HIGH PERFORMANCE,ROBUST, EASY-TO-USE
MULTI-ELEMENTAL
ANALYSIS
ICP-MS2

INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY
Advion Interchim ScientificTM has produced the SOLATION® ICP-MS - theultimate instrument for multi-element analysis, providing high sensitivity
measurement of trace elements from a wide range of matrices.
Designed for ease-of-use, with intuitive software, the SOLATION® ICP-MS
is the ideal instrument for environmental, pharmaceutical, food safety,
agricultural, and clinical laboratories everywhere.

ICP-MSMAXIMIZE EFFICIENCIES WITH ICP-MS
For quantitative, elemental analyses, the SOLATION® ICP-MS is
the ideal system for R & D laboratories seeking the perfect mix of
performance and ease-of-use.

ADVANCE YOUR APPLICATIONS WITH MULTIELEMENTAL ANALYSIS AT YOUR FINGERTIPS
Adding the SOLATION® ICP-MS to your lab opens up a world of possibilities forenvironmental, biomedical, food, agriculture and geological testing and research.

INCREASE YOUR THROUGHPUT,
DECREASE YOUR WORKLOAD
The thoughtfully designed SOLATION® ICP-MS puts the power oftrace, multi-elemental analysis in your hands by simplifying andoptimizing the typical ICP-MS workflow, inside and out.
The SOLATION® ICP-MS offers a state of the art quadrupole
deflector that ensures the analyzer and detector stay clean, andimproves S/N by preventing neutrals and particles from entering
the analyzer.

ADVANCED, INTUITIVE SOFTWARE FOR SPEED AND EASE OF USE
The SOLATION® ICP-MS is delivered with a full suite of robust, intuitive software designed to provide answers with the fewest
clicks, including:
ICP-MS Express: Provides seamless workflow to configure and control the instrument with integrated control of peripherals,
including: peristaltic pump, liquid autosampler and Rapid Sample Interface. The program offers an easy to use interface for system
control, method development, sample entry and data acquisition.
Quant Express: Simple user interface for batch processing of ICP-MS data for versatile quantitative analysis and easy creation ofreports.

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Food and Agriculture: Ensure the quality and safety of food and raw ingredientsby relying on the power of ICP-MS for full elemental analysis. Ideal for meeting
regulatory requirements for baby food and crop safety.
Environmental Analysis: Ensure Earth's most precious resources remain viable withthe help of ICP-MS technology. Determine purity of drinking water, well water,
waste water and soils, and use the system as a tool to monitor industrial site
remediation.
Biomedical: Monitor biological matrices, including urine, serum, plasma,
whole blood and tissue samples for toxicity and nutritional indicators. Satisfy
the allowable limits in pharmaceutical and clinical applications with a single
instrument.

INTRODUCING TLC/ICP-MS FOR PREP-FREE
SAMPLE ANALYSIS OF SWIPE SURFACES
Advion Interchim Scientific offers a new, novel sample
introduction technique, coupling the best-selling Plate
ExpressTM automated microextraction tool with the
SOLATION® ICP-MS for a new technique known as
TLC/ICP-MS.
Using a swipe surface or TLC plate, users can
now introduce a sample to the ICP-MS in minutes,
offering a significant advancement from the traditional
workflow. Obtain isotopic ratio measurements fasterand easier than ever before.

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3

4

THE SOLATION® ICP-MS

5Gate valve

Ion extraction cones

Allows quick and easy maintenanceand replacement of the cones whilst
maintaining vacuum integrity.

Triple-cone ion extraction. The third extraction cone, followed by an
Einzel lens, are electrically controlled to maximize transmission ofions into the vacuum system.

90° Quadrupole deflector
Ensures that the analyzer and detector are not in line with the plasmabeam, preventing neutrals and particles from entering the analyzer,
improving S/N and preventing contamination.

RF coil
Plasma generation with water cooled RF coil using industry
standard 27 MHz variable frequency generator for rapid
impedance matching and ultimate performance with challenging
matrices.

Torch
One-piece torch with fast, one-step connection of argon andigniter. Silver guard shield to prevent secondary discharge.

