## SGS Work Order:

Contents: Cover Page Case Narrative Final Report Pages Quality Control Summary Forms Chain of Custody/Sample Receipt Forms 

## Project: Client: 

# SGS North America Inc. Alaska Division Level II Laboratory Data Report

Released by:

Note: Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference. 

## 3354-010 Red Hill BFSF The Environmental Company, Inc. (TEC) 1095622

## CASE NARRATIVE Print Date: 10/30/2009

Workorder No.: 1095622 Project Name: 3354-010 Red Hill BFSF Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID 

## Sample Comments

Sample Type Client Sample ID Refer to the sample receipt form for information on sample condition.

1095622002 AK101 - MS recovery for GRO does not meet QC criteria (biased high). See LCS/LCSD for accuracy.

BMS OWDFMW01-WG-02 MS

1095622003 AK101 - MS/MSD RPD results for GRO does not meet QC criteria (biased high). See LCS/LCSD for accuracy.

BMSD OWDFMW01-WG-02 MSD

934050 8260B - LCS recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected above

the PQL in the associated samples LCS LCS for HBN 222065 [VXX/20165]

934051 8260B - LCSD recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected

above the PQL in the associated samples LCSD LCSD for HBN 222065 [VXX/20165

934053 8260B - CCV recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected

above the PQL in the associated samples CCV CCV for HBN 222066 [VMS/10954]

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2343 f(907 ) 561

.5301 w w w . us.sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

# Laboratory Analytical Report

Project: Client:

Workorder No.: The Environmental Company, Inc. (TEC)



### 1095622

Certification: I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, other than the conditions noted on the sample data sheet(s) and/or the case narrative. This certification applies only to the tested parameters and the specific sample(s) received at the laboratory. 1001 Bishop Street, Suite 1400 Honolulu, HI 96813

Attn: Rick Adkisson T: (808)528-1445 F:(808)528-0768

Heather Hall Heather.Hall@sgs.com Quality Assurance Manager 

### 3354-010 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please contact your SGS Project Manager.

S G S N orth A m erica Inc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2343 f(907 ) 561

.5301 w w w . us.sgs.com M em ber of S G S G roupEnclosed are the analytical results associated with this workorder. As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of our Quality Assurance Plan (QAP), which outlines this program is available at your request.
The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C). Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities. If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 907-562-2343. 

### All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm)
The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit PQL Practical Quantitation Limit (reporting limit). CL Control Limit U Indicates the analyte was analyzed for but not detected. F Indicates value that is greater than or equal to the MDL. J The quantitation is an estimation. ND Indicates the analyte is not detected B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits. D The analyte concentration is the result of dilution. GT Greater Than LT Less Than Q QC parameter out of acceptance range. M A matrix effect was present. E The analyte result is above the calibrated range. R Rejected DF Analytical Dilution Factor JL The analyte was positively identified, but the quantitation is a low estimation. <Surr> Surrogate QC spiked standard <Surr/IS> Surrogate / Internal Standard QC spiked standard QC Quality Control QA Quality Assurance MB Method Blank LCS (D) Laboratory Control Sample (Duplicate) MS(D) Matrix Spike (Duplicate) BMS(D) Site Specific Matrix Spike (Duplicate) RPD Relative Percent Difference ICV Initial Calibration Verification CCV Continuous Calibration Verification MSA Method of Standard Addition Notes: Soil samples are reported on a dry weight basis unless otherwise specified Print Date: 10/30/2009

Notes: All DRO/RRO analyses are integrated per SOP.

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2343 f(907 ) 561

.5301 w w w . us.sgs.com M em ber of S G S G roup

## SAMPLE SUMMARY Client Name: The Environmental Company, Inc. (TEC) Project Name: 3354-010 Red Hill BFSF Workorder No.: 1095622 

## Analytical Methods
Method Description Analytical Method 8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS AFCEE 3.1 8260 (W) SW8260B Dissolved Metals by ICP-MS SW6020 DRO by 8015C (W) SW8015C GRO (W) SW8015C Print Date: 10/30/2009 3:29 pm



## Sample ID Cross Reference
Client Sample ID Lab Sample ID 1095622001 OWDFMW01-WG-02 1095622002 OWDFMW01-WG-02 MS 1095622003 OWDFMW01-WG-02 MSD 1095622004 RHMW04-WG-02 1095622005 RHMWA01-WG-02 1095622006 HDMW2253-03-WG-02 1095622007 TB01-WG-02

S G S N orth A m erica Inc

. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2343 f(907 ) 561

.5301 w w w . us.sgs.com M em ber of S G S G roup (S ociété G énérale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### OWDFMW01-WG-02 SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6155 MXX22423 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6155 Analytical Method: SW6020 Analysis Date/Time: 10/22/09 20:08 Prep Batch: MXX22423 Prep Method: SW3010A Prep Date/Time: 10/21/09 16:15 Container ID:1095622001-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### OWDFMW01-WG-02 SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9728 VXX20181 30.0 1 4-Bromofluorobenzene <surr> 101 50-150 % VFC9728 VXX20181 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9728 Analytical Method: SW8015C Analysis Date/Time: 10/24/09 16:00 Prep Batch: VXX20181 Prep Method: SW5030B Prep Date/Time: 10/24/09 13:29 Container ID:1095622001-A Dilution Factor: 1 Analyst: KPW

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### OWDFMW01-WG-02 SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.444 mg/L XFC8990 XXX21847 0.167 1 5a Androstane <surr> 76.5 50-150 % XFC8990 XXX21847 1
Batch Information Initial Prep Wt./Vol.: 900 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8990 Analytical Method: SW8015C Analysis Date/Time: 10/26/09 11:16 Prep Batch: XXX21847 Prep Method: SW3520C Prep Date/Time: 10/19/09 10:35 Container ID:1095622001-J Dilution Factor: 1 Analyst: KDC

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### OWDFMW01-WG-02 SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10954 VXX20165 0.120 1 Toluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Styrene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromomethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Acetone ND 10.0 ug/L VMS10954 VXX20165 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10954 VXX20165 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10954 VXX20165 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 Chloroform ND 1.00 ug/L VMS10954 VXX20165 0.300 1 Bromobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromomethane ND 3.00 ug/L VMS10954 VXX20165 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### OWDFMW01-WG-02 SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 Methylene chloride ND 5.00 ug/L VMS10954 VXX20165 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Naphthalene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 o-Xylene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromoform ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Trichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloroethane-D4 <surr> 105 73-120 % VMS10954 VXX20165 1 Toluene-d8 <surr> 98.9 80-120 % VMS10954 VXX20165 1 4-Bromofluorobenzene <surr> 102 76-120 % VMS10954 VXX20165 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10954 Analytical Method: SW8260B Analysis Date/Time: 10/20/09 17:37 Prep Batch: VXX20165 Prep Method: SW5030B Prep Date/Time: 10/20/09 08:22 Container ID:1095622001-E Dilution Factor: 1 Analyst: SCL

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### OWDFMW01-WG-02 SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Acenaphthene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Fluorene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Phenanthrene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Anthracene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Fluoranthene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Pyrene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Benzo(a)Anthracene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Chrysene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Benzo[b]Fluoranthene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Benzo[k]fluoranthene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Benzo[a]pyrene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Indeno[1,2,3-c,d] pyrene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Dibenzo[a,h]anthracene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Benzo[g,h,i]perylene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Naphthalene ND 0.112 ug/L XMS5160 XXX21834 0.0346 1 1-Methylnaphthalene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 2-Methylnaphthalene ND 0.0559 ug/L XMS5160 XXX21834 0.0168 1 Terphenyl-d14 <surr> 96.5 50-135 % XMS5160 XXX21834 1
Batch Information Initial Prep Wt./Vol.: 895 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5160 Analytical Method: 8270D SIMS Analysis Date/Time: 10/24/09 08:09 Prep Batch: XXX21834 Prep Method: SW3520C Prep Date/Time: 10/16/09 09:15 Container ID:1095622001-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMW04-WG-02 SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6155 MXX22423 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6155 Analytical Method: SW6020 Analysis Date/Time: 10/22/09 20:18 Prep Batch: MXX22423 Prep Method: SW3010A Prep Date/Time: 10/21/09 16:15 Container ID:1095622004-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMW04-WG-02 SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9728 VXX20181 30.0 1 4-Bromofluorobenzene <surr> 99.8 50-150 % VFC9728 VXX20181 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9728 Analytical Method: SW8015C Analysis Date/Time: 10/24/09 17:08 Prep Batch: VXX20181 Prep Method: SW5030B Prep Date/Time: 10/24/09 13:29 Container ID:1095622004-B Dilution Factor: 1 Analyst: KPW

