SGS Work Order:

Contents:

Cover Page

Case Narrative

Final Report Pages

Quality Control Summary Forms

Chain of Custody/Sample Receipt Forms

Project:

Client:

SGS North America Inc.

 Alaska Division

Level II Laboratory Data Report

Released by: 

Note:

Unless otherwise noted, all quality assurance/quality control criteria is in compliance with the standards set forth by the proper regulatory authority, the 

SGS Quality Assurance Program Plan, and the National Environmental Accreditation Conference.

3354-010 Red Hill BFSF

The Environmental Company, Inc. (TEC)

1095622
CASE NARRATIVE Print Date: 10/30/2009

Workorder No.: 1095622

Project Name: 3354-010 Red Hill BFSF

Client Name: The Environmental Company, Inc. (TEC)

Lab Sample ID

Sample Comments

Sample Type Client Sample ID

Refer to the sample receipt form for information on sample condition.

1095622002

AK101 - MS recovery for GRO does not meet QC criteria (biased high). See LCS/LCSD for accuracy.

BMS OWDFMW01-WG-02 MS

1095622003

AK101 - MS/MSD RPD results for GRO does not meet QC criteria (biased high). See LCS/LCSD for accuracy.

BMSD OWDFMW01-WG-02 MSD

934050

8260B - LCS recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected above 

the PQL in the associated samples

LCS LCS for HBN 222065 [VXX/20165]

934051

8260B - LCSD recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected 

above the PQL in the associated samples

LCSD LCSD for HBN 222065 [VXX/20165

934053

8260B - CCV recoveries for several analytes do not meet QC criteria (biased high). These analytes were not detected 

above the PQL in the associated samples

CCV CCV for HBN 222066 [VMS/10954]

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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M em ber of S G S G roup (S ociété G énérale de S urveillance)
Laboratory Analytical Report

Project:

Client:

Workorder No.:

The Environmental Company, Inc. (TEC)

1095622

Certification:

I certify that this data package is in compliance with the terms and conditions of the contract, 

both technically and for completeness, other than the conditions noted on the sample data 

sheet(s) and/or the case narrative. This certification applies only to the tested parameters and 

the specific sample(s) received at the laboratory.

1001 Bishop Street, Suite 1400

Honolulu, HI 96813

Attn: Rick Adkisson

T: (808)528-1445 F:(808)528-0768

Heather Hall

Heather.Hall@sgs.com

Quality Assurance Manager

3354-010 Red Hill BFSF

If you have any questions regarding this report, or if we can be of further assistance, please 

contact your SGS Project Manager.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup
Enclosed are the analytical results associated with this workorder.

As required by the state of Alaska and the USEPA, a formal Quality Assurance/Quality Control Program is maintained by SGS. A copy of 

our Quality Assurance Plan (QAP), which outlines this program is available at your request.

The Laboratory certification numbers are AK971-05 (DW), UTS-005 (CS) and AK00971 (Micro) for ADEC and AK100001 for NELAP (RCRA 

methods: 1020A, 1311, 6010B, 7470A, 7471A, 9040B, 9045C, 9056, 9060, 8015B, 8021B, 8081A/8082, 8260B, 8270C).

Except as specifically noted, all statements and data in this report are in conformance to the provisions set forth by the SGS QAP, the 

National Environmental Laboratory Accreditation Program and, when applicable, other regulatory authorities.

If you have any questions regarding this report or if we can be of any assistance, please contact your SGS Project Manager at 

907-562-2343. All work is being provided under SGS general terms and conditions (http://www.sgs.com/terms_and_conditions.htm) 

The following descriptors may be found on your report which will serve to further qualify the data.

MDL Method Detection Limit

PQL Practical Quantitation Limit (reporting limit).

CL Control Limit

U Indicates the analyte was analyzed for but not detected.

F Indicates value that is greater than or equal to the MDL.

J The quantitation is an estimation.

ND Indicates the analyte is not detected

B Indicates the analyte is found in a blank associated with the sample.

* The analyte has exceeded allowable regulatory or control limits.

D The analyte concentration is the result of dilution.

GT Greater Than

LT Less Than

Q QC parameter out of acceptance range.

M A matrix effect was present.

E The analyte result is above the calibrated range.

R Rejected

DF Analytical Dilution Factor

JL The analyte was positively identified, but the quantitation is a low estimation.

<Surr> Surrogate QC spiked standard

<Surr/IS> Surrogate / Internal Standard QC spiked standard

QC Quality Control

QA Quality Assurance

MB Method Blank

LCS (D) Laboratory Control Sample (Duplicate)

MS(D) Matrix Spike (Duplicate)

BMS(D) Site Specific Matrix Spike (Duplicate)

RPD Relative Percent Difference

ICV Initial Calibration Verification

CCV Continuous Calibration Verification

MSA Method of Standard Addition

Notes: Soil samples are reported on a dry weight basis unless otherwise specified

Print Date: 10/30/2009

Notes: All DRO/RRO analyses are integrated per SOP.

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

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M em ber of S G S G roup
SAMPLE SUMMARY

Client Name: The Environmental Company, Inc. (TEC)

Project Name: 3354-010 Red Hill BFSF

Workorder No.: 1095622

Analytical Methods

Method Description Analytical Method

8270 PAH SIM Semi-Vol GC/MS Liq/Liq ext. 8270D SIMS

AFCEE 3.1 8260 (W) SW8260B

Dissolved Metals by ICP-MS SW6020

DRO by 8015C (W) SW8015C

GRO (W) SW8015C

Print Date: 10/30/2009 3:29 pm

Sample ID Cross Reference

Lab Sample ID Client Sample ID

1095622001 OWDFMW01-WG-02

1095622002 OWDFMW01-WG-02 MS

1095622003 OWDFMW01-WG-02 MSD

1095622004 RHMW04-WG-02

1095622005 RHMWA01-WG-02

1095622006 HDMW2253-03-WG-02

1095622007 TB01-WG-02

S G S N orth A m erica Inc . A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2343 f (907 ) 561.5301 w w w .us.sgs.com

M em ber of S G S G roup (S ociété G énérale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: OWDFMW01-WG-02

SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6155 MXX22423

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6155

Analytical Method: SW6020

Analysis Date/Time: 10/22/09 20:08

Prep Batch: MXX22423

Prep Method: SW3010A

Prep Date/Time: 10/21/09 16:15 Container ID:1095622001-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: OWDFMW01-WG-02

SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9728 VXX20181

4-Bromofluorobenzene <surr> 101 50-150 % 1 VFC9728 VXX20181

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9728

Analytical Method: SW8015C

Analysis Date/Time: 10/24/09 16:00

Prep Batch: VXX20181

Prep Method: SW5030B

Prep Date/Time: 10/24/09 13:29 Container ID:1095622001-A

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: OWDFMW01-WG-02

SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.444 0.167 mg/L 1 XFC8990 XXX21847

5a Androstane <surr> 76.5 50-150 % 1 XFC8990 XXX21847

Batch Information

Initial Prep Wt./Vol.: 900 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8990

Analytical Method: SW8015C

Analysis Date/Time: 10/26/09 11:16

Prep Batch: XXX21847

Prep Method: SW3520C

Prep Date/Time: 10/19/09 10:35 Container ID:1095622001-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: OWDFMW01-WG-02

SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

Toluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Styrene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Acetone ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10954 VXX20165

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

Chloroform ND 1.00 0.300 ug/L 1 VMS10954 VXX20165

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromomethane ND 3.00 0.940 ug/L 1 VMS10954 VXX20165

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: OWDFMW01-WG-02

SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10954 VXX20165

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Naphthalene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

o-Xylene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromoform ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane-D4 <surr> 105 73-120 % 1 VMS10954 VXX20165

Toluene-d8 <surr> 98.9 80-120 % 1 VMS10954 VXX20165

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS10954 VXX20165

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10954

Analytical Method: SW8260B

Analysis Date/Time: 10/20/09 17:37

Prep Batch: VXX20165

Prep Method: SW5030B

Prep Date/Time: 10/20/09 08:22 Container ID:1095622001-E

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: OWDFMW01-WG-02

SGS Ref. #: 1095622001 Collection Date/Time: 10/13/09 09:30

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Acenaphthene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Fluorene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Phenanthrene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Anthracene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Fluoranthene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Pyrene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Benzo(a)Anthracene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Chrysene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Benzo[b]Fluoranthene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Benzo[k]fluoranthene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Benzo[a]pyrene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Indeno[1,2,3-c,d] pyrene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Dibenzo[a,h]anthracene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Benzo[g,h,i]perylene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Naphthalene ND 0.112 0.0346 ug/L 1 XMS5160 XXX21834