Nebulizer
High efﬁciency concentric nebulizer available inquartz and PFA for compatibility with the widest
range of ﬂow rates and sample composition.

Octupole collision cell
Acts as an ion guide and a collision cell with He gas toprovide Kinetic Energy Discrimination (KED) to remove
interferences.

Spray chamber
The cyclonic spray chamber with optional temperature control anddilution gas further reduces droplet size to ensure stable, efficient
plasma.

Quadrupole Analyzer

Unique high frequency mass filter design with the highest
stability to simultaneously maximize transmission, resolution,
and abundance sensitivity.

Dual function detectors

Peristaltic pump

Measures in both analog and pulse detection modes
with seamless transmission between the two, to allow
measurement of high and low levels in a single analysis
with more than 9 orders of magnitude in linear dynamic
range.
Pulse Detection: captures ions generating pulses shorter than
20 ns; accurate and linear for up to 7 orders of magnitude.
Minimum dwell time of less than100 µs
Analog Detection: used for higher ion signals while
deactivating pulse detection to extend detector lifetime.

Integrated 4-channel,
12-roller pump for
maximum flexibility andultra-low pulsation.
Software controlled
flow rate from low µL/
min to mL/min.

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6

SOLATION® ICP-MS SOFTWARE PACKAGEUPGRADE YOUR WORKFLOW WITH ICP-MS EXPRESS

A modern user interface to help simplify method development,
experiment creation and data acquisition – starting and completingyour run with just a single click.

Experience a simplified user interface
and streamlined workflow for optimized,
automatic calibration and tuning.

•
•
•

•

Achieve optimized data acquisition withreal time graphing of spectrum and time
resolved signals during manual runs orbatch acquisition.

Autotune, including x,y position of torch, for resolution and maximum
sensitivity with minimum creation of oxides and doubly charged
species.
Optimize mass calibration, detector gain and pulse to analog factor
Reporting on 9 performance tests for instrument specifications:› Background› Abundance Sensitivity› Resolution and Mass Calibration› Detection Limit› Sensitivity› Oxide› Doubly Charged› Isotope Ratio Precision› Pulse/Analog Calibration
Real time display of spectrum and time-resolved signals

Optimized sample list for easy workflow
ICP-MS Express simplifies your setup to quickly and easily
create experiment batches.
••••

Multiple sample lists can be submitted.
Sample lists can be copied and pasted fromspreadsheets like Excel
Simple editing and reprocessing.
Supports autosampler position and vial size selection

With ICP-MS Express, data collection is automatically optimized by
selecting the pulse or analog data stream for each element depending on
signal intensity. Thanks to built-in onboard databases, users can accesseasy, automatic element selection and interference correction, with theability to utilize:• A graphical periodic table to select elements to analyze

Quantitative calibration curve for meticulous accuracy
With ICP-MS Express, the quantitation method supports:

•
•
•

•
•
•
•

NIST isotope table
Standard interference correction equations (user editable)
Standard list of excluded masses (user editable)

Automatically applies interference corrections, if selected,
and records semi quantitative results in the same report

Access qualitative, semi-quantitative and full quantitative data acquisition modes• View raw data from pulse, analog or auto signals in qualitative mode
• Semi quantitative feature allows scanning for unknowns during
quantitative analyses

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External standard (with or without internal standard)
Elemental and Isotope Ratio reporting
Quality Control standards
Standard addition

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7

8

9

NATURAL PRODUCTS, FOOD AND AGRICULTURE

Repeatability: Table 2
Six samples were spiked at 100% of the action level and digested. The results that aresummarized in Table 7 show that the %RSD
of the measured concentrations are between
1.3% - 3.7%, demonstrating repeatability
well below the 20% limit.

Fast and reliable testing methods for safety and nutrition in plantmaterial and foodstuffs, including screening and speciation analysisof raw ingredients, final products, and beverages.
APPLICATION STUDY:

Table 2: USP<233> Repeatability results
75

Repeatability

USP<233> also defines the accuracy, repeatability, and ruggedness
required for the analysis of these toxic elements:

Accuracy

Repeatability

Ruggedness

The matrix and materials underinvestigation must be spikes with target
elements at concentrations that are 50%,
100%, and 150% of the maximum
permitted daily exposure (PDE). Mean
spike recoveries for each target element
must be within 70%-150% of the actual.

