ᐇ㦂ሗ࿌᭩ᵝᘧ䠄୍⯡฼⏝ㄢ㢟䞉ᡂᯝබ㛤฼⏝䠅㻌䠄 䈜ᮏሗ࿌᭩䛿ⱥㄒ䛷グ㏙䛧䛶䛟䛰䛥䛔䚹䛯䛰䛧䚸⏘ᴗ฼⏝ㄢ㢟䛸䛧䛶᥇ᢥ䛥䜜䛶䛔䜛᪉䛿᪥ᮏㄒ䛷グ㏙䛧䛶䛔䛯䛰䛔䛶䜒⤖ᵓ䛷䛩䚹 䠅㻌Experimental Report㻌ᢎㄆ᪥ Date of Approval㻌 2016/06/20
ᢎㄆ⪅ Approver㻌 Jun‑ichi SUZUKIᥦฟ᪥ Date of Report㻌 2016/07/11

ㄢ㢟␒ྕ㻌 Project No.㻌 㻌 㻌 㻞㻜㻝㻡㻭㻜㻜㻟㻤㻌⿦⨨㈐௵⪅ Name of Instrument scientistᐇ㦂ㄢ㢟ྡ㻌 Title of experiment㻌㻶㼡㼚㻙㼕㼏㼔㼕㻌T㼡㼦㼡㼗㼕㻌㻱㼒㼒㼑㼏㼠㼟㻌㼛㼒㻌㻯㼍㼠㼕㼛㼚㻙㻼㼕㻌㻿㼠㼍㼏㼗㼕㼚㼓㻌㼎㼑㼠㼣㼑㼑㼚㻌㻵㼙㼕㼐㼍㼦㼛㼘㼕㼡㼙㻌㼍㼚㼐㻌㻮㼑㼚㼦㼑㼚㼑㻌 ⿦⨨ྡ Name of Instrument/䠄BL No.䠅㻌
㻾㼕㼚㼓㼟㻌 㼛㼚㻌 㻴㼑㼠㼑㼞㼛㼓㼑㼚㼑㼛㼡㼟㻌 㻿㼠㼍㼠㼑㻌 㼛㼒㻌 㻵㼙㼕㼐㼍㼦㼛㼘㼕㼡㼙㻙㼎㼍㼟㼑㼐㻌 㻵㼛㼚㼕㼏㻌 㻌 㻌 㼀㻭㻵㻷㻭㻺㻌 㻔㻮㻸㻝㻡㻕㻌㻸㼕㼝㼡㼕㼐㼟㻙㻮㼑㼚㼦㼑㼚㼑㻌㻰㼑㼞㼕㼢㼍㼠㼕㼢㼑㻌㻹㼕㼤㼠㼡㼞㼑㼟㻌ᐇ᪋᪥ Date of Experiment㻌ᐇ㦂㈐௵⪅ྡ㻌 Name of principal investigator㻌㻌 㻌 㻞㻜㻝㻢㻚㻶㼡㼚㼑㻘㻌㻝㻟㻌㻝㻜㻦㻜㻜㻌㻙㻌㻶㼡㼚㼑㻌㻝㻡㻌㻥㻦㻜㻜㻌㻌 㻌 㼀㼛㼟㼔㼕㼥㼡㼗㼕㻌㼀㼍㼗㼍㼙㼡㼗㼡㻌ᡤᒓ㻌 Affiliation㻌㻌 㻌 㻿㼍㼓㼍㻌㼁㼚㼕㼢㼑㼞㼟㼕㼠㼥㻌㻌ヨᩱ䚸ᐇ㦂᪉ἲ䚸฼⏝䛾⤖ᯝᚓ䜙䜜䛯୺䛺䝕䞊䝍䚸⪃ᐹ䚸⤖ㄽ➼䜢䚸グ㏙䛧䛶ୗ䛥䛔䚹䠄㐺ᐅ䚸ᅗ⾲ῧ௜䛾䛣䛸䠅㻌
Please report your samples, experimental method and results, discussion and conclusions. Please add figures andtables for better explanation.
㻝㻚㻌 ヨᩱ Name of sample(s) and chemical formula, or compositions including physical form.㻌
㼀㼔㼑㻌 㼜㼞㼑㼟㼑㼚㼠㻌 㼟㼍㼙㼜㼘㼑㼟㻌 㼣㼑㼞㼑㻌 㼎㼕㼚㼍㼞㼥㻌 㼙㼕㼤㼠㼡㼞㼑㼟㻌 㼛㼒㻌 㼕㼙㼕㼐㼍㼦㼛㼘㼕㼡㼙㻙㼎㼍㼟㼑㼐㻌 㼕㼛㼚㼕㼏㻌 㼘㼕㼝㼡㼕㼐㼟㻌 㻯㼚㼙㼕㼙㼀㻲㻿㻭㻌 㻔㼚㻌 㻦㻌 㼍㼘㼗㼥㼘㻌 㼏㼔㼍㼕㼚㻌㼘㼑㼚㼓㼠㼔㻕㻌㼍㼚㼐㻌㼐㼑㼡㼠㼑㼞㼍㼠㼑㼐㻌㼐㼕㼙㼑㼠㼔㼥㼘㻌㼟㼡㼘㼒㼛㼤㼕㼐㼑㻌㻔㻰㻹㻿㻻㻙㼐㻢㻕㻌㼣㼕㼠㼔㻌㼢㼍㼞㼕㼛㼡㼟㻌㻰㻹㻿㻻㻌㼙㼛㼘㼑㻌㼒㼞㼍㼏㼠㼕㼛㼚㼟㻌㼤㻰㻹㻿㻻㻚㻌㻝㻚㻌㻯㻞㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㻌 㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㻜㻚㻥㻌 㻌㻞㻚㻌㻯㻠㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㻌 㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㻜㻚㻥㻌㻟㻚㻌㻯㻢㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㻌 㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㻜㻚㻥㻌㻠㻚㻌㻯㻤㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㻌 㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㻜㻚㻥㻌㻡㻚㻌㻯㻝㻜㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㻌 㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㻜㻚㻥㻌㻢㻚㻌㻯㻝㻞㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㻌 㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㻜㻚㻥㻌㻌㻞㻚㻌 ᐇ㦂᪉ἲཬ䜃⤖ᯝ㻌 䠄ᐇ㦂䛜䛖䜎䛟䛔䛛䛺䛛䛳䛯ሙྜ䚸䛭䛾⌮⏤䜢グ㏙䛧䛶䛟䛰䛥䛔䚹䠅㻌
Experimental method and results.