1-Methylnaphthalene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

2-Methylnaphthalene ND 0.0559 0.0168 ug/L 1 XMS5160 XXX21834

Terphenyl-d14 <surr> 96.5 50-135 % 1 XMS5160 XXX21834

Batch Information

Initial Prep Wt./Vol.: 895 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5160

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/24/09 08:09

Prep Batch: XXX21834

Prep Method: SW3520C

Prep Date/Time: 10/16/09 09:15 Container ID:1095622001-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMW04-WG-02

SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6155 MXX22423

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6155

Analytical Method: SW6020

Analysis Date/Time: 10/22/09 20:18

Prep Batch: MXX22423

Prep Method: SW3010A

Prep Date/Time: 10/21/09 16:15 Container ID:1095622004-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMW04-WG-02

SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9728 VXX20181

4-Bromofluorobenzene <surr> 99.8 50-150 % 1 VFC9728 VXX20181

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9728

Analytical Method: SW8015C

Analysis Date/Time: 10/24/09 17:08

Prep Batch: VXX20181

Prep Method: SW5030B

Prep Date/Time: 10/24/09 13:29 Container ID:1095622004-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMW04-WG-02

SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.452 0.169 mg/L 1 XFC8990 XXX21847

5a Androstane <surr> 83.1 50-150 % 1 XFC8990 XXX21847

Batch Information

Initial Prep Wt./Vol.: 885 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8990

Analytical Method: SW8015C

Analysis Date/Time: 10/26/09 11:47

Prep Batch: XXX21847

Prep Method: SW3520C

Prep Date/Time: 10/19/09 10:35 Container ID:1095622004-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMW04-WG-02

SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

Toluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Styrene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Acetone ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10954 VXX20165

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

Chloroform ND 1.00 0.300 ug/L 1 VMS10954 VXX20165

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromomethane ND 3.00 0.940 ug/L 1 VMS10954 VXX20165

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMW04-WG-02

SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10954 VXX20165

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Naphthalene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

o-Xylene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromoform ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane-D4 <surr> 105 73-120 % 1 VMS10954 VXX20165

Toluene-d8 <surr> 100 80-120 % 1 VMS10954 VXX20165

4-Bromofluorobenzene <surr> 103 76-120 % 1 VMS10954 VXX20165

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10954

Analytical Method: SW8260B

Analysis Date/Time: 10/20/09 21:32

Prep Batch: VXX20165

Prep Method: SW5030B

Prep Date/Time: 10/20/09 08:22 Container ID:1095622004-A

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMW04-WG-02

SGS Ref. #: 1095622004 Collection Date/Time: 10/13/09 13:20

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Acenaphthene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Fluorene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Phenanthrene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Anthracene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Fluoranthene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Pyrene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Benzo(a)Anthracene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Chrysene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Benzo[b]Fluoranthene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Benzo[k]fluoranthene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Benzo[a]pyrene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Indeno[1,2,3-c,d] pyrene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Dibenzo[a,h]anthracene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Benzo[g,h,i]perylene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Naphthalene ND 0.115 0.0356 ug/L 1 XMS5161 XXX21834

1-Methylnaphthalene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

2-Methylnaphthalene ND 0.0575 0.0172 ug/L 1 XMS5161 XXX21834

Terphenyl-d14 <surr> 91.4 50-135 % 1 XMS5161 XXX21834

Batch Information

Initial Prep Wt./Vol.: 870 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5161

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/24/09 15:53

Prep Batch: XXX21834

Prep Method: SW3520C

Prep Date/Time: 10/16/09 09:15 Container ID:1095622004-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMWA01-WG-02

SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6155 MXX22423

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6155

Analytical Method: SW6020

Analysis Date/Time: 10/22/09 20:20

Prep Batch: MXX22423

Prep Method: SW3010A

Prep Date/Time: 10/21/09 16:15 Container ID:1095622005-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMWA01-WG-02

SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9728 VXX20181

4-Bromofluorobenzene <surr> 102 50-150 % 1 VFC9728 VXX20181

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9728

Analytical Method: SW8015C

Analysis Date/Time: 10/24/09 17:31

Prep Batch: VXX20181

Prep Method: SW5030B

Prep Date/Time: 10/24/09 13:29 Container ID:1095622005-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMWA01-WG-02

SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.465 0.174 mg/L 1 XFC8990 XXX21847

5a Androstane <surr> 76 50-150 % 1 XFC8990 XXX21847

Batch Information

Initial Prep Wt./Vol.: 860 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8990

Analytical Method: SW8015C

Analysis Date/Time: 10/26/09 11:58

Prep Batch: XXX21847

Prep Method: SW3520C

Prep Date/Time: 10/19/09 10:35 Container ID:1095622005-I

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMWA01-WG-02

SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

Toluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Styrene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Acetone ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10954 VXX20165

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

Chloroform ND 1.00 0.300 ug/L 1 VMS10954 VXX20165

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromomethane ND 3.00 0.940 ug/L 1 VMS10954 VXX20165

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMWA01-WG-02

SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10954 VXX20165

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Naphthalene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

o-Xylene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromoform ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane-D4 <surr> 103 73-120 % 1 VMS10954 VXX20165

Toluene-d8 <surr> 97.4 80-120 % 1 VMS10954 VXX20165

4-Bromofluorobenzene <surr> 104 76-120 % 1 VMS10954 VXX20165

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10954

Analytical Method: SW8260B

Analysis Date/Time: 10/20/09 20:58

Prep Batch: VXX20165

Prep Method: SW5030B

Prep Date/Time: 10/20/09 08:22 Container ID:1095622005-A

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: RHMWA01-WG-02

SGS Ref. #: 1095622005 Collection Date/Time: 10/13/09 12:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Acenaphthene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Fluorene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Phenanthrene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Anthracene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Fluoranthene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Pyrene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Benzo(a)Anthracene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Chrysene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[b]Fluoranthene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[k]fluoranthene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[a]pyrene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Indeno[1,2,3-c,d] pyrene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Dibenzo[a,h]anthracene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[g,h,i]perylene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Naphthalene ND 0.112 0.0348 ug/L 1 XMS5161 XXX21834

1-Methylnaphthalene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

2-Methylnaphthalene ND 0.0562 0.0169 ug/L 1 XMS5161 XXX21834

Terphenyl-d14 <surr> 95.5 50-135 % 1 XMS5161 XXX21834

Batch Information

Initial Prep Wt./Vol.: 890 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5161

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/24/09 16:28

Prep Batch: XXX21834

Prep Method: SW3520C

Prep Date/Time: 10/16/09 09:15 Container ID:1095622005-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: HDMW2253-03-WG-02

SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Dissolved Metals by ICP/MS

MDL DF

Lead ND 1.00 0.310 ug/L 5 MMS6155 MXX22423

Batch Information

Initial Prep Wt./Vol.: 50 mL

Prep Extract Vol.: 50 mL

Analytical Batch: MMS6155

Analytical Method: SW6020

Analysis Date/Time: 10/22/09 20:22

Prep Batch: MXX22423

Prep Method: SW3010A

Prep Date/Time: 10/21/09 16:15 Container ID:1095622006-G

Dilution Factor: 5 Analyst: NRB

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: HDMW2253-03-WG-02

SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9728 VXX20181

4-Bromofluorobenzene <surr> 101 50-150 % 1 VFC9728 VXX20181

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9728

Analytical Method: SW8015C

Analysis Date/Time: 10/24/09 17:54

Prep Batch: VXX20181

Prep Method: SW5030B

Prep Date/Time: 10/24/09 13:29 Container ID:1095622006-C

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: HDMW2253-03-WG-02

SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Semivolatile Organic Fuels Department

MDL DF

Diesel Range Organics ND 0.494 0.185 mg/L 1 XFC8990 XXX21847

5a Androstane <surr> 73.3 50-150 % 1 XFC8990 XXX21847

Batch Information

Initial Prep Wt./Vol.: 810 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XFC8990

