KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

1 of 7

THC Free Non Crystalized Distillate
Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/10/2022
Completed: 02/24/2022

Summary

Test
Cannabinoids
Cannabinoids (Additional)
Foreign Matter
Heavy Metals
Microbials
Mycotoxins
Pesticides
Residual Solvents

Date Tested
02/22/2022
02/22/2022
02/10/2022
02/14/2022
02/16/2022
02/24/2022
02/24/2022
02/17/2022

StatusTestedTestedTestedTestedTestedTestedTestedTestedCannabinoids by HPLC-PDA, LC-MS/MS, and/or GC-MS/MS
ND

47.6 %

58.0 %

Not Tested

Not Detected

Yes

Total Δ9-THC

CBD

Total Cannabinoids

Moisture Content

Foreign Matter

Internal Standard
Normalization

LOD
(%)
0.01
0.01
0.01
0.008
0.004
0.006
0.002
0.006
0.005
0.01
0.01
0.006
0.006
0.01
0.01
0.01
0.006
0.006
ND

LOQ
Result(%)(%)
0.02842.20
0.0543ND
0.018
ND
0.0242
47.6
0.013
ND
0.01820.875
0.0063ND
0.01723.09
0.0147ND
0.03350.704
0.0371ND
0.01693.54
0.0181ND
0.0312ND
0.0227ND
0.0251ND
0.0206ND
ND
0.0186ND
47.6
476
58.0580

M

Analyte

CBC
CBCA
CBCV
CBD
CBDA
CBDV
CBDVA
CBG
CBGA
CBL
CBLA
CBN
CBNA
Δ8-THC
Δ9-THC
Δ9-THCA
Δ9-THCV
Δ9-THCVA
Total Δ9-THC
Total CBD
Total

Result(mg/g)
22.0
ND
ND
476
ND
8.75
ND
30.9
ND7.04
ND
35.4
ND
ND
ND
ND
ND
ND

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; RL = Reporting Limit; Δ = Delta; Total Δ9-THC = Δ9-THCA * 0.877 + Δ9-THC; Total CBD = CBDA * 0.877 + CBD;

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Scott Caudill
Senior Scientist
Date: 02/22/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

2 of 7

THC Free Non Crystalized Distillate
ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USA

Received: 02/10/2022
Completed: 02/24/2022

ig
CB otoD

Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

Cannabinoids by HPLC-PDA, LC-MS/MS, and/or GC-MS/MS
AnalyteCBECBTTotal Additional Cannabinoids
TotalLOD(%)
0.00950.0181

LOQ(%)
0.02840.0543Result(%)
3.65
9.26
12.9
70.9

Result(mg/g)
36.5
92.6
129709M

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; RL = Reporting Limit; Δ = Delta; Total Δ9-THC = Δ9-THCA * 0.877 + Δ9-THC; Total CBD = CBDA * 0.877 + CBD;

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Scott Caudill
Senior Scientist
Date: 02/22/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

Certiﬁcate of Analysis
3 of 7

THC Free Non Crystalized Distillate
Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/10/2022
Completed: 02/24/2022Heavy Metals by ICP-MS
AnalyteArsenicCadmium
LeadMercury

LOD (ppb)
21212LOQ (ppb)20202050

Result (ppb)
ND
ND
NDND

M

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Nicholas Howard
Scientist
Date: 02/14/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

4 of 7

THC Free Non Crystalized Distillate
Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/10/2022
Completed: 02/24/2022

Pesticides by LC-MS/MS and GC-MS/MSAnalyteM

Abamectin
Acephate
AcetamipridAldicarb
Azoxystrobin
Boscalid
Carbaryl
Carbofuran
Chloranthraniliprole
Chlorfenapyr
Chlorpyrifos
Coumaphos
Daminozide
DiazinonDichlorvos
Dimethoate
Dimethomorph
Ethoprophos
Etofenprox
Etoxazole
Fenhexamid
Fenoxycarb
Fenpyroximate
FipronilFlonicamid
Fludioxonil

