标题：沃氏实用有机化学教程
图书信息
出版社: 世界图书出版公司; 第1版 (2004年1月1日)
外文书名: Vogel's Textbook of Practical Chemistry 5th ed. Vo1.1
平装: 823页
正文语种: 英语
开本: 24
ISBN: 7506265842
条形码: 9787506265843
尺寸: 22 x 14.6 x 4 cm
重量: 975 g
内容简介
《沃氏实用有机化学教程(第1卷)(第5版)》内容简介：This is the second time that we have prepared a new edition of Vogel's Textbook of Organic Chemistry and it is important to reaffirm the aims set out by the late Dr A. I. Vogel in the preface to the first edition. Thus in this new edition every endeavour is made to retain the comprehensive character of the book, and to ensure that it continues to be a one-volume reference text which is of value to practising organic chemists throughout their undergraduate, postgraduate and subsequent careers.
目录
CHAPTER 1 ORGANIC SYNTHESIS
1.1 INTRODUCTION
1.2 STRUCTURE OF THE TARGET MOLECULE
1.3 REACTION MECHANISM AND THE METHODOLOGY OF SYNTHESIS
1.4 REACTION MECHANISM AND THE STRATEGY OF SYNTHESIS
1.5 CONCLUSION
REFERENCES
CHAPTER 2 EXPERIMENTAL TECHNIOUES
2.1 GENERAL INSTRUCTIONS FOR SAFE WORKING IN ORGANIC CHEMICAL LABORATORIES
2.2 PLANNING OF EXPERIMENTS AND RECORDING OF RESULTS
2.3 HAZARDS IN ORGANIC CHEMISTRY LABORATORIES
APPARATUS AND REACTION PROCEDURES
2.4 INTERCHANGEABLE GROUND GLASS JOINTS
2.5 TYPES OF GROUND GLASS JOINTS
2.6 CARE AND MAINTENANCE OF GROUND GLASS JOINTS
2.7 APPARATUS WITH INTERCHANGEABLE GROUND GLASS JOINTS SUITABLE FOR GENERAL USE IN PREPARATIVE ORGANIC CHEMISTRY
2.8 OTHER TYPES OF INTERCHANGEABLE JOINTS AND STOPCOCKS
2.9 THE USE OF CORKS AND RUBBER STOPPERS
2.10 CUTTING AND BENDING OF GLASS TUBING
2.11 GENERAL LABORATORY APPARATUS
2.12 COOLING OF REACTION MIXTURES
2.13 JEATOMG PF REACTOPM MIXTIRES
2.14 MECJAMOCAL AGOTATION
2.15 TYPICAL GROUND GLASS JOINT ASSEMBLIES FOR STANDARD REACTION PROCEOURES
2.16 PRECAUTIONS FOR UNATTENEDE REACTINS
2.17 APPARATUS FOR SPECIAL REACTION TECHNIQUES
ISOLATION AND PURIFICATION PROCESSES
2.18 GENERAL CONSIDERATIONS
2.19 FILTRATION TECHNIQUES
2.20 RECRYSTALLISATION TECHNIQUES
2.21 SUBLIMATION TECHNIQUES-FREEZE DRYING
2.22 SOLVENT EXTRACTION
2.23 DRYING OF LIQUIDS OR OF SOLUTIONS OF ORGANIC COMPOUNDS IN ORGANIC SOLVENTS
2.24 DISTILLATION AT ATMOSPHERIC PRESSURE
2.25 STEAM DISTILLATION
2.26 FRACTIONAL DISTILLATION AT ATMOSPHERIC PRESSURE
2.27 DISTILLATION UNDER DIMINISHED PRESSURE ('VACUUM' DISTILLATION)
2.28 HIGH VACUUM DISTILLATION - MOLECULAR DISTILLATION
2.29 VACUUM PUMPS
2.36 MANOMETERS, VACUSTATS, VACUUM GAUGES AND MANOSTATS
2.31 CHROMATOGRAPHY
2.32 STORAGE OF SAMPLES
2.33 MELTING POINT - MIXED MELTING POINTS
2.34 DETERMINATION OF BOILING POINT
2.35 DETERMINATION OF MOLECULAR WEIGHT
2.36 DETERMINATION OF OPTICAL ROTATORY POWER
2.37 DETERMINATION OF REFRACTIVE INDEX
REFERENCES
CHAPTER 3 SPECTROSCOPIC METHODS AND THE INTERPRETATION OF SPECTRA
Introduction
The electromagnetic spectrum
3.1 INFRARED SPECTROSCOPY
Instrumental features of infrared spectrophotometers
Determination of infrared spectra
Sample preparation
Features of an infrared spectrum
Interpretation of an infrared spectrum
Characteristic group frequencies
3.2 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Features of the nuclear magnetic resonance spectrum