Six independent samples of the material
under investigation must be spiked at100% of the target limits defined andanalyzed. The measured percent relative
standard deviation (%RSD) must notexceed 20% for each target element.

Carrying out the repeatability measurement testing procedure by analyzing
the six repeatability test solutions either
on different days, either with a different
instrument or by a different analyst. The%RSD of the 12 replicates must be lessthan 25% for each target element.

ng/g

Hg

ng/g

208

Pb

ng/g

512.12

94.94

628.41

Hemp 100% spk 3

247.44505.0092.70

569.59242.88529.0099.86

558.30Hemp 100% spk 4

243.11535.7494.65

569.80Hemp 100% spk 6

242.42520.98104.68578.92244.08522.2397.74

578.46

2.8

11.8

4.4

25.4

SD

PDE limits for states that use the USP guidelines for heavy metal
exposure by inhalation.

202

Cd

247.60Hemp 100% spk 2

Average%RSD (< 20%)

The SOLATION® ICP-MS is the preferred method for heavy metal analysis of plant materials.
The system is suitable for the accurate, robust and reproducible analysis of heavy metals in plantmaterial – greatly exceeding the requirements of USP <233> protocol.

ng/g

111

Hemp 100% spk 1

Hemp 100% spk 5

ANALYZING HEAVY METAL IN PLANTS WITH THE
SOLATION® ICP-MS

As

241.051.1%

530.5399.59

565.71

2.3%

4.6%

4.4%

111 111111

202 202202

208 208
208

Table 3: USP<233> Ruggedness results
Ruggedness: Table 3
The repeatability sample set was preparedand run on a different day by a different analyst. The results from that run are combinedwith the previous run to determine the ruggedness. The ruggedness values are similar
to the repeatability values and the measured%RSD (2.4 – 4.0%) are comfortably underthe 25% limit defined by the USP method.
The results are summarized in Table 8.

75

Ruggedness
Ruggedness
Ruggedness

75 75

As AsAs

Cd Cd
Cd

Hg Hg
Hg

Pb PbPb

ng/gng/g
ng/g ng/gng/g
ng/g ng/gng/g
ng/g ng/gng/gng/g

DayDay
1 Day
Hemp
1 Hemp1 Hempspike
spike
1spike1247.60
1 247.60
247.60512.12
512.12512.12 94.94
94.94
94.94 628.41
628.41628.41
DayDay
1 Day
Hemp
1 Hemp1 Hempspike
spike
2spike2242.88
2 242.88
242.88529.00
529.00529.00 99.86
99.86
99.86 558.30
558.30558.30
DayDay
1 Day
Hemp
1 Hemp1 Hempspike
spike
3spike3247.44
3 247.44
247.44505.00
505.00505.00 92.70
92.70
92.70 569.59
569.59569.59
DayDay
1 Day
Hemp
1 Hemp1 Hempspike
spike
4spike4243.114 243.11
243.11535.74
535.74535.74 94.65
94.65
94.65 569.80
569.80569.80
DayDay
1 Day
Hemp
1 Hemp1 Hempspike
spike
5spike5241.05
5 241.05
241.05530.53
530.53530.53 99.59
99.59
99.59 565.71
565.71565.71

