KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

1 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Summary

Test
Cannabinoids
Foreign Matter
Heavy Metals
Microbials
Mycotoxins
Pesticides
Residual Solvents

Date Tested
03/09/2022
02/14/2022
02/14/2022
02/16/2022
02/24/2022
02/24/2022
02/25/2022

StatusTestedTestedTestedTestedTestedTestedTestedND

88.7 %

96.4 %

Not Tested

Not Detected

Yes

Total Δ9-THC

CBD

Total Cannabinoids

Moisture Content

Foreign Matter

Internal Standard
Normalization

Cannabinoids by HPLC-PDA, LC-MS/MS, and/or GC-MS/MS
LOD
(%)

LOQ
(%)

Result(%)

Result(mg/g)

CBC
CBCA
CBCV
CBD
CBDA
CBDV
CBDVA
CBE
CBG
CBGA
CBL
CBLA
CBN
CBNA
CBT
Δ8-THC
Δ9-THC
Δ9-THCA
Δ9-THCV
Δ9-THCVA

0.00950.0181
0.006
0.00810.00430.00610.0021
0.00950.00570.00490.01120.01240.00560.006
0.01810.01040.00760.00840.00690.00620.02840.05430.018
0.02420.013
0.01820.00630.02840.01720.01470.03350.03710.01690.0181
0.05430.03120.02270.02510.02060.0186

0.240
ND
ND
88.7
ND
1.31
ND
3.17
0.599
ND
ND
ND
1.13
ND
1.22
ND
ND
ND
ND
ND

2.40
ND
ND
887
ND
13.1
ND
31.7
5.99
ND
ND
ND
11.3
ND
12.2
ND
NDNDND
NDM

AnalyteTotal Δ9-THC
Total CBDTotal

ND
88.796.4

ND887964

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; RL = Reporting Limit; Δ = Delta; Total Δ9-THC = Δ9-THCA * 0.877 + Δ9-THC; Total CBD = CBDA * 0.877 + CBD;

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022

Tested By: Scott Caudill
Senior Scientist
Date: 03/09/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

2 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Heavy Metals by ICP-MS
AnalyteArsenic
Cadmium
LeadMercuryLOD (ppb)21212LOQ (ppb)20202050Result (ppb)
ND
NDNDNDM

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022

Tested By: Nicholas Howard
Scientist
Date: 02/14/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCALaboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza DriveNicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

3 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Pesticides by LC-MS/MS and GC-MS/MS
AnalyteM

Abamectin
Acephate
Acetamiprid
Aldicarb
Azoxystrobin
Boscalid
Carbaryl
Carbofuran
Chloranthraniliprole
ChlorfenapyrChlorpyrifos
Coumaphos
Daminozide
DiazinonDichlorvos
Dimethoate
Dimethomorph
Ethoprophos
Etofenprox
Etoxazole
Fenhexamid
Fenoxycarb
Fenpyroximate
FipronilFlonicamid
Fludioxonil

LOD
(ppb)
3030303030303030303030303030303030303030303030303030

LOQ
(ppb)
100100100
100
100100100100100100
100
100100
100
100
100
100
100
100
100
100
100
100
100
100
100

Result
(ppb)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

AnalyteHexythiazox
Imazalil
Imidacloprid
Kresoxim methyl
Malathion
Metalaxyl
Methiocarb
Methomyl
Mevinphos
Myclobutanil
Oxamyl
Paclobutrazol
Piperonyl Butoxide
Prallethrin
Propiconazole
Propoxur
Pyridaben
Spinetoram
Spinosad
Spiromesifen
Spirotetramat
Spiroxamine
Tebuconazole
Thiacloprid
Thiamethoxam
Triﬂoxystrobin

LOD(ppb)
3030303030303030303030303030303030
30
3030
30
30
30
30
3030

LOQ
(ppb)
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100

Result(ppb)
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022

Tested By: Jared Burkhart
Technical Manager
Date: 02/24/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCALaboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza DriveNicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

4 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Mycotoxins by LC-MS/MS
Analyte
B1
B2
G1
G2
Ochratoxin A

LOD (ppb)11111

LOQ (ppb)
55555Result (ppb)
ND
ND
ND
NDNDM

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022

Tested By: Jared Burkhart
Technical Manager
Date: 02/24/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

5 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Microbials by PCR and Plating
AnalyteColiforms
Aerobic Bacteria
Salmonella
Total Enterobacteriaceae

LOD (CFU/g)
11

Result (CFU/g)
ND
ND

Result (Qualitative)

Not Detected per 1 gram
Not Detected per 1 gram

M

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; CFU = Colony Forming Units; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022

Tested By: Alex Morris
Quality Assurance Manager
Date: 02/16/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABS
https://kcalabs.com
KDA Lic.# P_0058

6 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Residual Solvents by HS-GC-MS/MS
AnalyteM

AcetoneAcetonitrile
BenzeneButane1-Butanol
2-Butanol
2-Butanone
Chloroform
Cyclohexane
1,2-Dichloroethane
1,2-Dimethoxyethane
Dimethyl Sulfoxide
N,N-Dimethylacetamide
2,2-Dimethylbutane
2,3-Dimethylbutane
N,N-Dimethylformamide
2,2-Dimethylpropane
1,4-Dioxane
Ethanol
2-Ethoxyethanol
Ethyl Acetate
Ethyl Ether
Ethylbenzene

