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No

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Extraction*Solvent, LLE, SPE/SPME, Soxhlet, PSE/ASE

SPE

Extraction_details*Q;4

Solvent, Cartridge, Gel, Shaking, Homogenization, Sonication, etc.

Cartridge

Cleanup

ZgkjT^b*LLE, Deproteination, Alkali saponific, Filteration/ultrafiltration,
Chromatography

Filtration

Cleanup_details

ZgkjT^b*Q;4Solvent, Acid, Alkali, Filter, Cartridge, Gel, etc.

FilterDerivatization==96l/JPHRNone

None

Chromatography

Zic_[f`Uk

GC, LC, IC, TLC, Other, or NoneLC

Detector'HRMS, Q-MS, MS-MS, IT-MS, Tof-MS, Tof/tof, Q-tof, FID, ECD, or Other

MS-MS

Ionization

VXj

EI, NCI, PCI, FI, ESI, APCI, APPI, MALDI, or Other

ESI

Standard(+962

Diclofenac sodium

Recovery_correction.7).7)Q%,Yes or No

Yes

Calibration

Ydgahk\ej

1. External calibration, 2. Internal calibration (isotope dilution method),
3. Matrix-matched external calibration, 4. Standard additions

2LOD/MDL'E!

0.65 ng/L

LOQ/MQLCE!

Intra-day precision#!

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Recovery_CRM(+9"Q<8OQ

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0.83%

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80 ± 6.8%

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logPow 1)4.50

対水溶解度1)

23 mg/L @24℃

加水分解性1)

加水分解なし（pH=3,6,9 @25℃）

土壌中半減期1)

好気的分解：42-70日

土壌吸着性1)

Koc（土壌吸着係数）=708

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