Analytical Method: SW8015C

Analysis Date/Time: 10/26/09 12:08

Prep Batch: XXX21847

Prep Method: SW3520C

Prep Date/Time: 10/19/09 10:35 Container ID:1095622006-J

Dilution Factor: 1 Analyst: KDC

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: HDMW2253-03-WG-02

SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

Toluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Styrene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Acetone ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10954 VXX20165

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

Chloroform ND 1.00 0.300 ug/L 1 VMS10954 VXX20165

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromomethane ND 3.00 0.940 ug/L 1 VMS10954 VXX20165

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: HDMW2253-03-WG-02

SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10954 VXX20165

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Naphthalene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

o-Xylene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromoform ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane-D4 <surr> 105 73-120 % 1 VMS10954 VXX20165

Toluene-d8 <surr> 98.8 80-120 % 1 VMS10954 VXX20165

4-Bromofluorobenzene <surr> 102 76-120 % 1 VMS10954 VXX20165

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10954

Analytical Method: SW8260B

Analysis Date/Time: 10/20/09 20:25

Prep Batch: VXX20165

Prep Method: SW5030B

Prep Date/Time: 10/20/09 08:22 Container ID:1095622006-B

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: HDMW2253-03-WG-02

SGS Ref. #: 1095622006 Collection Date/Time: 10/13/09 11:00

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Polynuclear Aromatics GC/MS

MDL DF

Acenaphthylene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Acenaphthene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Fluorene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Phenanthrene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Anthracene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Fluoranthene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Pyrene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Benzo(a)Anthracene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Chrysene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[b]Fluoranthene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[k]fluoranthene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[a]pyrene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Indeno[1,2,3-c,d] pyrene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Dibenzo[a,h]anthracene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Benzo[g,h,i]perylene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Naphthalene ND 0.113 0.0350 ug/L 1 XMS5161 XXX21834

1-Methylnaphthalene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

2-Methylnaphthalene ND 0.0565 0.0169 ug/L 1 XMS5161 XXX21834

Terphenyl-d14 <surr> 84.8 50-135 % 1 XMS5161 XXX21834

Batch Information

Initial Prep Wt./Vol.: 885 mL

Prep Extract Vol.: 1 mL

Analytical Batch: XMS5161

Analytical Method: 8270D SIMS

Analysis Date/Time: 10/24/09 17:03

Prep Batch: XXX21834

Prep Method: SW3520C

Prep Date/Time: 10/16/09 09:15 Container ID:1095622006-H

Dilution Factor: 1 Analyst: JDH

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: TB01-WG-02

SGS Ref. #: 1095622007 Collection Date/Time: 10/13/09 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Fuels Department

MDL DF

Gasoline Range Organics ND 100 30.0 ug/L 1 VFC9728 VXX20181

4-Bromofluorobenzene <surr> 98.4 50-150 % 1 VFC9728 VXX20181

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VFC9728

Analytical Method: SW8015C

Analysis Date/Time: 10/24/09 15:37

Prep Batch: VXX20181

Prep Method: SW5030B

Prep Date/Time: 10/24/09 13:29 Container ID:1095622007-B

Dilution Factor: 1 Analyst: KPW

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: TB01-WG-02

SGS Ref. #: 1095622007 Collection Date/Time: 10/13/09 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Benzene ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

Toluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Ethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

n-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chlorobenzene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

4-Isopropyltoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

n-Propylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Styrene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromomethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Acetone ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Methyl-t-butyl ether ND 5.00 1.50 ug/L 1 VMS10954 VXX20165

Tetrachloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dibromochloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,3-Dichloropropane ND 0.400 0.120 ug/L 1 VMS10954 VXX20165

1,2-Dibromoethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Carbon tetrachloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

Chloroform ND 1.00 0.300 ug/L 1 VMS10954 VXX20165

Bromobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Chloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromomethane ND 3.00 0.940 ug/L 1 VMS10954 VXX20165

Bromochloromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Vinyl chloride ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Dichlorodifluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
The Environmental Company, Inc. (TEC) Print Date: 10/30/2009 3:29 pm

Client Sample ID: TB01-WG-02

SGS Ref. #: 1095622007 Collection Date/Time: 10/13/09 08:05

Project ID: 3354-010 Red Hill BFSF Receipt Date/Time: 10/15/09 11:00

Matrix: Water (Surface, Eff., Ground)

Analytical 

Batch

Prep

Parameter Result PQL/CL Units Batch Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

MDL DF

Chloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

sec-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromodichloromethane ND 0.500 0.150 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Butanone (MEK) ND 10.0 3.10 ug/L 1 VMS10954 VXX20165

Methylene chloride ND 5.00 1.00 ug/L 1 VMS10954 VXX20165

Trichlorofluoromethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

P & M -Xylene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

Naphthalene ND 2.00 0.620 ug/L 1 VMS10954 VXX20165

o-Xylene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Bromoform ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1-Chlorohexane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

tert-Butylbenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2-Chlorotoluene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Trichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

2,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Hexachlorobutadiene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloropropane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1-Dichloropropene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 1 VMS10954 VXX20165

1,2-Dichloroethane-D4 <surr> 106 73-120 % 1 VMS10954 VXX20165

Toluene-d8 <surr> 100 80-120 % 1 VMS10954 VXX20165

4-Bromofluorobenzene <surr> 105 76-120 % 1 VMS10954 VXX20165

Batch Information

Initial Prep Wt./Vol.: 5 mL

Prep Extract Vol.: 5 mL

Analytical Batch: VMS10954

Analytical Method: SW8260B

Analysis Date/Time: 10/20/09 19:51

Prep Batch: VXX20165

Prep Method: SW5030B

Prep Date/Time: 10/20/09 08:22 Container ID:1095622007-A

Dilution Factor: 1 Analyst: SCL

S G S N orth A m erica Inc. A laska D ivision 200 W est P otter D rive A nchorage A laska 99518

t (907 ) 562.2 343 f (907 ) 561.5 301 w w w .us.sgs.com

M em ber of S G S G rou p (S ociété G éné rale de S urveillance)
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

932199 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21834

SW3520C

10/16/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Polynuclear Aromatics GC/MS

Acenaphthylene ND 0.0500 0.0150 ug/L 10/24/09

Acenaphthene ND 0.0500 0.0150 ug/L 10/24/09

Fluorene ND 0.0500 0.0150 ug/L 10/24/09

Phenanthrene ND 0.0500 0.0150 ug/L 10/24/09

Anthracene ND 0.0500 0.0150 ug/L 10/24/09

Fluoranthene ND 0.0500 0.0150 ug/L 10/24/09

Pyrene ND 0.0500 0.0150 ug/L 10/24/09

Benzo(a)Anthracene ND 0.0500 0.0150 ug/L 10/24/09

Chrysene ND 0.0500 0.0150 ug/L 10/24/09

Benzo[b]Fluoranthene ND 0.0500 0.0150 ug/L 10/24/09

Benzo[k]fluoranthene ND 0.0500 0.0150 ug/L 10/24/09

Benzo[a]pyrene ND 0.0500 0.0150 ug/L 10/24/09

Indeno[1,2,3-c,d] pyrene ND 0.0500 0.0150 ug/L 10/24/09

Dibenzo[a,h]anthracene ND 0.0500 0.0150 ug/L 10/24/09

Benzo[g,h,i]perylene ND 0.0500 0.0150 ug/L 10/24/09

Naphthalene ND 0.100 0.0310 ug/L 10/24/09

1-Methylnaphthalene ND 0.0500 0.0150 ug/L 10/24/09

2-Methylnaphthalene ND 0.0500 0.0150 ug/L 10/24/09

Surrogates 

Terphenyl-d14 <surr> 93.7 50-135 % 10/24/09

Instrument

Method

Batch XMS5160

8270D SIMS

HP 6890 Series II MS2 SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

932694 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21847

SW3520C

10/19/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Semivolatile Organic Fuels Department

Diesel Range Organics ND 0.400 0.150 mg/L 10/26/09

Surrogates 

5a Androstane <surr> 79.2 60-120 % 10/26/09

Instrument

Method

Batch XFC8990

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

933881 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22423

SW3010A

10/21/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Metals by ICP/MS

Lead ND 1.00 0.310 ug/L 10/22/09

Instrument

Method

Batch MMS6155

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934049 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934049 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