DayDay
1 Day
Hemp
1 Hemp1 Hempspike
spike
6spike6242.42
6 242.42
242.42520.98
520.98520.98104.68
104.68104.68578.92
578.92578.92
DayDay2 Day
Hemp
2 Hemp2 Hempspike
spike
1spike1239.12
1 239.12
239.12488.82
488.82488.82102.34
102.34102.34625.59
625.59625.59
DayDay2 Day
Hemp
2 Hemp2 Hempspike
spike
2spike2249.26
2 249.26
249.26504.43
504.43504.43103.79
103.79103.79574.59
574.59574.59
DayDay2 Day
Hemp
2 Hemp2 Hempspike
spike
3spike3233.68
3 233.68
233.68478.98
478.98478.98 98.79
98.79
98.79 564.66
564.66564.66
DayDay2 Day
Hemp
2 Hemp2 Hempspike
spike
4spike4246.33
4 246.33
246.33512.50
512.50512.50 95.95
95.95
95.95 568.29
568.29568.29
DayDay2 Day
Hemp
2 Hemp2 Hempspike
spike
5spike5244.67
5 244.67
244.67508.67
508.67508.67 97.66
97.66
97.66 570.90
570.90570.90
DayDay2 Day
Hemp
2 Hemp2 Hempspike
spike
6spike6229.10
6 229.10
229.10496.94
496.94496.94 97.83
97.83
97.83 583.11
583.11
583.11
Average
Average
Average242.22242.22242.22510.31
510.31510.31 98.57
98.57
98.57 579.82
579.82579.82
SD SDSD5.9 5.95.9

17.117.1
17.1

3.7 3.73.7

23.023.0
23.0%RSD(< 25%)
2.4%
%RSD
%RSD
(<(<
25%)
25%)
2.4%
2.4% 3.3%
3.3%
3.3% 3.8%
3.8%
3.8% 4.0%
4.0%
4.0%

Table 1: Accuracy- Spike recoveries
Accuracy: Table 1
The samples were spiked at 50%, 100%,
and 150% of the action level (Table 2
above) and the percent recoveries calculated. Spike recoveries were all between
92.5% - 114.1%, well within the 70150% range defined by the USP method.

Spike Recoveries

75

As

111

Cd

202

Hg

208

Pb

Averages

ng/g

ng/g

ng/g

ng/g

Hemp unspiked avg.

42.2

305.6

5.7

52.5

50% Spike avg.

142.0

402.9

52.6

314.4

% recovery

99.8%

97.4%

93.6%

104.8%% recovery

100.3%

97.9%

93.8%

114.1%% recovery

100.0%

110.7%

92.5%

102.2%

100% Spike avg.
150% Spike avg.

242.7

342.2

501.4

637.6

99.6

144.5

622.9

818.8

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NIST 1575a Results: Table 4
The results for the NIST SRM are summarized in Table 9. The values for As
and Hg were less than the low standard
in solution but there is good agreement
between the experimental values and thecertified values.

Table 4: NIST 1575a Pine Needles SRM

NIST 1575 Pine ng/g

75

As

111

Cd

202

Hg

208

Pb

Certified Values

39.0

233.0

39.9

167.0

%error

-1.61%-4.37%-9.83%

1.39%%error

1.86%-0.59%-11.54%0.69%

Day 1 avg.

Day 2 avg.

38.4

39.7

222.8

231.6

36.0

35.3

169.3

168.2

THE SOLATION® ICP-MS GREATLY EXCEEDS THE REQUIREMENTS
OF USP <233>.
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10

SOIL ANALYSISThe combination of the quadrupole deflector and the collision cell minimizes drift andensures accuracy and precision over time. The reported method benefits from the fast
collision cell gas switching capabilities of the SOLATION® to analyze a wide range ofelements in soil for rapid, accurate and reproducible results.
APPLICATION STUDY:ANALYZING HEAVY METALS IN SOIL WITH THE SOLATION® ICP-MS
The SOLATION® ICP-MS offers an ideal method for routine elemental analysis. The system is suitable for elemental analysis ofsoil that meets and exceeds EPA requirements. Demonstrated through the analysis of a group of unknown soil samples and a
CRM, they were digested using EPA 3051a and analyzed according to method 6020a requirements.

EPA 6020a defines standards for the multi-elemental determination of analytes by ICP-MS inenvironmental samples.
Results & Discussion:
The results summarized
in Figure 1 show
excellent agreement
between the measured
data for CRM2706 andthe reported extracted
levels for these elements.
A slightly higher
recovery was observedfor K and Al, possibly
due to variability in theextraction efficiency ofthis digestion method.