The chemical shift
Spin-spin splitting
Protons attached to heteroatoms
Simplification of 'H spectra
Interpretation of the p.m.r, spectrum
Further information from 13 C-spectra
3.3 MASS SPECTROMETRY
The mass spectrum
Appearance of the mass spectrum
Interpretation of the mass spectrum
Mass spectra of classes of organic compounds
3.4 ULTRAVIOLET-VISIBLE SPECTROSCOPY
Instrumental features of ultraviolet-visible spectrophotometers
Determination of ultraviolet-visible spectra
Laws of light absorption
Solvents for ultraviolet spectroscopy
Solution preparation
Optical cells and their care
Features of an ultraviolet-visible spectrum
REFERENCES
CHAPTER 4 SOLVENTS AND REAGENTS
4.1 THE PURIFICATION OF COMMON ORGANIC SOLVENTS
Saturated aliphatic hydrocarbons
Aromatic hydrocarbons
Halogenated hvdrocarbons
Aliphatic alcohols
Ethers
Ketones
Esters
Nitrogen-containing solvents
Sulphur-containing solvents
Phosphorus-containing solvents
4.2 THE PREPARATION AND PURIFICATION OF REAGENTS
REFERENCES
CHAPTER 5 ALIPHATIC COMPOUNDS
5.1 ALKANES
Structure
Summary of preparative methods and of retrosynthetic strategies
Spectroscopic features
5.1.1 The catalytic hydrogenation and chemical reduction of alkenes
5.1.2 The hvdrolysis of alkylmagnesium halides and the hydrogenolysis of alkyl halides and of alkyl methane- or toluene-p-suiphonates
5.1.3 The reduction of aldehydes and ketones
5.1.4 Coupling reactions (a) using organometallic compounds, and
(b) at the anode
5.2 ALKENES
Structure
Summary of preparative methods and of retrosynthetic strategies
Spectroscopic features
5.2.1 1,2-Elimination processes ([i-elimination)
5.2.2 The partial hydrogenation of aikynes
5.2.3 Wittig and related reactions
5.2.4 Selected rearrangements of alkynes to allenes
5.3 ALKYNES
Structure
Summary of preparative methods and of retrosynthetic strategies
Spectroscopicfeatures
5.3.1 The dehydrogenation of vic- and gem-dihalides
5.3.2 The oxidation of dihydrazones of 1,2-diketones
5.3.3 Aikylation of a terminal alkyne
5.3.4 Coupling reactions leading to diynes
5.4 ALIPHATIC ALCOHOLS
Structure
Summary of preparative methods and of retrosynthetic strategies
Spectroscopicfeatures
5.4.1 The reduction of aldehydes, ketones and esters
5.4.2 The interaction of carbonyl-containing compounds with organometallic reagents
5.4.3 The hydroboration-oxidation of alkenes
5.4.4 The oxymercuration-demercuration of alkenes
5.4.5 The hydroxylation of alkenes
5.4.6 Methods for the protection of the hydroxyl group
……
CHAPTER 6 AROMATIC COMPOUNDS
CHAPTER 7 SELECTED ALICYCLIC ALICYCLIC COMPOUNDS
CHAPTER 8 SELECTED HETEROCYCLIC COMPOUNDS
CHAPTER 9 INVESTIGATION AND CHARACTERISATION OF ORGANIC COMPOUNDS
CHAPTER 10 PHYSICAL CONSTANTS OF ORGANIC COMPOUNDS
APPENDICES
Table of atomic weights
Index
Reference data
Abbreviations     

图书信息
出版社: 商务印书馆; 第1版 (2007年9月1日)
平装: 311页
开本: 32开
ISBN: 9787100040228
条形码: 9787100040228
尺寸: 20.5 x 14 x 1.5 cm
重量: 322 g
内容简介
本书汇集了1917年十月革命起至1945年二战结束后世界史学科的基础史料而成，分为亚洲国家、非洲国家和第二次世界大战三个部分。史料经过精心遴选，译文再三推敲达到较高水平。编者齐世荣是我国世界史学科最早的学术领头人之一，现为首都师范大学名誉校长、历史系教授。
目录
第五部分 亚洲国家
日本
朝鲜
越南
印度
印度尼西亚
土耳其
巴勒斯坦和外约旦
第六部分 非洲国家
埃及
摩洛哥
埃塞俄比亚
第七部分 第二次世界大战