Benzene ND 0.400 0.120 ug/L 10/20/09

Toluene ND 1.00 0.310 ug/L 10/20/09

Ethylbenzene ND 1.00 0.310 ug/L 10/20/09

n-Butylbenzene ND 1.00 0.310 ug/L 10/20/09

1,4-Dichlorobenzene ND 0.500 0.150 ug/L 10/20/09

1,2-Dichloroethane ND 0.500 0.150 ug/L 10/20/09

1,3,5-Trimethylbenzene ND 1.00 0.310 ug/L 10/20/09

4-Chlorotoluene ND 1.00 0.310 ug/L 10/20/09

Chlorobenzene ND 0.500 0.150 ug/L 10/20/09

4-Methyl-2-pentanone (MIBK) ND 10.0 3.10 ug/L 10/20/09

cis-1,2-Dichloroethene ND 1.00 0.310 ug/L 10/20/09

4-Isopropyltoluene ND 1.00 0.310 ug/L 10/20/09

cis-1,3-Dichloropropene ND 0.500 0.150 ug/L 10/20/09

n-Propylbenzene ND 1.00 0.310 ug/L 10/20/09

Styrene ND 1.00 0.310 ug/L 10/20/09

Dibromomethane ND 1.00 0.310 ug/L 10/20/09

trans-1,3-Dichloropropene ND 1.00 0.310 ug/L 10/20/09

1,2,4-Trichlorobenzene ND 1.00 0.310 ug/L 10/20/09

Acetone ND 10.0 3.10 ug/L 10/20/09

1,1,2,2-Tetrachloroethane ND 0.500 0.150 ug/L 10/20/09

1,2-Dibromo-3-chloropropane ND 2.00 0.620 ug/L 10/20/09

Methyl-t-butyl ether ND 5.00 1.50 ug/L 10/20/09

Tetrachloroethene ND 1.00 0.310 ug/L 10/20/09

Dibromochloromethane ND 0.500 0.150 ug/L 10/20/09

1,3-Dichloropropane ND 0.400 0.120 ug/L 10/20/09

1,2-Dibromoethane ND 1.00 0.310 ug/L 10/20/09

Carbon tetrachloride ND 1.00 0.310 ug/L 10/20/09

1,1,1,2-Tetrachloroethane ND 0.500 0.150 ug/L 10/20/09

Chloroform ND 1.00 0.300 ug/L 10/20/09

Bromobenzene ND 1.00 0.310 ug/L 10/20/09

Chloromethane ND 1.00 0.310 ug/L 10/20/09

1,2,3-Trichloropropane ND 1.00 0.310 ug/L 10/20/09

Bromomethane ND 3.00 0.940 ug/L 10/20/09

Bromochloromethane ND 1.00 0.310 ug/L 10/20/09

Vinyl chloride ND 1.00 0.310 ug/L 10/20/09

Dichlorodifluoromethane ND 1.00 0.310 ug/L 10/20/09

Chloroethane ND 1.00 0.310 ug/L 10/20/09

sec-Butylbenzene ND 1.00 0.310 ug/L 10/20/09

Bromodichloromethane ND 0.500 0.150 ug/L 10/20/09
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934049 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloroethene ND 1.00 0.310 ug/L 10/20/09

2-Butanone (MEK) ND 10.0 3.10 ug/L 10/20/09

Methylene chloride ND 5.00 1.00 ug/L 10/20/09

Trichlorofluoromethane ND 1.00 0.310 ug/L 10/20/09

P & M -Xylene ND 2.00 0.620 ug/L 10/20/09

Naphthalene ND 2.00 0.620 ug/L 10/20/09

o-Xylene ND 1.00 0.310 ug/L 10/20/09

Bromoform ND 1.00 0.310 ug/L 10/20/09

1-Chlorohexane ND 1.00 0.310 ug/L 10/20/09

1,2,4-Trimethylbenzene ND 1.00 0.310 ug/L 10/20/09

tert-Butylbenzene ND 1.00 0.310 ug/L 10/20/09

1,1,1-Trichloroethane ND 1.00 0.310 ug/L 10/20/09

1,1-Dichloroethane ND 1.00 0.310 ug/L 10/20/09

2-Chlorotoluene ND 1.00 0.310 ug/L 10/20/09

Trichloroethene ND 1.00 0.310 ug/L 10/20/09

trans-1,2-Dichloroethene ND 1.00 0.310 ug/L 10/20/09

1,2-Dichlorobenzene ND 1.00 0.310 ug/L 10/20/09

2,2-Dichloropropane ND 1.00 0.310 ug/L 10/20/09

Hexachlorobutadiene ND 1.00 0.310 ug/L 10/20/09

Isopropylbenzene (Cumene) ND 1.00 0.310 ug/L 10/20/09

1,2-Dichloropropane ND 1.00 0.310 ug/L 10/20/09

1,1-Dichloropropene ND 1.00 0.310 ug/L 10/20/09

1,1,2-Trichloroethane ND 1.00 0.310 ug/L 10/20/09

1,3-Dichlorobenzene ND 1.00 0.310 ug/L 10/20/09

1,2,3-Trichlorobenzene ND 1.00 0.310 ug/L 10/20/09

Surrogates 

1,2-Dichloroethane-D4 <surr> 103 73-120 % 10/20/09

Toluene-d8 <surr> 102 80-120 % 10/20/09

4-Bromofluorobenzene <surr> 104 76-120 % 10/20/09

Instrument

Method

Batch VMS10954

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934942 Method Blank

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20181

SW5030B

10/24/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter Results

Reporting/Control

Limit Units

Analysis

MDL Date

Volatile Fuels Department

Gasoline Range Organics ND 100 30.0 ug/L 10/24/09

Surrogates 

4-Bromofluorobenzene <surr> 103 50-150 % 10/24/09

Instrument

Method

Batch VFC9728

SW8015C

HP 5890 Series II PID+HECD VBA
- PRELIMINARY -

Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date Original

Prep

QC results affect the following production samples:

Parameter

QC

Result

Analysis

Date RPD

RPD

Limits

Original

Result Units

Surrogates 

Batch

Method

Instrument
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

932200 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21834

SW3520C

10/16/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Acenaphthylene LCS 0.411 82 ( 50-105 ) 0.5 ug/L 10/24/2009

Acenaphthene LCS 0.412 83 ( 45-110 ) 0.5 ug/L 10/24/2009

Fluorene LCS 0.421 84 ( 50-110 ) 0.5 ug/L 10/24/2009

Phenanthrene LCS 0.438 88 ( 50-115 ) 0.5 ug/L 10/24/2009

Anthracene LCS 0.436 87 ( 55-110 ) 0.5 ug/L 10/24/2009

Fluoranthene LCS 0.486 97 ( 55-125 ) 0.5 ug/L 10/24/2009

Pyrene LCS 0.470 94 ( 50-130 ) 0.5 ug/L 10/24/2009

Benzo(a)Anthracene LCS 0.476 95 ( 55-120 ) 0.5 ug/L 10/24/2009

Chrysene LCS 0.470 94 ( 55-120 ) 0.5 ug/L 10/24/2009

Benzo[b]Fluoranthene LCS 0.469 94 ( 46-130 ) 0.5 ug/L 10/24/2009

Benzo[k]fluoranthene LCS 0.463 93 ( 60-125 ) 0.5 ug/L 10/24/2009

Benzo[a]pyrene LCS 0.464 93 ( 55-120 ) 0.5 ug/L 10/24/2009

Indeno[1,2,3-c,d] pyrene LCS 0.435 87 ( 45-125 ) 0.5 ug/L 10/24/2009

Dibenzo[a,h]anthracene LCS 0.426 85 ( 41-140 ) 0.5 ug/L 10/24/2009

Benzo[g,h,i]perylene LCS 0.441 88 ( 46-125 ) 0.5 ug/L 10/24/2009

Naphthalene LCS 0.406 81 ( 42-100 ) 0.5 ug/L 10/24/2009

1-Methylnaphthalene LCS 0.416 83 ( 46-115 ) 0.5 ug/L 10/24/2009

2-Methylnaphthalene LCS 0.391 78 ( 45-105 ) 0.5 ug/L 10/24/2009

Surrogates 

Terphenyl-d14 <surr> LCS 87 ( 50-135 ) 10/24/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