SOLATION® ICP-MS IN BIOMEDICAL &PHARMACEUTICAL APPLICATIONS, BLOOD &PLASMA ANALYSIS
The reliability and high-throughput capabilities of the SOLATION® ICP-MS
put it as the centerpiece of any modern bioanalytical lab.
APPLICATION STUDY:

PLASMA ANALYSIS USING THE SOLATION® ICP-MS
The SOLATION® ICP-MS is ideally suited for the elemental analysis of biological fluids including whole blood. The highsensitivity and wide dynamic range of the SOLATION® ICP-MS are particularly important for the simultaneous determinationof trace levels of heavy metals, while measuring nutritionally relevant elements at higher levels.

Precision of six replicate analyses of blood samples

Figure 1: Certified reference material recovery data.

Accuracy vs 95% confidence limit of Seronorm Blood Level 1

SAMPLE DIGESTED USING EPA 3051A,
ANALYZED ACCORDING TO EPA METHOD
6020A, EXCEED EPA REQUIREMENTS.

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11

12

SEE OUR FULL RANGE OFMASS SPECTROMETRY & FLASHCHROMATOGRAPHY SOLUTIONSAdvion Interchim Scientific provides an extensive range of innovative
instrumentation with integrated novel sample introduction techniques
and unique coupling to streamline your workflow and simplify yourtime in the lab.

13

expression
ion CMS (Compact Mass Spectrometer)®

The expressionion® family of compact mass spectrometers wasdeveloped with maximum versatility in mind. They allow users toswitch rapidly between the many different sample introduction
techniques required throughout the chemist’s workflow; from
simple direct probe analysis to ultra-high performance liquid
chromatography and prep-scale purification.
The Advion Interchim Scientific expressionion® CMS offers a wide
range of prep-free sampling techniques, including:••

Plate Express™ Automated Microextraction Reader

Plate Express™ provides a simple, automated means of obtaining
mass spectra directly from TLC plates or swipe samples. The systemion®
can be combined with the Advion Interchim Scientific’s expression®
compact mass spectrometer or SOLATION ICP-MS, creating aproprietary technique known as TLC/CMS, or TLC/ICP-MS. Using
this technique, users can quickly and confidently identify products
even in complex mixtures without additional sample preparation.
••••

Mass analysis of spots in <1 minute, avoiding systembottlenecks
Avoid the risk of overloading the mass spectrometer –microextraction spots contain the ideal amount of sample formass spectrometry
Software controlled – spectra obtained within a few mouseclicksSimplify the process of obtaining spectra – ideal for multi-user
labs

puriFlash® Flash & Preparative Chromatography Systems

The puriFlash® range offers ow to high pressure LC purificationof small & large molecules with 3X detection UV, ELSD & MS.
Combining easy-to-use features and best-in-class design, purifications
by liquid chromatography is easier, intuitive, and even moreproductive than ever before.
•
•
•
•
•
•

Routine to sophisticated RP purification of small organics,
natural products, peptides and proteins.
Avoid risk of product loss thanks to sensors, overpressure
management, and pauses.
Runs 24/7 and requires minimal service and training
Easy, multi-profile software that requires minimal training with
the InterSoft®X software for flash systems and Mass Express®
software suite for mass spectrometry
Fast and easy sample preparation with multi-mode mass specand streamlined purification workflows
Minimal bench space thanks to compact designwww.advion-interchim.com••

Plate Express Microextraction/TLC Plate Reader for push-button
analysis of TLC Plates
ASAP® direct probe for one-touch analysis of liquid and solid
samplespuriFlash® integration for mass-directed purification
HPLC and UHPLC coupling, including the Advion Interchim
Scientific AVANT™ (U)HPLC

ASAP® Atmospheric Solids Analysis Probe

The ASAP direct analysis probe provides fast, simple, reliable mass
analysis of solid and liquid samples without the need for sample
preparation. The chemist simply dips the probe in a liquid, or rubs it
on a solid sample, and inserts it through a port directly into the ion
source yielding results in seconds. Ideal for:
•
•
•
•
•
•