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMW04-WG-02 SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.452 mg/L XFC8990 XXX21847 0.169 1 5a Androstane <surr> 83.1 50-150 % XFC8990 XXX21847 1
Batch Information Initial Prep Wt./Vol.: 885 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8990 Analytical Method: SW8015C Analysis Date/Time: 10/26/09 11:47 Prep Batch: XXX21847 Prep Method: SW3520C Prep Date/Time: 10/19/09 10:35 Container ID:1095622004-J Dilution Factor: 1 Analyst: KDC

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMW04-WG-02 SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10954 VXX20165 0.120 1 Toluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Styrene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromomethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Acetone ND 10.0 ug/L VMS10954 VXX20165 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10954 VXX20165 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10954 VXX20165 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 Chloroform ND 1.00 ug/L VMS10954 VXX20165 0.300 1 Bromobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromomethane ND 3.00 ug/L VMS10954 VXX20165 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMW04-WG-02 SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 Methylene chloride ND 5.00 ug/L VMS10954 VXX20165 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Naphthalene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 o-Xylene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromoform ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Trichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloroethane-D4 <surr> 105 73-120 % VMS10954 VXX20165 1 Toluene-d8 <surr> 100 80-120 % VMS10954 VXX20165 1 4-Bromofluorobenzene <surr> 103 76-120 % VMS10954 VXX20165 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10954 Analytical Method: SW8260B Analysis Date/Time: 10/20/09 21:32 Prep Batch: VXX20165 Prep Method: SW5030B Prep Date/Time: 10/20/09 08:22 Container ID:1095622004-A Dilution Factor: 1 Analyst: SCL

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMW04-WG-02 SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Acenaphthene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Fluorene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Phenanthrene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Anthracene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Fluoranthene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Pyrene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Benzo(a)Anthracene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Chrysene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Benzo[b]Fluoranthene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Benzo[k]fluoranthene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Benzo[a]pyrene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Indeno[1,2,3-c,d] pyrene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Dibenzo[a,h]anthracene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Benzo[g,h,i]perylene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Naphthalene ND 0.115 ug/L XMS5161 XXX21834 0.0356 1 1-Methylnaphthalene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 2-Methylnaphthalene ND 0.0575 ug/L XMS5161 XXX21834 0.0172 1 Terphenyl-d14 <surr> 91.4 50-135 % XMS5161 XXX21834 1
Batch Information Initial Prep Wt./Vol.: 870 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5161 Analytical Method: 8270D SIMS Analysis Date/Time: 10/24/09 15:53 Prep Batch: XXX21834 Prep Method: SW3520C Prep Date/Time: 10/16/09 09:15 Container ID:1095622004-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMWA01-WG-02 SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6155 MXX22423 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6155 Analytical Method: SW6020 Analysis Date/Time: 10/22/09 20:20 Prep Batch: MXX22423 Prep Method: SW3010A Prep Date/Time: 10/21/09 16:15 Container ID:1095622005-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMWA01-WG-02 SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9728 VXX20181 30.0 1 4-Bromofluorobenzene <surr> 102 50-150 % VFC9728 VXX20181 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9728 Analytical Method: SW8015C Analysis Date/Time: 10/24/09 17:31 Prep Batch: VXX20181 Prep Method: SW5030B Prep Date/Time: 10/24/09 13:29 Container ID:1095622005-B Dilution Factor: 1 Analyst: KPW

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMWA01-WG-02 SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.465 mg/L XFC8990 XXX21847 0.174 1 5a Androstane <surr> 76 50-150 % XFC8990 XXX21847 1
Batch Information Initial Prep Wt./Vol.: 860 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8990 Analytical Method: SW8015C Analysis Date/Time: 10/26/09 11:58 Prep Batch: XXX21847 Prep Method: SW3520C Prep Date/Time: 10/19/09 10:35 Container ID:1095622005-I Dilution Factor: 1 Analyst: KDC

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMWA01-WG-02 SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10954 VXX20165 0.120 1 Toluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Styrene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromomethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Acetone ND 10.0 ug/L VMS10954 VXX20165 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10954 VXX20165 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10954 VXX20165 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 Chloroform ND 1.00 ug/L VMS10954 VXX20165 0.300 1 Bromobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromomethane ND 3.00 ug/L VMS10954 VXX20165 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMWA01-WG-02 SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 Methylene chloride ND 5.00 ug/L VMS10954 VXX20165 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Naphthalene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 o-Xylene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromoform ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Trichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloroethane-D4 <surr> 103 73-120 % VMS10954 VXX20165 1 Toluene-d8 <surr> 97.4 80-120 % VMS10954 VXX20165 1 4-Bromofluorobenzene <surr> 104 76-120 % VMS10954 VXX20165 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10954 Analytical Method: SW8260B Analysis Date/Time: 10/20/09 20:58 Prep Batch: VXX20165 Prep Method: SW5030B Prep Date/Time: 10/20/09 08:22 Container ID:1095622005-A Dilution Factor: 1 Analyst: SCL

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### RHMWA01-WG-02 SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Acenaphthene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Fluorene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Phenanthrene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Anthracene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Fluoranthene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Pyrene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Benzo(a)Anthracene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Chrysene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Benzo[b]Fluoranthene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Benzo[k]fluoranthene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Benzo[a]pyrene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Indeno[1,2,3-c,d] pyrene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Dibenzo[a,h]anthracene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Benzo[g,h,i]perylene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Naphthalene ND 0.112 ug/L XMS5161 XXX21834 0.0348 1 1-Methylnaphthalene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 2-Methylnaphthalene ND 0.0562 ug/L XMS5161 XXX21834 0.0169 1 Terphenyl-d14 <surr> 95.5 50-135 % XMS5161 XXX21834 1
Batch Information Initial Prep Wt./Vol.: 890 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5161 Analytical Method: 8270D SIMS Analysis Date/Time: 10/24/09 16:28 Prep Batch: XXX21834 Prep Method: SW3520C Prep Date/Time: 10/16/09 09:15 Container ID:1095622005-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### HDMW2253-03-WG-02 SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 ug/L MMS6155 MXX22423 0.310 5
Batch Information Initial Prep Wt./Vol.: 50 mL Prep Extract Vol.: 50 mL Analytical Batch: MMS6155 Analytical Method: SW6020 Analysis Date/Time: 10/22/09 20:22 Prep Batch: MXX22423 Prep Method: SW3010A Prep Date/Time: 10/21/09 16:15 Container ID:1095622006-G Dilution Factor: 5 Analyst: NRB

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### HDMW2253-03-WG-02 SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9728 VXX20181 30.0 1 4-Bromofluorobenzene <surr> 101 50-150 % VFC9728 VXX20181 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9728 Analytical Method: SW8015C Analysis Date/Time: 10/24/09 17:54 Prep Batch: VXX20181 Prep Method: SW5030B Prep Date/Time: 10/24/09 13:29 Container ID:1095622006-C Dilution Factor: 1 Analyst: KPW

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### HDMW2253-03-WG-02 SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Semivolatile Organic Fuels Department

MDL DF
Diesel Range Organics ND 0.494 mg/L XFC8990 XXX21847 0.185 1 5a Androstane <surr> 73.3 50-150 % XFC8990 XXX21847 1
Batch Information Initial Prep Wt./Vol.: 810 mL Prep Extract Vol.: 1 mL Analytical Batch: XFC8990 Analytical Method: SW8015C Analysis Date/Time: 10/26/09 12:08 Prep Batch: XXX21847 Prep Method: SW3520C Prep Date/Time: 10/19/09 10:35 Container ID:1095622006-J Dilution Factor: 1 Analyst: KDC