932200 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21834

SW3520C

10/16/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5160

8270D SIMS

HP 6890 Series II MS2 SVOA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

932696 Lab Control Sample

932698 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

XXX21847

SW3520C

10/19/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Semivolatile Organic Fuels Department

Diesel Range Organics LCS 4.21 84 ( 75-125 ) 5 mg/L 10/26/2009

LCSD 4.02 81 4 (< 20 ) 5 mg/L 10/26/2009

Surrogates 

5a Androstane <surr> LCS 88 ( 60-120 ) 10/26/2009

LCSD 85 3 10/26/2009

Batch

Method

Instrument

XFC8990

SW8015C

HP 6890 Series II FID SV D R
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

933882 Lab Control Sample

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

MXX22423

SW3010A

10/21/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Metals by ICP/MS

Lead LCS 1020 102 ( 80-120 ) 1000 ug/L 10/22/2009

Batch

Method

Instrument

MMS6155

SW6020

Perkin Elmer Sciex ICP-MS P3
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Benzene LCS 28.3 94 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.0 90 5 (< 20 ) 30 ug/L 10/20/2009

Toluene LCS 27.4 91 ( 77-120 ) 30 ug/L 10/20/2009

LCSD 26.3 88 4 (< 20 ) 30 ug/L 10/20/2009

Ethylbenzene LCS 29.3 98 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 28.4 95 3 (< 20 ) 30 ug/L 10/20/2009

n-Butylbenzene LCS 30.7 102 ( 80-124 ) 30 ug/L 10/20/2009

LCSD 29.1 97 5 (< 20 ) 30 ug/L 10/20/2009

1,4-Dichlorobenzene LCS 28.5 95 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.7 93 3 (< 20 ) 30 ug/L 10/20/2009

1,2-Dichloroethane LCS 27.7 92 ( 80-129 ) 30 ug/L 10/20/2009

LCSD 26.1 87 6 (< 20 ) 30 ug/L 10/20/2009

1,3,5-Trimethylbenzene LCS 29.3 98 ( 80-128 ) 30 ug/L 10/20/2009

LCSD 27.6 92 6 (< 20 ) 30 ug/L 10/20/2009

4-Chlorotoluene LCS 29.0 97 ( 79-128 ) 30 ug/L 10/20/2009

LCSD 27.8 93 4 (< 20 ) 30 ug/L 10/20/2009

Chlorobenzene LCS 28.7 96 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.8 93 3 (< 20 ) 30 ug/L 10/20/2009

4-Methyl-2-pentanone (MIBK) LCS 93.3 104 ( 69-134 ) 90 ug/L 10/20/2009

LCSD 90.4 100 3 (< 20 ) 90 ug/L 10/20/2009

cis-1,2-Dichloroethene LCS 26.4 88 ( 80-125 ) 30 ug/L 10/20/2009

LCSD 25.4 85 4 (< 20 ) 30 ug/L 10/20/2009

4-Isopropyltoluene LCS 30.6 102 ( 80-125 ) 30 ug/L 10/20/2009

LCSD 29.1 97 5 (< 20 ) 30 ug/L 10/20/2009

cis-1,3-Dichloropropene LCS 33.1 110 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 30.4 101 9 (< 20 ) 30 ug/L 10/20/2009

n-Propylbenzene LCS 29.0 97 ( 80-129 ) 30 ug/L 10/20/2009

LCSD 27.9 93 4 (< 20 ) 30 ug/L 10/20/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Styrene LCS 30.2 101 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 29.3 98 3 (< 20 ) 30 ug/L 10/20/2009

Dibromomethane LCS 29.6 99 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 28.4 95 4 (< 20 ) 30 ug/L 10/20/2009

trans-1,3-Dichloropropene LCS 28.6 96 ( 80-124 ) 30 ug/L 10/20/2009

LCSD 27.2 91 5 (< 20 ) 30 ug/L 10/20/2009

1,2,4-Trichlorobenzene LCS 31.2 104 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 30.0 100 4 (< 20 ) 30 ug/L 10/20/2009

Acetone LCS 159 176 * ( 50-135 ) 90 ug/L 10/20/2009

LCSD 142 157 * 11 (< 20 ) 90 ug/L 10/20/2009

1,1,2,2-Tetrachloroethane LCS 29.0 97 ( 76-123 ) 30 ug/L 10/20/2009

LCSD 27.9 93 4 (< 20 ) 30 ug/L 10/20/2009

1,2-Dibromo-3-chloropropane LCS 30.9 103 ( 73-130 ) 30 ug/L 10/20/2009

LCSD 31.0 103 0 (< 20 ) 30 ug/L 10/20/2009

Methyl-t-butyl ether LCS 42.1 94 ( 80-120 ) 45 ug/L 10/20/2009

LCSD 39.2 87 7 (< 20 ) 45 ug/L 10/20/2009

Tetrachloroethene LCS 29.4 98 ( 79-122 ) 30 ug/L 10/20/2009

LCSD 28.7 96 2 (< 20 ) 30 ug/L 10/20/2009

Dibromochloromethane LCS 29.2 97 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.6 92 6 (< 20 ) 30 ug/L 10/20/2009

1,3-Dichloropropane LCS 28.2 94 ( 80-121 ) 30 ug/L 10/20/2009

LCSD 27.6 92 2 (< 20 ) 30 ug/L 10/20/2009

1,2-Dibromoethane LCS 29.9 100 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 28.5 95 5 (< 20 ) 30 ug/L 10/20/2009

Carbon tetrachloride LCS 28.1 94 ( 80-126 ) 30 ug/L 10/20/2009

LCSD 26.7 89 5 (< 20 ) 30 ug/L 10/20/2009

1,1,1,2-Tetrachloroethane LCS 28.5 95 ( 80-120 ) 30 ug/L 10/20/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

LCSD 27.3 91 4 (< 20 ) 30 ug/L 10/20/2009

Chloroform LCS 27.9 93 ( 80-124 ) 30 ug/L 10/20/2009

LCSD 26.4 88 6 (< 20 ) 30 ug/L 10/20/2009

Bromobenzene LCS 29.2 97 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.6 92 6 (< 20 ) 30 ug/L 10/20/2009

Chloromethane LCS 38.7 129 * ( 67-125 ) 30 ug/L 10/20/2009

LCSD 36.7 122 5 (< 20 ) 30 ug/L 10/20/2009

1,2,3-Trichloropropane LCS 27.6 92 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 26.8 89 3 (< 20 ) 30 ug/L 10/20/2009

Bromomethane LCS 33.3 111 ( 30-140 ) 30 ug/L 10/20/2009

LCSD 33.4 111 0 (< 20 ) 30 ug/L 10/20/2009

Bromochloromethane LCS 28.3 94 ( 77-129 ) 30 ug/L 10/20/2009

LCSD 26.8 89 6 (< 20 ) 30 ug/L 10/20/2009

Vinyl chloride LCS 38.0 127 ( 72-145 ) 30 ug/L 10/20/2009

LCSD 36.0 120 5 (< 20 ) 30 ug/L 10/20/2009

Dichlorodifluoromethane LCS 49.8 166 * ( 62-153 ) 30 ug/L 10/20/2009

LCSD 46.8 156 * 6 (< 20 ) 30 ug/L 10/20/2009

Chloroethane LCS 30.5 102 ( 67-133 ) 30 ug/L 10/20/2009

LCSD 29.5 99 3 (< 20 ) 30 ug/L 10/20/2009

sec-Butylbenzene LCS 29.6 99 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 28.4 95 4 (< 20 ) 30 ug/L 10/20/2009

Bromodichloromethane LCS 32.4 108 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 30.3 101 7 (< 20 ) 30 ug/L 10/20/2009

1,1-Dichloroethene LCS 29.2 97 ( 76-130 ) 30 ug/L 10/20/2009

LCSD 27.8 93 5 (< 20 ) 30 ug/L 10/20/2009

2-Butanone (MEK) LCS 118 131 ( 66-136 ) 90 ug/L 10/20/2009

LCSD 115 128 2 (< 20 ) 90 ug/L 10/20/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Methylene chloride LCS 29.5 98 ( 63-131 ) 30 ug/L 10/20/2009

