Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-
5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

3319 Santee Cooper-Jefferies Unit 2 No.6 Fuel Oil (residual or bunker C)Fuel Type 2 Fuel Type 3 Other Fuel Description No.6 Fuel Oil (residual or bunker C)EIA

Facility Code Facility Name Boiler ID Basis An alyte An alysis M ethod for each Analyte (example: ASTM D5865-04)
3319 Santee Cooper-Jefferies Unit 2 As Received Higher Heating Value ASTM D 240 3319 Santee Cooper-Jefferies Unit 2 As Received % Moisture ASTM D 2216 3319 Santee Cooper-Jefferies Unit 2 As Received Antim ony SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Arsenic SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Beryllium SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Cadmium SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Chlorine SW846 5050/9056A 3319 Santee Cooper-Jefferies Unit 2 As Received Chromium SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Cobalt SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Fluorine SW846 5050/9056A 3319 Santee Cooper-Jefferies Unit 2 As Received Lead SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Manganese SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Mercury SW846 7471B 3319 Santee Cooper-Jefferies Unit 2 As Received Nickel SW846 3050B/6020A 3319 Santee Cooper-Jefferies Unit 2 As Received Selenium SW846 3050B/6020AEIA

Facility Code Facility

Name Boiler ID 3319 Santee Cooper-Jefferies Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1(7) 7/14/2010 7/14/2010 18000.00 Btu/lb 287000 RUN 2 (9) 7/15/2010 7/15/2010 18100.00 Btu/lb 351000 RUN 3 (10) 7/15/2010 7/15/2010 18700.00 Btu/lb 294000 Mercury and non-mercury metalic HAPs HAPs Test Group

Fuel Testing ResultsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg <10.0 μg/Kg 561 μg/Kg <984 μg/Kg <98.4 μg/Kg μg/Kg <10.6 μg/Kg 591 μg/Kg <952 μg/Kg <95.2 μg/Kg μg/Kg <10.2 μg/Kg 539 μg/Kg <911 μg/Kg <91.1 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) 20.5 μg/Kg 347 μg/Kg 6640 μg/Kg 230 μg/Kg 138 19.8 μg/Kg 335 μg/Kg 5990 μg/Kg 233 μg/Kg 138 <182 μg/Kg 325 μg/Kg 5340 μg/Kg 210 μg/Kg 126Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg <984 μg/Kg <198000 μg/Kg <197 μg/Kg μg/Kg <952 μg/Kg <199000 μg/Kg <190 μg/Kg μg/Kg <911 μg/Kg <199000 μg/Kg <182 μg/KgEIA

Facility Code Facility

Name Boiler ID 3319 Santee Cooper-Jefferies Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1(4) 7/13/2010 7/13/2010 18400 Btu/lb 311000 RUN 2 (5) 7/13/2010 7/13/2010 18300 Btu/lb 433000 RUN 3(6) 7/13/2010 7/13/2010 18500 Btu/lb 303000 Fuel Testing Results HAPs Test Group Acid gas HAPsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg <11.4 μg/Kg 480 μg/Kg <980 μg/Kg <98.0 μg/Kg μg/Kg <10.2 μg/Kg 513 μg/Kg <978 μg/Kg <97.8 μg/Kg μg/Kg <11.0 μg/Kg 611 μg/Kg <954 μg/Kg <95.4 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 23.7 μg/Kg 343 μg/Kg 5400 μg/Kg 200 μg/Kg 122 21.3 μg/Kg 367 μg/Kg 6210 μg/Kg 213 μg/Kg 112 27.5 μg/Kg 370 μg/Kg 6810 μg/Kg 245 μg/Kg 151Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg <980 μg/Kg <196000 μg/Kg <196 μg/Kg μg/Kg <978 μg/Kg <195000 μg/Kg <196 μg/Kg μg/Kg <954 μg/Kg <200000 μg/Kg <191 μg/KgEIA

Facility Code Facility

Name Boiler ID 3319 Santee Cooper-Jefferies Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1(1) 7/12/2010 7/12/2010 18200.00 Btu/lb 306000 RUN 2 (2) 7/12/2010 7/12/2010 18500.00 Btu/lb 386000 RUN 3 (3) 7/12/2010 7/12/2010 18400.00 Btu/lb 298000 HAPs Test Group Non-dioxin/furan organic HAPs

Fuel Testing ResultsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg <10.1 μg/Kg 739 μg/Kg <969 μg/Kg <96.9 μg/Kg μg/Kg <11.2 μg/Kg 487 μg/Kg <965 μg/Kg <96.5 μg/Kg μg/Kg <10.7 μg/Kg 465 μg/Kg <940 μg/Kg <94.0 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 20.3 μg/Kg 354 μg/Kg 6340 μg/Kg 278 μg/Kg 180 31.9 μg/Kg 365 μg/Kg 6700 μg/Kg 230 μg/Kg 142 19.2 μg/Kg 322 μg/Kg 5560 μg/Kg 248 μg/Kg 125Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg <969 μg/Kg <197000 μg/Kg <194 μg/Kg μg/Kg <965 μg/Kg <200000 μg/Kg <193 μg/Kg μg/Kg <940 μg/Kg <196000 μg/Kg <188 μg/KgEIA

Facility Code Facility

Name Boiler ID 3319 Santee Cooper-Jefferies Unit 2

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) Chlorine

(Dry Basis) RUN 1 (8) 7/15/2010 7/15/2010 19200.00 Btu/lb 269000 RUN 2 (10) 7/15/2010 7/15/2010 18700.00 Btu/lb 294000 RUN 3 (11) 7/16/2010 7/16/2010 18100.00 Btu/lb 267000 Dioxin/furan HAPs HAPs Test Group

Fuel Testing ResultsChlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units μg/Kg <11.5 μg/Kg 396 μg/Kg <936 μg/Kg <93.6 μg/Kg μg/Kg <10.2 μg/Kg 539 μg/Kg <911 μg/Kg <91.1 μg/Kg μg/Kg <11.9 μg/Kg 537 μg/Kg <914 μg/Kg <91.4 μg/KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel

(Dry Basis) 21.2 μg/Kg 319 μg/Kg 6020 μg/Kg 203 μg/Kg 104 <182 μg/Kg 325 μg/Kg 5340 μg/Kg 210 μg/Kg 126 25.2 μg/Kg 347 μg/Kg 6530 μg/Kg 258 μg/Kg 146Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units μg/Kg <936 μg/Kg <199000 μg/Kg <187 μg/Kg μg/Kg <911 μg/Kg <199000 μg/Kg <182 μg/Kg μg/Kg <914 μg/Kg <198000 μg/Kg <183 μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg μg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/Kg