Reaction monitoring
Compound identification
Food safety
Forensics
Natural products
Tablets

AVANT TM HPLC & UHPLC Chromatography Systems

Advion Interchim Scientific’s range of AVANT™, high performance,liquid chromatography provides seamlessly integrated LC/CMS
and LC/ICP-MS under the full control of Advion Interchim Scientific’s
simple, intuitive Mass Express software suite.
From the simplest manual injection HPLC to a fully automated,streamlined UHPLC system and everything in-between, the AVANT™
series can be configured to fit your analytical requirements and yourbudget.
The Advion Interchim Scientific AVANT™ series offers:
•
•
•
•
•
•

HPLC and UHPLCUV and UV-Vis DAD
Column oven
Autosamplers with optional cooling
Modular and stackable design
High-pressure mixing with optional degassing

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14

SOLATION® ICP-MS PRODUCT SPECIFICATIONS

Installation Requirements

Model Options
System Model Options
Available models

HM and E

Sample Interface
Sample Introduction
Peristaltic pump

15

Installation, Facility Requirements

Environmental Requirements

Size: W X D X H (cm)

90 x 66 x 70 cm

Operating Temperature

Volume (m3)0.42Weight (Kg)

115

Argon (99.95% mL/min)24

15 to 30 °C (59 – 86 °F).
Performance specifications
require +/- 2 °C fromcalibration temperature

Cell gas (mL/min)

10 (99.999% He)

Operating Humidity

10% and 80% RH,
non-condensing

Optics4 channels
12 rollers

Cones

Cu or Ni

Spray chamber

T-controlled, Cyclonic, Quartz

Sampler cone i.d.

1mm

Spray chamber T (°C)
(optional)-10 to 10

Skimmer cone i.d.

0.4mm

Extraction cone i.d.

3mm

Nebulizer

PFA and Quartz

Lens

Einzel

Optics90° quad deflector

PlasmaTorch
Rf generator frequency (MHz)27

Rf generator power (W)500-1600

Peripheral Equipment & Sample Inlets

Mass Spectrometer
Collision Cell

Autosampler

Mass Spectrometer

Collision cell type

Octupole

Mass range (u)2-260 (212 for E)

Kinetic energy
discrimination

Yes

Resolution

0.9

No. Gases

1 (He)

Scan speed (u/s)

5000

Abundance sensitivity m-1

1.00E-07

Abundance sensitivity m+1

1.00E-07

Detector
Dwell time (µs)

100Linear dynamic range> 9 orders

Simplifying sample introduction,
increasing throughput
The ASX-560 Autosampler offers:• Optional dual rinse station• Optimal chemical compatibility• Redefined and configurable
XYZ movement• Integrated enclosure (optional)

Vials Opening

Vial Compatibility

90

13.3 mm round

8 mL round bottom or 7 mLflat bottom

60

17.0 mm square

14 mL or 15 mL

21

30.5 mm square

50 mL

Rapid Sample Introduction

Performance Specifications
Sensitivity (Kcs/ppb)

Sample Racks

More sample throughput, less time
The ASXPRESS PLUS rapid sample introduction accessory reduces time required for autosampler movement,
sample uptake, stabilization and rinse operations, thereby reducing sample run times significantly.

Other Specifications

7Li

>40

CeO/Ce (%)

<1.5

89Y

>300

Ba /Ba (%)

<3

205Ti

>100

Background cps (@ m/z
220)

<1

Sample Introduction
Step

Time
Required

Sample Introduction
Step

Time
Required

Stability, 20 min (%)<3

1. Autosampler Movement

5 sec.

20 sec.

Stability, 2 hours (%)<4

2. Sample Uptake

15 sec.

107Ag/109Ag (%)<0.5

3. Stabilization

20 sec.

1. Autosampler Movement,
Sample Uptake, Stabilization
and Rinse

4. Measurement

10 sec.

2. Measurement

10 sec.

5. Rinse

30 sec.

Total Time

30 sec.

Total Time80 sec.

Detection Limits (ppt)
9Be

<1

115In

<0.5

209Bi

<0.5

++

+

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