LCSD 27.8 93 6 (< 20 ) 30 ug/L 10/20/2009

Trichlorofluoromethane LCS 33.4 111 ( 68-145 ) 30 ug/L 10/20/2009

LCSD 31.0 103 7 (< 20 ) 30 ug/L 10/20/2009

P & M -Xylene LCS 58.5 98 ( 80-120 ) 60 ug/L 10/20/2009

LCSD 56.5 94 4 (< 20 ) 60 ug/L 10/20/2009

Naphthalene LCS 30.2 101 ( 75-120 ) 30 ug/L 10/20/2009

LCSD 28.5 95 6 (< 20 ) 30 ug/L 10/20/2009

o-Xylene LCS 29.4 98 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 28.9 96 2 (< 20 ) 30 ug/L 10/20/2009

Bromoform LCS 31.6 105 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 30.5 102 4 (< 20 ) 30 ug/L 10/20/2009

1-Chlorohexane LCS 44.2 98 ( 70-125 ) 45 ug/L 10/20/2009

LCSD 42.7 95 4 (< 20 ) 45 ug/L 10/20/2009

1,2,4-Trimethylbenzene LCS 29.5 98 ( 80-125 ) 30 ug/L 10/20/2009

LCSD 28.1 94 5 (< 20 ) 30 ug/L 10/20/2009

tert-Butylbenzene LCS 29.5 98 ( 80-122 ) 30 ug/L 10/20/2009

LCSD 27.8 93 6 (< 20 ) 30 ug/L 10/20/2009

1,1,1-Trichloroethane LCS 29.7 99 ( 80-122 ) 30 ug/L 10/20/2009

LCSD 27.6 92 7 (< 20 ) 30 ug/L 10/20/2009

1,1-Dichloroethane LCS 28.4 95 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.0 90 5 (< 20 ) 30 ug/L 10/20/2009

2-Chlorotoluene LCS 27.8 93 ( 80-125 ) 30 ug/L 10/20/2009

LCSD 26.3 88 6 (< 20 ) 30 ug/L 10/20/2009

Trichloroethene LCS 29.0 97 ( 80-125 ) 30 ug/L 10/20/2009

LCSD 27.5 92 5 (< 20 ) 30 ug/L 10/20/2009

trans-1,2-Dichloroethene LCS 29.6 99 ( 79-132 ) 30 ug/L 10/20/2009

LCSD 27.1 90 9 (< 20 ) 30 ug/L 10/20/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dichlorobenzene LCS 28.1 94 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.2 91 3 (< 20 ) 30 ug/L 10/20/2009

2,2-Dichloropropane LCS 30.3 101 ( 80-132 ) 30 ug/L 10/20/2009

LCSD 27.5 92 9 (< 20 ) 30 ug/L 10/20/2009

Hexachlorobutadiene LCS 30.8 103 ( 77-125 ) 30 ug/L 10/20/2009

LCSD 30.0 100 3 (< 20 ) 30 ug/L 10/20/2009

Isopropylbenzene (Cumene) LCS 29.9 100 ( 80-121 ) 30 ug/L 10/20/2009

LCSD 29.0 97 3 (< 20 ) 30 ug/L 10/20/2009

1,2-Dichloropropane LCS 29.7 99 ( 80-121 ) 30 ug/L 10/20/2009

LCSD 28.3 94 5 (< 20 ) 30 ug/L 10/20/2009

1,1-Dichloropropene LCS 30.0 100 ( 80-122 ) 30 ug/L 10/20/2009

LCSD 28.5 95 5 (< 20 ) 30 ug/L 10/20/2009

1,1,2-Trichloroethane LCS 29.7 99 ( 77-120 ) 30 ug/L 10/20/2009

LCSD 28.4 95 5 (< 20 ) 30 ug/L 10/20/2009

1,3-Dichlorobenzene LCS 28.6 95 ( 80-120 ) 30 ug/L 10/20/2009

LCSD 27.1 90 5 (< 20 ) 30 ug/L 10/20/2009

1,2,3-Trichlorobenzene LCS 29.9 100 ( 77-120 ) 30 ug/L 10/20/2009

LCSD 28.9 96 4 (< 20 ) 30 ug/L 10/20/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> LCS 98 ( 73-120 ) 10/20/2009

LCSD 93 5 10/20/2009

Toluene-d8 <surr> LCS 99 ( 80-120 ) 10/20/2009

LCSD 101 2 10/20/2009

4-Bromofluorobenzene <surr> LCS 100 ( 76-120 ) 10/20/2009

LCSD 99 2 10/20/2009
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934050 Lab Control Sample

934051 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20165

SW5030B

10/20/2009

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Gas Chromatography/Mass Spectroscopy

Batch

Method

Instrument

VMS10954

SW8260B

HP 5890 Series II MS3 VNA
Matrix

SGS Ref.#

Client Name 

Project Name/#

Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Prep

934943 Lab Control Sample

934944 Lab Control Sample Duplicate

The Environmental Company, Inc. (TEC)

3354-010 Red Hill BFSF

Water (Surface, Eff., Ground)

VXX20181

SW5030B

10/24/2009

QC results affect the following production samples:

1095622001, 1095622004, 1095622005, 1095622006, 1095622007

Parameter

QC

Results

Pct

Recov

Spiked

Amount 

Analysis

RPD Date

LCS/LCSD

Limits

RPD

Limits

Volatile Fuels Department

Gasoline Range Organics LCS 206 103 ( 79-108 ) 200 ug/L 10/24/2009

LCSD 197 98 5 (< 20 ) 200 ug/L 10/24/2009

Surrogates 

4-Bromofluorobenzene <surr> LCS 99 ( 50-150 ) 10/24/2009

LCSD 100 2 10/24/2009

Batch

Method

Instrument

VFC9728

SW8015C

HP 5890 Series II PID+HECD VBA
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

MXX22423

3010 H20 Digest for Metals ICP-MS

10/21/2009

QC results affect the following production samples:

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Dissolved Metals by ICP/MS

Lead BMS ND 974 97 ( 80-120 ) 1000 ug/L 10/22/2009

BMSD 989 99 2 (< 15 ) 1000 ug/L 10/22/2009

Batch

Method

Instrument

MMS6155

SW6020

Perkin Elmer Sciex ICP-MS P3

Volatile Fuels Department

Gasoline Range Organics BMS ND 527 117* ( 79-108 ) 450 ug/L 10/24/2009

BMSD 420 93 23 * (< 20 ) 450 ug/L 10/24/2009

Surrogates 

4-Bromofluorobenzene <surr> BMS 53.9 108 ( 50-150 ) 10/24/2009

BMSD 53.0 106 2 10/24/2009

Batch

Method

Instrument

VFC9728

SW8015C

HP 5890 Series II PID+HECD VBA

Semivolatile Organic Fuels Department

Diesel Range Organics BMS ND 4.47 81 ( 75-125 ) 5.49 mg/L 10/26/2009

BMSD 4.29 78 4 (< 30 ) 5.49 mg/L 10/26/2009

Surrogates 

5a Androstane <surr> BMS .0938 85 ( 50-150 ) 10/26/2009

BMSD 0.0893 81 5 10/26/2009

Batch

Method

Instrument

XFC8990

SW8015C

HP 6890 Series II FID SV D R

Volatile Gas Chromatography/Mass Spectroscopy
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

VXX20165

Volatiles Extraction AFCEE 3.1 8260 (

10/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

Benzene BMS ND 29.1 97 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.2 97 0 (< 20 ) 30.0 ug/L 10/20/2009

Toluene BMS ND 27.3 91 ( 77-120 ) 30.0 ug/L 10/20/2009

BMSD 28.4 95 4 (< 20 ) 30.0 ug/L 10/20/2009

Ethylbenzene BMS ND 29.8 99 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 30.1 100 1 (< 20 ) 30.0 ug/L 10/20/2009

n-Butylbenzene BMS ND 30.2 101 ( 80-124 ) 30.0 ug/L 10/20/2009

BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 10/20/2009

1,4-Dichlorobenzene BMS ND 28.5 95 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.1 97 2 (< 20 ) 30.0 ug/L 10/20/2009