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### HDMW2253-03-WG-02 SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10954 VXX20165 0.120 1 Toluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Styrene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromomethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Acetone ND 10.0 ug/L VMS10954 VXX20165 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10954 VXX20165 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10954 VXX20165 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 Chloroform ND 1.00 ug/L VMS10954 VXX20165 0.300 1 Bromobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromomethane ND 3.00 ug/L VMS10954 VXX20165 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### HDMW2253-03-WG-02 SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 Methylene chloride ND 5.00 ug/L VMS10954 VXX20165 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Naphthalene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 o-Xylene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromoform ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Trichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloroethane-D4 <surr> 105 73-120 % VMS10954 VXX20165 1 Toluene-d8 <surr> 98.8 80-120 % VMS10954 VXX20165 1 4-Bromofluorobenzene <surr> 102 76-120 % VMS10954 VXX20165 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10954 Analytical Method: SW8260B Analysis Date/Time: 10/20/09 20:25 Prep Batch: VXX20165 Prep Method: SW5030B Prep Date/Time: 10/20/09 08:22 Container ID:1095622006-B Dilution Factor: 1 Analyst: SCL

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### HDMW2253-03-WG-02 SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Acenaphthene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Fluorene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Phenanthrene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Anthracene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Fluoranthene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Pyrene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Benzo(a)Anthracene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Chrysene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Benzo[b]Fluoranthene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Benzo[k]fluoranthene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Benzo[a]pyrene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Indeno[1,2,3-c,d] pyrene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Dibenzo[a,h]anthracene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Benzo[g,h,i]perylene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Naphthalene ND 0.113 ug/L XMS5161 XXX21834 0.0350 1 1-Methylnaphthalene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 2-Methylnaphthalene ND 0.0565 ug/L XMS5161 XXX21834 0.0169 1 Terphenyl-d14 <surr> 84.8 50-135 % XMS5161 XXX21834 1
Batch Information Initial Prep Wt./Vol.: 885 mL Prep Extract Vol.: 1 mL Analytical Batch: XMS5161 Analytical Method: 8270D SIMS Analysis Date/Time: 10/24/09 17:03 Prep Batch: XXX21834 Prep Method: SW3520C Prep Date/Time: 10/16/09 09:15 Container ID:1095622006-H Dilution Factor: 1 Analyst: JDH

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### TB01-WG-02 SGS Ref. #: 1095622007 Collection Date/Time: 10/13/09 08:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Fuels Department

MDL DF
Gasoline Range Organics ND 100 ug/L VFC9728 VXX20181 30.0 1 4-Bromofluorobenzene <surr> 98.4 50-150 % VFC9728 VXX20181 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VFC9728 Analytical Method: SW8015C Analysis Date/Time: 10/24/09 15:37 Prep Batch: VXX20181 Prep Method: SW5030B Prep Date/Time: 10/24/09 13:29 Container ID:1095622007-B Dilution Factor: 1 Analyst: KPW

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### TB01-WG-02 SGS Ref. #: 1095622007 Collection Date/Time: 10/13/09 08:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 ug/L VMS10954 VXX20165 0.120 1 Toluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Ethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 n-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,4-Dichlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dichloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3,5-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chlorobenzene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 cis-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 4-Isopropyltoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 cis-1,3-Dichloropropene ND 0.500 ug/L VMS10954 VXX20165 0.150 1 n-Propylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Styrene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromomethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,3-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Acetone ND 10.0 ug/L VMS10954 VXX20165 3.10 1 1,1,2,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,2-Dibromo-3-chloropropane ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Methyl-t-butyl ether ND 5.00 ug/L VMS10954 VXX20165 1.50 1 Tetrachloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dibromochloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,3-Dichloropropane ND 0.400 ug/L VMS10954 VXX20165 0.120 1 1,2-Dibromoethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Carbon tetrachloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1,2-Tetrachloroethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 Chloroform ND 1.00 ug/L VMS10954 VXX20165 0.300 1 Bromobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Chloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromomethane ND 3.00 ug/L VMS10954 VXX20165 0.940 1 Bromochloromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Vinyl chloride ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Dichlorodifluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)

### The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: 

### TB01-WG-02 SGS Ref. #: 1095622007 Collection Date/Time: 10/13/09 08:05 Receipt Date/Time: 10/15/09 11:00 Project ID: 3354-010 Red Hill BFSF Matrix: Water (Surface, Eff., Ground)

Analytical Batch Prep

Batch PQL/CL Units Qualifiers Parameter Result 

### Volatile Gas Chromatography/Mass Spectroscopy

MDL DF Chloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 sec-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromodichloromethane ND 0.500 ug/L VMS10954 VXX20165 0.150 1 1,1-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Butanone (MEK) ND 10.0 ug/L VMS10954 VXX20165 3.10 1 Methylene chloride ND 5.00 ug/L VMS10954 VXX20165 1.00 1 Trichlorofluoromethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 P & M -Xylene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 Naphthalene ND 2.00 ug/L VMS10954 VXX20165 0.620 1 o-Xylene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Bromoform ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1-Chlorohexane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,4-Trimethylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 tert-Butylbenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,1-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2-Chlorotoluene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Trichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 trans-1,2-Dichloroethene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 2,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Hexachlorobutadiene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 Isopropylbenzene (Cumene) ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloropropane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1-Dichloropropene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,1,2-Trichloroethane ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,3-Dichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2,3-Trichlorobenzene ND 1.00 ug/L VMS10954 VXX20165 0.310 1 1,2-Dichloroethane-D4 <surr> 106 73-120 % VMS10954 VXX20165 1 Toluene-d8 <surr> 100 80-120 % VMS10954 VXX20165 1 4-Bromofluorobenzene <surr> 105 76-120 % VMS10954 VXX20165 1
Batch Information Initial Prep Wt./Vol.: 5 mL Prep Extract Vol.: 5 mL Analytical Batch: VMS10954 Analytical Method: SW8260B Analysis Date/Time: 10/20/09 19:51 Prep Batch: VXX20165 Prep Method: SW5030B Prep Date/Time: 10/20/09 08:22 Container ID:1095622007-A Dilution Factor: 1 Analyst: SCL

S G S N orth A m ericaInc. A laskaD ivision 200 W est P otterD rive A nchorage A laska 99518 t(907 ) 562

.2 343 f(907 ) 561

.5 301 w w w . us.sgs.com M em ber of S G S G rou p (S ociété G éné rale de S urveillance)Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 932199 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX21834 SW3520C 10/16/2009 QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Polynuclear Aromatics GC/MS 

### Acenaphthylene ND 0.0500 ug/L 10/24/09 

### 0.0150 Acenaphthene ND 0.0500 ug/L 10/24/09 

### 0.0150 Fluorene ND 0.0500 ug/L 10/24/09 

### 0.0150 Phenanthrene ND 0.0500 ug/L 10/24/09 

### 0.0150 Anthracene ND 0.0500 ug/L 10/24/09 

### 0.0150 Fluoranthene ND 0.0500 ug/L 10/24/09 

### 0.0150 Pyrene ND 0.0500 ug/L 10/24/09 

### 0.0150 Benzo(a)Anthracene ND 0.0500 ug/L 10/24/09 

### 0.0150 Chrysene ND 0.0500 ug/L 10/24/09 

### 0.0150 Benzo[b]Fluoranthene ND 0.0500 ug/L 10/24/09 

### 0.0150 Benzo[k]fluoranthene ND 0.0500 ug/L 10/24/09 

### 0.0150 Benzo[a]pyrene ND 0.0500 ug/L 10/24/09 

### 0.0150 Indeno[1,2,3-c,d] pyrene ND 0.0500 ug/L 10/24/09 

### 0.0150 Dibenzo[a,h]anthracene ND 0.0500 ug/L 10/24/09 

### 0.0150 Benzo[g,h,i]perylene ND 0.0500 ug/L 10/24/09 

### 0.0150 Naphthalene ND 0.100 ug/L 10/24/09 

### 0.0310 1-Methylnaphthalene ND 0.0500 ug/L 10/24/09 

### 0.0150 2-Methylnaphthalene ND 0.0500 ug/L 10/24/09 

### 0.0150 Surrogates 

### Terphenyl-d14 <surr> 93.7 50-135 % 10/24/09

Instrument Method Batch XMS5160

8270D SIMS HP 6890 Series II MS2 SVOAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 932694 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX21847 SW3520C 10/19/2009 QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Semivolatile Organic Fuels Department 