If you failed to conduct experiment as planned, please describe reasons.

㻌 㼀㼔㼑㻌 㼟㼙㼍㼘㼘㻙㼍㼚㼓㼑㼘㻌 㼚㼑㼡㼠㼞㼛㼚㻌 㼟㼏㼍㼠㼠㼑㼞㼕㼚㼓㻌 㻔㻿㻭㻺㻿㻕㻌 㼟㼜㼑㼏㼠㼞㼍㻌 㼒㼛㼞㻌 㼠㼔㼑㻌 㻝㻞㻌 㼟㼍㼙㼜㼘㼑㼟㻌 㼛㼒㻌 㻯㼚㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌 㼣㼑㼞㼑㻌㼙㼑㼍㼟㼡㼞㼑㼐㻌 㼍㼠㻌 㼍㻌 㼞㼛㼛㼙㻌 㼠㼑㼙㼜㼑㼞㼍㼠㼡㼞㼑㻌 㼡㼟㼕㼚㼓㻌 㼀㻭㻵㻷㻭㻺㻌 㼟㼜㼑㼏㼠㼞㼛㼙㼑㼠㼑㼞㻌 㼠㼛㻌 㼑㼘㼡㼏㼕㼐㼍㼠㼑㻌 㼠㼔㼑㻌 㼙㼕㼏㼞㼛㼕㼚㼔㼛㼙㼛㼓㼑㼚㼑㼕㼠㼥㻌 㼛㼒㻌 㼠㼔㼑㻌㼕㼛㼚㼕㼏㻌㼘㼕㼝㼡㼕㼐㻙㻰㻹㻿㻻㻌㼙㼕㼤㼠㼡㼞㼑㼟㻚㻌㻴㼛㼣㼑㼢㼑㼞㻘㻌㼍㼘㼘㻌㼛㼒㻌㼠㼔㼑㻌㼟㼍㼙㼜㼘㼑㼟㻌㼐㼕㼐㻌㼚㼛㼠㻌㼓㼕㼢㼑㻌㼟㼕㼓㼚㼕㼒㼕㼏㼍㼚㼠㻌㻿㻭㻺㻿㻌㼕㼚㼠㼑㼚㼟㼕㼠㼕㼑㼟㻚㻌㼀㼔㼑㻌㼜㼞㼑㼟㼑㼚㼠㻌㼞㼑㼟㼡㼘㼠㼟㻌 㼟㼡㼓㼓㼑㼟㼠㼑㼐㻌 㼠㼔㼍㼠㻌 㻯㼚㼙㼕㼙㼀㻲㻿㻭㻌 㼍㼚㼐㻌 㻰㻹㻿㻻㻌 㼍㼞㼑㻌 㼔㼛㼙㼛㼓㼑㼚㼑㼛㼡㼟㼘㼥㻌 㼙㼕㼤㼑㼐㻌 㼣㼕㼠㼔㻌 㼑㼍㼏㼔㻌 㼛㼠㼔㼑㼞㻌 㼑㼢㼑㼚㻌 㼛㼚㻌 㼠㼔㼑㻌㼙㼛㼘㼑㼏㼡㼘㼍㼞㻌㼟㼏㼍㼘㼑㻚㻌㼀㼔㼕㼟㻌㼟㼑㼑㼙㼟㻌㼠㼛㻌㼎㼑㻌㼡㼚㼕㼚㼠㼑㼞㼑㼟㼠㼕㼚㼓㻌㼕㼚㼒㼛㼞㼙㼍㼠㼕㼛㼚㻌㼕㼚㻌㼠㼔㼑㻌㼒㼕㼑㼘㼐㻌㼛㼒㻌㻿㻭㻺㻿㻌㼑㼤㼜㼑㼞㼕㼙㼑㼚㼠㼟㻚㻌㻺㼑㼢㼑㼞㼠㼔㼑㼘㼑㼟㼟㻘㻌㼣㼑㻌㼏㼛㼡㼘㼐㻌㼏㼛㼚㼒㼕㼞㼙㻌㼠㼔㼑㻌㼜㼞㼑㼢㼕㼛㼡㼟㻌㼞㼑㼟㼡㼘㼠㼟㻌㼒㼞㼛㼙㻌㼠㼔㼑㻌㻺㻹㻾㻌㼍㼚㼐㻌㻵㻾㻌㼙㼑㼍㼟㼡㼞㼑㼙㼑㼚㼠㼟㻌㼎㼥㻌㼠㼔㼑㻌㼜㼞㼑㼟㼑㼚㼠㻌㻿㻭㻺㻿㻌㼞㼑㼟㼡㼘㼠㼟㻧㻌㼕㻚㼑㻚㻘㻌㻰㻹㻿㻻㻌 㼙㼛㼘㼑㼏㼡㼘㼑㼟㻌 㼣㼕㼠㼔㻌 㼠㼔㼑㻌 㼔㼕㼓㼔㻌 㼑㼘㼑㼏㼠㼞㼛㼚㻌 