1,2-Dichloroethane BMS ND 29.3 98 ( 80-129 ) 30.0 ug/L 10/20/2009

BMSD 29.3 98 0 (< 20 ) 30.0 ug/L 10/20/2009

1,3,5-Trimethylbenzene BMS ND 28.9 96 ( 80-128 ) 30.0 ug/L 10/20/2009

BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 10/20/2009

4-Chlorotoluene BMS ND 28.6 96 ( 79-128 ) 30.0 ug/L 10/20/2009

BMSD 29.2 97 2 (< 20 ) 30.0 ug/L 10/20/2009

Chlorobenzene BMS ND 28.7 96 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.9 100 4 (< 20 ) 30.0 ug/L 10/20/2009

4-Methyl-2-pentanone (MIBK) BMS ND 103 115 ( 69-134 ) 90.0 ug/L 10/20/2009

BMSD 102 113 1 (< 20 ) 90.0 ug/L 10/20/2009

cis-1,2-Dichloroethene BMS ND 27.3 91 ( 80-125 ) 30.0 ug/L 10/20/2009

BMSD 28.4 95 4 (< 20 ) 30.0 ug/L 10/20/2009

4-Isopropyltoluene BMS ND 30.1 100 ( 80-125 ) 30.0 ug/L 10/20/2009

BMSD 30.5 102 1 (< 20 ) 30.0 ug/L 10/20/2009

cis-1,3-Dichloropropene BMS ND 33.6 112 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 33.7 112 1 (< 20 ) 30.0 ug/L 10/20/2009

n-Propylbenzene BMS ND 28.5 95 ( 80-129 ) 30.0 ug/L 10/20/2009

BMSD 29.3 98 3 (< 20 ) 30.0 ug/L 10/20/2009

Styrene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 30.7 102 3 (< 20 ) 30.0 ug/L 10/20/2009

Dibromomethane BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 30.4 101 2 (< 20 ) 30.0 ug/L 10/20/2009

trans-1,3-Dichloropropene BMS ND 29.2 97 ( 80-124 ) 30.0 ug/L 10/20/2009

BMSD 28.9 96 1 (< 20 ) 30.0 ug/L 10/20/2009

1,2,4-Trichlorobenzene BMS ND 31.9 106 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 31.6 105 1 (< 20 ) 30.0 ug/L 10/20/2009

Acetone BMS ND 90.6 101 ( 50-135 ) 90.0 ug/L 10/20/2009

BMSD 91.3 101 1 (< 20 ) 90.0 ug/L 10/20/2009

1,1,2,2-Tetrachloroethane BMS ND 29.7 99 ( 76-123 ) 30.0 ug/L 10/20/2009

BMSD 30.6 102 3 (< 20 ) 30.0 ug/L 10/20/2009
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

VXX20165

Volatiles Extraction AFCEE 3.1 8260 (

10/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,2-Dibromo-3-chloropropane BMS ND 31.8 106 ( 73-130 ) 30.0 ug/L 10/20/2009

BMSD 31.6 105 1 (< 20 ) 30.0 ug/L 10/20/2009

Methyl-t-butyl ether BMS ND 44.6 99 ( 80-120 ) 45.0 ug/L 10/20/2009

BMSD 45.4 101 2 (< 20 ) 45.0 ug/L 10/20/2009

Tetrachloroethene BMS ND 29 97 ( 79-122 ) 30.0 ug/L 10/20/2009

BMSD 30.5 102 5 (< 20 ) 30.0 ug/L 10/20/2009

Dibromochloromethane BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.2 97 2 (< 20 ) 30.0 ug/L 10/20/2009

1,3-Dichloropropane BMS ND 29.8 99 ( 80-121 ) 30.0 ug/L 10/20/2009

BMSD 30.3 101 2 (< 20 ) 30.0 ug/L 10/20/2009

1,2-Dibromoethane BMS ND 31.4 105 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 31.9 106 2 (< 20 ) 30.0 ug/L 10/20/2009

Carbon tetrachloride BMS ND 28.2 94 ( 80-126 ) 30.0 ug/L 10/20/2009

BMSD 27.8 93 2 (< 20 ) 30.0 ug/L 10/20/2009

1,1,1,2-Tetrachloroethane BMS ND 28.4 95 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 28.8 96 2 (< 20 ) 30.0 ug/L 10/20/2009

Chloroform BMS ND 28.3 95 ( 80-124 ) 30.0 ug/L 10/20/2009

BMSD 28.6 95 1 (< 20 ) 30.0 ug/L 10/20/2009

Bromobenzene BMS ND 29 97 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.5 98 2 (< 20 ) 30.0 ug/L 10/20/2009

Chloromethane BMS ND 34.5 115 ( 67-125 ) 30.0 ug/L 10/20/2009

BMSD 35.8 119 4 (< 20 ) 30.0 ug/L 10/20/2009

1,2,3-Trichloropropane BMS ND 28.6 95 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 28.3 94 1 (< 20 ) 30.0 ug/L 10/20/2009

Bromomethane BMS ND 35.8 119 ( 30-140 ) 30.0 ug/L 10/20/2009

BMSD 37.9 126 6 (< 20 ) 30.0 ug/L 10/20/2009

Bromochloromethane BMS ND 29.7 99 ( 77-129 ) 30.0 ug/L 10/20/2009

BMSD 29.4 98 1 (< 20 ) 30.0 ug/L 10/20/2009

Vinyl chloride BMS ND 35.1 117 ( 72-145 ) 30.0 ug/L 10/20/2009

BMSD 36.3 121 4 (< 20 ) 30.0 ug/L 10/20/2009

Dichlorodifluoromethane BMS ND 43.6 145 ( 62-153 ) 30.0 ug/L 10/20/2009

BMSD 45.3 151 4 (< 20 ) 30.0 ug/L 10/20/2009

Chloroethane BMS ND 34.3 114 ( 67-133 ) 30.0 ug/L 10/20/2009

BMSD 35.6 119 4 (< 20 ) 30.0 ug/L 10/20/2009

sec-Butylbenzene BMS ND 29.7 99 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 10/20/2009

Bromodichloromethane BMS ND 33.2 111 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 32.4 108 3 (< 20 ) 30.0 ug/L 10/20/2009

1,1-Dichloroethene BMS ND 29.6 99 ( 76-130 ) 30.0 ug/L 10/20/2009

BMSD 29.7 99 0 (< 20 ) 30.0 ug/L 10/20/2009
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

VXX20165

Volatiles Extraction AFCEE 3.1 8260 (

10/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

2-Butanone (MEK) BMS ND 87.2 97 ( 66-136 ) 90.0 ug/L 10/20/2009

BMSD 87.6 97 0 (< 20 ) 90.0 ug/L 10/20/2009

Methylene chloride BMS ND 29.7 99 ( 63-131 ) 30.0 ug/L 10/20/2009

BMSD 31.6 105 6 (< 20 ) 30.0 ug/L 10/20/2009

Trichlorofluoromethane BMS ND 32.7 109 ( 68-145 ) 30.0 ug/L 10/20/2009

BMSD 34.5 115 5 (< 20 ) 30.0 ug/L 10/20/2009

P & M -Xylene BMS ND 59.6 99 ( 80-120 ) 60.0 ug/L 10/20/2009

BMSD 60.9 102 2 (< 20 ) 60.0 ug/L 10/20/2009

Naphthalene BMS ND 31.2 104 ( 75-120 ) 30.0 ug/L 10/20/2009

BMSD 32.0 107 3 (< 20 ) 30.0 ug/L 10/20/2009

o-Xylene BMS ND 29.6 99 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 30.8 103 4 (< 20 ) 30.0 ug/L 10/20/2009

Bromoform BMS ND 31.1 104 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.8 99 4 (< 20 ) 30.0 ug/L 10/20/2009

1-Chlorohexane BMS ND 44 98 ( 70-125 ) 45.0 ug/L 10/20/2009

BMSD 45.8 102 4 (< 20 ) 45.0 ug/L 10/20/2009

1,2,4-Trimethylbenzene BMS ND 28.9 96 ( 80-125 ) 30.0 ug/L 10/20/2009

BMSD 29.8 99 3 (< 20 ) 30.0 ug/L 10/20/2009

tert-Butylbenzene BMS ND 29.2 97 ( 80-122 ) 30.0 ug/L 10/20/2009

BMSD 29.8 99 2 (< 20 ) 30.0 ug/L 10/20/2009

1,1,1-Trichloroethane BMS ND 30.2 101 ( 80-122 ) 30.0 ug/L 10/20/2009

BMSD 29.9 100 1 (< 20 ) 30.0 ug/L 10/20/2009

1,1-Dichloroethane BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.1 97 3 (< 20 ) 30.0 ug/L 10/20/2009