### Diesel Range Organics ND 0.400 mg/L 10/26/09 

### 0.150 Surrogates


### 5a Androstane <surr> 79.2 60-120 % 10/26/09

Instrument Method Batch XFC8990

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 933881 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22423 SW3010A 10/21/2009 QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Metals by ICP/MS



### Lead ND 1.00 ug/L 10/22/09 

### 0.310

Instrument Method Batch MMS6155

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934049 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009 QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934049 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy



### Benzene ND 0.400 ug/L 10/20/09 

### 0.120 Toluene ND 1.00 ug/L 10/20/09 

### 0.310 Ethylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 n-Butylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 1,4-Dichlorobenzene ND 0.500 ug/L 10/20/09 

### 0.150 1,2-Dichloroethane ND 0.500 ug/L 10/20/09 

### 0.150 1,3,5-Trimethylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 4-Chlorotoluene ND 1.00 ug/L 10/20/09 

### 0.310 Chlorobenzene ND 0.500 ug/L 10/20/09 

### 0.150 4-Methyl-2-pentanone (MIBK) ND 10.0 ug/L 10/20/09 

### 3.10 cis-1,2-Dichloroethene ND 1.00 ug/L 10/20/09 

### 0.310 4-Isopropyltoluene ND 1.00 ug/L 10/20/09 

### 0.310 cis-1,3-Dichloropropene ND 0.500 ug/L 10/20/09 

### 0.150 n-Propylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 Styrene ND 1.00 ug/L 10/20/09 

### 0.310 Dibromomethane ND 1.00 ug/L 10/20/09 

### 0.310 trans-1,3-Dichloropropene ND 1.00 ug/L 10/20/09 

### 0.310 1,2,4-Trichlorobenzene ND 1.00 ug/L 10/20/09 

### 0.310 Acetone ND 10.0 ug/L 10/20/09 

### 3.10 1,1,2,2-Tetrachloroethane ND 0.500 ug/L 10/20/09 

### 0.150 1,2-Dibromo-3-chloropropane ND 2.00 ug/L 10/20/09 

### 0.620 Methyl-t-butyl ether ND 5.00 ug/L 10/20/09 

### 1.50 Tetrachloroethene ND 1.00 ug/L 10/20/09 

### 0.310 Dibromochloromethane ND 0.500 ug/L 10/20/09 

### 0.150 1,3-Dichloropropane ND 0.400 ug/L 10/20/09 

### 0.120 1,2-Dibromoethane ND 1.00 ug/L 10/20/09 

### 0.310 Carbon tetrachloride ND 1.00 ug/L 10/20/09 

### 0.310 1,1,1,2-Tetrachloroethane ND 0.500 ug/L 10/20/09 

### 0.150 Chloroform ND 1.00 ug/L 10/20/09 

### 0.300 Bromobenzene ND 1.00 ug/L 10/20/09 

### 0.310 Chloromethane ND 1.00 ug/L 10/20/09 

### 0.310 1,2,3-Trichloropropane ND 1.00 ug/L 10/20/09 

### 0.310 Bromomethane ND 3.00 ug/L 10/20/09 

### 0.940 Bromochloromethane ND 1.00 ug/L 10/20/09 

### 0.310 Vinyl chloride ND 1.00 ug/L 10/20/09 

### 0.310 Dichlorodifluoromethane ND 1.00 ug/L 10/20/09 

### 0.310 Chloroethane ND 1.00 ug/L 10/20/09 

### 0.310 sec-Butylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 Bromodichloromethane ND 0.500 ug/L 10/20/09 

### 0.150Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934049 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Gas Chromatography/Mass Spectroscopy


### 1,1-Dichloroethene ND 1.00 ug/L 10/20/09 

### 0.310 2-Butanone (MEK) ND 10.0 ug/L 10/20/09 

### 3.10 Methylene chloride ND 5.00 ug/L 10/20/09 

### 1.00 Trichlorofluoromethane ND 1.00 ug/L 10/20/09 

### 0.310 P & M -Xylene ND 2.00 ug/L 10/20/09 

### 0.620 Naphthalene ND 2.00 ug/L 10/20/09 

### 0.620 o-Xylene ND 1.00 ug/L 10/20/09 

### 0.310 Bromoform ND 1.00 ug/L 10/20/09 

### 0.310 1-Chlorohexane ND 1.00 ug/L 10/20/09 

### 0.310 1,2,4-Trimethylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 tert-Butylbenzene ND 1.00 ug/L 10/20/09 

### 0.310 1,1,1-Trichloroethane ND 1.00 ug/L 10/20/09 

### 0.310 1,1-Dichloroethane ND 1.00 ug/L 10/20/09 

### 0.310 2-Chlorotoluene ND 1.00 ug/L 10/20/09 

### 0.310 Trichloroethene ND 1.00 ug/L 10/20/09 

### 0.310 trans-1,2-Dichloroethene ND 1.00 ug/L 10/20/09 

### 0.310 1,2-Dichlorobenzene ND 1.00 ug/L 10/20/09 

### 0.310 2,2-Dichloropropane ND 1.00 ug/L 10/20/09 

### 0.310 Hexachlorobutadiene ND 1.00 ug/L 10/20/09 

### 0.310 Isopropylbenzene (Cumene) ND 1.00 ug/L 10/20/09 

### 0.310 1,2-Dichloropropane ND 1.00 ug/L 10/20/09 

### 0.310 1,1-Dichloropropene ND 1.00 ug/L 10/20/09 

### 0.310 1,1,2-Trichloroethane ND 1.00 ug/L 10/20/09 

### 0.310 1,3-Dichlorobenzene ND 1.00 ug/L 10/20/09 

### 0.310 1,2,3-Trichlorobenzene ND 1.00 ug/L 10/20/09 

### 0.310 Surrogates 

### 1,2-Dichloroethane-D4 <surr> 103 73-120 % 10/20/09 

### Toluene-d8 <surr> 102 80-120 % 10/20/09 

### 4-Bromofluorobenzene <surr> 104 76-120 % 10/20/09

Instrument Method Batch VMS10954

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934942 Method Blank The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20181 SW5030B 10/24/2009 QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter Results Reporting/Control Limit Units Analysis Date MDL


### Volatile Fuels Department 

### Gasoline Range Organics ND 100 ug/L 10/24/09 

### 30.0 Surrogates


### 4-Bromofluorobenzene <surr> 103 50-150 % 10/24/09

Instrument Method Batch VFC9728

SW8015C HP 5890 Series II PID+HECD VBA

## - PRELIMINARY -

Matrix SGS Ref.# Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep

QC results affect the following production samples:

Parameter QC Result Analysis Date RPD RPD

Limits Original Result Units Surrogates

Batch Method InstrumentMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 932200 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX21834 SW3520C 10/16/2009

QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS 

### Acenaphthylene LCS 0.411 82 ( 50-105 ) 0.5 ug/L 10/24/2009
Acenaphthene LCS 0.412 83 ( 45-110 ) 0.5 ug/L 10/24/2009

Fluorene LCS 0.421 84 ( 50-110 ) 0.5 ug/L 10/24/2009

Phenanthrene LCS 0.438 88 ( 50-115 ) 0.5 ug/L 10/24/2009

Anthracene LCS 0.436 87 ( 55-110 ) 0.5 ug/L 10/24/2009

Fluoranthene LCS 0.486 97 ( 55-125 ) 0.5 ug/L 10/24/2009
Pyrene LCS 0.470 94 ( 50-130 ) 0.5 ug/L 10/24/2009
Benzo(a)Anthracene LCS 0.476 95 ( 55-120 ) 0.5 ug/L 10/24/2009
Chrysene LCS 0.470 94 ( 55-120 ) 0.5 ug/L 10/24/2009
Benzo[b]Fluoranthene LCS 0.469 94 ( 46-130 ) 0.5 ug/L 10/24/2009
Benzo[k]fluoranthene LCS 0.463 93 ( 60-125 ) 0.5 ug/L 10/24/2009
Benzo[a]pyrene LCS 0.464 93 ( 55-120 ) 0.5 ug/L 10/24/2009
Indeno[1,2,3-c,d] pyrene LCS 0.435 87 ( 45-125 ) 0.5 ug/L 10/24/2009
Dibenzo[a,h]anthracene LCS 0.426 85 ( 41-140 ) 0.5 ug/L 10/24/2009
Benzo[g,h,i]perylene LCS 0.441 88 ( 46-125 ) 0.5 ug/L 10/24/2009
Naphthalene LCS 0.406 81 ( 42-100 ) 0.5 ug/L 10/24/2009
1-Methylnaphthalene LCS 0.416 83 ( 46-115 ) 0.5 ug/L 10/24/2009
2-Methylnaphthalene LCS 0.391 78 ( 45-105 ) 0.5 ug/L 10/24/2009

