ca ppm

. . 0041 Al 

### ppm .011$9

, 008 1 .Oi87 .0240 

### Cd

. ppm

. 00073 

### As

· ppm

.0062

- . 0 , 016 ,

. P079 H. 

### Oi22



### co 

### ppm

. 0029 • 00097 • 0021

. 00054 . 00.25 .0053

. 0' 067 .0

. 0 .

04 . .0006 9 . 0041

## /Jf:..{U**.f.f:~,** 

## "'-.{ 

# p,., f::( Mn '" 

### ftrMovMo _,.. 

# "'-'1 ppm p pm

. 0 ),12 8:.0173 

### 8.0278

. 22 . 0 3/2 PPm**00~3** 

### .0024 .0009 -. 0163. 

### Se ppm .0 008

- . 0016 .0044

- '0

_ 003 y 

### ppm 38.07 37.98 38.09 38.15 . 00065 · . 0023 

## · .poo5,

. O<i0 . 82 '0005 ' 3 

## s ppm .()025 .0085 .003)

- . 004 1 Sn 

### ppm .0075

, 0083 .0 077 .0064 213Zn 

### ppm

. 0017 

### .0 021

. 0023

. 0008 .QQ2 . 9 H.0055

-.0016**'l:t-.~7** 

### H . Ol89 H.Ol25 

### . Vf.

Sr 

### pp m '00020

, 00025 .00017

. 00019 Zn 

### pp m .01)25 • 002 4 . .0025 .0026 

## · . ... ·

.¥" ·- . "i**~** . ••**:: .**  

### · .**~ ~**  

# I**~8/21/08** 

### 03:13 ! 28 PM : 

### page 1 

### Operator : BGI
B 

### ppm

. 004!)

. 00 · 35 .'0.045

. . 0 . 064 Cr 

### ppm .0 035

. 0023 .0043 .0039 

### Na ppm

. (>.1 0 6 .0095

. 0106 .0118 1960/1 

### ppm .014 2 .0080 .0041 

### ,0305 Ti 

### ppm H.00 1 22 H.OOll..4 H, 09113 H.00138



### Zr PP'1' 

### .0020 .0 012

. 0019 H. 0027 '-: · 

### Ba ppm .00020 .00()33

. 0005() -.**0002~** 

### Gu 

### , · ; ppm ' · ' . -' 001?

. · . · . .; . -: :·0041**:,-.~; '** **~: PO** **l2** 

# · it·'' · . o · oo 2 Ni ppm

. 0020 

## -.ooo5**(!~20**
. 0044 

### 1960/2 · 

### ppm

- . 0059

- . 0064

. 0045

- .0158 

### Tl ppm .0097



### . 0006 H.Ol81

.0103 ·Be 

### ppm

- . 00054

- . 0004-7 .

- .000 51 -. 00064 

### Fe 

### ppm .OOH



### . 0049

. OO·P.

. 0006 p



### · ppm

. . 0141

.0052 .Oi74 .0198 

### Si

. ppm

-. 0011 

### -.0005 .0022 -.0050 

## u ppm

. 2200

. ·

1 381 .2366 .2852 ·.: · . 

### Bi ppm . :0118 

### .0043 .0139 ' . H . 0172

K .- . 

### PPI!I :· 

### .0051**0027**

# ~~**g~~~** 

# . .. . .... . 2203 /1 

### ppm

. 0069. 