㼐㼛㼚㼕㼏㼕㼠㼥㻌 㼍㼞㼑㻌 㼔㼥㼐㼞㼛㼓㼑㼚㻙㼎㼛㼚㼐㼑㼐㻌 㼣㼕㼠㼔㻌 㼠㼔㼑㻌 㼠㼔㼞㼑㼑㻌 㼕㼙㼕㼐㼍㼦㼛㼘㼕㼡㼙㻌 㼞㼕㼚㼓㻌㼔㼥㼐㼞㼛㼓㼑㼚㻌㼍㼠㼛㼙㼟㻌㼍㼠㻌㼠㼔㼑㻌㼜㼛㼟㼕㼠㼕㼛㼚㼟㻌㼛㼒㻌㻞㻘㻌㻠㻘㻌㼍㼚㼐㻌㻡㻌㼍㼟㻌㼟㼔㼛㼣㼚㻌㼕㼚㻌㻲㼕㼓㻚㻌㻝㻚㻌㼀㼔㼑㻌㼔㼥㼐㼞㼛㼓㼑㼚㻌㼎㼛㼚㼐㼕㼚㼓㻌㼛㼒㻌㼠㼔㼑㻌㼕㼙㼕㼐㼍㼦㼛㼘㼕㼡㼙㻌㼞㼕㼚㼓㻌㼔㼥㼐㼞㼛㼓㼑㼚㻌㼍㼠㼛㼙㼟㻌㼣㼕㼠㼔㻌㻰㻹㻿㻻㻌㼞㼑㼟㼡㼘㼠㼟㻌㼕㼚㻌㼠㼔㼑㻌㼔㼛㼙㼛㼓㼑㼚㼑㼛㼡㼟㻌㼙㼕㼤㼕㼚㼓㻌㼛㼒㻌㼎㼛㼠㼔㻌㼘㼕㼝㼡㼕㼐㼟㻚㻌 㻌㻌 㻭㼟㻌 㼟㼔㼛㼣㼚㻌 㼕㼚㻌 㻲㼕㼓㻚㻌 㻞㻘㻌 㼕㼚㻌 㼠㼔㼑㻌 㼙㼕㼐㼐㼘㼑㻌 㻽㻙㼞㼍㼚㼓㼑㻘㻌 㼍㻌 㼜㼑㼍㼗㻌 㼍㼠㻌 a㻜㻚㻞㻌 㽐㻙㻝㻌 㼍㼜㼜㼑㼍㼞㼟㻌 㼕㼚㻌 㼠㼔㼑㻌 㻿㻭㻺㻿㻌 㼟㼜㼑㼏㼠㼞㼍㻌 㼒㼛㼞㻌㻯㼚㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌㼙㼕㼤㼠㼡㼞㼑㼟㻌㼣㼕㼠㼔㻌㼠㼔㼑㻌㼍㼘㼗㼥㼘㻌㼏㼔㼍㼕㼚㻌㼘㼑㼚㼓㼠㼔㻌㼛㼒㻌㼙㼛㼞㼑㻌㼠㼔㼍㼚㻌㻝㻜㻚㻌㼀㼔㼕㼟㻌㼜㼑㼍㼗㻌㼙㼍㼥㻌㼓㼕㼢㼑㻌㼡㼟㻌㼠㼔㼑㻚㻌㻞㻚㻌 ᐇ㦂᪉ἲཬ䜃⤖ᯝ䠄䛴䛵䛝䠅㻌 Experimental method and results (continued)㼕㼚㼒㼛㼞㼙㼍㼠㼕㼛㼚㻌㼛㼚㻌㼠㼔㼑㻌㼘㼕㼝㼡㼕㼐㻌㼟㼠㼞㼡㼏㼠㼡㼞㼑㻌㼛㼒㻌㼕㼛㼚㼕㼏㻌㼘㼕㼝㼡㼕㼐㼟㻌㼍㼚㼐㻌㼠㼔㼑㻌㼏㼔㼍㼚㼓㼑㻌㼕㼚㻌㼠㼔㼑㻌㼟㼠㼞㼡㼏㼠㼡㼞㼑㻌㼛㼒㻌㼠㼔㼑㻌㼕㼛㼚㼕㼏㻌㼘㼕㼝㼡㼕㼐㼟㻌㼣㼕㼠㼔㻌㼕㼚㼏㼞㼑㼍㼟㼕㼚㼓㻌 㻰㻹㻿㻻㻌 㼏㼛㼚㼠㼑㼚㼠㻚㻌 㼃㼑㻌 㼣㼕㼘㼘㻌 㼍㼚㼍㼘㼥㼦㼑㻌 㼠㼔㼑㻌 㼜㼑㼍㼗㻌 㼎㼥㻌 㼟㼛㼙㼑㻌 㼒㼡㼚㼏㼠㼕㼛㼚㻌 㼠㼛㻌 㼏㼘㼍㼞㼕㼒㼥㻌 㼠㼔㼑㻌 㼟㼠㼞㼡㼏㼠㼡㼞㼑㻌 㼛㼒㻌 㼠㼔㼑㻌 㼕㼛㼚㼕㼏㻌㼘㼕㼝㼡㼕㼐㼟㻚㻌 㻌
㻌