LOD
(ppb)
3030
3030
30
30
303030303030303030303030
3030
30
30
30
30
30
30

LOQ
(ppb)
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

Result
(ppb)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

AnalyteHexythiazox
Imazalil
Imidacloprid
Kresoxim methyl
Malathion
Metalaxyl
Methiocarb
Methomyl
Mevinphos
Myclobutanil
Naled
Oxamyl
Paclobutrazol
Piperonyl Butoxide
Prallethrin
Propiconazole
Propoxur
Pyridaben
Spinetoram
Spinosad
Spiromesifen
Spirotetramat
Spiroxamine
Tebuconazole
Thiacloprid
Thiamethoxam
Triﬂoxystrobin

LOD
(ppb)
303030303030303030303030303030303030303030303030303030

LOQ(ppb)
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100100100100100100100100100100

Result(ppb)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Jared Burkhart
Technical Manager
Date: 02/24/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

5 of 7

THC Free Non Crystalized Distillate
Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/10/2022
Completed: 02/24/2022

Mycotoxins by LC-MS/MSAnalyte
B1
B2
G1
G2Ochratoxin A

LOD (ppb)11111

LOQ (ppb)
55555Result (ppb)
ND
ND
NDNDNDM

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Jared Burkhart
Technical Manager
Date: 02/24/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

6 of 7

THC Free Non Crystalized Distillate
Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/10/2022
Completed: 02/24/2022

Microbials by PCR and Plating
AnalyteColiforms
Aerobic Bacteria
Salmonella
Total Enterobacteriaceae

LOD (CFU/g)
11Result (CFU/g)NDND

Result (Qualitative)

Not Detected per 1 gram
Not Detected per 1 gram

M

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; CFU = Colony Forming Units; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Alex Morris
Quality Assurance Manager
Date: 02/16/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

7 of 7

THC Free Non Crystalized Distillate
Sample ID: SA-220207-7089
Batch: CR-20211019-0211
Type: Finished Products
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/10/2022
Completed: 02/24/2022

Residual Solvents by HS-GC-MS/MS
AnalyteM

AcetoneAcetonitrile
BenzeneButane1-Butanol
2-Butanol
2-ButanoneChloroform
Cyclohexane
1,2-Dichloroethane
1,2-Dimethoxyethane
Dimethyl Sulfoxide
N,N-Dimethylacetamide
2,2-Dimethylbutane
2,3-Dimethylbutane
N,N-Dimethylformamide
2,2-Dimethylpropane
1,4-Dioxane
Ethanol
2-Ethoxyethanol
Ethyl Acetate
Ethyl Ether
Ethylbenzene

LOD
(ppm)
167
140.5167
167
167
167
21290.54167
37101030167
13167
6167
167
3LOQ
(ppm)
500
41
1500
500
500
500
6388
110500
109
2929
88500
38500
16500
500
7Result
(ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDND
ND
ND
ND
ND
ND
ND
ND

AnalyteEthylene Glycol
Ethylene Oxide
Heptanen-Hexane
Isobutane
Isopropyl Acetate
Isopropyl Alcohol
Isopropylbenzene
Methanol
2-Methylbutane
Methylene Chloride
2-Methylpentane
3-Methylpentane
n-Pentane
1-Pentanol
n-Propane
1-Propanol
Pyridine
Tetrahydrofuran
TolueneTrichloroethylene
Tetramethylene Sulfone
Xylenes (o-, m-, and p-)

LOD
(ppm)
21
0.5
167
10167
167
167
167
100
1020
1010167
167
167
167
72430
3673

LOQ(ppm)
62
1500
29500
500500500300
29602929500
500
500
500
207289816217

Result(ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 02/24/2022

Tested By: Scott Caudill
Senior Scientist
Date: 02/17/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.