Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

3319 Santee Cooper-Jefferies Unit 2 No.6 Fuel Oil (residual or bunker C)
Fuel Type 2 Fuel Type 3 Other Fuel Description

 or bunker C)
EIA Facility Code Facility Name Boiler ID Basis Analyte

Analysis Method for each Analyte 

(example: ASTM D5865-04)

3319 Santee Cooper-Jefferies Unit 2 As Received Higher Heating Value ASTM D 240

3319 Santee Cooper-Jefferies Unit 2 As Received % Moisture ASTM D 2216

3319 Santee Cooper-Jefferies Unit 2 As Received Antimony SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Arsenic SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Beryllium SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Cadmium SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Chlorine SW846 5050/9056A

3319 Santee Cooper-Jefferies Unit 2 As Received Chromium SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Cobalt SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Fluorine SW846 5050/9056A

3319 Santee Cooper-Jefferies Unit 2 As Received Lead SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Manganese SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Mercury SW846 7471B

3319 Santee Cooper-Jefferies Unit 2 As Received Nickel SW846 3050B/6020A

3319 Santee Cooper-Jefferies Unit 2 As Received Selenium SW846 3050B/6020A
EIA Facility Code Facility Name Boiler ID

3319 Santee Cooper-Jefferies Unit 2

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture

(as received)

Chlorine

(Dry Basis)

RUN 1(7) 7/14/2010 7/14/2010 18000.00 Btu/lb 287000

RUN 2 (9) 7/15/2010 7/15/2010 18100.00 Btu/lb 351000

RUN 3 (10) 7/15/2010 7/15/2010 18700.00 Btu/lb 294000

Mercury and non-mercury metalic HAPs

HAPs Test Group

 Fuel Testing Results


Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

μg/Kg <10.0 μg/Kg 561 μg/Kg <984 μg/Kg <98.4 μg/Kg

μg/Kg <10.6 μg/Kg 591 μg/Kg <952 μg/Kg <95.2 μg/Kg

μg/Kg <10.2 μg/Kg 539 μg/Kg <911 μg/Kg <91.1 μg/Kg


Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel 

(Dry Basis)

20.5 μg/Kg 347 μg/Kg 6640 μg/Kg 230 μg/Kg 138

19.8 μg/Kg 335 μg/Kg 5990 μg/Kg 233 μg/Kg 138

<182 μg/Kg 325 μg/Kg 5340 μg/Kg 210 μg/Kg 126


Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

μg/Kg <984 μg/Kg <198000 μg/Kg <197 μg/Kg

μg/Kg <952 μg/Kg <199000 μg/Kg <190 μg/Kg

μg/Kg <911 μg/Kg <199000 μg/Kg <182 μg/Kg


EIA Facility Code Facility Name Boiler ID

3319 Santee Cooper-Jefferies Unit 2

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture 

(as received)

Chlorine

(Dry Basis)

RUN 1(4) 7/13/2010 7/13/2010 18400 Btu/lb 311000

RUN 2 (5) 7/13/2010 7/13/2010 18300 Btu/lb 433000

RUN 3(6) 7/13/2010 7/13/2010 18500 Btu/lb 303000

 Fuel Testing Results

HAPs Test Group

Acid gas HAPs


Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

μg/Kg <11.4 μg/Kg 480 μg/Kg <980 μg/Kg <98.0 μg/Kg

μg/Kg <10.2 μg/Kg 513 μg/Kg <978 μg/Kg <97.8 μg/Kg

μg/Kg <11.0 μg/Kg 611 μg/Kg <954 μg/Kg <95.4 μg/Kg


Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis)

23.7 μg/Kg 343 μg/Kg 5400 μg/Kg 200 μg/Kg 122

21.3 μg/Kg 367 μg/Kg 6210 μg/Kg 213 μg/Kg 112

27.5 μg/Kg 370 μg/Kg 6810 μg/Kg 245 μg/Kg 151


Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

μg/Kg <980 μg/Kg <196000 μg/Kg <196 μg/Kg

μg/Kg <978 μg/Kg <195000 μg/Kg <196 μg/Kg

μg/Kg <954 μg/Kg <200000 μg/Kg <191 μg/Kg


EIA Facility Code Facility Name Boiler ID

3319 Santee Cooper-Jefferies Unit 2

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture

(as received)

Chlorine

(Dry Basis)

RUN 1(1) 7/12/2010 7/12/2010 18200.00 Btu/lb 306000

RUN 2 (2) 7/12/2010 7/12/2010 18500.00 Btu/lb 386000

RUN 3 (3) 7/12/2010 7/12/2010 18400.00 Btu/lb 298000

HAPs Test Group

Non-dioxin/furan organic HAPs

 Fuel Testing Results


Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

μg/Kg <10.1 μg/Kg 739 μg/Kg <969 μg/Kg <96.9 μg/Kg

μg/Kg <11.2 μg/Kg 487 μg/Kg <965 μg/Kg <96.5 μg/Kg

μg/Kg <10.7 μg/Kg 465 μg/Kg <940 μg/Kg <94.0 μg/Kg


Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis)

20.3 μg/Kg 354 μg/Kg 6340 μg/Kg 278 μg/Kg 180

31.9 μg/Kg 365 μg/Kg 6700 μg/Kg 230 μg/Kg 142

19.2 μg/Kg 322 μg/Kg 5560 μg/Kg 248 μg/Kg 125


Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

μg/Kg <969 μg/Kg <197000 μg/Kg <194 μg/Kg

μg/Kg <965 μg/Kg <200000 μg/Kg <193 μg/Kg

μg/Kg <940 μg/Kg <196000 μg/Kg <188 μg/Kg


EIA Facility Code Facility Name Boiler ID

3319 Santee Cooper-Jefferies Unit 2

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

% Moisture

(as received)

Chlorine

(Dry Basis)

RUN 1 (8) 7/15/2010 7/15/2010 19200.00 Btu/lb 269000

RUN 2 (10) 7/15/2010 7/15/2010 18700.00 Btu/lb 294000

RUN 3 (11) 7/16/2010 7/16/2010 18100.00 Btu/lb 267000

Dioxin/furan HAPs

HAPs Test Group

 Fuel Testing Results


Chlorine 

Units

Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

μg/Kg <11.5 μg/Kg 396 μg/Kg <936 μg/Kg <93.6 μg/Kg

μg/Kg <10.2 μg/Kg 539 μg/Kg <911 μg/Kg <91.1 μg/Kg

μg/Kg <11.9 μg/Kg 537 μg/Kg <914 μg/Kg <91.4 μg/Kg


Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel 

(Dry Basis)

21.2 μg/Kg 319 μg/Kg 6020 μg/Kg 203 μg/Kg 104

<182 μg/Kg 325 μg/Kg 5340 μg/Kg 210 μg/Kg 126

25.2 μg/Kg 347 μg/Kg 6530 μg/Kg 258 μg/Kg 146


Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry

Basis) Cobalt Units

μg/Kg <936 μg/Kg <199000 μg/Kg <187 μg/Kg

μg/Kg <911 μg/Kg <199000 μg/Kg <182 μg/Kg

μg/Kg <914 μg/Kg <198000 μg/Kg <183 μg/Kg


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

μg/Kg

nit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm

μg/Kg