## .oou .

. ·

- .0 0 54 

### .!\251 PI;> 

### ppm**~** 

### . · 9006 .0020

. - .0012 -. 0025



## · v

ppm .0017

. 0015

. 0037 

### .000 0



### VES 005696

### , Analysis Report Me thod: PSC3 4 

### Sample 

### »a me: CCB**15:2 :54**  

### Pactor: 1 

### Run TiDe : 08/21/08 

### Comment : 1592280 

### Mode:**C~** 

### Corr.

# ~i**-) .** **Avg~** .0067 AS 

### ppm .0002 #1 L-. 0056 11 2 L·. 0061 11 3 L· : 0055 

### Blem U

nits Avg e 

### Ill #2 ' #3 

### Blem Units Avg e 

### #.1 # 2 #3 

### Elem 

### On its Avge 

### #l #2 #3 

### Elem Units Avge Ill 112 113 

### Elem Units Avg . e 

### #1 #2 

### OJ Ca ppm

- .001 2 -.0053

. 0009


## · :ooo8 Mg ppm -.00 42



### - .P047

- .. 0042**.00 38**  220 3 / 2 

### ppm .0063

- .002 5 .012 4 .0090 Se 

### ppm .0 005

- .0043 .0019 

### .0041 y 

### ppm 38 . 00 38 . 0). 38.07 37.93 .0042 • 

## .o no .ooso Cd

# ~~6oo8o ·. OO Q.73

- .OQ08 3 -.00085 

### Mn ppm

- .0 0036

- ·

. 0003 1

- .00037. • . 00037 

## s PPill -.0005

-. 0103 .0050 .0038 

### Sn 

### ppm -. 0025 -.0024

- .0018

- .0033 213Zn 

### ppm .000 4 .0001 .0005 .0006 -. 0046 .0027 .0()23 

### Co ppm

- .OOOj; -.0013



# - .oooo -.0004 

### M

o**PP'~**

- .0001

-. ' 0015 -.0004

. 00 1 5



## - -"" · Sb ppm 

## I L - .0183 

### I



## . ,./ ·



### - . '212 L-. 0 18 7 L". 0 149



### Sr 

### pp m

- . 00004



## - . ooop5

- .00 00 4

- · .00003 Zn 

### ppm -.000 1 -.0006 .0002 .0002 08/21/08 03: 2 7:20 PM

B 

### ppm -.0015

-**.00~9**

- . \)00 4

- .**00~1** 

### C

r PP!lt ;. . 0014

-. 00 . 2 . 5 . 

### -. 0 . 011

- .0004 

### Na 

### ppm

. 0023

. 0019 .' 00 ' 28 .0 0 21 1960/l 

### 'Ppm

- . 0030

. 0072

·-· . 0089 " .0073 

### Ti ppm -.00 035

- .00035

- . 0002 1

- . 000 49 

### Zr ppm -.0006

-. 0006 -.0006 -. 0006 

### Operator : BGI 

### Ba PP'l' -.00027

• . 00065 -. 000!)2 -. 0\)013 

### cu ppin



## - : . ool3 

# ::ggg;

· -. o ' o23 · 

# .Ni ppm , .0013

- . • 0018

- . 00 , 19 . 

## .- .opo2 i960/2 ppm .OQ23 -.0 1 01

. 0073 .Q098 

### Tl 

### ppm .0053 .0 0 62 -. 0029 .0 125 

### Be 

### ppm

- . 00071

- . 00085 -.Ob060 -. 00068 FJ> 

### ppm -. 0002 .
-. 0027 :0013 .0007 p 

### ppm .0062 ,0149**-.002~** .0066 

# si ppm . -.OQSS L-. 0118

- .00 1 5

- . 0032 

### u

# ~~802 -. 1164 -.0895

- .0345 

### page 1



### Bi ppm . -.0076**.90~ 6**  · - .0021

- . 0152 K 

### ppm -.0314 ·.
-. 0278 .

- .0397 -. 0266 2203/1 . 

### ppm -. 0 ' 071 .0097 . 7 . 0.172 -.0155 Pb ' 

### ppm

. 00 1 6 .0016 .0025 .0008 

## v ppm

- . OOll -.0030

· -.0015

.0013



### VES 005697I ·



### · .

st . andard i zat.ion Rpt. 08/ 21 /08 · ' 03 : 36:16 PM**·. pag~**  l ' ' M

ethod : P SCl4 . Standard: CAL-BLK Rlll_l**Ti~ .**  OB/21/08 15:33: 4 8



### Elem 

### A g Sb . 

### A

vge -. 0 1 20 . _**0~40** #1 .0020 .0050 

### 112
- . 014'0 

## .oo7 . o

. . 113 -.0240**~** .024 . 0 .



### VES 005698

### Standa:rdization Method: PSC34 Blem(!nt 1\9 . 

### Sb 

### Wave len 328.068 206.838 

### Report QS/21/JJS 03:36: 20 PM 

### page 1 Slope • Conc(SIR)/IR High std 

### STO,B STD-B Low std ' CAI,.-BLK CAL-BLK 

### Slope .042768 .1 ,

03108 

### Y-intercept ,0005 13**.000~12** Date

### Stand~rdized 

### ·. 08/21/08 03:33 :48 08/21/08 03:33:48



### VES 005699