2-Chlorotoluene BMS ND 27.4 91 ( 80-125 ) 30.0 ug/L 10/20/2009

BMSD 28.2 94 3 (< 20 ) 30.0 ug/L 10/20/2009

Trichloroethene BMS ND 29.4 98 ( 80-125 ) 30.0 ug/L 10/20/2009

BMSD 29.7 99 1 (< 20 ) 30.0 ug/L 10/20/2009

trans-1,2-Dichloroethene BMS ND 30 100 ( 79-132 ) 30.0 ug/L 10/20/2009

BMSD 30.2 101 1 (< 20 ) 30.0 ug/L 10/20/2009

1,2-Dichlorobenzene BMS ND 28.3 94 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.2 97 3 (< 20 ) 30.0 ug/L 10/20/2009

2,2-Dichloropropane BMS ND 30.2 101 ( 80-132 ) 30.0 ug/L 10/20/2009

BMSD 30.1 100 0 (< 20 ) 30.0 ug/L 10/20/2009

Hexachlorobutadiene BMS ND 30.2 101 ( 77-125 ) 30.0 ug/L 10/20/2009

BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/20/2009

Isopropylbenzene (Cumene) BMS ND 30.1 100 ( 80-121 ) 30.0 ug/L 10/20/2009

BMSD 31.1 104 4 (< 20 ) 30.0 ug/L 10/20/2009

1,2-Dichloropropane BMS ND 30.4 101 ( 80-121 ) 30.0 ug/L 10/20/2009

BMSD 31.0 103 2 (< 20 ) 30.0 ug/L 10/20/2009
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

VXX20165

Volatiles Extraction AFCEE 3.1 8260 (

10/20/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Volatile Gas Chromatography/Mass Spectroscopy

1,1-Dichloropropene BMS ND 31 103 ( 80-122 ) 30.0 ug/L 10/20/2009

BMSD 30.6 102 1 (< 20 ) 30.0 ug/L 10/20/2009

1,1,2-Trichloroethane BMS ND 30.1 100 ( 77-120 ) 30.0 ug/L 10/20/2009

BMSD 31.3 104 4 (< 20 ) 30.0 ug/L 10/20/2009

1,3-Dichlorobenzene BMS ND 28.6 95 ( 80-120 ) 30.0 ug/L 10/20/2009

BMSD 29.0 97 1 (< 20 ) 30.0 ug/L 10/20/2009

1,2,3-Trichlorobenzene BMS ND 30.8 103 ( 77-120 ) 30.0 ug/L 10/20/2009

BMSD 32.1 107 4 (< 20 ) 30.0 ug/L 10/20/2009

Surrogates 

1,2-Dichloroethane-D4 <surr> BMS 30 100 ( 73-120 ) 10/20/2009

BMSD 29.6 99 1 10/20/2009

Toluene-d8 <surr> BMS 30.2 101 ( 80-120 ) 10/20/2009

BMSD 30.2 101 0 10/20/2009

4-Bromofluorobenzene <surr> BMS 29.3 98 ( 76-120 ) 10/20/2009

BMSD 28.8 96 2 10/20/2009

Batch

Method

Instrument

VMS10954

SW8260B

HP 5890 Series II MS3 VNA

Polynuclear Aromatics GC/MS
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

XXX21834

3520 Liquid/Liquid Ext for 8270 SIM

10/16/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Acenaphthylene BMS ND .436 79 ( 50-105 ) 0.549 ug/L 10/24/2009

BMSD 0.411 76 6 (< 30 ) 0.543 ug/L 10/24/2009

Acenaphthene BMS ND .412 75 ( 45-110 ) 0.549 ug/L 10/24/2009

BMSD 0.398 73 3 (< 30 ) 0.543 ug/L 10/24/2009

Fluorene BMS ND .436 79 ( 50-110 ) 0.549 ug/L 10/24/2009

BMSD 0.423 78 3 (< 30 ) 0.543 ug/L 10/24/2009

Phenanthrene BMS ND .436 79 ( 50-115 ) 0.549 ug/L 10/24/2009

BMSD 0.415 76 5 (< 30 ) 0.543 ug/L 10/24/2009

Anthracene BMS ND .491 89 ( 55-110 ) 0.549 ug/L 10/24/2009

BMSD 0.487 90 1 (< 30 ) 0.543 ug/L 10/24/2009

Fluoranthene BMS ND .523 95 ( 55-125 ) 0.549 ug/L 10/24/2009

BMSD 0.495 91 5 (< 30 ) 0.543 ug/L 10/24/2009

Pyrene BMS ND .507 92 ( 50-130 ) 0.549 ug/L 10/24/2009

BMSD 0.489 90 4 (< 30 ) 0.543 ug/L 10/24/2009

Benzo(a)Anthracene BMS ND .529 96 ( 55-120 ) 0.549 ug/L 10/24/2009

BMSD 0.508 93 4 (< 30 ) 0.543 ug/L 10/24/2009

Chrysene BMS ND .516 94 ( 55-120 ) 0.549 ug/L 10/24/2009

BMSD 0.498 92 3 (< 30 ) 0.543 ug/L 10/24/2009

Benzo[b]Fluoranthene BMS ND .516 94 ( 46-130 ) 0.549 ug/L 10/24/2009

BMSD 0.480 88 7 (< 30 ) 0.543 ug/L 10/24/2009

Benzo[k]fluoranthene BMS ND .529 96 ( 60-125 ) 0.549 ug/L 10/24/2009

BMSD 0.516 95 3 (< 30 ) 0.543 ug/L 10/24/2009

Benzo[a]pyrene BMS ND .536 98 ( 55-120 ) 0.549 ug/L 10/24/2009

BMSD 0.500 92 7 (< 30 ) 0.543 ug/L 10/24/2009

Indeno[1,2,3-c,d] pyrene BMS ND .491 89 ( 45-125 ) 0.549 ug/L 10/24/2009

BMSD 0.445 82 10 (< 30 ) 0.543 ug/L 10/24/2009

Dibenzo[a,h]anthracene BMS ND .486 89 ( 41-140 ) 0.549 ug/L 10/24/2009

BMSD 0.435 80 11 (< 30 ) 0.543 ug/L 10/24/2009

Benzo[g,h,i]perylene BMS ND .481 88 ( 46-125 ) 0.549 ug/L 10/24/2009

BMSD 0.447 82 7 (< 30 ) 0.543 ug/L 10/24/2009

Naphthalene BMS ND .405 74 ( 42-100 ) 0.549 ug/L 10/24/2009

BMSD 0.394 73 3 (< 30 ) 0.543 ug/L 10/24/2009

1-Methylnaphthalene BMS ND .414 75 ( 46-115 ) 0.549 ug/L 10/24/2009

BMSD 0.393 72 5 (< 30 ) 0.543 ug/L 10/24/2009

2-Methylnaphthalene BMS ND .39 71 ( 45-105 ) 0.549 ug/L 10/24/2009

BMSD 0.377 69 3 (< 30 ) 0.543 ug/L 10/24/2009

Surrogates 

Terphenyl-d14 <surr> BMS .515 94 ( 50-135 ) 10/24/2009

BMSD 0.492 90 5 10/24/2009
Matrix

SGS Ref.# Printed Date/Time 10/30/2009 15:29

Batch

Method

Date

Original

Prep

1095622002 Billable Matrix Spike

1095622003 Billable Matrix Spike Dup.

1095622001

Water (Surface, Eff., Ground)

XXX21834

3520 Liquid/Liquid Ext for 8270 SIM

10/16/2009

Parameter

QC

Result

Pct

Recov

Spiked

Amount 

Analysis

Date

MS/MSD

Limits RPD

RPD

Limits

Original

Result Qualifiers

Polynuclear Aromatics GC/MS

Batch

Method

Instrument

XMS5160

8270D SIMS

HP 6890 Series II MS2 SVOA