Surrogates 

### Terphenyl-d14 <surr> LCS 87 ( 50-135 ) 10/24/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 932200 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX21834 SW3520C 10/16/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5160

8270D SIMS HP 6890 Series II MS2 SVOAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 932696 Lab Control Sample 932698 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) XXX21847 SW3520C 10/19/2009

QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Semivolatile Organic Fuels Department 

### Diesel Range Organics LCS 4.21 84 ( 75-125 ) 5 mg/L 10/26/2009 LCSD 4.02 81 4 (< 20 ) 5 mg/L 10/26/2009

Surrogates 

### 5a Androstane <surr> LCS 88 ( 60-120 ) 10/26/2009 LCSD 85 3 10/26/2009

Batch Method Instrument 

### XFC8990

SW8015C HP 6890 Series II FID SV D RMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 933882 Lab Control Sample
The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) MXX22423 SW3010A 10/21/2009

QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Metals by ICP/MS


### Lead LCS 1020 102 ( 80-120 ) 1000 ug/L 10/22/2009

Batch Method Instrument 

### MMS6155

SW6020 Perkin Elmer Sciex ICP-MS P3Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene LCS 28.3 94 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.0 90 5 (< 20 ) 30 ug/L 10/20/2009

Toluene LCS 27.4 91 ( 77-120 ) 30 ug/L 10/20/2009 LCSD 26.3 88 4 (< 20 ) 30 ug/L 10/20/2009
Ethylbenzene LCS 29.3 98 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 28.4 95 3 (< 20 ) 30 ug/L 10/20/2009
n-Butylbenzene LCS 30.7 102 ( 80-124 ) 30 ug/L 10/20/2009 LCSD 29.1 97 5 (< 20 ) 30 ug/L 10/20/2009
1,4-Dichlorobenzene LCS 28.5 95 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.7 93 3 (< 20 ) 30 ug/L 10/20/2009
1,2-Dichloroethane LCS 27.7 92 ( 80-129 ) 30 ug/L 10/20/2009 LCSD 26.1 87 6 (< 20 ) 30 ug/L 10/20/2009
1,3,5-Trimethylbenzene LCS 29.3 98 ( 80-128 ) 30 ug/L 10/20/2009 LCSD 27.6 92 6 (< 20 ) 30 ug/L 10/20/2009

4-Chlorotoluene LCS 29.0 97 ( 79-128 ) 30 ug/L 10/20/2009 LCSD 27.8 93 4 (< 20 ) 30 ug/L 10/20/2009

Chlorobenzene LCS 28.7 96 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.8 93 3 (< 20 ) 30 ug/L 10/20/2009
4-Methyl-2-pentanone (MIBK) LCS 93.3 104 ( 69-134 ) 90 ug/L 10/20/2009 LCSD 90.4 100 3 (< 20 ) 90 ug/L 10/20/2009
cis-1,2-Dichloroethene LCS 26.4 88 ( 80-125 ) 30 ug/L 10/20/2009 LCSD 25.4 85 4 (< 20 ) 30 ug/L 10/20/2009
4-Isopropyltoluene LCS 30.6 102 ( 80-125 ) 30 ug/L 10/20/2009 LCSD 29.1 97 5 (< 20 ) 30 ug/L 10/20/2009
cis-1,3-Dichloropropene LCS 33.1 110 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 30.4 101 9 (< 20 ) 30 ug/L 10/20/2009
n-Propylbenzene LCS 29.0 97 ( 80-129 ) 30 ug/L 10/20/2009 LCSD 27.9 93 4 (< 20 ) 30 ug/L 10/20/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### Styrene LCS 30.2 101 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 29.3 98 3 (< 20 ) 30 ug/L 10/20/2009

Dibromomethane LCS 29.6 99 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 28.4 95 4 (< 20 ) 30 ug/L 10/20/2009
trans-1,3-Dichloropropene LCS 28.6 96 ( 80-124 ) 30 ug/L 10/20/2009 LCSD 27.2 91 5 (< 20 ) 30 ug/L 10/20/2009
1,2,4-Trichlorobenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 30.0 100 4 (< 20 ) 30 ug/L 10/20/2009

Acetone LCS 159 176 ( 50-135 ) * 90 ug/L 10/20/2009 LCSD 142 157 * 11 (< 20 ) 90 ug/L 10/20/2009
1,1,2,2-Tetrachloroethane LCS 29.0 97 ( 76-123 ) 30 ug/L 10/20/2009 LCSD 27.9 93 4 (< 20 ) 30 ug/L 10/20/2009
1,2-Dibromo-3-chloropropane LCS 30.9 103 ( 73-130 ) 30 ug/L 10/20/2009 LCSD 31.0 103 0 (< 20 ) 30 ug/L 10/20/2009
Methyl-t-butyl ether LCS 42.1 94 ( 80-120 ) 45 ug/L 10/20/2009 LCSD 39.2 87 7 (< 20 ) 45 ug/L 10/20/2009

Tetrachloroethene LCS 29.4 98 ( 79-122 ) 30 ug/L 10/20/2009 LCSD 28.7 96 2 (< 20 ) 30 ug/L 10/20/2009

Dibromochloromethane LCS 29.2 97 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.6 92 6 (< 20 ) 30 ug/L 10/20/2009
1,3-Dichloropropane LCS 28.2 94 ( 80-121 ) 30 ug/L 10/20/2009 LCSD 27.6 92 2 (< 20 ) 30 ug/L 10/20/2009
1,2-Dibromoethane LCS 29.9 100 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 28.5 95 5 (< 20 ) 30 ug/L 10/20/2009

Carbon tetrachloride LCS 28.1 94 ( 80-126 ) 30 ug/L 10/20/2009 LCSD 26.7 89 5 (< 20 ) 30 ug/L 10/20/2009
1,1,1,2-Tetrachloroethane LCS 28.5 95 ( 80-120 ) 30 ug/L 10/20/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### LCSD 27.3 91 4 (< 20 ) 30 ug/L 10/20/2009

Chloroform LCS 27.9 93 ( 80-124 ) 30 ug/L 10/20/2009 LCSD 26.4 88 6 (< 20 ) 30 ug/L 10/20/2009

Bromobenzene LCS 29.2 97 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.6 92 6 (< 20 ) 30 ug/L 10/20/2009

Chloromethane LCS 38.7 129 ( 67-125 ) * 30 ug/L 10/20/2009 LCSD 36.7 122 5 (< 20 ) 30 ug/L 10/20/2009
1,2,3-Trichloropropane LCS 27.6 92 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 26.8 89 3 (< 20 ) 30 ug/L 10/20/2009

Bromomethane LCS 33.3 111 ( 30-140 ) 30 ug/L 10/20/2009 LCSD 33.4 111 0 (< 20 ) 30 ug/L 10/20/2009

Bromochloromethane LCS 28.3 94 ( 77-129 ) 30 ug/L 10/20/2009 LCSD 26.8 89 6 (< 20 ) 30 ug/L 10/20/2009
Vinyl chloride LCS 38.0 127 ( 72-145 ) 30 ug/L 10/20/2009 LCSD 36.0 120 5 (< 20 ) 30 ug/L 10/20/2009

Dichlorodifluoromethane LCS 49.8 166 ( 62-153 ) * 30 ug/L 10/20/2009 LCSD 46.8 156 * 6 (< 20 ) 30 ug/L 10/20/2009