2
HH3C
6N

F
N

CnH2n+1FCF

H
4

H
5C

NSOFFFSO OO㻌㻲㼕㼓㻚㻌㻝㻌㻿㼠㼞㼡㼏㼠㼡㼞㼑㻌㼛㼒㻌㼕㼙㼕㼐㼍㼦㼛㼘㼕㼡㼙㻙㼎㼍㼟㼑㼐㻌㼕㼛㼚㼕㼏㻌㼘㼕㼝㼡㼕㼐㻌㻯㼚㼙㼕㼙㼀㻲㻿㻭㻚㻌㻌

100

I(Q)/cm-1xDMSO = 0.5

10-1 -2
100.9

10-1
Q/Å-1100㻌㻲㼕㼓㻘㻌㻞㻌㻿㻭㻺㻿㻌㼟㼜㼑㼏㼠㼞㼍㻌㼒㼛㼞㻌㻯㻝㻞㼙㼕㼙㼀㻲㻿㻭㻙㻰㻹㻿㻻㻙㼐㻢㻌㼙㼕㼤㼠㼡㼞㼑㼟㻌㼍㼟㻌㼍㻌㼒㼡㼚㼏㼠㼕㼛㼚㻌㼛㼒㻌㼍㼠㻌㼤㻰㻹㻿㻻㻌㻩㻌㻜㻚㻡㻘㻌㻜㻚㻣㻘㻌㻜㻚㻤㻘㻌㼍㼚㼐㻌㻜㻚㻥㻚㻌