LOD
(ppm)
167
140.5167
167
167
167
21290.54167
37101030167
13167
6167
167
3LOQ(ppm)
500
41
1500
500
500
500
6388
110500109292988500
38500
16500
500
7Result(ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND

AnalyteEthylene Glycol
Ethylene Oxide
Heptanen-Hexane
Isobutane
Isopropyl Acetate
Isopropyl Alcohol
Isopropylbenzene
Methanol
2-Methylbutane
Methylene Chloride
2-Methylpentane
3-Methylpentane
n-Pentane
1-Pentanol
n-Propane
1-Propanol
Pyridine
Tetrahydrofuran
TolueneTrichloroethylene
Tetramethylene Sulfone
Xylenes (o-, m-, and p-)

LOD
(ppm)
21
0.5
167
10167
167
167
167
100
1020
1010167
167
167
167
72430
3673

LOQ(ppm)
62
1500
29500
500
500
5003002960
2929500
500
500
500
2072
89
816217

Result
(ppm)
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDNDND

ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022

Tested By: Scott Caudill
Senior Scientist
Date: 02/25/2022

This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA
Laboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.

KCA Laboratories
232 North Plaza Drive
Nicholasville, KY 40356

Certiﬁcate of Analysis+1-833-KCA-LABShttps://kcalabs.com
KDA Lic.# P_0058

7 of 7

THC Free CBD Distillate
Sample ID: SA-220207-7060
Batch: T00PER7612
Type: In-Process Materials
Matrix: Concentrate - Distillate

ClientRising Sun Exports
2777 Yulupa Ave #142
Santa Rosa, CA 95405
USAig
CB otoD

Received: 02/07/2022
Completed: 03/09/2022

Reporting Limit Appendix

Pesticides - CA DCC
AnalyteHeavy Metals - Colorado CDPHE
AnalyteArsenic

Cadmium

Limit (ppb) Analyte
1500
500

LeadMercury

Limit (ppb)
500
1500

Imidacloprid

3000

Aldicarb

3040000

Kresoxim methyl

1000
5000

10000
5003040000

Metalaxyl

Azoxystrobin
Boscalid
Carbaryl

Chlorfenapyr
Chlorpyrifos

AnalyteColiforms

Limit (CFU/Analyteg)
100

Aerobic Bacteria

Limit (CFU/g)

Coumaphos

10000

DiazinonDaminozide
Dichlorvos

Dimethoate

Residual Solvents - USP 467

Dimethomorph
Ethoprophos

AnalyteLimit (ppm) Analyte

Limit (ppm)

Etofenprox

620
15000

Etoxazole

Fenpyroximate

Isopropyl Acetate

290
5000
5000

5000

Isopropyl Alcohol

5000

Fludioxonil

Chloroform
Cyclohexane

60
3880

Isopropylbenzene
Methanol

5000
3000

1,2-Dichloroethane

5100

2-Methylbutane

Methylene Chloride

290
600

5000
10902902908805000
3805000
1605000
5000
70

2-Methylpentane

290

Analyte3-Methylpentane

290
5000
5000
5000
5000
200
720
890
801602170

B1

Ethylene Glycol

2-Butanol

5000
410
25000
5000
5000

2-Butanone

AcetoneAcetonitrile
BenzeneM

Butane1-Butanol

1,2-Dimethoxyethane
Dimethyl Sulfoxide

N,N-Dimethylacetamide
2,2-Dimethylbutane

N,N-Dimethylformamide
2,2-Dimethylpropane
1,4-Dioxane
Ethanol

2-Ethoxyethanol
Ethyl Acetate
Ethyl Ether

Ethylbenzene

Ethylene Oxide
Heptanen-Hexane

Isobutanen-Pentane
1-Pentanol

n-Propane
1-Propanol
Pyridine

Tetrahydrofuran
TolueneTrichloroethylene

Tetramethylene Sulfone
Xylenes (o-, m-, and p-)

Limit (ppb)

5000

Carbofuran
Chloranthraniliprole

Microbials - Colorado CDPHE

Limit (ppb) Analyte

Acetamiprid

Fenhexamid
Fenoxycarb
FipronilFlonicamid

Malathion

Methiocarb
Methomyl
Mevinphos

3030Myclobutanil

30
30

Paclobutrazol

200
30
30

Prallethrin

20000
30

Pyridaben

30
1500

Spinosad

10000
30
2000
30
2000
30000

Spirotetramat

OxamylPiperonyl Butoxide
Propiconazole
Propoxur

Spinetoram

Spiromesifen
Spiroxamine

Tebuconazole
Thiacloprid

Thiamethoxam
Triﬂoxystrobin

15000
30
100
30
9000
200
30
8000
400
20000303000
3000
3000
12000
13000
30
2000
30450030000

Mycotoxins - Colorado CDPHEG1Ochratoxin A

Limit (ppm) Analyte
555

B2G2Limit (ppm)
55Pesticides - CA DCC
AnalyteAbamectin
Acephate

Limit (ppb) Analyte
300
5000

Hexythiazox
Imazalil

Limit (ppb)
2000
30

Generated By: Ryan Bellone
Commercial Director
Date: 03/09/2022
This product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substancetested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCALaboratories makes no claims as to the efﬁcacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certiﬁcate of Analysis shall not be reproduced
except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.