Chloroethane LCS 30.5 102 ( 67-133 ) 30 ug/L 10/20/2009 LCSD 29.5 99 3 (< 20 ) 30 ug/L 10/20/2009
sec-Butylbenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 28.4 95 4 (< 20 ) 30 ug/L 10/20/2009

Bromodichloromethane LCS 32.4 108 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 30.3 101 7 (< 20 ) 30 ug/L 10/20/2009
1,1-Dichloroethene LCS 29.2 97 ( 76-130 ) 30 ug/L 10/20/2009 LCSD 27.8 93 5 (< 20 ) 30 ug/L 10/20/2009
2-Butanone (MEK) LCS 118 131 ( 66-136 ) 90 ug/L 10/20/2009 LCSD 115 128 2 (< 20 ) 90 ug/L 10/20/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy 

### Methylene chloride LCS 29.5 98 ( 63-131 ) 30 ug/L 10/20/2009 LCSD 27.8 93 6 (< 20 ) 30 ug/L 10/20/2009

Trichlorofluoromethane LCS 33.4 111 ( 68-145 ) 30 ug/L 10/20/2009 LCSD 31.0 103 7 (< 20 ) 30 ug/L 10/20/2009
P & M -Xylene LCS 58.5 98 ( 80-120 ) 60 ug/L 10/20/2009 LCSD 56.5 94 4 (< 20 ) 60 ug/L 10/20/2009
Naphthalene LCS 30.2 101 ( 75-120 ) 30 ug/L 10/20/2009 LCSD 28.5 95 6 (< 20 ) 30 ug/L 10/20/2009
o-Xylene LCS 29.4 98 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 28.9 96 2 (< 20 ) 30 ug/L 10/20/2009

Bromoform LCS 31.6 105 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 30.5 102 4 (< 20 ) 30 ug/L 10/20/2009

1-Chlorohexane LCS 44.2 98 ( 70-125 ) 45 ug/L 10/20/2009 LCSD 42.7 95 4 (< 20 ) 45 ug/L 10/20/2009
1,2,4-Trimethylbenzene LCS 29.5 98 ( 80-125 ) 30 ug/L 10/20/2009 LCSD 28.1 94 5 (< 20 ) 30 ug/L 10/20/2009
tert-Butylbenzene LCS 29.5 98 ( 80-122 ) 30 ug/L 10/20/2009 LCSD 27.8 93 6 (< 20 ) 30 ug/L 10/20/2009
1,1,1-Trichloroethane LCS 29.7 99 ( 80-122 ) 30 ug/L 10/20/2009 LCSD 27.6 92 7 (< 20 ) 30 ug/L 10/20/2009
1,1-Dichloroethane LCS 28.4 95 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.0 90 5 (< 20 ) 30 ug/L 10/20/2009

2-Chlorotoluene LCS 27.8 93 ( 80-125 ) 30 ug/L 10/20/2009 LCSD 26.3 88 6 (< 20 ) 30 ug/L 10/20/2009

Trichloroethene LCS 29.0 97 ( 80-125 ) 30 ug/L 10/20/2009 LCSD 27.5 92 5 (< 20 ) 30 ug/L 10/20/2009
trans-1,2-Dichloroethene LCS 29.6 99 ( 79-132 ) 30 ug/L 10/20/2009 LCSD 27.1 90 9 (< 20 ) 30 ug/L 10/20/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy



### 1,2-Dichlorobenzene LCS 28.1 94 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.2 91 3 (< 20 ) 30 ug/L 10/20/2009
2,2-Dichloropropane LCS 30.3 101 ( 80-132 ) 30 ug/L 10/20/2009 LCSD 27.5 92 9 (< 20 ) 30 ug/L 10/20/2009

Hexachlorobutadiene LCS 30.8 103 ( 77-125 ) 30 ug/L 10/20/2009 LCSD 30.0 100 3 (< 20 ) 30 ug/L 10/20/2009
Isopropylbenzene (Cumene) LCS 29.9 100 ( 80-121 ) 30 ug/L 10/20/2009 LCSD 29.0 97 3 (< 20 ) 30 ug/L 10/20/2009
1,2-Dichloropropane LCS 29.7 99 ( 80-121 ) 30 ug/L 10/20/2009 LCSD 28.3 94 5 (< 20 ) 30 ug/L 10/20/2009
1,1-Dichloropropene LCS 30.0 100 ( 80-122 ) 30 ug/L 10/20/2009 LCSD 28.5 95 5 (< 20 ) 30 ug/L 10/20/2009
1,1,2-Trichloroethane LCS 29.7 99 ( 77-120 ) 30 ug/L 10/20/2009 LCSD 28.4 95 5 (< 20 ) 30 ug/L 10/20/2009
1,3-Dichlorobenzene LCS 28.6 95 ( 80-120 ) 30 ug/L 10/20/2009 LCSD 27.1 90 5 (< 20 ) 30 ug/L 10/20/2009
1,2,3-Trichlorobenzene LCS 29.9 100 ( 77-120 ) 30 ug/L 10/20/2009 LCSD 28.9 96 4 (< 20 ) 30 ug/L 10/20/2009

Surrogates 

### 1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 10/20/2009 LCSD 93 5 10/20/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 10/20/2009 LCSD 101 2 10/20/2009

4-Bromofluorobenzene <surr> LCS 100 ( 76-120 ) 10/20/2009 LCSD 99 2 10/20/2009Matrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934050 Lab Control Sample 934051 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20165 SW5030B 10/20/2009

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Gas Chromatography/Mass Spectroscopy

Batch Method Instrument 

### VMS10954

SW8260B HP 5890 Series II MS3 VNAMatrix SGS Ref.#

Client Name Project Name/# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Prep 

### 934943 Lab Control Sample 934944 Lab Control Sample Duplicate The Environmental Company, Inc. (TEC) 3354-010 Red Hill BFSF Water (Surface, Eff., Ground) VXX20181 SW5030B 10/24/2009

QC results affect the following production samples: 

### 1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter QC Results Pct

Recov Spiked Amount Analysis

Date RPD LCS/LCSD Limits RPD Limits


### Volatile Fuels Department 

### Gasoline Range Organics LCS 206 103 ( 79-108 ) 200 ug/L 10/24/2009 LCSD 197 98 5 (< 20 ) 200 ug/L 10/24/2009

Surrogates 

### 4-Bromofluorobenzene <surr> LCS 99 ( 50-150 ) 10/24/2009 LCSD 100 2 10/24/2009

Batch Method Instrument 

### VFC9728

SW8015C HP 5890 Series II PID+HECD VBAMatrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) MXX22423 3010 H20 Digest for Metals ICP-MS 10/21/2009

QC results affect the following production samples:

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Dissolved Metals by ICP/MS


### Lead BMS ND 974 97 ( 80-120 ) 1000 ug/L 10/22/2009 BMSD 989 99 2 (< 15 ) 1000 ug/L 10/22/2009
Batch Method Instrument 

### MMS6155

SW6020 Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department 

### Gasoline Range Organics BMS ND 527 117* ( 79-108 ) 450 ug/L 10/24/2009 BMSD 420 93 23 (< 20 ) 450 ug/L 10/24/2009 * Surrogates 

### 4-Bromofluorobenzene <surr> BMS 53.9 108 ( 50-150 ) 10/24/2009 BMSD 53.0 106 2 10/24/2009
Batch Method Instrument 

### VFC9728

SW8015C HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department 

### Diesel Range Organics BMS ND 4.47 81 ( 75-125 ) 5.49 mg/L 10/26/2009 BMSD 4.29 78 4 (< 30 ) 5.49 mg/L 10/26/2009 Surrogates 

### 5a Androstane <surr> BMS .0938 85 ( 50-150 ) 10/26/2009 BMSD 0.0893 81 5 10/26/2009
Batch Method Instrument 

### XFC8990

SW8015C HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass SpectroscopyMatrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) VXX20165 Volatiles Extraction AFCEE 3.1 8260 (W) 10/20/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy


### Benzene BMS ND 29.1 97 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.2 97 0 (< 20 ) 30.0 ug/L 10/20/2009 Toluene BMS ND 27.3 91 ( 77-120 ) 30.0 ug/L 10/20/2009 BMSD 28.4 95 4 (< 20 ) 30.0 ug/L 10/20/2009 Ethylbenzene BMS ND 29.8 99 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 30.1 100 1 (< 20 ) 30.0 ug/L 10/20/2009 n-Butylbenzene BMS ND 30.2 101 ( 80-124 ) 30.0 ug/L 10/20/2009 BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 10/20/2009 1,4-Dichlorobenzene BMS ND 28.5 95 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.1 97 2 (< 20 ) 30.0 ug/L 10/20/2009 1,2-Dichloroethane BMS ND 29.3 98 ( 80-129 ) 30.0 ug/L 10/20/2009 BMSD 29.3 98 0 (< 20 ) 30.0 ug/L 10/20/2009 1,3,5-Trimethylbenzene BMS ND 28.9 96 ( 80-128 ) 30.0 ug/L 10/20/2009 BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 10/20/2009 4-Chlorotoluene BMS ND 28.6 96 ( 79-128 ) 30.0 ug/L 10/20/2009 BMSD 29.2 97 2 (< 20 ) 30.0 ug/L 10/20/2009 Chlorobenzene BMS ND 28.7 96 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.9 100 4 (< 20 ) 30.0 ug/L 10/20/2009 4-Methyl-2-pentanone (MIBK) BMS ND 103 115 ( 69-134 ) 90.0 ug/L 10/20/2009 BMSD 102 113 1 (< 20 ) 90.0 ug/L 10/20/2009 cis-1,2-Dichloroethene BMS ND 27.3 91 ( 80-125 ) 30.0 ug/L 10/20/2009 BMSD 28.4 95 4 (< 20 ) 30.0 ug/L 10/20/2009 4-Isopropyltoluene BMS ND 30.1 100 ( 80-125 ) 30.0 ug/L 10/20/2009 BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 10/20/2009 cis-1,3-Dichloropropene BMS ND 33.6 112 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 33.7 112 1 (< 20 ) 30.0 ug/L 10/20/2009 n-Propylbenzene BMS ND 28.5 95 ( 80-129 ) 30.0 ug/L 10/20/2009 BMSD 29.3 98 3 (< 20 ) 30.0 ug/L 10/20/2009 Styrene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 10/20/2009 Dibromomethane BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 30.4 101 2 (< 20 ) 30.0 ug/L 10/20/2009 trans-1,3-Dichloropropene BMS ND 29.2 97 ( 80-124 ) 30.0 ug/L 10/20/2009 BMSD 28.9 96 1 (< 20 ) 30.0 ug/L 10/20/2009 1,2,4-Trichlorobenzene BMS ND 31.9 106 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 31.6 105 1 (< 20 ) 30.0 ug/L 10/20/2009 Acetone BMS ND 90.6 101 ( 50-135 ) 90.0 ug/L 10/20/2009 BMSD 91.3 101 1 (< 20 ) 90.0 ug/L 10/20/2009 1,1,2,2-Tetrachloroethane BMS ND 29.7 99 ( 76-123 ) 30.0 ug/L 10/20/2009 BMSD 30.6 102 3 (< 20 ) 30.0 ug/L 10/20/2009Matrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) VXX20165 Volatiles Extraction AFCEE 3.1 8260 (W) 10/20/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,2-Dibromo-3-chloropropane BMS ND 31.8 106 ( 73-130 ) 30.0 ug/L 10/20/2009 BMSD 31.6 105 1 (< 20 ) 30.0 ug/L 10/20/2009 Methyl-t-butyl ether BMS ND 44.6 99 ( 80-120 ) 45.0 ug/L 10/20/2009 BMSD 45.4 101 2 (< 20 ) 45.0 ug/L 10/20/2009 Tetrachloroethene BMS ND 29 97 ( 79-122 ) 30.0 ug/L 10/20/2009 BMSD 30.5 102 5 (< 20 ) 30.0 ug/L 10/20/2009 Dibromochloromethane BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.2 97 2 (< 20 ) 30.0 ug/L 10/20/2009 1,3-Dichloropropane BMS ND 29.8 99 ( 80-121 ) 30.0 ug/L 10/20/2009 BMSD 30.3 101 2 (< 20 ) 30.0 ug/L 10/20/2009 1,2-Dibromoethane BMS ND 31.4 105 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 10/20/2009 Carbon tetrachloride BMS ND 28.2 94 ( 80-126 ) 30.0 ug/L 10/20/2009 BMSD 27.8 93 2 (< 20 ) 30.0 ug/L 10/20/2009 1,1,1,2-Tetrachloroethane BMS ND 28.4 95 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 28.8 96 2 (< 20 ) 30.0 ug/L 10/20/2009 Chloroform BMS ND 28.3 95 ( 80-124 ) 30.0 ug/L 10/20/2009 BMSD 28.6 95 1 (< 20 ) 30.0 ug/L 10/20/2009 Bromobenzene BMS ND 29 97 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.5 98 2 (< 20 ) 30.0 ug/L 10/20/2009 Chloromethane BMS ND 34.5 115 ( 67-125 ) 30.0 ug/L 10/20/2009 BMSD 35.8 119 4 (< 20 ) 30.0 ug/L 10/20/2009 1,2,3-Trichloropropane BMS ND 28.6 95 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 28.3 94 1 (< 20 ) 30.0 ug/L 10/20/2009 Bromomethane BMS ND 35.8 119 ( 30-140 ) 30.0 ug/L 10/20/2009 BMSD 37.9 126 6 (< 20 ) 30.0 ug/L 10/20/2009 Bromochloromethane BMS ND 29.7 99 ( 77-129 ) 30.0 ug/L 10/20/2009 BMSD 29.4 98 1 (< 20 ) 30.0 ug/L 10/20/2009 Vinyl chloride BMS ND 35.1 117 ( 72-145 ) 30.0 ug/L 10/20/2009 BMSD 36.3 121 4 (< 20 ) 30.0 ug/L 10/20/2009 Dichlorodifluoromethane BMS ND 43.6 145 ( 62-153 ) 30.0 ug/L 10/20/2009 BMSD 45.3 151 4 (< 20 ) 30.0 ug/L 10/20/2009 Chloroethane BMS ND 34.3 114 ( 67-133 ) 30.0 ug/L 10/20/2009 BMSD 35.6 119 4 (< 20 ) 30.0 ug/L 10/20/2009 sec-Butylbenzene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 10/20/2009 Bromodichloromethane BMS ND 33.2 111 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 32.4 108 3 (< 20 ) 30.0 ug/L 10/20/2009 1,1-Dichloroethene BMS ND 29.6 99 ( 76-130 ) 30.0 ug/L 10/20/2009 BMSD 29.7 99 0 (< 20 ) 30.0 ug/L 10/20/2009Matrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) VXX20165 Volatiles Extraction AFCEE 3.1 8260 (W) 10/20/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 2-Butanone (MEK) BMS ND 87.2 97 ( 66-136 ) 90.0 ug/L 10/20/2009 BMSD 87.6 97 0 (< 20 ) 90.0 ug/L 10/20/2009 Methylene chloride BMS ND 29.7 99 ( 63-131 ) 30.0 ug/L 10/20/2009 BMSD 31.6 105 6 (< 20 ) 30.0 ug/L 10/20/2009 Trichlorofluoromethane BMS ND 32.7 109 ( 68-145 ) 30.0 ug/L 10/20/2009 BMSD 34.5 115 5 (< 20 ) 30.0 ug/L 10/20/2009 P & M -Xylene BMS ND 59.6 99 ( 80-120 ) 60.0 ug/L 10/20/2009 BMSD 60.9 102 2 (< 20 ) 60.0 ug/L 10/20/2009 Naphthalene BMS ND 31.2 104 ( 75-120 ) 30.0 ug/L 10/20/2009 BMSD 32.0 107 3 (< 20 ) 30.0 ug/L 10/20/2009 o-Xylene BMS ND 29.6 99 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 30.8 103 4 (< 20 ) 30.0 ug/L 10/20/2009 Bromoform BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.8 99 4 (< 20 ) 30.0 ug/L 10/20/2009 1-Chlorohexane BMS ND 44 98 ( 70-125 ) 45.0 ug/L 10/20/2009 BMSD 45.8 102 4 (< 20 ) 45.0 ug/L 10/20/2009 1,2,4-Trimethylbenzene BMS ND 28.9 96 ( 80-125 ) 30.0 ug/L 10/20/2009 BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 10/20/2009 tert-Butylbenzene BMS ND 29.2 97 ( 80-122 ) 30.0 ug/L 10/20/2009 BMSD 29.8 99 2 (< 20 ) 30.0 ug/L 10/20/2009 1,1,1-Trichloroethane BMS ND 30.2 101 ( 80-122 ) 30.0 ug/L 10/20/2009 BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 10/20/2009 1,1-Dichloroethane BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.1 97 3 (< 20 ) 30.0 ug/L 10/20/2009 2-Chlorotoluene BMS ND 27.4 91 ( 80-125 ) 30.0 ug/L 10/20/2009 BMSD 28.2 94 3 (< 20 ) 30.0 ug/L 10/20/2009 Trichloroethene BMS ND 29.4 98 ( 80-125 ) 30.0 ug/L 10/20/2009 BMSD 29.7 99 1 (< 20 ) 30.0 ug/L 10/20/2009 trans-1,2-Dichloroethene BMS ND 30 100 ( 79-132 ) 30.0 ug/L 10/20/2009 BMSD 30.2 101 1 (< 20 ) 30.0 ug/L 10/20/2009 1,2-Dichlorobenzene BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.2 97 3 (< 20 ) 30.0 ug/L 10/20/2009 2,2-Dichloropropane BMS ND 30.2 101 ( 80-132 ) 30.0 ug/L 10/20/2009 BMSD 30.1 100 0 (< 20 ) 30.0 ug/L 10/20/2009 Hexachlorobutadiene BMS ND 30.2 101 ( 77-125 ) 30.0 ug/L 10/20/2009 BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/20/2009 Isopropylbenzene (Cumene) BMS ND 30.1 100 ( 80-121 ) 30.0 ug/L 10/20/2009 BMSD 31.1 104 4 (< 20 ) 30.0 ug/L 10/20/2009 1,2-Dichloropropane BMS ND 30.4 101 ( 80-121 ) 30.0 ug/L 10/20/2009 BMSD 31.0 103 2 (< 20 ) 30.0 ug/L 10/20/2009Matrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) VXX20165 Volatiles Extraction AFCEE 3.1 8260 (W) 10/20/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Volatile Gas Chromatography/Mass Spectroscopy 

### 1,1-Dichloropropene BMS ND 31 103 ( 80-122 ) 30.0 ug/L 10/20/2009 BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/20/2009 1,1,2-Trichloroethane BMS ND 30.1 100 ( 77-120 ) 30.0 ug/L 10/20/2009 BMSD 31.3 104 4 (< 20 ) 30.0 ug/L 10/20/2009 1,3-Dichlorobenzene BMS ND 28.6 95 ( 80-120 ) 30.0 ug/L 10/20/2009 BMSD 29.0 97 1 (< 20 ) 30.0 ug/L 10/20/2009 1,2,3-Trichlorobenzene BMS ND 30.8 103 ( 77-120 ) 30.0 ug/L 10/20/2009 BMSD 32.1 107 4 (< 20 ) 30.0 ug/L 10/20/2009 Surrogates 

### 1,2-Dichloroethane-D4 <surr> BMS 30 100 ( 73-120 ) 10/20/2009 BMSD 29.6 99 1 10/20/2009 Toluene-d8 <surr> BMS 30.2 101 ( 80-120 ) 10/20/2009 BMSD 30.2 101 0 10/20/2009 4-Bromofluorobenzene <surr> BMS 29.3 98 ( 76-120 ) 10/20/2009 BMSD 28.8 96 2 10/20/2009
Batch Method Instrument 

### VMS10954

SW8260B HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MSMatrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) XXX21834 3520 Liquid/Liquid Ext for 8270 SIM 10/16/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS 

### Acenaphthylene BMS ND .436 79 ( 50-105 ) 0.549 ug/L 10/24/2009 BMSD 0.411 76 6 (< 30 ) 0.543 ug/L 10/24/2009 Acenaphthene BMS ND .412 75 ( 45-110 ) 0.549 ug/L 10/24/2009 BMSD 0.398 73 3 (< 30 ) 0.543 ug/L 10/24/2009 Fluorene BMS ND .436 79 ( 50-110 ) 0.549 ug/L 10/24/2009 BMSD 0.423 78 3 (< 30 ) 0.543 ug/L 10/24/2009 Phenanthrene BMS ND .436 79 ( 50-115 ) 0.549 ug/L 10/24/2009 BMSD 0.415 76 5 (< 30 ) 0.543 ug/L 10/24/2009 Anthracene BMS ND .491 89 ( 55-110 ) 0.549 ug/L 10/24/2009 BMSD 0.487 90 1 (< 30 ) 0.543 ug/L 10/24/2009 Fluoranthene BMS ND .523 95 ( 55-125 ) 0.549 ug/L 10/24/2009 BMSD 0.495 91 5 (< 30 ) 0.543 ug/L 10/24/2009 Pyrene BMS ND .507 92 ( 50-130 ) 0.549 ug/L 10/24/2009 BMSD 0.489 90 4 (< 30 ) 0.543 ug/L 10/24/2009 Benzo(a)Anthracene BMS ND .529 96 ( 55-120 ) 0.549 ug/L 10/24/2009 BMSD 0.508 93 4 (< 30 ) 0.543 ug/L 10/24/2009 Chrysene BMS ND .516 94 ( 55-120 ) 0.549 ug/L 10/24/2009 BMSD 0.498 92 3 (< 30 ) 0.543 ug/L 10/24/2009 Benzo[b]Fluoranthene BMS ND .516 94 ( 46-130 ) 0.549 ug/L 10/24/2009 BMSD 0.480 88 7 (< 30 ) 0.543 ug/L 10/24/2009 Benzo[k]fluoranthene BMS ND .529 96 ( 60-125 ) 0.549 ug/L 10/24/2009 BMSD 0.516 95 3 (< 30 ) 0.543 ug/L 10/24/2009 Benzo[a]pyrene BMS ND .536 98 ( 55-120 ) 0.549 ug/L 10/24/2009 BMSD 0.500 92 7 (< 30 ) 0.543 ug/L 10/24/2009 Indeno[1,2,3-c,d] pyrene BMS ND .491 89 ( 45-125 ) 0.549 ug/L 10/24/2009 BMSD 0.445 82 10 (< 30 ) 0.543 ug/L 10/24/2009 Dibenzo[a,h]anthracene BMS ND .486 89 ( 41-140 ) 0.549 ug/L 10/24/2009 BMSD 0.435 80 11 (< 30 ) 0.543 ug/L 10/24/2009 Benzo[g,h,i]perylene BMS ND .481 88 ( 46-125 ) 0.549 ug/L 10/24/2009 BMSD 0.447 82 7 (< 30 ) 0.543 ug/L 10/24/2009 Naphthalene BMS ND .405 74 ( 42-100 ) 0.549 ug/L 10/24/2009 BMSD 0.394 73 3 (< 30 ) 0.543 ug/L 10/24/2009 1-Methylnaphthalene BMS ND .414 75 ( 46-115 ) 0.549 ug/L 10/24/2009 BMSD 0.393 72 5 (< 30 ) 0.543 ug/L 10/24/2009 2-Methylnaphthalene BMS ND .39 71 ( 45-105 ) 0.549 ug/L 10/24/2009 BMSD 0.377 69 3 (< 30 ) 0.543 ug/L 10/24/2009 Surrogates 

### Terphenyl-d14 <surr> BMS .515 94 ( 50-135 ) 10/24/2009 BMSD 0.492 90 5 10/24/2009Matrix SGS Ref.# Printed Date/Time 

### 10/30/2009 15:29 Batch Method Date Original Prep 

### 1095622002 Billable Matrix Spike 1095622003 Billable Matrix Spike Dup.

1095622001 Water (Surface, Eff., Ground) XXX21834 3520 Liquid/Liquid Ext for 8270 SIM 10/16/2009

Parameter QC Result Pct

Recov Spiked Amount Analysis

Date MS/MSD Limits RPD RPD Limits Original Result Qualifiers


### Polynuclear Aromatics GC/MS

Batch Method Instrument 

### XMS5160

8270D SIMS HP 6890 Series II MS2 SVOA